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MALAVIYA NATIONAL INSTITUTE OF TECHNOLOGY JAIPUR Materials Research Centre Information Brochure

Materials Research Centre

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MALAVIYA NATIONAL INSTITUTE OF TECHNOLOGY JAIPUR

Materials Research Centre

Information Brochure

Institute Vision

To create a centre for imparting technical education of

international standards and conducting research at the cutting

edge of technology to meet the current and future challenges

of technological development.

Institute Mission

To create technical manpower for meeting the current and

future demand of industry; to recognize education and

research in close interaction with industry with emphasis on

the development of leadership qualities in the young men and

women entering the portals of the institute with sensitivity to

social development and eye for opportunity for growth in the

international perspective.

Quality Policy

MNIT shall strive to impart knowledge in such a manner as to achieve total satisfaction of

student parents, employers, and the society.

Vision – MRC

The Materials Research Centre envisions emerging as research intensive centre for

interdisciplinary research in frontiers of materials technology. It further envisions creation and

maintenance of appropriate ambience entailing drives in research for development of

appropriate materials technology. The centre aims at fostering the growth of demanding

technology research of the day vis-à-vis creation of new knowledge pertaining to meaningful

industry-institution interaction.

Being a centre for invention and innovation of materials science and technology, it contemplates

thriving for excellence, knowledge creation & dissemination for useful economic activities,

beside creation of new generation scientist resources of the country to take the lead role in

mastering the technology development activities across the globe. The Materials Research

Centre of MNITJ will continue hybridization of newer and newer faculties of science and

engineering in order that a true culture of cooperative and participative activities in material

science and technology emblems the birth of real sense interdisciplinary entity.

About the Institute

The Malaviya National Institute of Technology Jaipur is an

Institute national Importance for technical education in India. It

was established in 1963 with the name of Malaviya Regional

Engineering College, Jaipur as a joint venture of the

Government of India and the Government of Rajasthan,

Subsequently on June 26, 2002 the college was given the status

of National Institute of Technology and on 15 August 2007,

proclaimed Institute of National Importance through an Act of

Parliament. The Institute is fully funded by Ministry of Human

Resource Development (MHRD), Government of India.

In 1963, the college started functioning from its temporary

campus at Pilani with 30 students in Electrical Engineering and

Mechanical Engineering. The college moved to the present

campus at Jaipur in 1965. The college received inspiration from

the great educationist and freedom fighter Pt. Madan Mohan

Malaviya and named after him as Malaviya Regional

Engineering College. Professor V. G. Garde, the great

educationist and visionary, was the first principal to nurture the

college into a world renowned institution.

At present there are seven 4 year undergraduate courses of

study leading to the Bachelor of Technology degree in Chemical,

Civil, Computer, Electrical, Electronics and Communication,

Mechanical and Metallurgical & Materials Engineering and 5

year Bachelor of Architecture degree and there are several PG

specializations leading to M. Tech degree, M. Sc in Physics,

Chemistry and Mathematics, M. Planning (Urban Planning) and

M.B.A. besides doctoral programmes. There are about more

than 200 highly motivated and dynamic faculty members

engaged in teaching and research in the Institute.

Currently there are several Centres of Excellence for teaching

and research purpose at MNITJ including Materials Research

Centre.

Spread over 317 acres of lush greenery, the campus of MNITJ

presents a spectacle of harmony in modern architecture, and

natural beauty which enthrals and inspires. The institute is

actively engaged in research, consultancy and developmental

activities and collaborates with leading industrial houses and IT

companies in various national and international projects.

About the Centre

Materials Research Centre (MRC) has been established as a Centre of Excellence for research in

materials at Malaviya National Institute of Technology Jaipur. It was inaugurated by Prof.

Govardhan Mehta, National Research Professor and a leading scientist and researcher in the

august presence of Shri Ashok Thakur, the Education Secretary, MHRD and Prof. I. K. Bhat, former

Director MNITJ on January 21, 2014.

Since being operational, MRC has provided research facilities, an equipment base support

infrastructure that enables faculty members, student and industry professional to conduct

successful, team oriented research and development for the fundamental understanding, and

design and creation of materials.

The Centre boasts of highly sophisticated equipment like High Resolution Transmission Electron

Microscope, X-Ray Photoelectron Spectroscopy, Nuclear Magnetic Resonance, Field Emission

Scanning Electron Microscope, Raman Spectrometer, SPM (AFM/MFM/STM), XRD, Mass

Spectrometer, AAS, GDS, RF/DC Sputtering, Thermal CVD, High Vacuum Coating Unit, FTIR, TGA,

DMA, FL, UV-VIS-NIR, Four Probe Station, SDA, Impedance Analyzer, Hall Measurement, Zeta

Potential and Particle Size Analyzer, UTM, Ion Milling, Ball Milling, DI Water Plant, Liquid

Nitrogen Plant, IR furnace, Hot Sintering Press etc. and acts as an active hub for the researchers

working in the field of materials.

The Centre have been visited by eminent professors and scientists Dr. R. A. Mashelkar, former

Director General of the Council of Scientific & Industrial Research,Dr. Kasturi Rangan, former

Chairman ISRO, Dr. Vijay Kumar Saraswat, former Director General, DRDO, Prof. Ashutosh

Sharma, Secretary, DST, Govt. of India appreciated for providing absolutely world class advanced

physical infrastructure. Recently many expert lectures/invited talks in thrust areas have been

organized. Many international and national workshop and Short Term Training Programmes/

symposia were conducted in the last few years at MRC.

The faculty members associated with the centre and providing their expertise come from the

various science and engineering departments of MNITJ viz, Physics, Chemistry, Metallurgical &

Materials, Electronics & Communication, Mechanical, Civil and Chemical Engineering. As of now,

more than 30 sponsored research projects at national and international level are being run by

the faculty. Currently there are two Scientific Officers, eight Technical Assistants and three

Technicians working at MRC to provide the required scientific and technical support to the users.

Since 2016 MRC have started M. Tech and Ph. D in Material Science & Engineering.

Director’s Message

MNIT Jaipur consistently efforts towards the growth and

transformation of young science and technical persons to develop leadership qualities,

interpersonal skills, creativity along with strong moral values to make them a better human

being. We continuously effort to attract the best students throughout the country and abroad

for our Bachelor’s, Master’s and Doctorate programs in several disciplines of science and

technology.

The excellence in teaching and research comes from the careful choice of faculty members in

which MNIT Jaipur has not made any compromise. The global perspective of our faculty makes

us a premiere Institute of higher learning in India. MNIT Jaipur has expanded its outreach to

industry and the best academic institution in the world by entering into active collaborations

with them.

The Material Research Centre envisions emerging as research intensive centre for

interdisciplinary research in frontiers of Materials technology. It further envisions creation and

maintenance of appropriate ambience entailing research in drives for development of

appropriate materials technology. The center aims at fostering the growth of demanding

technology of the day vis-à-vis creation of new knowledge pertaining to meaningful industry-

institution interaction for invention & being a centre for innovation on materials science and

technology, it contemplates striving for excellence knowledge creation & dissemination for

useful economic activities beside creation of new generation scientist resources of the country

to take the lead role in mastering the technology development activities across the globe. The

Materials Research Centre of MNIT will continue hybridization of be latest facilities of science

and engineering in order that a true culture of cooperative and participative activities in material

science and technology emblems the birth of the real sense interdisciplinary entity.

I with the Centre a bright future in furthering the cause of research.

Prof. Udaykumar R Yaragatti

Message from the Head, MRC

Materials Science and engineering (MS&E) is one the most important of

the engineering disciplines as it impacts nearly all the traditional fields of engineering. The

discipline is concerned with the structure, properties and application of materials used in

modern technology. Undoubtedly, Materials Science and Engineering is at the forefront of high

technology as the advancements in technology are the direct result of advances in materials.

Material Research Centre (MRC) was established at MNIT Jaipur, with the vision to translate the

fundamental understanding of materials into sustainable and environmental friendly

technologies and products for the social benefits. MRC is deeply involved in various domains,

namely, structural materials, functional materials, nanotechnology, energy materials and

computational materials science. With a goal of achieving excellence in education and research,

MRC houses state of the art research facilities equipped with sophisticated instrumentation for

synthesizing, characterizing, processing and imaging various types of advanced materials and

samples, which makes the MRC, second to none in the country.

MRC offers a two years M.Tech degree program in Material Science & Engineering and Ph.D.

degree program, where Course curriculums are uniquely designed, to meet the demand of

industries as well as R&D. Department believes in the holistic development of student, leading to

a good human being, to serve the nation and society.

MRC provides access of all the research facilities to the academic and industrial users in their

research work. In the Centre several Workshops, Seminars, National and International

Conferences and Visits from eminent persons are organized for active collaborations and benefit

of the industry, academia and students. This brochure provides the information about the

activities and resources of the Material Research Centre.

Prof. Vijay Janyani

High Resolution Transmission Electron Microscope (HRTEM)

1. The Tecnai G2 20 (FEI) S -Twin is

a 200 kV transmission electron

microscope which offers high

resolution imaging and

analysis solution for life

sciences, materials science,

nanotechnology and the

semiconductors.

2. The TecnaiG2 supports a wide

range of techniques including

high resolution scanning

S/TEM diffraction and

chemical analysis. The on axis

BF/DF detectors provide the Z-

contrast imaging.

3. The high angle, annular dark field detector

generates atomic resolution dark field

STEM images. The equipment provides a

point resolution of 0.24 nm, line resolution

of 0.14 nm and STEM resolution of 1.0 nm.

Attached EDS gives the elemental

compositionof material.

Applications: Provide topographical, morphological,

compositional and crystalline information.

Can be used in semiconductor analysis & production and manufacturing of computer and Si chips.

To identify flaws, fractures and damages to micro-sized objects.

Multi Mode Scanning Probe Microscope

Multimode Scanning Probe Microscope (Bruker) hasall

standard operating modes and many unique

capabilities to characterize everything from

mechanical to electrical properties at high resolution

for surface analysis of materials.

Applications:

Electrical property mapping (current and

capacitance)

Direct mapping of nanomechanical properties,

including elastic modulus, adhesion and

dissipation, at high resolution and normal scan

rates.

Field Emission Scanning Electron Microscope (FESEM)

1. Nova Nano FE-SEM 450 (FEI)

provides ultra high resolution

characterization &analysis giving

precise, true nanometer scale

information of materials.

2. Advanced optics& detection,

including beam deceleration, in

lens TLD-SE & BSE,DBS offer best

selection of information &

image optimization. Beam

landingenergy can go down from

30 keV to 0.5 keV.

3. It gives a resolution of 1.4 nm at

1 kV (TLD-SE) & 1 nm at 15 kV

(TLD-SE). The FE-SEM is coupled to

EDS detector for measuring the

elemental and chemical

composition of materials.

4. EBSD attachment (Bruker) for

microstructure properties.

Applications: Metallic materials

Ceramics and composites

Polymeric materials

Geology and mineralogy

Dental materials

Biological Materials

X-Ray Diffractometer (XRD)

1. The X-Ray Diffractometer

(Panalytical X-Pert Pro) is a

versatile equipment designed for

a wide variety of applications in

X-ray diffraction analysis on

powders, thin films, epitaxial

layers, machined materials,

ceramics etc.

2. The use of pre FIX optical

modules, sample platform &tube

rotation feature enable the user

to change the system from a high

resolution or stress texture point

focus application to a normal

Bragg-Brentano line focus

configuration or a reflectrometry

system.

Applications: •Determination of crystal

structure (phase crystallinity,

Bragg’s plane, particle/crystallite

size, etc)

•Quantitative texture analysis

•Preferred orientation studies

•Reflection topography, etc.

XPS (X-Ray Photoelectron Spectroscopy)

Features (ESCA+ Omicron Nano

Technology):

• Small Spot XPS for High Speed Depth

Profiling

• Dual Beam Charge Neutralization

•Fully Integrated Software Control and

Automation

• Rapid Quantification within MultiPak

or CASA XPS

Applications:

• Surface analysis of organic and inorganic materials

• Determining composition and chemical state information from surfaces

• Depth profiling for thin film composition

• Thin film oxide thickness measurements

Confocal Raman Spectrometer with PL

Features (STR500Airix):

• Compact & flexible system configuration.

• High resolution: <0.5 cm-1 and

measurement

down to <50 cm-1.

• Confocal optics and fully automated 2D, 3D

&

4DRaman imaging.

•Lasers available: 325 nm, 532 nm, 785nm.

Applications:

Thin films, semiconductor, polymers, Carbon nano particles (CNT, grapheme ), composites,

petrochemical, pharmaceutical, gems, etc.

Nuclear Magnetic Resonance Spectrometer(NMR)

1. ECS 400 MHz (JEOL) NMR

spectrometer is a 2- channel

console with a flexible broad

band RF performance.

2. It is capable of providing

spectra of a variety of NMR-

active nuclei such as 1H, 13C, 19F and metals like 29Si, 31P, 119Sn, 51V, 77Se,113Cd, 195Pt,

etc. in distinct chemical

environments without any

timedelay.

3. Low temperature accessory permits variable temperature.

4. Capable of recording 2D spectra (COSY, NOESY, HETCOR, etc.)

Applications:

• Determination of the content and purity of a sample through space connectivity

(Overhauser effect)

• Chemical dynamics (Line shapes, relaxation phenomena)

• Synthetic organic chemistry, inorganic chemistry, bio-organic chemistry, bio-inorganic

Chemistry, polymer chemistry & organometallic chemistry.

Mass Spectrometer

1. Xevo G2-S Q-Tof (Waters, USA)

provides a wide range of mass

analysis of small organic, inorganic

and organometallic compounds to

large polymeric & proteomics

samples including proteins &

peptides.

2. The Q-Tof technology in this

instrument provides superior UPLC-

compatiblemass resolution, matrix-

tolerant dynamic range, quantitative

performance, simultaneous mass

accuracy and speed of analysis.

Fast data directed analysis allows

full structural characterization of

unknown compounds.

3. The UPLC/MS data acquisition comprehensively catalogs complex samples in a single

analysis. Universal Ion Source Architecture enables the most extensive range of interface

capabilities to service the broadest range of applications.

Applications:

• Chemistry (organic, inorganic materials, etc.)

• Life Sciences and Pharmaceuticals

• Pesticide Detection

• Food Analysis

Environmental

Atomic Absorption Spectrometer (AAS)

It is used for ppm to high ppb determination of metals in aqueous solutions. An aqueous sample is aspirated into a flame that has a beam of light passing through it which is specific to the element being determined. Atoms of that element absorb some of the light, which ismeasured by adetector. The absorbance is proportional to the concentration of the element in the original sample. Thus, by comparing the absorbance in an unknown sample with that of solutions of known composition (standards), the concentration of theanalytic inthe original sample canbe determined.

Applications:

• Facilitates analysis of metal ion concentrations in aqueous solution

• It can analyze metals including Fe, Cu, AI, Pb, As,

Zn, Cd, etc. Typical lower limit for determination is in the mg/L range.

Glow Discharge Spectrometer (GDS)

Glow Discharge Spectrometer utilizes a lowpressure, non-thermal process in which material is uniformly sputtered from the sample surface by a stream of argon ions. The sputtered material is then atomized and excited in a low-pressure plasma discharge, away from the sample surface. It delivers highly accurate bulk analysis as well as compositional depth profiling for coatings analysis and surface treatments. This instrument offers aspectral range from 120to 800 nm.

Applications:

• Used for detection of a wide range of elements in materials such as steel, cast iron, aluminum,

copper, zinc, nickel, cobalt, tungsten, and titanium, etc.

• Can also work with low melting alloys, powder metals, resulphurized steel and other complex

materials

UV-Vis NIR spectrophotometer

LAMBDA 750 (Perkin Elmer) UV-Vis NIR

Spectrophotometer instrument is a bench-

top, true double-beam, double-

monochromator design providing high

stability & accurate performance for

samples in the area of chemical sciences,

biochemistry, materials science,

nanoscience and technology.

Applications:

• Application areas range from surface

characterization of solids to the photometric

analysis of turbid, colloidal, transparent and

translucent samples.

• Typical uses encompass quality assurance

testing and product development

measurements on textiles, dyes, paper and

glass.

• Measurement of transmittance,

absorbance and refractive index of

transparent thin films.

Fourier Transform Infrared spectrometer (FTIR) 1. FT-IR Spectrum 2 (Perkin Elmer) is

acompact, easy to use, powerful

instrument with fully integrated,

universal sampling system for

measurements in the range of 4000-400

cm-1 for liquid (in KBr cell) and solid

(inKBrpellets) samples.

2. It also finds applications in IR sampling,

spectral and field based analysis.

Applications:

• Pharmaceuticals and Nutraceuticals

• Polymers

• Environmental

• In-service lubricants and fuels

Fluorescence Spectrophotometer

The LS 55 (Perkin Elmer) Fluorescence

spectrophotometer provides all types of data

applications that require fluorescence,

phosphorescence, bioluminescence,

chemiluminescence etc. with excitation range

of 200-800 nm.

Applications:

• Cell based cytotoxicity, cell viability, cell quantification, cell proliferation, adhesion, and

reporter gene expression, apoptosis, clinical enzyme and substrate assays, porphyrins, steroids,

blood flow.

• Environmental pesticide detection on many substrates including leaves, ground water tracing,

oil contamination of fresh and marine water, EROD assays, chlorophyll determination of normal

and toxic algae.

• Pharmaceutical vitamins, biogenic amines, pharmaceutical and abuse drugs, toxicity assays,

cell function assays.

• Inorganic aluminium, lead, magnesium, manganese, selenium, tin, zinc, etc.

Zeta Potential and Nano Particle SizeAnalyzer The Zetasizer Nano ZSP (ZEN 5600) is used for the measurement of particle size upto 0.3 nm,

zeta potential of nanoparticles and surfaces.

High Vacuum Thermal Coating Unit

1. High vacuum thermal/e-beam coating unit

(Model BC-300 HHV) is a versatile coating

unit for thin film fabrication which includes

evaporation, glow discharge cleaning, etc.

2. The system offers a variable source to target

distance of 30-80 cm & uniform deposition

over 3cm diameter.

3. The temperature of the substrate can be

varied from RT to 550 ˚C. Possible

deposition materials are all semiconductors,

oxides and metals.

Applications:

• Protective coatings and interference filters

•Reflection & anti-reflection layers

• Anti-corrosive layers

• Electrically conductive & transparentcoatings

Contact layers

Thermal Chemical Vapour Deposition

Thermal chemical vapour deposition unit

(Technos Instruments) is an economical

R&D system with uniform heating zone

providing process solutions for

production of single and multi walled

carbon nanotubes (SWCNT and MWCNT

respectively) using fixed bed method.

Applications:

• CNT growth for various devices

• Metal oxides, Graphene

• Carbon nanofiber and particles

RF/DC Magnetron Sputtering Unit

1. RF/DC magnetron sputtering unit

(APT) can coat thin films of metals,

semiconductors and oxides capable

of producing vacuum up to 5x10-

6Torr.

2. The system has two magnetron

cathodes (size of each sputtering

target is 2 inches) with possibility of

both RF and DC operations.

3. Rotatable substrate holder is

capable of holding substrates of

sizes from one cm to one inch diameter and substrate heating upto 800 ˚C .

4. The system has two mass flow controllers, one

for argon and the other for nitrogen / oxygen.

Reactive sputtering can also be done.

Applications:

•Metals, oxides & semiconductor thin films

• Solar cell

• Reactive sputtering

Spin Coater

1. Spin Coating System (APEX) is an

Indispensable tool for fabricating

thin films on asuitable substrate.

2. Easy to use, safe and inexpensive.

This method is extremely desirable for

many applications where high qualities

of layers are required.

Applications:

Thin film coatings on semiconductors/ metals & glass

• Deposition of organic films

Dynamic Mechanical Analyzer (DMA)

DMA - 8000 (Perkin Elmer) is widely

used to characterize materials

properties as a function of

temperature, time, frequency, stress,

atmosphere or a combination of

these parameters; where a small

deformation isapplied to asample in a

cyclic manner. Any solid material

including powders (with material

packets) can be characterized using

DMA.

Applications:

• DMA can measure stiffness, loss modulus, storage modulus, tan 0, Young's modulus, glass

transition temperature Tg, Beta transition and stress relaxation behaviours for various

visco-elastic materials under time as well as temperature scan conditions

• One ofthe most unique and useful features of the DMA is its rotating analysis head, which can

be oriented through a full 180° for optimal analysis head configuration for virtually any test type

and sample geometry

• DMA permits operation in a "constant force (TMA) mode" vs. time or temperature.

Applications such as expansion coefficient, softening and penetration, or extension or

contraction in tension geometry provide valuable data equivalent to many commercial

standalone TMA instruments

• Ideal for advanced research and routine quality testing in polymers, composites,

pharmaceutical, and food industry in controlled humidity, UV environment and temperatures

ranging from -190 ˚C to 400 ˚C

TGA-DTA 1. The STA 6000 (Perkin Elmer)

features the innovative SaTurnA™

Sensor for high quality,

simultaneous TO and DTA

measurements.

2. This advanced sensor is optimized

to achieve flat DTA baselines and

high sensitivity. Simultaneous

measurement of both sample and

reference provides accurate

analysis.

3. The corrosion-resistant, pure platinum pan holder and reference ring make the instrument

suitable for a wide variety of samples and applications.

4. Temperature range 15˚C-1000˚C.

Applications:

Oxidative stabilities

Thermal stabilities

• Glass transition temperatures

• Transition and reaction enthalpies

Abrasive Cutter

The AbrasiMatic® 300 (Buehler) abrasive cutter is

abenchtop cutter featuring manual cutting action in

three directions and automated cutting in one

direction .

High Speed Diamond Cutter Isomet 4000 (Buehler) is a versatile linear precision

saw which enables to cut all kind of delicate

specimen with minimal damage due to deformation.

Semi-Automatic Polisher

MetaServ® 250 (Buehler) High Speed Twin

grinderpolishers offer a combination of

performance, economy and reliability for most

microstructural analysis applications. The platen

diameter is 8inch with 50-500 rpm speed in 10rpm

increment.

Hot Mounting Press Simplimet 3000 (Buehler) Automatic Mounting

Press is a durable press with basic features that

provides effective mounting, increases productivity

and specimen consistency verses manual mounting

press.

Disc Grinder, Disc Punch & Hot Plate

Model 623-40 (Gatan) specimen mounting Hot Plate

is thermostatically controlled at the precise mounting

temperature of 130°C. It can be used for preparing 3

mm metallic disc of thickness less than 200 µm.

Dimple Grinder with Stereomicroscope

Model 656 (Gatan) Dimple Grinder can reduce, with

minimal damage, the central region of a typical

100 µm thick, 3 mm diameter specimen blank to a

few microns in times ranging from 20 minutes for

silicon to 100 minutes for sapphire. It can be used

for direct preparation of TEM specimens.

Ion Beam Milling

1. PIPS II incorporates the patented Whisperlok®

with the X, Y positioning stage for precise

centering of the milling target. The PIPS II

incorporates a 10 inch touch screen for ease of

use and increased control and reproducibility

ofthe milling process.

2. The Digital Zoom Microscope monitors the

polishing process and the color images can be

stored in Gatan's Digital Micrograph" software

for review and analysis during preparation of

sample for TEM.

Ilion-II

Vacuum load-lock and liquid nitrogen cold stage to

provide rapid workflows on beam sensitive samples.

Real-time observation of the polishing process

including an optical microscope with digital imaging;

images can be stored and analyzed with Digital

Micrograph® software from Gatan.

Repeatable results from recipes and operation of the

Ilion™ II via a 10 inchcolour touch screen interface.

Damage-free surfaces for analytical techniques, such

as cathodoluminescence and EBSD, where the signal

is generated near the surface.

Twin Jet Tenupol

1. TenuPol-5 (Struers) provides a perforated specimen for

transmission electron microscopy from a sample of 3

mm dia. in just a few minutes.

2. It can perform electrolytic polishing and chemical

thinning.

3. The specimen is polished from both sides

simultaneously, thus providing a structure with a

minimum of deformation.

Ultrasonicator

Ultramet 2005 (Buehler) sonicator with a 9.5 litre capacity.

It can quickly clean samples suitable for the next

preparation step.

Planetary Ball Mill

1. Pulverisette 6 (Fritsch) Planetary Ball Mill is capable of

mixing and perfect homogenising of emulsions or

pastes.

2. Maximum output sample quantity is40 ml.

3. Tungsten carbide and tempered steel ball and bowl

material with variable speed upto 650 rpm.

4. GTM attachment for temperature monitoring.

Optical Microscope

Capabilities of CarI Zeiss (AX10 Vert.A1)

• Inverted optical microscope

• Large area scanning is also possible

• Suitable for metallic, ceramic, polymer and

biological samples

•Bright field, dark field and polarized imaging

• IVF contrast system

• Resolution: 0.1 µm

Microwave Reactor 1. Microwave reactor (CEM Discover) offers

the possibility of reactions running up to

300°C and 300 psi in 10mL to 80 mL sealed

vessels. Additionally, open-vessel reactions

can be run using conventional round-bottom

flasks (up to 125 mL) equipped with a reflux

condenser.

Applications:

• Opening of new reaction pathways

• Increase in yields in difficult chemistries

• Increase of purity profiles/selectivity in product mixtures

• Decrease of reaction times from hours or days to minutes

Semiconductor Device Analyzer

1. (Agilent B 1500A) integrates multiple

measurement and analysis capabilities

for accurate and quick device

characterization into a single instrument.

2. It supports all aspects of measurement,

from fundamental current-voltage and

capacitance-voltage characterization up

to state-of the art fast pulsed current

voltage testing.

Applications:

• CMOS Transistor: Id-Vg,Id-Vd,Vth ,breakdown, capacitance, QSCV, etc.

• Bipolar Junction Transistor (BJT): lc-Vc , diode, Gummel plot, breakdown, hfe, capacitance, etc.

Discrete device: Id-Vg,Id-Vd,lc-Vc, diode, etc.

• Memory: Vth , capacitance, endurance test, etc.

Probe Station The MicroXact's SPS-2200 system IS premier

manual probe station designed to be flexible

and easy to use with up to 200 mm wafer

capabilities, DC or RF probes, optional thermal

chuck, and a variety of shielding options. The

probe station can be used for the wide range of

applications, such as failure analysis, reliability

testing, IV/CV testing and general

characterization. Thermal chuck with

temperature range of -20 ˚C to +200 ˚Cis there.

Precision Impedance Analyzer The 6500 series of Precision Impedance Analyzers

provide precise and fast testing of components at

frequencies up to 120MHz. Basic measurement

accuracy is±0.05% making the instruments the best

inthe class.

Measurement Parameters: Capacitance

(C),Inductance (L), Resistance (R),Reactance (X),

Conductance (G), Susceptance (B), Dissipation Factor

(D), Quality Factor (Q), Impedance (Z), Admittance (Y),

Phase Angle (ø).

Hall Effect Measurement System

The HMS-5000 series / HMS-7000 series

Hall Effect Measurement Systems have

automated magnet movement, variable

temperature capability, and powerful

analysis software.

The systems can be used to characterize

various materials including all semiconductors

including Si, SiGe, SiC, GaAs, InGaAs, InP, GaN

(N Type & P Type can be measured), metal

layers, oxides, etc. Sample testing can be

performed to demonstrate the system’s capability.

Electrochemical Work Station

K-Lyte 1.0 is a versatile instrument for

electrochemical analysis. This instrument

facilitates CV, LSV, Chronoamperometry.

K-Lyte 1.0 includes well customized

software which helps in analyzing the

results from hardware. Overall this

instrument is suitable platform for

learners and researchers.

Specifications:

Instrument current limit is 100 mA

Voltage ranges from -1.5 to 1.5

USB interface with computer

Inbuilt dummy cell for calibration

Auto cut at limiting currents

Water Purification System

aquaMAX™ Basic Series: YL aquaMAX Basic 360 Series is the water purification system that produces pure water from tap or underground water. This system can reject more than 99% of inorganic and organic contaminants in the feed water.

aquaMAX™ Ultra Series: The aquaMAX™ Ultra 370

Series – Ultra Water Purification System produces

ultra-pure water in resistivity 18.2 MΩcm and

inorganics reduction up to 99.99% (TOC level to <10

ppb). The water quality aquaMAXTM- Ultra complies

with ASTM, CAP, ACS and NCCLS to be used with

HPLC, GC, IC, AAS, ICP and ICP - MS.

Liquid Nitrogen Plant

Production of Liquid

nitrogen takes place in two

distinct steps. First,

nitrogen gas is produced

from air. Second, the

gaseous nitrogen is passed

through a cryo refrigerator

to liquefy the gas to

produce liquid nitrogen.

Plant producing capability

is 40 liters/day of liquid

nitrogen.

Applications:

Freezing and transport of food products Cryopreservation of biological samples such as bull semen Cryo-therapy to remove skin abnormalities Shielding materials from oxygen exposure Coolant for superconductors, vacuum pumps, and other materials and

equipment Cooling material for easier machining or fracturing

Universal Testing Machine (UTM)

Instron-5967 Universal testing machines can perform tensile, compression, bend, peel, tear, and other mechanical tests on materials.

Specifications:

30 kN (6,750 lbf) capacity 1212 mm (47.7 in) vertical test space 1712 mm (67.4 in) vertical test space (Extra-

height model)

Micro Hardness Tester

Capabilities of NEXUS 4303

• Automatic Micro- Vickers, Macro-Vickers, Knoop

hardness tester

• Variable loads are possible for Vickers 20 gf-30 kgf, for

Knoop 20 gf -2k gf

• Variable loading speed

• Display resolution: 0.1 HV and 0.1 HK

Sintering Hot Press

Maximum attainable temperature : 1000 °C

Max Ramp rate: 10°C/ min

Maximum load attainable : 25 Ton

Acceptable load on graphite die is up to 5 Ton

Sintering in Ar atmosphere

Chiller water cooling

Accelrys Materials Studio 8.0 Materials Studio is a complete modeling and simulation environment designed to allow

researchers in materials science and chemistry to predict and understand the relationships of a

material's atomic and molecular structure with its properties and behavior. Using Accelrys

Materials Studio 8.0, researchers in many industries are engineering better performing materials

of all types, including pharmaceuticals, catalysts, polymers and composites, metals and alloys,

batteries and fuel cells, and more.

Materials Studio software has been integrated with the following modules:

CASTEP, DMo13, DFTB+, Forcite, Adsorption Locator, Amorphous Cell, Blends, CCDC,

Conformers, DPD, Discover, Equilibria, Gaussian, GULP, Kinetix, Mesodyn, Mesocite,

Morphology, ONETEP, Polymorph, QMERA, Reflex, Sorption, Synthia VAMP.

COMSOL: Multiphysics Software

1. COMSOL Multiphysics™ is finite element analysis,

solver and simulation software. FEA Software

package is an especially coupled phenomena or

multiphysics for various physics and engineering

applications.

Available Modules

AC/DC Module, Acoustics Module, Batteries & Fuel Cells Module, CAD Import Module, CFD

Module, Chemical Reaction Engineering Module, Corrosion Module, ECAD Import Module,

Electrochemistry Module, Electrodeposition Module, Fatigue Module, Geomechanics Module,

Heat Transfer Module, Live Link Products for CAD, LiveLink for MATLAB, LiveLink for

Excel,Material Library, MEMS Module, Microfluidics Module, Molecular Flow Module, Multibody

Dynamics Module, Nonlinear Structural Materials Module, Optimization Module, Particle Tracing

Module, Pipe Flow Module, Plasma Module, RF Module, Semiconductor Module, Structural

Mechanics Module, Subsurface Flow Module, Wave Optics Module.

IC Cap Device Software 1. Integrated Circuit Characterization and Analysis Program (lC-CAP) is the industry

standard for DC and RF semiconductor device modeling. IC-CAP extracts accurate

compact models used in high speed/digital, analog and power RF applications.

2. The most advanced semiconductor foundries and IDMs rely on IC-CAP for modeling

silicon CMOS, Bipolar, compound gallium arsenide (GaAs), gallium nitride (GaN) and

many other device technologies. IC-CAP is the most advanced, customizable modeling

software and includes measurement, simulation, optimization and statistical analysis

tools.

Applications:

• Open software architecture enables maximum accuracy and provides ultimate flexibility to

create and automate measurement, extraction and verification procedures.

• Turnkey extraction solutions for industry standard CMOS models, such as BSIM3/BSIM4, PSP

and HiSIM, minimize the learning curve and maximize model accuracy.

• Most direct links to commercial simulators ensure consistency between extracted models and

the simulators used by circuit designers.

Faculty Profile

Dr. Vijay Janyani

Professor & Head, MRC

Ph.D. (UK), M.E. (Electronics & Electrical Comm), B.E. (Electronics and

Communication)

Research Interests: Optical Communication, Optoelectronics and

Photonics, Numerical Modelling, Nonlinear Optics, RF and Microwaves,

Optical Networks, Solar Energy.

Prof. Kanupriya Sachdev

Professor, MRC

Ph.D. (Physics), M.Phil. (Physics) M.Sc. (Physics), B.Sc. (Physics, Maths,

Chemistry)

Research Interests: Material Science and technology, Condensed Matter

Physics, Transparent Conducting thin film oxides , Metal oxide doped

with metal & rare earth metal , Surface modification by ionbeam

irradiation/ Glow Discharge Plasma, Thermo-chemical behaviour of

amorphous alloys.

Prof. Ragini Gupta

Professor, MRC

Ph.D. (Organic Chemistry), M. Sc. (Organic Chemistry) , B.Sc.

Research Interests: Synthetic Organo-Fluorine Compounds, Some aspects

of the Chemistry of Biologically Active Heterocyclic Compounds, Click

Chemistry, Nano-chemistry, Green Chemistry, Biocatalysis, Phase Transfer

Catalysis and Microwave Chemistry.

Dr. Amit Kumar Singh

Assistant Professor, MRC

Ph.D. (Mechanical Engg), M.Tech.(Manufacturing Systems Eng), B.Tech.

(Mechanical Engg)

Research Interests: Bio-Mechanics, Additive Manufacturing, Rapid Tooling,

CAD/CAM/CAE.

Prof. Malay Kumar Banerjee Chair Professor Ph.D. (Metallurgical Engineering), M.E.(Physical Metallurgy), B.E.(Metallurgical Engineering) Research Interests: Nonlinear Mathematical Models, Neural Networks, Modeling and Simulation, Material Science and technology, Materials Science: Atom Transport Studies, Mechanical Metallurgy.

Dr. Himmat Singh Kushwaha DST-INSPIRE Faculty

Ph.D. (Material Science), M.Tech (Nanotechnology), B.Tech

(Nanotechnology)

Research Interests:Redox Flow Batteries, Solar Fuels, Alkaline Fuel Cells,

Self Cleaning Glass Ceramics.

Scientific & Technical Staff

Mohtashim Reza

Scientific Officer

B.Tech. (Instrumentation & Control Engg.)

ChetanyaPrakash

Scientific Officer

M. Sc. (Physics),

Advanced P. G. Diploma (Nanotechnology)

Ramesh Chandra Prajapati

Technical Assistant

B.Tech. (Electronics & Communication Engg.)

Shubham Gautam

Technical Assistant

Diploma, AMIE (Electronics & Communication Engg.)

Hitesh Kumar Sharma

Technical Assistant

Diploma, B.E. (Electronics & Communication Engg.)

Atul Kumar Sharma

Technical Assistant

B.E. (Electronics & Communication Engg.), M.Tech. (Optoelectronics)

Amit Kumar Sharma

Technical Assistant

B.Tech. (Electronics & Communication Engg.)

Dr. Shriniwas Yadav

Technical Assistant

B.Tech. (Instrumentation), M.Tech (Nanotechnology), Ph.D. (Nanotechnology)

Sourabh Sharma

Technician

M.Sc. (Physics), PGDCA, CPLT

Bhupesh Kumar Sharma

Technical Assistant (Contract)

B.Tech. (Mechanical Engineering)

Dr. BhagwanSahaiYadav

Technical Assistant (Contract)

M. Sc. (Chemistry), Ph. D.

Jai Prakash Dixit

Technician (Out Source)

Diploma (Electrical Engg.)

Deepak Kumawat

Technician (Out Source)

ITI (Mechanical)

Office Staff

Surendra Kumar Kumawat

Office Assistant

ITI (Mechanic Diesel), Diploma (Electrical Engg.) & B.A.

Industrial Beneficiaries

Materials Research Centre

MALAVIYA NATIONAL INSTITUTE OF TECHNOLOGY JAIPUR

JawaharLal Nehru Marg, Jaipur-302017, E-mail: [email protected]

Phone No: +91-141-2713568

Director’s Office: +91-141-2529087, Registrar: +91-141-2529078, Fax: +91-141-2529029

www.mnit.ac.in