MedKoo Biosciences Product Quality Control Data · 2017-08-17 · Oven Temperature: 50 C MS" ESI-POS Mass 103-1000. 0.5 1 1.5 2 2.5 min* mV 0 100 200 300 *ELS1 A, Voltage . 1. 104

0.00.51.01.52.02.53.03.54.04.55.05.56.06.57.07.58.08.59.0f1 (ppm)

-500

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

5500

chp1003-A PROTON DMSO D:\ nmr1

2.07

3.13

4.03

4.05

1.06

2.00

1.68

1.03

1.02

1.03

4.08

2.01

1.01

0.98

A (s)5.17

B (m)5.06

C (d)6.14

D (dd)3.38

E (t)3.10

F (m)2.13

G (p)1.94

H (dd)7.00

I (d)7.07

J (s)7.14

K (m)7.37

L (d)7.48

M (s)7.61

N (s)8.13

1.09

1.92

1.94

1.96

2.12

2.15

2.17

2.46

2.47

2.48

2.50

3.08

3.10

3.11

3.34

3.37

5.06

5.17

6.99

6.99

7.01

7.01

7.06

7.08

7.14

7.34

7.36

7.37

7.39

7.41

7.43

7.47

7.49

7.61

8.13

MedKoo Biosciences www.medkoo.com [email protected]

MedKoo Biosciences Product Quality Control Data

www.medkoo.com | [email protected]





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MedKoo#: 204210 Name: AEW-541 CAS#: 475489-16-8 Lot#TZC40313 Chemical Formula: C27H29N5O Exact Mass: 439.23721 Molecular Weight: 439.55

File D:\DATA\A01\MONITOR\CHP10003-A-01947-LCMSA034.D Injection Date : 11 Mar 14 12:20 pm +0800 Tgt Mass(EZX) : Sample Name : CHP10003-A Location : P2-A-03 Acq. Operator : A01-Monitor Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\METHODS\1-POS-MON.M Analysis Method : D:\METHODS\1-POS-MON.M Sample Info : Easy-Access Method: '1-POS-MON' Method Info : Mobile Phase: A: water(0.01%TFA) B: ACN(0.01%TFA) Gradient: 5%-95% B in 1.3min Flow Rate: 2ml/min Column: Sunfire C18, 4.6*50mm,3.5um Oven Temperature: 50 C MS" ESI-POS Mass 103-1000

min*0.5 1 1.5 2 2.5

mV

0100200300

*ELS1 A, Voltage

1.10

4

min*0.5 1 1.5 2 2.5

mAU

0

1000

2000

*DAD1 A, Sig=214,4 Ref=off

1.10

7

1.85

1

min*0.5 1 1.5 2 2.5

mAU

0

500

1000

*DAD1 B, Sig=254,4 Ref=off

1.10

8

1.94

4

min0.5 1 1.5 2 2.50

50000010000001500000

MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.11

3

2.06

9

2.16

7

Integration Results for ELS1 A, Voltage

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.10 0.04 1131.52 445.02 100.00

Integration Results for DAD1 A, Sig=214,4 Ref=off

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.11 0.02 4746.90 2734.92 99.56 1.85 0.03 21.02 10.83 0.44

Integration Results for DAD1 B, Sig=254,4 Ref=off

RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.11 0.02 2165.52 1470.02 99.67 1.94 0.02 7.07 5.08 0.33

LC/MS Report

LCMSA034 03/11/2014 12:24:28 PM A01-Monitor Page 1 of 2 Med

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Ret. Time: 1.11 <<<< POSITIVE SPECTRA >>>>

m/z225 250 275 300 325 350 375 400 425

50000

100000

150000

200000

250000

*ES-API Positive

442

.2

220

.7

441

.2 4

40.2

Ret. Time: 2.07

m/z200 400 600 800 1000 1200

5000

10000

15000

20000

25000

*ES-API Positive

241

.1

764

.5

103

.2

420

.3

375

.2

295

.0

124

6.7

200

.1

318

.3

464

.3

507

.3

441

.2

138

2.6

111

0.7

130

.2

159

.0

974

.7

702

.8

838

.8

566

.9

105

.2

317

.3

Ret. Time: 2.17

m/z200 400 600 800 1000 1200

5000

10000

15000

20000

25000

*ES-API Positive

854

.7

106

.1 1

29.2

380

.2

241

.1

429

.3

295

.0

138

2.6

341

.3

124

6.6

318

.3

200

.1

111

0.7

159

.0

974

.8

496

.0

838

.8

702

.8

566

.8

385

.3

430

.9

317

.3

105

.1

LC/MS Report

LCMSA034 03/11/2014 12:24:28 PM A01-Monitor Page 2 of 2 Med

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MedKoo Biosciences Product Quality Control Data · 2017-08-17 · Oven Temperature: 50 C MS" ESI-POS Mass 103-1000. 0.5 1 1.5 2 2.5 min* mV 0 100 200 300 *ELS1 A, Voltage . 1. 104