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^ L X ^ AnalyficalTechnoiogies, Inc
SFUND RECORDS CTR
88015256 SFUNO RECORDS CTR
0222-00703
GCMS - RESULTS
REAGENT BLANK
7717^ y / u A
AR055S
TEST : VOLATILE ORGANICS (EPA 624)
CLIENT : MONTGOMERY & ASSOCIATES PROJECT # : 661D PROJECT NAME : HASSAYAMPA CLIENT I.D. : REAGENT BLANK
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
806130 06/29/88 06/29/88 UG/L N/A
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE, 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4~METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES
<10 <10 <1 <1 TR TR <1 <1 <1 <1 <1 <1 <10 <1 . <1 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <5 <10 <10 <1 <1 <1 <1 <1 <1
1 ^ - ' . • - ' • C - . \ , I r : J o/ti,»;;j
SURROGATE PERCENT RECOVERIES
1,2-DICHLOROETHANE-D4 BFB (%) T0LUENE-D8 (%)
(%) 97 111 98
{oT-'H >>90 - ' / 77^
DHTH: Bb23 iil CALI: 8629 #2
RIC ^z2S/yi?i 12:34:06 SAMPLE: REAGENT BLANK SML CONDS.: C ^ RAHGE: G 1.. 1200 LABEL: N O. 4 . 8 QUAN: A
lOO.y-i
c o
o
n
Z CD - ' CG G V. X 0-
r\i r- V
a . I <
-- c Z UJ — X Li. cn
I—»
V 2 '_' •— i~ U
RIC
71
'6\Zl
IS i ^A •"'=
384
JiiJLs / 435
t-Or"
J L.
SCAN JC 1 TO 1200
0 J 0 BASE: U 28.. 3
753
, I
I I ^ ^ J SnK
153784.
2tIH 4L1L1
13:20 b'JL'' . '1: f-t r-l 26:40
1000 33:20
—I 1209 SCAN 40:08 TIME
PROCEDURE DATA F I L E REFERENCE NAME L I S T
REPORT
TCA DIAGNOSTIC REPORT B629 B629 VQN INITIALIZATION OPTION; 2 VQSTDS
6 / 2 9 / 8 8 13; 1 '3; 11
PROCESSING OPTION;
: STANDARDS X PLUS UNKNOWNS PROC USED POSS RMS PROC USED POSS
6 6 1 44 18 7 1 6 6 1 44 18 6 1 6 6 1 44 18 6 1
-— ><: - L I S T NAMES - : RMS STANDARD/UNKNOWN
56 VQSTDS/VQl 44 VQSTDS/VQ2 44 VQSTDS/VQ3
42 COMPOUNDS PROCESSED, 7 FOUND
COMPOUND >^ MO L I B ENTRY
1 VQ 1 2 VQ 2 3 VQ 3 4 VQ 4 5 VQ 5 6 VQ 6 7 VQ 7 8 VQ 8 9 VQ 9
10 VQ 10 11 VQ 11 12 VQ 12 13 VQ 13 ' 4 VQ 14
j VQ 15 16 VQ 16 17 VQ 17 18 VQ 18 19 VQ 19 20 VQ 2 0 21 VQ 21 22 VQ 2 2 23 VQ 23 24 VQ 24 25 VQ 25 26 VQ 26 27 VQ 27 28 VQ 28 29 VQ 29 30 VQ 30 31 VQ 31 32 VQ 32 33 VQ 33 34 VQ 34 35 VQ 35 36 VQ 36 37 VQ 37 38 VQ 38 39 VQ 39
1 VQ 40 rl VQ 41 42 VQ 42
REF - 3 0 0 - 6 0 8 - 7 5 8 - 3 8 2 - 7 2 1 - 9 0 2
- 5 4 - 8 5
- 1 0 7 - 1 3 7 - 2 0 3 - 2 2 2 - 2 5 2 - 2 8 6 - 3 2 6 - 3 4 6 - 3 6 3 - 3 8 5 - 3 8 2 - 4 2 4 - 4 3 6 - 4 3 8 - 4 5 0 - 6 8 6 - 4 9 1 - 4 9 9 - 5 1 5 - 5 3 4 - 5 3 7 - 5 3 1 - 5 3 7 - 5 7 0 - 6 1 6 - 6 3 1 - 6 7 8 - 6 8 7 - 7 2 7 - 7 6 2 - 8 2 4 - 9 4 7 - 9 8 7 - 9 5 6
PRED 3 0 2 6 1 0 7 5 9 3 8 4 7 2 2 9 0 3
5 8 8 9
1 1 1 1 4 1 2 0 6 2 2 5 2 5 5 2 8 9 3 2 9 3 4 9 3 6 6 3 8 8 3 8 4 4 2 6 4 3 8 4 4 0 4 5 2 6 8 7 4 9 3 5 0 1 5 1 7 5 3 6 5 3 9 5 3 3 5 3 9 5 7 2 6 1 7 6 3 2 6 7 9 6 8 8 7 2 8 7 6 3 8 2 5 9 4 7 9 8 7 9 5 6
- SEARCH -SEL DELTA PEAKS F I T 303 1 1 97£ 609 - 1 1 92C 759 1 995 3 8 4 7 2 2 9 0 3
2o: 7
1 997 1 9 4 t 1 97C
I 3
'
I 893
>< SAT >< PEAKS M/Z
1 2 8 1 1 4
, . 1 1 7 6 5
) 98 3 95
5 0 9 4 6 2 6 4 8 4 4 3 7 6 9 6 6 3 9 6 8 3 6 2 7 2 9 7
1 1 7 4 3 8 3 8 3 6 3 7 5
1 3 0 1 2 9
9 7 7 8 7 5 6 3
1 7 3 1 7 3
4 3 1 6 4
9 2 1 1 2 1 0 6 1 0 4 1 0 6 1 0 6
— CHRO — TOP DELTA 302 - 1 6 0 9 7 5 9 3 8 4 7 2 2 9 0 3
206 - ] 2 2 5
5 3 3
6 7 9
7 2 7
7 6 2
— —. PEAKS
L 1 1
1
Cl .
1 1
Q i j a n t i t a t i on Repor t F i l e ; B629
D.-!ta'; B629, TI OA/29/88 12;34;00
pie: REAGENT BLANK SML Conds, ; GC4 Formula; Instrument; 1050 Weight; 0.004 Submitted by: Analyst: MGB Acct. No. ;
AMOUNT=AREA * REF AMNT/<REF AREA * RESP FACT) Resp. fac. from Library Entry
No Name 1 ISl BROMOCHLOROMETHANE 2 IS2 1,4-DIFLUOROBENZENE 3 IS3 CHL0R0BENZENE-D5 4 SSI DICHL0R0ETNANE-D4 5 SS2 TOLUENE-DS 6 SS3 BROMOFLUOROBENZENE 7 45V CHLOROMETHANE 8 46V BROMOMETHANE 9 88V VINYL CHLORIDE 10 16V CHLOROETHANE 11 44V METHYLENE CHLORIDE 12 13H ACETONE 13 15H CARBON DISULFIDE 14 29V 1, l-DICHLOROETHENE 15 13V 1,1-DICHLOROETHANE 16 30V TRANS-1<2-DICHLOROETHENE •7 23V CHLOROFORM i IOV 1,2-DICHLOROETHANE
19 14H 2-BUTAANONE 20 IIV 1,1.1-TRICHLOROETHANE 21 6V CARBON TETRACHLORIDE 22 19H VINYL ACETATE 23 48V BROMODICHLOROMETHANE 24 15V 1,1,2,2-TETRACHLaROETHANE 25 32V 1,2-DICHLOROPROPANE 26 33VT TRANS-1, 3-DICHLOROPROPANE 27 87V TRICHLOROETHENE 38 51V DIBROMOCHLOROMETHANE 29 14V 1,1,2-TRICHLOROETHANE 30 4V BENZENE 31 33VC CI3-1,3-DICHLORQPROPENE 32 19V 2-CHLOROETHYL VINYL ETHER 33 47V BROMOFORM 34 4-METHYL-2-PENTAN0NE 35 16H 2-HEXANONE 36 85V TETRACHLOROETHENE 37 86V TOLUENE 38 7V CHLOROBENZENE 39 38V ETHYLBENZENE 40 18H STYRENE 41 20H TOTAL XYLENES 42 XYLENES
Nrj
1 2 "i
4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 ^9 ?
30 31 32 33 34 35 36 37 38 39 40 41 42
m/ z 128 114 117 65 98 95
NOT NOT NOT NOT 84 43
NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT NOT 78
NOT NOT NOT NOT 43
NOT 92 112 NOT NOT NOT NOT
Scan 302 609 759 384 722 903
FOUND FOUND FOUND FOUND
206 225
FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND FOUND
533 FOUND FOUND FOUND FOUND
679 FOUND
727 762
FOUND FOUND FOUND FOUND
Time 10: 04 20: 18 25: 18 12; 48 24: 04 30: 06
6: 52 7: 30
17; 46
22:38
24: 14 25; 24
Ref 1 2 3 1 3 3
RRT 1. 000 1. 000 1. 000 1. 272 0. 951 1, 190
Meth A BB
Area(Hght) Amount XTot
A A A A A
BB BB BB BQ QB
0. 682 A BB 0, 745 A BB
0. 875 A BB
3 0. 895 A*VV
3 0. 958 A BQ 3 1, 004 A BQ
56196, 346341. 268720. 103712. 360490, 223139,
865.
50, 000 50, 000 50, 000 97. 015 98, 203 111. 114
UG/L UG/L UG/L 7. 7. y.
10. 10, 10, 20, 21.
70 70 70 75 01
23, 77
3799, 3658,
2, 100 UG/L 7. 892 UG/L
0. 45 1. 69
/ y
0. 141 UG/L 0. 03
804,
260. 1801.
0,
0, 0,
624
064 341
UG/L
UG/L UG/L
0,
0. 0,
13
01 07
/ \ AnalyticalTechnologies, Inc GCMS - RESULTS
77/TV-^U A
TEST : VOLATILE ORGANICS (EPA 624)
ATI I.D. : 80613002
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 661D HASSAYAMPA TRIP BLANK
SAMPLE MATRIX : AQUEOUS
DATE SAMPLED DATE RECEIVED DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
06/22/88 06/23/88 N/A 06/29/88 UG/L
1
COMPOUNDS RESULTS
CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM 1,2-DICHLOROETHANE 2-BUTANONE (MEK) 1,1,1-TRICHLOROETHANE CARBON TETRACHDDRIDE VINYL ACETATE BROMODICHLOROMETHANE 1,1,2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYLVINYLETHER BROMOFORM 2-HEXANONE (MBK) 4-METHYL-2-PENTANONE (MIBK) TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES
<10 <10 <1 <1 12 B <10 <1 <1 <1 <1 <1 <1 <10 <1 <1 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <5 <10 <10. <1 <1 <1 <1 <1 <1
y
SURROGATE PERCENT RECOVERIES
l,2-DICHLOROETHANE-D4 (%) BFB (%) T0LUENE-D8 (%)
y y
100 104 y 103
D INDICATES ANALYTE ALSO FOUND IN REAGENT DLANK,
CsX-^- ynuj--7uA
kit DAIH: :50S1302 «1 Qiili=LiiLJS:3o:00 CALl: S0bl302 #2 SAMPLE: .iOF A0K!:-:0-2 TRIP BLANK 5ML CONDS. :_iLL-RANGE: G 1.1200 LPBEL: N O- 4.0 QU-r*: n 0- :.0 J
lyO. 0 1
^CANS 1 TO 1200
•J r-H-.c: • • 1 ,
118312,
\
RIC
:r c: CJ L i -
pv.
• - >
u X cr, — ":» >— ^
I )
(—
V
O Oi V
-0
1—
< Q U I Ul
'_,' W . 4
L
64
203
161,1
500
IJ\-.'J 531 ,^
301
U —-O'/;K _J L.^JlZ2..J033
V. JOU 6:40
4v30 13:20
t.yu •'0:00 - - . c . I \',
^ i Z - . •^ V
1 OOG 33:20
1209 SCAN 40:08 TIME
PROCEDURE DATA FILE REFERENCE NAME LIST
REPORT
TCA 8061302 8061302 VQN INITIALIZATION VQSTDS
DIAGNOSTIC REPORT 6/29/88 19;18;48
OPTION: 2 PROCESSING OPTION: 3
: STANDARDS — PROC USED POSS
6 6 1 6 6 1 6 6 1
X PLUS UNKNOWNS RMS PROC USED POSS 57 18 7 1 57 18 6 1 57 18 6 1
-— >< - LIST NAMES - Z RMS STANDARD/UNKNOWN 52 VQSTDS/VQl 57 VQSTDS/VQ2 57 VQSTDS/VQ3
COMPOUNDS PROCESSED, 7 FOUND
COMPOUND > NO LIB ENTRY 1 VQ 1 2 VQ 2 3 VQ 3 4 VQ - 4 5 VQ 5 6 VQ 6 7 VQ 7 8 VQ 8 9 VQ 9 10 VQ 10 11 VQ 11 12 VQ 12 13 VQ 13 14 VQ 14 15 VQ 15 16 VQ 16 17 VQ 17 18 VQ 18 19 VQ 19 20 VQ 20 21 VQ 21 22 VQ 22 23 VQ 23 24 VQ 24 25 VQ 25 26 VQ 26 27 VQ 27 28 VQ 28 29 VQ 29 30 VQ 30 31 VQ 31 32 VQ 32 33 VQ 33 34 VQ 34 35 VQ 35 36 VQ 36 37 VQ 37 38 VQ 38 39 VQ 39 40 VQ 40 41 VQ 41 42 VQ 42
REF -300 -608 -758 -382 -721 -902 -54 -85
-107 -137 -203 -222 -252 -286 -326 -346 -363 -385 -382 -424 -436 -438 -450 -686 -491 -499 -515 -534 -537 -531 -537 -570 -616 -631 -678 -687 -727 -762 -824 -947 -987 -956
PRED 300 608 758 382 721 902 54 85 107 137 203 222 252 286 326 346 363 385 382 424 436 438 450 686 491 499 515 534 537 531 537 570 616 631 678 687 727 762 824 947 987 956
— SEARCH >< SAT >< SEL DELTA PEAKS FIT PEAKS M/Z 300 608 758 381 -1 721 901 -1
203
I 97 i I 92; I 99; I 99E I 99-I 97
1 99"
3 . 1 2 8 3 114 ^ 117 3 65 7 98 I 95
50 94 62 64
7 B4 43 76 96 63 96 83 62 72 97 117 43 83 83 63 75 130 129-97 78 75 63 173 173 43 164 92 112 106 104 106 106
CHRO TOP DELTA PEAKS 299 -] 608 758 381 721 902
203 221
53 1
/
L 1
I 1
1 1
1
Quantitation Report File; 8061302
Data; 8061302. TI 06/29/88 18:38:00
mple: JOB 806130-2 -nds. ; GC4
Formula: Submitted by;
TRIP BLANK SML
Instrument; 1050 Analyst: MGB
Weight; Acct, No,
0. 004
AMOUNT=AREA * REF AMNT/(REF AREA » RESP FACT) Resp, fac. from Library Entry
No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 3
19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42
Name ISl IS2 IS3 SSI SS2 SS3 45V 46V 88V 16V 44V 13H 15H 29V 13V 30V 23V IOV 14H IIV 6V 19H 48V 15V 32V 33VT 87V 51V 14V 4V
33VC 19V 47V
BROMOCHLOROMETHANE 1, 4-DIFLUOROBENZENE CHL0R0BENZENE-D5 DICHL0R0ETNANE-D4 TOLUENE-DS BROMOFLUOROBENZENE CHLOROMETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1-DICHLOROETHENE 1.1-DICHLOROETHANE TRANS-1,2-DICHLOROETHENE CHLOROFORM 1,2-DICHLOROETHANE 2-BUTAANONE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE 1.1.2,2-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1, 3-DICHLOROPROPANE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,S-DICHLOROPROPENE 2-CHLOROETHYL VINYL ETHER BROMOFORM
4-METHYL-2-PENTAN0NE 16H 85V a6V 7V
38V 18H 20H
2-HEXANONE TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYLBENZENE STYRENE TOTAL XYLENES
XYLENES
A ^ -
No m / z S c a n T i m e R e f RRT M e t h A r e a ( H g h t ) A m o u n t / . T o t 1 128 299 9:58 1 1.000 A BB 46021, 50.000 UG/L 10,46 2 114 608 20 :16 2 1.000 A BB 224472 50.000 UG/L 10.46 1 117 758 25:16 3 1.000 A BB 152827, 50.000 UG/L 10,46 4 65 381 12:42 1 1.274 A BB 87586. 100.044 '/. 20 .92 , 5 98 721 24:02 3 0.951 A BB 215238. 103.098 7. 2 1 . 5 6 ^ 6 95 902 30:04 3 1.190 A BB 119282. 104.440 /. 2 i . Q A y 7 NOT FOUND 8 NOT FOUND 9 NOT FOUND
10 NOT FOUND 11 84 203 6:46 1 0,679 A BB 17783, 12.002 UG/L 2.51 12 43 221 7:22 1 0,739 A BB 3252, 8.568 UG/L 1 79 13 NOT FOUND 14 NOT FOUND 15 NOT FOUND 16 NOT FOUND 17 NOT FOUND 18 NOT FOUND 19 NOT FOUND 20 NOT FOUND 21 NOT FOUND 22 NOT FOUND 23 NOT FOUND 24 NOT FOUND 25 NOT FOUND 26 NOT FOUND 27 NOT FOUND ''8 NOT FOUND ? NOT FOUND
30 78 531 17:42 2 0.873 A QB 476. 0.120 UG/L 0.03/,.. 31 NOT FOUND 32 NOT FOUND 33 NOT FOUND 34 NOT FOUND 35 NOT FOUND 36 NOT FOUND 37 NOT FOUND 38 NOT FOUND 39 NOT FOUND 40 NOT FOUND 41 NOT FOUND 42 NOT FOUND
.,Z
7 ^ AnalyticalTechnologies, Inc
GCMS - RESULTS
REAGENT BLANK
TEST : SEMI-VOLATILE ORGANICS (EPA 625)
CLIENT : MONTGOMERY & ASSOCIATES PROJECT # : 661D PROJECT NAME : HASSAYAMPA CLIENT I.D. : REAGENT BLANK
Th/u-'AUA
ATI I.D. DATE EXTRACTED DATE ANALYZED UNITS DILUTION FACTOR
806130 06/29/88 08/01/88 UG/L N/A
COMPOUNDS RESULTS
N-NITROSODIMETHYLAMINE PHENOL ANILINE BIS(2-CHLOROETHYL)ETHER 2-CHLOROPHENOL 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE BENZYL ALCOHOL 1,2-DICHLOROBENZENE 2-METHYLPHENOL BIS(2-CHLOROISOPROPYL)ETHER 4-METHYLPHENOL N-NITROSO-DI-N-PROPYLAMINE HEXACHLOROETHANE NITROBENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BIS(2-CHLOROETHOXY)METHANE 2,4-DICHLOROPHENOL 1,2,4-TRICHLOROBENZENE NAPHTHALENE 4-CHLOROANILINE HEXACHLOROBUTADIENE 4-CHLORO-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CH LORONAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE ACENAPHTHENE 2,4-DINITROPHENOL 4-NITROPHENOL DIBENZOFURAN 2,4-DINITROTOLUENE 2,6-DINITROTOLUENE DIETHY LPHTHALATE 4-CHLOROPHENYL-PHENYLETHER
<10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <50 <10 <50 <10 <10 <50 <10 <50 <50 <10 <10 <10 <10 <10
(CONTINUED NEXT PAGE)
/ \ AnalyticalTechnologies, Inc GCMS - RESULTS
REAGENT BLANK ATI I.D.
'- 77UA''7/ A^
806130
TEST : SEMI-VOLATILE ORGANICS (EPA 625)
COMPOUNDS RESULTS
FLUORENE 4-NITROANILINE 4,6-DINITRO-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL-PHENYLETHER HEXACHLOROBENZENE PENTACHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE BENZIDINE PYRENE BUTYLBENZYLPHTHALATE 3,3'-DICHLOROBENZIDINE BENZO(a)ANTHRACENE BIS(2-ETHYLHEXYL)PHTHALATE CHRYSENE DI-N-ETHYLPHTHALATE BENZO(b)FLUORANTHENE BENZO(k)FLUORANTHENE BENZO(a)PYRENE INDENO(1,2,3-cd)PYRENE DIBENZO(a,h)ANTHRACENE BENZO(g,h,i)PERYLENE
<10 <50 <50 <10 <10 <10 <50 <10 <10 10 <10 <100 <10 <10 <20 <10 TR <10 <10 <10 <10 <10 <10 <10 <10
SURROGATE PERCENT RECOVERIES
NITR0BENZENE-D5 (%) 2-FLUOROBIPHENYL (%) TERPHENYL (%) PHEN0L-D5 (%) 2-FLUOROPHENOL (%) 2,4,6-TRIBROMOPHENOL (%)
77 84 82 85 98 108
^M b^^
RIC 08/01/88 0:25:00 , . ^ A SAiiPi:Er"^o^/:n5'^ \7/7kl CO»DS.! IUL lL->2XiriL RANGE: G 1,2600 LABEL: N 0,
'S07s\ 3o
An/jJ-^u/ i DATA: 88I13B2495 #2213 SCANS 300 TO 2600 CALI: 88M3B2495 «2
4.0 QUAN: A 0, 1.0 J 0 BASE: U 20, 3
100.0-1 162048.
RIC
L^N^ jLk.
1000 r-1500 7^'.m
"• I'' \ J-. .<•»»«'
I 2000 33:20
— I 2500 41:40
SCAN TIME
PROCEDURE DATA FILE REFERENCE NAME LIST
REPORT
y r^^-
<. — — — PROC
2 2 2 2 2
. 2 2 2 1
TCA 88M3B2495 aaM3B2493
DIAGNOSTIC
> f^/ff '1 Kl INITIALIZATION XI
a 1 n i -*uryr^ua USED POSS
2 1 2 1 2 1 2 1 2 1 2 1 2 1 2 1 4 0
^ . M V,rf^
— ^% RMS
0 0 0 0 0 0 0 0 0
r \
C^aj OPTION:
1 if^ 1 ikii
REPORT 8/0
2 PROCESSING OPTION: 3
— P L w a ui''(rM'<ij¥iii' a PROC
11 9 9 9 12 12 11 10 7
USED 2 4 2 3 2 4 3 4 0
POSS I 3 1 2 1 1 1 1 1
_ ^ ^ V >- 1 T C ^ klAhtf^f? _ — >>v. — uxai •''"nc.a — RMS
0 838
0 230
0 317 182 243
0
STANDARD/UNKNOWN Xl/Zl Xl/ZA X2/Z2 X2/ZB X3/Z3 X3/ZC X4/Z4 XS/Z3 X6/Z6
1:09: 29
ao COMPOUNDS PROCESSED. 14 FOUND
< COMPOUND >< NO LIB ENTRY REF 1 SV 1 -644 2 SV 2 -866 3 SV 14 -239 4 SV 13 -613 3 SV 16 -600 6 SV 17 -617 7 SV 18 -613 8 SV 19 -637 9 SV 20 -647 10 SV 21 -680 11 SV 22 -677 12 SV 7 -611 13 SV 8 -449 14 SV 23 -710 15 SV 24 -710 16 SV 25 -737 17 SV 26 -734 18 SV 27 -729 19 SV 3 -1189 20 SV 28 -748 21 SV 29 -793 22 SV 30 -303 23 SV 31 -828 24 SV 32 -867 25 SV 33 -343 26 SV 34 -849 27 SV 9 -743 28 SV 33 -361 29 SV 36 -869 30 SV 37 -902 31 SV 38 -910 32 SV 39 -988 33 SV 40 -996 34 SV 4 -1461 35 SV 41 -1041 36 SV 42 -1037 37 SV 43 -1063 38 SV 44 -1083 39 SV 45 -1114 40 SV 46 -1164 41 SV 47 -1158 42 SV 48 -1114 43 SV 49 -1195
PRED 641 863 236 610 397 614 612 634 644 677 674 617 462 713 713 739 736 731 1186 743 790 802 823 864 840 846 743 860 868 901 909 986 994 1439 1037 1034 1060 lOBO llll 1161 1133 llll 1192
— SEARCH X SAT >< SEL DELTA PEAKS FIT PEAKS M/Z 641 863
626 9 461 -1
1186
746 1
1439
I 988 I 913
1 996 3 932
, , . .
1 996
, , . , .
2 987 , , . , .
, , 1 941 , ,
,
.
, ,
132 136 42 94 93 93 128 146 146 108 146 99 112 108 43 108 70 117 164 77 82 139 122 122 93 162 82 180 128 127 223 107 142 188 237 196 196 162 63 163 132 138 153
CHRO TOP DELTA PEAKS 641 1 863 1
• • >
624 -2 1 461 1
• • • • • • • • •
• .
1186 1 • • • • •
• B •
• • • • • • • * • • • • • >
746 1 •
• • • • - . • • .
• • • .
• • 1460 1 1
• •
• •
• .
•
. • *
.
V4 \-5' \ 6 \ 7 \Q \ 9 30 51 52 53 54 55 56 57 58 59 60 61 62 63 64 65 66 67 68 69 70 71 72 73 74 75 76 77 78 79 80
SV SV SV SV SV SV SV SV SV SV SV SV SV SV
sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv sv
50 -1210 10 -1073 11 -1337 51 -1235 52 -1225 53 -1241 54 -1171 35 -1299 36 -1298 57 -1289 58 -1310 5 -1962
59 -1315 60 -1323 61 -1387 62 -1407 63 -1444 64 -1465 65 -1474 66 -1609 67 -1689 6 -2211 12 -1776 68 -1776 69 -1728 70 -1887 71 -1967 72 -1959 73 -2010 74 -1967 75 -2121 76 -2151 77 -2155 78 -2202 79 -2393 80 -2401 81 -2443
1207 1072 1336 1234 1224 1240 1170 1298 1297 1268 1309 1961 1312 1320 1384 1404 1441 1462 1471 1606 1687 2213 1773 1773 1725 1885 1966 1957 2009 1966 2121 2151 2155 2202 2393 2401 2443
.
1072 1340 ^
1961
1605 ,
2213 1774
, , , .
2006 .
, , , , , .
1 996 \ 1 973
• •
< . •
•
1 919
. ,
, , , , , , ,
1 1 993 ,
1 930 1 1 983
,
t • •
, , ,
, . •
3 1 990 .
• • •
• • • • •
• •
> • •
184 172 330 139 168 89 165 149 204 166 138 240 198 169 248 284 266 178 178 149 202 264 244 184 202 149 252 228 149 228 149 252 232 232 276 278 276
1072 1339 -]
. , ,
, ,
, , , , ,
1961 , , , , , , ,
1605 ,
2213 1774
, , , . .
2006 , , , , , , , ,
.
1 L 1
1
1 ,
1 1
1
•
l u a n t i t a t i o n R e p a r t File: 88M3B2493
l a t a : a0M3B2495. TI ) 8 / 0 1 / a 8 0 : 2 5 : 0 0 ^ ^ Jatnple: ^ T - l ^ ^ - f C A 6 J ;onds. : IUL 1L->2X1ML i t a n d a r d ID: 2-BNA-7-1A J e n s i t i v i t y ID: 2491
I n s t r u i n e n t : 5100 A n a l y s t : RJT I n s t C a l i :
>MOUNT=AREA • REF AMNT/(REF AREA • RESP FACT) Jesp. f a c . f rom L i b r a r y E n t r y NO 1 2 3 4 3 6 7. 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24
No 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24
NAME ISl IS2 I S3 IS4 ISS IS6 SS2 SSI SS3 SS4 SSS SS6 688 66B
1. 4-DICHL0R0BENZENE-D4 NAPHTHALENE--D8 (SV#2) ACENAPHTHENE-DIC PHENANTHRENE-DIC
(SV#1)
\ (SV#3) > (SV#4)
CHRYSENE-D12 (SV#3) PERYLENE-D12 (SV#6> PHENOL-DS (SV#73 1
2-FLUaROPHENaL (SV#8) NITROBENZENE-DS (SV#9) /
2-FLUOROBIPHENYL (SV#10) 2.4. 6-TRIBROMOPHENOL (SV#11) TERPHENYL-D14 (SV#12) DI-N -BUTYL PHTHALATE (SV#66) BIS(2-ETHYLHeXYL)PHTHALATE (SV#73)
CYCLOHEXENE UNKNOWN PHENOL, 2-UNKNOWN D4-1
FLUORO-
.4-DICHLOROBENZENE (INT. D8-NAPHTHALENE (INT. STD. ) DIO-DIO-D12-D12-
m/z 152 136 164 188 240 264 99 112 82 172 330 244 149 149 RIC RIC RIC RIC RIC RIC RIC RIC RIC RIC
ACENAPTHENE (INT. STD. ) PHENANTHRENE ' CHRYSENE (INT. PERYLENE (INT.
Scan 641 863 1186 1460 1961 2213 624 461 746 1072 1339 1774 1605 2006 174 393 446 2169 641 863 1186 1460 1961 2213
Time 10:41 14:23 19:46 24: 20 32:41 36: S3 10:24 7:41 12:26 17: 32 22: 19 29: 34 26:43 33:26 2: 54 6: 33 7: 26
36:09 10: 41 14: 23 19: 46 24: 20 32:41 36; 53
(INT. STD. STD.
Ref
d) 3 4 3 6 1
^ 3 3 5 4 5
22 22 22 22 19 20 21 22 23 24
STD. ) ) )
RRT 1. 000 1. 000 1. 000 1, OOO 1. 000 1. 000 0.973 0.719 0. 864 0. 904 1. 129 0. 903 1.099 1. 023 0. 119 0. 269 0, 303 1, 486 1. 000 1. 000 1. 000 1. 000 1. 000 1. 000
STD. )
M« A A A A A A A A A A A A A A A A A A A A A A A A
• th BB BB BB BB BB BB BV VB BB BB BB BB BB BB BB BB BB BB VB BB BV BB BB BB
A r e a ( H g h t ) 29659. 124200. _ '97338. 202101. 149890. 116543. 10530. 2186.
33123^
mos4. 16661.
147977. 29849. 14489.
293242. 32632. 36352. 7761.
204303. 246476. 412322. 513708. 433213. 330115.
Ainount 40. 40. 40. 40. 40. 40. 14. 6.
39. 31. 33. 31. 3. 4.
000 000 000 000 000 000 122 564 761 175 880 662 178 114
NG/UL NG/UL NG/UL NG/UL NG/UL NG/UL NO/UL NO/UL NG/UL NO/UL NO/UL NO/UL NO/UL NO/UL
36. 962^ 6. 7. 1.
40. 40. 40. 40. 40. 40.
328 049 505 000 000 000 000 000 000
UO/L UO/L UG/L UG/L UO/L UG/L
7.Tot 4. 4. 4. 4. 4. 4. 1. 0. 4. 5. 6. 6. 0. 0. 6. 0. 0. 0. 4. 4. 4. 4. 4. 4.
66 66 66 66 66 66 64 76 63 96 27 01 60 48 62 74 82 18 66 66 66 66 66 66
A / j , ! ^ AnalyticalTechnologies, Inc
GAS CHROMATOGRAPHY - RESULTS
REAGENT BLANK
TEST : ORGANOCHLORINE PESTICIDES AND PCB'S (EPA 608)
777 TJ-777 7
CLIENT PROJECT # PROJECT NAME CLIENT I.D.
MONTGOMERY & ASSOCIATES 661D HASSAYAMPA REAGENT BLANK
ATI I.D. : DATE EXTRACTED : DATE ANALYZED UNITS DILUTION FACTOR
806130 06/30/88 07/13/88 UG/L
: N/A
COMPOUNDS RESULTS
ALDRIN ALPHA BHC BETA BHC GAMMA BHC (LINDANE) DELTA BHC CHLORDANE 4,4'-DDD 4,4'-DDE 4,4'-DDT DIELDRIN ENDOSULFAN I ENDOSULFAN II ENDOSULFAN SULFATE ENDRIN JNDRIN ALDEHYDE HEPTACHLOR HEPTACHLOR EPOXIDE METHOXYCHLOR TOXAPHENE AROCLOR 1016 AROCLOR 1221 AROCLOR 1232 AROCLOR 124 2 AROCLOR 1248 AROCLOR 1254 AROCLOR 1260
< 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 0 5 < 0 . 5 < 0 . 1 < 0 . 1 < 0 . 1 < 0 . 1 < 0 . 0 5 < 0 . 1 < 0 . 1 < 0 . 1 < 0 . 1 < 0 . 0 5 < 0 . 0 5 < 0 . 5 < 1 . 0 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5 < 0 . 5 < 1 . 0 < 1 . 0
SURROGATE PERCENT RECOVERIES
ISODRIN % 99
DE':: "CCitlF I RMATORY COLUMN
CHART SPEED 0.6 CM/MIN ATTEN: 16 ZERO: 10% 1 MIN/TICK
-STAT~T INJECT
0. 903
'2.171 2.627
= ^ ^ ^
~^R:OFF
3.474
8. 890 -A BHCT 9.66 1
, B BKec. 1 1 . 258 11.694
ATTEN: 32 ZERO: 5% 1 MIN/TICK
'- - R E P I ^ P X M . 9 4 4 ^ 1 5 . 4 8 3
' ENDe-Zl 1 6 . 0 7 0 -DDE:^ 16.858
17.721 , 18.214
^ _IiDD=} 18. 686
! _D.DT—i^ 19.607 ' END0-B04 20.306
' METHej«;Y 22.401 )
~" 24.285 24.922
— —I 25.802
^ - ^ . 2 1 2
=• 14.539
TITLE: P E S T I C I D E S - ^ ^ ^ G./50
CHANNEL NO: 2 SAMPLE: 9
20:21 13 JUL 88
METHOD: DB608
>\^^J-*1UA
TITLE
CHANh
PEAK NO
1 2 3 4 5 6 7 8 9 10 1 1 12 13 14 15 16 17 18 19 20 1 2
23 24 25 26 27 28 29
: PESTICIDES
EL NO: 2
PEAK NAME
A BHC LINDANE B BHC
HEPTACHLO D-BHC
ALDRIN ISODRIN HEPT EPX
ENDO I DDE DIELDRIN
ENDRIN DDD ENDO I I DDT ENDRIN AL ENDO S04 METHOXY END KETON
TOTALS:
g / < ^ Use
SAMPLE: 9
RESULT UG/ML 0 . 0000 0.0000 0.0017 0.0022 0.001 1 0,0000 0.0012 0,0019 0 . 0000 0.0000 0.0029 /
98.8270 "• 0.0026 0.0000 0.00 1 0 0,0014 0.0018 0,0000 0,0000 0,0030 0,0006 0,00 1 0 0,0017 0,0021 0,0015 0,0061 0,0020 0,0000 0,0000
98,8628
TIME CMIN) 7,835 8. 185 9.661 10.992 1 1 ,258 1 1 .694 12.029 12.471 12,899 13.123 13.196 14.539 14.944 15.483 16.070 16.858 17.068 17.721 18.136 18.214 18.686 18.864 19.607 19.910 20.306 22.401 22.699 24.285 24.922
20:
METHOD
TIME OFFSET
-0,069 -0,068 -0,062
-0,071 -0,069
0.016 -0,121 -0,096
-0,090 -0,082 -0,082
-0,106 -0,064 -0,056 -0.083 -0.080 -0.064 -0.079 -0,091
-1,417
21 13
: DB608
AREA COUNTS
686 808
3340 4130 1770 5290 1968 3505 1755 5325 5251
349212 3808 3887 1512 2053 2657 3156 2444 1406 668 1372 1790 2746 2226 1406 2968 574
9106
426819
JUL 88
SEP CODE BV VB BB BV VV VV VB BB BV VV VB BV VV VV VB BV VB BV VV VV VV VB BV VV VB BV VB BV VB
&'*
?
? ?
?
? ? ? ? ?
? ?
Wl/2 CSEC) 7,65 6,10 6,75 7.05 6, 45 7.65 7.35 6,05 7,20 10,40 2.65 7,80
10, 15 9,70 7, 00 7,55 7. 80 8. 60
13, 60
14. 00 9, 90 7, 90 8, 10 1 1 .20 6.70 7.55 13.60 41 ,65
DETECTED PKS: 55 REJECTED PKS: 26
DIVISOR: 1,00000 MULTIPLIER: 1,00000
NOISE: 8.5 OFFSET: 19
RACK: 16 VIAL: 1 INJ: 1
NOTES: DB608 PRIMARY COLUMN
TITLE: PESTICIDE CONFIRMATORY
CHANNEL NO: 1 SAMPLE: SAME
PEAK PEAK NO NAME
RESULT UG/ML
20:21 13 JUL 88
METHOD: DBS
TIME CMIN)
TIME OFFSET
AREA COUNTS
SEP CODE
Wl/2 CSEC)
TITLE : PESTICIDE
CHANNEL NO: 1
PEAK NO
1
2 3 4 5 6 7 8
PEAK NAME
LINDANE D-BHC
ALDRIN
TOTALS:
CONFIRMATORY
SAMPLE:
RESULT UG/ML J _ Q-yc i i ^
1 .7247 2.5303 2.0686 1.8830 3.4014 3.4640
82.9491
100.0000
SAME
TIME CMIN) O .ttr 1
10,659 1 1 ,356 12.094 12,720 13.109 14,075 14,999
20:
METHOD
TIME OFFSET
0.116 0, 174
-0.225
0,065
21 13
: DBS
AREA COUNTS
7175 6253 9174 7500 6827 12332 12559
300741
362561
JUL 88
SEP CODE BS BB BB BB BV VB BB BB
Wl/2 CSEC) 6. 25 5,65 6,80 7,35
? 6,05 6.75 7.50 9,80
REJECTED PKS; DETECTED PKS: 26
MULTIPLIER: 1,00000
NOISE: 71.6 OFFSET: -20
RACK: 16 VIAL: 1 INJ: 1
NOTES: DBS CONFIRMATORY COLUMN
18
CHART SPEED 0,6 CM/MIN (ATTEN: 16 ZERO: \e% 1 MIN/TICK
-STAT" INJECT
==?^ ^7.'\^7 -zAzz---'-= C : 3.697 ^ ^ ^ . - A . 266
— -—1^ 4,938 __ =? 5,5-;7i SR:OFF
7. 845
DAhfE 1 1 . 004 11.717
1 14
ezzB. ALDR^M" 13.
" — ' — L 4 ,
0,918
ATTEN: 32 ZERO: 5% 1 MIN/TICK
_ISODR:
' 1 5 , 4 8 8 PENDe-Zl 1 5 . 9 2 2
" 1 4 , 5 5 2 .
~ S R : O K T '
r
3 . 2 2 5
1 5 . 0 0 9