14
) UN I TEO STATES ENV I AONMENTAL PROTECT I ON AGENCY REGION I Environmental Services Div isi on 60 We stview Street, le xi ngton, 1'1A 02173 -3 185 MEP10RAN0UI'1 DATE : August 15, 1990 r SUBJ: Char 1es George Landf i 11 Site - F 1 i "7 FROM: Oenn 1 s ses Va 1d8s , -, '!xi!JY-rft' Se '\. \ . Env1ronmental Stud1es TO: Oav'id Dickerson, RPM MA Superfund Sect1on ESD personnel collected water sample s from Flint Pond in Ty ng sboro MA on June 16, 1990 . The res ult s for the vol at i l e organic and semi-volatile organic analyses is attac hed . The CL P numbers corres pon d to the following locations: Station CLP Number Location Number TA I POl AT528 Trip blank SW01 AT529 Marsh .,. •• b y F I int Pond near route 3. SW0 2 AT530 Marsh area by flint pond. SW03 AT531 F 1 int Pond If you need additional i nformat ion on the s tat ion locations, please contact myself or Dan Granz. If you have any que stions, please contact me at 860-4378 .

MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

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Page 1: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

) UN I TEO STATES ENV I AONMENTAL PROTECT I ON AGENCY REGION I

Environmental Services Div isi on 60 Westview Street lexi ngton 11A 02173 -3 185

MEP10RAN0UI1 DATE August 15 1990

r SUBJ Char 1es George Landf i 11 Site - F 1 i 7 ~o~d

FROM Oenn 1 s ses Va 1d8s - xiJY-rftSe Env1ronmental Stud1es ~ 1-

TO Oavid Dickerson RPM MA Superfund Sect1on

ESD personnel collected water samples from Flint Pond in Tyngsboro MA on June 16 1990 The result s for the vol at i l e organic and semi-volatile organic analyses is attac hed The CL P numbers corres pond to the following locations

Station CLP Number Location Number

TA IPOl AT528 Trip blank

SW01 AT529 Marsh bullbull b y F I int Pond near route 3

SW0 2 AT530 Marsh area by flint pond

SW03 AT531 F 1 int Pond

If you need additional i nformat ion on the s tat ion locations please contact myself or Dan Granz

If you have any questions please contact me at 860-4378

CH

AR

LE

S

GE

OR

GE

L

AN

D

RE

CL

AM

AT

ION

T

RU

ST

L

AN

DF

ILL

A

DM

INIS

TR

AT

I VE

R

EC

OR

D

r 1

(-~~

~

1-

I -

L 1

~

H i J

r~_J j

~

I ~ -

L-~bull s

-1

(

h y~ l

II

-~

1 JV ~ ~-middot-

lt ~-

shy

~

) poundSAT PROJECT LANDMARK ONE ONE VAN DE GRMFF DRIVE BURLINGTON MA 01amp03

- (617)22$-2050 bull FAX (6m229()046

July 24 1990 Revised August 10 1990

H-0-7 -24

Mr Dennis Gagne Regional Sampl e Control Custodian U S Environmental Protection Agency 90 Can a l Street Boston Massachusetts 02114

Re TID No 01-9007-10 Case No 14355 SOG No AT 528 Southwest Research Institut e Charles George Site Tyngsboro Ma Volatile 4 Aqueous AT528 throuqh AT531 Semivolatile 3AqueousfAT529 through AT531

Dear Mr Gagne

A validation was performed on the organic analytical data for 4 water samples collected by the Environaental Studies Secti on of USEPA at the Charles George site Four samplea were analyzed for volatiles and three samples were analyzed for semivolatiles The sabullplea were analyze-1 according to the 288 statement of Work (SOW) one trip blank and one set of matrix spikejaatrix spike duplicates were abullong the 4 samples There were no field blanks or field duplicates The data were evaluated based on the following parameters

bull data completeness bull holding times bull GCHS tuning bull calibration bull blanks bull surrogate recoveries bull bullatrix spikejmatrix s pike duplicates

field duplicate r esults internal standard performance

bull compound identification bull compo und quantitation

- All criteria were met for this parameter Table I summari zes the validation r ecommendations which were based o n the following information

)

Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990

H-0 - 7 - 2 4

Calibratiopbull

IC CC ~~

llroa011ethane X

chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X

Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO

The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples

Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults

xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects

RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s

Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990

H-0-7-24

Semiyolatile cc ~

bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X

Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD

No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea

x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results

Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects

RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects

bullbull

)

Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990

H-0-7-2 4

aurroqatt Rtcoyeriet

Semiyolatile

The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below

Ill A

mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5

QC Liaita JS 10 21 to to to to 114 116 100

The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 2: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

CH

AR

LE

S

GE

OR

GE

L

AN

D

RE

CL

AM

AT

ION

T

RU

ST

L

AN

DF

ILL

A

DM

INIS

TR

AT

I VE

R

EC

OR

D

r 1

(-~~

~

1-

I -

L 1

~

H i J

r~_J j

~

I ~ -

L-~bull s

-1

(

h y~ l

II

-~

1 JV ~ ~-middot-

lt ~-

shy

~

) poundSAT PROJECT LANDMARK ONE ONE VAN DE GRMFF DRIVE BURLINGTON MA 01amp03

- (617)22$-2050 bull FAX (6m229()046

July 24 1990 Revised August 10 1990

H-0-7 -24

Mr Dennis Gagne Regional Sampl e Control Custodian U S Environmental Protection Agency 90 Can a l Street Boston Massachusetts 02114

Re TID No 01-9007-10 Case No 14355 SOG No AT 528 Southwest Research Institut e Charles George Site Tyngsboro Ma Volatile 4 Aqueous AT528 throuqh AT531 Semivolatile 3AqueousfAT529 through AT531

Dear Mr Gagne

A validation was performed on the organic analytical data for 4 water samples collected by the Environaental Studies Secti on of USEPA at the Charles George site Four samplea were analyzed for volatiles and three samples were analyzed for semivolatiles The sabullplea were analyze-1 according to the 288 statement of Work (SOW) one trip blank and one set of matrix spikejaatrix spike duplicates were abullong the 4 samples There were no field blanks or field duplicates The data were evaluated based on the following parameters

bull data completeness bull holding times bull GCHS tuning bull calibration bull blanks bull surrogate recoveries bull bullatrix spikejmatrix s pike duplicates

field duplicate r esults internal standard performance

bull compound identification bull compo und quantitation

- All criteria were met for this parameter Table I summari zes the validation r ecommendations which were based o n the following information

)

Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990

H-0 - 7 - 2 4

Calibratiopbull

IC CC ~~

llroa011ethane X

chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X

Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO

The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples

Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults

xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects

RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s

Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990

H-0-7-24

Semiyolatile cc ~

bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X

Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD

No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea

x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results

Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects

RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects

bullbull

)

Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990

H-0-7-2 4

aurroqatt Rtcoyeriet

Semiyolatile

The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below

Ill A

mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5

QC Liaita JS 10 21 to to to to 114 116 100

The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 3: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

) poundSAT PROJECT LANDMARK ONE ONE VAN DE GRMFF DRIVE BURLINGTON MA 01amp03

- (617)22$-2050 bull FAX (6m229()046

July 24 1990 Revised August 10 1990

H-0-7 -24

Mr Dennis Gagne Regional Sampl e Control Custodian U S Environmental Protection Agency 90 Can a l Street Boston Massachusetts 02114

Re TID No 01-9007-10 Case No 14355 SOG No AT 528 Southwest Research Institut e Charles George Site Tyngsboro Ma Volatile 4 Aqueous AT528 throuqh AT531 Semivolatile 3AqueousfAT529 through AT531

Dear Mr Gagne

A validation was performed on the organic analytical data for 4 water samples collected by the Environaental Studies Secti on of USEPA at the Charles George site Four samplea were analyzed for volatiles and three samples were analyzed for semivolatiles The sabullplea were analyze-1 according to the 288 statement of Work (SOW) one trip blank and one set of matrix spikejaatrix spike duplicates were abullong the 4 samples There were no field blanks or field duplicates The data were evaluated based on the following parameters

bull data completeness bull holding times bull GCHS tuning bull calibration bull blanks bull surrogate recoveries bull bullatrix spikejmatrix s pike duplicates

field duplicate r esults internal standard performance

bull compound identification bull compo und quantitation

- All criteria were met for this parameter Table I summari zes the validation r ecommendations which were based o n the following information

)

Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990

H-0 - 7 - 2 4

Calibratiopbull

IC CC ~~

llroa011ethane X

chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X

Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO

The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples

Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults

xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects

RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s

Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990

H-0-7-24

Semiyolatile cc ~

bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X

Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD

No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea

x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results

Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects

RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects

bullbull

)

Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990

H-0-7-2 4

aurroqatt Rtcoyeriet

Semiyolatile

The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below

Ill A

mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5

QC Liaita JS 10 21 to to to to 114 116 100

The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 4: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

)

Mr Denni s Gag-ne July 24 1990 Page Two Revi s e d August 10 1990

H-0 - 7 - 2 4

Calibratiopbull

IC CC ~~

llroa011ethane X

chloroethane X acetone 1 1-dicbloroethane XX vinyl acetate X

Abullbullociatad saaples VBLkOl VBLkOl AT528 AT528 AT529 AT529 AT530 ATSJO ATSJl AT531 AT531MS AT531MS AT531MSD AT532KSO

The non-detected 11 -dichloroethane will be estiaated (UJ) due to the calibration not aeetinq criteria No action ibull necessary for the reaaining coa pounds since they were not detected i n the volatile samples

Pe r cent RSD gt30 Percent D gt25 Est i ma te (J ) a ll posi t i ve res ults

xx Percent RSO Pe r c ent D gt50 Estimate ( J ) all pos i shytive res ults and estimate (UJ) all non-de t ects

RF RF lt0 05 Es t i ma t e (J) al l posi t ive resul t s and rejec t (R) all no n- dete c t s

Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990

H-0-7-24

Semiyolatile cc ~

bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X

Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD

No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea

x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results

Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects

RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects

bullbull

)

Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990

H-0-7-2 4

aurroqatt Rtcoyeriet

Semiyolatile

The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below

Ill A

mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5

QC Liaita JS 10 21 to to to to 114 116 100

The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 5: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

Hr Dennis Gagne July 24 1990 Page Three Revsed August 10 1990

H-0-7-24

Semiyolatile cc ~

bia (2-chloroethyl) ether X 2-nitroaniline X 3-nitroaniline 2 4-dinitrophenol 4-nitroaniline X 4 6-dinitro-2-aethylphenol X

Aaaociated Saaples SBLXOl AT529 AT530 AT531 AT531MS AT531MSD

No action i a required since the coapounds listed above vere not detected in the aeaivolatile aaaplea

x Percent RSD gt3 0 Percent D gt25 Estiaate (J all pos itive results

Percent RSD Percent D gt50 Estimate (J) all posishytive res ults and estimate (UJ) all non-detects

RFRF lt0 05 Estimate (J all positive results and reject (R) all non-detects

bullbull

)

Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990

H-0-7-2 4

aurroqatt Rtcoyeriet

Semiyolatile

The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below

Ill A

mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5

QC Liaita JS 10 21 to to to to 114 116 100

The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 6: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

bullbull

)

Mr Dennis Gagne July 24 1990 Page Four Revised Auqus t 10 1990

H-0-7-2 4

aurroqatt Rtcoyeriet

Semiyolatile

The semivolatile surrogates which did not meet criteria for percent recovery are sulldllarized below

Ill A

mJ_ IIIZ lBI IIIL zn AT5JlKS AT531MSD 26 J5

QC Liaita JS 10 21 to to to to 114 116 100

The laboratory noted in the cas e narrative that the aatrix apike and aatrix apikbull duplicate were extracted usinq 500 al rather than one liter due to an insufficient aaount of aaaple This is a d eviation froa the 288 sow which indicates that aatrix spike and aatrix spike duplicate saaplea should be extracted with the same volue as the original aaaple No action is necessary since the validity of the data for saaple AT531 is not a f fec ted

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 7: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

)

Mr Dennis Gagne July 24 1990 Page Five Revised August 1 0 1990

H-0-7 - 2 4

It appears that there was a problem during the extracshytion or concentration process tor ATSJlMSD In ATSllMSO two acid s urrogates recovered less than lOt Recoveries ot the two surrogates were within criteria in ATSJl and ATSllMS Since s urrogate recoveries in AT531 were all within criteria and only one surroqate was slightly low in aaaple AT531MS no action will be taken for the original aaaple ATSJl Matrix SpikeMatrix Spike Duplicate

StpiyolatiJa

la t IISUJtl and ATU1JISD QC

IJaitJI

IIUIIall ~ 1BAl RfQ 1BAl RfQ

HSIISD 1 4-dichlorobenzene 2523 36-97 HSIISD n-nitroao-di-n- 3129 41-116

propylamine IISIISD 1 2 4-trichlorobenzene 3431 39-98 HSIISD acenaphthene 3635 46-118 IISD phenol 4 158 12-89 42IISD 2-chlorophenol 2 177 27-123 40IISD 4-chloro-3-methylphenol 22 2 3-97

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 8: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

Mr Dennis Gagne July 24 1990 Page Six Revised August 10 1990

H-0-7-24

Due to matrix spike recoveries less than ten percent the undetected phenol and 2-chlorophenol in aample AT5J1 will be rejected (R) bull The remaining compounds which did not meet matrix spike criteria were not detected in the original aamp1e therefore no action is required

Very truly yours

ROY F WESTON INC

~~ Zoe Horton Ot9anic Data Reviewer

~~tA-o ltA_

Cheryl Blaine

~~~middotFmiddot-Tea Manager ESAT Reqion I

Zh Enclosure(amp)

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 9: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

)

CnnEB GEOROB Case 14355

TABLE I - Recommendations Summary

amp llli A

AT528 A A A AT529 A A A AT530 A A A AT531 A AA

A Accept all data

Accept the reaulta for the aaaple but eatiaate the non-detected 1 1-dichloroethane since calishybration criteria waa not aet Inatruaent rashyaponae to thia coapound ia not atable therefore quantitation aay be affected

Accept the reaulta for the aaaple but reject (R) the undetected phenol and 2-chlorophenol due to low aatrix spike duplicate recoveriea Thia aay indicate that in the original aaaple theae acid coapounda vera not recovered accurately during extraction poaaibly resulting in falae negatives

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 10: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

Charibullbull Georqe Table II - Tentatively Identified Compoundbull (TICbull) awamary

AT529

FURAN TETRAHYDRO

X - CoJapound was detected

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 11: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

)

Data s ummary Xey

A Acceptable data

J The associatec1 nWDerical value is an estimated quantity

R Rej act data due to qual ty control criteria The data are unusable (compound may or may not be present) Reaampl inq and reanalysis is necessary tor verification

u The compound was analyzed tor but was not detected The associated numerical value is the sample quantitation limit

UJ The coapound was analyzed tor but was not detected The saaple quantitfltion liait is an estiaated quantity

The capounc1 Vfla analyzed tor but waa not c1etected The saaple quantitation liait ia the same as the CRQL presentec1

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

---------middotmiddotmiddot-------middotmiddotmiddotmiddot--middotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddotmiddot bull-IAJ1 101

-bullbulln -NIIIIAtt11

-bulln-oIO)JUOLmiddotll ll wbullbulln-o101J1bull1

-middotbullbull-z oa -wtd-z-14tt_

s 0middot-middotmiddot S tuldoldDIOJI0-[ 1--bull1

_1011bull1 -l l l __IO__ o

-0-JO Ioi~ IJI

-diDIdDJOIol-10-[ 1-l -

OOIdDJO)IP0-l l

- 1-JoOIPIIIbullbullu l 1I IIV AIIA

111)) Jo0 )1PtJIIIUCiqJI]

_Joell lol-1bull1-1 1 1 _nz

- IOIO)Iol-0-ll

( )UOJ )-Ioll-oIO JI-10 bullll

-ot-oJOllol-10middot 1 1

-ot-oJOl l-10 -1 1

M) 0UDqJI]

JO )Ioll-l Aiol

01 PIJOIfl AIIJA

01 -~~~-middotmiddot 01 __Jo01]

l[SIY oun llSJY _ ~~~ d j JI

I[SIr oun

WI _11110A OIOQIeampAI~H)JIIQ

~

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

_~~~~~

middot~middotlbullllllod lllj~-

lll~liimiddotZ -1bull11~1fMuoH1Jrpz

1-pHIIPI~I -Sl loHIJII~~Imiddotl

-~ludoiHI)IPft

-~~~PMgtJAIIImiddotZ -lodIIII~ [ middot OHI)ICbull

-~~~IIQOHIJIPftOI

OII J)jueGHIJIQbull

_bull lfdtl

-n-qoo~OJIPI~I middottll

1-lfdioHI)II~IOmiddotl

-~~~-liiIOiji-HIIIO middotZgtbullIq

P71 ~011101

p~~ ~bullmiddotz

~---~bullu-z

~---middot -NiqO~I1

-1HIJIPObull

-IbullAdold-U-Pmiddot-~~11bull1

1-lfIIAIII

~bull1110 ( iildoJdoOjOHIIOmiddotl)Ojq

1-lod AII1middotl

-NiqOHI JIPI Omiddotll

10110~ jA NOI

-NOqOHI JIP0middot1

-laqiiIHI JIP 0middot [ 1

_- o z

~Otf10 (1Aij1MHii10middotllbull lq

lliMIIIoiOIAOIY1

MIUfXI1 Jl IZS OIIOS

w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

06R9bull 06ll9 I QJ131111] UYO 0616l9 0616l9 0616ll9 IQ]41fn]1YO

11))-fJIIOUnliO

Ol -)Lecl( )lf l )orut

01 -OJifl(ljI ) NIIq)Q

Ol -Md(PmiddotpoundlI)OUIIpU)

Ol -Md( I )O

II -~~~-l f(~)OIWI

01 -IUUIlf (q)Ollel

111 ) lljd)J110middotUmiddot)0

Ul)l lfllld()JIj)llfUmiddotl)I U

01 -w10

01 -OJif1UI( I )ONII

P) lWqOJO)IP0bullpoundpound

l l l ) llfl lld lAlMCI )Il11

~middot lll)l~jlfdlAIIqmiddotUmiddot0

OS l-lfdoHJifOI4 01 -NiqOJO)IPIIIII 01 Jllj)I)Aulf4middot1Aui~Jbull bull

01 l)aulbull l lldiposoJlUmiddotI

OS 1--PIAbullIl_middot l middotOJ1)U)Qbull9t

OS au10JIUmiddott

Ol J lbulllWIfltllmiddotl~JO)IOmiddott

01 lll)llflfdAij11 )0

_)OIOJI)U)Qmiddottl

0) UljONiqjQ

os bull-fdonu os _lfdoJI UOmiddot middotz

_lry IU1Y OU1Y 6lS1Y n AIOUIOIYl 1101Ul0l Jl4WYS l fSn 0[51Y J8WII JldWS

tlSlY middoto11 CIS SSOI =nn u --o 1 1 1100 -s til OJOq1llluAj lllo U )Ji tQ uu

~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 12: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

ADMINISTRAT IVE RECORD

( ) 06ll9 lQDllflrf JnO 0616V9 oI6V9 0616119 06161 on-snvo

Ol bullbull bullbull m l-wJIICIIInliO

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CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

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  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 13: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

CHARLES GEORGE LAND RECLAMATION TRUS T LANDFI LL

AOHINISTRATI VE RECORD

()

ann usn oun

_11_

6lSU

lllnll middot[ -~O~Dl~WObulll

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w bull bull ~bullbulll~bulloo bullbullll

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

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  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910
Page 14: MEMO REGARDING 06/16/1990 SAMPLING AT FLINT POND … · Mr. Dennis Gagne July 24, 1990 Page Six Revised: August 10, 1990 H-0-7-24 . Due to matrix spike recoveries less than ten percent,

_

CHARLES GEORGE LAND RECLAMATION TRUST LANDFILL

AOHINISTRATI VE RECORD

~----~__ filii

til

tltMoshy

( I

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01 l)aulbull l lldiposoJlUmiddotI

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~ ~--~----4--===================- middot middotc~-====================--_j

  1. barcode 555910
  2. barcodetext SDMS Doc ID 555910