Matrix: (soil/water) WATER Lab Samp la ID: 7SAA2A ...108-9O-7——— 100-41-4——-lorobeniene 100-42-9 ——————— FORM I VOA 100 SO 10 10 U u U u J 2 U 2 73 3,. 2

IEVOLATILE ORCANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Nam«: VERSAR INC

-Lib Cod*: VERSAR Cas* No.

Matrix: (soil/water) WATER

S-ampla ut/vol: 25. Q <g/mL>

Lav*1: <lou/mad} LOW

% Moisturt: not dac. ___

Column (pack/cap) PACK

Numoar TICs found: _Q.

___«. Contract:

430 17 SAS NO. :

EPA SAMPLE NO.

EEF5O

SDQ No. : EEE1Q

Lab Samp la ID: 7SAA2A

Lab Fila ID: YA581

Data Racaivad: 06/29/89

Data Analgzad: QA/3Q/99

Dilution Factor: 5. O___

CONCENTRATION UNITS:<ug/L or ug/Kg) UQ/L

ti: CAS NUMBERi

i :COMPOUND NAME ! RT I EST. CONC.

i i• i

Q

FORM I VOA-TIC 1/87 Rev.

100284

IAVOLATILE ORQANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

1 EEF31ib Name: VERSAR INC Contract:

uab Code: VERSAR Case No. : 43Q 17 SAS No. : 4733E SDG No. :

Matrix: (soil/water) MATER,

Sample ut/vol: 23. Q Cg/ffiL) ML

Level: <low/med) LOW

7, Moisture: not dec. , _

Column: (pack/cap) PACK

GAS NO. COMPOUND

Lab Sample ID: 736A3A

Lab File ID: YASSa

Data Received: 06/59/89

Data Analyzed: QA/3Q/B9

Dilution Factor: S. Q


1Ar * n 1 • 1 n

Chloride

79-O9-2—————•Ar.tnn*

340-99-0- •It 2-Dichloroathene (total)

71-33-6———————1. 1* l^Trichloroethane36-23-3———————Carbon Tetrachloride_

10O610-1-3- •cis-l» 3-Dichloropropene,

124-48-1--79-OO-3——

•Dibrofflochloromathana_-li 1. 2-Trichloroathane, i

10061-O2-6——•110-73-8————•73-23-2—————•ioa-io-1—

•trans-i« 3-Dichloropropene,__!•g-ghlQf*o«thulvlnif lather 1

_____1_ 1•——4-Methgl-2-Pentanone,

;7f-34rW •1* it 2i a^TttracNloToathana.

108-9O-7———100-41-4——-

lorobeniene

100-42-9 ———————

FORM I VOA

100SO1010

UuUuJU2

2733

,. 2--12229O221922222221223

9O IUQ; :ei'J.2

' 222

iU:u:uTJii:uIUtutu;uiUtuIUtuI

tu;ututututu;u

tuIU!U:u!U

1/87 Rev.

100292

LB/1

n: —^-OC-OECT !

IEVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE

•»b Name: VEPSAR INC Contract:EEF31

•wab Code: VERSAR Case No.


Sample ut/vol: 23. O <fl/mL) ML

Level: Clow/med) LOU

X Moisture: not dtc. _^_


Number TIC* found: _3

43Q 17 SAS No. : 4723E SDO NoT. : SEE 10

L,ab Sample ID: 73663A

Lab File ID: YA5S3

Date Received: 06/28/89

Date Analyzed: QA/3O/S9

Dilution Factor: 5. Q____

CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

CAS NUMBER

1.2. 73-43-43. 629-14-1

1

\ UNKNOWN! METHANE/! ETHANE>t

COMPOUND NAME

DICHLOROFLUORO-l.a-DXETHOXY-

.

!RT ! ES7

2.29 t6.47 !12.37 !

I

: i. CONC. ! Q

S u3 !J/ ij

t' • '•

y•' .' ' •.'•'.* •'

FORM I VGA-TIC 1/S7 Rev.

100294

1AVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

EEF32b Name: VERSAR INC

_4b Cod»: VERSAR Cat* No. : 43Q 17

Matrix: (soil/uattr) WATER

Contract:

SAS No. : 4723E SDQ No. : SSElfi.

Lab Samp It ID: 79664A

Sample ut/vol: 29. 0 (g/mL) ML

Ltvtl: (low/mtd) LOW

" Moisture: not dtc. ___


Lab Fila ID: Y69B3

Data Rtctivad: Q6/28/89

Datt Analgztd: 06/30/89

Dilution Factor: S Q

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

1107-02-8——107-13-1——

74-83-9———73-01-473-00-373-09-267-64-1-73-13-O73-33-73-33-3—340-39-0-67-66-3—107^06-2-78-93-3—71-33-6-36-23-3-

•Acrolain.-———Ac rglonitrilt .

•—Bromo<nathana_inyl Chloridt.

•Chloroathana.

•1, l-Dichloi*o«thana.•1, 2-Dichloi*o«thant•Chloroform^_____

(total)

•' 7*±?r'*-**'78-87-3———'•*100610-1-3—79-01-6———•124-48-1——79-00-3———-71-43-2-10061-02-6-110-73-8——73-23-2——108-10-1——

•1* 1* l-Trichloroathan«,•Carbon T»trachlorida_•Vi,o»l ,Acft*t*-.

-1.2--ci»-l» 3-Dichloropropana.-Trichloroathana______

JfI

It

1* 1* 2-Trichloroathana

•tran«-l* 3-Dichloropropana.•2-Chloroathylvinyltthrr_

'i*'lift.ah*Tat?«Klbf6a*h«na.108-88-3-108-9O-7-100-41-4-100-42-3-

•—Ethylbtnztna.

FORM I VOA

1003010101022

73322222

3022

IS;" 2

2222221223

30. . - . - a:• 2

222

. 1

:u:u:utu:u;uitu:u:u!U;u;u;ututu:utuTU!U:u:u:u:utu!U:utuiUluib;tutu!UJUiU

1/87 R«v.100324

i 1330-20-7—————Tot* 1 X y 1t n«*______________I 5 ! <J !• _ (___________i____1

FORM I VOA 1/87 R»v .

100325

IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

EEF32b Name; VERSAR INC. ________ Contract:

v-i_ab Codt: VERSAR Case No. : 43O 17 SAS NO. :

Matrix: (soil/water) MATER

Sampl* wt/vol: 23. 0 (g/mL) ML

Ltvt 1: (low/med) LOW

% Moisture: not dtc. ___


SDO No. : EEE10

Lab Sample ID: 736A4A

Lab Fila ID: Y&5S3

Date Received: Q6/2Q/89

Date Analyzed: QA/30/89

Dilution Factor: 5.Q____

TICs found: _£CONCENTRATION UNITS:<ug/L or ug/Kg) UQ/L

CAS NUMQER1

COMPOUND NAME i RT

J

EST. CONC. Q

FORM I VOA-TIC 1/87 R«v.

100326

1AVOLATILE QROANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

EEF33Nam»: VERSAR INC Contract:

ab Cod»: VERSAR Cast No. : 43Q 17 SAS No. :

Matrix: (soil/uattr) WATER

SDO No. : EEE10

Lab Saflipl* ID: 73665A

Sampl* wt/vol: 23. Q (g/nL> ML

Lcvtl: (low/mid) LQUI

X Moistur»: not dtc. •

Column: <pack/cap) PACK

Y6384Lab Fil* 10:

Datt Rtctivtd: 06/29/89

Data Analyzed: Q6/3O/S9

Dilution Factor: 5. 0___

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

*'.•

107-02-8-107-13-1-74-87-3—

•Acrol«in

-Chlorofflathan*74-83-9————————1 _73-01-4——————Vingl Chlorid».73-00-3———————Chloroathana_73-09-2———————67—64— 1 —— *•——••- ________73-13-0—————r-Carbon Dt«ulfid«.73-33-4——————73-33-3——————

67-66-3—107-06-2-78-93-3—71-33-6—36-23-3—10eTOS-4-

2-Dichloro«thtn» (total)

•——1, 1* l-Trichloroathan»,•——Carbon T»trachlorid»_

Acatajta

-1* 2-Dlchloroprbpanff.78-87-3——————•100610-1-3—————ci»-l* 3-Dichloroprop«na.79-O1-6——————-Trichloroathana______124-48-1——————79-OO-3——————— I71-43-2—————•

1, 2-Trichloro«than»

10061-O2-6—————tran»-l*3-Diehloroproptn«,110-73-8——————2-Chloro«thylvinyl«th»r.73-23-2———————108-10-1——————

I ~79 3*>*>'i• i.•'; >".V.il>:x>:2>'.a Tj>»iPirc?yioToyt:h-an«r:108-88-3—————-Tolu»n'«108-90-7——————Ch 1 or ob »n i tn t___________100-41-4——————Ethy10O-42-3———————Styrtnt.

100301010102373322222SO22132222222122330

' • a•--. .*'2221

:u:u:u;u;u;ui!U!U:u!U:u1UJU!U:u!UtuIU:uIU:u:u!UIU:u:u:utumIU

uUUu

FORM I VOA 1/87 R»v.

innaa-4

133O-2O-7———;——Total Xyltn**. 3 IU 1I____I

FORM I VGA 1/87 Rtv.

100335

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET —————————————

TENTATIVELY IDENTIFIED COMPOUNDS *t EEF59

«b Nam«: vgRSAR INC.________.———— Contract: ————————— I ——————

•__j Cod.: VERSAR Ca«« No.: ao 17 SAS No.: 4223E—— SD® No-

Matrix: <*oil/uat»r> UATER Lab Sample ID:

Samp It wt/vol: 23-0 <fl/«L) ML Lab Fil« ID:

Ltv.l: (low/m«d) LQU D«t» R«c»iv»d:

% Moiftur*: not dtc. ___ Datt Analyxtd: QA/3Q/89

Column (pack/cap) PACK Dilution Factor: J^j———

CONCENTRATION UNITS:Numbtr TIC* found: 0 <ug/L or ug/Kg)

—————————i———————————: i iGAS NUMBER ! COMPOUND NAME I RT I EST. CONC.

FORM I VOA-TIC 1/87 Rtv.

100336

1AVOLATILE OROANICS ANALYSIS DATA SHEET

EPA SAMPLE

: EEEoaN*m«: VSRSAR INC. Contract:

Cast No. : 43Q 1ft SAS No. : 4723E SDO No. : EEF73

r i - i i - .'toil/uatar > WATER Lib Samplft ID: 73933

*r,pl» ws/ve.1: 23. Q (g/mL) HL Lab Fill ID: YAQ17

*.*:• <low/m«d) LOW Date R»c«ivtd; QA/3Q/Q9

not d«c

•:p«ck/cap) PACK

Data Analyztd: Q7/17/99

Dilution Factor: 3. Q___

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UQ/L

Acrylonitrilt.Chloromtthant

: 37-02-8-——————Aero 1 • i n:C7-13-1————74-87-3—————74-83-9—————79-01-4—————79-00-3—————73-09-2—————

•Vinyl Chlorida•Chlorotthana•Mathylana Chloride.•Act ton*________'

'9-15-0- --Carbon Disul'idt79-39-4———————l. 1-Dichloroathant______73-35-3———————1> I-Dichloroatbana______m34O-39-O——————1, 2-Dichloroathana (total)*7-66-3————————Chloroform ______107-06-2—————— 1 * 2-Dich 1 orotthant______75-93-3----- —-—2~autanona71-33-6————•——li 1. 1-Trichloroathana____36-23-3———————Carbon TetrachJorida_____103-03-4———————Vinyl Acttata___________T 5-27-4—-—————8rofliadiehlQrQiB«than«7S-S7-5———————1* 2-Dichloroayaaan*100610-1-9———ci»-l* S-Dichloropropana.^^79-01-6————•——Tr i c h 1 o roa thana______ .124-4S-1———————PthrQinnehlorQaathana79-OO-5———————1. l*.2-Trichloro»than»____71-43-2—————————Bmnz»nm _________^_10C61-02-6————tran»-l» 3-Dichloropropana_110-79-8———————2-Chloroathylvinvlathar.73-23-2————————Bromo-Porm.103-10-1———————391-78-6———————127-18-4——————— _______79-34-3———————l, l, 2, 2-Tatrachloroathana.108-88-3———————Talu«na ________„103-90-7———————Ch 1 or ob tn i ana ________1OC—41 -4———————Et h y 1 b an z ant ___________100-42-5————————Sturana ____________

1009010101021

79322222

5022

1922222221223

90222221

FORM i VOA

:u:u:u4U:u;u:u:u1U:utu:uiU:u:u:u!U;u:u!U:u!U:u:u:u:u:u:u;u!U:u;u:u:u:u:u

1/87 Rav.

10Q02G

: 1330-20-7————•—Total Xy l*n»« 5 !U

TORM I VGA 1/B7 R»v.

100027

IE EPA SAMPLE fVOLATILE ORflANICS ANALYSIS DATA SHEET .______TENTATIVELY IDENTIFIED COMPOUNDS !

I EEE08Namt: VERSAR INC.______________ Contract: __________ 1______

ta*D Codt: VgRSAR Cast No. : 43Q 1A SAS No. : 4723C SDO No. : EEF73

riitrii (ioil/uattr) WATER Lab Samp It ID: 73933

Samp It wt/vol: 23. Q (g/mL) M^__ Lab Filt ID: YAfll7

Ltvtl: (low/mtd) LOW Datt Rtctivtd:

:: ôi»tur«: not die. ___ Datt Analyzed: 07/17/99

Column (pack/cap) PACK Dilution Factor: S. Q

CONCENTRATION UNITS:Numbtr TICs found: _2 (ug/L or ug/Kg) UQ/L

CAS NUMBER COMPOUND NAME

. - . : • :

1 ti RT I EST.

_ 1 I

CONC. ! a

, • . r

FORM I VOA-TIC ' 1/87 Rtv.100028

1AVOLATILE ORGANIC3 ANALYSIS DATA SHEET

Nama: VERSAR INC Contract:

EPA SAMPLE NO.

EEE34

'- .u Coda: VERSAR C«ft No. : 43Q 16 SAS No. : 4723E SOG No. : FEF73

M a t r i x ; vsoil/uatar) UJATER

Sampl* wt/vol:

Laval:

23.0 <g/mL) QL,_

Clow/mad) LOW

Lab Sampla ID: 75963

Lab Fila 10: Y6S32

X Moistur*: not dac. ^^_

Calumn- (pack/cap) PACK

Oat* Racaivad: Q6/3Q/S9

Data Analyzad: 07/18/99

Dilution Factor: 50____

c

CA3 NO. COMPOUNDCONCENTRATION UNITS:(ufl/L or ug/Kg) UQ/L

\ 07-,-i2-a ————— • —— -Aff-ral »in107-13-1— ————— Aerylonitrila74-97-3 ——————— Ch 1 or omathan*74-B3-9 —— -"-" • -BTQaQ««tftana75-01-4 ————————— Vinifl Chl«firf« „,-_75-OO-3 ———— — T— Chloroathana_ . „.75-09-2— —————— M«thijlana Chlorid.A7-A4-1 ————————— Ae»tan«75-15-0 ————————— C*rhan DiftUlfid* . , , _,75-35-4 ————————— 1. l-piehlaroath»n« _ ,75-35-3 ——————— l. l-Dichlorea*han. „.540-59-0 ——————— l,2-Dichloro«thana (total) __A7-AA-3 ————— • ——— Chlof oform. ^ ____ ti107-OA-2- —————— 1, 2-Dichloroa*han»

T1-S5-A ————————— 1. 1. l-Trichlai-a«th*n.5A-23-5 ————————— Carbon Tatraeh 1 ari ri«loe-05-4 ———— • —— Vinyl Acatata . _75-27-4- ————————— Hr omn d i C h 1 Or Om» than. _79-57-5 ——————— — 1, 2-Diehlorooronan*100610-1-5 ————— ci»-l» 3-Dichloropropana _____79-0 1 -A ————————— Trichloroathana124-48-1 ———— « — -DihT-nmflchlorom.than.79-00-5 ————————— 1. 1. 2-Triehloro«th*n«7 1 -43-2— — -—————B »n i • n •10061-02-6 —— • —— trans-1* S-Dichloropropana.^.^,1 1 0-75-S ——————— 2-Ch l oroathy Iviny 1 «th »r75-23-2 ————————— B-Pomoârm1 OS-10-1 ———————— 4-M«trhyl-2-Pant*nan«591-78-A ———————— =>-W.»anon« am mi127-19-4 ———————— T.traehloro«th.n«79-34-5 ———— • —— l. 1, 2* 2-Tatrachloroathana— _ _1 OS-Sa-3 ————————— Ta 1 u • n •108-9O-7 ——————— ChlaTObanzana1 00-41-4 ——————— et h 4 1 b an z ana _1 00-42-5 ————————— Sty r • n*

1000500100

. . . ... 100

1510750301515

-_1201515500151515015» *2031151515101 •15305OO59i «15151510

11;u:u• 1 1-4U !U!UiU;u:u> 1 1i ^ x"IU!U

iU1 1 1iU:u:uiu

!U:u!U;u' 1 1!U:u;u1 ^-^~1' 1)iU!U:u;u

FORM i VOA 1/87 Rtv.

J.GGG33

I 1330-20-7 Total X y l t n « « 45 IU I


100034

IEVOLATILE ORGAN:cs ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

i >e^^ » o r hi/*• g?tsAet L JVC Contract:EEE34

uac Cod*: VERSAR C*ft» No. : 43O 16 SAS No. : 4723E SDG No. : EEF73

73963

L»vtl: (lou/ffi*d) LOW

r. Moistur*: not d*e. _^^


Numbfr TICs found: _0

L3t 3809 Iff ID

Lab Fll* ID:

Datt R«ctlv«d: QA/3Q/99

D«t« Analyzed: Q7/19/99

Dilution Factor: SO ____


11

CAS NUMBER i

1

COMPOUND NAME

.- . - . - • • • . • ' .. - .

RT

. . . . . . . J

iEST. CONC. !

• 1

Q

!

r.

FORM I VOA-TIC 1/87 R»v.100035

1AVOLATILE ORSANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Nam«: VERSAR INC.ECE39 v/i

Contract:

C0 d t: VERSAR Cast No. : 43Q 1A- SAS No. : 4723E SCO No. : EEF73

Matrix: (ioil/uattr) WATER

5ampIt wt/vol:

Levtl:

23. Q <9/mL) QL,_

<lou/m»d> LQUI

Lab Samp It ID: 75934

Lab Filt ID: Y6819

7. Moisturt: not d»c. ^_


Dat» RtCtivtd: 06/3Q/99

Date Analyzed: Q7/17/89

Dilution Factor: 30QQ

CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kfl) UQ/L

107-02-8 ————107-13-1 ————

74-83-9 —————73-01-4 —————

75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-35-3 —————540-59-0 ————67-66-3 —————1C7-06-2 ————

71-35-6 —————36-23-5 —————1 'te . n^ _ ri __«_ .

75-27-4 —————

—— Aerel*in |11B_—— Aery ion itril*— -Ch lor om» than*—— Br ooio «• t h an •—— Vinul Chlorid*

\*i\ i of Ovv nan* ^—— Mvthyltn* Chlarid*——— Aeatan*——Carbon Ditultid*—— 1, l-Dichloro*th*««—— 1, l-Dichloro«than*—— •!, 2-Dichloro»th»n* <total>__——Chloroform™ 1* 2-Dichloro»th«n*— -2-Butanon*——- 1. 1, l-TrichlOTa*th*n«—— Carbon T*trachlar id*—— Vinyl Ac»tat»—— Bromod ichlora««th*n«

79-57- 5— -—-—-1* 2-Dichloroprapana100610-1-5 ——79-01-6 ——————124-48-1 ————79-00-5 ——————71-43-2 —————10061-02-6 ——110-75-8 ————75-25-2 —————108-10-1 ————591-78-6 —————127-18-4 ————79-34-5 ——————1 08-88-3 —————

100-41-4 —————100-42-5 ————

— —— c im— 1 . 3— Diehloraprop»n«——Trieh loro«th»n»—— -Dibrofflochlorom«than*—— 1, 1. 2-Trichlora*th*n»-«Q«nr»n»—— trans— 1* 3— DiehlaraaroDtna—— 2-Chloroathulvinul«th*r-—— Bromof arm-— 4-M»thul-2-Ptntanan»—— 2-H» v anon* ^

—— 1. 1. 2* 2-Tttrachloro»than*-- __—— Talu*n» MIIIIII—— Chlorob*nz«n»—— Eth^lbtni^nt—— Styr*n*

10000030000100001QOOO1OOOO1900100079000300015OO130013OOO15001300300001200150015000130013002000130013001300150010001300130030003000097013003300130071001000

i•:u:u!Utututu1U:u:uIU:u:u;uIU

;u!U:u:u:u:u:u:u:uIU:u:u:u!Uu

!U

:uFORM I VOA 1/97 R«v.

1GQ052

133O-20-7——————Total 14000 ! 1

FORM I VGA 1/87 R»v.

100053


EPA SAMPLE NO.

EEE39L*b Nam»: VERSAR INC Contract:

Codt: VERSAR Cast No.

^latTix: (soil/uattr) UATER

Samalt ut/vol: 25. Q <g/mL> ML

L»v»l: (low/mtd) LOW

7. ttoisturt: not dec, , __

Column <pack/cap) PACK

Numbtr TIC» found: _2

43Q 16 SAS NO. : 47236 SDO No. : EEF73

Lab Sampl* ID: 73934____

Lab Fil* ID:

Date Rtctiv*d

Y&S19

Date Analyztd: 07/17/99

Dilution Factor: 5OOQ

CONCENTRATION UNITS:(ug/L or ug/K0) UO/L

CAS NUM5ER

1. 96-14-02.

COMPOUND NAME

PENTANE* 3-MKTHYU-UNKNOWN

RT i EST. CONC.mImmmmmmmmmmmm

1 19. 8O I OOO Ui 22.97 ! 0 UI_______I ________!_


100054

escooininininjnintnininiH{ninsn;n:nin:nin;niniH!n:nin!ni*nsn:nin:t\\nimn:n:ns

VGA I

TzzzzzocczzI

zzzzzCTzftoczzzzzctLTe.0101OToc001

'•uou» IE »H-Z———————9-8£- I6C'•uour»mri»e-Tftq»«w-fr———————I-01-SOT

——Z-CZ-C^B-C^-OtT

9-ZO-T900I

•»u»Mi»oo.o:y3|ui-z 'i 'T. -C-00-6t

' •u»doadoaotM3TQ-C'T-*T3——————6-T-OT900T

• piJ-oiVDra^.*^ uoqav>•*-eO-80T-C-E2-9C

• uo u v » n B-Z———————C-£6-S^'»urM*»oaotMDia-Z 'T——————Z-90-iOT

u T • t———————8-ZO-iOT

QNOOdWOD 'ON

MOVd :uu inrc- .

6B/OC/9O

0 SZ

©OS * : 'ON

08333

133HS SISXTVNV SOINVOdO'ON HldWVS

1330-2O-7——————Total Xyl«n««______________! 5 !U


100CS6

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS I

1 EEE80Nam»: VERSAR INC.___________«. Contract: _______ 1______

- .L. Cod«; VER5AR Cast No. : 43Q 16 SAS No. : 4723E SDO No. :

Matrix: doil/wattr) WATER Lab Sample ID: 73964

wt/vol: 23.0 (g/mL> QL,__ Lab Fil« ID: Y6831

L*v*i: (lou/mtd) LOW Dat* R»C»ivad: OA/3Q/89

X Moiiturt: not d«c. ___ Dat* Analyxtd: Q7/18/89

Cslumn ipack/cap) PACK Dilution Factor: 5. Q___

CONCENTRATION UNITS:Numbtr TICs found: 3 (ug/L or ug/Kg) UQ/L

CAS NUMBER

i. -2. 79-43-43.

i *I COMPOUND NAME

I UNKNOWN..-' ' '.-: .: '! METHANE, DICHLOROFLUORO-! UNKNOWN

I iRT f

•M--, SLW-'-N! 6.47'JI 12.42 t

EST. CONC.

^'••'*&.' r-33

Q

J .JJ

c

FORM I VOA-TIC 1/87 R»v.

100C37

1AVOLATILE QRQANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

EEE82Namt: VERSAR INC. Contract:

-•ft Cod*: VERSAR Cast No. : 43Q 16 SAS No..: 4733E SCO No. : EEF73

Matrix, doil/uatar) WATER Lab Samplt ID: 75959

Sample ut/vol: ^ 25. Q (g/mL) QL,_ Lab Filt ID: YAMS

Ltv»l: Uow/mtd) LOU Dat» Ractivtd: OA/3Q/99

Moisture, not dtc.

Column; (pack/cap) PACK

Datt Analynd: 07/19/99

Dilution Factor: SO

r

CAS NO. COMPOUNDCONCENTRATIONtufl/u or ug/ng>

UNITS:uo>/i-

f

i oT-oa-e ————— AC T a i • i n107-13-1 ——— — —— Aefij lonitrl !•74-B7-3 ——— - ——— — ChlaromathanaTA-as-9—— — .' • •» a-« aw t hafia : . . . . . . - • ". '. • • • • :75-01-4 ————— - —— Vinyl ChloMda79-00-3- ————— — £hlai»oftthan«_75-09-2— — — • —— n«thyl»n« Chlor id t ______ _Â7-aA-l ————————— Ae*«an«75-19-0 ———— : ———— C^rhan Di«Ul* id . _ , ,__ _75-3S-4 —————————— 1. 1-Dtchlaro.th.n. _ __,„., ,79-3S-3 ———————— i. l-Diehlora.th*n. _ IB nm ,540-59-0 ——————— I/ 2-Dichlofotth»n« (total )A7-6A-3 — - —————— Chlo ro fo rm107-06-2 —————— 1* 2-Dichloro«than«79-93-3— — -5-8utanona71-5S-& —————— • — 1. 1. l-Trichloâ«th*n«3A-23-3 ———— - —— Ca-rhon T»traehlar id«1 OS-05-4 ———— —— -- V in 4 l AC* tat*75-27-4——— —— — ———Bârtia d i Ch 1 oran«-fchAn*79-37-3 ————————— 1. 2-Dichlorooi<aa*n«lOQalQ-1-3- • gi«-l . 3-Dichlo-popT-op»n«T9-0 1 -A ————————— T^ i e h 1 ar a«th •«•124-48-1 ——————— FHhT-omaehlaro««th*n.79-00-3 ————— » —— 1. 1, 2-Triehloi»a«than«7 1 -43-2 ———— - —— - ——— a*n T »n»10061-02-6 ———— tran«-l» 3-Dichloropropan*.. __110-75-S ———— "— -2-Ch 1 oraathu Ivini^ lath »r73-23-2 —————— - ——— Bromoforfll1 OS-10-1 ———————— 4-M«thvl-2-P*ntanan*99 1 -7S-A ——————— S-H« » anon*12T-1S-4 ————————— T.*-r»chloro»th.n.79-34-5 ——————— i, 1, 2> 2-Tttr«chloro«than« ___10H-SS-3 ————————— Ta lu«n»l OS-9O-7 ——— - —— Ch 1 or o b »n z «n • „ ..,100-41-4 —————— E t h y l b « n z t n » _100-42- 5 ———————— Stt/r»n»

100050010O

L.. • • : . . - ,'.' .-iOO• ; '• • ido

1510

1903015IS571515

500160

15150

15IS2O

15IS1510IS1523

500

15190

IS1510

1

:u:u1UIU .I Ut u;u;j:u:u:uii:u;u:u•:u:ui U;u:u:c:uiu:ui U;u:u:jx:u;eI U••:u:u:ui

•FORM I VOA 1/87 Rtv.

100121

1330-2O-7——————Total Xyltn**^______ t 90 !

T ynA 1/57 *•

100122

IEVOLATILE OROANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

•• Namt: VERSAR INC. ______^«— Contract:

Ca*» Ne. : 43Q 1A SAS No. :

EPA SAMPLE NO.

t EEE82J______

v-uao Codt: VSRSAR

Matrix, (soil/wattr) WATER

Samplt wt/vol: 2S. Q (g/mL) HL

L»v»l: <lou/m«d) LQU

" Moi»tur«: not dec, .^


SDO No. : ggF73

Lab Sampl* ID: 75939

Lab Fil« ID: YABas

Dat» R»c»ivtd: QA/3Q/99

Data Analyzed: 07/18/99

Dilution Factor: 50

Numb«r TIC» found:CONCENTRATION UNITS:(ug/L or ug/Kg) UO/L

CAS NUMBER COMPOUND NAME RT t EST. CONC.

JLt

FtWM I VOA-TIC 1/87 Riv.

100123

1AVOLATILE ORCANICS ANALYSIS DATA SHEET

Nam»: VERSAR INC Contract:

EFA SAflFLE MO.

I EEEB2-DLI________

w*b Codt: VERSAR Ca«* No

ttatnx Ctoil/watar) WATER

Sample wt/vol:

43Q SAS No. : 4723E SDO No. : EEF73

Lab Samp It ID: 73939-PL

23. 0 (fl/mL) QL _ Lab File ID: VA949

Ltvtl (low/mad) Data Received OA/ao/99

noiiturt: not dtc,

Cslomn: (pack/cap) PACK

Datt Analyzed: 07/35/89

Dilution Factor: 1QQ___

GAS NO. COMPOONDCONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

1C? -02-8 ————107-13-1 ————74-87-3 —————74-83-9 —————79-01-4 ———— -73-OO-3 —————75-09-2 —————67-64-1 —————75-13-0 —————

73-33-3 —————340-39-0 ————67-66-3 —————1C7-06-2 ————

- — Aerolein , .—— Ac T ii I on i tr 1 1 •

——— ft* a««M **!«•«•- •:.••:.•.-•' . --j^v • ••.-—— Vin^l Chlarld.

———Ma t h n 1 ana Cn 1 ar i 4 *_ ^ Âeafcane

- — -Carhan Dicultida——— 1, 1-niehlorettthana- —— 1. l-Diehloro«thana— -I/ 2-Dichloroethene (total)___——Chloroform .—— 1. 2-Diehloro«than»

7S-93-3 ————————— 2-Butancn«71 — 3 3—6™™36-23-3 —— ——108-03-4 ————73-27-4 —————78-67- 3 —————100610-1-3 ———79-O1 -6— ———— -124-48-1 —————79-00-3 ——————71-43-2 ——————10061-02-6 ——110-75-8 ————75-23-2 —————108-10-1 ————391-78-6 ————127-18-4 ————79-34-3; —————1 08-88-3 ————108-90-7 ————100-41-4 ————100-42-3 ————

——— 1, 1, 1-Triehleraathana _———Carbon T»traeh Tot- i d«—— Vinijl Aotata , .

——— eli-l. 3-DiChlBf»aaraa«n«

—— tran»-l» 3-Dichloropropene __ B—— 2-Chloroathi(lvinVl»ther——— Branaform——— 4-M» t h i| 1 -2-P mn tan an •— -2-H» x anona— — T»tT>aehlara«th«n«—— 1, 1. 2» 2-Tetrachlorotthane_ __ .

— — Chlorobentene—— Ethyl h»ni»n»

20001000200

v.'" "'aoo'3020

1900603030303030

1000303030O303040480303O3020303060

10004903030303020

t1

iU!UIU.tu:. ••'- iIUIUIU:u:u:u:u!U;u:u;u:utu!UIUIU:D:u;u:u!UiUtuJU:uIU:u:u:u:u

FORM I VOA 1/87 Rav.

100I4G

! 1330-SO-7 Tot«l Xyl«n«« 90 !U

FORM I VOA 1/97 R*v.

100147

IEVOLATILE OROANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Namt: VERSAR INC

EPA SAMPLE NO.

It EEEB2-DL

Contract:

w.- Codt: VERSAR Cast No. : 43Q 1A SAS No. : 47gaE SDG* No. : ggF73

Matrix. («oil/uat»r) WATER Uab Simp If ID: 739S9-PL

Sampl* wt/vol: 29. Q Cg/flO.) ML Lab Fila ID: Y6949_

Clow/mad)L*vtl

29. Q (g/«L)

LOW

" Moifturt: not dtc. _^^_


Datt Rtctivtd: Q&/3Q/89

Dat» Analgitd: 07/22/Qg

Dilution Factor: 1QO

Numbtr TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

CAS NUMBER COMPOUND NAME RT EST. CONC.

FORM I VGA-TIC 1/87 R»v.

100148

1AVOLATILE ORGAN I CO ANALYSIS DATA SHEET . i c.

It- "EPA SAMPLE NO.

EEEB3Nama: VgRSAR INC Contract:

»ib Codt: VERSAR Cast No. : 43Q 16 SAS No. : 4733E SDQ No. : EEF73

Matrix: (toil/watar) WATER Lab Samp It ID: 759SA

Sampl* wt/vol: 23.Q Cg/mL) ML Lab Fila ID: YAg34

Utvtl: (low/mad) LOW Datt Racaivad: QA/3Q/89

Moisturt: not dtc

C-lumn: (pack/cap) PACK

Data Analytad: 07/19/89

Dilution Factor: 30

c

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg> UQ/L

i fl7-Q2-9 ——————— Acr Q lain107-13-1 ————74-87-3 —————74-83-9 —————73-01-4 —————73-00-3 —————73-09-2 —————67-64-1 —————73-15-0 —————73-33-4 ——————75— 35— 3——— ———340-39-0 ————67-66-3 —————107-06-2 ————78-93-3 —————

36-23-3 —————108-03-4 ————73-27-4 —————78-87-3 —————10O61O-1-3 ——79-01-6 —————124-48-1 ————79-OO- 3 —————71-43-2 —————10061-02-6 ——110-73-8 ————73-23-2 —————108-10-1 ————39 l -78-6 ————127-18-4 ————

1 08-88-3 ————108-90-7 ————100-41-4 ————100-42-3 ————

—— Acrylonitrilt—— Chl aroma than*

—— Vinul Chldrida__ -—— Chlaroathana

—— Ae*tona_—— Carbon Diftulfid*—— 1, l-Diehloro«th.n«

—— I* 2-Di eh lor oath ana <total>_^—— Chloroform _,..—— 1, 2-Dichlaroathan»—— 2-Butanona •— — — 1, 1. 1— Tr ieh ltM»a»th*n»—— Carbon Tatraeh larid.-—Vinyl Acatatt—— -Bramadich lor OA» than* _—— -1. 2-Dich laraprop«n»——— eift-_l j 3-Diehlaraprap»na—— -Trieh loroathan*—— Dihromochloro*«than» _——— 1, 1. 2-Triehlora«than»

Bcnzvna—— tran»-l» 3-Dichloroproptna ___—— g-ChlQroathulvinul«thar—— Brofflaforn ._

~2-H»ianona

— -1* 1, 2' 2-Tatrachloroathana—— Toluana _ ., .—— Chlorobanxana—— Ethyl baniana—— Styrvna

1000500100

>..•'••;-•• ;- .too100131073030IS131313135OO34131301313207013131310131330300731313131310

i•:u:uiU

•-iu; -IUtu:u;u:uiUIU:utu!U:u:u:u:u:u:uiU:u:u:u:u:u:u:u!U:u:u!U;u


100159

I 1330-20-7——————Total Xyltn»«______________! 43 !U !! _____________________________ ________I_____________1_____!


1001GQ

IE EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS !

t EEEB3Nama: VERSAR INC._____„_____ Contract: _________ J______C o d«- VERSAR Cast No. : 43Q 1A SAS No. : 47g3E SDG No. : EEF73

Matrix: Csoil/uatar) WATEH__ Lab Samp It ID: 7595A

Samplt wt/vol: 23. O (g/ffli.) ML Lab Fila ID: YA834

Laval: <low/mad) LOW Data Racaivad: Q6/3Q/99

" ttciftur*: not dac. ___ Data Analyzad: 07/19/99

Cslumn (pack/cap) PACK Dilution Factor: 90____

CONCENTRATION UNITS:Numtoar TICi found: Q <ug/L or ug/Kg) UQ/L

CA£ NUMBER COMPOUND NAME ! RT ! EST, CONC.

FORM I VOA-TIC • 1/87 Rav.

100161

1.4VOLATILE OROANICS ANALYSIS DATA SHEET

wn

Nam»: VERSAR INCEEES4

Contract:

-wab Cod»: VER5AR Cast No. : 430 16 SAS No. : 4723E

ttatrix: Csoil/wattr) UATER

Sampl* ut/vol: 25. Q <g/nL> ML

L»vil: <lou/ffl»d> LOW

H Moisturt: not dtc. ___

Column: ( p a c k / c a p ) PACK

SOO No.


Lab Fila ID:

Data Ractivad

Y6826.

06/30/89

Datt Analyztd: O7/15/99



107-02-9————•107-13-1————-74-87-3—————-74-93-9—————75-01-4—————-75-00-3—————-75-09-2—————-67-64-1—————-75-15-0—————-75-35-4—————-

•Aery Ion itr lit,•Chloroatthant'

•Vinyl Chlortdt.-Chlorocthana '•Math^lana Chlorida.

-Carbon Disulfidt

75-35-3——540-59-0——67-66-3———107-06-2—-79-93-3——•

•————I/2-Dicbloroathtn» (total)

71-55-656-23-510B-05-475-27-473-37-5 ———————100610-1-5

—1*1*1-Trichlorotthant,—Carbon Tatrachloridt_—Vinyl Acttatt. —

•Trichloroathana124-49-1——79-00-5———71-43-2—————•10061-02-6——•110-75-9————-

I* 2-TrichXoroathanr

-1» 3-Dichloroproptna.

•———2-H» i anon«.

——2-Ch1 oroathYIvinylath «r.75-25-2————•——Bro<no*or*___________10S-10-1————•591-79-6—127-19-4—75-24-5—-108-89-3—1OS-9O-7—1CO-41-4—100-42-5—

I/ 1. 2> 2-Tatraehloroathana.

•——Ethylbanitnt.

100SO1010.10217532

• 2322SO221522

3a22•

223

SO222221

FORM I VGA

iU:u:uIUIU!UIU:u:u:u:uii:u:u:u:u!U:u:uiuIU••;u;u:u:uIU!U:u:uiU;u;u!U;u;u

1/97 R»v.

100175

: 1330-20-7———————Total X u l « n « « _____________! 3 1U 1


10017G

IE EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS ! I

! EEE84 1Name: VgRSAR INC. Contract: __________ 1______ *

Cod*: VgRSAR Cat* No. : 43Q 1A SAS No. : *7ME SDO No

•ii. Cioil/uattr) WATER Lab Sample ID:

S«mplt wt/vol: 53. Q <g/«L) JJU__ Lab Fil» ID: YAB3A

Ltv»l: Clow/mad) LOW Dat» R«c»iv»d: QA/3O/99

7. Moisturt: not d»c. ___ Datt Analyzed: Q7/18/99

Column (pack/cap) PACK Dilution Factor: ijQ———

CONCENTRATION UNITS:Numbtr TICf found: _Q. <u«/L or ug/Kg) Vg/U

CAS NUMBER COMPOUND NAME

...... ....-.• •

•: RTJ •• --

I 1: EST. CONC. : QI . . - - . . 1.


10C177


Narn*; VgRSAR INC. Contract:

EPA SAMPLE NO.

I EEEB9i_______

,-ab Codt: VERSAR Cast No. : 43O 16 SAS No. : 47236 SOG No. : EEF73

Matrix: <soil/wat»r> UATER Lab Sampl* ID: 75998____

Samplt wt/vol: 29. Q (g/mL) Q±_ Lab Filt ID: YAB27____.

L*v»l: Uou/mad) LOW Datt R»caiv»d: QA/3O/99

Mciitur»; not dtc,

Cslumn: (pack/cap) PACK

Data Analyzed: Q7/18/99


GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/L

107-G2-B ———————— Aeral«in „_„_,.„ ., „107-13-1 ——————— Aerylonitrila74-87-3 —— — -—- Chloromtthana74-83-9 ——————— Bromomathana^ _75-01-4 ———————— Vinyl Chlorida75-OO-3- ——— • —— Chloro»th*n«75-09-2 ———————— Mftthylana Chlorid. -BM IIB67- 4-1 —— ««.- —— Aotana „ , „75-1S-0 ———————— Carbon Diculfid*75-35-4 ——————— 1. l-Diehloro*than*75-35-3 ——————— 1. l-Dichlaro»than« , _,.„.,., ..540-59-0 ——————— l,2-Dichloro«thtnt (total) __67-fcA-3 ———————— Chlaroôr*107-06-2 ——————— l,2-Dichloro«than» _,.„., , ,.,79-93-3 ———————— -2-Butanon»71-55-6 ———————— 1, 1, l-Triehloroath«n«56-23-5 ——————— Carbon Tttrachlorid*10S-05-4 ——————— Vinyl Ac»tat«75-27-4 ———————— BromodiChlorom»th*n»7S-S7-5 ———————— 1* 2-DichloroDropan*100610-1-5— — — — ci«-l» 3— DiCh loroprap»n»79-01-6 ———— • —— Triehlorotth»tia124-48-1 -« — —— »Dibramochloro»athan»79-00-5 ————————— 1, 1. 2-Trichloro«th.n»7 1 -A3- 2 ——— - — • ——— B mn imnm10061-02-6 —— • — -tran»-l»3-Dichloropro ?!«•..__110-75-8 ————— — 2-Chloro«thulvinul«th»r75-2S-2 ————————— BromaforA108-10-1 ——————— 4-F1»thul-2-Ptntanon»591-78-6 ——————— 2-M»ianon«^ ____ __127-18-4 —————— »T«trachloro«than« _, ,79-34-5 ——————— 1, l,2*2-T«tr«chloro«thant ___1 08-39-3 ———————— To 1 u«n«1OB-9O-7 ——————— Chlarobanzanaioc-41-4 ————— ethyl btnitnt100-42-5 ——————— S«t/i»»na

10O50101O1021

322222

2215222222

2122

50222221

1ttu!Utu:u:u•IUIE!UIU:ui!U •;uIE!U:u:u:u;uIU:u:u:u:u;u:u!U!E:utu;ut:u!U:u*


100138

I 1330-20-7- -Total Xgl»n*s 3 !

FORM I VOA 1/B7 R»v.

100189

IE EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS !

! EEE89 iN*mt: VgRSAR INC._____________ Contract: _________ !_____________I

i—— Cod»: VgRSAR Ca«» No. : 43Q 16 SAS No. : A7ggg SDO No. : EEF73

Mi-srix: (*oil/uattr) MATER Lab Sample ID: 739BB

Samplt wt/vol: 25. 0 (g/mL) ML Lab Fll« ID: YAS27

L*vtl: <low/mtd) LQU Data R«c»iv»d: Q&/3Q/99

X Moisturt: not d«c. __^ Data Analyzed: 07/19/99

Cclumn (pack/cap) PACK Dilution Factor: S. Q

CONCENTRATION UNITS:Numbtr TICs found: _i (ug/L or ug/Kg) UQ/L

CAS NUMBER

1.

COMPOUND NAME

UNKNOWN

! ii RT ! EST.

I 2.29 1! I

CQNC.

2

•: Qu

FORM I VOA-TIC 1/S7 R»v.100190


EPA SAMPLE NO.

t EEEB3-DLNam«: VERSAR INC.__^_ Contract:

Cat* No. : 43Q la SAS No. : 47Codt: VERSAR

natrix: <§oil/wat»r> UATER

Sampl* wt/vol: 23. Q <g/«L) ML

L*vtl: (low/mod) LOW

7. Moiiturt: not dtc. ..

Cciumn: ( p a c k / c a p > PACft

SDO No. : EEF73

Lab Safliplt ID: 73938-DL

Lab Flla ID: Y&948

Data Ractivvd: QA/3Q/89

Date Analyzed: Q7/22/B9

Dilution Factor: 1QQ____


107-02-8 —————107-13-1 —————74-87-3— ——— —74-83-9 ——————73-01-4 ——————79-00-3 ——————73-O9-2 ————— -67-64-1 ——————73-19-0 ——— • ——73-39-4 ——————79-39-3 ——————34O-59-O- ——— —67-66-3 ——— — -107-06-2 —————78-93-3 ———————71-33-6 ——————36-23-3 ——————10S-03-4 —————73-27-4 ——————78-S7-3 ———————100610-1-3 ———79-01-6 ——————124-48-1 —————79-OO-3 ———————71-43-2 ——————10061-02-6 ———1 1 0-73-8 —————73-23-2 ——————108-10-1 —————391-78-6 ——————127-18-4 —————

—— Aeral tin |||(1

~Aeryloniti»il»— Chlaroatathan*

— Vinyl Chloride— Chlora«than»— -M-thy !•«• Chlot-id.

—— Carhan Di*ulfid»

—— 1. 1-DichloroBthan*— 1* 2-Dichlorotthtn» <total)_ __— Chloroform _ .— 1. 2-Diehloro»than» .__— a*Butanona— 1. 1* l-Trichloi»a»than» ._

— Vint/l Acttat*— -Br omo d i c h 1 or aa«than*

i 2— Dieh lorapT»flp«n»

— -Trichloroathan*— DibramoehloroiBtfthan*—— 1. 1, 2-TriChloro»than» __

— tranf-1* 3-Diehloraoraoana— a*Chloro»thulvinul»th»r

— ~~a^H»x ' ^^ i ^^^ -..,..,— T»tr»chloro«th«n«

/ 9— 34— 3—— ———"•———** ±i «* » IVIM •biiAuruv v H«II VM ^^ »lQS-aB-3 • -—— Taluana1 08-9O-7 —————100-41-4 —————100-42-3 —————

—— Chlarahanxan*— Ethif Ibanzana. .— Stur»n»

20001000200

2003020

240603O30303030353030

3003030403030303020303031

10OO303030303020

i:uiUtu

IU "tu:u!DJ:u!U!U:u:u:u!U!U!U:u!U;u!U:u:u:uiU:u:u:OJ!U:uiU!U!U!U:u

FORM i VGA 1/87 R«v.

100207

! 1330-20-7 Total Xyl»n»«. 90 IU

C

FORM i VGA

100^08

IEVOLATILE ORCANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Namt: VERSAR INC

EPA SAMPLE NO.

I EEEB9-OL_^____^^——» Contract:

- Codt: VERSAR Ca*» No. : 43Q 1A SAS No. :

matrix: (soil/wat»r> WATER

S«mpl» wt/vol: 25. Q (g/mL) ML

Ltvtl: (low/mad) LDU

" rtoisturt: not dtc. ____


SDO No. : EEF73

Lab Sampl* ID: 7S9S8-DL

Lab Filt ID: YA948

Data R»ctiv»d: QA/3Q/S9

Dat« Analyitd: 07/22/99

Dilution Factor: 1OO____

Numb»r TICi found: 0CONCENTRATION UNITS:<UB/L or uj/Kg) UQ/L

GAS NUMBER

C


100^09

1AVOLATILE OROANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Namt: VERSAR INC. Contract:EEEB8

Cod«: VERSAR Cat* No. : 43O' 1A SAS No. : 47235 SDO No. : g£F73

Matri*: (soil/water) MATE*

Saatpl* ut/vol: 25. 0 <g/mL) QL,__

L*v»l: (low/mtd) LDU

X Moisturt: not d»c. ___


7B9A1

Y6829

Lab Sample ID:

Lab Fil» ID: _______

Dat* Rvctivtd: Q6/3Q/99

Data Analyztd: 07/19/99



1Q7-02-S ————— - — -Aeral»in .107-13-1 ————74-97-3 —————

• 74-93-9 ———— -75-01-4 —————75-00-3 —————75-09-2 —————67-64-1 —————75-1 5-O —————TT — "55— A— — ——«75-35-3 —————54O- 59— O—— ———67-66-3 —————107-06-2 ————

71-55-6 —————56-23-5 —————1 03-05-4 ————

73-87-5 —————10O610-1-5 ——79-01-6 ————— -

79-00-5 ————— -71-43-2 —————10061-02-6 —— •110-75-3 ————75-25-2 —————103-10-1 ————591-78-6 ————127-19-4 ————TOÎ /I — — — — — «—

108-88-3 ————108-90-7 ————100-41-4 —————100-42-5 ————

—— Aer if 1 on i tr i 1 •—— Chloronathan*

-Br*«o •« t»*a« • - . - • - • . • • • • • • •. •——— Vinyl Chlorid.— —Chlaroftthan*..,—— -M»thy l»n« Chlai»id« MI IMI

—— -Ae»tan» m t——— Cat-ban D i f t u l f i d *——— 1, l-DichloTO»th»n«——— 1. l-Diehlflra»th*n.—— I* 2-Dichloro»thtn* (total).. _——— Chlaâfar in——— 1, 2-niehlaro»*h^n»—— -2-Butanon«-^_———— 1. 1. t-Triehla^««th*n«——— Carhan T»traeh laî d«——— Vini /1 Ac»tat»——— B-ramod iehloro*«th^n«—— 1. 2-Diehlaraprap*n»— — c i » — 1 , 3— Diehlarapr>ap*n«— — Tr ich loro«th*n«- —— Dibra(iochlarom«th*n«—— -1. 1. 2-Triehlora»*h*n«———Ban Tan* : , „ 1-n_—— tran§-l» 3-Diehloroproptfn*^ _ , _ _—— 2-Ch lor oath u lv inu 1 «-feh »r—— — B-rnmo Qrm—— 4-M»thul-2-Pafitanan«—— 2-H« v anan» _—— -T«t-p*ehlara«th«n«—— 1* 1. 2* 2-Tttr»ehloro«than»— ___-— Talu«n« — t ,— —— Ch 1 ot»Qh»ni«n»—— E t h y l b tnztn*—— Sti/r»n» ,_,,.,.__ „„ „

1005010

-•V^V-v**1021

753222

212

5022

1522222221223

502222Q

1

FORM I VGA

ii:u:uIUJU .iUIUJ UJ UJ UJU:u:uJ UJ UJ UJ UJ UJ U;u:uI U:u:uJ UJ UJ UJ U:u:u!UJ UJ U:uJ U:u*

. .,..

1/87 Rtv

100235

! 1330-20-7——————Total Xyl»n«»______________i 9 IU 1

C

FORM I VOA 1/87 Rtv.

10023G

IEVOLATILE QRCANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

EEES8Namt: VERSAR INC__________^____. Contract:

w«b Coda: VERSAR Casa No. : 430 16 SAS No. :

natri*: (soil/uatar) WATER

Samplt ut/vol: 23. Q (g/mL) HL

Laval: (low/mad) LDU

7. Moiitura: not dac. .^


SDO No. : 5EF73

Lab Samp la ID: 759A1

Lab Fila ID: YAB29

Data Racaivad: QA/3Q/99

Datv Analyzed: Q7/19/89


Numbar TICs found: _J2.CONCENTRATION UNITS:(ug/L or ug/Kg) UO/L

CAS NUMBER COMPOUND NAME ! RT ! EST. CONC. Q

I * •-•- 1-

r

FORM I VOA-TIC 1/87 Rav.100237


EPA SAMPLE NO.

ib Nama: VgRSAR INC.

âb Coda: VgflSAR Casa No.

Matrix: (soil/water) WATEff

Samplt wt/vol: 23. 0 (g/mL> HL

Leval: <low/mad) LOW

X floisturt; not dtc. ___

Column: (pack/cap > PACK

. __ Contract:

430 16 SAS NO. : 47

EEF71

SDQ No. : 5EF73

Lab Sample ID: 759A3

Lab File ID:

Data Raceivad: QA/3O/B9




107-02-9 ——107-13-1 ——74-87-3 ———74-83-9 ———73-01-4 ———73-00-3 ———73-09-2 ———67-64-1 ———73-13-O ———73-33-4 ———73-33-3 ———^ .4.O _ 4Q«^ w—

67-66-3 ——— r,107-04-3*—7»-93r3- =r-71-W-6 ———36-23-3 ———108-03-4 ——73-27-4 ———70—07— g— -— —/ a o / <j100610-1-3-79-01-6 ———124-48-1 ——79-OO- 3 ———71-43-2 ———10061-02-6-110-73-S ——73-23-2 ———108-10-1 ——391-78-6 ——127-19-4 ———

- ———— -Aei-alBin———— Acryloni t r i la•• • 'Chlaromathana

— '— —— Bramamathana .———— Vinij l Chlor ida— —— Chloroathana—— ——— M«thy l«n« Chla r id* _~ — —Ac •tana II-B- ———— Carbon D l t u l f i d a————— 1. i -niehlaro«th»n« —_ __———— -I. i-niehlorQ»*h*n«———— 1. 2-Dichloroathana ( to ta l ) __— — —— Ch laf*af aroi- —— — 1. 3-nieJfclaraa-feh^n* MIIM

« • g^»u*«tftti«;- • • . . -— . —— .1, i. i-Triehloâ.th-n.— • ——— C^rhan Tatraeh lar i dm——— — V i n y l Acetate—— —— — a-rnmod ich loram»-fchan«— —— l. 2-Oiehlaraprapan«—— ——— e i « — 1. 3-DiehldT-opT»np»n» _— —— Trichloroethena— — -Oihrofliochlora««fchan«———— -1. 1. 2-TriehlBT»a«fchan« m_mi ,

&»ni»n*—— — tran«-l» S-Dichloropropene.^.^^———— .2-Chlaroathulvinul«th»r——— __ Branaâra

4-M^thif l-2-P«nfc^nf>n»— • ——— 2-Havanena , IM———— T»tr«chloroeth»n»

79-34-3 ——————— 1, 1, 2' 2-T«trachloro«thana— . __1 OS-aa-3 —— - ———— To Inmnm1 08-90-7 ——— • —— C h 1 or ob an s tn a100-41-4 —————— Ethulbeniena1 00-42- 3 ——————— S t u T- • n •

100301010102

73322222

. SO' 2

2132229^

2g

1

223

3Og

w

^v4

1

i U:u:u!U:u:u^ \!Ui Ui U:u:u!U:u(U:u:u!U:u:u;u;u!U;u:u!U;u:u!U!U:u;u:u:u:u!Ui


100289

1330-20-7——————Total Xyl»n»« -____________! S 1U


100230

IEVOLATILE QRGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

3 Narnt: VERSAR INC Contract:ECF71

i_*3 Codt: vgRSAR

riAtri*: (ioil/wat*r) WATER

Samp It ut/vol: 23. Q < g/mL) ML

L*vtl: (low/m»d) LOW

" Moi*turt: not d«c. _ _

(pack/cap) PACK

TIC* found: Q

Cast No. : 43Q 16 SAS No. : 4723E SDO No. : EEF73

Lab Samp It ID: 73963

Lab Filt ID: Y693Q

Datt Rtctivtd 06/30/99

Dat» Analyzed: 07/19/99


CONCENTRATION UNITS:Cug/L or ug/Kg) UQ/L

_:-s W^BES COMPOUND NAME

iRT ! EST. CONC.

*

Q

FORM I VQA-TIC 1/97 R*v.

IAQRQAN1CS ANALYSIS DATA 8HKT

PPA

0 Nam«: VgRSAR INC.EEF72

Contract:

••<_«& Cod*: VERSAR Cast No. : 43O 16 3*5 NO. : 4733E SOQ No. : EEF73

Matrix: < 30 i l/wat»r ). WATER Lab Samp It ID: 73966

Samp It wt/vol: 29. Q <g/mL> ML

Ltvtl: <low/mad) LOW

". Moisturt: not dtc. _^_


Lab Filt ID:

Data Rtctivtd

Y6S33

Q6/3Q/99

Data Analyrtd: 07/19/89


CA5 NO. COMPOUNDCONCENTRATION UNITS:Cug/L or ug/Kg) UQ/L

107-02-8 — ——107-13-1 — ——Â— OT—T™ — _i

74-33-9 —————73-01-4 —————73-QO-3 —————73-09-2 —————67-64-1 —————73-13-O —————73-33-4 —————73-33-3 —————^<m_^Q_/^__— __67-66-3 —————107-O6-2 ————78-93-3. —— ; ——71-33-6 —————36-23-3 —————103-03-4 ————T--27-4 —————79-97-3 ——————100610-1-3 ———79-O1 -6 ——————124-48-1 ————79-00-3 ——————71-43-2 —————

—— -Acrol*in ami m—— Acrylonitril*—— Chloromathanr— -Brofltomathan*—— Vinul Chlorida—— Chlorot thant——— Mtthultn* Chlarid*—— Aettan* n nnuim—— Carbon Ditulfid*—— 1. l-Dichloro»th*n«—— 1* 1-Dichlorotthan*—— 1. 2-Dichlorotth*n* < total)—— Ch 1 ar of or a- — -1* 2-Dichloro*than*—— 2-1 u.t anon*—— •!. 1. l~Trichloi»o*than*—— Carbon Tatrachlor id*—— Vinul Acttatt—— Br omo dich lor OIB* than*— — I/ 2-Dichlorooropan*—— cifli 3-DiChloroprop*n*—— Tr ich laro«th*n*- — Dibromochlorom*than*—— 1* 1* 2-Trichloro*than*—— B*nz*n* ,_ .

10C61-O2-6—— —— -trant-1* 3-DlchIaroorQOtn*

73-23-2 —————103-10-1 ————

127-19-4 —————79-34-3 ——————

10S-9O-7 —————100-41-4 ————100-42-3 ————

—— *— -n iarowsnyiviny L ttn*r— -Bromoform—— 4-Mathul-2-Ptntanon*- — -2-H* t anon* _—— T»trachlorotth*n*—— 1* 1, 2' 2-T*tr*chloro*than* ___—— Toluana „ ._,—— Chlorobtnztnt—— Ethulb«nzan«—— Sti/r*n* __ ,

ri

1000 :u300 :u100 !U100 :u65 :j15 iU10 :u

730 !U30 iUis :u37 T140 J-15 IU13 IU

5OO tUis :u13 ;u

130 !Uis ;u13 :u20 :uiso r13 ;uis :u13 !U10 iU13 :uis :u30 :usoo :u84 :is :u13 :u15 IUis :u10 :ui

FORM I VGA 1/87 R*v,

100298

133O-2O-7 Total 43


100233

IE EPA SAMPLE NO.VOLATILE ORGANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS !

! EEF72^ Namt: VER3AR INC._____________ Contract: _______^ I______

Cod*: VERSAR Cat* No. : 43Q 1A SAS No. : 4733E SDO No. : EEF73

ix: <30il/uat*r) UATER Lab Sampl* ID:

Sampi* ut/vol: 23. Q <g/«L) CB._ Lab Fil» ID:

L»v«l: (low/m«d) LOW Dat» R»ctiv»d: QA/3O/89

" Moiitur*: not d«c. _. Dat* Anali^ztd: 07/18/89

Cglunn (pack/cap) PACK Dilution Factor: Jfl____

CONCENTRATION UNITS:Numbar TICs found: _2 (ug/L or ug/Kg) UQ/L

11

CAS NUMBERI

COMPOUND NAME RT EST. CONC. Q

I


100300

1AVOLATILE ORQANICS ANALYSIS DATA SHEET

EFA NO.

b Nam«: VERSAR INC.EEF73

Contract:

*0 Cod«: VERSAR Cat* No. : 43Q 16 SAS No. : 4723E 500 No. : EEF73

Platr ix: ( 30il/uat«r) WATER

Sjmplt wt/vol: 23. Q (g/mL) Q^__

Ltvtl: <low/mad) LOW

7. Moisturt: not dtc. ..___


Lab Sampla ID: 73BQ3

Lab Fil» ID:

Data R»ctiv»d

Y67B4

Q6/29/S9

Data Analyztd: Q7/13/89



107-02-8 ————107-13-1 ————74-87-3 —————74-33-9 ————— •73-01-4 —————73-00-3 —————73-09-2 —————67-64-1 —————73-13-0 —————73-33-4 —————•*•_•*• f* .... ./ 3—33—3——————340-39-0 ————67-66-3 —————

—— Acralain .,—— Acrulonitrilt— -Ch lor am* than t— -Bromomathan*—— Vinul Chlorida—— Chloroathana——— Mathultna Chlarid*—— -AcBtona B—— Carbon Dl*ul*id«—— 1» l-Dichloroath«n«— -1* l-Dichloroathan»—— 1* 2-Dichloro«than« (total)—— Chlai»a<ai*A

107-O4-2 —— -i —— -l*2-Dtcblaroath«n«7Sr-*a*»3 i.i . • a-gu*anam«. . ., - , .-71-33-6 —————36-23-3 —————i rtQ_o^«<i_____, — — A, — •*— -•-•78-87-3 —————100610-1-3 ——79-01-6 —————

79-OO- 3 —————71-43-2 —————10061-02-6 ——110-73-8 ————73-23-2 —————108-10-1 ————391-79 6 ————127-18-4 ————79-34-3 —————108-88-3 ————108-9O-7 ————100-41-4 ————100-42-3 ————

—— 1* 1. l-Tri«hlora«th*n«—— Carbon Tt trachlarid*—— Vinul Acttatt—— •aromodichlorom«th*n»——— 1* 2-DiChloroorapan*— — ci«— 1» 3— DlChlaraprap*na—— Trichloroathana—— Oibrofloehloromathana—— I/ 1. 2-Trichloro«than« ,, _—— B»nz»na—— trans-1* S-Dichlorooropana—— 2-ChloroathMlvin^lathar—— Bramaôr* „.- — 4-tta t h u 1 -2-P tn tan an •—— 2-Hax.anona -B_—— Tatrachloroath«n«—— 1. 1, 2* 2-Tatrachlorotthant ___—— Tbluana ui— -Chlorobanztn*—— Ethulbanztna-— -Stur»na _ni

100301010^321

7332218229O2213

24

t.2221223SO222221

i:uiU:u:uu!UiU:u!U;u!U

***\:u:u(U:u!U:u:u;u!U û :uiU:uIU:u:uiU:u: *s!U:u;u:u;ui<

FORM i VOA 1/87 Rtv.

100320

1330-2O-7——————Total Xyltfl«»______________! 3 !U

FORM I VQA 1/87 R»v .

100321

IEVOLATILE ORQANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

EEF73b Name: VgRSAR INC Contract:

Codt: VERSAR Case No. : 43Q '1A SAS No. : 4753E

Matrix: <*oil/uater> MATER

Sample wt/vol: 25. Q (g/mU) ML

Level: (low/med) LOW

£ Moistur*: not d»c. 1 —


Numbtr TICs found: Q

SDQ No. : EEF73

73803

Y67S4

Lab Sample ID:

Lab Fll« ID: _______

Data R«ctivtd: OA/29/99




CAS NUMBER COMPOUND NAME RT EST. CONC. Q


100322


EPA SAMPLE NO.

EEF74Namt: VgRSAR INC.

Codt: VgRSAR Cast No.

Matrix: (»oil/wat»r> WATER

Samplt wt/vol: 29. Q (g/mL) HL

Ltvvl: (low/mad) LOW

7. Moistura: not dtc. ___


CAS NO. COMPOUND

___^_ Contract:

43Q 16 SAS No. : 4 SDO No. : EEF73

Lab Samp It ID: 75BQ4

Lab Fila ID: VAaiQ

Data Rtctivvd: 06/29/89

Data Analyitd: Q7/17/99


CONCENTRATION UNITS:<ufl/L or ug/Kg) UQ/L

107-02-9 ————107-13-1 ————74-87-3 —————74-83-9 —————79-01-4 —————79-00-3 —————79-09-2 —————67-64-1 —— : ——79-19-0 —————79-39-4 —————79—39—3——————94O-59-0 ————67-66-3 —————107-O6-2 —— y=

71-99-6 ——— -

108-09-4 — • ——

79-87-9 ——————100610-1-9-r-79-01-6 —————124-48-1 ————79-00-9 —————71-43-2 —————1 rt^ / i _• rt^ /1 UC6 1 — O«— 6— ——1 1 O T 0«> « ^

79-29-2 ———— 109-10-1 ————991-78-6 ————127-18-4 ————79-34-9- ————109-S8-3 ————108-90-7 ————100-41-4 ————100-42-9 ————

——— Aeralain—— Aerylonitrila—— Chloronathana—— Bromomathana—— Vinyl Chlorid* „_,.,,. ., ,.—— Chlaroathana .

---A4.a*«««—— C*rban Diaultid*

—— 1, l-Dichloi»oath.an«—— •!* 2-Oichloroathana (total >~ Chloroform

—— 2-Butanana.—— 1. 1. 1-TriehlofaafehAn*— —— C^-rhon Tatraehlai»id» iwi t u—— Vinyl Acatata ,_._„_„_„ ,——— Bromodich larom«*han»

——Triehloraathan*

——— 1, 1. 2-Trichlora«than«-— a»n?«n» ,„.,„„.,., ,—— trans-1* 3-Oichloropropana_ „__—— S-Chloroathulvinulvthar—— - Qr-natofarm

~~~ 5 * * * * ^ ' « ««

—— •!. 1* 2i 2-Tatrachloroathana ___—— Tolu«na , IIMI—— Chlarobanzana—— -ethif ibanzana ,——— Stijrtna „„._„.,„„

1000O900010OO100O22019O100

73OO3001901901600190

-_...:: 1901 —— * 900O

190190190019019O20011019019019010019O19O300900024O190190190190100

1

:u:u:u:u! JIUiU:uiUiU:u!U

--10T-. ..1U!U:u!U:u:u:u!J :u:uiU;u:u:u:u:u;u!UiU;u:ui


100340

I 1330-20-7——————Total Xyltn«*______________I 43O !U

FORM I VOA 1/87 R«v.

100341

IE EPA SAMPLE NO.VOLATILE OROANICS ANALYSIS DATA SHEET ________TENTATIVELY IDENTIFIED COMPOUNDS :

! EEF74Nam»: VgRSAR INC._________.—-.- Contract: ^_^_______ I____________

ab Codt: VERSAR Ca*» No. : 43Q 1A SAS No. : 4723E SDO No. : gSF73

x: (toil/uattr) WATER Lab Sampl* ID: 759Q4

S«mplt ut/vol: 23. 0 Cg/mL) HL Lab Filt ID: YABIQ

Ltvtl: (low/mtd) LOW Dat« R»c»iv»d: QA729/99

X Moitturt: not dtc. ^__ Oat* Analyttd: 07/17/89

Calumn (pack/cap) PACK Dilution Factor: 5OO

CONCENTRATION UNITS:TIC» found: _fi (ug/L or ug/Kg) (JQ/L

1

CAS NUMBER !

i>

iCOMPOUND NAME ! RT

J

EST. CONC. Q

FORM I VOA-TIC 1/S7 R.v.

100342

1AVOLATILE ORQANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

EEF91ab Nama: VgRSAR INC. Contract:

-uab Cod«: VERSAR Gas* No. : 43O 16 SAS NO. : 4723E SDG No. : EgF73

Matrix: (soil/uattr) WATER Lab Samp It ID: 7SBQ5

Sampl* wt/vol: 25. Q (g/nL) 0 __ Lab Fill ID: YAflll

Livvl: (lou/mtd) LOW Datt Rtctivtd: 06/29/89

Motsturt: not dec


Datt Analyitd: 07/17/99


CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kj> UO/L

. 107-02-8 ——107-13-1 ——7 A— a?** 9 »— —/ **— O / J74-83-9 ———75-01-4 ———75-00-3 ———7S— G9— 2—— ——67-64-1 ———75-15-0 ———73-35-4 ———~n— ^fl—^™— ™/ 3 — 33— 3— —— —34O-39-0 ——67—66—3107-O6-2 ——78-93*-*———71-35-6 ———36-23-5 ———i no— /^— A———73-S7-4 ———78-87-3 ———10O610-1-3-79-01-6 ————124-48-1 ——79-00-3 ————71-43-2 ———10061-02-6-110-75-8 ——75-25-2 ———108-10-1 ——391-78-6 ——t 27~ 1 9— 4«*_ •1« / LQ •*79-34-5 ———108-98-3 ——108-90-7 ——100-41-4 ———100-42-3 ——

—— ——— Aera 1 • in _____———— Aery lonitr i l t— —— Ch loromathan*-----aramomathan* ,^__———— V i n t f l Chlor ide———— Chloroe/than*^ ___ mm- —— — M«th 4 l»n« Chlor id .- ——— Aotana———— Carhan D i « u l f i d « |||B1 1B||— —— 1, l-Diehlarafl«h»n«_——— — 1, l-Dichloroafchan*--- •• i» 2-Diehloro«than« ( total )__—— —— Chlaro*or«

ft Bu*<nofia -.. . ...1* 1* l-Tricflloro«than«

———— Carbon Tatrachlar id* , _.,_———— Vini/1 Ac* tat*

aramadiehlorQ«»than» ___.. , __._—— ——— 1, 2-Dichlorooraaan*

ei«— 1< 3— Oiehlaranraa*n«———— Triehloroath*n«——— »DihranaehlaramBthan* t— ——— 1. 1. 2-TrichlOT»a»th«n»—— .—__{)»„ , mni BBBBB-B_Bp

———— tran«-li 3-Dichloroprop«n« ___———— >2-Chlara*thijlvinyl*th*r ____ _

• •" Srnmaform I B I————— 4-M«th9l-2-P«ntanon«—— — 2-H*ianon*——— —— T»traehloro*th«n» B-I ," •-•!< 1^ 2* 2-T*traehloro»thana- ——— Toluana—— — Chlorobonzana——— Ethi j lb tnz tn*- ——— St^r»n» M _IB

11005010101021

73322222

3022

132222223

^

so^

^

22^

<t:u!U

:u:u:u:u;u:u:u:u;u;u:utu:u:u:uJ U:u:u;u!Ui U

:ui U:ui W

I U:u:u:ut u! 1

FORM i VOA 1/87 R«v.

100359

; 1330-2O-7——————Total Xyltnt*______________! 3 !U


1003GO

IEVOLATILE QRGANICS ANALYSIS DATA SHEET


EPA SAMPLE NO.

EEF91»b Nam*: VgRSAR INC Contract:

•uab Cod»: VERSAB. Ca*« No. : 43Q 16 SAS NO. : 47g3E

Matrix: Csoil/uat»r> MATER

Sample wt/vol: 2S. Q (g/mL) ML

L«v»1: (Iow/m«d) LOW

51 Moiaturt: not d»c. _^_


Number TICs found: __1

SDO No. : -EEF73

73801Lab Samp It ID:

Lab Fil» ID: _______

Datt Rtctivtd: QA/39/99




GAS NUMBER

1.

COMPOUND NAME

UNKNOWN

1 RT ! EST. CONC. Q

t 12. 42 ! £& J

FORM I VOA-TIC • 1/87 Rtv.

100361

1AVOLATILE QRGANICS ANALYSIS DATA SHEET

0 Nam«: VERSAR INC._____________ Contract: _

EPA SAMPLE NO.

EEF93

-Cab Cod*: VERSAR Cat* No. : 43Q 16 9AS No. : *Z2S&

Matrix: (soil/uat*r) UATER

Samp 1* wt/vQl: 25. Q <g/mL) ML

L«v*1: (low/nid) LOW

7. Moisturt: not d«c. ___

SDO No. ESF73

Lab Samp It ID: 758QA

Lab Fil» ID: Y6fll2


CAS NO. • COMPOUND

Data Rtctived: O6/29/99

Datt Analyzed: 07/17/99


*• :S


107-02-9 ————107-13-1 ————74-87-3 —————74-83-9 ——— - —75-01-4 —————75-00-3 —————75-09-2 —————67-64- 1 —————75-15-0 —————73-35-4 —————75-35-3 —————540-59-0 ————67-6A-3 —————

.78r9O-3 —— ~-71-55-6 ——— : —56-23-5 —————108-05-4 ————73-27-4 ——————78-87- S —— - ———100610-1-S ———79-O1 -6 ——————124-48-1 ————79-00- S —————71-43-2 —————10061-02-6 ——110-75-8 ————7S-2S-2 —————108-10-1 ————59 1-79-6 ————127-18-4 ————

108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————

—— A e i » a l a i n B „,—— -Aei»ylanl trill—— Ch 1 aâmthan*— — Sromoflu thane _—— Vinyl Chlorid.—— Chloro»than« M—— «.-fehi,l»n« Chloi-id.-—Ac •tana ima——— Cî-han D i m u l ^ i d .—— 1, l-Dichloro»th«n»—— 1, l-Diehloroathan*—— -1. 2-Dichlorotthtnt ( to t a l ) __——— Chla*a*fl*a— — 1* 2*Diehloro«th*n« -—— a-ButAfton* • -. :—— 1, 1, 1-Triehlafa.than.—— Carhan Tatrachlar id»—— Vinu l Acttat*——— a-ramad ich laTOm»th*n«—— -1. 2-Dichlaraprapjn. _ mm __ ,_—— ei*-l, 3-Dichlaraoroo»n«—— -Trieh loro«th»n«—— Dihromoch laram«than«—— -1. 1* 2-Trichlo*a«than«—— H « n r « n « „ „,_,—— tran*-l* 3-Oichloraproptn» ___ ,—— 2-Chloro«thtf lv in i f l« th«r—— Bi>amafarfli ,_.——— 4-M»thvl-2-P»ntanan« m_—— a-Haianona^^^^—— T»tTaehloro«th«n«— -1, 1. 2* 2-Tttr«chloro»than» ___~Talu»na—— Ch larob an lana- — g thu lb tn i tn*—— Styr»na ,

1005010101021

75322222

9022

IS22222221223

SO322221

I;u:u!U:u;u;u:u;u:u:u!U:u:u:u!U:u:u;u:u1UI U:u:u!U!U:u:uI U:u!U••;u:u!U:u:u•


100363

! 1330-2O-7——————Total Xyltnt*________ \ 5 iU

FORM 1 VGA 1/87 Rtv.

100370

IE EPA SAMPLE NO.VOLATILE ORCANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS

b Nam«: VERSAR INC.___________._ Contract:EEF92

Cod»: VERSAR Ca«» No. : 43Q 16 3AS NO. : 47336 SDQ No. : EEF73

Matrix: Cioil/uattr) WATER Lab Samp It ID: 73SQA

Sampl* wt/vol: 23.Q (g/«L) QL,_ Lab Fll» ID: Y&812

L«v«l: (low/mad) LOW Oat* R«c»iv»d: QA/29/99

Z floiiturt: not dtc. __^ Oat* Analyzed: Q7/17/S9

Column (pack/cap) PACK Dilution Factor: 3. Q

CONCENTRATION UNITS:Number TlCs found: Q (ug/L or ug/Kg) UQ/L

11CAS NUMBER t

ti

: : :COMPOUND NAME ! RT ! E5T. CONC. I Q

! i i

FORM I VOA-TIC 1/87 R»v.

100371


EPA SAMPLE NO.

EEF94ib Nam*: VgRSAR INC__ ________^__ Contract:

Cod*: VERSAR Cast No. : 43Q 16 SA3 No. :

Ma tr i x: t so i1/uat*r) WATER

Sampl* ut/vol: 23. Q (g/mL) QL_

Ltvtl: (lou/m*d> LOW

7. Moisture: not dec. _^_—


{

SD« No. : EEF73

Lab Samp It ID: 7B9O7

Lab Fil* ID: Y&S13

Dat* R*c*iv*d 06/29/99

Dat* Analyzed:. 07/17/99


CAS NO. COMPOUNDCONCENTRATION UNITS:<ug/L or ug/Kg) UQ/L

107-02-9-107-13-1————-74-97-3—————-74-93-9—————-73-01-4—————-73-OO-3—73-09-2-67-64-1^-73-13-0—73-33-4—73-33-3-34O-39-0————67-66-3—r———107-oar-a-——7«-93-3———-71-33-6-—————36-23-3—————109-03-4————73-27-479-97-3——100610-1-379-01-6——124-49-1-79-00-3-71-43-2-

•Acroltin.^^^^•Aery lonitr i l*_•Chlorom*than*'

'V inyl Chlorid*.•Chloro*than* '

•Ac* ton*-Carbon

'1, 2-Dichlore*th*n* ( t o t a l )

•a-ffutanon*•1* 1. l-Tt*iehloTO*than*.•Carbon Tttrachlorid*-Viny l Ac*tat*

•cis-l» 3—Oichloroprop*n*,-Trichloro*th*n*

1. 1. 2-Triehlot«a«thin«

10061-02-6————trani-1* 3-110-73-9———•——'2-Chloro*thylvinyl*th*r73-23-2———108-10-1——391-79-6——127-19-4—— _______79-34-3—————™1, 1, 2' 2-T*trachloro*than*.109-88-3-—- ——Talu*n*1 OS-90-7-100-41-4-100-42-3-

Chlorobtnzin*

2001002020433

1306320373

10O213303344333a336

100

iU;u!U!U: J:u(:u:u;u

:u:u

:u:uiU;u:u!U!U:u:u:u!U:u:u:u:u: u:u:u


oseooiLB/\ VOA i uucy

n: 6 I——— «»u»t f tx T**OI————Z-OE-OCCT

IE EPA SAMPLE NO.VOLATILE ORQANICS ANALYSIS DATA SHEET _____________TENTATIVELY IDENTIFIED COMPOUNDS I

! EEF94b Nam«: VgRSAR INC._______,^___ Contract: __^___ !______.

i_*b Codt: VERSAR Ca*« No. : 43Q 1A SAS No. : 4723g SDO No. : EEF73

Matrix: (*oil/uat»r> WATER Lab Samp It ID: 79SO7

Samplt ut/vol: 25.Q <g/«L) fiU_ Lab Fil* ID: X6fli2

Ltvtl: (low/n«d) LOW Date Rvctivod:

7. Moiiturt: not dtc. ___ Data Analijztd: Q7/17/99

Column (pack/cap) PACK. Dilution Factor: Ifl____

CONCENTRATION UNITS:Numb»r TICs found: _a <ug/L or ug/Kfl) UO/L

CAS NUMBER COMPOUND NAME: i :! RT I EST. CONC. I

1 1 1f 1 1

Q

^ •M


10038.1

UNITED STATES CKVlROmiEMTAL FROTECTIOH AGENCYREfilO* V .

C53/Central Regional LaboratoryCAT* THACK1NG FORM FOR CONTRACT

CM. Data Stt HoSF CERCLIS Ho

C«e Me.\lM5J3 V,Stte *a»e and Location: ____Na«e of Contractor «r EPA Laboratof^Cj^^^fNy-PdV Bata User:

Ho. of Samples: <=>£2) Pate Staples or Data Received:1. Have ehain-ef-custody records been received? YES2. Have Tsattic Reports or packing lists been receiv«3T" .*„__-—, .3. If no. art T r a f f i c Report or packing lisf numbers written on the cRatn-of-custody

record? T£S HO__4* If no. which Traff ic report or packing list numbers are Kissing?

LX

of samples received:P*tt:

Art basic data forms 1n? YES

Mumber of samples claimed:

Checked by;

ved by Contract Project Hanajement Section: s\J/?L//L Bate: 3 ~

Started: 3/23/^^7 Reviewer Signature:

Total time spent on rtvle*:Copied (xeroxed) by:

to Pata User bv:

USERS:

Data, rtvie* caspleted: 3/3//^

Bate:Bate:

Please fill in tht blanks belw and riturn this fora to: Sjlvia firiffin. BataManagement Coordinator, Region Y, 5SCRL

Data received by:

0-A. review received by:

Bate:

6*te:

Inorganic Bate Conplctt t 'Organic Data Complete COioiintlata Co«plett tSAS Datt Complete C

, Suitable for Intended Purposes. Suitable for Intended Purposes, Suitable for Intended Purposes, Suitable for Intended Purposes

/[ 1 if acceptable.List problem belo«.

Attachtd "Missing Bata Reouest Form" C 3"BLEMS: Please indicate reasons lif any) nhy data are not suitable for your uses.

Other problems.

Received by Data Management Coordinate^ CRU for Fil t : Oate:_

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY1 OF -?-

R e « w of Region V CLP Oat.Received for Review on

rnoo. Curtis Ross, Director (5SCRL)Central Regional Laboratory

Ve have reviewed the data for tht following.case(s).

SITE NAME: \JU CXV\Q< UjloJli vL ±o ffO SMO Cast Mo..

EPA Data Set No^P (AS..*

SMO Traffic Mo.

CLP Laboratory; CTo!I owing art our findings:

**1\r Reêw^

Data are acceptable for use.Data are acceptable for use with qualifications referenced above.Ste Data Qualifier sheets and Calibration Outlier forms for flags andauction*! comments.

) Data ire preliminary - pending verification by Contractor Laboratory.Set Case Summary above.

( ) Data are unacceptable.

cc: Carli Ofnpsey.CLP Quality Assurance Officer, Analytical Operations BranchJames Pftty. Chief Quality Assurance Research, EMSL, Las Vegas

USEPA CONTRACT LABORATORY PROGRAMSAMPLE MANAGEMENT OFFICEP.O BOX BIB ALEXANDRIA. VA 22JI3703/557-2490 FTS-5572490

ORGANIC TRAFFIC REPORTffOHCLP US! ONLY I

TYPf OF ACTIVITY (CWO-E ONE) (D* esra?% RO RA ER

NP1D

SfTEMAUft

_WCiOTTY, STATE:5i*nic

•m SPILL O;>*I/OI

REOION NO: SAUPUNO COMPANYCJ43A* *JIU

SAMPLER; (NAME)CATMY

ATT**- WAT/3/ fC

SAMPLMOOATE:

sea** _aî=_i:9

DATE 8HrPED:il3bI3CAftRIER: F 9

v 1*7*5-11063.

' . SAMPLE DESCRIPTION(ENTERMBOXA) 4. SOS.1. SURFACE WATER S. SEDIMENT1. QROUNO WATER S. Oft, (SAS)1 LEACHATE T. WASTE (SAS)

TRIPLE VOLUME REOUWEO POR UATRKSPKI/DUPUCATE AQUEOUS SAMPLE

SHIP MEDIUM AND WOH CONCENTRATIONSAMPLES IN PAJNT CANS

SEE REVERSE FOR ADOmONALMSTRUCnONS

CLPSAMPLENUMBER

(FROM LABELS)

CAW

CAW 4SCAW

£AW

€8EflW

70"7*

CAW

CAW

CAW

ANALYSISSPECIAL

HANDUNQ

2.17^70

STATIONLOCATION

SW-T06-OI

;w- CM 1070-0*

01

. roi-oi

•- RECEIVED INGOOD CONDITION

-.: -^v. i '* ...

',_. _ . _ . _f ___

EPA Fwn 2071-7 («-«7)

WHITE - SMO COPY PINK - CLIENT COPY WHITE — LAB COPY FOR RETURN TO SMO YELLOW - IAB COP

3 1883 CENTRAL REGIONAL LAUORAT^Y SAMPLE DATA REPORTrtt/l ORGANICS/I PANICS5/7 J TH|S FORM |S Q BE USED pon SAMPLES SENT TO CONTRACT ONLY J <//5

CASE NUMUtR/SAS No,

SUPERFUND DU NUMBER

AC 11VIIY NUMBER

PA HPM « OSC |S M S

PJ\1-\*'\^* f » ' «* JI

OAIE

rpnr».g NUMBEn .PAGE

wAicn on i inmDS SEDIMENTS « SOILS

Of

CRL LOGNUMBER

ORGANICTRAFFICREPORTNUMBER

INORGANICTRAFFICREPORTNUMBER

orSAS Packing List No. e " P Is a?

?

1i* tu M /K

535

S/VA;

ss?

cMAR 0 0 1909 CENTRAL REGIONAL LAUOHA" «Y SAMPLE DATA REPORT

ORGANICS/ JRGANICS DfiTl l/tt/rf '5?^? THIS FOI1M IS TO BE USED TOM SAMPLES SENT TO CQNTnACTjDNLY

SHEM*"* H/i/vi*-/ ytLU. /-ujL«C IAOOMAIQIIY.SUPtfifUNDDU HUM

At 1IVIIY NUMBER I

CRL LOGNUMBER

3Ux

ntn 1 /°.

— /*îAj J

^4

> EPA RPM oi C


OISAS Packlr

^S?4/^

5t=j Wtui'W^3t>^ |£axJ 26*5(p^5(5^* /^^?J)

5w5/70Vrtl

5?-x/1.4

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\»*\

S9S"S^vS-77iO ^ •

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fitu) I/-GuJ 11-f^ 13-ftUAj #/"

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fijAj'??*'feuxi?/ -c<\Ô*T^

fflLU ^S

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0 List No.

—

SC |S M S I/ICESriff'/'N1 ~t(la#('A~J r/

ERCI is NUMBERwAuii nniinuins

rMP

3M

£3

3r-

O

SMy

i-03

3

Mr

i!o• a

•*;ntsh

ii

o3

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2

: O3

1i

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SEDIMENTS M SOUS

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PASS 1 OFUNITED STATES ENVIRONMENTAL PROTECTION AGENCY

R e V e w of Region V CLP DataReceived for Review on

y,APR 0 7

moo. Curtis Ross. Director (5SCRL)Ctntr«l Rigionil Ltborttor,/

<-s

V« hive rtvfcwtd tht tfata for the fol lowing. c*»t(s).SITE HAME: \ }fl rmQ UjlOJ) G. ^ ffO S« C«t »0,

SHO Traffic N

CLP Laboratory: ________ j s for R«v1«w;

following arc our findings:

_f ?stiÂ* s\ \s L A Hrs. Required(

Oata art acceptable for use*Data arc acceptable for use wl' __ See Data Qualifier sheets and \ 'TOaUdltlonal comments* /

) Data are preliminary - pendingSee Case Sunmary above* ^

( ) Data are unacceptable. l/l/Vl"

cc: Carla Dempsey^P Quality AssurJames Petty, Chief Quality Assu /

\J

DATA QUALIFIERSPAGE ^ OF j_

Contractor:/

( C a s e //*/ 9 V2'3'

Below 1s a summary of the out-pf-control audits and the possible effect on thedata for this case:

i"i^/* TiVvw-*

U TKA.

*)a .•*) AW /vo/J -tt•*) AW

** 67*

i^- *L*^^^ Tt< I b(2**~

(ad

fcr.'t^.V^ j .

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> J A l.y Ac.s ,^-

CAl.aAl ^/ / V bt.

Ccvi4.Uu. A F

Reviewed by;Phone:Date:

3X3- S3

DATA QUALIFIERSPAGE -3 OF j

Contractor: Case 3/

Below Is a summary of the out-of-control audits and the possible effect on thedata for this case:

*_ ft^»

frffl*

/^Â. JV#/>7— -

_»k*. fC/jw^^d, m

. 1.J

(ft .7 / e vCu_ "ffc". K X 3V n-

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Ass**.**,**,*. uiiU. A4i.t

/a

Reviewed by:Phone:Date:

PAGEDATA QUALIFIERS

Contractor: K. Case /


( Vrf/K

Aon£j_ i&rQc,«V»J-fcl Us.'-A +ft,3 69

a. A-**

i ^(^v^KjLti

WA,

JJAxi

/ •_L&) >tLO^ rO.C. /

Reviewed by:Phone: ^^Date:

DATA QUALIFIERSPAGE £_ OF *)

Contractor: | Case //</?3/y2.3/i /

Below Is a sunmary of the out-of-control audits and the possible effect on thedata for this case:

. trvi * g. .1

ca .c . l.w>>j.

T ^tf^ / L>o

A_ c. 4-ij 1^0 3 .

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(/£"Tk^ At^^f I."AA( r^-fuf -t S fcv* -fK»3

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^ l/Ar. i/<3LT3 - 83 o

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

. ,*.-> /H**l rv**TILE HSL COMPOUNDSCAS£/SAS i //V^S/^73' * CONTRACTOR

PAGE OF

nstrument # 'DATE/TIME:

IChloromethaneIBromomethanejVinyi ChlorideiChloroethaneIMetnylene Chloridecetone

iCarbop nisuifioe11,1-Dichioroethanell.l-nichioroethene|Trans-l.?»D1chloroethene

j l^Z-D^cnioroetnaneII .1.1-Tr-ichlorciethane

Tetracnlorvde[ V i n y l Acetate

115iTrlcMoroethene

U.l.Z-TrycmoroethaneBeizene

I Z-Cnioroetn_v1 vinyl ether

l,!,Z.Z-TetracnioroethanejTc.uene

AFFECTEDSAMPLES:

InU* Cil .*1 /«'«*

5D

51

Cont. Cal

RF ID

1'

LC

Cont. Cal.

Wi*

'*

PK

fi Aw

Coni. Cal

*£»TIF f

'

JU1

'

X

Oo

^Jftjg.i (jJ Of /ft

bJ 6ft

Cont. Cal7l

'

10

CAui

I

nnfcftLO

Ul,-.\. > 17»*-**^ ^^

* These flags should be applied to the analytes on the sample'data sheets.

UNITE" STATES ENVIROHHEPfTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDSCAS£/SAS $ JifTSy V23j g1 CONTRACTOR

PAGE J. OF 0

Instrument * tl.DATE/TIME;

IChlorometnaneBroffiomethaneVinyl ChlorideChloroethaneMethyiene ChlorideAcetoneCarbon Pisulfide1,1-DichloroethaneLl-OuMoroetheneTrans-l.Z-O^chloroetheneCh'iO*OformZ-5utanon^l.Z-D-'Chioroetnane1 ,1,1-TrichioroethaneCarDO" Tetrachlor^devn\i Acetatep. ro~ 3 „ * Cni oroê* nans1 mfc"»*ChioroDropane

iTra^s™ 1 »3~Dichiorop rope^ eTricMoroetheneP • oroôch l oromet hane1 ,l.Z-TrichloroetnaneBenzeneC* S-l , 3-3' chl oropropene2-Chioroetnviv!nyi etherSro^rÔ""f i-M&;«v i_2-Pe"tanone2-He*siDr.eTefachloroetnene1,1 ,2,2-TetrachloroethaneTc'ueieCnlo*ODe r-zeneEtnyioerzenej t V *C^ S

fP— ft V l C C

o.-;-Xyieief9

AFFECTEDSAMPLES:

Rev'ewe- 's /. / /Initials/Date: -^ . 7 ^t

./, . •

Inl^-iRF', t^j

J2*/<IJ3c<4C>

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* These flags'should be applied to the analytes on the sample data sheets.*

For reporting reaulta tr *«o ttOA, tae following eoatraot apeelflequaliflera are to bo uaed. The arren qualifier* defined belowSB* aubjoet to aodifieatloa by the laboratory. Up to fivequaliflora aay bo roportod oa Fora X for oaoaThe aewea PA*deflnod foui&ftora to DO uaed oro aa followa:

0 r Indleetoa uuajimim! «M o&Alyzod for but not dotootod. thoooaplo qu«ntltatlott Halt oust bo oorrootod for dilution oadfor porooat •oloeuro* For ouaplo, 10 V for pboaol la mtor Iftho Maplo ft nil olioao to tho protoool-opoclflod flaol oluao.Zf a 1 to 10 dllutlott of oxtraet la aoooaaary, tho roportodHalt la 100 V. For * aoll aaaplo, tho Tmloo aoat Alia boadjuttod for porooat •olatoro. for omoaplo, If tho aaaplo bad24% •olataro «nd a 1 to 10 dilution faotor, tho aaaplofoantltatloa Halt for pboaol (330 V) would bo oorrootod to:

and df • dilution faotorat 24% aoiatura, 0 *

100

- 0.7«100

•MO ™ x 10 - 4300 O.7*

roundod to tho approprlato•Ipalfloaat flfuroa

vaibor of

C -

For aoll aaaplea aubjoated to CPC elean-up prooedurea. the C&QLla alao nultlpUod by 2. to account for the fact that only halfof tho extract la recovered.Xndlaateo an oatlaatod value. Thia flag la uaed either whenoatiaatiag a aonaoatratloa for tentatively Identified compoundswhore a 1:1 reapoaae la aaauaed, or waea the naaa spectral dtta.indicate the pveaenaa of a oonpound that aeetj theidentification criteria but tho result la leaa th«a the aaapleojuaatltatioa Unit but greater then aero. For exaaple; if theoeaple *uantitatien Halt la 10 ug/L, but a concentration of 3ug/L la calculated, roport it aa 3J. Tho aaaple ouaatltatlon"Ttifi aii•! \m afljinrod ffeir lull <niittta ami r»*»—» «>t«gnr»aa dlaouaaed for the V flag, ao that If a aaaple with 24%aolature and a 1 to 10 dilution faotor baa a calculatedconcentration of 300 ug/L and a aaaple oîantltation Halt of430 ug/kg. roport the aoneontratlea aa 300J oa Fora X.

This flag applloa tat poatleldo reaulta whore tho Identificationhaa been ooaflcaed by GC/KS. Single eeaponent poatieideang/ul in tfw final extract shall bo eoafiraed by 6C/MS.

B*29 2/88

ft • Taia flag ta used vfaa* the aaalyto la fouad ia tbo aaaoeiatedblank aa vail aa la tbo aaaplo. It ladioataa pooalblo/^robabloblaak oontiafna'tjoa and vans tba data user to tako approprlatoaction. Tbla flag auat bo used for a TIC aa voll aa for ap*sici'vely Idoatlfiod tCL •••gunnj.

trations exceed theThia fl^g ideatifiaacalibration reage of tbo CC/HS laatcaaeat for that apeeificaaalyala. Thia flag *ill as£ apply to poctieidaa/TCla oaalyxodby CC/IC aetheds. Zf one or acre snojpuimdi have a responsegreater then full Male, the sample or extract •oat bo diluted•ad re-anclyxod •••gliding Co the •pooifjaationa Sa ftthibit D,All ayah MOT •!••*• vtth a response greater then full cedeaheuld have the •eojssoj«sclsu flagged with an *1* en the Tora Ifor the origiaal aaalTtla. If the dilution of the extract

balav t« aalttrairosulta of both aaalyooa shall bo roportod oa aaparato Tetbo fora I f or «BO fUatod aaapU aball bav* tbo •&!.• auf f ixappoadod to tba aaojplo «uob«r. VOTX: for total xyl«t»«, «h« :rthroo laoaora aro fttiatifiod aa two poaka, th« ealibrotionrang* of •«*! *>«V aboold bo ooaaidorod ooparatalj, o.g. , adllu&td aaalysia ia U£ roquirod for total xyl«n«« mloas th»

tratioa of ottaar poak ooparataly oaeooda 200 ug/L.

Thia flag ideatifiaa all oe •pounds identified ia aa aaelysia ata secondary dilution footer. If a aaaple or extract iareanalyzed at a hitter dilution factor, aa ia the "I* flag

the *OL* auffix ia appended to the aanple nusber on th*Tora I for ô diluted aaoale, and *H concentration valuesreported on that fora 1 aro flagged vith Ac •&* flag.

Thia flag indicates that a TICaloal-eondtnsation product.

ia a auapoctod

Other specific flags aay bo required to properly definerooulta. If used, they auat be fully deacribed and suchdescription attaahod ta the Saaple Data Suojaary Package and *.Case Kerrative. Begin by using *XV. If aore than one flag &.

M<qualifiers are roojuirod for a aanple result, uce the "X" fla;to •osribiao aoveral flaga* aa aoodad. for iastancot the *X*flag might •sailLas the *A*. "*•. aad "D* flags for aooje 00091

ia tocprossly prohibited. 11.. •.«h«n thoy aro also dotoctod ia -s-i

»iaatiOB of fiftga •BO*ilaaata aro flaggod •§

aaaplo.

Tf analysts at two different dilution fhctors OTO roûirodExhlMt D>, foils* thft data reporting inatruetioac glvtn in Kxh:9 a*d vlth tbo •&• «ad.*t* flags above.

DAR 0 a 1* CENTRAL REGIONAL LAUORAT^'W SAMPLE DATA REPORTO S)*?4(/1 ORGANICS/IK .iGANICS3t//*tX! FM*V 577 J TH|S FORM |S j0 BE USED pon S^MPLES SENT TO CONTRACT ONLY

CASE NUMBEH/SAS No

SUPEHFUNO DO NUMBER

ACIIVIIY NUMBER

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CASE NARRATIVE — SAS * 4231 ECASE * 0000 SDC « EAU60

CONTRACT tt SAS4231ECompuChem Laboratories, Inc.

Sample Number*: EAU60, EAU61, EAUS2, EAU63, EAU64, EAU6S, EAU66, EAU&7,EAU6S, EAU69, EAU70, EAU71, EAU72, EAU73, EAW74, EAU75,EAU76, EAU77, EAU78, EAU79

This Case consists of twenty water samples analyzed for low detection l i m i tvolatiles. The samples arrived intact in a sealed shipping container withTraffic Reports, Chain-of-Custody (COO Records, and sample tags on March£ and 3, 1989. Federal Express was the courier from the client to CompuChemChem Laboratories, Inc. The sample number* on the containers matched theTraffic Reports. All sample* were logged into CompuChem's Laboratory Manage-ment System and were stored at 4*C.

V» PILES;All samples for volatiles were analyzed within holding time requirements.Most instrument blanks contained low levels of 1-? Target Compound List (TCL)volatiles. Tentatively Identified Compound* (TIC) were not detected in thein»trument blank*. The blank contaminant* were well within the contract QA/QCcriteria. Uith the exception of EAU64, all samples contained low to mediumlevels of 1-14 TCL volatiles. The multipoint was exceeded for some compoundsin five of the samples. Consequently, we havo reported the undiluted (orleeser dilution) and the diluted analyse* for the following samples: FAU6SREM.t;l dilution), EAW67PE MOOM dilution), EAU70RE <3. 61 1 dilution), EAU7IPE(2.2:1 dilution), £AU72RE (27.8:1 dilution). A 4M dilution was performedfor EAU69. Nine of the samples contained 1,I,2-trichloro-1,2,2-trifluoroethanein the NBS Library Search. This compound is known to be a common lab contam-inant. It is used as a solvent in Oil and Grease extraction* in a separateOrganic* Characterization Laboratory within CompuChem. The Volatile GC/MSLaboratory has an isolated ventilation system/ ami the lab is under positiveair pressure to prevent contaminants frost entering the lab through doorway*.The air handling system also contain* an activated carbon filter that remove*volatile organic contaminant* from the outside air. Various Freons are alsoused in refrigeration units and as aerosol propellants. The same compoundwas detected in the associated blank, but not at sufficient concentration torequire a Library Search. Nevertheless, the compound ha* been flagged in thesample data with a "B", denoting it* presence in the blank. The compoundshould be considered a lab contaminant not native to the as-received sampleEAU67 contained 5 lIC's, and the remaining samples did not contain TIC's.CompuChem follow*-] the EPA rounding convention for CRQL's, and the volatile

fraction was reported to on* significant figurt when the values were b#lowten. "J" values were reported down to 1/2 of ih* modified CROC's. Th*word "no" on the quantitation rtport n*ani tho compound was not found orth* compound was !*«« than 1/2 of th» CRQL. All criteria w»r« mat for th*initial and continuing calibration standard*) th* surrogate standards, andth* internal standards. Th* matrix spike/matrix spik* duplicat* (MS/USD)g*n*rat*d from EAU61 had good spik* r*cov*ri*s.

Rslaas* of th? data contained in this hardcopy data package has been authorizedby th* Laboratory Managvr or his d*sign*e» as v*rifi*d by th* following signa-ture.

Becky C. Linvill 3/21/89Technical Reviewer

Note: This report is paginated for reference and accountability in decreasingnutterical sequence.

2AWATER VOLATILE SURROGATE RECOVERY

Lab Name: CQMPOCHEM LABS contract: SA54231B

Lab Cod*: CQMPU Case No.: OQQQ SAS No.: 4231E SDG No.EAW&O

010203040506070809101112131415161718192021222324252627282930

EPASAMPLE NO.

EAW60EAH61EAW62EAW62REEAW63EAW64EAW65EAW66EAW67EAW67REEAW68EAW69EAW70EAW70REEAW71EAW71REEAW72EAW72REEAW73EAW74EAW75EAW76EAW77EAW78EAW79EAW61MSEAW61MSDVBLKBOVBLKPRVBLKXJ

SI(TOL)I

1081081041031079610810310110310710410295110107100 .94102103105107104108108103106101103101

32(BFB) I

9394939597101931019697919889899295979197991021031011051009394979894

S3(DCE)|

929290991011009610591100991019085951009987100105107110.108'1101059698999998

OTHER TOTOUT

000000000000000000000000000000

QC LIMITS81 (TOL) - TolU«IM-d* ( 88-110)82 (BFB) * Bromofluorobenzena ( 86-115)S3 (DCE) - l,2-Dichloro«than«-d4 ( 76-114)

I Column to b« u*«d to flag recovery value*

* Values outbid* of contract required QC limits

D Surrogates diluted out

pag« 1 of 2FORM II VOA-1 1/87 Rev.

SAMPLE SUMM8RV

2AHATER VOLATILE SURROGATE RECOVERY

Lab Name: CQMPPCHEM LABS________ Contract: SAS4231E.

Lab Coda: coMPU CAM No.: QQQQ SAS No.: 4231E SDC No.: EAW6Q

01020304

EPASAMPLE NO.

VBLXPOVBLKXLVBLKXNVBLXXQ

SI(TOL)I

10110210798

S2(BFB) *

969610292

S3(DCE)I

9992108101

OTHER TOTOUT

0000

QC LIMITSSI (TOL) - Tolu*n«-d8 ( 88-110)32 (BFB) - Bronofluorob«nz*n* ( 36-115)S3 (DCS) - l,2-Dichloro«than*-d4 ( 76-114)

I Column to ba u»ad to flag r*cov*ry values

* Values out»id« of contract required QC limits


pag« 2 of 2FORM II VOA-1 1/87 R«v,

SffMPLE OPTP SUMMPRY

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Nan«: CQMPUCHEM LABS________ Contract: SAS4231E

Lab Cod«: CQMPU Castt No.: OOQQ SAS No.: 4231E SDG No.: EAW60

Matrix Spiks - EPA Saapl* No.:

COMPOUND

l, l-Dichloro«th«n«____Trichloro«th«n«BanzanaTolu«n«Chlorob«nz«n« ,

SPIKEADDED(ug/D

12.512*512.512.512*5

SAMPLECONCENTRATION

(ug/D0001.650

MSCONCENTRATION

Cug/L)16.314.413.015.413.2

MSt

REC #

130115104110106

QCLIMITS

REC.

61-14571-12076-12776-12575-130

COMPOUND

1 , l-Dichloro«th«n« ___Trichloro«th«n«B«nz«n«ToluanaChlorob«nz«n«

SPIKEADDED<u*/L)

12.512.512.512.512.5

MSDCONCENTRATION

(ug/L)

16.414.613.315.613.7

MSD%

REC #

131117106112110

%RPD «

-1-2-2-2-4

QC L3RPD

1414111313

CMITSREC.

61-14571-12076-12776-12575-130

I Column to b« u»«d to flag r«cov*ry and RPD valu*» with an a»t«ri»)c

* Valu«« out«id« of QC limits

RPD: _Q out ofSpik* R«cov«ry: _

out»id« limitsout of 10 out*id* limits

COMMENTS: CLP ,4231,E£AW60,-BAW6,LOW,WATER,247680,PEST, ,

FORM III VOA-1 1/87 Rev,

SBHPLE SUMMPRV ~ \->

4AVOLATILE METHOD BLANK SUMMARY

Lab Naina: gQMPOCHEM LABS________ Contract: SAS4231E

Lab Coda: coma Casa No.: OQQQ SAS NO.: 4231E SDG No.: EAWSO

Lab File ID: CS890306B12 . Lab Sample ID: VBLKBQ____

Data Analyzed: 03/06/89 Time Analyzed: 1653

Matrix: («oil/vater) WATER Level:(low/mad) LOW

Instrument ID: 12

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSO:

0102

EPASAMPLE NO.

EAW63EAW65

LABSAMPLE ID

247868247870

LABFILE ID

CR047868B12CN047870B12

TIMEANALYZED

18521802

COMMENTS: CLP , , , , , , ,PEST,BLANK,TUNE: 0012 030689 1401

page 1 of 1FORM IV VOA 1/87 Rav,

SffMPL£ P8T0 SUMMPRV


Lab Naaa: eoMPUCHEM LABS________ Contract: SAS4231E

Lab Coda: CQMPU Caaa Ko.: QQQQ SAS Ko.: 4231E SDG No.: EAW60

Lab Fila ID: CB89Q307C12 Lab Sanpla ID: VBLKPRData Analyzad: 03/07/aq Tina Analyzad: Q249

Matrix: (»oil/watar) WATER Laval:(low/mad) LOWInatruaant ID: 12

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD:

010203

EPASAMPLE NO.

EAW64EAW66EAW67

LABSAMPLE ID

247869247S71247872

LABFILE ID

CN047869A12CN047871A12CR047872C12

TIMEANALYZED

090408180408


paga 1 of 1FORM IV VOA 1/87 Rev,

SPMPLE para SUMHBRV 13


Lab Nan*: CQMPPCHEM LABS________ Contract: SAS4231E

Lab Cod*: COMPO Case No.: QQQQ SAS No.: A231E SDG No.: EAW60

Lab Fil« ID: CC89Q3Q7B12 Lab Sampl* ID: VBLKXJ_____Data Analyzed: D3/Q7/B9 Tim« Analyzed: ITQS

Matrix: («oil/vat*r) WATER L«v«l:(low/mad) LOWInstrument ID: 12


010203040506

EPASAMPLE NO.

EAW68EAW70EAW70REEAW71EAW71REEAW72

LABSAMPLE ID

247873247875247875247876247876247877

LABFILE ID

C2R47873C12CN047875B12CR047875B12CN047876B12CR047876B12CN047877B12

TIMEANALYZED

012918192059191221592246


paga l of lFORM IV VOA 1/87 Rav,

SffHPLE OPTff SUMMBRV 15


Lab Nam«: CQMPPCHEM LABS_______ Contract: SAS4231ELab Cod*: COMPP Cas« No.: OOQQ SAS No.: 423IE SDG No.: EAW6Q

Lab Fil« ID: cca903oaei2 Lab Saapla ID: VBLKPQ___Data Analyzed: 03/oa/aq Tina Analyzed: Q7Q8Matrix: («oil/wat«r) WATER Lav«l:(lov/aad) LOWInstrument ID: 12

THIS METHOD BLANK APPLIES .TO THE FOLLOWING SAMPLES, MS AND MSD:

01020304050607

EPASAMPLE NO.

EAW73EAW74EAW75EAW76EAW77EAW78EAW79

LABSAMPLE ID

247878247879247880247881247882247883247884

LABFILE ID

CN047878A12CN047879A12CN047880A12CN047881A12CN047882A12CN047883A12CN047884A12

TIMEANALYZED

1402085509461030111512021248


pag« 1 of 1FORM IV VOA 1/87 Rev.

OPTff SUMMBRV


Lab Nam«: eQMPUCHEM LABS________ contract: SAS4231E

Lab cod«: CQMPO cam* No.z Qooo SAS MO.: 4231ELab Fila ID: cea903oaBi2 Lab Sampla ID: VBUOTT.Data Analyzed:

SDG NO.: EAW60

03/08/89

Matrix: (»oil/wat«r) WATERin»trun«nt ID: 12

Tina Analyzed: 2149L«v«l:(low/mad) LOW

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND MSD

010203040506

EPASAMPLE NO.

EAW60EAW61EAW62EAW72REEAW61MSEAW61MSD

LABSAMPLE ID

247679247680247867247877247681247682

LABFILE ID

CR047679C12C2R47680C12CR047867B12CR047877B12CN047681C12CN047682C12

TIMEANALYZED

03590448OOCO230505330618

COMMENTS: CLP ,,,,,, ,PEST,BLANK,TUNE: 0012 030889 1*22

pag« 1 of 1FORM IV VGA 1/87 Rev.

SBMPLE OPT ft SUMMPXV


Lab Ham*: CQMPPCHEM LABS_______ Contract: s>5423iELab Coda: COMPP Casa No.: QOQQ SAS No.: A231E SDG No.: EAWSQ

Lab Fila ID: CC89Q3Q9B12 Lab Sanpla ID: VBLKXNData Analyzed: 03/09/89 Tim* Analyzed: 1914Matrix: (»oil/vatar) WATER Lava!:(low/mad) LOW

Instrunant ID: 12


0102

EPASAMPLE NO.

EAW67REEAW69

LABSAMPLE ID

247872247874

LABFILE ID

C3R47872C12C4R47874C12

TIMEANALYZED

03530119


paga 1 of 1FORM IV VOA 1/87 Rav,

S&HPLE DPTff SUMMQRV


Lab Namt: COMPUCHEM LABS_________ Contract: SAS4231E

Lab Cod«: CQMPO Ca»« No.: OQQO SAS No.: 4231B SDG No.: EAW6Q

Lab Fil« ID: cca903i3Bia Lab Sampl* ID: VBLKXQDat* Analyzed: 03/13/89 Tim* Analyzed: aoSA

Matrix: (»oil/wat«r) WATER L«v«l:(low/mad) LOW

In«trun«nt ID: 12


01

EPASAMPLE NO.

EAW62RE

LABSAMPLE ID

247867

LABFILE ID

C3R47867B12

TIMEANALYZED

2202

COMMENTS: CLP , , , , , , ,PEST,BLANK,TUNE: 0012 031389 1*23

pag« 1 of 1FORM IV VOA 1/87 Rev,

SBMPL£ SUMMPRV


EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS__________

Lab Code: CQMPU Case No.: OQQQ


Sample wt/vol: 20.Q (g/mL) ML


% Moisture: not dec. ___


VBLKBOContract: SAS4231E

SAS No.: 4231E SDG No.: EAW6Q

Lab Sample ID: VBLKBQLab File ID: CB890306B12

Date Received: ______Date Analyzed: Q3/Q6/89

Dilution Factor:


74-87-3-——--——Chlorome thane__________74-83-9™--——•Bromouethane__________75-01-4—•————Vinyl Chloride_________75-00-3——————Chloroethane_________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform __________107-06-2———-—1,2-Dichloroethane______78-93-3————™2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4-—————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-i,3-Dichloropropene__79-01-6-—————Trichloroethene_______124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane____71-43-2-—-———Benzene______________10061-02-6————Trans-l,3-Dichloropropene—75-25-2———-—Bromofon*_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4——————Tetrachloroethene_______79-34-5——————1,1,2,2-Tetrachloroethane^108-88-3——————Toluene______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

10.80.912510.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev,

SBMPLE QQTQ SUMM8RV


EPA SAMPLE NO,

Lab Name: CQMPUCHEM LABS________

Lab Code: COMPU Case No.: QQQQ

Matrix: (soil/water) WATEfr

Sample wt/vol: 20.0 (g/mL) HL__

Level: (low/med) LOW% Moisture: not dec. ___


Number TICs found: _0

VBLKBOContract: SASA231E

SAS No.: 4231E SDG No.: EAW60

Lab Sampl* ID: VBLKBQ___Lab Fil« ID: CB89Q3Q6B12

Data R«c«iv«d: ______


Dilution Factor: *^Q

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L


FORM I VOA-TIC 1/87 Rev,

SQMPLE &OTB SUMMBRV 1 9


EPA SAMPLE NO.

VBLKPRLab Mama: COMPUCHEM LABS________ Contract: SASA231E

Lab Code: CQMPU Can No.: QQQQ SAS No.: *231E SDG No.: EAW6Q

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/mL) ML


t Moisture: not d*c. ___


Lab Sample ID: VSLKPR

Lab File ID: CB89Q307C12

Oat* Received: ______

Data Analy.zad: 03/07/89

CAS NO. COMPOUND

Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L ft*

74-87-3——————Chloromethane__________74-83 -9 ———-——Bromomathana___________75-01-4——————Vinyl Chlorida_________75-00-3-™—-—Chloroethane_________75-09-2——————Methylene Chloride______67-64-1——————Acatona______________75-15-0——————Carbon Di»ulfide_______75-35-4——————1,1-Dichloroathana______75-34-3——————1,1-Dichloroathana______540-59-0——————1,2-Dichloroathana (total).67-66-3™--——-Chloroform __________107-06-2—————1,2-Dichloroethane_____78-93-3™————2-Butanone___________71-55-6——————1,1,1-Trichloroathane____56-23-5——--——-Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4—————Bromodichloronathana____78-87-5—————-1,2-Dichloropropana_____10061-01-5———-cia-l,3-Dichloropropana__79-01-6——————Trichloroathana_______124-48-1—————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroathana____71-43-2——————Ban z ana __________10061-02-6-™—Trans-l,3*Dichloropropene_75-25-2——————Bromoform,_____________108-10-1——————4-Mathyl-2-Pantanona____591-78-6——————2-Haxanona____________127-18-4—————Tatrachloroathana______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene______________108-90-7—————Chlorobanzana__________100-41-4——————Ethylbanzana__________100-42-5—————Styrana_____________1330-20-7—————Total Xylanaa__________107-02-8—————Acrolain____________107-13-1—————Acrylonitrila_________

l0.80.912210.90.90.90.9141111111111121110.910.9112

2026

FORM I VGA 1/87 Rev,

SffMPLE SUMMBRV 1 7


EPA SAMPLE NO.

Lab Nam«: CQMPUCHBM IABS________

Lab Cod«: COMPU Cas« No.: OQOQ

Matrix: (soil/watar) WATERSample wt/vol: 20.0 (g/mL) ML

L*v«l: (low/m«d) LOW

% Moistura: not dac. —__


Numbar TICs found: _0

VBLKPRContract: SAS4231E

SAS NO.: 4231E SDG No.: EAW6Q

Lab Sampl* ID: VBLKPR

Lab Fil* ID: CB890307C12

Data Racaivad: ______Dat* Analyzed: 03/07/89

Dilution Factor:



FORM I VOA-TIC 1/87 ReV,

SffMPLE Of) TO SUMM8RV


EPA SAMPLE NO.

Lab Name: COMPUCHEM IABS_______Lab Code: COMPU Case No.: QQQQMatrix: (soil/water) WATERSample wt/vol: 20.Q (g/mL) ML




VBLKXJContract: SAS4231E


Lab Sample ID: VBLKXJ

Lab File ID: CC89Q3Q7B12

Data Received: .______

Data Analyzed: Q3/07/89

GAS NO. COMPOUND

Dilution Factor:


74-87-3———-———Chloromethane__________74-83-9—————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3———————Chloroethane___________75-09-2——————Methylene Chlorid*______67 -64-1——————Acetone______________75-15-0——————Carbon Di»ulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total),67-66-3—————-Chloroform___________107-06-2—————1,2-Dichloroethane______78-93-3——————2-Butanone_____________71-55-6———————1,1, 1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4-—————Bromodichlorome thane____78-87-5—————- 1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1————-Dibromochloronethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene_______________10061-02-6———Tran«-l,3-Dichloropropene_75-25-2——————Bromofonn____________108-10-1—————4-Methyl-2-Pentanone____591-78-6———:——2-Hexanone____________127-18-4————-Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3————-Toluene_______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5————styrene______________1330-20-7————Total xylenes_________107-02-8————-Acrolein_____________107-13-1—————Acrylonitrile_________

10.80.912210.90.90.90.9141111111111121110.910-91122026


S0MFLE DGTff SUMMPRY


EPA SAMPLE NO.

Lab Nan*: COMPTJCHEM IABS_______Lab Cod«: CQMPU case No.: QQQQ

Matrix: (»oil/wat«r) WATER

Sampl* wt/voli 20.0 (g/mL) ML

L*v«l: (low/ra«d) LOW

% Moi»tur«: not d*c. ___Column (pack/cap) PACK

Numb«r TICs found: _Q

VBLKXJContract: SAS4231E


Lab Sampl* ID: VBLKXJ

Lab Fil« ID: CC89Q3Q7B12

Dat« R«c«iv«d: ______

Dat« Analyzed: 03/07/89I ,

Dilution Factor: ^r.o___




S8MPLE OOTP SUMMQRV


EPA SAMPLE NO.

Lab Name: CQMPUCHEM LABS_________

Lab Code: CQMPU Case No.: QQQQ


Sample vt/vol: 20.0 (g/mL) ML




CAS NO. COMPOUND

VBLKPOContract: SAS4231E

SAS NO.: 4231E SDG NO.: EAW6Q

Lab Sample ID: VBLKPOLab File ID: cca9Q308Ci2

Data Received: ______

Date Analyzed: 03/08/89//Dilution Factor: x. o___

CONCENTRATION UNITS:(ug/L or ug/Kg) uc/L

74-87-3——-——Chloromethane_________74-83 -9—————Bromomethane_________75-01-4———————Vinyl Chloride ______75-00-3———————Chloroethane _______75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0——————Carbon Diaulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total),67-66-3™——-—Chloroform___________107-06-2—————1,2-Dichloroethane______78-93-3——————2-Butanone ________71-55-6——————1,1,1-Trichioroethane___56-23-5—————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————Bromodichlorome thane____78-87-5—————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6—————-Trichloroethene_________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Banzana__________10061-02-6————Trans-1,3-Dichloropropene_75-25-2——————Bromoform________,_____108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene____\_________108-90-7——-——Chlorobenzene________„100-41-4—————Ethylbenzene__________100-42-5—————Styrene______________1330-20-7—————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.912410.90.90.90.9141111111111121110.910.9112

2026


SQMPLE OffTff SUMMBRV 1 1


EPA SAMPLE NO,


Lab Code: CQMPU Case No.: QOQQ

Matrix: (moil/water) WATERSample wt/vol: 20.0 <g/mL) MLLevel: (low/med) LOW

% Moisture: not dec. .__


Number TICs found: 0

VBLKPOContract: SAS4231E

SAS No.: A231E SDG No.: EAW60

Lab Sample ID: VBLKPo

Lab Fil« ID: CC8903Q8C12

Dat« R«c«iv«d: ______

Dat« Analyzed: 03/08/89\/

Dilution Factor: y.o___


, IffGAS NUMBER COMPOUND NAME RT EST. CONC. Q


1O

1AVOLATILE ORGANXCS ANALYSIS DATA SHEET

______ Contract: SAS4231E

EPA SAMPLE NO.


Lab Coda: CQMTO Case No.: QQQQ



Laval: (low/mad) Low

* Moisture: not dac. __


VBLKXL

SAS NO.: 423IE SDG No.: EAW60

Lab Sample ID: VBLKXL____

Lab File ID: CC8903Q8B12

Data Racaivad: ______


Dilution Factor: 4<0____


74-87-3——————Chloronatharia ________7 4 -8 3-9——------ Bromomathana__________75-01-4———————Vinyl Chloride_________75-00-3——————Chloroethane__________75-09-2——————Mathylane Chloride_____67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene_____7 5-3 4 -3™———1, l-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform ___________107-06-2——————1,2-Dichloroethane______78-93-3—-———2-Butanone___________71-55-6——————l, 1, l-Trichloroethane___56-23-5——————Carbon Tatrachlorida____108-05-4—————vinyl Acetate_________75-27-4-—————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5——-—ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——-———Benzene_______________10061-02-6———-Tran»-l,3-Dichloropropene_75-25-2———————Bromoform ____________108-10-1——————4-Mathyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4————Tetrachloroethene______79-34-5——————i ,1,2,2-Tetrachloroethane__108-88-3——————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrena______________1330-20-7—————Total Xylene*_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.912710.90.90.90.9141111111111121110.910.9112

2026


SQMPLE


EPA SAMPLE NO,

Lab Name: COMPtlCHEM LABS_________

Lab Cod*: CQMPU Case No.: 0000


Sample wt/vol: 20.o (g/mL) ML


% Moieture: not dec. __...


Number TICs found: _Q

VBLKXLContract: SAS4231ESAS No.: 4231E SDG No.: EAW6Q

Lab Sample ID: VBLKXL

Lab File ID: CC89Q3Q8B12

Date Received: ______

Date Analyzed: Q3/Q8/89I;

Dilution Factor: *.Q




SQMPLZ


EPA SAMPLE NO.

Lab Name: CQMPOCHEM LABS_______Lab code: CQMPU case No.: OQQQ



% Moisture: not dec. ____


VBLKXQContract: SAS4231E

SAS NO.: 4231E SDG No.: EAW60

Lab Sample ID: VBLKXOLab File ID: CC89Q313B12

Date R«c«ived: ______


Dilution Factor: 4^0___


74-87-3-————Chloromethane.,_________74-83-9—————Bromomethane__________75-01-4——————vinyl Chloride________75-00-3™————-Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——:———1,2-Dichloroethene (total).67-66-3——————Chloroform _________107-06-2——————1,2-Dichloroethane______78-93-3———™2-Butanone___________71-55-6——————l, l, 1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4———————Bromodichloromethane_____78-87-5—————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1-—————Dibromochlorone thane_____79-00-5———————1,1,2-Trichloroethane____71-43-2—————'-Benzene______________10061-02-6———Trans-l,3-Dichloropropene_75-25-2—————Bronoform____________108-10-1———:——4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18 -4 -————Tetrachloroethene______79-34-5——————l ,1,2,2-Tetrachloroethane_108-88-3—————Toluene ________108-90-7-————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes_________107-02-8——————Acrolein__________•107-13-1—————Acrylonitrile_________

l0.80.912210.90.90.90.9141111111111121110.910.91122026


DBTB SUMMBRV


EPA SAMPLE NO

Lab Name: CQMPUCHEM IABS_________



Sample vt/vol: 20.0 (g/mL) MLLevel: (low/med) LOW



Number TIC* found: _Q

VBLKXQContract: SASA231E


Lab Sampla ID: VBLKXO

Lab Pile ID: CC89Q313B12Data Received: ______

Date Analyzed: 03/13/89

Dilution Factor:


ti*GAS NUMBER COMPOUND NAME RT EST. CONC. Q


SPMPLE OQTP SUMMPRV



EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS_________

Lab Code: COMPU Cast No.: OQQQ

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/mL) MLLevel: (low/med) LOW



VBLKXN


Lab Sample ID: VBI1KXN

Lab File ID: CC8903Q9B12


Data Analyzed: 03/09/89(

Dilution Factor: 4/.Q____

GAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3———-——Chloromethane_________74-83-9——————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————l, l-Dichloroethene______75-34-3——————l, l-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform ________107-06-2—————1,2-Dichloroethane_____78-93-3—•—•——2-Butanone___________71-55-6——————l, l, 1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6———-——Trichloroethene________124-48-1-——---Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2—•————-Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_7S-25-2———————Bronoform __________108-10-1——————4-Methyl-2-Pentanone____591-78-6————--2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene _______108-90-7-————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-4 2 -5—————Styrene_____________1330-20-7—————Total Xylenee_________107-02-8—————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.912710.90.90.90.9141111111111121110.910.91122026


S8MPLE £>0TP SUMM0RV

IEVOLATILE ORGANZCS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO

Lab Name: gOMPUCHEM LABS_________

Lab Code: CQMPO case No.: 0000Matrix: (soil/water) WATERSample wt/vol: 20.Q (g/nL) ML


% Moisture: not d*c. ___Column (pack/cap) PACK

Number Ties found: _0

VBLKXNContract: SAS4231ESAS No.: A231E SDG No.: EAW6Q

Lab Sample ID: VBLKXNLab File ID: CCS9Q3Q9B12

Date Received: ______Date Analyzed: 03/09/89

Dilution Factor:




SQMPLE OPTP SUMMPRV


EPA SAMPLE NO.

Lab Nan*: COMPOCHEM LABS________

Lab Coda: COMPU Gas* No.: QQQO

Matrix: (soil/water) WATERSample wt/vol: 20.Q (g/mL) ML

Level: (1ow/med) LOW

% Moisture: not dec. __


EAW60Contract: SAS4231E


Lab Sample ID: 247679 ____

Lab File ID: CRQ47679C12



CAS NO. COMPOUND

Dilution Factor:


itfQ

74-87-3——————Chloromethane_________74-83-9———-——Bromome thane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone______________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total),67-66-3——————Chloroform___________107-06-2—————1,2-Dichloroethane______78-93-3—————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-i,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——•————Benzene_______________10061-02-6————Tran«-l,3-Dichloropropen«_75-25-2——————Bromoform____________108-10-1—————4-Methyl-2-Pentanona____591-78-6—————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5-——————l,l,2,2-Tetrachloroethane_108-88-3———————Toluene _____________108-90-7—————Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7—————Total Xylene«_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.910.9510.930.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev

SP/TPZ.F OffTff SUHHQRV


EPA SAMPLE NO.

Lab Name: CQMPUCHEM IABS ____Lab Code: CQMPU Case No.: QQQQ



\ Moisture: not dec. •


Number TICs found: _p.

EAW60Contract: SAS4231ESAS No.: 4231E SDG NO.: EAW6Q


Lab film ID: CRQ47679C12


Data Analyzed: 03/09/89I

Dilution Factor:



FORM I VOA-TIC 1/87 Rev

SAMPLE SUMHQRV

Lab Name:


LABS________ Contract: SAS4231E

EPA SAMPLE NO.

EAW61

Lab Code: CQMPU Caaa No.: oooo

Matrix: (moil/water) WATERSample wt/vol: 20.0 (g/mL) ML

Level: (low/mad) LOW

% Moiature: not dec. __



Lab Sample ID: 247680

Lab File ID: C2R47680C12


Data Analyzed: 03/09/89I

Dilution Factor: .0____

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L If.

74-87-3 —————74-83-9 —————75-01-4 —————75-00-3 —————75-09-2- —67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 ————107-06-2—- —78-93-3— ———71-55-6 —————56-23-5 —————108-05-4— ——75-27-4 —————

10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6 ——75-25-2 ————108-10-1 ————591-78-6 ————

79-34-5 —————108-88-3 ————108-90-7 ————100-41-4 ————100-42-5 ————1330-20-7 ———107-02-8 ————107-13-1 ————

— — Chlo romethane——Bromomethane—— Vinyl Chloride—— Chloroethane___.. .—— Methyl ene Chloride—— Acetone—— Carbon Diaulf ide__ . , „—— 1 r 1-Dichloroethene—— 1, l-Dichloroathane—— 1, 2-Dichloroathana (total) __——Chloroform—— 1 , 2-Dichloroethane.._—— 2-Butanone—— 1 . 1 . 1-Trichloroethane——Carbon Tetrachloride—— Vinyl Acetate—— Bromod ichl oromethane—— 1 r 2-Dichloropropana—— cia-l,3-Dichloropropene— — Tr ichl oroathana— »— Dibronochloroaetharm—— 1 . 1 . 2-Triehleroethana——Benzene— — Tran»-l, 3-Dichloropropana ___——Bromof orm ,„.,_—— «4-Mathyl-2-Pentanone—— 2-Hexanone , ,—— Tetrachloroathane .„.„. ,—— 1 ,1,2, 2-Tetrachloroethane __——Toluene—— Chlorobenzene ,— — Ethvlbenzene—— Styrene—— Total Xylenea—— Acrolein— -Acrylonitrile ,

10.80.912610.90.90.90.9141111111111121110.920.91122026

UUu •u

uuuuuuuuuuuuuuuuuuuuuuuuuuuuu

FORM I VOA 1/87 Rev

SQMPLE DPTP SUHMQRV


EPA SAMPLE NO,


Lab Code: CQMPU Cas* No.: oooo


Sample wt/vol: 20.0 (g/mL) ML


% Moisture: not dec. _





Lab Sample ID: 24768Q

Lab File ID: C2R4768QC12


Date Analyzed: 03/09/89\,Dilution Factor: 4<Q




SQMPLE &PTB SUMMQRY


EPA SAMPLE NO.

Lab Name: CQMPUCHEM LABS_______Lab Code: CQMPU Case No.: 0000


Sample wt/vol: 20 0 (g/mL)

Level: (low/ned) LOW



CAS NO. COMPOUND



Lab Sample ID: 247867____

Lab File ID: CR047867B12



Dilution Factor: Jr.O____


74-87-3——————Chloromethane_________74-83-9——————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1——-——--Acetone______________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3———————Chloroform_____________107-06-2—————-1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane___56-23-5———*——Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————-Bromodichloromethane____78-87-5—-----1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene_________124-48-1—-———Dibromochloromethane____79-00-5——————1,1,2-Triehloroe thane___71-43-2———————Benzene_______________10061-02-6————Trans-l,3-Dichloropropene_75-25-2—————Bromoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone__________•127-18-4—————Tetrachloroethene______79-34-5———————1,1,2,2-Tetr»chloroethane_108-88-3——————Toluene_______________108-90-7-————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—-———Styrene______________1330-20-7—————Total Xylenes_________107-02-8——————Acrolein______________107-13-1——————Acrylonitrile__________

10.8

2621

12010.919440.9242111114113121110.910.90.510.6

2026

JMEUJ


SQHPLE SUHMQffY


EPA SAMPLE NO

Lab Name: CQMPUCHEM LABS_______Lab Code: CQMPU Caee No.: 0000




Number TICs found: _p.




Lab File ID: CRQ47867B12


Date Analyzed: 03/09/89I

Dilution Factor: fr'.o


CAS NUMBER COMPOUND NAME RT EST. CONC. . Q


SQHPLE £>PTt9 SUHHBRV



EPA SAMPLE NO.

Lab Name: COMPUCHBM LABS________

Lab Coda: COMPU Cast No.: 0000

Matrix: (*oil/vat*r) WATERSample wt/vol: 6.5 (g/mL) ML


% Moiature: not dac. ___


EAW62RE



CAS NO. COMPOUND

Lab Fila ID: C3R47867B12

Data Racaivad: Q3/Q3/89

Data Analyzad: 03/13/893,1

Dilution Factor:


74-87-3——————Chloromathana_________74-83 -9——«—- Bromomethane__________75-01-4———————Vinyl Chlorida_________75-00-3———————Chloroethane___________75-09-2——————Mathylana Chlorida______67-64-1———————Acatona________________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroathana______75-34-3——————1,1-Dichloroethane_____540-59-0—————l,2-Dichloro«thene (total)67-66-3—————-Chloroform __________107-06-2—————1,2-Dichloro«thane______78-93-3——————2-Butanona_____________71-55-6———————1,1,1-Trichloroethane____56-23-5-—————Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4——————Bromod ichloronathana____78-87-5——————1,2-Dichloropropane_____10061-01-5————cia-1,3-Dichloropropene__79-01-6—————Trichloroethene_________12 4 -4 8-1-—————Dibromochloromathana____79-00-5——————1,1,2-Trichloroethane___71-4 3 -2——————Benzene______________10061-02-6————Trana-l,3-Dichloropropene_7 5-2 5-2———-——Bromof orm__,____________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanona_____________127-18-4--————Tetrachioroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3—— --——Toluene _______108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-4 2 -5—————styrene______________1330-20-7—————Total Xylenea__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

42272J5.6933

226032133343444434454433333366181

UUDDJyBCTUUDDUDJUUUUUUUDUUDJUUUUUUUUUUUUU


SBHPLE DP TO SUHMBRV


EPA SAMPLE NO


Lab Code: CQMPU Cave No.: OOOQ


Sample wt/vol: 6.5 (g/mL)Level: (low/med) LOW



Number TIC* found: _1

EAW62REContract: SAS4231ESAS No.: 4231E SDG No.: EAW6Q


Lab File ID: C3R47867B12


Date Analyzed: 03/13/89J-/

Dilution Factor:


CAS NUMBER

1.

COMPOUND NAME

LAB CONTAMINANT

RT

13.22

EST. CONC.

22

Q*rjJI _


DOT0 SUHMQRY


EPA SAMPLE NO.


Lab Code: GQMPU Case No.: QQQQMatrix: (soil/water) WATERSample wt/vol: 20.Q (g/mL) ML




CAS NO. COMPOUND







Dilution Factor:


. Q

*Q

74-87-3————-—Chloromethane_________74-83-9——————Bromomethane__________75-01-4——————Vinyl Chloride.;________75-00-3——————Chloroethane__________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform_____________107-06-2——————1,2-Dichloroe thane______78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichlorome thane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dicnloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochlororaethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6———-Trans-l,3-Dichloropropene_7S-2S*2-——————Bromofonn_________108-10-1———-—4-Methyl-2-Pentanone____591-78-6——————2-Hexanone __________127-18-4————-Tetrachloroethene______79-34-5———•———1,1,2,2-Tetrachloroethane_108-88-3--——---Toluene_______________108-90-7——'•——Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_______________1330-20-7—————Total Xylenes_________107-02-8--————-Acrolein______________107-13-1—————Acrylonitrile_________

l0.80.911210.90.90.90.9141111111111121110.920.921

102026


SQHPLE D0TB SUHHBRV 71


EPA SAMPLE NO


Lab Coda: CQMPU Caee No.: QOQQ

Matrix: (soil/water) WATERSample vt/vol: 20.0 (g/mL) ML


% Moisture: not dec. ___Column (pack/cap) PACK







Date Analyzed: 03/06/89\,

Dilution Factor: -4<0


CAS NUMBER

1. 76-13-1

COMPOUND NAME

ETHANE, 1, 1, 2-TRICHLORO-l ,2,2

RT

13.47

EST. CONC. .

2.0

Q

3


SBHPLE DP TO SUHM8BY


EPA SAMPLE NO.

Lab Name: CQMPUCHEM mas________

Lab Code: COMPU Case No.: OQOO


Sample wt/vol: 20.Q (g/mL) Mt.


% Moisture: not dec. ___Column: (pack/cap) PACK



GAS NO. COMPOUND


Lab File ID: CKQ47869A12


Date Analyzed: 03/07/89I

Dilution Factor:


74-87-3——————Chloromethane_________74-83-9——————Bromomethane__________75-01-4-p—————Vinyl Chloride_________75-00-3——-———Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3-—-———-Chloroform ________107-06-2—————l,2-Dichloro«thane______78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6—————Trichloroethene________124-48-1—————Dibromochloronethane____79-00-5-—————1,1,2-Trichloroethane___71-4 3 -2——————-Benzene_______________10061-02-6————Tran»-l, 3-Dichloropropene_75-25*2———————Bromoform ________108-10-1——————4-Methyl-2-Pentanone_____591-78-6——————2-Hexanone_____________127-18-4 ™——Tetr achl or oethene_______79-34-5———————l,l,2,2-Tetr»chloroethane_106-88-3—————Toluene ______108-90-7—--——-chlorobenzen«__________100-41-4—————Ethylbenzen*__________100-42-5—————Styrene______________1330-20-7—————Total Xylene*_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.912210.90.90.90.9141111111111121110.910.91122026


S(3HPL.E DOT ft SUHMBRV


EPA SAMPLE NO

Lab Nan*: COMPUCHEM IABS________

Lab Cod«: COMPU ca*a No.: QQQQ

Matrix: (»oil/wat«r) WATERSampl« wt/vol: 20.0 (g/mL) ML

Lev«l: (low/mad) LOW

* Moi»tur«: not dac. ___


Numb«r TICs found: _1




Lab Fil« ID: CN047869A12

Data R«c«iv«d: 03/03/89

Data Analyzed: Q3/Q7/89

Dilution Factor: Jf. o___


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

13.42

EST. CONC.

2.0

Q

fT


SAMPLE O0T0 SUHHBRY



EPA SAMPLE NO.


Lab Coda: COMPU Gas* No.: 0000

Matrix: (soil/wat*r) WATER

Sampla wt/vol: 20.Q (g/mL) ML

L«v«l: (low/mad) LOW

% Moisture: not d«c. ___

column: (pack/cap) PACK

EAW65



Lab File ID: CNQ4787QB12

Date Received: p3/03/89


Dilution Factor: **Q____


74-87-3 ——™——Chloromethane_________74-83 -9—««——Bro»omethane__________75-01-4——————Vinyl Chloride_________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——----- Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3-.—————1, 1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total),67-66-3——————Chloroform__________107-06-2—————l,2-Dichloroethane_____78-93-3——————2-Butanona _____71-55-6—————--1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetata__________75-27-4——————Bromodichloromethane____78-87-5—————-1,2-Dichloropropane_____10061-01-5————"Ci»-l,3-Dichloropropene__79-01-6——--——-Trichloroethene________124-4 8-1-—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Banzana_______________10061-02-6———-Tran»-l,3-Dichloropropene_75-25-2——————— Bromoforn_____________108-10-1—————4-Methyl-2-P«ntanon«____591-78-6—————2-HaxanoM _______127-18-4—————Tetrachloroathana;______79-34-5——————1,1,2,2-Tatrachloro«thana_108-88-3—————Toluana _________108-90-7-————Chlorobanzana^^________100-41-4 —————Ethylbanzana__________100-42-5——————Styrane____;__________1330-20-7—————Total Xylanaa_________107-02-8—————Acrolain_____________107-13-1—————Acrylonitrila_________

10.80.913210.90.90.90.5141111111111121110.910.9112

2026


SAMPLE SUMMPRY 67


EPA SAMPLE NO


Lab Code: CQMPU Case No.: 0000


Sample vt/vol: 20.0 (g/nL) ML

Level: (low/ned) LOW



EAW65Contract: 5A54231E



Lab File ID: ' CNQ4787QB12



Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) us/L

CAS NUMBER

1. 76-13-1

COMPOUND NAME

ETHANE ,1,1, 2-TRICHLORO-l ,2,2

RT

13.47

EST. CONC.

6.0,

Q

&LL __


S0MPLE D8T0 SUHHQRY


EPA SAMPLE NO.


Lab Code: CQMPU Case No.: OOQQ

Matrix: (soil/water) WATERSample wt/vol! 20.0 (g/mL) ML


t Moisture: not dec. ___





Lab File ID: CN047871A12



Dilution Factor: a'.Q


74-87-3——————Chloromethane_______74-83-9-—————Broaomethane__________75-01-4——————Vinyl Chloride_________75-00-3—————-Chloroe thane__________75-09-2—————Methylene Chloride______67-64-1—————-Acetone______________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform___________107-06-2——• -——1,2-Dichloroethane______78-93-3——————2-Butanone _________71-55-6——————1,1,1-Trichloroethane___56-23-5--————carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————Bromodichloromethane____78-87-5—————i, 2-Dichloropropane_____10061-01-5———cis-l,3-Dichloropropene__7 9-01-6——————Tr ichloroethene________124-48-1————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2 —-""——Benzene ________10061-02-6————Tran«-l,3-Dichloropropene_75-25-2——————Bromo form_____________108-10-1—————4-Methyl-2-pentanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5——————i ,1,2,2-Tetrachloroethane_108-88-3—————Toluene______________108-90-7-"——-Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5——————Styrene_______________1330-20-7————Total xylenes_________107-02-8—————Acrolein_____________107-13-1——•———Acrylonitrile__________

10.80.912210.90.90.90.9144111113111121110.910.9112

2026


SAMPLE Df*T0 SUMMARY


EPA SAMPLE NO

Lab Name: coMPUCHgM LABS_________

Lab Code: CQMPU Case No.: QOOQ



t Moisture: not dec. ___Column (pack/cap) PACK






Data R«c«iv«d: 03/03/89

Data Analyzed: 03/07/89/

Dilution Factor: *.Q


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

13.42

EST. CONC.

3.0

Q

*


SBHPLE OffTff SUHHQ&Y


EPA SAMPLE NO.




Sample wt/vol: 20.0 (g/mL) ML -







Lab File ID: CR047872C12


Date Analyzed: Q3/07/B9/.

Dilution Factor: tr. 0 ____^


74-87-3——————Chloromethane_________74-83-9——*-——Bromome thane__________75-01-4———————Vinyl Chloride_________75-00-3——————Chloroethane__________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform___________107-06-2——*--—i, 2-Dichloroethane______78-93-3——————2-Butanone ____________71-55-6———————1,1, l-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4™-———Bromodichloromethane____78-87-5-—————1,2-Dichloropropane_____10061-01-5-——--cis-1,3-Dichloropropene__79-01-6———— -- Trichloroethene________124-48-1—--—•-- Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6-———Trans-1,3-Dichloropropene_75-25-2——————Bronoform____,_______108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5———-———1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7—————-chlorobenzene_________100-41-4—————Ethylbenzen*__________100-42-5—————Styrene______________1330-20-7—————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10,0,14211754

13001

1345311111

11011

431211

1700,91

801

362026

U

UUuuuEu.uuuuu£U

FORM I VOA 1/87 Rev

SAMPLE OffTff SUMnORV


EPA SAMPLE NO,

Lab Name; CQMPUCHEM LABS__________

Lab Code: COMPU Case No.: QQOQ




t Moisture: not dec. ___


Number Ties found: _5




Lab File ID: CRQ47872C12



Dilution Factor: tf. 0____


CAS NUMBER

1. 109-66-02. 110-82-73. 96*37-74. 110-54-35.

COMPOUND NAME

PENTANECYCLOHEXANECYCLOPENTANE , METHYL-HEXANEUNKNOWN

RT

14.6915.7016.4220.5423.89

EST. CONC.

4.08.05.06.02.0

Q

JJJJJ


SQMPLE SUMHBRY


EPA SAMPLE NO.


Lab Code: CQMPP Case Ho.: 0000




CAS NO. COMPOUND

EAW67REContract: SAS4231E



Lab Pile ID: C3R47872C12


Date Analyzed: 03/10/89/OC.O

Dilution Factor: 4.Q •


74-87-3———-—Chloromethane_________74-83 -9——————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide;________75-35-4——————l,l-Dichloro«thene______75-34-3——————l, l-Dichloro«thane______540-59-0—————l,2-Dichloro«th«ne (total)67-66-3———————Chloroform ________107-06-2—————l, 2-Dichloro«thane_____78-93-3——--———2-Butanone _________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————Bromodichlorome thane____78-87-5——————l, 2-Dichloropropane_____10061-01-5———cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1™——— Dibromochl oromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2—————Benzene______________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2——-———-Bromoform ________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone____________127-18-4——•——Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——^———Toluene ________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene______________1330-20-7—————Total Xylene*__________107-02-8——————Acrolein ___________107-13-1—————Acrylonitrile_________

13077941003005901109362

32009111043062100120110130120170120110140120160120140340851108914010021020002600

U.

uDJDUUUDJUUUUUDUUUUUuuDUUuDUUUU

FORM X VOA 1/87 Rev

S8MPLE OffTff SUHMBRV


EPA SAMPLE NO.

Lab Name: COMPTJCHEM LABS_________

Lab Cod*: COMPU Cave No.: OOQQ

Matrix: (moil/water) WATERsample wt/volx 0.20 (g/mL) MLLevel: (low/med) LOW



Number TIC» found: 0





Date R«c«iv«d: 03/03/89


Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Xg) UG/L



SftHPLE OPTP SUMM8RY


_____1 Contract: SAS4231E

EPA SAMPLE NO.

Lab Name: CQMPUCHEM LABS_______Lab code; • eoMPD case No.: oooo

Matrix: (»oil/watar) WATERSample wt/vol: 20.0 (g/mL) ML


* Moisture: not dec. ___


EAW68





Date Analyzed: 03/08/89i

Dilution Factor: X". o____


74-87-3—-———Chloromethane_________74-83-9——————Bronomethane__________75-01-4——————Vinyl Chloride________75-00-3—————Chloroe thane__________75-09-2——————Methylene Chloride______67-64-1———————Acetone_______________75-15-0——————Carbon Dieulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total)67-66-3—————Chloroform,____________107-06-2—————1,2-Dichloroethane______78-93-3——————2-Butanone __________71-55-6——————1,1, l-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————vinyl Acetate_________75-27-4™———Bromodichloromethane____78-87-5-—————1,2-Dichloropropane_____10061-01-5———-cie-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2————™-Benzene_____________10061-02-6———Tran»-l,3-Dichloropropene_75-25-2—-————Bronoform_______108-10-1—————4-Methyl-2-*entanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene______________1330-20-7————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.913210.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev

SftHPLZ O0T0 SUHHBRV 59


EPA SAMPLE NO,

Lab Name: LABSEAW68







Number TICs found: Q

Contract: SAS4231E

SAS No.s 4231E SDG No.: EAW60


Lab Fll« ID: C2R47873C12



Dilution Factor: .Q




S0HPLE PffTff SUHMBRV


EPA SAMPLE NO.

Lab Name: CQMPDCHEM LABS__________

Lab Code: CQMPU case No.: oooo





EAH69Contract: SAS4231E





Date Analyzed: Q3/1Q/89

Dilution Factor: 4.0____


74-87-3——-———Chloromethane_________74-83-9——------Bromoma thane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroe thane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone________________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3—————Chloroform___________107-06-2—————1,2-Dichloroethane_____78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cia-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2—————Benzene______________10061-02-6———Tran»-l,3-Dichloropropene_7 5-2 5-2——————-Bromof orm_____________108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-Kexanone___________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3————Toluene____m_________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————styrene______________1330-20-7—————Total Xylenes__________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

53575

231545291404517445455

13054756555632444880110

U


SQHPLE DffTff SUMHQRY


EPA SAMPLE NO,


Lab Code: COMPU Case No,: OOQQ







Lab Sample ID: 24787*








SAMPLE &QT0 SUMM0RV



EPA SAMPLE NO.


Lab Code: COMPU Cam* No.: OQOQ

Matrix: («oil/wat«r) WATERSample wt/vol: 20.0 (g/mL) MLLevel: (low/med) LOW

% Moisture: not dec. _____


EAW70



Lab File ID: CNQ47875B12



Dilution Factor: rf. 0____


74-87-3——————Chloromethane_________74-83-9———--——Bromomethane_________75-01-4———————Vinyl Chloride_________75-00-3——————chloroethane______________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene______75-34-3——————l,l-Dichlproethane______540-59-0——————1,2-Dichloroethene (total)67-66-3--—————Chloroform,___________________107-06-2—————1,2-Dichloroethane______78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachldride____108-05-4—————Vinyl Acetate_________75-27-4—————-Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1-—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2———————Benzene_______________10061-02-6———Tran»-l,3-Dichloropropene_75-25-2——————Bromoform____________108-10-1—————4-Methyl-2-Pentanone____591-78-6-—————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3—-———Toluene_______________108-90-7—————-Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

l0.811116115

1500.5140.811111610.62121170.940.40.81162026


SBHPLE DOT0 SUMMBRV


EPA SAMPLE NO

Lab Name: CQMPUCHEM LABS -Lab Code: CQMPU Case No.: 0000


Sampl* wt/vol: 20.0 (g/mL) ML



Column (pack/cap)

Number TICs found:

EAW70Contract: SAS4231ESAS NO.: 4231E SDG No.: EAW60



Date Received: Q3/Q3/89

Date Analyzed: 03/07/89I,

Dilution Factor: x. o____


CAS NUMBER

1.

COMPOUND NAME

LAB CONTAMINANT

RT

13.42

EST. CONC.

4.0

Q

BJ


SPHPLE OffTff SUHMBBY


EPA SAMPLE NO.


Lab Code: CQMPU Case No,: QQOO



t Moisture: not d«c. ___



SAS No,: 4231E SDG No.: EAW60





Dilution Factor!


74-87-3——-———Chloromethane_________74-83-9——————Bromomethane ________75-01-4——————vinyl Chloride_________75-00-3——————Chloroetharm__________75-09-2——————Methylene Chloride______67-64-1——————Acetone______________75-15-0———————Carbon Di«ulfide________75-35-4————————1. l-Diehloyoethena75-34-3—-————l,l-Dichloro«thane______540-59-0——————l,2-Dichloro«thene (total).67-66-3—————Chloroform___________107-06-2—————1,2-Dichloroethane______78-93-3————--2-Butanone__________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon T«trachloride____108-05-4—————Vinyl Acetat*_________75-27-4—--———Bromodichlorome thane____78-87-5———^———1.2-Dichloropropane10061-01-5————ci«-l,3-Dichloropropene__79-01-6——————Trichloroethtne________124-48-1——•—--Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2-————-Benzene________________10061-02-6————Tran«-l,3-Dichloropropene_75-25-2———————Bromoform_________108-10-1—————4-M«thyl-2-P«ntanone____591-78-6———™2-Hexanon«____________127-18-4——-——T«trachloro«th*ne______79-34-5——————1,1,2,2-T«trachloroethane_108-88-3————--Toluene _________^108-90-7————Chlorobenz«n«_________100-41-4—————-Ethylbenzena__________100-42-5—————-Styrene______________1330-20-7—————Total Xylenes_________107-02-8—————Acrol«in____________107-13-1—————Acrylonitril«_________

539436434

160341544445464454645633344197396

UUD •UJ OUUUo0UUUUUUUUUDUUUUUUUDUJDUUUDUU


SQMPLE PffTff SUHH8RY


EPA SAMPLE NO

Lab Nam«: COMPUCHEM LABS_________

Lab Code: CQMPU Case No.: OQQO










Lab File ID: CRQ4787SB12



Dilution Factor: 4.0 3. L>


CAS NUMBER

1.

COMPOUND NAME

LAB CONTAMINANT

RT

13.42

EST. CONC.

44

Q

*}


SBMPLE OffTP SUMM8RY 52


EPA SAMPLE HO.

Lab Nan*.: CQMPUCHEM LABS_______Lab Cod*: CQMPU Caee Ho.: 0000






GAS NO. COMPOUND


SAS No.: 4231E SDG NO.: EAW60





Dilution Factor: fr'.o


74-87-3——————Chloronethane_________74-83-9-————Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0——————carbon Disulfide_______75-35-4—————-1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——«———Chloroform____________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone___________71-55-6——————1,1, l-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________7 5-27-4 —————Bromodichloronethane____78-87-5———————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1-————Dibromochloronethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene______________10061-02-6———Trans-l,3-Dichloropropene_75-25-2— —————Bronoform_________108-10-1—————4-Methyl-2-Pentanone____591-78-6————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5——————i ,1,2,2-Tetrachloroethane_108-88-3————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4 —————Ethylbenzene_________100-42-5—————Styrene______________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

10.80.911210.90.910.91411111111111287110.940.90.5122026


SBMPLE OPTQ SUMMBRY 51


EPA SAMPLE NO


Lab Coda: CQMPU Caee No.: QOQO




Number TICs found: ._1


SAS NO.: 4231E SDG NO.: EAW60





Dilution Factor: Xo____


CAS NUMBER

1.

COMPOUND NAME

LAB CONTAMINANT

RT

13.42

EST. CONC.

3.0

Q

X


SBMPLE DBTQ SUMMBRV


EPA SAMPLE NO.

Lab Nam«: CQMTOCHEM IABS________

Lab Code: CQMPU Gas* No.: QQQQ


Sampl« vt/vol: 9.2 (g/mL) ML



column: (pack/cap) PACK



CAS NO. COMPOUND


Lab File ID: CS047876B12


Date Analyzed: 03/07/892-^

Dilution Factor:


74-87-3——————Chlorome thane_________7 4 -83-9———————Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1—————Acetone_____ _______75-15-0———————Carbon Diaulfide75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform___________107-06-2—————1,2-Dichloroethane______78-93-3———————2-Butanone ________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——>———Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-1,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1-————-Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2————-Benzene____.__ _______10061-02-6———Trane-l,3-Dichloropropene_75-25-2——————Bromororm____________108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3-————Toluene_____«,________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————-Styrene_______________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1——————Acrylonitrile__________

3222242222229223233232333

10032242224

4357

UuUuDJUUUuuuuuuuuuuuuuuuuuDuuuDuuuuuu


SAMPLE 00 T0 SUHHBRV 49


EPA SAMPLE NO


Lab Cod«: CQMPU Cas* No.: QQQQ

Matrix: (soil/wat*r) WATER

Sanpltt wt/vol: 9.2 (g/nL) ML

X*v«l: (low/m«d) LOW



Nunb«r TICs found: _1




Lab Fil« ID: CR047876B12

Date R«c«iv«d: 03/03/89

Dat* Analyzed: 03/07/892.2-

Dllution Factor:


GAS NUMBER

1.

COMPOUND NAME

LAB CONTAMINANT

RT

13.47

EST. CONC.

13

Q


S8MPLS DBTf* SUMHQRV


EPA SAMPLE NO.


Lab Code: COMPU Case No.: 0000

Matrix: (eoil/vater) WATER

sample wt/vol: 5.0 (g/mL) MLLevel: (low/med) LOW



CAS NO. COMPOUND




Lab Fil* ID: CN047877B12




CONCENTRATION UNITS:(ug/L or ug/Kg) UC/L

74-87-3——————Chloromethane_________74-83-9———————Bromomethane___________75-01-4——————vinyl Chloride________75-00-3——————Chloroethane__________7 5-09-2 ———————Methylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————l,1-Dichloroethene______75-34-3——————l, 1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3——————Chloroform _________107-06-2—————1,2-Dichloroethane_____78-93-3———————2-Butanone_____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————vinyl Acetate_________75-27-4—————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__7 9-01-6——————Tr ichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——-——Benzene______________10061-02-6——~Trans-l,3-Dichloropropene_7 5-2 5-2——————-Bromoform_____________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_______100-41-4—————Ethylbenzene__________100-42-5—————styrene______________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

53974137"4931

110044172845455

11054145655

2103

464634

12080110


DPT8 SUMMQRY


EPA SAMPLE HO


Lab Code: COMPU Cast No.: QQQQ


Sample vt/vol: 5.Q (g/mL) ML

Level: (low/m«d) LOW





SAS NO.: A231E SDG NO.: EAW60


Lab Fil« ID: CNQ47877B12







SQMPLE OPTff SUMMARY



EPA SAMPLE NO.


Lab Code: CQMPU Cas* No.: 0000


Sample wt/vol: 0.72 (g/aL) ML




EAW72RE

CAS NO. COMPOUND






Dilution Factor: *i-&- J?- 6


74-87-3--————Chloromethane_________74-83-9—————-Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone ___________75-15-0———————Carbon Dieulfide________75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total)67-66-3—--—-—Chloroform __________107-06-2—————1,2-Dichloroethane______78-93-3-——————2-Butanone __________71-55-6——————l, l, 1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—-—-—•-- Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5™——cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2———————Benzene_______________10061-02-6———Trans-l,3-Dichloropropene_75-25-2——————Bromoform ___________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene______________1330-20-7—————Total Xylenes__________107-02-8——————Acrolein______________107-13-1—————Acrylohitrile_________

37211602846210301237

15002530120342934293632150333022344332383102456258428160550730

UJ POpUUUDUUUUUoUUJ DUUUUoUE>UDUDUU

FORM I VOA 1/87 Rev

SQMPLE OBTP SUMMBRY 45


EPA SAMPLE NO,


Lab Code: CQMPU Case No.: QOQQ

Matrix: (moil/wat«r) WATER





Number TICs found: ,_Q.







Dilution Factor:




PffTff SUMMBBV



EPA SAMPLE NO.


Lab Code: CQMPU Cas* No.: 0000




% Moisture: not dec. M_


EAW73

SAS NO.: A231E SDG No.: EAW60





CAS NO. COMPOUND

Dilution Factor:


I

74-87-3——————Chloromethane_________74-83-9—————Bromomethane___________75-01-4——————Vinyl Chloride________7 5-00-3 ——————Chloroethane__________75-09-2———————Methylene Chloride______67-64-1———-——Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3——————Chloroform ________107-06-2—————1,2-Dichloroethane______78-93-3———-——2-Butanone____________71-55-6——————1, l, l-Trichloro«thane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Broraodichloronethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—•————Dibroaochloronethane____79-00-5——————1,1,2-Trichloroethane___71-43-2—————-Benzene_______________10061-02-6————Tran«-l,3-Dichloropropene_75-25-2——-———Bromoform______________108-10-1—-———4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene______________1330-20-7—————Total xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.912710.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev

SIMPLE PffTff SUMH8RV


EPA SAMPLE NO,


Lab Code: CQMPU case No.: QQQQ




Number TICs found: _0.




Lab Pile ID: CN047878A12


Date Analyzed: 03/08/89\

Dilution Factor: fC. Q____


GAS NUMBER COMPOUND NAME RT EST. CONC. Q


SPMPLE OftTQ SUMM8RY 42


EPA SAMPLE NO.

EAW74Lab Name: COMPUCHEM" LABS_________ Contract: S&S4231E

Lab Code: coMPU Case No.: OQQQ SAS No.: 4231E SDG No.: EAW60







Lab File ID: CNQ47879A12



Dilution Factor: Xo


74-87-3——————Chloromethane_________74-83 -9——————Bromomethane__________75-01-4——————Vinyl Chloride_________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Diaulfide________75-35-4——————l,l-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total)67-66-3-——•————Chloroform _________107-06-2—————1,2-Dichloroethane______78-93-3-—————2-Butanone _________71-55-6——————l, 1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-2 7 -4 ——————Bromodichloromethane_;___78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1——-——Dibromochloromethane___'_79-00-5——————1,1,2-Trichloroethane___71-4 3 -2 —-———Benzene______________10061-02-6———Trans-l,3-Dichloropropene_75-25-2—<————-Bromoform_____________108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone_____________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane^.108-88-3————-Toluene__________________108-90-7-————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-4 2 -5—————styrene_____________1330-20-7————Total Xylene-_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

10.80.910.7610.90.90.90.914111iiiiiiii21110.910.91122026

FORM I VOA 1/87 Rev

SBMPLE DP TO SUHM8RV 41


EPA SAMPLE NO.


Lab Cod*: COMPU Caee No.: QQOQ








SAS No.: 4231E SDG NO.: EAW6Q





Dilution Factor:




SQMPLE PQTf) SUMM8RY


EPA SAMPLE NO.

Lab Nam«: COMPUCHEM LABS_______Lab Cod*: COMPU Gas* No.: OOOQ

Matrix: <soil/wat*r) WATER

Sampl* wt/vol: 20.Q (g/mL) ML

L*v*l: (low/m*d) LOW

% Moistur*: not d*c. ___Column: (pack/cap) PACK




Lab Fil* ID; CN047880A12

Dat* R*c*iv*d: 03/03/89

Dat* Analyzed: 03/08/89

CAS NO. COMPOUND

Dilution Factor:


\

74-87-3——————Chlorom*than*_________74-83-9---————Bromom*than*__________75-01-4——————Vinyl Chlorid*________75-00-3——™——Chloro* than*,__________75-09-2———————M*thyl*n* Chlorid*______67-64-1———————Ac*ton«______j________75-15-0———————Carbon Disulfid*________75-35-4——————l,l-Dichloro*th*ne_____75-34-3———————1, l-Dichloro*than*______540-59-0——————l,2-Dichloro*th*n* (total)67-66-3—————Chloroform ___________107-06-2——————l,2-Dichloro*than«______78-93-3———————2-Butanon*_____________71-55-6——————l, l, i-Trichloro*than*___56-23-5——————Carbon T*trachlorid*____108-05-4——————Vinyl Ac*tat*__________75-27-4——————Bromodichlorom*thane____78-87-5———•——l, 2-Dichloropropan*_____10061-01-5————cia-l,3-Dichloropropene__79-01-6™———Trichloro*th*n*________12 4 -4 8-1—————Dibromochlorom*than*____79-00-5——————l, l, 2-Trichloro*thane___71-4 3 -2——————B*nz*n* ____________10061-02-6————Tran»-l,3-Dichloropropen*_75-25-2—--———Bromoforw___________108-10-1—————4-M*thyl-2-P*ntanon«____591-78-6——————2-H*xanon«_____________127-18-4————-T*trachloro*th*n*______79-34-5——————l ,1,2,2-T*trachloroethan«_108-68-3——-———Toluana_________.108-90-7—————Chlorob*nz*n*_________100-41-4—————Ethylb*nz*n*__________100-42-5——————Styr*n«_______________1330-20-7—————Total Xyl*n*»_________107-02-8—————Âcrol«in______________107-13-1—————Acrylonitril*_________

10.80.910.9510.90.90.90.9141111111112121110.910.91122026

FORM I VGA 1/87 Rev

SBMPLE D8TB SUHMBRV


EPA SAMPLE NO.

Lab Nan*: COMPTJCHEM LABS_________

Lab Coda: COMPI? Case No.: QQQQ

Matrix: (soil/wat*r) WATERSample wt/vol: 20.o (g/mL) Mi.

Lavel: (low/mad) LOW




EAW75Contract: SASA23IE



Lab File ID: CN04788QA12


Data Analyzed: 03/08/89i

Dilution Factor: A<Q____


GAS NUMBER COMPOUND NAME RT EST. CONC. Qmmmmm


SOMPLE DBT8 SUHH8RV JS


EPA SAMPLE NO.


Lab Coda: CQMPU Casa No.: OQOQ

Matrix: (soil/vatar) WATERSample wt/vol: 20.0 (g/mL) ML

Laval: (low/mad) LOW

% Moistura: not dac. ___




Lab Sampla ID: 247881____

Lab Fila ID: CNQ47881A12



Dilution Factor: ko


74-87-3—-————Chlorome thane_________74-83-9—————-Bromomethane__________75-01-4——————Vinyl Chlorida_________75-00-3——————Chloroathana__________75-09-2——————Mathylana Chlorida______67-64-1———————Acatone_______________75-15-0———————Carbon Disulfida________75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroathana______540-59-0—————1,2-Dichloroathana (total)67-66-3——————Chloroform___________107-06-2—————1,2-Dichloroathana______78-93-3———————2-Butanona_____________71-55-6——————1,1, l-Trichloroa thane___56-23-5——————Carbon Tatrachloride____108-05-4—————Vinyl Acatata_________75-27-4——————Bromodichloromathane____78-87-5-——-——-1,2-Dichloropropane_____10061-01-5——-—cis-1,3-Dichloropropene__79-01-6——————Trichloroathana________124-48-1———---Dibromochloroma thane____79-00-5——————1,1,2-Trichloroethane___71-43-2———-———Banzana_______________10061-02-6————Tran«-l,3-Dichloropropene_75-25-2—————-Bromoform_____________108-10-1—————4-Mathyl-2-Pantanone____591-78-6—™-——2-Haxanona __________127-18-4—————Tetrachloroathana______79-34-5——————l,l,2,2-Tetrachloroethana_108-88-3—————Toluana ____________108-90-7—————chlorobanzana_________100-41-4—————Ethylbanzana__________100-42-5—————styrana______________1330-20-7—————Total Xylenes__________107-02-8—————Acrolain_____________107-13-1—————Acrylonitrila_________

10.80.912510.90.90.90.9141111111111121110.910.91122026

UUUUUffUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU


SAMPLE OPTff SUHMQRY


EPA SAMPLE NO.

Lab Name: CQMPUCHEM IABS_______Lab Code: COMPU case No.: QQQQ

Matrix: (soil/water) EAIEE-










Date Analyzed: Q3/Q8/89

Dilution Factor:


GAS NUMBER COMPOUND NAME RT EST. CONC.


S8MPLE DffTff SUMMBRY


- Contract: SAS4231E

EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS____.

Lab Coda: COMPU Case No.: OOQO


Sample wt/vols 20.Q (g/mL) MLLevel: (low/med) LOW

% Moimture: not dec. ___


CAS NO. COMPOUND

EAW77



Lab rile ID: CN047882A12


Date Analyzed: 03/08/89L,

Dilution Factor: *. 0____


74-87-3———————Chloromethane________74-83-9——————Bromomethane________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1———————Acetone________________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene______75-34-3——————l,l-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3—————"Chloroform ________107-06-2—————1,2-Dichloroethane______78-93-3-——————2-Butanone_____________71-55-6—————-1,1,1-Trichloroethane___56-2 3 -5——-———Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-4 3 -2———————Benzene _______10061-02-6————Trans-l,3-Dichloropropene_75-25-2———————Bronoform_________108-10-1—————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone_____________127-18-4—————Tetrachloro«thene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene______________108-90-7—————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————Styrene______________1330-20-7—————Total Xylene*_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

l0.80.910.8510.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev

SBHPLE PPTff SUMHQRV J5


EPA SAMPLE NO,

Lab Name: CQMpnCHEM LABS________


Matrix: (soil/water) WATERSample wt/vol: 20 To (g/mL) ML











Dilution Factor: r.Q____




SOMPLE OBTB SUMMPRY



EPA SAMPLE NO.








EAW78

SAS No.: 4231E SDG NO.: EAW6Q





Dilution Factor: Q


74-87-3——————Chloromethane_________74-83-9————™Bromomethane__________75-01-4——————Vinyl Chloride_________75-00-3—————-Chloroe thane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Diaulfide_______75-35-4——————l,l-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total),67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3—— ———-2-Butanone_____________71-55-6——————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride.____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5————-—1,2-Dichloropropane_____10061-01-5——™ci»-l,3-Dichloropropene__79-01-6———————Trichloroethene_________124-48-1—————Dibromochloromethane____79-00-5-—————1,1,2-Trichloroethane___71-43-2——————Benzene __________10061-02-6———-Trans-l,3-Dichloropropene_75-25-2—-—————Bromoforn_________108-10-1—————4-Methyl-2-Pentanone____591-78-6-—————2-Hexanone_____________127-1 s -4 -————Tetrachl oroethene______79-34-5————.—1,1,2,2-Tetrachloroethane_108-88-3—————Toluene________________108-90-7——————Chlorobenzene__________100-41-4——————Ethyl^-enzene___________100-42-5——————Styre.ie_______________1330-20-7—————Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

10.80.910.7410.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev

SAMPLE OffTff SUMM88V


EPA SAMPLE NO,

Lab Name: COMPUCHEM LABS_______Lab Cod«: COMPU Cast No.: QOOQ



% Moisture: not d*c. ___.



EAW78Contract: SASA231ESAS NO.: 4231E SDG No.: EAW60.


Lab Fil* ID: CNQ47883A12



Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Xg) UG/L



SBMPLE Off TO SUMMQRV


EPA SAMPLE NO.

Lab Namt: COMPUCHEM LABS_________

Lab Cod*: CQMPU Case No.: QQQQ

Matrix: (soil/water) WATERSampl* wt/vol: 20.0 (g/mL) ML

Lav«l: (low/m«d) LOW



EAW79Contract: SAS4231ESAS NO.: 4231E SDG No.: EAW60

Lab Sampl« ID: 247884____



Oat* Analyzed: 03/08/89(

Dilution Factor: 4<Q____


74-87-3———-——Chloromethane_________74-83-9™————Bronomethane__________75-01-4——————Vinyl Chloride_________75-00-3—————chloroethane_________75-09-2——————Methylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————l,lrDichloroethene______75-34-3——————1, 1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3-—————Chloroforw____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichlgroethane___56-23-5-—————Carbon Tetrachloride____108-05-4—————vinyl Acetate_________75-27-4——————Bromodichloroaethane____78-87-5—————l,2-Dichloropropan«_____10061-01-5————ci»-l,3-Dichloropropen«__79-01-6——————Trichloro«th«na_______124-48-1——-——Dibromochlorom*than«____79-00-5——————1,1,2-Trichloroathane___71-43-2-——————-B«n2«n« _____________10061-02-6————Tran«-l,3-Dichloroprop«n«_75-25-2™———Bromoform___________„.108-10-1——————4-M«thyl-2-P«ntanon«____591-78-6—————2-H«xanon«___________127-18-4—————T«trachloro«th«n«______79-34-5——————1,1,2,2-T«trachloroethan«_108-88-3———————TolU«n«_________________108-90-7—-———Chlorob«nz«n*__________100-41-4——————Ethylb«nz«n«__________100-42-5—————Styran«_____________1330-20-7—————Total Xylan«s__________107-02-8—————Acrolein____________107-13-1—————Acrylonitril«_________

10.80.911510.90.90.90.9141111111111121110.910.911^2026


SPMPLE PffTff SUMMQRV


EPA SAMPLE NO.

EAW79Lab Name: CQMPUCHEM LABS________ Contract: -SAS4231E

Lab Code: COMPU Gas* No.: QQQQ SAS No.: 4231E SDG No.: EAW6Q






Number TIC* found: _Q,


Lab Pile ID: CNQA7afl4Al2


Date Analyzed: 03/08/89(

Dilution Factor: 4<Q____




DPT8 SUMMBRV

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V

fa*** y,1JICT: Review of Region V CLP Data

-Received for Review on___mou. Curtis Ross, Director (5SCRL)

Central Regional Liberator,?

PAG5 1 OF _ ^

RECEIVEDDPR 0 7 1989

We have reviewed the data for tht following ease(s).

SITE HAKE: {J^JLSVflO (/Jfffff Lj*J(>J S» C.f(9/ - x- l.,/-., ». •<• y/ O.U./AC

Hrs. Required —for Review:_7

Following are Our, findings:

V

^cxT

^=- ^7

cc:

Data are acceptable for use.Data are acceptable for use witSee Data Qualifier sheets and Cadditional comments*

I Data are preliminary * pendingSee Case Summary above*

) Data are unacceptable.Carla Dempsey.CLP Quality AssurJunes Petty. Chief Quality Assu

DATA QUALIFIERSPAGE IT OF L

Contractor: COM Case


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Reviewed by:Phone:Date: /

DATA QUALIFIERSPAGE _£_ OF (&

Contractor Case / / 3 5^5

Below 1s a summary of the out-of-control audits and the possible effect on thedata for this case:

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Contractor: "»•I.

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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERSfOLATlLE HSL COMPOUNDS

CONTRACTOR/: &M

Instrument « //DATE/TIME: U-/S-W 3VSJT

ChloromethaneBromomethaneVinyl ChlorideChloroethaneHethylene ChlorideAcetoneCarbon nisulfide1,1-Dichloroethane1.1-DichloroetheneTrans-l.Z-DichloroetheneChloroformZ-Butanonel,Z-D1chloroethane1.1.1-Tri ChloroethaneCarbon TetracnlorideVinyl AcetateBronDd*i cnl ororoethane

.Z-DTChloropropaneTrans-1 ,3-DichloropropeneTrichloroetheneDibromochloromethane1 .1 ,2-Trichl oroethaneBenzeneci s-1 ,3-Di chl oropropene

Bromoform4-Methyl-Z-Pentanone2-HexanoneTetrachioroethene1 ,1 ,?,Z-TetrachioroethaneTolueneChiorobenzeneEthyl benzeneStyreneIflrXylene (JCr&sfJfl/B"Xyl>ne Ac,rv leHlTrife

AFFECTEDSAMPLES:

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* These flags should be applied to the analytes on the sample data sheets.

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OF

Instrument * /IDATE/TIME: 3-3-9"? M'y?

CnlopomethaneBPomomethaneVinyl ChlorideChiopoethaneMethyl ene ChlorideAcetoneCapbon HisuUlde1,1-Dichloroethane1,1-DichloroetheneTPans-l.Z-DichloPoetheneChlopofopmZ-Butanone, ,2-DichloPOethane: .1.1-TpichiopoethaneCapbon TetPacMoPldeVinyl AcetateBPOôdi chl OPomethaneI.z-DichlopoppopaneTpans-1 ,3-DichloPooPOpeneTPichlopoetheneDibpomochl OPomethaneKl,Z-TpichloPoethaneBenzeneci s-1 ,3-Dichl opoppopeneg CMpEoethyivinylatherBromoform4-Methyl-Z-PentanoneZ-HexanoneTetpachlopoethenel.l.Z.Z-TetPachlopoethaneTolueneChlopobenzeneEthylbenzeneStypenefly-Xylene (*£yfaj)0/p-Xr*g»c A&.rv/aitj'TrilA'/

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For reporting reaulta tr -fee QSXFA, the follovlag contract apeeificqualiflara ara to be uaed. The acren qualif lera defined below mBpjt aubject to aodiflection by the laboratory. Up to fivequalifiara aay bo reported on Fora Z for each uoapiinnrt.

IPA-deflned qualifiA?s to bo uaed ara aa follow:

- Indicate* eoapound wu analyzed for bice not detected. Theaaapla qoantitatioa liait Boat be corrected for dilution andfor percent aolsture. For exaapla, 10 V for phenol la water ifthe aaaplo final voluao ia the protocol-apecified final volune.If a 1 to 10 dilution of extract la neeeaaary, the reportedliait ia 100 V. For * aoil aaaplo, tho value auat Alia beadjuatad for percent aoiatuze. For exaapla, if the aaaple had24% aotsture uA c 1 to 10 dilution factor, tho aaaplequantitation Halt for phenol (330 V) would bo corrected to:

100

and df » dilution factor

at 24% aolatura. 0 - lfifi*2i - 0.76100

Tn x 10 - 4300 9.76

rouadod to th« appropriata auabar ofalanifieaat fifuraa

J •

For aoil aaaplea aubj acted ta CFC clean-up procedures, the C&QLia also Multiplied by 2, to account for the fact that only halfof tho extract ia recovered.Indicates aa eatiaatad value. Thia flag la uaed either whenestimating a concentration for tentatively Identified eaapoundawhere a 1:1 response la assumed, ar when the aaaa spectral dataindicate the presence of a compound that aeets theidentification criteria but the result ia leaa than Ac aaaplequantitation liait but greater than xero. For exaaple; if tho

quantitation Halt ia 10 ug/L, but a concentration of 3la calculated, report it aa 3J. The aaaple quantitation

C -

aa diaeuaaod for tho V Oaf, ao that If a aaapla vith 24%•aiaturo and * 1 to 10 dilution footer haa a calculatedeoaeeacratioa of 300 «|/L and a aaaplo quantitatloa liait of430 ui/kg, report tho oonaaatratioa aa 300J oa Fora 1.Thia flag appllea to peatieida raaulta vh*ro the Identificationhaa been eenfiraod by CC/HS. Single eooponent peatlcldeang/ul ia tho final extract ahall be eonflraod by GC/MS.

2/88

whose cone operations oxaeed the

B - This flag la used whoa tba aaalyta la found la the associatedblank aa veil as la the aaapla. It indicates possible/probableblank contamination aad warns tba data user to take appropriateaction. This flag auat bo used for a TIC aa veil as for apositively Identified TO,

calibration raage of tao CC/KS Instrument for that specifieanalysis. This flag will ««t apply Co posticidee/Tds aaalyxedby CC/IC methods. Xf one or aore aemp dirndl here a response

full Mala, the aample or extract oust bo dilutedkocordlag to taa specifications la FrMMt D.

All ouch aampuiaidi with a response greater tbaa full acalomhculd hare tbo eoaoontretioa flagged with aa "I* oa tbo Fora Xfor tbo origiaal aaalysls. Xf tbo dilution of the extract

belov the calibration raage la cae oolresults of both aaalyees shall bo reported oa separate foras iThe Fora X for the dilated aample ahall have the *Dt.* auffixappended to the sample aumber. VOtI: For total xylenea, wh« :throe iaomera aro ajuaatlfied aa two peaks, tho calibration

of «Meh M«V should be aonaidered separately, e.g., adiluted aaaljtla la fifi£ zooulrod for total xylonoa unloas

toatratlon of oltbar poak aoparataly azeaoda 200 ug/L.

fi * tala flag laoatlflaa all imarpminrti Idoatlflod la aa aaalyals *'a aocondary dilution factor. Xf a aaoalo or oxtraet la

ilyxod at a blghor dilution factor, aa la tao "E" flagtho *BL* auffix la appond^ to tbo oaaplo auabor on

Tora X for tbo dllutad aaaplo, aad *ll concentration valoojraportod oa that Fora X aro flagged wld} tao •&* flag.

- This flag indicates that a TIG la a auapectedproduct.

specific flap may be required to prootrly defineresults. Xf used, they must bo fully described and suchdescription attached to the Sample Data, tnamry Faekage andCase narrative. Begin by using *XV Xf more than one flag

Tf ir"Ti ghm fi e ___ojualifiers are roomlrod for a aample result, use tho *Z* flaxCo combine several flags, aa needed, for Instance, the *X*flag alght combine the 'A*. "»•. aad «0- flags for some aampl

Ibo combination of flags "»T or*CB" la axproasly problbltod. 11..eoatasilaaaca aro flagged *g* gnl^r vboa tboy aro also dttoetod in 1aaarplo.

If analysoa at two dlfforont dilution factors OT« rooulrod C*ooExhibit D), follow tao data reporting instructions glvtn in Exh:a ard vich tho "0" and "»- nags abovo.

1-30

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tot n

o

+•

WMTTE - SMO COPY PINK - CLIENT COPY WRIT I—' COPY POW KCTUm TO SMO YtLLOW -1M GOT

SOHPLS oara POCKQBE 506

USiPA CONTRACT LABORATORY PHOf.HAM

SAMPLE MANAGEMENT OmCff 0 BOX RIB ALEXANDRIA. VA 7? it I

ORGANIC TRAFFIC REPORT* im OP ust UNIYI

TYPE OF ACTIVITY (CIRCLESUPERPUNO-PA SI ESI

NPLO 04M OTHER _________PROGRAM

EONE^ 0/WPB RD RA ER

-•AMPLE DESCRIPTION(EKTO IN BOX A) 4. SOILv SURFACE WATER s SEDIMENT2 OHOUMQ MA1B1 * OIL (SAS)3. LEACHATE 7. WASTE (SAS)

S I

ATTN

,PTO:,

u; it'DATE REC'D:.3/6/69 to

P-ECOlY:

LABORATORY CONTRACT NO. UNIT PRICE

SAMPLE D8TR PPCKQ6E 50S

ERA CASE NARRATIVE—CASE ttOOOOContract No. SAS4231E SAS No. 4231E SDC No. EAC13

CompuChem Laboratories, Inc.

Sample Numbers: EAG13 EAC14 EAC1S EAG16 EAC17 EAG18 EAU90 EAU91EALJ92 EAU93 EAU94 EAU95 EAU96 EAU97 EAU98 EAU99

This portion of SAS #4231E consisted of 16 water samples for low detectionUnit volatile analysis. The sample* were received in good condition on3-6-89 in properly sealed shipping containers with traffic reports. Du* toan overshipment of MS/MSD, Cindy Shreyer of SHO was contacted and CompuChemwas instructed to pick one MS/MSD per SDC group. CompuChem is following EPArounding rules for the Contract Required Quantitaion Limits and final reportingresults. Volatile fractions are being reported to one significant figurebelow a value of ten. "J" values are being reported down to one-half themodified CRQL. Th* word "No" on the quant report means the compound was notfound or the compound was less than one-half the CRQL.

All fractions were analyzed within holding time requirements. TCL compoundswere present in all the samples at various levels. Two analyses of sampleEAU97 war* reported and billed. In the initial undiluted analysis, the levelso' , 2-dichloroethene and tetrachl*broethene exceeded multipoint range. TheS, le was reanalyzed at a dilution and both analyses were reported due to theloss of some compounds in the dilution. A freon tentatively identified com*pound was present in samples EAU96, EAU97, and EAU97RE which should be con-sidered a laboratory contaminant. A qualifier was included with each sample.None of the other samples contained any tentatively identified compounds.Sample EAU96 required a diluted analysis due to the high levels of TCL com-pounds present. Surrogate recovery criteria were met for all samples, blanks,and spikes. The QC matrix spike/matrix spike duplicate results were acceptableThe recoveries of trichloroethene exceeded QC limits in both the MS/USD. TheRPO value for 1,1-dichloroethene exceeded QC limits.

Release of the data contained in this hardcopy data package has been authorizedby the Laboratory Manager or his designee, as verified by the followingsignature.

Note: This report was paginated for reference and accountability in decreasingnumerical sequence.

>anet C. Carrett 3-30-89Technical Reviewer

51-7

1. CASt NTnU documtn: shall bt clearly libffltd "Cist Narrative" and shall contain:laboratory name; case number; tampIt numbers In the Sample Delivery firouo(SOS), differentiating between Initial analyses and re-analyses; SD6 ruTi-ber; Contract number; and detailed documentation of any quality control,sample, shipment and/or analytical problems encountered 1n processing tnesamples reported 1n the data package.Whenever data from sample re-analyses are submitted, the Contractor shallstate in tne Case narrative for each re-analysis, whether n considers there-analysis to be blllable, and If so, why.Tne contactor must also Include documentation of any 1nte-na- Qualitycontrol o-ocesses used, a summary of corrective actions ta<«r,, and toeresolution.

SOMPLE Off TO PaCKBBE SIS


Lab Nan*: CQMPUCHEM LABS________ Contract: SAS4231E

Lab Code: COMPU Case No.: QQOQ SAS No.: 4231E SDG No. EAfili.

0102030405060708091011121314151617181920212223

EPASAMPLE NO.

EAG13EAG14EAG15EAG16EAG17EAG18EAW90EAH91EAW92EAW93EAW94EAW95EAH96EAW97EAW97REEAH98EAW99EAG15MSEAG15HSOVBLKXDVBLKBQVBLKAAVBLKAC

SI(TOL) I

10099961051061051031041101101041021001039510010510098100101107101

S2(BFB)#

971059594101979296969696969592928896102901019810197

S3(DCE)#

97103969810098939799100969398949092941049899101102100

OTHER TOTOUT

00000000000000000000000

QC LIMITS51 (TOL) - Toluene-d8 ( 88-110)52 (BFB) - Bromofluorobenzene ( 86-115)53 (DCE) » l,2-Dichloroethane-d4 ( 76-114)

I Column to be used to flag recovery values* Values outside of contract required QC limits


page 1 of 1FORM II VOA-1 1/87 Rev,

SBMPLE OffTff

3AHATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Nan*: COMPUCHEM IABS____• Contract: SAS4231ELab Coda: CQMPP Caaa No.: QQQQ SAS No.: 4231E SDG No.: EAG13

Matrix s'piJca - EPA Sanpla No.:

COMPOUND

1 , 1-Dichloroathana ____TrichloroathanaB*nz«n*Toluan*Chlorobanzana

SPIKEADDED(ug/L)

12.512.512.512.512.5

SAMPLECONCENTRATION

(ug/L)

00000

MSCONCENTRATION

(ug/L)15.015.614.413.714.5

MS%

REC i

120125 *115110116-

QCLIMITSREC.

61-14571-12076-12776-12575-130

COMPOUND

1,1-Dichloroathane.Trichloroathana__Ban z ana________Toluana________BChlorobanzana____

SPIKEADDED(ug/L)

immt12.512.512.512.512.5

MSDCONCENTRATION

(ug/L)17.516.114.614.814.9

QC LIMITSRPD«*i1414111313

REC.

61-14571-12076-12776-12575-130

I Column to b« u*ad to flag raeovary and RPD valuaa with an aatarisk

* Valuas outsid* of QC Unit*RPD: _1 out ofSpika Racovary: ,

outaida Unitsout of 10 outsida limita

COMMENTS: CLP ,4231,EEAG13(-EAC1,LOW,WATER,248720,PEST, ,TUNE: 0012 031089 0725

FORM III VOA-1 1/87 Rav,

SPHPLE DQTP SUHMRRV 14


Lab Name: CQMPUCHEM LABS________ Contract: SAS4231E

Lab Code: COMPU Cast No.: 0000 SAS No.: 4231E SDG No.: EAG13

Lab File ID: CBa9Q3lQCll Lab Sample ID: VBLKXD

Data Analyzed: 03/10/89 Tin* Analyzed: 0721

Matrix: (soil/water) WATER Level:(low/med) LOWInstrument ID: 11


01

EPASAMPLE NO.

EAW99

LABSAMPLE ID

248744

LABFILE ID

CN048744A11

TIMEANALYZED

1314


page 1 of 1FORM IV VOA 1/87 Rev,

SPHPLE OffTff


Lab Name: COMPUCHEM LABS________ Contract: SAS4231E

Lab Code: COMPU Case No.! 0000 SAS No.: 4231E SDC No.: EAG13

Lab File ID: CB89031QA12 Lab Sample ID: VBLKBQ____

Data Analyzed: 03/10/89 Tin* Analyzed: 0900

Matrix: (soil/water) WATER Level:(low/med) LOW

Instrument ID: 12


01020304050607080910

EPASAMPLE NO.

EAG13EAG14EAG15EAG16EAG17EAG18EAW90EAW91EAG15MSEAG1SMSD

LABSAMPLE ID

248714248715248720248721248722248723248724248726248716248717

LABFILE ID

CN048714A12CN048715B12CN048720A12CN048721A12CN048722A12CN048723A12CN048724B12CN048726B12CN046716A12CN048717A12

TIMEANALYZED

1506160010021048131714171657175211351222


pag* 1 of 1FORM IV VOA 1/87 Rev,

SBMPLE DPTB


Lab Nan*: COMPUCHEM LASS________ Contract: SAS4231E

Lab Cod*: CQMPU Ca»« No.: QQOQ SAS No.: 423IE SDG No.: EAG13

Lab File ID: CBfl9Q3iiAia Lab Sanpl* ID: VBLKAA

Data Analyzed: oa/n/ao Tin* Analyzed: 0841Matrix: (soil/water) WATER L«v«l:(low/m*d) LOW

Instrument ID: 12

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AND M5D:

01020304

EPASAMPLE NO.

EAW92EAW93EAW94EAW95

LABSAMPLE ID

248728248730248731248732

LABFILE ID

CN048728A12CN048730A12CN048731A12CN048732A12

TIMEANALYZED

1033112112151338

COMMENTS: CLP ,4231,EEAG13,-EAW9,LOW,WATER,248744,PEST,BLANK,TUNE: 0012 031189 0709

page 1 of lFORM IV VGA 1/87 Rev,

SPMPLE DPTP SUfiMPKV


Lab Nam«: CQMPPCHEM LABS_____«^_ Contract: SAS4231E

Lab Cod«: COMPO Cas* No.: oooo SAS No.: 4231E SDG No.: EAC13Lab Fil« ID: CB890312A12 Lab Sample ID: VBLKAC

Data Analyzed: 03/12/89 Tim* Analyzed: 0840

Matrix: (»oil/wat«r) WATER L«v*l:(low/m«d) LOW

Instrument ID: 12


01020304

EPASAMPLE NO.

EAW96EAW97EAW97REEAW98

LABSAMPLE ID

248738248741248741248742

LABFILE ID

CR048738B12CN048741A12C2R48741A12CR048742A12

TIMEANALYZED

1631100814471357

COMMENTS: CLP ,4231,EEAG13,-EAW9,LOW,WATER,248732,PEST,BLANK,TUNE: 0012 031289 0710

pag« 1 of 1FORM IV VOA 1/87 R«v.

SPMPLE OPTff


EPA SAMPLE NO.

Lab Nan*: CQMPUCHEM LABS________

Lab Code: COMPU Case-No.: QOQQ

Matrix: («oil/wat«r) WATERsample vt/vol: 20.0 (g/nL) MLLevel: (low/med) LOW% Moimture: not dec. —_


CAS NO. COMPOUND

VBLKXDContract: SAS4231E

SAS No.: 4231E SDG No.: EAG13

Lab Sample ID: VBLKXP

Lab File ID: CB8903iocn



Dilution Factor: -*rfr /. C & ,


74-87-3————--Chlorone than*_________74-83-9--———-Bronone thane__________75-01-4——————vinyl Chloride________75-00-3——-—--Chloroethane.,_________75-09-2——<———Methylene Chloride_____67-64-1--—-—--Acetone_________________75-15-0-————--Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3—————2-Butanone___________71-55-6——————1,1, l-Trichloro«than«___56-23-5——-———Carbon T«trachlorid«____108-05-4—————vinyl Acatata_________75-27-4——————Bronodichloromathana____78-87-5——————1,2-Dichloropropane_____10061-01-5——-—cis-1,3-Dichloroprop«n«__79-01-6——————Triehloro«th«na________124-48-1—————Dibro»ochloromathan«____79-00-5———>——-l,l,2-Trichloro«than«____71-43-2™—-—-B«nz«n«_____________10061-02-6——-—Tran«-l,3-Dichloroprop«n*_75-25-2————-Bronofora_____________108-10-1————4-M»thyl-2-P«ntanon*____591-78-6—-—-—2-H»xanon«___________127-18-4—————T«trachloro«th«n«_______79-34-5—————1,1,2,2-T*trachloro«than«_108-88-3————-—Tolu«n«_________________108-90-7———«Chlorob«nzan«_________100-41-4————--Ethylb*nz«n*__________100-42-5——————Styr«n«_______________1330-20-7————Total Xyl«n«s_________107-02-8—————Acrol«in___________107-13-1—————Acrylonitrila_________

10.80.912210,90.90.90.9141111111111121110.910.91122026


SPMPLE OPTP SUMMffRV 11


EPA SAMPLE NO.

Lab Nan*: CQMPUCHEM LABS________

Lab Coda: CQMPU Cas« No.: 0000

Matrix: (*oil/wat«r) HAZES.Sanpl* wt/vol: 20.0 (g/mL) ML

L*v«l: (low/n«d) LOW

% Moistur*: not dac. ___


Numb«r TIC« found: _2

VBLKXDContract: SAS4231E

SAS NO.: 4231E SDG No.: EAG13

Lab Sanpl* ID: VBLKXD

Lab Fil* ID: CBB9Q3iocn

Data R«caiv«d:


Dilution Factor: A+4- /-O ,,A


GAS NUMBER COMPOUND NAME RT EST. CONC. Q


SBMPLE OPTP


EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS________






CAS NO. COMPOUND

VBLKBQContract: SAS4231ESAS No.: 4231E SDG NO.: EAC13

Lab Sample ID: VBLKBQ____

Lab Fila ID: CB89Q310A12



Dilution Factor:


74-87-3——————Chloromethane_________74-83-9-————Bromomathane__________75-01-4———————Vinyl Chloride_________75-00-3——————Chloroathane__________75-09-2———————Mathylana Chloride______67-64-1——————Acatona_____________75-15-0——————Carbon Disulfide_______75-35-4 ——————— 1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3-—------chloroform___________107-06-2——————1,2-Dichloroathane______78-93-3——————2-Butanona___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tatrachlorida____108-05-4——————Vinyl Acetate__________75-27-4——™—-Bromodichloroma thane____,78-87-5———————1,2-Dichloropropane_____10061-01-5——--cis-l,3-Dichloropropene__79-01-6™————Trichloroa thane________.124-48-1—————Dibromochloromathana____„79-00-5———————1,1,2-Trichloroethana____71-43-2———™-B*nzaM_____________10061-02-6——™Tran«-l,3-Dichloropropena_75-25-2-—————Bromoform_____________108-10-1———-——4-M«thyl-2-Pentanone____591-78-6——————2-Hexanone____________,127-18-4—————Tatrachloroethene_______79-34-5———•——l,l,2,2-Tatrachloroathan«_108-88-3———-—Tolu«na______________108-90-7—————Chlorobenzene___________100-41-4 —————Ethylbanzana__________100-42-5—————styr«n«______________1330-20-7—————Total Xylanas_________107-02-8——-——Acrolein_____________107-13-1—————Acrylonitrila_________

0.80.912510.90.90.90.9141111111111121110.910.91122026

FORM I VGA 1/87 Rav,

SOMPLE OffTP SUMMQRV


EPA SAMPLE NO

Lab Naaa: COMPUCHEM LABS_________

Lab Coda: COKPU Ca«a No.: OOOQ

Matrix: (*oil/watar) WATER

Sanpla wt/vol: 20.0 (g/mL) ML


% Moiatura: not dac. ___


Nunb*r TICs found: _0

VBLKBQContract: SAS423ie


Lab Saapla ID: VBLKBQ___Lab Fila ID: CB89Q31QA12

Data Racaivad: _____Data Analyzad: 03/10/89

Dilution Factor: -4 -Q- /. 0

CONCENTRATION UNITS(ug/L or ug/Kg)


FORM I VOA-TIC 1/87 Rav,

S8MPLE Off TO SUMHPXV


EPA SAMPLE NO.

Lab Nama: CQMPUCHEM LABS________Lab Coda: COMPO Caca No.: OQQQ

Matrix: (soil/watar) WATER

Sampla wt/vol: 20.0 (g/nL) MLLav«l: (lov/nad) LOW



CAS NO. COMPOUND

VBLKAAContract: SAS4231E

SAS NO.: 4231E SDG No.: EAC13

Lab Sanpla ID: VBLKAA

Lab Fila ID: CB89Q311A12

Data Racaivad: ______


Dilution Factor: ~4~e~I.C 'CONCENTRATION UNITS:(ug/L or ug/Kg) UC/L

74-87-3 —— - —74-83-9 ——— —75-01-4 —— ™75-00-3 ——— —75-09-2 —————67-64-1 —————75-15-0 —————75-35-4 —————75-34-3 —————540-59-0 ————67-66-3 ———— -107-06-2 ————78-93-3 —————71-55-6 —————56-23-5 —————108-05-4 — - —75-27-4 —————78-87-5 —————10061-01-5 ——79-01-6 —————124-48-1 ————79-00-5 —————71-43-2 —————10061-02-6——75-25-2 —————108-10-1 — - —591-78-6 ————127-18-4 ————79-34-5 — - — -108-88-3 ————108-90-7 ——— -100-41-4 ——— -100-42-5 — - —1330-20-7 —— -107-02-8 ————107-13-1 ————

—— Chloroaathana—— Broaoaathana—— Vinvl Chlorida—— Chloroathana—— Mathvlana Chlorida-— Actton*-—Carbon Diaulfid*— -1. 1-Dichloroathana——1, 1-Dichloroathana- — 1,2-Dichloroathana (total) __—— Chl oro form——1 1 2 — Di Chloroathana- — 2-Butanona—— 1 . 1 . l-Trichloro«thana—— Carbon T«trachlorid«—— Vinyl Acatata—— Bronodiehloroia«than«—— 1 . 2»DichloroDronan«— -cia-1. 3-DichlorooroDan«— - Trichloroathana— — Dibronochl or onathana-—1 . 1 . 2-Trichloro«than«—— B«nz«n«— -Trana-l, 3-Dichloropropana __—— Broaoforn..— -4-M«thyl-2-P«ntanon«-«2-Haxanona ,—— Tat rachl ora*than«— -1 ,1,2, 2-Tatrachloroathana __~»Toluan«—-Chl orobanz ana—— Ethylbanzana- — Styantt—-Total Xylanaa , _.— -Acrolain— -Acrylonitrila

10.80.910.8310.90.90.90.9141111111111i21110.910.91122026

UUUUJUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU


DP TO SUMMBR 5


EPA SAMPLE HO,

Lab Name: COMPUCHEM LABS______^_

Lab Code: CQMPU cave No.: OQQQ

Matrix: (»oil/water) WATER

Sample wt/vol: 20.0 (g/aL) MLLevel: (low/ned) LOW



Number TIC« found: _fl

VBLKAAContract: SAS4231E

SAS No.: 4231E SDG No.: EAS13

Lab Sample ID: VBLKAA

Lab File ID: CB89Q311A12



Dilution Factor:




SPMPLE DPTff


EPA SAMPLE NO.

Lab Nam«: CQMPOCHEM IABS________

Lab Cod*: COMPU Cas* No.: QQQQ

Matrix: (soil/water) WATERSampla vt/vol: 20.0 (g/mL) ML

Laval: (low/m«d) LOW

% Moistura: not dac. __


VBLKACContract: SAS4231E

SAS NO.: A231E SDC No.: EAG13

GAS NO. COMPOUND

Lab Sample ID: VBLKAC____

Lab Fil« ID: CB89Q312A12



Dilution Factor:


74-87-3—————-Chloronethana_________74-83-9———---Bromomethana__________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroethane__________75-09-2——————Mathylana Chlorida_____67-64-1——————Acetone_____________75-15-0———————Carbon Di»ulfide________75-35-4———————l,l-Dichloroath*n«______75-34-3————-—l,l-Dichloro«thana______540-59-0——————1,2-Dichloroethene (total),67-66-3—————Chloroform___________107-06-2——————l,2-Dichloro«than«______78-93-3—————— 2-Butanon«____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon T«trachlorida____108-05-4—————Vinyl Acatat*_________75-27-4—————Bromodichloromathana____,78-87-5—————-1,2-Dichloropropana_____10061-01-5———-cis-l,3-Dichloropropan«__79-01-6—————Trichloroathana________124-48-1—————Dibromochloromathana____79-00-5——————1,1,2-Trichloroathana___71-43-2—————™B*nz«na_____________10061-02-6———Tran»-l,3-Dichloropropan«_75-25-2—————BroBOfom____________108-10-1—————4-M«thyl-2-P«ntanona____591-78-6-———•—2-H«xanona___________127-18-4—————Tatrachloro«th«n*_______79-34-5—————-1,1,2,2-Tatrachloroathan*..108-88-3-————-Tolu«n«—_________.^_MM_108-90-7—————-Chlorobanzana__________100-41-4—————-Ethylbanzane___________100-42-5—————Styran*_____________1330-20-7—————Total Xylanas_________107-02-8—————Acrol«in_____________107-13-1—————Acrylonitrile_________

10.80.912310.90.90.90.9141111111111121110.910.91122026


SfWPLE OPTff


EPA SAMPLE NO.

Lab Name: COMPOCHEM L A B S _ _ _ _

Lab Code: COMPU Case No.: OQQQ

Matrix: (soil/water) WATERSample wt/vol: 2O.Q (g/mL) ML




Nunbar TICs found: _Q

VBLKACContract: SAS4231E

SAS No.: 4231E SDG No.: EAS13

Lab Sample ID: VBLKAC____

Lab File ID: CS890312A12



Dilution Factor: +*&-/. 0 Ob




SffMFLE OffTP SUMMPRV

1AVOLATILE ORGANZCS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Nam*: COMPUCHEM LABS_______Lab Cod«: COMPU Gas* No.: 0000

Matrix: («oil/watar) WATERSanpla vt/vol: 20.0 (g/mL) MLLaval: (low/mad) LOW

% Moimtura: not dac. ___Column: (pack/cap) PACK

EAG13Contract: SAS4231ESAS No.: 4231E SDG No. : EAG13

CAS NO. COMPOUND


Lab Fila ID: CN048714A12

Dat* Racaivad: 03/06/89

Data Analyzad: 03/10/89Dilution Factor: 4iO • i-c


74-87-3——————Chloromathana__________74-83-9—————-Broaom«than«__________75-01-4————-—Vinyl Chlorida________75-00-3——————chloro«than«______;___75-09-2——————M«thyl«na Chlorida_____67-64-1——————Acatona_____________75-15-0———————carbon Dimulfid*________75-35-4———————l,l-Dichloro«than«______75-34-3———————l,l-Dichloro«than«______540-59-0——————1,2-Dichloro«th«n« (total).67-66-3—————-Chloroform___________107-06-2——————l,2-Dichloroathan«______78-93-3—-----2-But«non«___________71-55-6——————1,1, l-Trichloro«than«___56-23-5——————carbon Tatrachloride____108-05-4——————Vinyl Acatata__________75-27-4—————Bromodichloromathan«____78-87-5——«™1,2-Dichloropropana_____10061-01-5——™ci»-l,3-Dichloroprop«na__79-01-6—————Trichloro«th«n«________124-48-1—————DibromochloroBiathana____79-00-5———————i,l,2-Trichloro«than«____71-43-2————— B*nz«n«_____________10061-02-6————Tran»-l,3-Dichloroprop«na_75-25-2——™—Bronoforn___________108-10-1——————-4-M*thyl-2-P«ntanon«____591-78-6——————2-H«xanon«____________127-18-4—-———Tatrachloroathana_______79-34-5——————1,1,2,2-T«trachloro«than«_108-88-3—————-Tolu«n«_______________108-90-7 —————*chlorob«nzan*_________100-41-4—————Ethylb«n*«na__________100-42-5—————styr«n«_____________1330-20-7—————Total Xylan«>__________107-02-8-™--—Acrolain_____________107-13-1—————Acrylonitrila_________

l0.80.912610.90.90.90.9141111111111121110.910.91122026

FORM I VGA 1/87 R«v,

SOHPLE DP TO SUHHBRV


EPA SAMPLE NO

Lab Name: COMPPCHEM LABS_______Lab Cod*: CQMPU Case No.: QQOO


Sample vt/vol: 20.0 (g/B>L) ML



Number Ties found: o

EAG13Contract: SAS4231E

SAS NO.: 4231E SDG No.: BAG13




Date Analyzed: 03/10/89Dilution Factor:




SBHPLE 52


EPA SAMPLE NC


Lab Coda: COMPU Casa No.: 0000





Column: (pacJc/cap) PACK

CAS NO. COMPOUND

EAC14Contract: SAS4231E

SAS NO.: 4231E SEW No.: EAG13


Lab Pile ID: CN048715B12



Dilution ractor: -4-s-e-/.oCONCENTRATION UNITS:(ug/L or ug/Kg) PG/L

74-87-3——————Chloronethane_________74-83-9——————Bronomethane__________75-01-4——————Vinyl Chloride________75-00-3-————-Chloroethane__________75-09-2——•———Methylene Chloride______67-64-1——————Acetone_____________75-15-0———————Carbon Diiulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroe thane______540-59-0——————1,2-Dichlproethene (total),67-66-3——-———Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5————-Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4———————Bromodiehloroinethane____78-87-5—————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1-————-Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2—-————Benzene_____________„10061-02-6———Tran«-l,3-Dichloropropene_75-25-2—--———Bronofom,___________.108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————'Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————-Toluene ____________108-90-7—————Chlorobenzene_________100-41-4————-Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenea_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VGA

0.80.9

10.90.90.90.9140.6111111111121160.910.9112

2026

1/87 Rev,

OPTP SI


EPA SAMPLE NO


Lab coda: CQMPP cac* No.: QQooMatrix: (soil/water) WATERSample vt/vol: 20.o (g/aL) MLLevel: (1ow/med) LOW




EAG14Contract: SAS4231ESAS No.: 4231B * SDG No.: gAC13


Lab Fil« ID: CN04871SB12

Dat« R«c«iv«d: 03/06/89

Data Analyzed : 03/10/89

Dilution Factor: 4-rft-y £


GAS NUMBER COMPOUND NAME RT•

EST. CONC.- Q


50


EPA SAMPLE NO

Lab Name: CQMPUCHEM LABS_______Lab code: CQMPU caee No,: 0000

Matrix: (eoil/water) WATER

Sample vt/vol: 20.0 (g/mL) MLLevel: (low/med) LOW .

% Moisture: not dec. —_mColumn: (pack/cap) PACK

GAS NO. COMPOUND




Lab File ID: CNQ4872QA12



Dilution Factor:CONCENTRATION UNITS :(ug/L or ug/Kg) Ufl/L

r

74-87-3———————Chloromethane__________74-83 -9-—————Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2———————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3-————Chloroform___________107-06-2——————1,2-Dichloroe thane______78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroe thane___56-23-5—————-Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————-Bromodiehloromethane____78-87-5———————1,2-Dichloropropane_____10061-01-5———ci»-l,3-Dichloropropene__79-01-6—————-Trichloroethene________124-48-1————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2————-Benzene______________10061-02-6——--Tran«-l,3-Dichloropropene_75-25-2-—-———Bromoform___________108-10-1—————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetraehloroethene______79-34-5——————l,l,2,2-Tetrachloroathane_108-88-3————-Toluene ____________m108-90-7——-——Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————-styrene_____________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein___________107-13-1—————Acrylonitrile_________

l0.80.912510.90,90.90.9141111111111121110.910.91122026

a-'

FORM I VOA 1/87 Rev

SPHPLE DP TO 49


EPA SAMPLE NC


Lab Code: CQMPU case No.: OQQQ




* Moisture: not dec. ____


Number TICs found; 0




Lab File ID: CNQ4872QA12


Date Analyzed: 03/10/89Dilution Factor: -*-*-'

CONCENTRATION UNITS:(ug/L or ug/Kg) US/L



oar* sunna*v 48


EPA SAMPLE NO

Lab Nana: COMPUCHEM LABS________Lab Coda: CQMPU caaa No.: QQQQMatrix: (soil/vatar) WATERSanpla vt/vol: 20.0 (g/mL) ML_


% Moisture: not dac. ___Column: (pack/cap) PACK

EAG16Contract: SAS4231ESAS No.: 4231E SDG No.: EAG13

ofGAS NO. COMPOUND

Lab Sanpla ID: 248721

Lab Fila ID: CK048721A12

Data Racaived: 03/06/89


Dilution Factor: +1-6- t.G J&


74-87-3——————Chloronathana_________74-83 -9——--——Broaonathana__________75-01-4——————Vinyl Chlorida________75-00-3————-—Chloroathana___________75-09-2——————Mathylana Chlorida_____67-64-1——————Acatona_____________75-15-0——————Carbon Diaulfida_______75-35-4——————1, l-Dichloroathana_____75-34-3———————1,1-Dichloroathana______540-59-0——————1,2-Dichloroathana (total),67-66-3——«——Chloroform____________107-06-2——————1,2-Dichloroathana______78-93-3——————-2-Butanona___________71-55-6——————1,1,1-Trichloroathane___56-23-5———————Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4—————Bronodichloronathana____78-87-5—————i,2-Dichloropropana_____10061-01-5—-—-cis-l,3-Dichloropropana__79-01-6——————Trichloroathana________124-48-1—------Dibronocbloromathana____79-00-5——-——--1,1,2-Trichloroathana____71-43-2-—————Ban x an a_______________10061-02-6--™-Tran»-l,3-Dichloropropana_75-25-2—————Bronofonn___________108-10-1——————4-Mathyl-2-Pantanona____591-78-6—————2-Haxanona___________127-18-4—————Tatrachloroathana_______79-34-5——————1,1,2,2-Tatrachloroathana_108-88-3————Toluana_____________108-90-7—————Chlorobanzana_________100-41-4—————Ethylbanzana__________100-42-5—————Styrana_____________1330-20-7—————Total Xylanas_________107-02-8———-—Acrolain_____________107-13-1—————Acrylonitrila_________

0.80.9

310.90.90.90.914111111111.112111010112

2026


DBTP


• EPA SAMPLE NO,

Lab Nama: COMPUCHEM LABS________

Lab Coda: COMPU Cas* No.: OQOQ

Matrix: (soil/vatar) WATERSanpla wt/vol: 20.0 (g/mL) MLLaval: (low/nad) LOW

% Moistura: not d«c. ___


Numbar TIC« found: _a



Lab Saapla ID: 248721

Lab Fil« ID: CNQ48721A12



Dilution Factor:




SBHPLE


EPA SAMPLE NO


Lab code: COMPU case No.: QQQo

Matrix: (soil/water) WATERSample wt/vol: 20.0 (g/mL)




CAS NO. COMPOUND



Lab Sampla ID: 248722 ____

Lab Tila ID: CN048722A12



Dilution Factor:


74-87-3—————Chloro»e thane_________74-83-9-—————Bromomathana__________75-01-4——————Vinyl Chloride________75-00-3—————Chloroa thane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total),67-66-3—————-Chloroform___________107-06-2—————1,2-Dichloroe thane_____78-93-3——————2-Sutanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4———————Bromodichloromethane____78-87-5—--———1,2-Dichloropropane_____10061-01-5-———ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________12 4 -4 8 -1———"Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2—————-Benzene_______________10061-02*6————Tran»-l,3-Dichloropropene_75-25-2———————Broaofom_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenxene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes__________107-02 -8 ——————Acrolein.______________107-13-1—————Acrylonitrile_________

0.80.9

10.90.90.90.9141111111111121110.910.91122026

FORM I VOA 1/87 Rev

S0HPLE DPTB 45


EPA SAMPLE NO

Lab Nan*: COMPUCHEM TABS________

Lab Code: COMPU case No.: oooo


Level: {1ow/med) LOW



EAG17Contract: SAS4231B

SAS No.: 4231E SDG NO.1 EAC13



Date Received: 03/06/89Date Analyzed: 03/10/89Dilution Factor:





EPA SAMPLE NO

Lab Name: COMPUCHEM LABS Contract: SAS4231EEAG18

Lab Coda: COMPU Ca*« No.: OQQQ SAS NO.: 4231E SDG NO.: EAG13


Level: (low/aed) LOW



notCAS NO. COMPOUND





Dilution Factor :


74-87-3——————Chloroaethane_________74-83-9—————Bromomethane__________75-01-4———————Vinyl Chloride_________75-00-3——————Chloroe thane___________75-09-2———————Methylene Chloride______67-64-1———————Acetone_______________75-15-0———————Carbon Disulfide________7 5-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3———-—Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone___________71-55-6————-—1,1,1-Trichloroe thane____56-23-5-————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————-Bromodichloromethane____m78-87-5————*——1,2-Dichloropropane_____10061-01-5————ci«-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochlorome thane____79-00-5—————1,1,2-Trichloroethane____71-43-2—————Benzene_____________10061-02-6———Tr«n«-l,3-Dichloropropene_75-25-2—————Bromoforw_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—-——-Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4 ————--Ethylbenzene__________100-42-5————-Styrene_____________1330-20-7————Total Xylenes_________107-02-8——•——Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VGA

0.80.9

10.90.90.90.9141111111111121110.930.91122026

1/87 Rev

SBHPLE 00 TO SUHMORV


EPA SAMPLE NO

Lab Name: CQMPUCHEM IABS _____Lab Cod*: COMPU Case No.: QQQO




* Moieture: not dec. ____












SQHPLE SUMM8BY


EPA SAMPLE NO

Lab Name: CQMPnCHEM LABS________

Lab Code: COMPU Case No.: QOQO

Matrix: (soil/water) WATERSample vt/vol: 20.0 (g/aL) ML

Level: (low/Bed) LOW




SAS NO.: 4231E SDG No.: EAG13.

CAS NO. COMPOUND


Lab File ID: CN048724B12



Dilution Factor: -+T-O- I<C &


74-87-3 — - —74-83-9 ————75-01-4 ———— •75-00-3 ———— -75-09-2 ——— -67-64-1— —— •75-15-0 ————75-35-4 ———— -75-34-3 ———— •540-59-0 ——— •67-66-3 ———— -107-06-2 ——— •78-93-3 ———— •71-55-6 ———— •56-23-5 ———— •108-05-4 ——— -75-27-4 ———— -78-87-5 ———— •10061-01-5——79-01-6 —— -«124-48-1 ——— •79-00-5 —— ——71-43-2 ———— •-10061-02-6 — -75-25-2™ — -108-10-1 ——— -591-78-6 ——— -127-18-4 — -—79-34-5 ———— -108-88-3 ——— -108-90-7— — -100-41-4 —— —100-42-5 —— —1330-20-7 —— -107-02-8 ——— -107-13-1 ——— -

— — Chloromethane

-——Vinyl Chloride— — Chloroethane—— Methylene Chloride-—-Acetone,

-——1 . l-Dichloroeth«ne

—— 1,2-Diehloroethene (total) __

-—— 2-Butanone ,——— 1 . 1 . 1-Trichloroethane•- —— Carbon Tetrachloride- —— Vinyl Acetate—— Bromodiehloromethane

• — -ei*-lf3-Diehloropropene ,— — Trichloroethene

• — -1 . 1 . 2-Triehloroethana— --Benzene — „-—— Tran«-l, 3-Dichloropropene—— -4-Methvl-2-Pentanone—— -2-Hexanone _

——1 ,1,2, 2 -Tetra Chloroethane __'—-Toluene

— — Styrene

——Acrylonitrile

10.8112210.90.540.9141111111111121110.910.91122026

U-U

uuuuuJuuuuuuuuuuuuuuuuuuuuuuuuuu


S0MPLE OffTff SUMM0RV

IEVOLATILE ORCANXCS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

Lab Name: COMPUCHEM tABS________

Lab Coda: CQMPU Case No.: 0000

Matrix: (aoil/water) WATER

Sample wt/vol: 20.0 (g/mL) MLLevel: (low/mad) LOW

% Moisture: not dac. ___


Numbar TICs found: _p.




Lab Fila ID: CN048724B12

Date Racaivad: 03/06/89


Dilution Factor:


CAS NUMBER COMPOUND NAME RT EST. CONC. ' Q


SBHPLE OffTff SUHM0RY 40

1AVOLATILE ORfiANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Nam«: COMPUCHEM LABS_________

Lab Coda: COMPU Case No.: OQQO

Matrix: (moil/water) WATER

Sample wt/vol: 2Q.Q (g/mL) ML


% Moisture: not dec. ___Column: (pacfe/cap) PACK


SAS NO.: 4231E - SDC No.: EAG13

CAS NO. COMPOUND





Dilution Factor:


74-87-3 ————--Chloronethane_________74-83-9™—-—-Brononethane__________75-01-4——————Vinyl Chloride________75-00-3——-———Chloroethane__________75-09-2———————Methylene Chloride______67-64-1———————Acetone ___________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroethene______75-34-3———————l,l-Dichloroethan«______540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3--————2-Butanone___________71-55-6———-——1,1,1-Trichloroethane___56-23-5——————carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4-—————Bromodichloromethane____78-87-5™—--—1,2-Dichloropropane_____10061-01-5———cis-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1——————Dibronochlorone thane____79-00-5—-————l, 1,2-Trichloroethane____71-43-2--————Benzene_______________10061-02-6——™Tran»-l,3-Dichloropropene_75-25-2——-———Bromofora____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——-————l,l,2,2-Tetrachloroethane_108-88-3————-Toluene_____________108-90-7———-—Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————styrene_____________1330-20-7—————Total xylenes_________107-02-8——-——Acrolein_____________107-13-1—————Acrylonitrile_________

l0.80.912210.90.90.90.9141111111111121110.910.91122026

FORM I VGA 1/87 Rev

SfMPLE OP TO SUHM0BY


EPA SAMPLE NO.

Lab Nan*: COMPUCHEM LABS

Lab Code: COMPU Cas* No.: QQQQ

Matrix: (coil/water) WATER

Sanpl« vt/vol: 20.0 (g/mL) ML

Laval: (low/m«d) LOW

% Moi»tur»: not d«c. ___



EAW91Contract: SAS4231ESAS NO.: 423IE SDG No.: EAG13

Lab Sampl« ID: 248726____

Lab Fil« ID: CNQ4B726B12

Data R«c«iv«d: 03/06/89

Dat« Analyzed: oa/io/as

Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) nc/L



Of) TO


EPA SAMPLE HO.

Lab Kama: COMPUCHEM LABSEAW92

Lab Code: COMPU Cace No.: OQQOMatrix: (soil/water) WATER


Leva1: (1ow/med) LOW



Contract: SA54231E

SAS No.: 4231E SDG No.: EAG13_

CAS NO. COMPOUND





Dilution Factor:


g o/i"'

Q

74-87-3—-————ChloroBe thane_________74-83-9—-———-Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3———————Chloroe thane___________75-09-2——————Methylene Chloride_____67-64-1———————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total)57-66-3——————Chloroform___________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————-Bromodichloroinethane____78-87-5———--— 1,2-Dichloropropane_____10061-01-5———-ci*-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1————Dibromochloronethane____79-00-5———————1,1,2-Trichloroethane____71-43-2——-———Benzene_____________10061-02-6™-—Tran«-l,3-Dichloropropene_75-25-2——————Bromoforn_____________108-10-1—————4-M«thyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3*————Toluene ____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbeniene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenem__________107-02-8—-——-Acrolein_____________107-13-1—————Acrylonitrile_________

0.80.91

610.90.90.90.9141111111111121110.910.9112

2026

FORM I VOA 1/87 Rev

SOHPLE DBTO SUHMQRV jr


EPA SAMPLE NO"


Lab code: CQMPU Case No.: OQQQ

Matrix: (soil/water) WATERSample vt/vol: 20.Q (g/mL) ML




Number TICs found: _a


SA5 No.: 4231E SDG No.: EAG13_

Lab Sample ID: 24872B




Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Xg) uc/L



SQHPLE SUMMBRV


EPA SAMPLE NO.

Lab Nana: COMPUCHEM LABS________

Lab Coda: COMPIJ case No.: QQQQ

Matrix: (aoil/watar) WATERSaaple vt/vol: 20.0 (g/aL) ML

Laval: (low/Bad) LOW

% Moistura: not dac. ___Column: (pack/cap) PACK

CAS NO. COMPOUND


SA5 No.: 4231E SDG No.: EAG13

Lab Saapla ID: 248730____

Lab Fila ID: CN04373QA12



Dilution Factor: -4 i o- /.0 . ,


74-87-3—————-Chloromathana_________74-83 -9—————Bronomathana__________75-01-4——————Vinyl Chloride________75-00-3———————Chloroathana___________75-09-2———————Mathylana Chlorida______67-64-1———————Acatona_______________75-15-0———————Carbon Diaulfida________75-35-4——————1,1-Dichloroathana_____75-34-3——————1,1-Dichloroathana_____540-59-0—————-1,2-Dichloroathena (total).67-66-3——-———Chloroform,___________107-06-2—-———1,2-Dichloroathana_____78-93-3 ——————2 -Butanona___________71-55-6———————1,1,1-Trichloroathana____56-23-5———-—Carbon Tatrachlorida____108-05-4—————Vinyl Acatata__________75-27-4—————Bromodichloromathana____78-87-5—————1,2-Dichloropropana_____10061-01-5————cis-l,3-Dichloropropana__79-01-6——————Trichloroathana________124-48-1—————DibroBOchloromathana____79-00-5———--—1,1,2-Trichloroathana____71-4 3 -2——————Banzana_____________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2--————-Broaofora____________108-10-1—————4-Mathyl-2-Pantanona____591-78-6—————2-Haxanona___________127-18-4—————-Tatrachloroathana_______79-34-5——————1,1,2,2-Tatrachloroathana_108-88-3—————Toluana_____________108-90-7—————Chlorobanzana_________100-41-4—————Ethylbanzana__________100-42-5—————Styrana_____________1330-20-7—————Total Xylanaa_________107-02-8—————Acrol«in___________107-13-1—————Acrylonitrila_________

10.80.912210.90.90.90,9141111111111121110.910.91122026

*/

FORM I VOA 1/87 Rav,

SAMPLE OffTff SUKMBRV JS

IEVOLATILE ORGANZCS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO,

Lab Nan*: CQMPUCHEM LABS__________

Lab Cod*: COMPU case No.: QQQQ








SAS No.: 4231E SDG No.: EAGIT





Dilution Factor:




OP TO SUHHQRV 34

1AVOLATILE ORGANICS" ANALYSIS DATA SHEET

EPA SAMPLE NO.

Lab Nama: COMPUCHEM IABS_________

Lab Coda: COMPU Casa No.: 0000

Matrix: (soil/vatar) WATER

Sampla wt/vol: 20.0 (g/mL) MLLaval: (low/mad) LOW

% Molstura: not dac. __.Column: (pack/cap) PACK

CAS NO. COMPOUND

CAW94Contract: SAS4231ESAS NO.: 4231E SDG No.: EAC13





Dilution Factor:CONCENTRATION UNITS:(ug/L or ug/Kg) cc/L

74-87-3—————Chloromathana__________74-83-9---™——Bromomathana___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroathana__________75-09-2——————Mathylana Chlorida_____67-64-1——————Acatona_____________75-15-0———————Carbon Disulfide________75-35-4———————1,1-Dichloroathana______75-34-3——————1,1-Dichloroathane_____540-59-0——————1,2-Dichloroathana (total).67-66-3——-——Chloroform___________.107-06-2——————1,2-Dichloroathana______78-93-3--—————2-But«nona____________71-55-6——————1,1,1-Trichloroathana___56-23-5—————Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4——-——Bromodichloromathana____78-87-5—-————1,2-Dichloropropana_____10061-01-5————ci«-l,3-Dichloroprop«na__79-01-6——————Trichloroathana________124-48-1————Dibromochl or omathana____79-00-5———————1,1,2-Trichloroathana____71-4 3 -2————- Ban z an a_____________10061-02-6—-——Tran«-l,3-Dichloroprop«n«_75-25-2—-———Bromoform_____________108-10-1——————4-M«thyl-2-Pantanona____591-78-6—————2-Haxanona___________127-18-4—————Tatrachloroathana______79-34-5———————l,l,2,2-Tatrachloroathan«_108-88-3——————Toluana_______________108-90-7—------Chlorobanzana__________100-41-4—————Ethylbanzana__________100-42-5—————Styrana_____________1330-20-7——-—Total Xylanas__________107-02-8————-Acrolain_____________107-13-1—————Acrylonitrila_________

l0.80.912310.90.90.90.9141111111111121110.90.80.91122026

V


SPHPLE t>8TP SUHHBRY 3*3"


EPA SAMPLE NO.

Lab Nam«: COMPUCHEM LABS__________

Lab Coda: CQMPU Ca** No.: 0000

Matrix: (»oil/wat«r) WATERsampla wt/vol: 20.0 (g/mL) ML

Laval: (low/mad) LOW% Moistura: not dac. —__Column (pack/cap) PACK

Number Ties found: _Q




Lab Pil* ID: CN048731A12

Data R«c«iv«d: 03/06/89Dat« Analyzed: 03/11/89

Dilution Pactor: «4- - A



PORM I VOA-TIC 1/87 R«v,

SPMPLE OffTff


EPA SAMPLE NO

Lab Nana: COMPUCHEM IASS________

Lab Coda: COMPU Casa No.! OOQQMatrix: (soil/water) WATERSampla wt/vol: 20.Q (g/mL) ML_


% Moistura: not dac. __.



SAS No.: 4231E SDC No.! EAG13

CAS NO. COMPOUND


Lab Fil« ID: CN048732A12



Dilution Factor:


74-87-3——————-Chloronathana__________74-83-9—————Broaomathana__________75-01-4——————Vinyl Chlorida________75-00-3——————Chloroathana__________75-09-2——————Mathylana Chlorida_____67-64-1——————Acatona_____________7 5-15-0———————Carbon Diaul f ida________75-35-4———————1,1-Dichloroathana______75-34-3———————1,1-Dichloroathana______540-59-0——————1,2-Dichloroathana (total),67-66-3—-———Chloroform___________107-06-2——————1,2-Dichloroathana______78-93-3—————2-Butanona___________71-55-6——————l, 1,1-Trichloroathana___56-23-5————-—Carbon Tatrachlorida____108-05-4—————Vinyl Acatata_________75-27-4—————Bronodichloromathana____78-87-5——-----1,2-Dichloropropana_____10061-01-5———«ci»-l,3-Dichloroprop«ne__79-01-6——-———Trichloroathana________124-48-1——-——DibroBochloromathana____79-00-5———————1,1,2-Trichloroathana____71-4 3 -2———————B«nzana_______________10061-02-6———Tran»-l,3-Dichloropropan«_75-25-2——————Bromoform____________108-10-1————4-M«thyl-2-Pantanona____591-78-6—————2-Haxanona___________127-18-4——-——Tatrachloroathana______79-34-5—————-1,1,2,2-Tatrachloro«thana_108-88-3——-—-Toluana_____________108-90-7————-Chlorob«nzana__________100-41-4————-Ethylbanzana___________100-42-5—————Styrana_____________1330-20-7————Total Xylanaa_________107-02-8—————Acrolain_____________107-13-1—————-Acrylonitrila_________

l0.80.912310.90.9

280.914111111711112

151

100.910.9112

2026

FORM I VGA 1/87 Rav

S8MPLE DBT0

IEVOLATILE OPGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.


Lab Code: COMPU case No.: QQQQ


Sample wt/vol: 20.0 (g/»L)




Number TICs found: _fi


SAS NO.: 4231E SDG NO. : EAG13_


Lab File ID: CNQ4B732A12



Dilution Factor:




D0TB SUMH0RY


EPA SAMPLE NO

Lab Nana: CQMPDCHEM LABS

Lab Coda: COMPP casa Ho.: QQQQ

Matrix: (soil/vatar) WATERSanpla vt/vol: 15.0 (g/mL) ML

Laval : (low/mad) LOW

% Moistura: not dae. _ __Column: (pack/ cap)


SAS NO.: 4231E SDG No.: EAG13_

CAS NO. COMPOUND


Lab Fila ID: CR048738B12

Data Racaivad: 03/Qfi/89


Dilution Factor:


74-87-3—————Chloroaathana___________74-83-9——————Broaoaathana____________75-01-4——————Vinyl Chlorida__________75-00-3——————Chloroathana____________75-09-2———————Mathylana Chlorida________67-64-1———————Acatona_________________75-15-0———————Carbon Diaulfida__________75-35-4——————1,1-Dichloroathana________75-34-3————-—1,1-Dichloroathana________540-59-0—————1,2-Dichloroathana (total)__67-66-3————---Chloroform_____________107-06-2——————1,2-Dichloroathana________78-93-3——————2-Butanona_____________71-55-6——————1,1,1-Trichloroathana_____56-23-5——————Carbon Tatrachlorida______108-05-4——————Vinyl Acatata____________75-27-4——————-Broaodichloronathana_______78-87-5—--———1,2-Dichloropropana_______10061-01-5————-cia-ljS-Dichloropropane____79-01-6——————Trichloro«thana__________124-48-1—————Dibroaochloroaathana______79-00-5—————-—1,1,2-Trichloroathana______71-43-2——-——Banzana________________10061-02-6-—™Tran»-l,3-Dichloropropana__75-25-2—-———-Bromoforn______________108-10-1—————4-Mathyl-2-Pantanona______591-78-6————-2-Haxanon«_____________127-18-4—————Tatrachloroathana_________79-34-5——-———1,1,2,2-Tatrachloroathana__108-88-3—"•———Teluana______________108-90-7—-———Chloroban* ana___________100-41-4—————EthylbMisana____________100-42-5—————styrana________________1330-20-7—————Total Xylanaa___________107-02-8—————Acrolain_______________107-13-1—————Acrylonitrila___________

2111221351116

34121220.721222226010.811132735

u

/^(^L, tfr AsCejfc^FORM I VOA

sfasCWC.-1/87 Rev,

29


EFA SAMPLE NO

Lab Nan*: CQMPUCHEM IABS________

Lab Coda; CQMPTJ casa No.: ooooMatrix: (aoil/vatar) WATERSample wt/vol: 15.0 (g/mL) ML


* Moistura: not dac. ___


Nuntbar TICs found: _1


SAS No. : 4231E SDG No. : EAG13_


Lab Fila ID: CRQ48738B12



Dilution Factor:

CONCENTRATION UNITS:(ug/L or ug/Kg) us/L

CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.98

EST. CONC.

4.0

Q

F"


SBMPLE OPTff


EPA SAMPLE NO

Lab Nan*: COMPurHEM LABS________

Lab Cod*: COMPU Cace No.: QQQQ

Matrix: (moil/water) WATERSample wt/vol: 20.0 (g/nL) ML

L«v«l: (low/iwd) LOW

% Moisture: not d*c. ___„


EAW97Contract: SAS4231ESAS No.: 4231E SDG No.: EAG13

CAS NO. COMPOUND



Data R«c«iv«d: 03/06/89


Dilution Factor:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3---—-——Chloronethan*_________74-83-9-—————Brononethana__________75-01-4——————Vinyl Chloride________75-00-3—————Chloroethane___________75-09-2——————Methylen* Chloride_____67-64-1——————Acetone_____________75-15-0———————Carbon Disulfida________75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethan*______540-59-0——————1,2-Dichloroethene (total).67-66-3-—————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3-——————2-Butanone____________71-55-6———————1,1, l-Trichloro*thane____56-23-5———————Carbon Tetrachloride____108-05-4—————Vinyl Ac«tat«_,_______75-27-4———————BroBOdichloronethane____78-87-5--——-—1,2-DiChloropropane_____f10061-01-5———-ci»-l,3-Dichloroprop«n«__79-01-6——————Trichloro«th«ne________124-48-1————Dibronochloromethane____79-00-5—————1,1,2-Trichloroe than*____71-43-2———————Benzene________;______10061-02-6———-Tran«-l,3-Dichloropropen*_75-25-2—————Bronoforn_____________108-10-1——————4-Methyl-2-Pentanone_____591-78-6—————2-Hexanone____________127-18-4—————T«trachloro«th*ne______79-34-5———————1,1,2,2-T«trachloro«than*_108-88-3————--Toluane_______________108-90-7————Chlorob«nz«n*_________100-41-4—————Ethylbenzene__________100-42-5-———-styr*n«____________1330-20-7—————Total Xylanes_________107-02-8—————Acrol«in_____________107-13-1—————Acrylonitril*_________

0.820.523126

2000.924611111

531121211890.90.823172026

U'U

U

Ui/

FORM I VGA 1/87 Rev

SOMPLE OffTff SUMMffRY


EPA SAMPLE NO



Matrix: (soil/water) WATERSample vt/vol: 20.Q (g/mL) ML






SAS No.: 423IE SDG No.: EAG13

Lab Saaple ID: 248741____



Date Analyzed: Q3/12/89Dilution Faetor:-*n»- f.P

CONCENTRATION UNITS:(ug/L or ug/Kg) DG/L

CAS NUMBER

1.

COMPOUND NAME

FRZON

RT

13.47

EST. CONC.

5.0

Q

V

/


SOMPLE SUMMBRV


EPA SAMPLE NO

Lab Name: COMPUCHEM tABS________

Lab Coda: CQMPU Case No.: 0000

Matrix: (soil/water) WATERSampla wt/vol: 5.5 (g/mL) ML


% Moisture: not dec. ___Column: (pack/cap) PACK

CAH97REContract: SAS4231E


CAS NO. COMPOUND


Lab File ID: C2R48741A12



Dilution Factor: +rO- 1.0CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3————™ Chloronethane__________74-83-9—————Brononethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Disulfida_______75-35-4——————l,l-Dichloroethene_____75-34-3——————1,1-Dichloroethane_____540-59-0—————1,2-Dichloroethene (total).67-66-3——————chloroform___________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanona______,____71-55-6———————1,1,1-Trichloroethane____56-23-5—————-Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————BroBOdichloromethane____78-87-5——------1,2-Dichloropropane_____10061-01-5————cis-l,3-Dichloropropene__79-01-6——————Trichloroethane________124-48-1—————Dibronochloromethane____79-00-5—————--1,1,2-Trichloroe thane____71-43-2——-——-Benzene______________10061-02-6--—«Tran»-l,3-Dichloropropene_75-25-2——————BroBoforn____________108-10-1—————-4-Methyl-2-Pentanone____591-78-6————2-Hexanona___________127-18-4————-Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3————Toluene_____________108 -90-7—————Chlorobenzena_________100-41-4—-——-EthyIbenzene__________100-42-5—————styrene_____________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

533438434

1703415344454

43445464566323243

7396

uDDUUUDJUUuuuDUUuuuuuDUDJUDJUDJUU

FORM I VGA 1/87 Rev

SOMPL£ OffTP SUMMPBV


EPA SAMPLE NO.

Lab Nan*: CQMPUCHEM LABS________Lab Code: CQMPU Case No.: OOQQ






SAS NO.: 4231E SDG No.: EACH.



Date Received: 03/Q6/B9


Dilution Factor:


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.95

EST. CONC. •

25

Q

V

tWW j}

^*\sf*r


DBT8 24


EPA SAMPLE NO.

Lab Nana: COMPUCHEM LABS

Lab Coda: COMPU ca*« Ho.: QQQQ

Matrix: («oil/watar) WATERSampla wt/vol: 20TQ (g/mL) ML

Laval: (low/»ad) LOW

% Moistura: not dac. ___Column: (pack/cap) PACK

CAS NO. COMPOUND


SA5 No.: 4231E SDC No.: EAG13


Lab Flla ID: CRQ48742A12



Dilution Factor:


74-87-3——————Chloroaathana_________74-83-9——————Bromomathana__________75-01-4——————vinyl Chloride________75-00-3——————Chloroathana__________75-09-2——————Mathyl«n« Chlorida_____67-64-1——————Acatona_____________75-15-0——————Carbon Diaulfida_______75-35-4——————1,1-Dichloroathana_____75-34-3———————1,1-Dichloroathana______540-59-0——————1,2-Dichloroathana (total),67-66-3—————Chloroform __________107-06-2—————1,2-Dichloroathana_____78-93-3———————2-Butanona____________71-55-6———————1,1,1-Trichloroathana____56-23-5—————-Carbon Tatrachlorida____108-05-4——————Vinyl Acatata__________75-27-4—————Bromodichloromathana____78-87-5—————-1,2-Dichloropropana_____10061-01-5———-ci»-l,3-Dichloroprop«na__79-01-6——————Trichloroathan*________124-48-1————-Dibro»ochloronathana____79-00-5———————1,1,2-Trichloroathana____71-43-2——-——Bantana_____________10061-02-6—-—-Tran*-l,3-Dichloropropan«_75-25-2—————Broaofora_____________108-10-1——-——-4-Mathyl-2-Pantanona____591-78-6——-—-2-Haxanona___________127-18-4-———-T«trachloroathana______79-34-5———-——l,l,2,2-Tatrachloroathana_108-88-3—————Toluana_____________108-90-7—————Chlorob«ncana_________100-41-4——-——Ethylbanzan*__________100-42-5——————Styrana_______________1330-20-7—————Total Xylana*_________107-02-8——-—-Acrolain_____________107-13-1—————Acrylonitrila_________

10.80.911210.90.910.91411111

" 11111121110.950.9112

2026


SfUIPLE


EPA SAMPLE NO


Lab Code: COMPU Cave No.: QOOQ

Matrix: (moil/water) WATER


Level: (lov/med) LOW



Number TIC* found:




Lab File ID: CR048742A12



Dilution Factor: 4 i o • /. 6 .


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.98

EST. CONC.

3.0

Q

~

-f-vx /C&UL, fa0&?<sL*Zs&~f]

JJj^MMsf(

gJistrl*^^ ^H^} sfi*


SBMPLE Off TO


EPA SAMPLE NO.



Matrix: (soil/water) WATERSample vt/vol: 20.0 (g/mL)


% Moisture: not dec. __Column: (pack/cap) PACK



CAS NO. COMPOUND




Date Analyzed: 03/10/89Dilution Factor: •4r»/.£


74-87-3 ——-——Chloromethane_________74-83 -9——————Bromonethane__________75-01-4——————Vinyl Chloride________75-00-3———•——Chloroe thane__________75-09-2——————Methylene Chloride_____67-64-1———--—Acetone._____________75-15-0———————Carbon Disulfide________75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Diehloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3—————Chloroform_____________107-06-2——•——1,2-Dichloroethane_____78-93-3————-2-Butanone.___________71-55-6——————1,1,1-Trichloroe thane___56-23-5—————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____,78-87-5—————1,2-Dichloropropane_____10061-01-5———cis-l,3-Diehloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochl or ome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2——•———Benzene_______________10061-02-6———Tran»-l,3-Dichioropropene_75-25-2—————Broa»oforn_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane-.108-88-3————Toluene_______________108-90-7—-———Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.821

910.9140.9141111110.6111121110.90.60.91122026

3'

1/87 Rev

S0MPLE OPTff SUHHQRY

IEVOLATILE ORSANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO,

Lab Nama: CQMPUCHEM LABS________

Lab Coda: COMPP Case No.: QQQQ


Sampla wt/vol: 20.Q (g/mL) MI.

Laval: (low/nad) LOW



Number TIC* found: _Q


SAS NO.: 4231E SDG No.: EAC13

Lab Saapltt ID: 2487*4


Data R«c«iv«d: 03/06/89

Data Analyzed: Q3/1Q/89

Dilution Factor: >4re-/.t'i

CONCENTRATION UNITS:(ug/L or ug/Kg) PC/I.



SOHPLE SUMMBRY

UHITEO STATH CHWOlwSWTAL nOTECTlOMKCIOH V .

CSw/Central ttglonal laboratoryDATA TEACKtMC fQP* rQR CONTRACT

CM. Data Stt Ho C£*Cm Ho

Ctse No. MQ^| S l? Site Mem and Location: Uo^n/nC UJ.DIUA* of. Contractor or EFA Laboratory: COYViftJudi^ BUa User:

no, of Samples: [Cr? Date Staples or Omti Rtcifvtd:

1. »Uvt ch»ln*of-custody rtco^ds betn rtcifved? T£S —— IUL2. H»vt TtatUc Reports or pacfcing lists been recetveTT" Tt3. tf no, are Traffic Report or puking lf»f numbers written on the chata-of -custody

record? t£S «0 __ t4* If no. which Traffic report or packing list numbers art slsslng?

Art basic data forms in? YES HO

Number of san^lts claimed:, / fc Huatfatr of samples received: / X^

by: ________ Cj{ _____ Jj CM }

-ejvtd by Contract Project Management Section: sCJY?L/?L Date

Stirttd: ^? /)H**>6& IWI Reviewer SI §aaturt:

Total tiffit sptnt on rtvte**: / tA** . Date review canpleted:

Copied (xeroxed) by: r*^ ________________ Date:

«a.iled to Data User by: 0 C/' A^r C^ . .A^n Date;

DATA USERS:

Please fill In the blanks belo* and return this fora to: SjlvU CrUfln, DataHanagement Coordinator. Region V. SSCJU.

Data received by: ______^^^______ Patt:

O.A. review rtctivtd by:________________________fi»tt:

Inorganic Date CompleteOrganic Data Complete

ComplttoSAS Data Complete

, SuUjble for Intended Purposes ! 3 /E 1 if acceptable.List problem below.f ]. Suitable for Intended Purposes '. \

L ' • Suitable for Intended Purposes \ J[ \ . SuUable for Intended Purposes . J

See Attache* 'Missing DaU fewest Form* C 110BLEMS: Please indicate reasons (if my} xhy data art not suUiblt for your uses.

Other problems*

Received by Data Minagewent Coordinator^ CRL for File: Date:

ifir/ff

i orUNITED STATES ENVIHONMENTAL PROTECTION AGENCY

REGION V

/EJECT: Review of Region V CLP DataReceived for Review on

Curt is Ross. 9*r%£*-j-* <{*y*i.}Central Regions: kiboraitf;? ff. /

Tft »•" u"r: ———————C^cX————————— MAR 30 1989

We have reviewed tht data for ihe following caje{s)*SITE NAME: \l LUW\& (U&JM juiLcflvO CM. »o.

C R L I O . Z^5' // ,• .S/ - 5 .

CLP Liber.tory:

Following are Our findings:

( VData are acceptable for use. -—-~( i / l Data are acceptable for use wit / i

See Data Qualifier sheets and C 'additional comments.

t / Data are preliminary - pending . /^ * t r~ n —ISee Case Summary above. 4vZ^r/\ V lAJ-f- Kc--'^ -L

( ) Data are unacceptable. ' v ' ;

cc: CarTa Dempsey.CLP Quality Assur. , ,James Petty. Chief Quality Assui /c^

DATA QUALIFIERSPAGE 2^ OF L?

Contractor:

I.Below is a summary of the out-of-control audits and the possible effect on thedata for this case:

(D

Reviewed by:Phone:Date: J?/ (

DATA QUALIFIERSPAGE J_ OF L?

Contractor: (Case


Reviewed by;Phone;Date; J.7 272

PAGEDATA QUALIFIERS

Contr.ctor:


SfTVL-^-t >t y%/VL^ «r

Reviewed by;Phone:Date: 21

CASE/SAS 0

UN1TEO STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDS

OF

Instrument * £?9DATE/TIME: 3--2-S^ /^5"/

CnloromethaneBromomethane "Vin^l ChlorideChloroethaneHethylene ChlorideAcetoneCarbon nisuiflde1,1-Oichloroethane1.1-DichloroetheneTrans-l.Z-DichioroetheneCnloroformZ-Butanone

,2-D1! Chloroethane,1 ,1-Trichioroethane

Carbon TetrachlorldeVin\l AcetateBroôdi cnl oromethane1,2-DichioropropaneTrans-1 ,3-OichioropropeneTrichloroetheneDibromochloromethane1 .1 ,2-TricM oroethaneBenzeneCTSÎ ,3-Dichioropropene2 Chle^BetHjivinyiothe^Bromoform4-Methyl-Z-Pentanone2-HexanoneTetrathloroethenel.l.Z.Z-Tetrachi oroethaneTolueneCnlorobenzeneEthylbenzeneStyrenei^Xylene t TOTAL)0/p,Yyl8na hCRQLEIN

AFFECTEDSAMPLES:

Reviewe-'s *,/ , _rt #gInitials/Date: ftf W>*1

Inlt* Cal.

ki/r>TItfQ

I'ii

otf

A 2.•17

r*ft

Srrn(IRSO

.sr

i?ii

*ta a

f'T/*

T/

t

J

7/^

Cont. Cal.H-jkl-i,r/Ti^

rl/T

, ?

^?rlfrfc

•

,^30VL

f? ^'îb •

w

TRt/Âtl

EAM/D*eA.W23&kVI/ 10

Cont. Cal*3-*/-3? 7:31RFIr37Ttt

tltf

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These flags should be applied to the analytes on the sample data sheets.

€/87

UN1TEO STATES ENVIRONMENTAL PROTECTION AGENCY REGION V_ CALIBRATION OUTLIERS

i t , l & l / i o,X2l-ATlLE HS1- COMPOUNDSCASE/SAS 9 / / T V 3/4-231E CONTRACTOR

°F &

Instrument * O°lDATE/T IME: 3-7-jW 2/;3^

CnlopomethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon nisulfideU-Dichloroethane1.1-DichloroetheneTrans-1 .Z-DichlopoetheneChlorofopmZ-ButanoneI.z-Dichlopoethane1.1.1-TrichloroethaneCarbon TetracniorideVinyl AcetateBro^Ddichloromethanel.Z-DicnloropropaneTrans-1 ,3-OichlopopPOpeneTpichloroetheneDi bromochl opomethanel.l.Z-TrichloroethaneBenzenecis-l,3-DichioropPOpene

B r 0^ D T 0 TfTifl-Methyl-Z-PentanoneZ-Hexanone

ITetrachloroethene1 ,1 ,Z,Z-TetPachloroethaneTolueneCnlorobenzeneEthyl benzeneStyreneivXylene CT^r*L)

AFFECTEDSAMPLES:

Reviewe-'s ., ./Initials/Date: ffl f-fctf\

1m?/kfi.lb

\t*^&

jQ&b

OLl

i6H

;. Cai"? JitIRSD

34>K

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These flags should be applied to the analytes on the sample data sheets*

€/87

For reporting reeulta tr "be OSX?A. tba fallowing contract apaeificualifiera era ta be uaed. Tba aeven quellflera daflnad below

«ofc subject ta •edification by tba laboratory. Up to flvaqualifiera may ba raportad an Farm Z far each caapound.

The ecron ZFA-deflaed qualifiers ta ba oaad are aa fellova:

» Zndieatea compound was analysed for but not detected. Tbeaeaple quantitation liait auat be corrected for dilution andfor percent no is cure. For exsaple, 10 U for phenol ia water iftbo aaapla final voluae ia tba protocol-specified final value.Zf a 1 ta 10 dilution of attract ia neceaaery, the reportadliait ia 100 9. For a aoil aaaple, the value auet el«a beadjusted for percent •eistura. For aouaplo, if the aaapla bed24% •oiature gaA a 1 ta 10 dilution factor, tbo aaaploquantitation liait far phenol (330 V) would be corrected ta:

100

and df * dilution factor

at 24% aoiatura, 0 • 100.34 . 0.74100

f MO tn.76

10 - 4300 U ronndad ta tba approprlata nuabar ofal ifieant figuraa

For aoll aaaplaa aubjaetad ta CTC elacn-up proeaduraa, tha C&QZ.ia alao antltipliad by 2, ta account far tba fact that only•f tba extract ia racovarad.

C •

Zadieataa an aatiaatad value. Tbia flag ia uaad aitbar vbanaatiaacing a aoneantration for tantativaly identified coapeundavbara a 1:1 raaponaa ia aaaunad, or vban tba naaa apaceral ditaindicate tha praaanaa of a coarpovmd tbet Meta tbaidentification criteria but tbe reault ia laaa tnan tbe aaapleojuantitaeian liait but greater then sare. For aaceBpla; if thaaeaple queatitetian liait ia 10 uf/X., but a concentration of 3«C/L ia celculeted, report it ee 3J. Tbe aeaple quentitetlon"t*a*1 _ ——— . —ea diacuaaed for the V flag, ao that if a aaaple with 24%aoiature and a 1 to 10 dilution factor baa a calculatedconcentration of 300 ug/L and a aeaple quentitetion liait of430 vf/kf. report the ooncantretien aa 300J on Fora Z.

Thia fleg appllea to poatieida reaulta Acre the identificationboa been confined by GC/H5. Single cooponent peaticideang/ul in tba final extract ahall bo eonfiiaad by CC/MS.

B-29 2/88

£2.

This flag *• *sod whan tho aaalyta ia fiound la the associatedblank as wall as ia the Maplo. Zt ladicataa possible/probableblank contamination sad vans tba data user to take appropriateAction, this flag mt*t bo used for a TIC aa well aa for afoaitivoly ida&tlfiad TCL

B * Thf • &og idaatifisa laapgmdi whose •oneoarxations exceed the•alibration range of tho CC/M5 l&atrtaMOC for that *p*cificanaljala. thia flag will ait «Ppl7 ta faatieldaa/K3a an«ljx»dby CC/ZC •atfaoda. Zf ana or BOTO •napnimdi bavo a roapoaaaf oatar âa full aaala, tfca aaMpla or oxtraet auat bo dllutadamd ro*aaal7xo4 aaaordlag to tiba aToclflaAtloaa la frbThlc D.All auch •••yiiuiiti vita a roapoftoo groatar tfeaa full aealoateuld bar* taa ooucoucxatiou flauod vith a& •!• oa tho Ton 1for Cfco original aaalTaia. Zf tao dilution of tb« oxtraet

________ mlTT** ^ boWlov ta« calibration Mago ia tto Aoferoaolta of both aaalyooa shall b« roportad o& aaparato ToIho Fora X for tao dttvtod aaayla ahall bavo tho •DL* auf fixaypoadad to tao aaapla va^bor. 90IZ: for toeal zylonoa. vh< :»Chroo laoaara aro fuaadflod aa two poaka, tao calibration

af •«gfc **«le ahvold bo ooacldorod ooparataly, «.(.. aaaaljila la agfc taqolrod for total xylonos unltas

oatratlon of olthor foak aaparataly axeaoda 200 uj/L.

B * thia flag idaatlfiaa all aaa>pnimrti Uontlflod la aa aaaljals ar• aaeondazy dilution factor. Zf a aaa lo or oztraet laro-aaalyxod at a blghar dilution factor, aa la tho *Z* flagabow, tho *DL0 auf fix ia appotkdod ta tho aaxplo ouab«r on ch^fora I for tho dllutod aaaflo, and *11 eonesaeration valuajvoportad oa that fora Z aro flagxod with tho *D* flag.

Ihis flag indicates that a TIC ia a suspected«ldal««ond«nsation product.

Other specific flags say bo required to properly define tlvosults. Zf used, they smut bo fully described and suchdescription attachod ta the gampla Bsta TIHHII j faekage and vCaao Harrative. login by uaiag "XV Zf store than one flag i

•—and *8*i as nilqualifiers are required for a sample rnault, use tho *X" flaxto oaafeiao soveral dags, aa aaodad. for Instance, tho *X*Gag might BMMns tho "A". •**. and "D" flags for some sampi

ilnatloa of flags "BO*ilaaata aro flagged »g

•avplo.

is «xproasly prohibited. II..vn«a they aro also detected in •?

If analyses at two different dilution factors are required ('••Exhibit B>, follow the data reporting Instructions glv*n In £xhd ard vith tho *0* and "I" nags above.

B-30

rIk.-RR 0 0 fl« CENTRAL REGIk.-AL LAUORATPHY SAMPLEVATA REPORT

rV

rfu«»/ u; i»*si unuMwiua/n\ IUMUI O Gu&DlPr&' 4/o,- 7^Hf£ft-FUM) $*& THIS FORM IS TO BE USED FOR SAMPLES SENT TO CONTRACT ONLY ' i l l'*.5€ NUMBEfl/SAS «- '• 7T3/ *r25/o SIIFMAUF lAfA irl W^M. /'Ux<-tC lAnnnAinnv C-/y*- i C/tJ^?l n41K «M««« /--''* * ^ff'tt

iUPtriFUND OU NUfc S'VftC THCI^- 1 f".5- EPA RPM or C

AC1IVIIY NUMBER JL^j*'*^ \ 1 1~ ft 1 (/*£-

CRL LOGNUMBER

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PO HC,K HID Al { XANUFI IA . VA j>J]13

70 I/'.W .M'lt) I IS '.'j/ -"t~lrl

APPUCAgLEr

ORGANIC TRAFFIC REPORT

tAMPLEAt 4.

t.«UM>AC8WA1VI2.QHOUNOWATVI1L1ACHAT1 ;..... 7.WAITI(tM)

LAIOflATOMY CONTRACT t«X UNTT PMOI

•AMPUNODMI:

SAMPUCONDITIONONMCOPT

HKJHCONCPHAMS(CHicn

RECEIVED IN300DCONDIT10

WHITE - SMO COPY PINK - CUEWT COPY WHITE - LAB COPY POP-RBTWW TO SMO YELLOW - LAB COPY

USEPA CONTRACT LABORATORY PROGRAMSAMPLE MANAGEMENT OFFICEPO BOX BIB ALEXANDRIA VA 22313

703/SW 2490 FTS «7 2440

ORGANIC TRAFFIC REPORT

TYPE C* ACTIVITY ipftCLtaa. <£SUPCTPUNO—PA'BI'UI JWTIMO MA m

NPLO -Otir-efflNBX _^__

ffNTBJt M BOX A) -4.1.BUWACiWATW2.QROUNO WATW B.OL<8AB)S.LEACHATE . , T.WASTf (BAB)

ATTM

SAMPUNaMTft

OATIWCIk_ ;ltM -fl?

LABOKATOKY COKTWACT NO. UNIT PMCC

HUNSPCN TCt OATI ftfC'O: / | _„

\h]

WHfTI - SMO COPY PINK - CLIENT COPY WHTTI - LAB COPY FOR RETURN TO SMO YELLOW - LAB COPY

Case Narrative-SAS* 4231ESDG No. EAU20

Contract: SAS4S31ECompuChem Laboratories* Inc

SAMPLE: EAW20, EAW21, EAW23, EAU33, EAW24, EAU2S, EAU36, EAUS7,EAU28, EAU29, EAW30, EAU31, EAW32, EAU33, EAW34, EAU3S,EAU36, EAU37, EAU38, EAU39

Attached art pert inent Quality Assurance not ices dealing with th*analysis of twenty (30) LOL water samples associated with SAStt 4231E,SOC No. EAU20 The samples were scheduled for volatile analysis.

The samples were received in good condition on March 153, 1989 withthe chain-of-custody in order. No irregularities were encounteredduring receipt of the sample.

Lower Detect ion Limit (LDL) Comments•1) Compuchem is following EPA rounding convention for CRQL's and

result reporting. Volatiles are reported to one significantfigure below ten.

2) J values are being reported down to half of modified CRQL.3) The word 'NO' on quantitation report means compounds were not

found and also means the compounds concentration was less thanhalf CRQL.

VOLATILES:All volatile fractions were prepared and analyzed within holdingtime requirements. The samples contained 0-32 Target Compounds.Some samples contained the Target Compounds, methylene chloride, ben-zene and acetone in varying concentrations. If these compounds werepresent in low levels in the associated blanks, all concent rat ionsw i l l be flagged with a '8'. Zero to eight Tentatively IdentifiedCompounds (TIC) were found. Many samples contained Freon, tentativelyidentified by NBS Library Search as 1,1,2-trichioro-1,2,2-trifluoro-ethane was detected. This is occasionally observed in volatile instru-ment blanks, and is known to be a commom lab artifact. The same compoundwas detected in the associated blank, but not at a sufficient concentra-tion to require a 1ibrary search. Nevertheless, the compound has beenflagged in the sample data with a 'B', denoting its presence in th* blankThe compound should be considered a lab contaminant not native to the as-received sample. Please note the attached QA notice. Some samples alsocontained an early eluting peak on the RIC believed to be an instru-ment artifact, which is a mixture of water and atmospheric gases ThisInstrument art ifact was also present in blank, VBLKFY, all samples as-sociated with this blank and contain this TIC, will be flagged with a 'B'In the inital injection, of the neat extract, of sample EAU34 containedsignificant amounts of nine <9) Target Compounds which were flagged withan '£' . Due to column overload* potent ial peak splitting and retentiontime shift, the quantitation in the neat injection is not meaningfullThe diiution/re-inject ion produced the data being reported. An attached <

laboratory not ice serves to clarify this data being; reported for th* neatand diluted injection. Also note the surrogates for the inital analysiswere flagged (*) on form 2A and should be disregarded. Th* surrogate re-covery of DS-toluene for ianple EAW36 was calculated using a secondaryion to confirm that a native compound was interfering with the normalquantitation ion. Samples EAUSS and EAU29 were identified as beingsampling blanks. These samples contained 4 and 2 target compounds re-spectfully. Since the preceding analyzed sample did not contain elevatedlevels of these compounds, we do not beleive the reported values are aresult of caryover. The original, MS and MSD comparisons and internalstandard recoveries were within the control limits

Release of the data contained in this hardcopy data package and in thecomputer readable data submitted on floppy diskette has been authorizedby the laboratory manager or his designee, as verified by the followings ignature.

Bett y J. AndershockTechnical ReviewerMarch 16, 1989

Note: This report Is paginated for reftrence and accountability in dcreasing numerical sequence.

2AWATER VOLATILE SURROGATE RECOVER*

Lab Name: CQMPUCHEM LABS________ Contract: SAS4231E;

Lab Code: CQMPO Case Ho.: QOQO SAS Mo.: 4231R SDG Mo, EAW20

010203040506070809101112131415161718192021222324252627282930

EFASAMPLE NO.

EAW20EAW21EAW22EAW23EAW24EAW25EAW26EAW26REEAW27EAW28EAW29EAW30EAW31EAH32EAW33EAW34EAW34REEAW35EAW36EAW37EAW38EAW39EAW36MSEAW36MSDVBLKAMVBLKANVBLKATVBLKFYVBLKYRVBLKXK

SI(TOL) 1

94102991101109711010110498102102106103106184 *97971071021081011021049610410110310198

52(BFB)#

9395941019910396991069610110899101100107959511510010498109109971061091039897

S3(DCE)I

898889959396999890919489949395210 *96949697102959393919793999492

OTHER TOTOUT

000000000000000200000000000000

QC LIMITS31 (TOt) - Toluene-d8 ( 88-110)52 (BPB) - Bromofluorobenzene ( 86-115)53 (DCE) * l,2-Dichloro«than«-d4 ( 76-114)

I Column to be used to flag recovery values* values outside of contract required QC limits


page 1 of 1FORM II VOA-1 1/87 Rev.

3AWATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

Lab Name: COMPUCHEM LABS_________ Contract: SA54231E

Lab Coda: COMPU Case No,: QQQQ SAS No.: 4231E SDG No.: EAW20

Matrix Spike - EPA Sample No.: EAW36______

COMPOUND

1, l-Dichloroetnena ___ _TrichloroetheneBenzeneTolueneChlorobanzene

SPIKEADDED(ug/L)

125125125125125

SAMPLECONCENTRATION

(ug/L)0

178000

MSCONCENTRATION

(ug/L)

138325141143143

MS%

REC #

110118113114114

QCLIMITSREC.

61-14571-12076-12776-12575-130

COMPOUND

1 , 1-Dichloroethene ___TrichloroetheneBenzeneTolueneChlorobenzene

SPIKEADDED(ug/L)125125125125125

MSDCONCENTRATION

(ug/L)

135311140143142

MSD%

REC *

108106112114114

%RPD #

211100

QC L3RPD

1414111313

•MITSREC.

61-14571-12076-12776-12575-130

# Column to ba used to flag racovary and RPD valuaa with an asterisk

* Values outside of QC limits

RPD: _£ out of _1 outside limitsSpike Recovery: _0, out of 1Q outside limits

COMMENTS: CLP ,4231,E£AW20,-EAW3,LOW,WATER,247650,PEST, ,TUNE: 0009 030589 0708

FORM III VOA-1 1/87 Rev.

TH SUJWfUTV 20"


Lab Name: COMPUCHEM LABS_________ Contract: SAS4231E

Lab Code: COMPU Case Mo.: QQOQ SAS Mo.: 4231E SDG No.: EAW2Q

Lab File ID: q98.9Q3Q3B09 Lab Sample ID: VBLKAM____

Date Analyzed: 03/03/89 Time Analyzed: 1636

Matrix: (soil/water) WATBB Level:(low/med) LOW

Instrument ID: Q9

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS AMD MSD:

010203

EPASAMPLE NO.

EAW20EAW28EAW29

LABSAMPLE ID

247520247531247532

LABFILE ID

CN047520B09CN047531B09CN047532B09

TIMEANALYZED

211118132022

COMMENTS: CLP ,4231,EEAW20,-EAW3,LOW,WATER,247647,PEST,BLANK,TUNE: 0009 030389 1457

page 1 of 1FORM IV VGA 1/87 Rev.



Lab Code: COMPU Case HO.: QQOO SAS Mo.: 4231B SDG Mo.: EAW2Q

Lab File ID: CB89Q3Q4AQ9 Lab Sample I-D: VBLKAM____


Matrix: (soil/water) wxrgB Level:(low/med) LOW

Instrument ID: 09


010203040506

EPASAMPLE NO.

EAW21EAW22EAW23EAW24EAW25EAW26

LABSAMPLE ID

247521247522247524247527247528247529

LABPILE ID

CN047521A09CN047522A09CN047524A09CN047527A09CN047528A09CN047529A09

TIMEANALYZED

101511011144122813351432


page 1 of 1FORM IV VOA 1/87 Rev.

f!TSflflPLfc OPT a SUIMflKV



Lab Code: CQHPU Case Mo.: OQQO SAS Mo.: 4231E SDG No.: EAW20

Lab File ID: gpfl9Q3Q5AQ9 Lab Sample ID: VBLKAT____



Instrument ID: 09


0102030405

EPASAMPLE MO.

EAW27EAW30EAW36EAW36MSEAW36MSD

LABSAMPLE ID

247530247533247650247523247525

LABFILE ID

CN047530A09CR047533B09CN047650B09CN047523B09CN047525B09

TIMEANALYZED

14461907162617271825




Lab Name: COMPUCHEM LASS________ contract: SAS4231E

Lab Coda: COMPU Ca*e MO.: QQQQ SAS NO.: 423iq SDC No.: EAW20

Lab File ID: gpa9Q3Q6AQ9 Lab Sample ID: VBLKFY___

Data Analyzed: 03/06/89 Tine Analyzed: 1437


Instrument ID: 09


01020304

EPASAMPLE NO.

EAW31EAW32EAW33EAW34

LAB •SAMPLE ID

24764S247646247647247648

LABFILE ID

CN047645A09CN047646B09CN047647B09CN047648B09

TIMEANALYZED

1541163517381825




Lab Nam«: COMPUCHEM LASS____.____ Contract: SAS4231E

Lab Coda: COMPU Ca«« Mo.: 0000 SAS No.: 4231E SDG No.: EAW20

Lab Fil« ID: gsa903Qaco9 Lab Sample ID: VBLKYRData Analyzed: os/oa/aq Tin* Analyzed: ossoMatrix: (aoil/wat«r) WATER L«v«l:(low/m*d) LOW

Instrument ID: 09


01020304OS

EPASAMPLE NO.

EAW26REEAH34REEAW35EAW37EAW38

LABSAMPLE ID

247929247648247649247651247652

LABFILE ID

C2R47529A09C2R4764SA09CR047649A09CR047651A09CN047652A09

TIMEANALYZED

13191223143410000908


pag« 1 of 1FORM IV VOA 1/87 R«v.

mj my?*r



Lab Coda: CQMPU Case Mo.: QQQQ SAS No.: 4231E SDG No.: EAW2Q

Lab File ID: c.ppQQ3Q8BQ9 Lab Sample ID: VBLKXK____



Instrument ID: 09


01

EPASAMPLE NO.

EAW39

LABSAMPLE ID

247653

LABFILE ID

CR047653B09

TIMEANALYZED

2135

COMMENTS: CLPTUNE: 0009 030889 1535

page 1 of 1FORM IV VOA 1/87 Rev,


EPA SAMPLE NO.


Lab Code: COMPU Case No.: OOQQ






CAS NO. COMPOUND

VBLXAMContract: SAS4231E


Lab Sample ID: VBLKAM____

Lab File ID: CB89Q3Q3B09



Dilution Factor:


74-87-3——————Chloromethane__________74-83-9—————-Bromomethane__________75-01-4——————vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total),67-66-3——————Chloroform____________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane____56-23-5-————--Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4-——-——-Bromodi chloromethane____78-87-5—«——-1,2-Dichloropropane_____10061-01-5-———ci«-l,3-Dichloropropene__79-01-6-————-Trichloroethene________124-48 -1————--DibroBOchlorome thane____79-00-5———————1,1,2-Trichloroe thane____71-43-2——————Benzene_____________10061-02-6™——Tran»-l,3-Dichloropropene_75-25-2——————Bromoform____________108-10-1——————4-Hethyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane..108-88-3————Toluene..m_____________108-90-7—————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5—————styrene_____________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

FORM I VGA

10.80.911610.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE WO


Lab Code: CQMPU Case No.: OOQQ



Level: (1ow/med) LOW

% Moisture: not dec. , __


VBLKAMContract: SAS4231E


Lab Sample ID: VBLKAM____

Lab File ID: CB890303BQ9


Nu r TICs found: _p.


Dilution Factor:


NUMBER COMPOUND NAME RT EST. CONC. Q


M, nu t if


EPA SAMPLE NO.


Lab Code: CQMPU Case No.: oooo






VBLKANcontract: SAS4231E


CAS NO. COMPOUND

Lab Sample ID: VBLKAN___Lab File ID: CB8903Q4AQ9



Dilution Factor:


74-87-3--———-Chloronethane__________74-83-9—-—-----Bromomethane__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroe thane__________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Diaulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-bichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3——-——-Chloroform____________107-06-2——————1,2-Dichloroe thane______78-93-3——————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4————-Bromodichloroaethane____78-87-5-—————1,2-Dichloropropane_____10061-Q1-5-———ci«-l,3-Dichloropropene__79-01-6——————Triehloroethene__;______124-48-1——-—-DibroTOChloromethane____79-00-5——————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-6————Tran«-l,3-Dichloropropene_75-25-2—————-Broaoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_loa-88-3—————Toluene_____________loe-90-7—————-Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylenes_________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

10.8

0.7210.90.90.90.9141111111111121110.910.91122026

FORM I VOX 1/87 Rev,

U


EPA SAMPLE NC


Lab Code: COMPU Caie No.: QOQO



L«vel: (low/med) LOW



Number TICs found: _fi

VBLKANContract: SAS4231E


Lab Sample ID: VBLKAN ____

Lab File ID: CB8903Q4AQ9



Dilution Factor: «-rft /. o





EPA SAMPLE NC


Lab Code: COMPU ca*e No.: QQOQ





Column: (pack/cap) PACT

VBLKATContract: SAS4231E


CAS NO. COMPOUND

Lab sample ID: VBLKAT___Lab File ID: CD8903Q5AQ9


Dilution Factor:


74-87-3—————Chlorow thane__________74-83-9—-———Bromome thane__________75-01-4——————Vinyl Chloride________75-00-3—— ------Chloroethane___________75-09-2———————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform___________107-06-2—-—-—-1,2-Dichloroethane______78-93-3—————2-Butanone___________71-55-6———————1,1,1-Trichloroe thane___56-23-5——•—•—Carbon Tetrachloride____108-05-4————Vinyl Acetate_________75-27-4—-—-—-Bromodichloromethane____78-87-5———-—1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochl or ome thane____79-00-5———————1,1,2-Trichloroe thane___71-43-2——————Benzene_____________10061-02-6———-Tran»-l,3-Dichloropropene_75-25-2——-——BroBOform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6-————-2-Hexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7———-—Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/37 Rev,


EPA SAMPLE NO


Lab Coda: COMPU Ca»e Wo.: OQOQ







VBLKATContract: SA54231E


Lab Sample ID: VBLKAT____

Lab File ID: CD890305A09



Dilution Factor:

CONCENTRATIOM UNITS:(ug/L or ug/Kg) UG/L



10-



Lab Code: COMPP Case Ho.: 0000


Sanple wt/vol: 20.Q (g/mL) ML

Level: (low/Bed) LOW



EPA SAMPLE MC

VBLKFYContract: SAS4231E


Lab Sample ID: VBLKFY

Lab File ID: CD890306A09



Dilution Factor: 4- 0 /. °


74-87-3——————chloromethane_________74-83-9—————Bromomethane___________75-01-4——————-Vinyl Chloride_________75-00-3——————Chloroethane__________75-09-2——————Mathylene Chloride______67-64-1——————Acetone_____________75-15-0——————carbon Diaulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————l,2^Dichloroethene (total).67-66-3-————-Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3 ———————2-Butanone____________71-55-6——————1,1,1-Trichloroethane____56-23-5——————carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4 ——————Bromodichlorometnane____78-87-5——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————-Trichloroethene________124-48-1—————Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2—————Benzene_____________10061-02-6———Tren«-l,3-Dichloropropene_7 5-2 5-2 ——•———Bromof ona_____________108-10-1——-—~4-H«thyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4————Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—------Tolu«n«_________________108-90-7—————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7————-Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOX

10.80.912210.90.90.90.9141111111111121110.910.9112

2026

1/87 Rev


EPA SAMPLE NO


Lab Code: COMPU case No.: 0000Matrix: (soil/water) WATER






VBLKFYContract: SAS4231E


Lab Sample ID: VBLKFYLab Pile ID: CD89Q306A09



Dilution Factor: 4i-9- /.O


CAS NUMBER

I.

COMPOUND NAME

INSTRUMENT ARTIFACT

RT

0.58

EST. CONC.

6.0

Q

J


1AVOLATILE ORGAN1CS ANALYSIS DATA SHEET

EPA SAMPLE NO


Lab Code: COMPU case Ho.: OOQQ



Level: (low/»ed) LOW



VBLKYRContract: SAS4231E

SAS No.: 4231S SIX* No.: EAW2Q

Lab Sample ID: VBLKYR




Dilution Factor: 4-r-fr f- °


74-87-3——-———Chloromethane__________74-83-9——————Bromome thane__________75-01-4——————Vinyl Chloride_________75-00-3——————Chloroethane___________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0———————carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone_____________71-55-6———————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____108-05-4—————-Vinyl Acetate__________75-27-4——————Bromodi Chloromethane____78-87-5————«1,2-Dichloropropane_____10061-01-5—-™ci»-l,3-Dichloropropene__79-01-6—————-Trichloroethene_______124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene_____________10061-02-6—--—Tran»-l,3-Dichloropropene_75-25-2™——« Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————-Tetrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3™———Toluene_____________108-90-7™———Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylenee_________107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912610.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO

Lab Name: COMPUCHEM LASS

Lab Coda: COMPU Case No.: pQQQ


Sample wt/vol: 20.Q (g/mL)





VBLKYRContract: SAS4231E


Lab Sa&ple ID: VSLKYR____



Date Analyzed: Q3/oa/89

Dilution Factor:





EPA SAMPLE NO

Lab Name: CQMPUCHEM LABS__________

Lab Code: COMPU Case Ko.: QOQQ






CAS NO. COMPOUND

VBLKXKContract: SA54231E


Lab Sample ID: VSLKXK

Lab File ID: CD890308BQ9


Date Analyzed: 03/08/8?

Dilution Factor: 4-rfr Ao

CONCENTRATION UNITS:(u«j/L or ug/Kg) UG/L

74-87-3——————Chloroaethane__________74-83-9——-——— Bromoaethane___________75-01-4——————Vinyl Chloride________75-00-3——————chloroethane__________75-09-2———————Methylene Chloride______67-64-1——————Acetone_____________75-15-0———————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total).67-66-3—— -———Chloroform___________107-06-2——————1,2-Dichloroe thane______78-93-3———————2-Butanone____________71-55-6——————1,1,1-Trichloroethane____56-23-5—————--Carbon Tetrachloride____108-05-4————-Vinyl Acetate_________75-27-4—————-Bromodichloromethane____78-87-5——-—— 1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————Benzene_____________10061-02-6———-Tran*-l,3-Dichloropropene_75-25-2——-—— Bromoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6———-—2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—-———Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylenee_________107-02-8—————Acrolein_____________107-13-1——————Acrylonitrile__________

FORM I VOA

10.80.912410.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NC


Lab Coda: CDMPU case No.: 0000






VBLKXKContract: SAS4231E

SAS No.: 4231E SDG Wo. : EAW2Q

Lab Sample ID: VBLKXK

Lab File ID: CD89Q3Q8B09


Dilution Factor: 4rfr/.o


'CAS NUMBER COMPOUND NAME RT EST. CONC. Q



EPA SAMPLE NO

Lab Name: COMPUCHEM LABS Contract: SAS4231EEAW20

Lab Code: COMPU case No.: OQQO


Level.: (low/med) LOW





Lab File ID: CN04752QB09



Dilution Factor: 4-r6 /. o


74-87-3—————-Chlorome thane__________74-83-9———————Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3———-———Chloroethane___________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total),

, 67-66-3——-———Chloroform___________107-06-2—————-1,2-Dichloroethane______78-93-3—————2-But a none____________71-55-6——————1,1,1-Trichloroethane___56-23-5——-—-—Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4————-—BroModichlorome thane____78-87-5———-—1,2-Dichloropropane_____10061-01-5———-ci«-l(3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1————-DibroBOchloromethane____79-00-5——————1,1,2-Trichloroethane___71-43-2————--Benzene_____________10061-02-6———Tran»rl,3-Dichloropropene_75-25-2——————Bromoform_____________los-io-i——————4-M«thyl-2-Pentanone____591-78-6——•——2-Heacanone___________127-18-4—————Tetrachloroethene______79-34-5-™———-1,1,2,2-Tetrachloroethane_108-88-3™———Toluene_____________108-90-7—————-Chlorobenzene__________100-41-4————-Ethylbenzene__________100-42-5—————-Styrene_____________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Aerylonitrile________1

FORM I VOA

10.80.91

210.90.90.90.9141111111111121110.910.9112

2026

A I/

1/87 Rev.


EPA SAMPLE NC

Lab Name: COMPUCHEM LASS________

Lab Code: COMPU Ca»e No.: OQQO


Sample wt/vol: 20.Q (g/raL)

Leve1: (1ow/med) LOW




EAW20Contract: SAS42315


Lab Sample ID: 247S20




Dilution Factor: <rtt /. Q >j

COHCENTRAT10M UHITSr(ug/L or ug/Kg) UG/L

CAS NUMBER

1.

COMPOUND NAME

LABORATORY ARTIFACT

RT

12.65

EST. CONC.

2.0

Q

*#

13



Lab Nan«: COMPUC'HEM lAgg _____ Contract:

Lab Cod*: CQMPP Case Ho.: QQQQMatrix: (soil/watar) WATER

Sampl* wt/vol: 20.Q (g/mL) ML

L«val: (low/mad) LOW

% Moistura: not d«c. ____


EPA SAMPLE MO.

EAH21

SAS HO.: 4231E SDG No.: EAW2Q


Lab Pila ID: CN047S21AQ9

Data R«c»ivad: 03/01/89


Dilution Pactor:

CAS HO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3———-——chlorom* than*__________74-83-9——————Broaomathan*__________75-01-4——————vinyl Chlorid*________75-00-3———————Chloroathan*___________75-09-2——————M«thyl«n* Chlorid*_____67-64-1————————AC«ton«__________________75-15-0——————Carbon Di«ulfid«_______75-35-4——————l,l-Dichloro«th«n«_____75-34-3——————l,l-Dichloro«thana______540-59-0——————l,2-Dichloro*th«n« (total).67-66-3——————Chloroform___________107-06-2—————l,2-Dichloro«than«_____78-93-3——————2-Butanon«___________71-55-6——————l,l,l-Trichloro«than«___56-23-5——————Carbon T«trachlorid«____108-05-4—————Vinyl Ac«tat«_________75-27-4——————Bro«odichlorom«than«____78-87-5-——-—-l,2-Dichloropropan«_____10061-01-5———ci»-l,3-Dichloroprop«n«__79-01*6——————-Trichloro«th«n«________124-48-1—————Dibromochloromathan*____79-00-5——————l,l,2-Trichloro«than«___71-43-2——-————B*ni«M_________________10061-02-6—-——Tran«-l,3-Dichloroprop«n«_75-25-2———-——Bromoform____________108-10-1———-——4-M«thyl-2-P«ntanon«_____591-78-6—————-2-H«xanon«____________127-18-4——-——T«trachloro«th«n«______79-34-5———-——l,l,2,2-T«trachloro«than«_108-88-3———————Tolu«n«_________________108-90-7—————Chlorob«nz«n«__________100-41-4———•—Etnylb«nzan«___________ioo-4 2 -5————-Styr«n«_____________1330-20-7————Total Xyl*n«»_________107-02-8——————Acrolsin______________107-13-1—————Acrylonitril*_________

PORN I VOA

10.80.912210.90.90.90.914111111111112110.90.910.91122026

1/87 Rev.


EPA SAMPLE NO

Lab Naaa: COMPtTCHEMEAW21

Lab Coda: CQMPP Ca«« Ho.: QQQQ

Matrix: (aoil/watar) WATERSampla vt/vol: 20.Q (g/nL) ML


% Moistura: not d«c. ___

column (pack/cap) PACK

Numbar Tics found: _1

Contract: SAS4231E


Lab Sanpl* ID: 247521____


Data Racaivad: Q3/Q1/89


Dilution Factor:


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.75

EST. CONC.

2.0

Q

^ "

FORK I VOA-TIC 1/87 R«v,


EPA SAMPLE NO


Lab Code: COMPU ca*e HO.: QOOQ







SAS Mo.: 4231E SDG No.: EAW20

CAS NO. COMPOUND


Lab File ID: CNQ47522AQ9



Dilution Factor:


74-87-3 —•—-—-Chloromethane__________74-83-9——-———Bromone thane___________75-01-4——————Vinyl Chloride________73-00-3——————Chloroethane__________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3—————-Chloroform___________107-06-2—————1,2-Dichloroethane_____78-93-3-————— 2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————-Bromodichlorome thane____78-87-5————«l,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————-Trichloroethene________124-48-1—-———Ditoremochlorome thane____79-00-5——————-1,1,2-Trichloroethane____71-43-2———-——Benzene_____________10061-02-6————Tr«n»-i,3-Dichloropropene_75-25-2——————Bromoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6———-—2-Hexanone___________127-18-4————-Tetr»chloroethene______79-34-5——————-l,l,2,2-Tetrachloroethane__108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————-Styrene_______________1330-20-7—————Total Xylenes__________107-02-8———•——Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev.


EPA SAMPLE NO


Lab Code: COMPn Case No.: QQQQ



Level.: (low/med) LOW



Number TICs found:







Dilution Factor: -4-^6 /.a


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.73

EST. CONC.

2.0

Q

^

^b*V

j&Lt



EPA SAMPLE NO


Lab Coda: COMPU case Mo.: QQOO



Lave1: (1ow/med) LOW





CAS NO. COMPOUND


Lab Pile ID: CNQ47524A09



Dilution Factor: -+TQ- /. o


74-87-3——————Chlorome thane__________74-83-9™———-BroBomethana__________75-01-4——————Vinyl Chloride________75-00-3——————Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total),67-66-3—— ————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3—————— 2-Butanone____________71-55-6——————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Broaodichloromethane____78-87-5—————1,2-Dichloropropane_____10061-01-5——«ci»-l,3-Dichloropropene__79-01-6——————-Trichloroethene________12 4 -4 8 -1————Dibromochloromethane____79-00-5—————--1,1,2-Trichloroe thane____71-43-2——•—-—Benzene_____________10061-02-6-——«Tr«n«-l,3-Dichloroprop«ne_75-25-2—————Bromoform____________108-10-1—————4-M«thyl-2-Pentanone____591-78-6———-——2-Hexanone____________127-18-4————--Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene__________100-41-4—————Etbylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenee__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev,


EPA SAMPLE NO

Lab Nam«: COMPUCHEM LABS________

Lab code: COMPU case Ho.: QQOO












Date Analyzed: 03/04/89Dilution Factor: 4-rfi-TA*_9'4-


CAS NUMBER

1.2.

COMPOUND NAME

INSTRUMENT ARTIFACTFREON

RT

0.573.73

EST. CONC.

5.02.0

QJ

r



EPA SAMPLE NO

Lab Nan*: COMPUCHEM LABS________

Lab Cod«: COMPU Case Ko.: 0000



L*v«l: (low/raed) LOW

% Moisture: not dec. _____




Lab Sanple ID: 247527

Lab File ID: CN047527AQ9



Dilution Factor: _ _ _ _ _


74-87-3——-—-Chloromethan*_________74-83-9——------Bromom* than*__________75-01-4——————Vinyl Chlorid*_________75-00-3——————Chloroethan*__________75-09-2——————M*thyl*ne Chloride_____67-64-1———————Acetone____________________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene_____75-34-3——————1,1-Dichloroethan*_____540-59-0——————1,2-Dichloroethene (total).67-66-3———-—"Chioroforn___________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon T*trachlorid*____108-05-4—————Vinyl Acetate_________75-27-4—-————Bromodichloromethane____78-87-5———————1,2-Dichloropropane_________10061-01-5—-——-ci«~1.3-DiehloroBrQDene79-01-6——————Trichloroethene_______12 4 -4 8 -1——-----DibroBOChloromethane____79-oo-S———————1,1,2-Trichloroethan*____71-43-2—————-Benzene_____________10061-02-6———.Tran»-l,3-Dichloroprop*ne__75-2 5-2 —-———Broaof orm____________________loa-io-i—————4-M*thyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4————-T*trachloroethene_______79-34-5——————1,1,2,2-Tetrachloro*than*_108-88-3———————Tolu«n*_________________108-90-7————-Chlorobenzena__________100-41-4—————Ethylbenzen*__________100-42-5—————Styren*_____________1330-20-7—————Total Xylenes_________107-02-8—————Acrol«in_____________107-13-1—————Acrylonitril*_________

FORM I VOA

10.80.912210.90.90.90.9141111111111128110.90.60.91122026

1/87 Rev,

- IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO

Lab Name: COMPUGHEM LASS_________










Lab Pile ID: CNQ47527A09



Dilution Factor: 4-rQ- i-o


CAS NUMBER

1. 64-17-5

COMPOUND NAME

ETHANOL

RT

1.50

EST. CONC.

5.0

Q

J



EPA SAMPLE N


Lab Code: COMPU Case Ho.: QQQQ



Lave1: (1ow/med) LOW



EAW25Contract: SAS42313






Dilution Factor: +r» A o


74-87-3-————-Chloromethane_________74-83-9—-—-—•Bromomethane__________75-01-4——————vinyl Chloride________75-00-3——————Chloroe thane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Dieulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total).67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone___________71-55-6———————1,1,1-Trichloroe thane___56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4--————-Bronodichloromethane____78-87-5-——— -1,2-Dichloropropane_____10061-01-5-————ci»-l,3-Dichloroprop«n«__79-01-6—————Trichloroethene_______124-48-1-————DibroBOChl or one thane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-6————Tran«-l,3-Dichloropropene_75-25-2——————Bromoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—-———2-Heacanone___________127 -18-4—————Tetrachloroethene______79-34-5——————-l,l,2,2-Tetrachloroethane_108-88-3————Toluene_____________108-90-7™——- Chlorobenzene__________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7———-—Total Xylenes__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111124110.910.91122026

1/87 Rev.


EPA SAMPLE NC

Lab Nama: CQMPUCHEM LABS________Lab Coda: COMPP ca«a Ho.: QOQQ

Matrix: (soil/watar) WATERSample wt/vol: 20.Q (g/mL) ML

Lava1: (1ow/mad) LOW

% Moistura: not d*c. __—Column (pack/cap) PACK

Numbar Ties found: _1

EAW2SContract: SAS4231E



Lab Fila ID: CNQ47528AQ9



Dilution Factor: 4-rQ t.O ;


CAS NUMBER

1.

COMPOUND NAME

INSTRUMENT ARTIFACT

RT

0.55

EST. CONC.

4.0

QJ

FORM I VOA-TIC 1/87 R«v,


EPA SAMPLE MC


Lab code: COMPO caie No.: 0000



* Moisture: not d«c. ___


' 4EAW26

Contract: SAS4231E






Dilution Factor: 4i-Q- /. o


74-87-3--————Chloromethane__________74-83-9——————Bromomethane___________75-01-4———————Vinyl Chloride_________7 5-00-3 ——————chloroethane__________75-09-2——————Methylena Chloride_____67-64-1——————Acetone__________•75-15-0——————carbon Disulfide_______75-35-4———————1,1-Dichloroe thane______75-34-3———————1,1-Dichloroethane______540-59-0—————1,2-Dichloroethene (total),67-66-3——————Chloroform___________107-06-2—————1,2-Dichloroethane_____78-93-3———----2-Butanone____________71-55-6——————1,1, 1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Broaodiehloromethane____78-87-5———-—-1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————'Trichloroethene________124-48-1————-DibrOBOChloromethane____79-00-5———•——1,1,2-Trichloroethane___71-43-2 —-———-Benzene_____________10061-02-6——™Tran»-l, 3-Dichloropropene_75-25-2————--—Bromoform____________108-10-1—-—-—4-Methyl-2-Pentanone____591-78-6-————2-Hexanona____________127-18-4—--——Tetrechloroa thane_______79-34-5———————1,1,2,2-Tatrachloroethana_108-88-3——————Toluene_______________108-90-7——-——Chlorobenzena__________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenas__________107-02-8———-—Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.821481118

14017847211111

1901161261

1500.9

2100.9121592026

1/87 Rev,


EPA SAMPLE NO

Lab Naa«: CQMPUCHEM LABS________

Lab Coda: CQMPP Ca«« Ho.: QQQQ


Sampla wt/voli 20.0 (g/mL) ML

Leval: (low/mad) LOW

* Moistur*: not d«c. ___


Numbar Tics found: _2



Lab Sampla ID: 247529

Lab Pil« ID: CNQ47529AQ9

Dat* R«c«ivad: 03/01/89


Dilution Factor: 4-r« /,a

CONCEHTRATION UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER

1. 115-07-12.

COMPOUND NAME

1-PROPENEFREON

RT

0.653.73

EST. CONC.

2.02.0

Q

J

V

0,

3



EPA SAMPLE NO


Lab Code: CQMPU Case No.: OQOOMatrix: (soil/wat«r) WATER

Sample wt/vol: 4.0 (g/mL) ML_


% Moisture: not d«c. _—Column: (paclc/cap) PACK



CAS NO. COMPOUND

Lab Sample ID: 247S29____




Dilution Factor:


74-87-3——-——-Chlorome thane_________74-83-9——------Bromomethane___________75-01-4——————Vinyl Chloride_________75-00-3————Chloroethane___________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_______________75-15-0——————Carbon Disulfide_______75-35-4——————'1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3—————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3-————2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————Bromodichl or ome thane____78-87-5————-1,2-Dichloropropane_____10061-01-5———ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1————Dibromochloromethane____79-00-5—-——-—1,1,2-Trichloroethane____71-43-2—-—•——Benzene_____________10061-02-6™——Tr an«-l, 3-Dichloroprop*n«_75-25-2————-Brcaoform_____________108-10-1——————4-Methyl-2-Pentanone____591-78-6————-—2-H«xanone_____________127-18-4——————Tetrachloroethane_______79-34-5-—-———1,1,2,2-Tetrachloroethane__108-88-3————--Toluene_______________108-90-7—————Chlorobenzene__________100-41-4—————Bthylb«nzene__________100-42-5—————styrene_____________1330-20-7——-—Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

74254

11055897168214656576

13065116867

1004

1304

13560100130

uuDJ

3

1/87 Rev


EPA SAMPLE NC

Lab Name: CQMPUCHEM LABS_______Lab Code: CQMPU Caee No.: oooo






Number TICs found: _ft

EAW26REContract: SAS4231ESAS No.: 4231E SDG No.: EAW20

Lab Sample ID: 247529 '

Lab File ID: C2R47S29A09



Dilution Factor:

CONCENTRATION DUITS:(ug/L or ug/Kg) UG/L



1AVOLATILE ORGAMICS ANALYSIS DATA SHEET

Lab Name: COMPUCHEM LABS________Lab Cod*: COMPU Case No.: OQQQ


Sample wt/vol: 20.Q (g/mL) JO,_




CAS NO. COMPOUND

EPA SAMPLE NO.






Date Analyzed: 03/05/39ft H

Dilution Factor:


74-87-3-——-—--Chloromethane__________74-83-9————---Bromome thane___________75-01-4——————Vinyl Chloride_________75-00-3--———-Chloroathane___________75-09-2——————Nathylane Chloride_____67-64-1———————Acetona______________75-15-0———————Carbon Disulfide_______75-35-4——————1,1-Dichloroethena_____75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Diehloroethene (total)67-66-3———----Chloroform___________107-06-2——————1,2-Diehloroe thane______78-93-3-————-2-Butanone___________71-55-6———————1,1,1-Trichloroe thane___56-23-5——————Carbon Tetrachlorida____108-05-4————vinyl Acetate_________75-27-4————-Bromodichloromethane____78-87-5™———1,2-Dichloropropane_____10061-01-5-———ci»-l,3-Dichloropropene__79-01-6———-—Trichloroe thane________12 4 -48-1————-DibroMOChl or ome thane____79-00-5———————1,1,2-Trichloroethane___71-43-2——————Benzene_____________10061-02-6———Tran»-l,3-Dichloropropene_75-25-2————-Bromofora_____________108-10-1——————4-M«thyl-2-Pentanone____591-78-6———•——2-Hexanone____________127-18-4 —————Tetrachl oroethena______79-34-5——-———l,l,2,2-Tetrachloroethane_108-88-3—— -----*Toluen«_______________108-90-7—-———Chlorobanzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene______________1330-20-7—————Total Xylenes_____•107-02-8—————Acrolein____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.911210.90.90.90.9141111111111121110.910.91122026

1/87 Rev.


EPA SAMPLE NO


Lab Coda: COMPU CaM Ho.: QOQQ

Matrix: (soil/watar) WATERSample wt/vol: 20.0 (g/mL) ML




Number TICs found:







Dilution Factor:


GAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.83

EST. CONC.

4.0

Q

**


1AVOLATILE ORGAK1CS ANALYSIS DATA SHEET

EPA SAMPLE NO.


Lab code: COMPP Gas* Mo.: QOQQMatrix: (soil/wat«r) WATERSample wt/vol: 20.0 (g/mL) ML


% Moisture: not dec. ___m



SAS NO.: 4231E SDG Mo.: EAW2Q

QJ

o

CAS NO. COMPOUND


Lab Pile ID: CN047531B09



Dilution Factor: 4-rQ- l-o

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

74-87-3--—--—-Chlorone thane_________74-83-9—————Bromoaethane__________75-01-4—————Vinyl Chloride________75-00-3——————chloroethane__________75-09-2——————Methylene chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Dieulfide_______75-35-4———————1,1-Oichloroethene______75-34-3——————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4———————Bromodiehloromethane____78-87-5—-——•——1,2-Dichloropropane_____10061-01-5———-ci»-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5——————1,1,2-Trichloroe thane___71-43-2——————Benzene_____________10061-02-6———Trans-l,3-Dichloropropene_75-25-2--—————BroBOform____________108-10-1—————4-*tothyl-2-Pentanone____591-78-6-————2-Hexanone___________127-18-4-——-—Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3————Toluene.._____________108-90-7--—-—-Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenea__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

0.80.9

510.930.90.914111111111112110.70.910.9112

2026

uuuuuuuiu ?uuuuuuuuuuuJuuuuuuuu

1/87 Rev,

, IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO

Lab Warn*: COMPUCHEM LABS________

Lab cod«: COMPU Case Ho.: OQQOMatrix: (soil/water) WATER





Number TICs found:


SAS NO.: 4231E SDG Mo.: EAW20


Lab File ID: CN047S31BQ9



Dilution Factor:

COMCEMTRATIOH UNITS:(ug/L or ug/Kg) UG/L

COMPOUND NAME

LABORATORY ARTIFACT

EST. CONC.

2.0

gj^rd^9 /*^"st*"j t IKJ&t*uU<tf £> tT fa

FORM I VOA-T1C 1/87 Rev,


EPA SAMPLE NO


Lab Code: COMPU case No.: OQOQ





Column: (pack/cap) PACK1

CAS NO. COMPOUND




Lab Pile ID: CNQ47S32B09



Dilution Factor: -4-rO /,


74-87-3———-——Chlorome thane_________74-83-9—————-Bromomethane___________75-01-4——————Vinyl chloride________75-00-3—-———Chloroethane___________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————l,l-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3—————Chloroform___________107-06-2———————1. 2*Diehloroethane78-93-3————2-Butanone___________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachlorid*____108-05-4—————vinyl Acetate_________75-27-4————-Bromodichloroaie thane____78-87-5—-------1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6—-———Trichloroethene________12 4 -48-1——————Dibromochloronethane____79-00-5——————1,1,2-Trichloroethane___71-43-2——————-Benzene______________10061-02-6———Tran»-l,3-Dichloropropene_75-25-2————-—Bromofom_____________108-10-1——•———4-M«thyl-2-Pentanone____591-78-6——————2-Kexanone____________127-18-4——————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane__108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5——————Styrene______________1330-20-7————-Total Xylenes__________107-02-8—————Acrolein____________^107-13-1—————Acrylonitrile_________

FORM I VOA

0.80.9

210.90.90.90.9141111111111121130.910.91122026

1/87 Rev.

IEVOLATILE. ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NC

Lab Nam«: COMPUCHEM LABS

Lab Cod«: CQMPP Case No.: 0000Matrix: (soil/wat«r) WATER

Sampl* wt/vol: 20.Q (g/raL)

L*v«l: (low/m«d) LOW

% Moistura: not d«c. ___mColumn (pacX/cap) PACK



SAS No.: 4231B SDG No.: EAW20


Lab Fil« ID: CN047S32B09

Dat« R«c«iv«d: 03/01/89


Dilution Factor: *rq~ /, O


CAS NUMBER

1.

COMPOUND NAME

LABORATORY ARTIFACT

RT

12.60

EST. CONC.

2.0

Q

^f

/A/S

4 y - K / B,

20



EPA SAM9L£

Lab Mama: COMPUCHEM LABS________

Lab Code: COMPU Cas« No.: 0000






M»l


SAS No.: 423IE SDG No.: EAW20

CAS NO. COMPOUND






74-87-3——-——Chloromethane__________74-83-9—-————Bronomethane___________75-01-4——————Vinyl Chloride________75-00-3—-———Chloroethane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Oichloroethene______75-34-3———————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total).67-66-3—-——-—Chloroform___________107-06-2————-1,2-Dichloroe thane______78-93-3———-———2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4-———-—Bromodichlorome thane____78-87-5——————'1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1——-——Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-6——-—Tran»-l,3-Dichloropropene_75-25-2——————Bromoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6—-—-—2-Hexanone____________127-18-4—————-Tetrachloroethene______79-34-5——————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene______________108-90-7™———Chlorobenzene__________100-41-4——————Ethy Ibenzene___________100-42-5—————Styrene_____________1330-20-7————Total Xylenes_________107-02-8————-Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev.


EPA SAMPLE NO


Lab Code: COMPU case No.: OQQQMatrix: (soil/water) WATER





Number TICs found: _fl




Lab Pile ID: CR047533B09



Dilution Factor: *rQ- /.o





EPA SAMPLE NO

Lab Kama: COMPUCHEM LABS_________

Lab Code: CQMPU ca«e Ho.: QQOQ






EAW31Contract: SAS4231S

SAS MO.: 4231E SDG Ko.: EAW20


Lab File ID: CNQ47645AQ9



Dilution Factor: 4-r-ft. /, o


74-87-3——-——Chloroae thane__________t74-83-9————-—Bromome thane__________75-01-4——————Vinyl Chloride________75-00-3——-———Chloroe thane__________75-09-2——————Kethylene Chloride______67-64-1——————Acetone______________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total).67-66-3——-f———Chloroform___________107-06-2——————1,2-Dichloroe thane______78-93-3——————2-Butanone___________71-55-6———————1,1,1-Trichloroethane____56-23-5—————-Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4-—-———Bromodichloromethane____78-87-5—-—'——1,2-Dichloropropane_____10061-01-5———-cie-l,3-Dichloropropene__79-01-6————-Trichloroethene_______124-48-1————-Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-6———-Tran»-l,3-Dichloropropene—75-25-2——————Bromoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————-Tetrachloroethene_______79-34-5——-——1,1,2,2-Tetrachloroethane_108-88-3——--—Toluene_____________108-90-7—————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOX

10.80.912510.90.90.90.9141111111111121110.910.91122026

1/87 Rev.


EPA SAMPLE NO

Lab Name: COMPUCHEM LABS______ •

Lab Code: COMPU Case No.: OQOQ

Matrix: (soli/water) WATER


Level: (low/mod) LOW



Number TICs found: _l







Dilution Factor:


CAS NUMBER

1.

COMPOUND NAME

INSTRUMENT ARTIFACT

RT

0.62

EST. CONC.

9.0

Q

^

r



EPA SAMPLE NO


Lab Coda: COMPU Case Mo.: QOQQMatrix: (soil/water) WATER


Lev«l: (low/mcd) LOW



EAW3Contract; SAS4231E






Dilution Factor: +T-Q- /.a

CAS NO. CONFOUNDCONCENTRATIOM UNITS:(ug/L or ug/Kg) UG/L

74-87-3——-——-Chlorome thane__________74-83-9——————Brononethane__________75-01-4——————Vinyl Chloride________75-00-3——————chloroethane__________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15-0———————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3—•——-—chloroform___________107-06-2-————-1,2-Dichloroe thane______78-93-3—•————2-Butanone___________71-55-6———————1,1,1-Trichloroethane___56-23-5——————carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Brcaodichlorome thane____78-87-5-—-———1,2-Dlchloropropane_____10061-01-5————cl»-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1————Dibroaochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-*———Tran»-l,3-Dichloropropene_75-25—2———————Broaoform _______108-10-1—————4-M«thyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4——————Tetrachloroethene_______79-34-5———————1,1,2,2-Tetrachloroethane_ios-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7—————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_______.

FORM I VOA

10.80.911210.90.90.90.9142111111111121110.920.91122026

1/87 Rev.


EPA SAMPLE NO


Lab Code: COMPU case No.: QOQQ





Column (pacJc/cap) PACK

Number TICs found:







Dilution Factor: 4^» '-o


GAS NUMBER

1.

COMPOUND NAME

INSTRUMENT ARTIFACT

RT

0.63

EST. CONC.

10

Q

~



EPA SAMPLE NC


Lab Coda: COMPU Ca«« Mo.: QQQQ


Sample wt/vol: 2Q.O (g/mL) ML





SAS Ho.: 4231E SDG No.: EAW2Q





Dilution Factor: <-re f?c>


74-87-3—•———-Chlorome thane_________74-83-9—————Bromome thane__________75-01-4——————Vinyl Chloride________75-00-3—————Chloroethane___________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3-—-——--Chloroform____________107-06-2—————1,2-Dichloroethane_____78-93-3——————2-Butanone____________71-55-6———————1,1,1-Trichloroe thane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4-——-——Bromodichloromethane____78-87-5——-———1,2-Dichloropropane_____10061-01-5————ci«-l,3-Dichloropropene__79-01-6-———--'Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5—————1,1,2-Trichloroethane___71-43-2 —————Benzene_____________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2——™———Bromofona______________108-10-1——————4-Methyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-S———————1,1,2,2-Tetrachloroethane_108-88-3-————Toluene______________108-90-7-————Chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————styrene_____________1330-20-7————Total Xylenes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

10.80.912210.90.90.90.9141111111111121110.910.9112

2026

1/87 Rev.

' IEVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS


Lab Code: CQMPU case Ho.: OQOQ


Sample wt/vol: 20.Q (g/mL) JH,_





EPA SAMPLE NO.







Dilution Factor: 4i-e- f.o

CONCEHTRATIOM UNITS:(ug/L or ug/Kg) UG/L

CAS NUMBER

1.

COMPOUND NAME

INSTRUMENT ARTIFACT

RT

0.63

EST. CONC.

9.0

Q

V


40"


EPA SAMPLE NC

Lab Name: COMPPCHEM LABS_______Lab Code: COMPU case No.: 0000




* Moisture: not dec. __

Column: (pack/cap) PACT



CAS NO. COMPOUND


Lab File ID: CNQ47648BQ9



Dilution Factor:


74-87-3-—————Chlorome thane__________74-83-9———————Bromome thane___________75-01-4———-———Vinyl Chloride_________75-00-3———————Chloroe thane___________75-09-2———————Methylene Chloride______67-64-1——————-Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Oichloroethene (total)67-66-3——---—Chloroform____________107-06-2——————1,2-Dichloroe thane______78-93-3——————2-Butanone____________71-55-6——————1,1,1-Trichloroethane___56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————Bromodichloromethane____78-87-5—————-1,2-Dichloropropane_____10061-01-5™ ™ci»-l,3-Dichloropropene__79-01-6-————-Trichloroethene_______124-48-1——-—-Dibromochl or ©methane..___79-00-5———————1,1,2-Trichloroe thane___71-43 -2——————Benzene_____________10061-02-6-———Tr«n«-l,3-Dichloropropene_7 5-2 5-2—————-Bromofonn____________108-10-1—————4-M«thyl-2-Pentanone____591-78-6—————-2-Hexanon«___________127-18-4—————-Tetrachloroethene_______79-34-5————-—1,1,2,2-Tetrachloroethane_108-88-3————-Toluene_______________108-90-7—————-Chlorobenzene__________100-41-4———-—Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7——-——Total Xylenes_________107-02-8——————Acrolein______________107-13-1—————Acrylonitrile_________

FORM I VOA

10,

47002

430112

110084018

27028011011111

14011

14012

14001

1500.

1406

3301

10002026

1/87 Rev.


EPA SAMPLE NO


Lab Code: CQMPU Case No.: QQQO




% Moisture: not dec. '


Number TICS found: _8

EAW34Contract: SA54231E






Dilution Factor: 4-1 o- A o


CAS NUMBER

1.2.3.4.5. 109-66-06.7. 96-37-78.

COMPOUND NAME

UNKNOWN 9UTENEUNKNOWN BUTENEUNKNOWN PENTENEUNKNOWN PENTENEPENTANEUNKNOWNCYCLOPENTANE , METHYL-UNKNOWN ALCOHOL

RT

0.983.303.854.124.234.374.686.75

EST. CONC.

460130048437.0

220114.0

QJJJJJJJJ



EPA SAMPLE NO

Lab Nam«: COMPUCHEM LABS______

Lab cod«: COMPP Ca» No.: ooooMatrix: (soil/wat*r) WATERSampl* wt/vol: Q.3Q (g/mL) ML

L«v«l: (low/m«d) LOW

% Moisture: not d*c. _^_


EAW34REContract: SAS423iq

SAS Mo.: 4231S SDG Ho.: EAW2Q

Lab Sanpl« ID: 247648___Lab Pil« ID: C2R47648AQ9

Dat« R«c«iv«d: 03/02/89


Dilution Factor: 4-rO /, o


74-87-3—————Chlorom«than«_________74-83-9™—-—-Bromom«than«__________75-01-4——————Vinyl Chlorid*_________75-00-3——————Chloro«than«__________75-09-2——————M«thyl«n« Chlorid*_____67-64-1——————Acaton*_____________75-15-0——————carbon Disulfid*_______75-35-4——-——l,l-Dichloro«th«n«_____75-34-3——————l,l-Dichloro«than«_____540-59-0——————i,2-Dichloro«th«n« (total).67-66-3—————Chloroform___________107-06-2—————'l,2-Dichloro«than«______78-93-3—————-2-Butanon«___________71-55-6——————1,1, l-Trichloro«than«___56-23-5——————Carbon T*trachlorid«____108-05-4——————Vinyl Ac«tat»__________75-27-4———-—-Bro»odichlorom«than«____78-87-5————™l,2-Dichloropropan*_____10061-01-5———ci»-l,3-Dichloroprop«n«__79-01-6——————Trichloro«th«n«________124-48-1——™Dibro*ochlorom«than«____79-00-5——————l,l,2-Trichloro«than«___71-43-2——————B«nz«n«_____________10061-02-6———Tran»-l,3-Dichloroprop«n«_75-25-2———-—-Broaozoni___________108-10-1—————4-M«tnyl-2-P«ntanon«____591-78-6™———2-H«xanon«_____________127-18-4-————T«tr*chloro«th«n«______79-34-5———————1,1,2,2-T«trachloro«than«_108-88-3——————-TolU«n«_________________108-90-7--———-Chlorob«nz«n«_________100-41-4——————Ethylb«ni«n«___________100-42-5——-——styr«n«_____________1330-20-7————Total Xyl«n«»_________107-02-8——————Acrol«in________________107-13-1—————Acrylonitrila_________

FORM I VOX

3851

2000671006707162

270014006116028063698171877712079727408110018009113057

3200591706759013001800

3-

1/87 Rav


EPA SAMPLE NO

Lab Nama: COMPUCHEM LABS________

Lab cod«: coMPtr CAM Mo.: QQQQMatrix: (soil/wat*r) WATER

Sampla wt/vol: 0.30 (g/mL) ML_

L«v«l: (low/m«d) LOW

* Moistura: not dac. ___



EAW34REContract: SAS4231S



Lab Fila ID: C2R47648A03


Dat* Analyzad: Q3/Q8/89

Dilution Factor:


CAS NUMBER

1.

COMPOUND NAME

FREOH

RT

3.65

EST. CONC.

8700

Q

BJ



EPA SAMPLE NO.

Lab Name: COMPUCHEM LABS

Lab Code: COMPU case No.! QQOOMatrix: (soil/water) WATER

Sample wt/vol: Q.20 (g/mL)




SAW 3 5contract: SAS4231E


CAS NO. COMPOUND


Lab File ID: CRQ47649AQ9



Dilution Factor:


74-87-3---—-——Chloromethane_________74-83-9———-——Bromone thane__________.75-01-4——————Vinyl Chloride_________75-00-3-———-Chloroethane___________75-09-2——————Methylene Chloride______67-64-1————————Acetone_________________75-15-0———————Carbon Disulfide_______75-35-4——————1,1-Dichloroethene______75-34-3——————1,1-Dichloroethane_____540-59-0——————1,2-Dichloroethene (total).67-66-3—————Chloroform___________

J 107-06-2——————1,2-Dichloroethane______78-93-3———-———2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5—————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4—————Bromodichloromethane____78-87-5-—-———1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6—————Trichloroethene_______124-48-1————Dibroaochlorome thane____79-00-5———————1,1,2-Trichloroethane___71-43-2—————Benzene______________10061-02-6———Tran«-l,3-Dichloropropene_75-25-2-————Bromoform____________108-10-1——————4-M«thyl-2-Pentanone____591-78-6————-2-Hexanone___________127-18-4—————Tatrachloroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylanes_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

13077

230010015080011093

29001500911804306910012011013012095120110850120160200014010085

35008918010066020002600

FORM I VOA 1/87 Rev.


EPA SAMPLE NO


Lab Coda: COMPU cas* No.: QOQQ


Sample vt/vol: Q.2Q (g/mL) ML


% Moisture: not dec. __.



EAW35Contract: SAS423i^



Lab Pile ID: CRQ47649AQ9



Dilution Factor: 4-rfr '.o


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.65

EST. CONC.

20000

Q

~

#&T/£- c^™*~ *ff*+i-fl^tl yCb^^ *A

^4^c-W

V

PORK I VOA-TIC 1/87 Rev,


EPA SAMPLE NO








EAW3&Contract: SAS4231E






Dilution Factor: 4- fr /.o


74-87-3—————Chloromethane_________74-83-9-—•———BroBomethane___________75-01-4——————Vinyl Chloride________75-00-3——————Chloroe thane__________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______

J 540-59-0——————1,2-Dichloroethene (total).67-66-3—————Chloroform___________107-06-2——————'1,2-Dichloroethane______78-93-3——————2-Butanone___________71-55-6———————1,1,1-Trichloroethane____56-23-5———————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4—————-Bromodichloromethane____78-87-5-—-——-1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1———— DibroBochlorome thane____79-00-5———————1,1,2-Trichloroethane___71-43-2™———Benzene_____________10061-02-6—™-Tran»-l,3-Dichloropropene_75-25-2-————Bromoform____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4—————Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7————chlorobenzene_________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7—————Total Xylene*__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

FORM I VOA

138

281034171197

7291143111012111312180121114121612145409119101021200260

1/87 Rev,


EPA SAMPLE NC

Lab Name: COMPUCHEM LABS_______Lab code: COMPU Case No.: OQQQ


Leve1: (1ow/med) LOW





SAS NO.: 4231E SDG NO.: EAW20

Lab Sample ID: 2476SO

Lab Pile ID: CN047650BQ9



Dilution Factor: 4r«-Ao





EPA SAMPLE NO

Lab Nana: COMPUCHEM LABS________

Lab Coda: COMPU Casa No.: OQQQ

Matrix: (soil/watar) WATEBsampla wt/vol: 1.2 (g/mL) ML


% Moisture: not dac. ___





Lab File ID: CRQ47651AQ9



Dilution Factor: -*rO /• o


74-87-3——————Chloromethane_________74-83-9-—————Brononethane__________75-01-4——————Vinyl Chloride________7 5-00-3-—————Chloroethane__________75-09-2——————Mathylene Chloride_____67-64-1——————Acetone_____________75-15-0——————carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————-1,1-Dichloroethane______540-59-0——————1,2-Dichloro«th«n« (total).67-66-3———-----Chloroform____________107-06-2——————l,2-0ichloro«than«______78-93-3——-———2-Butanon«___________71-55-6——————l,l,l-Trichloro«than*___56-23-5——————Carbon T«trachlorid«____108-05-4—————Vinyl Acctat*_________75-27-4——————Bromodichloron«than«____78-87-5—————-l,2-Dichloropropan«_____10061-01-5™™ci»-l,3-Dichloroprop*n«__79-01-6———————Trichloro«th*n*________124-48-1——-——-Dibro«ochlorom« than*____79-00-5——————l,l,2-Trichloro«than«___71-43-2—————B*nz«n«_____________10061-02-6—----Tran»-l,3-Dichloropropan*75-25-2—————-Bromoforn_____________108-10-1——————4-M«thyl-2-P«ntanon«____591-78-6———•——2-H«xanon«___________127-18-4————T«trachloro«th«n«______79-34-5———————l,l,2,2-T«trachloro«than«_108-88-3————Tolu«n«_______________108-90-7-—-——Chlorob«nz«n«__________100-41-4—————Ethylb*nz«n«__________100-42-5—————Styr«n«_____________1330-20-7—————Total Xylana*__________107-02-8—————Acrolain____________107-13-1—————Acrylonitrila_________

FORM I VOA

221314172684181$165815187119172018221914020131520261923370141815161735330440

v

1/87 Rev,

IEVOLATILE ORGAN1CS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO


Lab Coda: COMPU Case No.: OQQQ





column (pack/cap) PACK

Number TICs found; _1




Lab Pile ID: CR047651AQ9



Dilution Factor: *ro" '-o


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.65

EST. CONC.

570

Q

£"~

;pu T/4&*J<- ~w

!' S.



EPA SAMPLE NC

Lab Mama: COMPUCHEM LABS________

Lab Code: COMPU case No.: QQQQ



L«val: (low/med) LOW

% Moisture: not dec. __,_








Dilution Factor: 4--Q ( ,n


74-87-3-————-Chl orome thane__________74-83-9————- —-Bromomethana__________75-01-4——————Vinyl Chloride________75-00-3——— —-Chloroethane___________75-09-2———————Methylene Chloride______67-64-1——————Acetone__________75-15-0——————Carbon Diaulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total).67-66-3———-—-Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3————-—2-Butanone____________71-55-6———————1,1,1-Trichloroe thane____56-23-5——————Carbon Tetrachloride_____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichl orome thane____78-87-5—————1,2-Dichloropropane_____10061-01-5———-ci»-l,3-Dichloropropene__79-01-6 ——————Trichloroethene_______124-48-1—-———Dibromochl orome thane____79-00-5——————-1,1,2-Trichloroethana___71-43-2——————Benzene_____________10061-02-6———-Trmn«-l,3-Dichloropropene_75-25-2-————Broaoform_______________108-10-1——————4-M«thyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4—————Tetrachioroethene______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluen*_____________108-90-7—-———Chlorobenzene__________100-41-4————-Ethylbenzene__________100-42-5—————Styrene_____________1330-20-7————Total Xylene*_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile__________

FORM I VOX

10.80.912610.90.90.90.9141111111110.8121110.910.91122026

U3U s

••

1/87 Rev,


EPA SAMPLE NO

Lab Name: COMPTJCHEM LABS_________

Lab coda: COMPU case Ho.: QOOQ





Column (pacfc/cap) PACK

Number TICs found: _0.







Dilution Factor: 4-rO ' -0





EPA SAMPLE NO

Lab Name: coMPUCHEM LABS_______Lab Code: COMPU case No.: OQOOMatrix: (soil/water) WATER







CAS NO. COMPOUND





Dilution Factor: +r4- t.O


74-87-3——-———chloro»ethane__________74-83-9-————Bromome thane___________75-01-4-:—————Vinyl Chloride________75-00-3———————Chloroethane___________75-09-2——————Methylene Chloride_____67-64-1——————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3——————1,1-Dichloroe thane______540-59-0——————1,2-Dichloroethene (total).67-66-3——————Chloroform___________107-06-2——————1,2-Dichloroe thane______

j 78-93-3——————2-Butanone___________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4-————-Bromodichloromethane____78-87-5————-1,2-Dichloropropane____^_10061-01-5————ci«-l,3-Dichloropropene__79-01-6——————Trichloroethene________124-48-1—————Dibroaochl or one thane____79-00-5———————1,1,2-Trichloroethane____71-43-2—————-Benzene_____________10061-02-6-——-Tran»-l,3-Dichloropropene_75-25-2——————Broaofora____________108-10-1-——-—-4-Methyl-2-P«ntanone_____591-78-6—•———2-Hexanone___________127-18-4—————Tetrachloroethene______79-34-5——————1,1,2,2-Tetrachloroethane_108-88-3—————-Tolu«n«L_______________108-90-7—————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5—————Styrene_____________1330-20-7—————Total Xylenea_________107-02-8—————Acrolein_________•107-13-1—————Acrylonitrile_________

FORM I VQA

1o.a0.912210.90.90.90.9141111111111121110.910.91122026

1/87 Rev


EPA SAMPLE NO


Lab Code: COMPU Ca*e No.: OQOOMatrix: (soil/water) WATERSample vt/vol: 20.Q (g/mL) ML








Lab Pile ID: CRQ47653BQ9



Dilution Factor: 4-rfr /• o

CONCENTRATION UNITS:(ug/L or ug/Kg) US/L



UNITED STATES EHYIROHMSNTAL PROTECT IOH ACEHCYV

CS3/Central Regional LaboratoryDATA TRACKING FQRwFQR CONTRACT SAMPLES

CRL Pata Set CERCLtS Ho. M.T ts9J?H 79

SMfl CMO'NO, /S$*5^JV£-Si te Xa*t and Location: \\

Mam* of Contractor or EPA Uboratary: e 2 2 # Q / k u B « - U User:

Wo. of Samples: ^ Pate Staples or Data Received: C3 """ /S~o '1. Have chtln-of-cuuody records betn rectUed? YES2. Have Teattic Reports or packing lists been recetve^T*3. If no, are T r a f f i c Report or packing litC numbers written on the cfiam-of -custody

record? TgS «0 __4. If no, which T r a f f i c report or packing list numbers are Billing?

Are basic data foras in? T£S

Number of samples claimed: <^x Number of samples received:

Checked by: ________ U (%JLJL^? Pat,:

,ejved by Contract Project Management Section: X / / > . P»te; 3-J7 ~

Review Started: 3D Jn*A<fJ! IWrf Reviewer Stgnatun; JfJTotal time spent on rtvir-: / ^ Pate review csaspleted:

Copied (xeroxed) by: r x ^ X ______________ Bate:

Ma,! ltd to Data User by: t . X -^ ______ Bate:USERS;

Please f i l l in the blanks below »nd return this fora to: Sylvia Griffin. QataManagement Coordinator. Region V, SSCRU

Data received by: _^ ________________________ tiate:

O.A. review received by: _______________________ t)»te:

Inorganic Pate CompleteOrganic Gata CompletePiextn~0ata CompleteSAS Pata Complete

, Suitable for Intended Purposes t 2 /[ ] if teeeptableList probleos belo«C '.. Suitable for Intended Purposes C 1

L '., Suitable for Intended Purposes L jL ', . Suitable for Intended Purposes L J

See Attached "Hissing P«ta Request Fora* [ 1MOSLEMS: Plcast indicate reasans (if *ny] why data are not suitable for your uses

Other problems.

Received by Data Management Coordinate^ CRL for File: Patt:_

' \cr

ir^5 aa —H .i . 'o

rn

s ° . ,V CP O

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V

PAGE 1 OF 7"-*—

/?/;Review of Region <f CLP DataReceived for Review on

rnou. Curtls Ross. Bi'rectof (5SCRL)Laboratory

1k

We have reviewed the data for the following case{s)

SITE HAHE: j uavQ C«« ICo.

EPA D»t» Set M o ^ - . y " Simons; <J Kumbers

fic NO.CLP llboratory;

Following »re Our findinjs:

Laboratory.

jerations Branch

DATA QUALIFIERSMfiE Jg_ OF 7

Contrator:

I•flow 1% a tufwry of the out-of-control audits and the possible tffect ondata for this case:

F3

4. to

^^V^j*^

*r^7xff ,7-k& TT

ttviewed by:Phone:Date:

MGE 3 OFDATA QUALIFIERS

Contractor:

I1* • ftuflmarj of th* out-of-control audits and the pots 1 bit tffect on

tftt* for this cast:>i

<&i*~^ J2*, jf-*V4^t/fA*dl

^gx . (A*£j££-~

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by:Phone:Ofttt:

DATA QUALIFIERSWfiE .4- OF *?

Contrator:

(£

| Case

1s • ftuivnarjr of the out-of-control audits and tht possible tffact on thefata for this, case:

/fa#e> (7> d^*H

I I J~ TV/

n I, / /-r-~r » tJLJfi ro

** ~7~7£*S ri

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Date:

DATA QUALIFIERSMGE $- OF

Contractor: I CaseI

•elow 1s • sunrurj of the Out-of-control audits end the possible effect on thedata for tMs case:

/ Hi C

Lf

!eviewed by:

Date:

frd£.

CASE/SAS 9

HVJUUNMEWL PROTECTION AGENCT REGION VCALIBRATION OUTLIERS

VOLATILE HSL CO BOUNDS

instrument « //DA"£/T1H£:

ChioroêtnaneB ronoê t hgneVinjrl ChlorideCnloroethaneN? thy if ne ChlorideAcetoneCarbon niiulfide,1-Dichloroethane,1-DicMoroethene

Trans-l ,2-DichloroetheneCMoroformZ-Butenone).?-Dichioroethane3 J ,1-TricMoroethaneCe"t>on Tetrachloridevm>i Acetatef "0^5 3 1 c h i or oê t h a nji .?™r^*c^'«orop"opaneTra^S-1 ,3-DUhloropropeneTf.c^lo"oetheneD^D'o^ccMorof.ethane3J,?-Trichloroetft*neBep7eêc^s-1 .S-D^chioropropfneZ-CMo-oethyl vinyl etherB'OTfOrp.4 -êf.v 1-2- Pent a none?-Hefca*»D*\e

ITetra:** loroethene1 ,3 ,2,2-Tetr icrno-oetheneToluene

|Cî o'cr'-eTtêIt thj 1 t>e*7C**eStyreieir-;^ler-ec ' ; ->_ylen€wOrfi teiV

AFFECTED ——— "SA^-ÊS:

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These flags should be applied tc the analytes on the sample data sheets.

fi/87


VOLATILE HSL COMPOUNDS

OF

CASE/SAS

Instrument # //DATE /TIME:

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon nisulfide1,1-Dichloroethane1,1-DichloroetheneTrans-l,2-DichloroetheneChloroform2-Butanone1,2-Di chloroethane1,1,1-Tri chloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1,2-DichloropropaneTrans-l,3-DichloropropeneTrichloroetheneDibromochloromethane1,1,2-TrichloroethaneBenzenecis-l,3-Dichloropropene2-Chloroethyl vinyl etherBromoform4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 .1 ,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem-Xyleneo/p-Xylene

rtCnfU a*'™'*'AFTECTEDSAMPLES: ,/?

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* These flags should be applied to the analytes on the sample data sheets

fi/87

L-DATATor reporting results tr- **o 8SDA, the following contract specificqualifiers are to be used, the seven- qualifiers defined belovnoc subject to modification by the laboratory. Up to fivequalifiers may bo roportod on Fora I for oaeh compound.

The seven ZPA-defined qualifiers to bo usod are as follows:

- Indicates compound was analyzed far but not detected. Thesample quantltatlon limit must bo corrected for dilution andfor percent moisture. For example, 10 U for phenol in water iftbe sample final volume is the protocol-specified final volume.If a 1 to 10 dilution of extract is necessary, the reportedlimit is 100 V. For * Mil sample, tho value must •!«« boadjusted for poreoat moisture. For example, if the sample had24* moisture uid a 1 to 10 dilution factor, tho samplequandtatlon Halt for phenol (330 V) would bo corrected to:

100

and df - dilution factor

•t 24% aoisturo. 0 - too-** • 0.76100

10 - 4300 V76

roundad to tho appropriate nunbor of•igaificanc figuroa

C •

For ao£l aaaploa subjeatod to C?C eloan*up proeoduraa, tho C&QLis alao vultipliod by 2, to account for tho fact that only half•f tho oscract is recovered.

Indicate* sa astiaated value. This flag is used either vfcenostiaatlng a concentration for tentatively identified compoundsvhere a 1:1 response is assuoed, or vhen the naas spectral dataindicate the presence of a compound that aeets theidentification criteria but the result is less than tho aaspleOjuantitatioa limit but greater than zero. For example; if thesaaple ojuantitation limit ia 10 ug/L, but a concentration of 3ug/L ia calculated, report it as 3J. The sample quantltatlon

•d fof fcpjh Mlutimm discussed for the V flag, so that if a sample vlth 24%moisture and a 1 to 10 dilution factor baa a calculatedconcentration of 300 ug/t and a sample quantisation limit of430 ug/lcg, report tho concentration as 300J on Form 1.

This flag applies to pesticide results nhare the identificationhaa been confirmed by CC/MS. Single component pesticidesng/ul in the final extract shall be confined by CC/MS.

1-29 2/88

B • This flag la wed when the analyta la found In the associatedblank aa well as in tha aaaple. Xr Indicates possible/probableblank contsainadon and warns the data user to take appropriateaction. This flag vast be used for « TIC as v*ll as for apositively identified TO. coapoond.

TTili flag identifies snayunuifi whose concentrations exceed thtcalibration range of the 6C/HS instxtsscnt for that specificanalysis. Thia flag will aog apply to posdeldas/FCBs analyzedby GC/EC aothods. If ooa or aora eovpounda hava a rasponaagraatar than full aaala, tftxa aavpla or aoctxaet oust b« diluted

re*snalyxed oooordiag to tha opoeifleadens la Exhibit D.All such eoapowdo with ft response creator than full scaleabould hero Aa coaceatradon flagged with an •!• oa the Forafor the original analysis. Xf the diludon of tha extract

"" " "MLbolow the calibration rangeresults of both analyses shall be reported on separate FormsThe Fora X for the dilated aaaple shall have the •DL" suffixappended to the ssaple aober. VOTZ: For total xylenes, wh« :tthree isoaars ara quantified as two peaks, the calibrationrange of •»*** »>aV should be considered separately, e.g.. a

aaeond inaljftls, Lbai

oMlutad analysis is fiflt roquirad for total xylatias unlassionoradon of olthor paak saparataly aaeaods 200 ur/L.

ft • TMs flag Identifies oil coapomids Identified in aa analysis ata secondary dilution factor. Xf a aaaple or extract isro-aaalyzed at a higher dilution factor, as la the *£* flagabove, the "DL* suffix is appended to the seaple raaber on ch*Fora 1 for the diluted aaaple, and *ll concentration values *reported on that Fora t ore flagged with the *D* flag.

A - This flag Indicates that a TIC is a suspectedaldal-eondensadon product.

X - Other specific flags say be required to properly defineresults. Xf used, they Bust be fully described and such•ascription attached to the Sasfpla fiats Sissaary •aelcs.ge and *Case Rarrativo. Begin by using *X'. Xf vore than one flag irsquiejualifiers are required for a asjapla result, us* the *Z* flaxto ooobine several flags, as needed. For instance, the "X*flag ais>t ooobiae As 'A*. "**, and *D* flags for SOSM seapi

The eoofeinadoa of flags "JU* or*TO* Is expressly prohibited. 81.. •.contaainants are flagged •>• a-nl^r vhea they are also detected In _-isaaplo.

If analyses at two different dilution factors ate reoulred Cse«Exhibit D>, follow the data reporting instructions given in £xh:3 ard with the "D" and "I" flags above.

BOO a/--:

DATA REPORTCENTRAL REk.JNAL LAUOR/ 1RY SAMPL**• ORGANICS/i.xORGANICSTHIS FORM IS JO BE USED FOR SAMPLES SENT TO CONTRACT ONLY

supEnfUND DU NUMaftt lC?OS" A EPA RPM or t

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. EPA CASE NARRATIVE—CASE tOOOOContract No. SAS4231E SAS No. 4231E SDG No. EAUOO

CompuChem Laboratories, Inc.

Sample Numbers; EAUOO EAUOt EAU02 EAU03 EAU04 EAUOE EAU06 EAU07EAU08 EAU09 EAU10 EAU11 EAUie EAU13 EAU14 EAU15EAU16 EAU17 EAU18 EAU19

This portion of SAS »4£31E consisted of SO water camples for low detectionlimit volatile analysis. The sample* were received in good condition on3-1-39 in properly sealed shipping containers with traffic reports. In-correct paperwork was received with the samples and Cindy Shreyer was con-tacted at SMO to remedy the problem. Sample EAUOO was not listed on thechain-of-custody document*. Ue at CompuChem are following the EPA roundingrule* for the Contract Required Quantitaion Limits and final reportingresults. Volatile fractions are being reported to one significant figurebelow a value of ten. "J" values are being reported down to one-half themodi fied CRQL. The word "No" on the quant report means the compound was notfound or the compound was less than one-half the CRQL.

All fractions were analyzed within holding time requirements TCL compoundswere present in 16 of the samples at various levels. Most of the camplescontained chlorinated alkanes and alkenec. Six of the camples containedtentatively identified compound*. Sample EAU03 and EAU04 each contained afreon tent at ively identified compound which should be concidered a laboratorycontaminant. A qualifier was included with each sample. Two analyses ofsample EAU02 and EAU09 were reported and billed due to secondary dilutionsrequired to bring the levels of TCL compounds within the multipoint rangeof the instrument. Both analyses were reported due to the loss of some com-p'oundi in the dilutions. Samples EAU06 and EAU08 were each analyzed at dil-utions due to the high levels of TCL compounds. All surrogate recoverycriteria were met. The QC matrix spike/matrix cpike duplicate results wereacceptable. The recoveries of trichloroethene and toluene exceeded QC limitsin the MS.

Release of the data contained in this hardcopy data package has been authorizedby the Laboratory Manager or his designer, as verified by the followingsignature.

Note: This report was paginated for reference and accountability in decreasingnumerical sequence.

Janet C. Carrett 3-15-89Technical Reviewer

USEPA CONTRACT LABORATORY PROC.F1AM^ SAMPLE MANAGEMENT OFFICE" PO BOX 818 ALEXANDRIA. VA 22111f* 7O3/SS7 2490 FTS-SS7 2*90

APPLICABLE)

ORGANIC TRAFFIC REPORT[FOO CtP USE ONlYi

TYPE OF ACTIVITY (CIRCLE O«£) (£SUPEJVUNO—PA Bt ESI ,WS RD RA ER

- NPID O4M-OTHER ____NON-SUPEMPUND—________PHOQIUM

(ENTER-W9OX A) 4. SOL1. SURFACE WATER B. SEOMENT2. GROUND WATER •.OL(SA8)S.LEACHATE , - 7. WASTE (SAE)

SAMPLER: (NAME)-' • • « - ! • • . /'

•ftgmnr 9

£Aim

SAMPUNO OATt

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OATE AEC'O: SOQ NO:

RCC*DtY:

LABORATORY CONTRACT NO. UNIT PfUCC

TMANSFtfl TO: OAT| RtC'O:

RtCO BY: CONTRACT NO./FfllCt

CLP 'SAMPLENUMBER

(FROM LABELS)

®DE

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ANALYSISSPfCWL

HANDUNOSTATION

LOCATION

SAMPLECONOmONON RECEIPT

RECEIVED INJOOOCONDIT10!

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WHITE - SMO COPY

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0 _ _ CoCtto '*tf^ S" WHTTE-LABlCOPV FOR RETURN TO SMO ~r YELLOW - LAB COPY

SQHPLE OP TO PBCKQGE 599

USEPA CONTRACT LABORATORY PROGRAMSAMPLE MANAGEMENT OFFICEPO BOX Bid ALEXANDRIA. VA 22111703/5S72490 FTS-S57-2490

SASNO:tt(IF APPUCASLE

ORGANIC TRAFFIC REPORTiron CLP usi ONIYI

OATIREC'D: ..TYPE OF ACTIVITY (CIRCLEMB .* ist'Rirs no M

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SAUPUR: (NAME): (NAM,/rr4 > i * I /

SAMPLECONOIDONON RECEIPT

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RECEIVED INSOODCOBOmO

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(FROM LABELS) f,V*..r L,|.,>

WHITE - SMO COPY PMK - CUCNT COPY WHITE - LAS COPY FOR RETURN TO SMO YELLOW - LAB COPY

SAMPLE O0TB PBCKB8E 598


EPA SAMPLE NO.








EAWOOContract: SAS4231E

SAS No.: 4231E SDG No.: EAWQQ


Lab File ID: CN047497C11



Dilution Factor: -4 0- 1. C

CAS HO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

3-

74-87-3 ———— •74-83-9 ———— -75-01-4 ———— •75-00-3 ———— -75-09-2 ———— -67-64-1 ———— -75-15-0 ———— -75-35-4 ———— -75-34-3 ———— -540-59-0 ——— -67-66-3 ———— -107-06-2 ——— -78-93-3 ———— •71-55-6 ———— •56-23-5 ———— -108-05-4 ——— •75-27-4 ———— •

10061-01-5 — -79-01-6 ———— -124-48-1 ——— -79-00-5 ———— -71-43-2™ — •10061-02-6-—75-25-2 ———— •108-10-1 ——— -591-78-6 ——— -127-18-4 ——— -79-34-5 ———— -108-88-3 ——— -108-90-7 ——— -100-41-4 ——— -100-42-5 ——— -1330-20-7 —— -107-02-8 ——— •107-13-1 ——— -

— — Chl orome thane-—— Bromome thane• —— Vinyl Chloride-—— Chloroe thane- —— Methylene Chloride-——Acetone

— — 1 , 1-Dichloroethene— -1, 1-Dichloroethane- —— 1,2-Dichloroethene (total) __

— — 2 - Butanone— — 1 . 1 . 1-Trichloroethane——Carbon Tetrachloride- —— Vinyl Acetate— -Bromodichloromethane— -1 , 2-Dichloronrooane-—— ci»-l. 3-Dichloropropene .,..,.— — Trichloroethene—— -Dibronochloromethane—— 1 . 1 . 2-Trichloroethane...•Benzene

— — Bromoform—— -4-Methvl-2-Pentanone

— -Tetrmchloroethene ,„,• —— 1 , 1,2, 2-Tetrachloroethane ___——Toluene—— -Chloroben z ene- —— Ethylbenzene _.,.- —— Styrene- —— Total Xylenes— — Acrolein— — Acrylonitrile

10.80.912210.90.90.90.9141111112111121180.910.91122026

U .UUU

UUUUUUUUUUUUUU

UUUUUUU

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SBHPLE OOTO SUHUBBV


EPA SAMPLE NO


Lab coda: COMPU Case No.: 0000





Column (pacfc/cap) PACK


EAWOOContract: SAS4231E

SAS No.: 4231E SDG No.: EAWOO

Lab Sample ID: 247497_____

Lab File ID: CN047497C11



Dilution Factor:


CAS NUMBER COMPOUND NAME RT EST. CONC, Q


SAMPLE tMTO SWW0BV


EPA SAMPLE NO.


Lab Code: CQMPU Case No.: OQQQ






CAS NO. COMPOUND


SAS NO.: 4231E SDG No.: EAWQO





Dilution Factor: 4.Q-1.C ^

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L Q

74-87-3——————Chlorome thane__________74-83-9——————Bromomethane___________75-01-4——————Vinyl Chloride________75-00-3—————Chloroethane__________75-09-2———————Methylene Chloride______67-64-1——————Acetone_____________75-15-0———————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Oichloroethene (total).67-66-3—•—-——Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3———————2-Butanone____________71-55-6———————1,1,1-Trichloroethane____56-23-5——————Carbon Tetrachloride____108-05-4——————Vinyl Acetate__________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5-————ci«-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1—————Dibromochloromethane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene_____________10061-02-6————•Trane-l,3-Dichloropropene_75-25-2—-————Bromoforn____________108-10-1—————4-Methyl-2-Pentanone____591-78-6————— 2-Hexanone___________127-18 -4 —————Tetrachloroethene______79-34-5—————1,1,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————— Ethylbenzene___________100-42-5————-Styrene_____________1330-20-7—————Total Xylenee_______1__107-02-8——-——Acrolein____________107-13-1—————Acrylonitrile_________

10.80.912210.90.90.90.91431111161111211190.910.91122026

FORM I VOA 1/87 Rev

oara sutwaxv


EPA SAMPLE HO.


Lab Code: COMPU Case Mo.: 0000







SAS NO.: 4231E SDG No.: EAWOQ





Dilution Factor:


CAS NUMBER

1. 75-43-4

COMPOUND NAME

METHANE , DICHLOROFLUORO-

RT

1.40

EST. CONC.-

3.0

Q

J


SGHPLE DAT(9 SUMM0RY


SAMPLE NO.








CAS NO. COMPOUND


SAS No.: 4231E SDG No.: EAWOQ





Dilution Factor: -4-i-Q-l.C1 '-&


74-87-3——•——•——Chloromethane__________74-83-9——————Bronome thane__________75-01-4———————Vinyl Chloride_________75-00-3——————-Chloroethane___________75-09-2——————Methylene Chloride______67-64-1——————Acetone_____________75-15-0———————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total),67-66-3—————Chloroform___________107-06-2——————1,2-Dichloroethane______78-93-3™———2-But an one____________71-55-6———————1,1,1-Trichloroethane____56-23-5———-—Carbon Tetrachloride____108-05->4——————Vinyl Acetate__________75-27-4———————Bromodichl or one thane____78-87-5——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1—————-Dibromochlorome thane____79-00-5———————1,1,2-Trichloroethane____71-43-2——————Benzene _____________10061-02-6-———Trana-lfS-Dichloropropene.75-25-2——————BroaoforiB ___________108-10-1——•—-—4-M«thyl-2-Pentanone_____591-78-6——————-2-Haxanone____________127-18-4—————Tetrachloroethene_______79-34-5———————l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7——————Chlorobenzene__________100-41-4——————Ethylbenzene___________100-42-5——————Styrene_______________1330-20-7—————Total Xylenes__________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

10.818122149

3004194

22011111

36011

281211

2800.9

3400.6541

3002026

FORM I VOA 1/87 Rev

S0HPLE DOTO SUHHQBY


EPA SAMPLE NO

Lab Name: CQMPUCHEM LASS________

Lab Code: COMPU Cas* No.: 0000








SAS No.: 4231E SDG No.: EAWOQ


Lab Pile ID: CN0475Q2A11



Dilution Factor: -4^Q-l.C


CAS NUMBER

1. 110-54-32.3. 103-65-1

COMPOUND NAME

HEXANEUNKNOWNBENZENE, PROPYL-

RT

5.207.409.54

EST. CONC..

2.04.06.0

Q

JJJ


SOHPLE DBTB SUHHBRV


EPA SAMPLE NO.

Lab Name: CQMPUCHEM L A B S _ _ _ _ _

Lab Coda: coMPU Case Mo.; QQQQ







SAS NO.: 4231E SDG No.: EAWOQ

CAS NO. COMPOUND



Date Received: 03/01/89Date Analyzed: 03/04/89

Dilution Factor:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/L

74-87-3 ——————Chloroaethane_________74-83-9——————BroBomethane___________75-01-4———————Vinyl Chloride_________75-00-3———————Chloroe thane___________75-09-2———————Methylene Chloride______67-64-1--————Acetone_____________75-15-0——————Carbon Disulfide_______75-35-4——————1,1-Dlchloroethene_____75-34-3———————1,1-Dichloroethane______540-59-0——————1,2-Dichloroethene (total)67-66-3——————Chloroform___________107-06-2——————1,2-Dtchloroethane______78-93-3—————2-Butanone___________71-55-6——————1,1,1-Trichloroethane___56-23-5———————Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Bromodichloromethane____78-87-5——————1,2-Dichloropropane_____10061-01-5————ci»-l,3-Dichloropropene__79-01-6——————Trichloroethene_______124-48-1——--——Dibroaochl or ome thane____79-00-5--———.--i, i, 2-Trichloroethane___71-43-2——————Benxene_____________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2———--Bromofora____________108-10-1————«4-ltethyl-2-Pentanone____591-78-6—————2-Hexanone___________127-18-4——'•——Tetrachloroethene______79-34-5———————1,1,2,2-Tetrachloroethane_108-88-3——————Toluene_______________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenrene__________100-42-5—————Styrene____________L_1330-20-7————Total Xylenee_________107-02 -8 —————Acrolein____________107-13-1—————Acrylonitrile_________

22131217262918161629015197138017201822196402018272026192344014

780154417260330440

y .uDJUUuuuuDUDUDUUUUU0UUDUuuuDUDUDUDUU

FORM I VOA 1/87 Rev.

SAMPLE £M9Tf9 SUHHBRY


EPA SAMPLE NO










SAS No.: 4231E SDG No.: EAWQO


Lab File ID: C4R47SQ2A11



Dilution Factor: • 4. Q 1.0 ..!&




SAHPLE DBT0 SUHHBBV 59


E*A SAMPLE NO.


Lab Cod«: COMPO Case Ko.: 0000






CAS NO. COMPOUND


SAS No.: 4231E SDG No.: EAWQO





Dilution Factor: -4-i-e- ;-C -1#


74-87-3—————Chlorone thane_________74-83-9—————Bronooethane__________75-01-4———————Vinyl Chloride_________75-00-3———————Chloroethane___________75-09-2———————Methylene Chloride______67-64-1——————Acetone_____________75-15-0———————Carbon Disulfide_______75-35-4———————1,1-Dichloroethene______75-34-3———————1,1-bichloroe thane______540-59-0————--1,2-Dichloroethene (total)67-66-3———————Chloroform____________107-06-2——————1,2-Dichloroe thane______78-93-3-—-™—2-But«none_____________71-55-6———————1,1,1-Trichloroe thane____56-23-5———-—-Carbon Tetrachloride____108-05-4—————Vinyl Acetate_________75-27-4——————Broodichlorome thane____78-87-5—————1,2-Dichloropropane_____10061-01-5———ci*-l,3-Dichloropropene__79-01-6———————Trichloroethene________124-48-1—————Dibromochlorome thane____79-00-5———————1,1, a-Trichloroethane____71-43-2-™-——-Benzene_____________10061-02-6————Tran»-l,3-Dichloropropene_75-25-2————-- BroBQfonn____________108-10-1——————4-Methyl-2-Pentanone____591-78-6——————2-Hexanone____________127-18-4———~Tetrachloroethene______79-34-5———-—"l,l,2,2-Tetrachloroethane_108-88-3—————Toluene_____________108-90-7—————Chlorobenzene_________100-41-4—————Ethylbenzene__________100-42-5—————styr«n«_____________1330-20-7————Total Xylenee_________107-02-8—————Acrolein_____________107-13-1—————Acrylonitrile_________

10.80.9110710.90.90.70.61431111171111211120.9

330.9112

2026


SfiHPLE MT0 SUHMBRY


EPA SAMPLE NO




Sample • wt/vol: 20.Q (g/mL)

Level: (low/raed) LOW





SAS No.: 4231E SDG No.: EAWOO

Lab Sample ID: 2475Q3____

Lab File ID: CN0475Q3A11



Dilution Factor: -4-rO- l.C Jfi)


CAS NUMBER

1.

COMPOUND NAME

FREON

RT

3.25

EST. CONC..

2.0

Q

Xf R


SQHPLE Off TO SUHH8RY

UNITED STATES WVlROKMgNTM. PftQTECTlOK AGENCYRE&iOM V

E53/Central tegional laboratoryDATA TgACKlHC FORM FOR CONTRACT

CRU Data Set

SMO Case No.

5&Q5 OKLU «o. M ^P ts Q KTi 9 Q ?TJf<S

JC/Q. / 1 £ Site tta»e and Ucation: M Q JiC/YlQA I U 0 Q 6

fUoe of Contractor or PA laboratory: QfW^p^k&âta User: 0

»o, of Samples: S)Q Pate Samples or Beta Received:

1. Have che!n-of-custody records been received?2. Have TeatUc Reports or packing lilts been recetvtTP3. If no. are T r a f f i c Report or puking 1 ilf numbers written on thi chain-of -custody

record? Y£5 HO __4. If no, which T r a f f i c report or packing list numbers are Kissing?

Are basic data form* In? YES,

Number of simples claimed:

Checked by:____n_____Nu&ber of simples received:

i-C nui JLJL. c««;ejved by Contract Project Hanajement Section: AJ/7t. f/L Date: 3 - It, "

Started: ^2^/H/L &? Rtviwer

Total time spent on review: /

Cspied (xeroxed) by:

Date review cawpleted: -^4

'JI (j flfl^

Date:

Date:Mailed to Data User by:OATA USERS;Please f i l l In the blanks below and return this farm to: Sylvia Griffin. DataManagement Coordinator. Region V, 5SCRU

Data received by:

Q.A. revir* received by:

Date:

fimte:

Inorganic Date Complete [ *Organic Data Complete COioxin~0ata Complete CSAS Data Complete C

, Suitable for Intended Purposes ! ] /[ 3 if acceptable., Suitable for Intended Purposes, Suitable for Intended Purposes. Suitable for Intended Purposes

\ ] Ust proWems bela«».

iiSee Attached "Mi siing Data Request Fora* C 1PROBLEMS: Pleast indicate reasons tif any] «hy data art not suitable for your uses

Other problems.

Received by Data Management Coordinator^ CRL for File: Date:.

PAG? 1 OF

Review ofReceived f

Curtls to<Central .

Oata User,

SITt Itortg; X/gACyvSCJi: t ^ v ,

cut Me. . 07. ,

CUP L.b,r,tory: O^ljL /S

Following are Our findings:

3 f.f9 3 6.'

Data are acceptable for vse.Data are acceptable for vse with qualifications referenced above.See Data Qualifier sheets and Calibration Outlier foras for flags andadditional comments.

v 4 Data are preliainary - pending verification by Contractor Laboratory.See Case Sunoary abov*.

( ) Data «re unacceptable.

ec: Carla Oe-npsey.CLP Quality Assurance Officer. Analytical Operations BranchJames P»?t» ,^M»

DATA QUALIFIERSf AGE JL OF

Contractor: CAL I CastI .1

•flow 1s a tmmarj of tht out*of*contro1 audits and tht pots1bit tfftet on thtfata for this cast:

/,

t/OA

u

V*Cs tA >/5y.

fttv1a«td by:

OATA QUALIFIERSJ PF

!

1» • tuwnarj of t*t out-of-control audits and tht pot $1 bit tfftct en therfita for this cast:

TCL

Id

3 77 C^

T/C.

atfa. few* ef dt

7.

QC

\i)flfT» \i

V

by:

»AGE _V or ISLOATA QUALIFICftS """

Contractors CflLHlO _________ __ | cast // 403

U a suomarj of tha out»of-eontro1 audits and tha passlbla affact an thttfata far this case:

S > g tS|p

17)

QC

£$62$

CL

•avlawad by:

OATA QUALIFIERS

Contractor:II Casa //

•clow Is a tuMmarj of tha out-of-control audits and tha posslbla affact on thefata for this case:

9.XX3 &

ofTtC's faff* U/tW.

3 7

n.r?

s kcu/tit *-Vi J&S& cT/o*;

•avltwtd by:Phone:

CASE/SAS »

UNITE*. STATES CWriftONHCIITAi PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDSCONTRACTOR

PAGE OF

Instrument $ /BATE /TIME:

ChloromethaneBromomethaneVinyl ChlorideChloroethanenetnyiene ChlorideAcetoneCarbon nisulflde

,1-Dlchloroethane,1-Dichioroethene

Trans-1 .?-DichioroetneneChloroformZ-Rutanone

.?-Dichioroethane,1.1-Trlchloroethane

;arbe" Tetracnioridevinyl AcetateBroôcH chl oromet hanel.Z-D^chioropropaneTra^s-1 ,3-DlcMoropropeneTrichioroetheneDlbromochioromethanel.l.Z-Trl ChloroethaneBenrenec^s-1. 3-01 chl oropropene2-Cnloroethyi vinyl etherBro"5fonrii-Methyi-z-Pentanone12-HexaiDneITetrachioroethene1 .1 .2,2-Tetrachioroethane' olueneCnlorobenzeneEtnyibenzeneStyrenew-XyleneO/D-Xylene

AFFECTEDSAMPLES:

Rev1e**e-'sInitial s/Date: 3.?t*'eetAe4C'

V.,1.19

lnlt»$• *?•'Rr

rf*&

1

cai*k —ISO

53.3

•

1

TWIXtA

'.tft

>O3f.

375

V6.6

*$*tfS 6

f

/f

3£Y

£^ bt?5fS £j$ft |zL.f 5 £2.3*15£"5 & 25^5f S C.lf>2i-

Cont. Cai.

RF ID 9

.

Cont. cai*nr~ ID •

•

toni. cai.•

RF

,

ID •

tont, cai.

RF.

11) w


CASE/SAS


SEMI VOLATILE HSL COMPOUNDS

Il*i93 -1 CONTRACTOR

PAGE? OF/*-

Instrument *r2. 'J-DATE/TIME:

"Phenol ————————bis(-2-Chloroethyl JEther2-Chlorophe".o11.3-Oichlorobenzene1.4-OichlorobenzeneBenzyl Alcohol1,2-Oichlorobenzene2-MethylphenolbislZ-chloroisopropyi JEther4-Me;hyl phenolN-SitPOSO-Di-n-PropylamtneHexachloroethaneNitrobenzeneIsophorone2-Nnrophenol2, 4*0"! net hyl phenolBenzole Acidbis(2-Chioroetho»y)Methane2,4-OichlorophenolJ ,2,4-TrlchlorobenzeneNaphthalene4-Chloroan-i lineHe nachlorobut advene4-Chloro-3-Me*hyl phenol2-Methvl naphthaleneHexachlorocydopenta^-iene2.4.6-Trichloropnenol2,4,5-Trlcnlorophenol2-Chloronaphthaler.e

1 Z-MtroaninneDimethyl PhthalateAcenap^thylene3-NitroamlineAcenaphthene2,4-DinitPOphenol4-NitrophenolOibenzofuran

-"

AFFECTEDSAMPLES:

ReviewerInitials/Date:^.^'^*^^'^-

it ,{j OQV- /v- 1 y

Inr^•8vr

£^

d&

TWfÎRSD

f£

*

T"

ft

Comi&kl-

t / f /A

609

? -'/r??ff3 "f3 -rs- 1^S'

.. tjI$Hib

VUil

77?

-y-io .?i/'S'7^

'vr

nr[^

7

j4

Lont

ftr

•

TT1

16 '

T7i™

Loot

W-* Li

xb-T:T-

Cont

*r*mtir

r.Tf—

iI!

* These flags should be applied to the analytes on the sample data sheets. 8/F

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION V' . '•-• • CALIBRATION! OUTLIERS.'-•/I- * '• SEW VOLATILE HSL COMPOUNDS

CASE/SAS • 1/495 : ' ; . CONTRACTOR^

nstrument t-2.. . •1 Alt/TJME: "Z •

•<'.4-D1n1trotoluene .i!|6-Diet

Jinltrotoluenehyi ^hthaiate

4-th^ orophenyl-phenyl etherFluorene4-Nitroanlllne4 ,6-Di ni tro-Z-Methyl phenolN-.NItrosodl phenyl ami ne4-Brotnophenyi-phenyietherHexachlorobenzenePentachiorophenolPhenanthreneAnthraceneD1-n-ButyipnthaiateFluo •anthenePyreneButylbenzylphthalBenzole

atejAnthracene

bis(?-Ethylhexyl PnthalateChryseneDl-n-octyl Phthaiatelenzotenzotenzo

Dka

IndenoJibenz}enzo(g

FluorantneneFluoranthenePyrene.2 f3-cd)Pyrene

a. h Anthracene.h.-t) Per^'lent

Inlt. CaV

RF

LOW

t.Qfb

ill.iuj \\V-

2?.«

3

•

(

Cont. Cal*

RF

,w%

I,<X$

ID

95

j&i

•

y

y

Cont* Cal*

RF ID •

Cont. Cal.•

KT ID *

dont. Cal.

fcr~ tb *

j

SEE PASE 1 FOX AFFECTED SAMPLES.


Reviewer's In1t1 alt/Date;8/87


SEMIVOLATILE HSl COMPOUNDS

OF

CASE/SAS *

Instrument *2. "'•"DATE /TIME: "

'Phenol ' ' " '"bis(-2-Chloroethyl JEtherZ-Chlorophcnol1 ,3-Oichlorobenzene1 ,4-Dichl orobenzeneBenzyl Alcohol1,2-DicMorobenzene2-Methylphenolbis(Z-chloroTSOpropyl JEther4-Me*hyl phenolN-Ni troso-rh-n-P ropy 1 ami neHexachloroethaneNitrobenzeneIsophoroneZ-Nitrophenol2 ,4-Dinethyl phenolSenzoic AciobiS(2-Chloroethoxy)Methane2,4-DiChlorophenol3 ,2,4-Trichlorot>en2eneNaphthalene4-Chloroar>'' l ineHexachlorotJutadiene4-Chl oro*3-Methyl ph.enol2-Methyl naphthaleneHexachlorocyclopentac'' iene2,4.6-Trichlorophenol2.4,5-Tricnlorophenol2-Chloronaphthalene

! t-Mtroani lineDimethyl PhthalateAcenapnth^lene3-NitroamlineAcenapnthene2.4-Dinitrophenol4-NitrophenolDlbenzofuran

AFFECTEDSAMPLES:

Reviewer ,.I ni t i a 1 s /Dat e :3 • rf*/<e,u&g&£-

d iQ 83q. y. 3

T*

.0

£f££fE£

mi4

&

15f175•s5

.. La£S1RSD

IH'k.

73^7V361 S&2.S62JH£IS#62V

T"T"

I

i'W

ton1

RF

TT1ITT

iTTT"

Cont

*F"

-

TTi

«T

iTTv

'

lom

mrTHir

i:«—

Con"

nr. rsto

T.*

i

!

* These flags should be applied to the analytes on the sample data sheets 8/F

JAGE JO OF

CASE/SAS

UNITED STATES ENVIRONMENTAL MOTECTION AGENCY REGION V• . • • • ' • CALIBRATION OUTLIERS

--.;";- * • SEW VOLATILE HSL COMPOUNDS/f 93: ' ' ; . CONTRACTOR

nttrument »• .. . . •1 ATE/

~Jt'!*"Lt-

Thtt

TIME: - •*.-•

Hnltrotoluene.)lnltPOtolutnehylpnthaiatt

4-Chlorophenyl-phenyletherFluoptne4-NitPoanmnt

Inlt.3 .1

R? I

laLrISU

-

f

*

^ ••• iH y»!!L f fSJCI f^4.6-D1nitPO-2*MethyiphenolN-Ni tposodl ohtnyl ami nt4-Bromopheny 1 -pheny 1 etherHexachlorobenzenePentachlorophenolPhenanthreneAnthracene)i-n-8utvl pnthai ate:luoranthen«'yreneJutyl benzylJenzotabis

Ant^nthalateiracene

2-Ethylhexyl PnthalateCnryseneH-n-octyi Phthaiate>enzoenzoenzo

Dka

ndenoiibenz

J

FluorantneneFluoranthenePyrene.2.3-cd Pyrene

l.hjAnthracene"benzotQ hi Perylene

"

Cont. Cal.

RF 1U •

Cont. Cal.

RF ID •

Cont. Cal.•

RF 1U *

Cont. Cal.

ItF ID *

•

SEE PASE 1 FOH AFFECTED SAMPLES.

• These flags should be applied to tht analytes on tht sample data sheets.

«tv1t-tr's InltlaU/Datt; <// 19/998/87


SEMIVOLATILE HSL COMPOUNOS

PAGE // OF

CASE/SAS

Instrument #72 '*•" DATE /T i MET —"Phenolbis -Z-ChloPoethy JEthePZ-ChioPophcnoi1 ,3-OichloPObenzene1,4-DichloPObenzeneBenzyl Alcohol1.2-DichloPObenzene2-MethylphenolbistZ-chloPOTsopropyi JEther4-Methyl phenolN-NitPOSO-O^-n-PPOpylarrnneHexachiopoethaneNitrobenzeneIsophorone2-NitPOpnenol2, 4-Oi net hyl phenolBen;bis

oic AcidZ-Cni opoethoxy JMethane

2,4-DichloPOpnenol) .2,4-TPichlorobenzeneNaphthalene4-ChloPoan? lineHe xachloroût advene4-Chloro-3-Methyl phenol2-Methyl naphthaleneHexachlorocydopentat^-iene2,42.4

,6-Trichlorophenol,5-TpicnloPOphenol

2-ChloPonaphthalene1 t-N":tPOani line

Dimethyl PhthalateAcenaphthylene3-NitPoamlineAcenaphthene2.4-DinitPOphenol4-NnrophenolOibenzofuran

AFFECTEDSAMPLES:

Reviewer /u ^

Init, Cal*^//-&9n t

m^^^fj

f AO

•cSy

USD

5O

"$\.5

6f-(

t,.

3*

^

esGzsS& 626es WH€& 9^/«Zes 7*1

Cont. Cal.

RF1 %D

Cont. Cal.

Rp

-

ID

•

•

Cont. CaT7

Rf %D~ *

tom. Cal.

feF ID *

t!!

* These flags should be applied to the analytes on the sample data sheets. 8/P

CASE/SAS

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION v' . ' .' • CALIBRATION OUTLIERS

:•/:. * '- SEW VOLATILE MSL COMPOUNDS. Page 2

_____.' . CONTRACTOR

Instrument r ft.DATE/TIME:

2.4*Z.4-

•)1nltrotoluene .)1nltrotoiuene

"Dietnylphthalate4-CMorophenyl-phenyletherFluorene4-Nitroaninne4 ,6-Di ni tro*2-Met hyl phenolN-Ni t rosodl phenyl ami ne4*BromoDhenyi-phenyletherHexachlorobenzenePentachiorophenoiPhenanthreneAnthracene)1»n-5utylDhtnalateluoranthene»yrene(utylbenzylphthallenzo(a

ateAnthracene

b1s(Z-Ethylhexyl PnthalateCnryseneDi-n-octyl PhtnaiateJenzotenzolenzo

Dka

IndenoDibenz

.

FluorantneneFluorantnenePyrene,2.3-cd)^'yrene

a.hjAnthraceneBenzotQ .h.1* ) Perylent

Inn. Cal.***(kf-

'.59Wsff

••

Cont. Cal.

RF ID •

Cont. Cal.

RF ID •

Cont. Cal..

RF ID w

Cont. Cal.

R^" ID *

*

SEE PA3E 1 FOX AFFECTED SAMPLES.

* These flags should be applied to tht analytes on the sample data sheets.

Reviewer's Initials/Date: &*>**<<*£&*8/87

For reporting results tr *ho VSOA, the following contract specificqualifiers «ro to bo used, the seren qualifiers defined belowag£ subject to aodlfieation by t&e laboratory. Op to fl-requallfiozs aey *• reported aa Fora Z for ooebtho seven IPA-doflnod qualifiers to bo used are as follows:

:es miajinund was analyzed for but aot detected, tho •quantltatlon Halt aust bo corrected for dilution and

for percent aolstaro. For oxaapla, 10 0 for phenol la waterthe asaple final voluae Is tba protocol-specified finalZf a 1 to 10 dllutloa of extract Is necessary, the reportedllalt Is1100 U. For a soil Maple, tho value aust alia beadjusted for percent aolstoare. For exsople. If the ssaple had24% aolstare sjnd a 1 to 10 dilution factor* the oeapleftuatltatloB Halt for phoaol (330 V) would bo oorrootod to:

100

aad df - dilution factorat 24% aolatura, 0 -

10 - 4300

- 0.7«100

.7*roodod to tha cppreprlato ouabar of•Igalfleaat flgurao

For soil saaples subjected to CK clean-up procedures, the C&QZ.Is also aultlplled by 2, to account for the fact that only halfof the extract Is recovered. - -

J • Zndleseas sa estimated value, this flag Is used either whenestimating a ooaceatratlea for tentatively Identified compoundswhere a 1:1 response Is assumed, or whoa the BOSS spectral dataIndicate the presence of a •oapeijtid that aeets theIdentification criteria but tha result £» less than the saapleouaatltAtloa Halt but greater than sere* For example; if theoeaple quantltation Halt Is 10 ug/L, but a concentration of 3

Is calculated, report It os 3J. tho ssaple ojuantltatlonid f ot hua-*****

oo discussed for the V flag, so that If a aaapla with 24%aolsture sad a 1 to 10 dllutloa factor has a calculatedconcentration of 300 ug/L and a ssaple ojusatltatlon llalt of430 ug/kg, report the ooncentratlon oo 300J on Fora Z.

C * this flag applies to pesticide results where the Identificationhas been confirmed by GC/VJ. Single eoaponeat pesticidesag/ul la the flcal extract shell be confirmed by CC/HS.

l-2t 2/88

£52-

Thla flag la «Md whoablank aa wo.ll as la thablank agnfssrfna'Him andaction. This flag mat bovealtlwoly Idantlflad TO,

la found la tha aaaoclatadIt ladlcataa potalbla/probabla

tha data asar to taka approprlatafor a TIC as wall aa for a

S * Tala flag Idaatlflaa asojîiuuiTi wfaoaa aoneaatratlons axeaad thacalibration range af taa CC/H5 lastxtaaarnt for that apaelfieanalysis, this flag will ap£ apply to p«stleldac/?CBa analyxm

GC/XC aotboda. If an* or OJOT« ooayuiault bavo a raaponaafull aaala, tba aaapla or axtxact auat o« diluted

ordlag to tfaa apaelflaatlona la bchlbit D.All ouch BBBiniimiti vlch a roaponao graatar tfcaa full acala•hmild hcva tfaa tauuauexatlau flaggod with aa *X" aa th« Torafor caa orlglaal aaal7*la. If Aa dilution af taa axtract

*^**-1 ** f*in flnt imlT*** to baWlow taa aallbratioa mgo in t&a a*croaulta of both aaalTaaa shall ba raportad oa aaparata ToTha Ton I for tao dllvtad aaoyla ahall bcva ta« «DL- aufflx•ppoadad to taa aavpla muab«r. MIX: for total xylanoa,CbrM laoojar* ara ojuaaelfiad a* Cwo paaks, th« calibrationvaaga of «aeh a««k abould bo ooacldarod oaparataly, a.g.t aaUlutod aaalysla la Bfi£ raqulrad for total x/lanas ualaas t

taacratlon of altaor faak aapaxatalj oxeaoda 200 ug/L.

Z •

Thla flag Idoatlflaa all •no^maiiiU Idaatlflod la aa aaalyala ata aoeoadazy dilution factor. If a aaaplo or astraet laro*aaal7xad at a hlahar dilution factor, aa la tha •£• flagabovo, tho *OL' auffls la appandad to taa oaapla nunb«r on th*fora I for tha dllutad aaapla. and al^ eeneantratlen valuaj *raportad oa that Fora I ara flaggad visa tha 'D* flag.

Thla flag ladlcataa that a TIC la a vutfpaetada.ldol-«oadanaatloe product.

Othax apoelflc flags aay bo raoulrad to properly dafiaa th^raault*. If uaad. thty oust b« fully daacrlbad and suchoVaerlptloa attachad to tba gaarpla Oata Suonary faeleaga andCaaa Rarratlva. gagla by ualag *Z*. If aora than oaa flag i.

ajuallflars ara roaulrod for aca soofclao aararal flags* aa aflag algnt aoabiaa As "A", "1

la rmault. uso tha *Z* flacFor laatanca, thaD* flags for a

(laatlon af flags TtT or^JB* la axproasly prohlbltad. Bl..contaailaaAta ara flaggad "I" enlx vhaa thay ara alaa dttactad In caavplo.

If analysaa at two diffarant dilution fêtora ata raoulrad C«««Exhibit D), follow tha data raportlrg Icatruetioaa glvtn In Exh:3 ard vlth tha *D* and *X* flags abova.

1-30

CASE NUMBER/SAS

MAR 0 9 1989 CENTRAL REGIONAL LABORATORY SAMPLE DATA REPORT*WI/CM*SI ORGANICS/INORGANICS

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CALIFORNIA WATER LAB / ( U % ^P.O. Box 4249 r

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CASE NARRATIVE - Case # 11493 - SD6 ES624

April 14, 1989

This package contains data for the following:V v /•

VOA: ES624. ES624DL. ES625. ES626, ES626DL. ES629.BS625MS, ES625MSD

BNA; ES624. ES625. ES626, ES627, ES628. ESA29, ES737, ES738,. ES739. ES740. ES741, ES742. ES743, ES744, ES628MS,ES628M$D ' * " ' '

PEST: ES6 4, ES624DL, ES625, ES626, ES627. ES627DL,ES627MS, ES627MSD, ES627MSDL. ES627MSDDL. ES628. ES629

For pesticide sample ES627MS and MSD, three compounds were offscale. Therefore, these compounds were reported from the MSDLand the MSDDL.

"Release of the data contained in this hard copy data package andin the computer-readable data submitted on floppy diskette hasbeen authorized by the Laboratory Manager or his designee asverified by the following signature."

Gloria L.Contract Laboratory Program Manager

'"..ode: i..:AL_H2u


_____.___.__ Contract: 6 01-7277

Case No.: 11493 SAS No.: SDG No.: ES624

; tKA; SAMPLE NO.

Ol IES624(>2' : EbbX4DLU3 i ESfciiSO4 ! tSfc>:,-fcO5:t5b2bOLUfc>:E3b2'9(.)/ ! ESfc25MbOtt ! tbfa25MSDO'H ! VBLK1 3

;

SI( TUt_ .) l»

911U191K.)49394989O91

s;vC BF K > #

9b1O298By105999b9792

S3( DCE ) »

92K>«*n7&93yfidfciBS83

Ol HER lUTour

C)oooooooo

yc Lim rsSi ( i f J L ) = Toluene-dS C Hb-lU>.>Wwi < H>- H > = Hr omo 11 uor ooensene (. bb-1 li 'S3 OJi,:b ) = 1, 2-1 n rhi or oethane-d4 ( /b-114 >

*t l.:oJ Limn to ftp it«ip*rt r. ri t I ao recover y v«« J UPS

* Vîue? outside of contract ream red I1' l im i ts

i) Si if r r,nai.Fj«i rJjJntRri out

J 1 VUA-1

(1)

ab Name: CAL H20

.ab C^de: CALH20

2CWATER SEMIVOLATILE SURROGATE RECOVERY

______________ Contract: 63-01-7277

Case No.: 11493 SAS No.: _____ 3D3 No E5624

;•; 1

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0405'»607OS09.L •"'•

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E3624E5625r" r~ • ^ iEao^tES627ES628E5629E3737LTC~?TQ____ *-t I -—— ' *__l

E3739ES740£3741E5742£3743ES744ES74EES628MSEC62SMSDSELK4S3LK75BLK8

SI(NBZ)#

5359o97569593931"'7.= 677oo' J •

S37S6O3873SO4391

S2(FBP)#

5559716576614666746232916380753874554669

S3<TPH>*£S3SS3=

36735831918839426942918477906495748037113

S4(PHL)tt

1413cr i

4346395455465266T~>

4350484648'351261

S5<2FP)#

2424414147•iO5152455074724456434347522263

S6(TBP) #

44561555566">*-5253495789

i o :5973285657S 1~j j.46BO

OTHER TCTOUT

0o000o0000o0o00ot j

o',)

'-;

52 (FBP>53 (TPH)54 <=HL)SX <2FP>S6 (TBP)

Nitrobenzene-d52-PluorabiphenylTerphenylPhenol-d52-Fluoraphenol2,4,6-Tr i brcmophenol

QC LIMITS< 35-114?( 43-11=)( 33-141)( 10-94 *< 21-100)( 10-123)

# Column to b» used to flag recovery values* Values outsi de o-f contract recui red QC 11 TU0 Surrogates diluted out

:ORM II SV-1(191)

Name: CAL HICO

• b Cone: f.A'.H,

WATER PESTICIDE Sl,;-^L't^rL P£;.:CVEKY

r- -... • f ,.- •* • - =- S • - r"; j - 7 7r T

& No.: 11493 ?>AS Nc. : ' _• I . 1.Oi/l-

f*l *••J L

02' >304Tie;•-'•-jGoO708O9101112i ;?;

ERASAMPLE NO.

RSA2415S624DIE3625FS62&ES627E5627CLES627MSES627MSDES627M3DDLEB627MSDLES62SEE&29PBLK1

SI 'OTHER( DBC .' ** !

11^'- ! 0172 *! 0S4 !

ics ;L. Q 'ij V t

60 ! 077 ; 070 : c59 ; o5B ! O72 : 05t ; o70 ; c

t1

ADVISORYQC LIMITS

Si <DBC) = Dibutlychlorendate ( 24-136)

$ Column to be us-ed to flag recovery value's

* Values outside o-f contract required QC limits

D Surrogates di1uted out

143

3AWAIER VOLATILE MATRIX SHlKt/MA'l tfl X SPIKE DUPLICATE RECQVEh'Y

.ab Name: CAL__H2O___________________ Contr act: 68-Q1-7277

.£ one: CALH2U.. Case No. : 1_15'=*3_ SAS No. : ____.__. SD8 No. : Ebb.

v. SPike - ERA Samp 1 e No. : ES625_______

CUMPUUNU

1 . 1-DichloroetheneTr i ch J oroethene __BenreneI oluenea

L or oDens e

SP I KEADUEUtua/L >

50 . 0SO . 050.0M>. U5O . O

SAMPLEUJNCfcNlk'Al I UN

Cug/L.)

<^2.9±iOi")o

MSCONCENTRATION

(. ug / L :>

bi. i54.451.2SO. 152 . 2

MSX

REC **

1O21 031O210O1O4

QCL i M 1 ISREC .

61-14571-1.2076-1277b-l2S7 5- ISO

;UMPUIJND

1 . i — l.'i en i or net. henei r i r i--i I rir oethene __ .benzeneT o l uene_ . _ . . _ .

"t i rir i~trn=?n / fi

&K 1 K EADDED( HQ/L.J

5". "bO. Uf;<). O50. 0?SU. O

i;MSD

ONCENTRATiON«.ud/L )

54.852.5

37 . .250 . 4

M3D'/.

Kt£C »

1 1 '-'yy74 *

li . ) 1

'/.RKL> *

------

4

3O *-:

QC LIMITSKPO i KtC.

14141 113

e.. i -14 a/l-12"

r.o oe used to f i ao recovery and KPl> valuer wi th an asterisk

otJtsirt*?- of QC limits

i-'L>: 1 our or _ ^ outside limitsnike Hproverv: 1 out of 10 out.^t ue

LI.:ASKI 1 4'^^ J i.DW-b^4 C3OP1 X

iri J^PML ^MJL Sb/X lUfl . 1 NS I *

[L1 VUA-l

(2)

•'' a v «' e v

3CWATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY

ati Name: CAL H20________________ Contract: 63-01-7277

âb Cods: CALH20 Case No.: 11493 3AS No.:

Matrix Spike - EPA Sample

iiirI COMPOUND

i PhenolJ 2-C:-.lcrcphenol

No.: ES62S

SPIKEADDED(ug/U)

ssssasasBai2OO2OO

, \ . 4-Dic;hlarcfc«nzene ___ ! 100• N-Mitraso-di -r.-prop. (1) ! ' 100

1,2. 4-Tr i ch 1 or ob sn z en e_ ! 1 004-Ch I or o-3-fretny 1 phenol I 2OOAcendiphthene ! 1004-Ni trcoherol2,4-Dini trotcluanePentscMorophenolPvrens

20010020O1OO

SAMPLECONCENTRATION

(ug/L>««««•• ss sa=ss±

000c*00000o0

i

SDS No. : ES62*

MSCONCENTRATION

(ug/L)

93.011363.246.669, 112790.821394.5ISO110

•

MSy.

REC «

47S6?6847696491107 *9575110

GCLIMITSREC.

12- 8927-12336 9741 116.39 9323 9746-11310- 8024- 969-10326-127

COMPOUND

Phsncl2-Chlorophanol1 , 4-Dic:hlorobenzene ___ >N-Ni troso-di-n-prop. (1)1,2, l-Trichlorobensene^4--Chl oro— 3— methyl phenolAcjanachthene4-Ni trophsnol2,4-Dinitrotolu»nepsr.tachlorophenolPyrer.e

SPIKEADDED<ug/L)

=as=axsMV20020010010010020010020010O2OO100

MSDCONCENTRATION

<ug/L)*«««assaas=sa

95.212458,551.758.912473.821582.5143100

MSD•//.REC #

48625952B;Q

6279108 *8372100

'/.RPD #_a!3!atsz_-2-514

-1016

f•

14-113410

OC LRPD

424028382342

' 3150"?Q•_>O

5031

EMITSREC.

12- 392, -123-:>6 ?741 115'59 932-3 97

10- 3C24- 9/S9-10326-127

<l> N-Nitroso-di*n-propylamin«

4* Column tc be us 3d to -flag recovery and RPD values with an asterisk* VAI-J.B* outside o-f OC limits

RPD: _O out of 11 outside limitsSoika Racovarv: 2 out o-f 22 outside limits

INST82COMMENTS: CCA3£114933CES62S31LV1ML CON 3/4«A+B,2UL iNJ

OB-5, 30M X 0.25MM ID, 0.25 MICRON FILM THICKNESS,

FORM III SV-1(206)

1 '3

WATEF PE-STTCTDE MATRJX SPIUE/MATRTX PP'IKE DUP! ICnTF ^fcl

.w N«.i.«: CAL H20_________________ Contract: A8-Ot-7:i?''

Lab Code: r:ALH20 Case No.: 11493 8A5 No.': . _ _ _ _ _ _ St"3 I;--.;..

Matrix Spi!;e - ERA Sr.mpie Nc. : E5627______

COMPOUND

ge.mma-BHC (Lincis,n&) _, __HaptazhlorAldrinDielcJrinEndrin4. 4 '-DOT ___ _„ _

SPIKE 1 SAMPLEADDED ! CONCENTRAT I ON(ug/L) ! (ug/L)

0.200! 00.200: o0.20O1 00.500! 00.50C! 00.5001 0

it

MECONCENTRATION

(ug/L)

000. 1200

C . 4640.537

MS7.

R£C #

0 #O *600 *93107

C;Ci.. i M i rsREC.

So-i-,340- 13140-12052-126So-12133- -127

u

o

COMPOUND

garnma-BHC (Lindane) ___HeptachlorAldrinDieldrin ____Endrin4,4'-DDT

SPIKE i MSDADDED ! CONCENTRAT I ON(un/L) J (ug/L')

=S21^5a=S£»a ! SMlBABiaE=S=SESKS =

0 . 2OO ! 00.200! 00.200! 0.1160.5OO! 00.5001 0.4810.500! 0.485

i_ — ____ • _«fc_™___

MSDV.

REC **SSSSSSK

o *0 #

S80 *

9697

•/:RPD *

==3! = = »

O030

-410

QC LRPD

1?20*?*?182127

EMITSREC.

f. 6- 1 2340-13140-12032-126N6-12133- 127

« Column to be used to flag recovery and RPD values with &n asterisk

* Values outside of QC limits

RPD: _0 out o-fiipike Recovery:

COMMENTS:

outsideout o-f

1 imi tc12 outmida limits

3EWATET; '-fcr/i rciDt: MATRIX SPIKE/MATRI * SPIKfe DUPLICATE

. Mama: CAU H2u________________ Can tract: fed--01-7277

Lsfc Code: CALH20 C<?.se No.: 11493 EAS No.: ______ SD3 No.: ES624

trix Spike - EPA Sample No.: ES627DL

> ! SPIKE ! SAMPLE! ADDED ! CONCENTRAT I UN

COMPOUND ! (ug/L) ! <uc /L>

gamma-BriC (Lint iar ie) ___ ! 0.200,! . 0Hsotachlor ! 0.200! 0A l d r - i n 1 O.2OO! O

**T>ieldrin ! 0.500! OEndr in ! 0.5OO! 04,4 ' -ODT ! O.500! 0

1 !

MSCONCENTRATION

< u g / L >

o . i 2;-;V • i A.^.

O0.2S2

00

MSIm

RED #

67'i 12 4

0 *36

0 *0 *

QCL I M I T S

RFC.

56-12340-13140-12052-12£56-12133-12 •'

COMPOUND

gamffle.-BHC (Lindar.j; ___HeotachlorAldr in

./bieldrinEndrin4,4' -DOT __________

SPIKE ! MSDADDED ! CONCENTRATION(ug/L) 1 (ug/L)

0.200! O. 1200.200! 0.1120.200! . 0O.50O! O.2S6O.50OI 00.500! 0

!

MSD

REC tt

60560 *570 *0 *

RPD #

90

— «O0

QC LRPD

S320

- 22182127

EMITSREC.

56- 1 2340-13140-12052-12656-12138-127

;

tt Column to be used ta -flag recovery and RPD values with an asterisk

* Values outside o-f DC limits

RPD: _O out ofSpike Recovery:

COMMENTS:

6 outside limit*out o-f 12 outside limits

pRRM TVI FE3T-T

4AVOLATILE METHOD BLANK SUMMARY .

Lab N*mf»: CAL...H2O • ____._____ . Contract: 6B-0.1_r.y.2Z7_

l_ cone: MAl H U Case No.: I._14y3 SAS No.: _._.____ SD6 No.: HSb24_

Lab Fil» ID: VOBLieSQffia Lao Sample ID: VQBL1890313

Date Analyzed: O3/1.3/89 Tim* Analyzed: 174&

Matrix: (soil/water) WA_TER_ Level: Clow/m*d>

In st r ument IMS 1

LOW

THIS METHOD BLANK APPLIES TO THE FOLLOWIN6 SAMPLES. MS AND MSD:

04!

! EPA! SAMPLE NU.

! httfa !4DL{ ES62S* 4> Ci *y£%

! Efcib2bL>Li KSKk.":*i tbb25MS: b.H*2aMSDi

LABSAMPLE ID

CO1244VOCO1244VU2CO124SV/0CU12&SVUC0123bVU3uoii;b4voC01245VOMSC«.)r*;4 vor'ih(.)

_.. ._ „. . _..„ _ :

t LABF ILK ID

CO 1244 VOUO1244VO2C01245VOC0125SVOC0.1255V03UO12S4VOCO1245VOMSUOl' 4SjyUM«D

! TIMEANALYZED

18S1210219242O29232O19572213•~i' fACj: . >L tO

......... ___ .. ____

X .b X 1UM) P IN6T

paqe i of 1IV VGA

(3)

Names CAL H2Q

Lab Codes CALH2O Ca»e No.s 11493

Lab File ID: BNBL2e903O4

Date Extracted: . Q3/04/B9



Instrument ID: 2______

4BSEMIVOLATILE METHOD BLANK SUMMARY

__________ Contract: feS-01-7277

SA5 No.: ____ SDG No.: £3624

Lab Sample ID: BNBL289O3Q4

Extraction:(SepF/Cont/Sonc) CDNT

Time Analyzed: 1241

Level:(low/med) LOW


: EPA; SAMPLE NO.i

01 1ES62402 ! ES62703 ! ES&2S04 ! ES62905 I ES73706 ! E373807 1 ES739OS ! ES74009 ! ES743101ES7451 1 ! ES628MS12;ES628MSD

LABSAMPLE ID

mssSSKMMMM

C01244BNC01249BNC01230BNC01234BNC01247BNC01248BNC01232BNC01246BNC01233BNC01231BNC01230BNMSC01230BNM8D

LABFILE ID

'sBsas«a=zsssssaC01244BNC01249BNC01250BNC01254BNC01247BNC01248BNC01252BNC01246BNC01253BNC01231BNC01250BNMSC012SOBNMSD

DATEANALYZED

aa = M = 55.'3SS===

03/31/8903/29/8903/31/8903/31/8903/29/8903/29/8903/31/8903/29/8903/31/8903/29/8903/31/3903/31/89

COMMENTS CASE11493 (SBLK-04) CON 3/4, 1L/1ML, A+B, 2UL INJD9-3, 30M X 0.25MM ID, 0.23 MICRON FILM THICKNESS, INST#u

; of 1FORM IV SV

(192)1/3-

Lab Name: CftL H£0

Lab Cede: CALH2D Case No.: 11493

Lab File IDs BNBLA890307

Data Extracted: . 03/07/89

Data Analysedi 04/11/89

Matrix: <soi1'water> WATER


46SEMIVOLATILE METHOD BLANK SUMMARY

__________ Contract: 68-01-7277

3AS No.: ___________ SDG Me.: ES624

Lab Sample ID: BNBLA890307

Extraction: (SepF/Cont/Scnc) CCJMT

Time Analysed: 1319

Level: (low/med) LCUJ

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, ME AND MSD:

E?ASAMPLE MO.

LABSAMPLE ID

V 0 I I ES62S ;01243BN

\ LAB! FILE IDi ssBvsaasiEx::

J C01242BN

DATEANALYZED

04/11/8°

COMMENTS: CASE11493 <SBLK-07)CON 3/7, !L/lML,Ai-B, 2UL INJD8-5, 30M X 0.2SMM ID, 0.25 MICRON FILM THICKNESS, INST#2

•ifFORM IV SV

(193)

ab Name: CAL H20

Lab Cocie: CALH20 Case No.: 11493

Lab File ID: BNBL1B90308

Date Extracted: 03/08/89


Matrix! <soil/water) WATER


4BSEMIVQLATILE METHOD BLANK SUMMARY

__________ Contract: 66-01-7277

SAS No.: ___________ SDS No.: £5624

Lab Sample ID: BNBL1890308

Extraction:(SepF/Cont/Sonc) CDNT

Time Analyzed: 1511___

Level:(low/med) LOW


EPASAMPLE NO.

ES626ES741-ES742ES744 .

LABSAMPLE ID

C01225BNC01238BNC012S7BNC01256BN

LABFILE ID

C01235BNC01258BNC01257BNCO1236BN

DATEANALYZED

04/11/3904/11/8904/11/8904/11/89

COMMENTS: CASEl1493(SBLK-08)CON 3/8, 1L/1ML, A+B, 2UL INJDB-5, 30M X 0.25MM ID, 0.25 MICRON FILM THICKNESS, . INST#2

pace i o-f 1FORM IV SV

(194)1/37 F:&v

Lab Name: CAL H20

Lab Code: CALH2O- Cas* No.I 11493

Lao Sample ID: PBLK1_______

Matrix: <soil/water) WATER

Data Extractad: 03/O7/B9

Ddta-An<a/'zed (1): Q3/2O/89

Tima Anal ysad <1): 1637

Instrument ID (1): VA3740

GC Cr:lumn ID U): 3 3P210O

4CPESTICIDE METHOD BLANK SUMMARY

________ Contract: 68-01-7277

SAS No.: ______

Lab File IDi

Level:Uow/med)

SDB No.: ES624

LOW

Extraction:(SepF/Cont/Sonc) 5EPF

Date Analyzed (2)

Time Analyzed (2>

Instrument ID (2)

QC Column ID (2)

03/2O/89

1911

VA3740

_______ . 1 55P22S

HIS METHOD BLANK APPLIES TO THE FOLLOWINS SAMPLES, MS AND MSD:

EPASAMPLE NO.

ssi2sseaass.3««

ES624E3624DLES625£3626ES627E3627DLES627MSE3627MSDE3o27MSDDLES627MSDLES628ES629

LASSAMPLE ID

C01244C01244DLCO 1245CO 1255C01249C012490UC01249MSC01249M9DC01249MSDDLCG1249MS&LC01250CO 1254

DATEANALYZED 1=sassss««aO3/20/8903/22/8903/20/8903/22/8903/20/8903/20/8903/22/8903/22/8903/21/8903/21/8903/20/8903/20/89

DATEANALYZED 2at at 3 as at s*ss= ss03/22/8903/22/89O3/21/8903/22/89O3/21 /S903/21/3903/21/3903/21/39C3/21/3903/2 1./S903/21/8903/21 /S9

COMMENTS:

t '.-A 1IV FES'

(746)

1AVOLATILE ORGANI OS ANALYSIS DATA SHEET

tPA NO.

Lab Name: CAL H20. . Contract* bb-01-7277

l i-ode: i.:ALH'2U Case No.: 114ytt . **A** No.:

Matrix: C soil/water) WATER..

yamoin wt/voi s . _5.(-» (o/mLJ ML

Level: 1.1 ow/mert > LUW__

7. Moisture: not dec.

Column*" loack/cao.* CAP

No. :

t b Samo1e 10: VOHL183O313

Lao Kile ID:

Date Received:

Date Analvzedi

Dilution Factor: 1.o

UAS NO. COMPOUNDCONCENTNATION UN ft Si(ug/L or uo/KcjJ UG_/L_ Q

74-H3-97i-ul— 4/5-OO-3

Vinvi Chloridw. „_.Uh I oroethane, .........,Metnvien* Chlorltf

/;-,-- :••— o ————————— Uarhon DisuJ75-3Jis-4 ———————— i. i-Dichloro75-:.s*»-3 ———————— 1 . 1 -Dichj.orob4O-iDS-0 —————— i . -Uichloroethime Ctotai .>fc,7-6b-3 ————————— U h i o r o t o r mlu7-Otr.-, ——————— 1 .l'/H-'-*:-i-.:i ———————— -K _ _. ...71-^-j-b ———— •: ——— l . 1 . 1-Tr ichloroethaneb-2>;-s ——————— Carbon I etrachlor ide.___.lOS-Ob-4 ——————— Vinvl Acwtat»__.___7S-V7-4 ———————— Bromociit:hloroiw»th»ne .7B-8V-5 ——————— -1. 2-l)i chloroorodanrlOot>l-O2-b- ———— lrans-1.3-Oichiorooropene.79— o 1—6 ———————— Tr ichlorof»th»n*_1^4-4y— i ——————— Dibromochloromothane79-OO-3 ———————— 1, 1,2-Trichlorowthane .71-43-2 ——————— Benzene. . . . _ . _luv-'fn i-oi-S ———— cis-i . 2-l lt.)-;^j-B ——————— 2-Ch3 oro/5— 2t>— 2 ————— ; —— -Bromotorm&91 -/K-i-. ——————— -2-H(*xrinonl OR- 1 0- 1 ——————— 4-Me»t n vi -2-: ^'/ - i H— *i ——————— i F-fcr-acti i o79-M4-tj ———————— l .1,2. 2l()tJ~HH~:-;--— —————— i n l t t ^ n ej t.jy— '-»;»— / ——————— -uhi. t~tf or31. 1 iu— -il — *]- ———— •—— fc- ' f tKi v J flOO-42-b ——————— rttyrene?133«.)-2'-.i-/ —————— lo t f l i X

.1 VUA

10 !U10 tU1O lit1() tU3 :u

l O : U

: Uill:u: u:U:U:U!U;u

105b

i f j

;u:ut U:ui u

b in^ !i Jr : it;

: u

(169)

IEVOLATILE ORGAN ICS ANALYSIS'DAT A SHEE7


EPA SAMPLE NO.

Vfal.K 1. 3Lab Nam**: CAL_.H20.

t.:odf»i CALHÛ

______..____._ Contract: &B-O\-7;^77__ ! .

Case No.: 114^3 SAS No.: ..... _ S£>8 No.: Ewt. 4

M*t-,riv,: (soil /water.) WATE=R Lab Bamnie IDs VObLl 8 o;'-:i;i

.sample wt-'vr.ls' ....S.G La/ml > Ml . Lah I- i 1« IU: VOW »1 Hyo:-n:-;

Levai: ^low/med) Luw Date Keceived:

"/. MoiFvr.ure? not dec. ... _ Date Anaivr-ed: <>3/

n,».-k/cao") CAP Dilution Fart Of: t.Ui_.ri t i imn

Number T1C» found:

CAb

CONCENI'KATIUN UN ITS a<uq/L or uq/Ko> UG/L.

CUriPOUNll NAPIfc fc'ST. CUNC,

33

VUA-- !i.:

(169)

Documents

Matrix: (soil/water) WATER Lab Samp la ID: 7SAA2A ...108-9O-7——— 100-41-4——-lorobeniene 100-42-9 ——————— FORM I VOA 100 SO 10 10 U u U u J 2 U 2 73 3,. 2