Ltr: Discusses & transmits groundwater sampling rpt analytical … · 2016-12-20 · NEL LABORATORIES Reno • Las Vegas Phoenix • Burbank Las Vegas Division 4208 Arcata Way, Suite

SDMSDocIO 2027755

NEL LABORATORIESReno • Las VegasPhoenix • Burbank

Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, NV 89030

(702) 657-1010 • Fax: (702) 657-15771-888-368-3282

RSSN

RSSN7900 Vegas Valley DriveLas Vegas, NV 89142

TEL: 702-431-3020

RE Project: DI-WATER

Dear RSSN:

2027755

Order No.: L0204408

NEL Laboratories, Las Vegas received 2 samples on 4/26/02 for the analyses presented in thefollowing report.

There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.

If you have any questions regarding these tests results, please feel free to call.

— ̂ NJ U^v"'yxrervvyfcW{/xXX.Stan Van W^genen / " ALaboratory Manager

Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers

S*->o*^

RenoAZ05201707CertifiedCertifiedNV033Certified

Las VegasAZ05182002CertifiedCertifiedNV052CertifiedCertified

Date

Corporate Office & Reno Division • 1030 Matley Lane • Reno, NV 89502 • (702) 348-2522

NEL LABORATORIES

NEL Laboratories, Las Vegas Date: 06-May-02

CLIENT: RSSNProject: DI-WATERLab Order: L0204408

CASE NARRATIVE

Attached are the analytical results for samples in support of the above referenced project.

The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.

Analytical Comments:

EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Niether of these two compounds were present in the samples submitted in this work-order at or above5ppb.

Page 1 of 1

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DI- WATER

PROJECT #: DI-WATER

MATRIX: AQUEOUS

ParameterAcetone

Benzene

Bromobenzene

Bromochloromethane

Bromodichloromethane

Bromoform

Biomome thane

2-Butanone

n-Butylbenzene

sec-Butylben/ene

teit-Butylbenzeiu

Carbon disulfide

Carbon tetiachlonde

Chlorobenzene

Chloroethane

2-Chloroethyl vinyl ethei

Chloroform

Chloromethane

2-Chlorotoluene

4-Chloiotoluene

Dibromochloiomcthane

1 ,2-Dibiomo-3-chloi opi opane1 ,2-Dibroinoethane

Dibiomonie thane

1 ,2-Dichlorobeiuene

1 ,3-Dichlorobenzene

1 ,4-Diehlorobenzene

Dichlorodifluoiomethane

1,1-Dichloroetliane

1,2-Dichloroethane

1,1-Dichloroethene

cis-1 2-Dichloioelhene

tians-l,2-Dich!oioethene1,2-Dichloropropane

1 ,3-Dichloropropane


1 , 1 -Dichloropi opene

cis-l,3-Dichloropiopene

trans-1 ,3-Dichloropropcne

Fthylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

isopiopylberuene

ND - Not Detected at the Repoiting

DP - Dilution Factoi

Date: 06-May-02

Result Unit

ND ug/L

ND ug/L

ND ug/LND ug/LND ug/LND ug/L

ND ug/L

ND ug/LND ug/L

ND ug/LN D Hg/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND |ig/LND HS/LND ug/LND ug/LND ug/LND ug/L

ND ug/LND ug/LND ug/L

ND ug/LND ug/LND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/LND ug/L

ND ug/LND ug/L

ND ug/L

ND ug/LND ug/LND ug/LND ug/LND Hg/LND ug/L

Limit

ReportingLimit

255050505050

5025

505050505050505050

5050505 0

50505050505050505050505050505050

50

505050255050

B - Analyte detected

CLIENT ID: DI- Water

DATE SAMPLED: 4/26/02

NEL SAMPLE ID: L0204408-001A

DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

m the associated Method Blank

Analyzed

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM LVDRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

S - Spike Recovery outside accepted recovery limits

E - Value above quantitation range Page 1 of 4

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DI-WATER

PROJECT #: DI-WATER

MATRIX: AQUEOUS

Parameterp-[sopropyltoluene

Methylene chloride4-Methyl-2-penUnone

MTBENaphthalene

n-PropylbenzeneStyrene1 , 1 , 1 ,2-Tcti achloroethane1 , 1 ,2,2-Teti achloi oethaneTeti achloi oethene

Toluene1 ,2,3-Tnchlorobenzene1 ,2,4-Tnchlorobenzene

1,1,1-Tnchlorocthane1,1,2-TnchloroethaneTi ichloroetheneTiichlorofluoromethane

1 ,2,3-Tnchloropropane

1 ,2,4-Tnmethylbenzene1 ,3,5-TrmiethylbenzeneVinyl acetateVinyl chloride

o-Xylenem,p-Xylene

Total THMSurr: Dibromofluoromcthanc

Surr:Tolucne-d8Surr: 4-Bromolluorobcnzcnc

Result

ND

NDND

ND

NDND

NDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDND

NDND95.3108

92.7

Unit

ug/L

ug/Lug/Lug/L

ug/Lug/L

ug/Lug/Lug/L

ug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/Lug/L

ug/L

ug/Lug/Lug/Lug/Lug/Lug/L

%REC%REC

%REC

ReportingLimit

505025

50

50505050

5050

505050

505050

5050

505050505010

50926-108957-112853-104

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ID:

DF1lllllllllllll1llllll1llIlll

Method

SW8260BSW8260BSW8260BSW8260B

SW8260BSW8260BSW8260BSW8260B

SW8260BSW8260B

SW8260BSW8260BSW8260BSW8260BSW8260BSW8260B

SW8260BSW8260B

SW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260B

SW8260BSW8260B

SW8260B

DI-Water

4/26/02

L0204408-001A

Prep Date Analyzed

04/26/0204/26/02

04/26/0204/26/02

04/26/0204/26/0204/26/0204/26/02

04/26/0204/26/0204/26/0204/26/0204/26/0204/26/0204/26/02

04/26/0204/26/0204/26/02

04/26/0204/26/0204/26/02

04/26/0204/26/0204/26/0204/26/0204/26/0204/26/02

04/26/02

Analyst

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LVDRM-LV

DRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LV

DRM-LVDRM-LV

DRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LV

DRM-LVDRM-LV

ND - Not Detected at the Repoiting Limit

DF - Dilution Factor

Date: 06-May-02

B - Analyte detected m the associated Method Blank


E - Value above quantitation range Page 2 of4

NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DI-WATERPROJECT #: DI-WATER

MATRIX: AQUEOUS

ParameterTotal Dissolved Solids

Chloride

Nitiate, a sN

Nitnte, as N

Sulfate

Alkal ini ty, Bicarbonate (As CaCO3)

Alkal ini ty , Caibonate (As CaC03)

Hydroxide (As CaCO3)

Alkal ini ty , Total (As CaCO3)

SulfideAmmonia, as N

Chemical Oxygen Demand

ResultNDNDNDNDNDNDNDNDNDNDNDND

Unitmg/Lmg/L

mg/L

mg/L

mg/Lmg/Lmg/Lmg/L

mg/Lmg/Lmg/L

mg/L

ReportingLimit

1500 10

0100 10

0 10

252525

250030

030

10

CLIENT ID: Dl-WaterDATE SAMPLED: 4/26/02

NEL SAMPLE ID: L0204408-001B

DF Method Prep Date

1 SM2540 C

1 EPA 300 0

1 EPA 300 0

1 EPA 300 0

1 EPA 300 0

1 SM2320 B

SM2320 B

SM2320 B

SM2320 B

SM4500-S D

SM4500-NH3 C

SM5520 D

Analyzed04/26/02

04/26/02

04/26/02

04/26/02

04/26/02

04/29/02

04/29/02

04/29/02

04/29/02

05/03/02

04/30/02

04/29/02

AnalystCRA-LV

PJJ-LV

PJJ-LV

PJJ-LV

PJJ-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RWW-LV

RDA-LV

RDA-LV

ND - Not Deteued at the Repoitmg Limit


Date: 06-May-02

B - Analyte detected in the associated Method Blank


E - Value above quantitation range Page 3 of 4

NEL LABORATORIESCLIENT: RSSN

PROJECT ID: DI-WATERPROJECT #: DI-WATER

MATRLX: AQUEOUS

ParameterAluminum

Antimony

Arsenic

Barium

Beryllium

Cadmium

Calcium

Chromium

Cobalt

Copper

lion

Lead

Magnesium

Manganese

Mercury

Nickel

Potassium

Selenium

Silver

Sodium

Thallium

Vanadium

Zinc

ResultNDNDNDNDND

ND

ND

0.0010

ND

0.0012

ND

ND

ND

ND

ND

NDNDNDNDND

ND

ND

0.015

Unitmg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0050

00010

00010

00050

00010

00010

020

00010

00010

00010

0 10

00010

02000010

0 00020

00010

20

00010

00010

050

0 00040

00050

00010

CLIENT ID:DATE SAMPLED:

NEL SAMPLE ID:

DF1lll1llllllllllll1lllll

MethodSW 6010B-Total

SW 6020-Total

SW 6020-Total

SW6010B-Total

SW 6020-Total

SW 6020-Total

SW6010B-Total

SW 6020-Total

SW 6020-Total

SW 6020-Total

SW6010B-Total

SW 6020-Total

SW6010B-Total

SW 6020-Total

SW 7470-Total

SW 6020-Total

SW 6010B-Total

SW 6020-Total

SW 6020-Total

SW6010B-Total

SW 6020-Total

SW6010B-Total

SW 6020-Total

DI-Water-FFM4/26/02

L0204408-002A

Prep Date05/01/02

04/30/02

04/30/02

05/01/02

04/30/02

04/30/02

05/01/02

04/30/02

04/30/02

04/30/02

05/01/02

04/30/02

05/01/02

04/30/02

04/30/02

04/30/02

05/01/02

04/30/02

04/30/02

05/01/02

04/30/02

05/01/02

04/30/02

Analyzed05/02/02

05/01/02

05/01/02

05/02/02

05/01/02

05/01/02

05/02/02

05/01/02

05/01/02

05/01/02

05/02/02

' 05/0 1/02

05/02/02

05/01/02

04/30/02

05/01/02

05/02/02

05/01/02

05/01/02

05/02/02

05/01/02

05/02/02

05/01/02

AnalystFIF-Reno

DHG-Reno

DHG-Reno

FIF-Reno

DHG-Reno

DHG-Reno

FIF-Reno

DHG-Reno

DHG-Reno

DHG-Reno

FIF-Reno

DHG-Reno

FIF-Reno

DHG-Reno

ADHG-Reno

FIF-Reno

DHG-Reno

DHG-Reno

FIF-Reno

DHG-Reno

FIF-Reno

DHG-Reno

ND - Not Delected at the Repoitmg Limit


Date: 06-May-02

B - Analyte detected m the associated Method Blank


E - Value above quantitation range Page 4 of4

BSK A N A L Y T I C A LL A B O R A T O R I E S AMENDED REPORT

Vanessa Padilla Certificate of AnalysisNEL Laboratories Las Vegas ELAP Certificate #11804208 Arcata Way, StC A Report Issue Date: 05/08/2002

Las Vegas, NV 89030

BSK Submission #: 2002041423BSK Sample ID #: 202467Project ID: L0204408 Project Desc: Dumpco

Submission Comments:Sample Type: Liquid Date Sampled: 04/26/2002Sample Description: DI Water 01 Time Sampled: 1015Sample Comments: Date Received: 04/27/2002

Inorganics Prep Analysis

Analyte Method Result Units PQL Dilution DLR Date PateTotal Organic Carbon (TOC) SM5310-D ND mg/L Q.2 1 0.2 05/07/200205/07/2002

mg/L: Milligrams/Liter (ppm) PQL: Practical Quantitation Limit H: Analyzed outside of hold timemg/Kg: Milligrams/Kilogram (ppm) DLR: Detection Limit for Reporting P: Preliminary resultUg/L: Micrograms/Liter (ppb) : PQL x Dilution S: Suspect result. See Cover Letter for comments.ug/Kg: Micrograms/Kilogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory.%Rec: Percent Recovered (surrogates) See External Laboratory Report attachments.

Report Authentication Code: IIlllllI!ill!!IllllillllllHillII1IIIIIIIill!!HillIIIIIIIII! page j of ,

1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935

BSK A N A L Y T I C A LL A B O R A T O R I E S AMENDED REPORT

BSK Submission 2002041423

Client NEL Laboratories Las Vegas

Date Submitted 04/27/2002

Project ID L0204408Project Desc Dumpco

BSK StarLims Run #: 36194

Analyst Initials DONNAHAnalyte ResultsAnalyte

Dissolved Organic Carbon (DOC)





BSK StarLims Run #: 36613

Analyst Initials DONNAH

Analyte ResultsAnalyte

Total Organic Carbon (TOC)





1 Illlll II 11 ill Illl Illl Illl Instrument IDMethod Number

QCType

LCS

LCSD

MS

MS

MSD

MSD

RBLK

MatrixSpike ID

N/A

N/A

201118

201465

201118

201465

N/A

Result Units

1 03 mg/L

1 01 mg/L

23 87 mg/L

5 55 ,,ig/L

23 78 mg/L

549 mg/L

0 mg/L

% RecorRPD

103

101

110

99

110

98

< 0 2

SpikeRPD

2

037

1 2

SpkCone

1

1

10

2

10

2

DOCMatrix

Cone

ND

ND

12

36

12

36

UCL

130

130

130

130

130

130

02

LCL

70

70

70

70

70

70

N/A

Date

04/29/02

04/29/02

04/29/02

05/06 1>2

04/29/02

05/06/02

04/29/02

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

mm „ InstmmentID

Method Number

QCType

LCS

LCSD

MS

MSD

RBLK

MatrixSpike ID

N/A

N/A

202918

202918

N/A

Result Units

1 02 mg/L

1 01 mg/L

3 44 mg/L

346 mg/L

0 mg/L

% RecorRPD

102

101

104

104

SpikeRPD

099

058

SpkCone

1

1

2

2

TOCMatrix

Cone

ND

ND

13

13

< 0 2

Approved by £* ̂ (%&*'

UCL

130

130

130

130

02

tf^

LCL

70

70

70

70

N/A

Date

05/07/02

05/07/02

05/07/02

05/07/02

05/07/02

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

%Rec Percent Recovered

RPD Relative Percent Difference

UCL Upper Control Limit

LCL Lower Control Limit

Parent Sample Sample used as background matrix for MS/MSD

OOS-High QC Result Above UCL

OOS-Low QC Result Below LCL

Page 1 of 1

NEL LABORATORIES

HHHHIlL""

CLIENT: RSSNWork Order: L0204408Project: DI-WATER

Sample ID MB-R2950

Analyte

Chloride

Niti ate, as N

Nitrite, as N

Sulfate

Sample ID LCS-R2950

Analyte

Chlonde

Nitrate, as N

Niti ite, as N

Sulfate

Sample ID LCSD-R2950

Analyte

Chlonde

Nitrate, as N

Nitrite, as N

Sulfate

SampType MBLK

Batch ID R2950

Result

ND

ND

ND

ND

SampType LCS

Batch ID R2950

Result

1 981

0957

0995

2642

SampType LCSD

Batch ID R2950

Result

1 955

0964

0998

272

TestCode 300_W

TestNo E300

PQL SPK value

0100 10

010010

TestCode 300_W

TestNo E300

PQL SPK value

010 2

010 1

010 1

010 2 5

TestCode 300_W

TestNo E300

PQL SPK value

010 2010 1010 1

0 10 25

300_W

Units mg/L

SPKRefVal

Units mg/L

SPKRefVal

0

0

0

0

Units mg/L

SPKRefVal

0

0

0

0

ANALYTICAL QC SUMMARY REPORT

Test Method: EPA 300.0

Prep Date

Analysis Date 4/26/02

%REC LowLimit HighLimit RPD Ret Val

Prep Date


%REC LowLimit HighLimit RPDRefVal

99 80

957 80

995 80

106 80

Pi ep Date

Analysis Date

120 0

120 0

120 0

120 0

4/26/02

%REC LowLimit HighLimit RPD Ref Val

978 80

964 80

998 80

109 80

120 0

120 0

120 0

120 0

Run ID L_IC-1_020426A

SeqNo 22647

%RPD RPDLimit Qual


SeqNo 22646

%RPD RPDLimit Qual

00

0

0


SeqNo 22655

%RPD RPDLimit Qual

0

0

0

0

Qualifici s: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits

J - This concentration is considered an estimate due to LCS failure


Page 1 of30

Date: 17-May-02

CLIENT: RSSN

Work Order: L0204408

Project: DI-WATER 300 W


Test Method: EPA 300.0

Sample ID L0204369-001EMS

Analyte

Nitrate, as N

Nitrite, as N

Sample ID L0204242-001FMS

Analyte

Chloride

Sulfate

SampType MS

Batch ID R2950

Result

247

2807

SampType MS

Batch ID R2950

Result

176121

TestCode

TestNo

PQL

25

2 5

TestCode

TestNo

PQL

5050

300_W

E300

SPK value

25

25

300_W

E300

SPK value

5050

Units mg/L

SPKRefVal

00

Units mg/L

SPKRefVal

130

809

%REC

988112

%REC

92802

Prep Date


LowLimit HighLimit

80

80

Prep Date

Analysis Date

120

120

4/26/02

LowLimit HighLimit

80

80120

120

RPD Ref Val

0

0

RPD Ref Val

0

0

Run ID

SeqNo

L_IC-1_020426A

22656

%RPD RPDLimit

Run ID

SeqNo

00

L_IC-1_020426A

22657

%RPD RPDLimit

0

0

Qual

Qual

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recovery limits



Page 2 of 30

Date: J7-May-02

CLIENT: RSSN

Work Order: L0204408ANALYTICAL QC SUMMARY REPORT

Project: DI-WATER

Sample ID MB-873

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Manganese

Potassium

Sodium

Vanadium

Sample ID LCS-873

Analyte

Aluminum

Baiium

Calcium

Iron

Magnesium

Manganese

Potassium

Sodium

Vanadium

Sample ID L0204408-002A

Analyte

Aluminum

Barium

SampType MBLK

Batch ID R_873

Result

ND

ND

ND

ND

NDND

NDND

ND

SampType LCS

Batch ID R_873

Result

0952

0956

1906

09969

18804715

185719

02389

SampType MS

Batch ID R_873

Result

0955

09629

TestCode

TestNo

PQL

0050

00050

050010050

00050

20050

00050

TestCode

TestNo

PQL

0050

00050

050010050

00050

20050

00050

TestCode

TestNo

PQL

0050

00050

6010WJT

SW6010B

SPK value

6010WJT

SW6010B

SPK value

1

1

201

20

052020

025

6010W_T

SW6010B

SPK value

1

1

6010W_T

Units mg/L

SPKRefVal

Units mg/L

SPK Ret Val

0

0

0

0

0

0

000

Units mg/L

SPKRefVal

0

0

Test Method: SW 6010B-Total

%REC

%REC

952

956

953

997

94

943

928

95

956

%REC

955963

Prep Date

Analysis Date

5/1/02

5/2/02

LowLimit HighLimit RPD Ref Val

Prep Date

Analysis Date

5/1/02

5/2/02


85

85

85

85

85

85

85

85

85

Piep Date

Analysis Date

115 0

115 0

115 0

115 0

115 0

115 0

115 0

115 0

115 0

5/1/02

5/2/02


75

75

125 0

125 0

Run ID SUB-1895

SeqNo 24903

%RPD RPDLimit

Run ID SUB-1895

SeqNo 24902

%RPD RPDLimit

0

0

0

0

0

0

0

0

0

Run ID SUB-1895

SeqNo 24904

%RPD RPDLimit

0

0

Qual

Qual

Qual


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits

J - This concentration is considered an estimate due to LCS failuie


Page 3 of30

Date: ]7-May-02

CLIENT: RSSNWork Order: L0204408


Project: DI-WATER


Analyte

Calcium

lion

Magnesium

Manganese

Potassium

Sodium

Vanadium

Sample ID R0204325-002AMS

Analyte

Aluminum

Barium

Calcium

lion

Magnesium

Manganese

Potassium

Sodium

Vanadium


Analyte

Aluminum

Banum

Calcium

Iron

SampType MS

Batch ID R_873

Result

191509948

189604728

1891192

02394

SampType MS

Batch ID R_873

Result

0955

09629

191509948

189604728

1891

192

02394

SampType MSD

Batch ID R_873

Result

0951

09619

19 12

09883

TestCode

TestNo

PQL

0500 10

05000050

20050

00050

TestCode

TestNo

PQL

0050

00050

0500 10

05000050

20

050

00050

TestCode

TestNo

PQL

0050

00050

050

0 10

6010WJT

SW6010B

SPK value

201

20

052020

025

6010W_T

SW6010B

SPK value

11

201

20

05

20

20

025

6010WJT

SW6010B

SPK value

11

201

6010WJT

Units mg/L

SPK Ref Val

0

0

00000

Units mg/L

SPK Ref Val

0

0

00

0

0

0

00

Units mg/L

SPKRefVal

0000

Test Method: SW6010B-Total

%REC

958995948946946

96958

%REC

955963958995

948946

94696

958

%REC

951962956988

Prep Date

Analysis Date

5/1/02

5/2/02

LowLimit HighLimit

75

75

75

75

75

75

75

Piep Date

Analysis Date

125

125

125

125

125

125

125

5/1/02

5/2/02

LowLimit HighLimit

75

75

7575

7575

75

75

75

Prep Date

Analysis Date

125

125

125125

125

125

125

125

125

5/1/02

5/2/02

LowLimit HighLimit

RPD Ref Val

0

0

0

0

0

0

0

RPD Ref Val

0

0

0

0

0

0000

RPD Rel Val

0000

Run ID SUB-1895

SeqNo 24904

%RPD RPDLimit Qual

0

0

0

0

0

0

0

Run ID SUB-1895

SeqNo 25161

%RPD RPDLimit Qual

0

0

0000000

Run ID SUB-1895

SeqNo 24905

%RPD RPDLimit Qual

00

0

0





Page 4 of 30

Date: 17-May-02


Project: DI-WATER


Analyte

Magnesium

Manganese

Potassium

Sodium

Vanadium

Sample ID R0204325-002AMSD

Analyte

Aluminum

Barium

Calcium

lion

Magnesium

Manganese

Potassium

Sodium

Vanadium


Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Manganese


SampType MSD

Batch ID R_873

Result

1889

04732

1911

19202389

SampType MSD

Batch ID R_873

Result

0951

09619

1912

09883

1889

04732

1911

192

02389

SampType DUP

Batch ID R_873

Result

ND00059

ND

NDND

001868

TestCode

TestNo

PQL

05000050

20050

00050

TestCode

TestNo

PQL

0050

00050

050010050

00050

2 0050

00050

TestCode

TestNo

PQL

0050

00050

0500 10

05000050

6010W_T

SW6010B

SPK value

200520

20025

6010W_T

SW6010B

SPK value

11

201

20

0520

20

025

6010WJT

SW6010B

SPK value

000000

6010W_T

Units mg/L

SPKRefVal

00000

Units mg/L

SPKRefVal

000000000

Units mg/L

SPK Ref Val

000000

Test Method: SW 6010B-Total

Prep Date 5/1/02


%REC LowLimit HighLimit

944

946

956

96

956

Prep Date 5/1/02



951962956

988944

946

956

96

956

Pi ep Date 5/1/02



0 0 0

0 0 0

0 0 0

0 0 00 0 00 0 0

RPD Ref Val

00000

RPDRelVal

000000000

RPD Ref Val

000000

Run ID SUB-1895

SeqNo 24905

%RPD RPDLimit Qual

0

0

0

0

0

Run ID SUB-1895

SeqNo 25162

%RPD RPDLimit Qual

0

00

0

0

0

0

0

0

Run ID SUB-1895

SeqNo 24901

%RPD RPDLimit Qual

000000





Page 5 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER


Analyte

Potassium

Sodium

Vanadium

Sample ID R0204325-002ADUP

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Manganese

Potassium

Sodium

Vanadium


SampType DUP

Batch ID R_873

Result

ND

205

ND

SampType DUP

Batch ID R_873

Result

ND

00059

ND

ND

ND

001868

ND205ND

TestCode

TestNo

PQL

20050

00050

TestCode

TestNo

PQL

0050

00050

050010050

00050

20050

00050

6010W_T

SW6010B

SPK value

000

6010WJT

SW6010B

SPK value

0

0

0

0

00

000

6010WJT

Units mg/L

SPKRefVal

0

0

0

Units mg/L

SPKRefVal

0

0

0

0

0

0

0

0

0

Test Method: SW6010B-TotaI

%REC

000

%REC

000000000

Prep Date

Analysis Date

5/1/02

5/2/02

LowLimit HighLimit

0

0

0

Prep Date

Analysis Date

0

0

0

5/1/02

5/2/02

LowLimit HighLimit

0

0

0

0

00

0

0

0

0

0

0

0

00

00

0

RPD Ref Val

0

0

0

RPD Ref Val

0

0

0

0

0

0000

Run ID- SUB-1895

SeqNo 24901

%RPD RPDLimit Qual

0

0

0

Run ID SUB-1895

SeqNo 25158

%RPD RPDLimit Qual

0

0

0

00

0

0

00





Page 6 of 30

Date: 17-May-02

CLIENT: RSSNWork Order: L0204408Project: DI-WATER 6020W T


Test Method: SW 6020-Total

Sample ID MB-862

Analyte

SampType

Batch ID

MBLK

R_862

Result

TestCode

TestNo

PQL

6020WJT

SW6020

SPK value

Units mg/L

SPKRefVal

Prep Date

Analysis Date

4/30/02

5/1/02


Run ID

SeqNo

SUB-1821

24897

%RPD RPDLimit Qual

Antimony

Aisemc

Beryllium

Cadmium

Chromium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium

Silvei

Thallium

Zinc

Sample ID LCS-862

Analyte

Antimony

Aisemc

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

SampType LCS

Batch ID R_862

Result

0 05278

0 09495

009081

005113

0 04852

0 05039

0 04843

0 05027

004916

00497

00857

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

TestCode

TestNo

PQL

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

6020WJT

SW6020

SPK value

005

0 1

0 1

005

005

005

005

005

005

005

0 1

Units mg/L

SPKRefVal

0

0000000000

%REC

10695

908102

97

101

969101

983994857

Piep Date

Analysis Date

4/30/02

5/1/02

LowLimit HighLimit

85

85

85

85

85

85

85

85

85

85

85

115

115

115

115

115

115

115

115

115

115

115

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

Run ID SUB-1821

SeqNo 24426

%RPD RPDLimit Qual

0

0

0

0

0

0

0

0

0

0

0





Page 7 o/30

Date: 17-May-02

CLIENT: RSSN

Work Order: L0204408ANALYTICAL QC SUMMARY REPORT

Project: DI-WATER

Sample ID LCS-862

Analyte

Silver

Thallium

Zinc


Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chiormum

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


Analyte

Antimony

Arsenic

Beryllium

SampType LCS

Batch ID R_862

Result

0 1009

0 05409

0 04627

SampType MS

Batch ID R_862

Result

0 05589

01058

0 09692

00504

0 05347

00544

0 05027

0 04497

0296

0 05378

0 114

01085

005016

1 741

SampType MS

Batch ID R_862

Result

0 05589

01058

0 09692

TestCode

TestNo

PQL

00010

00010

00010

TestCode

TestNo

PQL

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

TestCode

TestNo

PQL

00010

00010

00010

6020W_T

SW6020

SPK value

01

005

005

6020W_T

SW6020

SPK value

0050 1

01005005005005005005005010 1

005

005

6020WJT

SW6020

SPK value

005

0 1

01

6020WJT

Units mg/L

SPK Ref Val

0

0

0

Units mg/L

SPK Ref Val

0

0

0

0

0

0 00279

0 00667

0

0231

0 00472

0 00352

0

0

1 808

Units mg/L

SPK Ref Val

00

0


%REC

101108

925

%R£C

112

106969101107103

872899130

98 1

110108100

-134

%REC

112

106

969

Prep Date

Analysis Date

4/30/02

5/1/02

LowLimit HighLimit

85

85

85

Prep Date

Analysis Date

115

115

115

4/30/02

5/1/02

LowLimit HighLimit

75

75

75

75

75

75

75

75

75

75

75

75

75

75

Piep Date

Analysis Date

125

125

125

125

125

125

125

125

125

125

125

125

125

125

4/30/02

5/1/02

LowLimit HighLimit

7575

75

125125

125

RPD Ref Val

0

0

0

RPD Ref Val

00000000000000

RPD Ref Val

0

0

0

Run ID SUB-1821

SeqNo 24426

%RPD RPDLimit

0

0

0

Run ID SUB-1821

SeqNo 24407

%RPD RPDLimit

0

0

0

0

0

0000

0000

0

Run ID SUB-1821

SeqNo 24898

%RPD RPDLimit

0

0

0

Qual

Qual

C

C

Qual


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recovery limits



Page 8 of 30

Date: 17-May-02



Project: DI-WATER


Analyte

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


Analyte

Antimony

Aisemc

Beiyllium

Cadmium

Chiomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

SampType MS

Batch ID R_862

Result

00504

0 05347

00544

0 05027

0 04497

0296

0 05378

011401085

005016

1 741

SampType MSD

Batch ID R_862

Result

00556

0105

01037

0 04925

00544

0 05496

0 05027

0 04569

0313

00542

0 116

0108005129

1795

TestCode

TestNo

PQL

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

TestCode

TestNo

PQL

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

6020WJT

SW6020

SPK value

005005

005

005

0050050050101

005005

6020WJT

SW6020

SPK value

005010 1

005005005005005005005

0 1

0 1

005005

6020WJT

Units mg/L

SPK Ref Val

00

0 00279

0 00667

00231

0 00472

0 00352

00

1 808

Units mg/L

SPKRefVal

0

0

0

0

0

0 00279

0 00667

0

02310 00472

0 00352

0

0

1 808


%REC

101107103

872899130

98 1

110108100

-134

%REC

111105

104

985

109

104

872

91 4

164

99

112

108

103-26

Prep Date

Analysis Date

4/30/02

5/1/02

LowLimit HighLimit

75

75

75

75

75

75

75

75

7575

75

Prep Date

Analysis Date

125

125

125

125

125

125

125

125

125

125

125

4/30/02

5/1/02

LowLimit HighLimit

RPD Ref Val

00

0

00000000

RPD Ref Val

0

0

0

0

0000000000

Run ID SUB-1821

SeqNo 24898

%RPD RPDLimit

00000000000

Run ID SUB-1821

SeqNo 24408

%RPD RPDLimit

00

0

0

0

000000000

Qual

C

C

Qual

C



J - This concentration is considered an estimate due to LCS tailuie


Page 9 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER 6020W T




Analyte

SampType

Batch ID

MSD

R_862

Result

TestCode

TestNo

PQL

6020W_T

SW6020

SPK value

Units mg/L

SPKRefVal

Prep Date

Analysis Date

4/30/02

5/1/02


Run ID

SeqNo

SUB-1821

24429

%RPD RPDLimit Qual

Antimony

Aisemc

Beryllium

Cadmium

Chromium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


Analyte

Antimony

Aisemc

Beiyllmm

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

00556

0 105

01037

0 04925

00544

0 05496

0 05027

0 04569

0313

00542

0116

0108

005129

1 795

SampType DUP

Batch ID R_862

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

TestCode

TestNo

PQL

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

0050101

0050050050050050050050 101

005005

6020WJT

SW6020

SPK value

0

0

0

0

0

0

00000

00000

0 00279

0 00667

00231

0 00472

0 00352

00

1 808

Units mg/L

SPK Ref Val

0

0

0

0

0

0

0

0

0

0

0

111

105104

985109104

87291416499

112

108103-26

%REC

00000000000

Piep Date

Analysis Date

4/30/02

5/1/02

LowLimit HighLimit

0

0

0

0

0

000000

0

0

0

0

0000000

00000000000

00

0

RPD Ref Val

00000000000

00000000000000 C

Run ID SUB-1821

SeqNo 24404

%RPD RPDLimit Qual

00

0

0

0

0

0

000

0


3\ - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recovery limits

] - This concentration is consideied an estimate due to LCS failure


Page 10 of 30

Date: 17-May-02

CLIENT: RSSNWork Order: L0204408Project: DI-WATER


Analyte

SiKer

Thallium

Zinc


Analyte

Antimony

Arsenic

Beiyllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

ThalliumZinc

~


SampType DUP

Batch ID R_862

Result

NDNDND

SampType DUP

Batch ID R_862

Result

ND

ND

ND

ND

ND

ND

NDND

NDND

NDNDNDND

TestCode

TestNo

PQL

00010

00010

00010

TestCode

TestNo

PQL

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

00010

6020WJT

SW6020

SPK value

000

6020W_T

SW6020

SPK value

0

0

00

0000000000

6020WJT

Units mg/L

SPKRefVal

000

Units mg/L

SPKRefVal

0

0

0

0

0

0

0

0

000000

Test Method : SW 6020-Total

%REC

000

%REC

00000000000000

Prep Date

Analysis Date

4/30/02

5/1/02

LowLimit HighLimit

0

0

0

Prep Date

Analysis Date

000

4/30/02

5/1/02

LowLimit HighLimit

0

0000000000000

0

0

0

0

0

0

0

0000000

RPD Ref Val

000

RPD Ref Val

00000000000000

Run ID SUB-1821

SeqNo 24404

%RPD RPDLimit Qual

0

0

0

Run ID SUB-1821

SeqNo 24895

%RPD RPDLimit Qual

0

0

0

0

0

0

0

0

0

0

0000

Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked



B -Analyte detected in the associated Method Blank

Page 11 of 30

Date: 17-May-02

CLIENT: RSSN




Test Method: SW8260B

Sample ID. Method Blank 02 SampType MBLK TestCode

Analyte

Batch ID R2933 TestNo

Result PQL

8260_W Units ug/L

SW8260B

SPK value SPKRefVal

Piep Date



Run ID L VOAMS-2 020426A

SeqNo 22527 I

%RPD RPDLimit Qual

Acetone

Benzene

Bromobenzene

Bromochlorome thane

Bi omodichloromethane

Bromoform

Bi omomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Caibon tetrachlonde

Chlorobenzene

Chloroethane

2-Chloroethyl vinyl ether

Chloroform

Chloromethane

2-Chloiotoluene

4-Chloiotoluene

Dibi omochloromethane

1 ,2-Dibi omo-3-chloi opropane

1,2-Dibiomoethane

Dibi omomethane

1 ,2-Dichloi obenzene



Dichloi odifluoromethane

1,1-Dichloroethane

1,2-Dichloioethane

ND

NDND

ND

NDND

ND

NDND

ND

ND

ND

NDNDNDNDNDND

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

ND

25

50

50

5050

5050

2550

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

0

0

0

0

00000000000000000000000

000

000000000

00000000000000

00

00

00

0

0

00

00000000000000

0000

0000

00000

0000000000000000000

00

0000

00

000

000000000000

00000

00000000

0000

0

0

000000000000000000000000

00

000

0000000

00

000

000

00

000000

00

00

00

0



J - This concentration is consideied an estimate due to LCS failure


Page 12 of 30

Date: ll-May-02

CLIENT: RSSN





Sample ID Method Blank 02 SampType MBLK

Analyte

Batch ID R2933

Result

TestCode 8260_W Units ug/L

TestNo SW8260B

PQL SPK value SPKRefVal

Prep Date



Run ID L_VOAMS-2_020426A

SeqNo 22527

%RPD RPDLimit Qual

1,1-Dichloroethene

cis-1 ,2-Dichloroethene

ti ans-1 ,2-Dichloroethene


1 ,3-Dichloropi opane

2,2-Dichloropropane

1 , 1 -Dichloropropene

cis-1 ,3-Dichloropropene

trans-1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

p-Isopropyltoluene

Methylene chloride

4-Methyl-2-pentanone

Naphthalene

n-Propylbenzene

Styrene

1,1,1 ,2-Teti achloi oethane

1 , 1 ,2,2-Teti achloroethane

Tetiachloroethene

Toluene

1,2,3 -Tn chl orobenzen e

1 ,2,4-Tnchl 01 obenzene

1,1,1-Tnchloroethane

1 , 1 ,2-Tnchl oroethane

Tnchloroethene

Tnchlorofluoromethane

ND

ND

ND

ND

ND

ND

ND

NDND

ND

ND

NDNDNDNDNDNDND

ND

ND

ND

ND

NDND

NDNDND

ND

ND

ND

5050

50

50

50

50505050505025

50

50

50

5025

1050

50

50

50

50505050505050

50

000000000000000000000000000

000

0

00000000000000000000000

00000

0

000000000000

00000

0000000000000

0

00000000000

00

00

0

000000000000

0

000000000000

00

0000000000000000

00000000000000000000000000000

0

00000000000000

00

0000000000000

0





Page 13 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER

Sample ID Method Blank 02

Analyte


1 ,2,4-Tnmethylbenzene


Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Sun Dibromofluoiomethane

Surr Toluene-d8

Surr 4-Bromofluorobenzene

Sample ID Vstd050CCV02042

Analyte

Acetone

Benzene

Bromobenzene

Bromochloromethane


Biomofoim

Bi omomethane

2-Butanone

n-Butylbenzene

scc-Butylbenzene

teit-Butylbenzene

Carbon disulfide

Caibon tetrachlonde

Chloiobenzene

Chloioethane

SampType MBLK

Batch ID R2933

Result

NDNDNDNDNDNDND

4769

5341

4545

SampType LCS

Batch ID R2933

Result

4874

4341

4388

41 713944

36

5787

31

4969

4947

4561

ND

39894406

56 17

TestCode

TestNo

PQL

5050

50

50

50

5010

50

50

50

TestCode

TestNo

PQL

255050

50

50

S O

502550

50

50

50

50

50

50

8260_W

SW8260B

SPK value

0

0

0

0

0

00

50

50

50

8260_W

SW8260B

SPK value

50

50

50

50

50

50

50

50

50

50

50

50

50

50

50

8260_W

Units ug/L

SPKRefVal

0

000000000

Units ug/L

SPK Ref Val

0

0

0

0

0

0

0

00000000



%REC

0

000000

954

107

909

%REC

975

868

878834789

72

116

62

994

98991 2

079888 1

112

Prep Date


LowLimit HighLimit

0

0

0

0

0

0

0

80

808562

Prep Date

Analysis Date

0

0

0

0000

120

119

139

4/26/02

LowLimit HighLimit

70

70

70

7070

70

70

70

70

70

70

70

70

70

70

130

130

130

130130

130

130

130

130

130

130130130130130

RPD Ref Val

0000000000

RPD Ref Val

000000000000000


SeqNo 22527

%RPD RPDLimit Qual

0

0

00000000


SeqNo 22530

%RPD RPDLimit Qual

0 S

0000000 S

00

0 i0 S0

00





Page 14 of 30

Date: 17-May-02


Project: DI-WATER


Analyte


Chloroform

Chloiomethane

2-Chlorotoluene

4-Chlorotoluene

Dibromochloromethane

1 ,2-Dibromo-3-chloropropane

1 ,2-Dibromoethane

Dibromomethane


1,3-Dichlorobenzene


Dichlorodifluoromethane

1,1-Dichloioethane

1 ,2-Dichloroe thane

1,1-Dichloroethene

cis-l,2-Dichloroethene

ti ans-1 ,2-Dichloi oethene



2,2-Dichloi opi opane

1 , 1 -Dichloi opi opene

cis-1 ,3-Dichloiopropene

ti ans-1, 3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopi opylbenzene

p-lsopropyltoluene

8260_W

SampType LCS

Batch ID R2933

Result

10542

58774455452

363541 75375939214326445

45356013446738424497465446 144362425143774464

413635432952753431

ND46774826


TestNo SW8260B


505050505050505050505050505050505050505050505050505025505050

505050505050505050505050505050505050505050505050505050505050

0000000000000000000

00000000000



Prep Date



SeqNo 22530


21

84

118

891

904

727

835752

784

865

89907120

89376889993 1

923

872

85875

89382

727

866

106

686

0

935

965

70

80

70

70

70

70

70

70

70

70

70

7070

70

70

80

7070

80

70

70

70

70

7080

70

70

70

70

70

130120130130130130130130130130130130130130

130

120

130130120130130130130130120130130130130130

000000000000000000000000000000

%RPD RPDLimit Qual

0 S

00000000000000000000000000 S

0 S

00


Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits



Page 15 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER


Analyte

Methylene chloride


Naphthalene

n-Propylbenzene

Styiene

1 ,1 ,1,2-Tetrachloroethane

1,1,2,2-Tetiachloroethane

Tetrachloroethene

Toluene

1 ,2,3-Tnchlorobenzene


1 ,1 ,1 -Tnchloroethane

1,1,2-Tnchloroethane

Tnchloroethene

Tnchlorofluoromethane




Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Sun Dibiomofluoromethane

SUIT Toluene-d8

Surr 4-Bromofluorobenzene

Sample ID L0204408-001AMS

Analyte


SampType LCS

Batch ID R2933

Result

4444

3504

5654

4554

2958

41484504

43 8541 66

5757

5224

4027

3906

423

5345

41 02

4602

4585

2389

4933

4443

95 19

47 19

5347

449

SampType MS

Batch ID R2933

Result

TestCode

TestNo

PQL

502510

50505050

5050

50

50

50

50

50

50

50

50

50

50

50

50

10

50

50

50

TestCode

TestNo

PQL

8260_W

SW8260B

SPK value

50

505050

50

50

50

5050

50

50

50

50

50

50

50

50

50

50

50

50

50

50

5050

8260_W

SW8260B

SPK value

8260_W

Units ug/L

SPKRefVal

0000000000000000000000000

Units ug/L

SPKRefVal


%R£C

88970 1

11391 1

59283

901877

833115104

8057818461078292

91 7

478987

889190

944

107

898

%REC

Prep Date


LowLimit HighLimit

70

70

70

70

70

70

70

70

80

70

70

70

70

70

70

70

70

70

70

80

70

70

80

808562

Prep Date

Analysis Date

130

130

130

130130130

130130120130

130130

130130130130130130130120130130120119139

4/26/02

LowLimit HighLimit

RPD Ref Val

0

000000000000000000000000

RPD Ref Val


SeqNo 22530

%RPD RPDLimit Qual

0

0

0

0

0 S

00000000000000 S

000 S

000


SeqNo 22528

%RPD RPDLimit Qual





Page 16 of 30

Date: 17-May-02

CLIENT: RSSN





Sample ID L0204408-001A MS

Analyte

SampType

Batch ID

MS

R2933

Result

TestCode

TestNo

PQL

8260_W

SW8260B

SPK value

Units "g/L

SPKRefVal

Prep Date



Run ID

SeqNo

L_VOAMS-2_020426A

22528

%RPD RPDLimit Qual

Acetone

Benzene

Biomobenzene

Bromochloromethane

Bromodichloromethane

Bromofoim

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

Chloiobenzene

Chloroethane


Chloioform

Chloromethane

2-Chlorotoluene

4-Chloro toluene

Dibi omochloi omethane

1 ,2-Dibi omo-3-chloi opi opane

1 ,2-Dibromoethane

Dibi omomethane


1,3-Dichloiobenzene

1 ,4-Dichloi obenzene

Dichloiodifluoromethane

1,1-Dichloroethane

1,2 Dichloroethane

3982

4836

4838

4721

4336

3657

61993337

4399

4553

45 12

ND

4478

4774

6035

ND4365

5635

47 12

4741

3952

3462

4087

4301

4452

4595

4748

61 6248 194088

25

50

50

50

50

50

50

25

50

50

50

50

50

50

50

5050

50

50

50

50

50

50

50

50

5050

50

5050

5050

50

5050

50

50

50

50

50

50

50

505050

5050

50

50

50

50

50

50

5050

50

50

5050

50

0

0

0

0

0

0

0

0000

0

0

0

0

000000000000000

796967

968944867

73 1124

667

88

91 1902

0

896

955

121

0

873

113942

948

79692

817

8689

91 9

95

123964

81 8

70

70

70

70

70

70

70

70

70

70

70

70

70

70

70

70

80

70

70

70

70

70

70

70

70

70

70

7070

70

130

130

130

130

130

130

130

130

130130

130

130

130

130

130

130120

130130130130130130130130130130130130130

000000000000000000000000000000

00

00000000

000000

000000000

0000

0





Page 17 of 30

Date: 17-May-02

CLIENT: RSSN






Analyte

SampType

Batch ID

MS

R2933

Result

TestCode

TestNo

PQL

8260_W

SW8260B

SPK value

Units (ig/L

SPK Ref Val

Prep Date



Run ID

SeqNo

L_VOAMS-2_020426A

22528

%RPD RPDLimit Qual

1,1-Dichloioethene


ti ans-1 ,2-Dichloroethene


1 ,3-Dichloropi opane

2,2-Dichloropropane

1 , 1 -Dichloropropene


trans-1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodome thane

Isopiopylbenzene

p-Isopropyltoluene

Methylene chloride


Naphthalene

n-Propylbenzene

Styiene

1,1,1 ,2-Teti achloi oethane

1,1 ,2,2-Tetrachloioethane

Tetiachloroethene

Toluene

1 ,2,3- frichloi obenzene

1 ,2,4-Ti ichlorobenzene

1 ,1 ,1-Tnchloroethane

1 ,1 ,2-Tnchloroethane

Ti ichloroethene

Tnclilorofluoromethane

5076

5085

5063

467

4533

4743

4931

4342

3883

4548

278

3502

542

4887

4623

48 13

3643

80614757

3624

4452

46124636

4572

2401

31 7444

4227

4632

5686

50

50

50

50

50

50

50

5050

50

50

2550

50

50

50

25

50

50

50

50

50

50

50

50

50

5050

5050

50

50

5050

50

50

50

5050

50

50

50

50

5050

505050505050505050505050

50

5050

0

00000000000000000000000000000

102102101

934907949986868111

91556

70108977925963729

161

95 1

725

89922

927

91 4

48

634

888845926114

80

70

70

80

70

70

70

70

70

80

70

7070

70

70

70

70

70

70

70

70

70

70

80

70

70

7070

70

70

120

130

130

120

130

130

130130130120

130130130130130130130130130130130130130120130130130130130130

000000000000000000000000000000

00000000000 S

00 S

00000 S

0000000 S

0 S

0000





Page 18 of 30

Date: 17-May-02


Project: DI-WATER


Analyte


1 ,2,4-Ti imethylbenzene


Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

SUIT Dibromofluoromethane

Surr Toluene-d8

Sun 4-Bromofluorobenzene

Sample ID L0204408-001A MSD

Analyte

Acetone

Benzene

Bromobenzene

Biomochloro methane


Bromoform

Bi omomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

teit-Butylbenzene

Caibon disulfide

Carbon tetiachlonde

Chloiobenzene

Chloroethane


SampType MS

Batch ID R2933

Result

4257

48 18

4678

228

5012

4556

9985

4627

5321

4363

SampType MSD

Batch ID R2933

Result

41 32

452

47 16

47

41 84

3815

ND

3485

4237

4508

4367

ND

4058

4602

5528

TestCode

TestNo

PQL

5050

50

50

5050

10505050

TestCode

TestNo

PQL

25

5050

505050502550

50

5050505050

8260_W

SW8260B

SPK value

50

50

50

50

50

50

50

50

50

50

8260_W

SW8260B

SPK value

50505050505050505050

5050505050

8260_W

Units ug/L

SPKRefVal

00

0

0

000000

Units fig/L

SPKRefVal

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0


%REC

851964

936456

100

91 1

200

925

106873

%REC

826904943

94

837

7630

697847

902

8730

81292

111

Prep Date

Analysis Date


4/26/02

LowLimit HighLimit

70

7070

70

80

70

70

926

957853

Prep Date

Analysis Date

130

130130

130

120

130130108112104

4/26/02

LowLimit HighLimit

70

70

70

70

70

70

70

70

70

70

70

70

7070

70

130

130

130

130130130130130130

130130130130130130

SeqNo 22528

RPD Ref Val

0

0

0

0

0

0

0000

%RPD

0000000000

Run ID L_

RPDLimit Qual

S

S

S^

ji

VOAMS-2_020426A

SeqNo 22529

RPD Ref Val

3982

4836

4838

4721

4336

3657

61 99

3337

4399

4553

45 12

0

4478

4774

6035

%RPD

370676

255

0446

357

423

0

434

375

0993

327

0984

367

877

^RPDLimit Qual

25

25

25

25

25

25

25 S ,

25 S

25

251

25

25 S

25

25

25

<-





Page 19 of 30

Date: 17-May-02

CLIENT: RSSNWork Order: L0204408Project: DI-WATER 8260_W

Sample ID L0204408-001AMSD SampType MSD

Batch ID R2933

Analyte


Chloroform

Chloromethane

2-Chlorotoluene

4-Chloro toluene

Dibromochloromethane

1 ,2-Dibromo-3-chloropropane

1 ,2-Dibromoethane

Dibromomethane




Dichlorodifluoromethane

1,1-Dichloroe thane

1 ,2-Dichloroethane

1,1-Dichloroethene


trans-l,2-Dichloroethene



2,2-Dichloiopropane

1,1-Dichloiopiopene


ti ans-1 ,3-Dichloropropene

Ethylbenzene

Hexachloi obutadiene

2-Hexanone

lodomethane

Isopropylbenzene

p-Isopropyltoluene

Result

ND41435241

45314557

3883

4233

41 694284

45414578

4707

5273

4609

3993

4534

4924

4827

45 1545614329

4465

4268

38 164407

3271364

5 164567

4368


TestNo SW8260B


505050505050505050

50

50

50

50

50

50

50

50

50

50

5050

5050505050255050

50

5050505050505050505050

50

50

50

50

50

50

50

50

50

50

50

50

505050

50505050

000000000000000000000000000000



Prep Date



SeqNo 22529


0

829

105

906

91 1

777

847

834

857

908

91 6

94 1

105

922

799

907

985

965

903

91 2

866

893854

763

88 1

654

728

10391 3

874

70

80

70

70

70

7070

70

7070

7070

70

70

70

80

70

70

80

70

70

70

70

70

80

70

70

70

70

70

130

120

130

130

130

130130130130130

130130

130

130

130120

130130

120

130130130130130120

130

130130130130

0

4365

5635

47 12

4741

3952

3462

4087

4301

4452

4595

4748

6162

48 19

4088

5076

5085

5063

467

4533

4743

49314342

3883

4548

278

3502

5424887

4623

%RPD RPDLimit Qual

0

522

725

392

396

176200

1 99

0396

198

03710867

155445

235

113322

477

33806169139921 72

1 74

3 15

162

386491677

567

25 S

25

25

25

25

2525

252525

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25

25 S

25

25 S

25

25





Page 20 o/30

Date: 17-May-02

CLIENT: RSSNWork Order: L0204408Project: DI-WATER 8260_W

Sample ID L0204408-001AMSD SampType MSD

Batch ID R2933

Analyte

Methylene chloride


Naphthalene

n-Piopylbenzene

Styiene

1,1,1 ,2-Tetrachloi oethane

1 , 1 ,2,2-Tetrachloroethane

Teti achloroethene

Toluene

1,2,3-Tnchlorobenzene


1,1,1-Trichl 01 oethane1 , 1 ,2-Ti ichloroethane

Tuchloioethene

Tnchloi ofluoi omethane

1 ,2,3-Tnchloropropane1 ,2,4-Ti imethylbenzene


Vinyl acetate

Vinyl chloride

o-Xylene

m,p-XyleneSurr Dibiomofluoromethane

Surr Toluene-d8SUIT 4-Biomofluorobenzene

Result

47 1

3777

6411

45023144

4403

4858

4395

4243

4443

4376

41084224

4335504

4486

4466

4399

2235

4511

4427

9495

4634

5269

4342


TestNo SW8260B

PQL SPK value SPK

50

25

50

5050

50

50

50

5050

505050

50

50

50

50

50

50

50

50

10

50

50

50

50

50

50

50

50

50

50

50

50

50

50

5050

50

50

50

50

50

50

50

50

50

50

50

50

Ref Val

0

0

0

0

0

0

0

0

0

00

0

0

0

0

0

0

0

0

0

0

0

0

0

0



Prep Date



SeqNo 22529


942

755

128

90

629

88 1

972

879

849

889

875

822845

867

101

897

893

88447

902

885

190

927

105

868

70

70

70

7070

70

70

70

80

70

70

7070

70

70

70

70

70

70

80

70

70

926

957

853

130

130

130

130

130

130

130

130

120

130

130

130130

130

130

130

130

130

130

120

130

130

108

112

104

4813

3643

8061

47573624

4452

46 12

46364572

2401

31 7444

4227

4632

5686

4257

48 18

4678

228

5012

4556

9985

0

0

0

%RPD RPDLimit

2 16

361

228

551142

1 11

520534

746597

320

777

00710

662

120

524

7586 15

1 99

105

287

503

0

0

0

25

25

25

2525

25

25

25

25

25

25

2525

25

25

25

25

25

25

25

25

25

0

0

0

Qual

S

R

R

S

S



J - This concentiation is consideied an estimate due to LCS failuie


Page 21 o/30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER

Sample ID MB-R2983

Analyte

Alkalinity, Bicarbonate (As CaC03)

Alkalinity, Carbonate (As CaC03)

Hydi oxide (As CaC03)

Alkalinity, Total (As CaC03)

Sample ID LCS-R2983

Analyte

Alkalinity, Total (As CaCO3)


Analyte


Sample ID L0204322-001BDUP

Analyte

Alkalinity, Bicaibonate (As CaC03)

Alkalinity, Caibonate (As CaC03)

Hydi oxide (As CaC03)



SampType MBLK

Batch ID R2983

Result

ND

ND

ND

ND

SampType LCS

Batch ID R2983

Result

144

SampType LCSD

Batch ID R2983

Result

122

SampType DUP

Batch ID R2983

Result

ND74

ND74

ALK_W

TestCode ALK_W Units mg/L

TestNo M2320B


25

25

25

25


TestNo M2320B


25 125 0


TestNo M2320B


25 125 0


TestNo M2320B


25 0 0

25 0 0

25 0 0

25 0 0

Test Method: SM2320 B

Prep Date



Piep Date



115 80 120 0

Prep Date



97 6 80 120 144

Prep Date



0 0 0 0

0 0 0 7 5

0 0 0 0

0 0 0 7 5

Run ID L_ATITR-1_020429A

SeqNo 22904

%RPD RPDLimit Qual


SeqNo 22903

%RPD RPDLimit Qual

0


SeqNo 22906

%RPD RPDLimit Qual

165 25


SeqNo 22905

%RPD RPDLimit Qual

0 10

1 34 10

0 10

1 34 10



J - This concentiation is considered an estimate due to LCS failuie


Page 22 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER COD


Test Method: SM5520 D

Sample ID MB-R2949 SampType MBLK TestCode

Analyte


Result PQL

COD Units mg/L

M5220 C

SPK value SPKRefVal

Prep Date



Run ID L_WC_020429C

SeqNo 22627

%RPD RPDLimit Qual

Chemical Oxygen Demand ND 10

Sample ID LCS-R2949 SampType LCS

Analyte

Batch ID R2949

Result

TestCode

TestNo

PQL

COD Units mg/L

M5220 C

SPK value SPKRefVal

Prep Date



Run ID

SeqNo

L_WC_020429C

22626

%RPD RPDLimit Qual

Chemical Oxygen Demand 533 10 500 107 80 120


Analyte

SampType

Batch ID

LCSD

R2949

Result

TestCode

TestNo

PQL

COD

M5220 C

SPK value

Units mg/L

SPKRefVal

Piep Date



Run ID

SeqNo

L_WC_020429C

22630

%RPD RPDLimit Qual

Chemical Oxygen Demand 503 10 500 101 80 120 533 579 15

Sample ID L0204310-001BMS SampType MS

Analyte

Batch ID R2949

Result

TestCode

TestNo

PQL

COD Units mg/L

M5220 C

SPK value SPKRefVal

Prep Date



Run ID L_WC_020429C

SeqNo 22628

%RPD RPDLimit Qual

Chemical Oxygen Demand 554 10 4625 75 104 70 130

Sample ID L0204310-001BMSD SampType MSD TestCode

Analyte


Result PQL

COD Units mg/L

M5220 C

SPK value SPKRefVal

Piep Date



Run ID L_WC_020429C

SeqNo 22629

%RPD RPDLimit Qual

Chemical Oxygen Demand 546 10 4625 75 102 70 130 546 25





Page 23 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER HG 7470 T



Sample ID MB-854

Analyte

Meicuiy

Sample ID MB-854

Analyte

SampType

Batch ID

SampType

Batch ID

MBLK

R_854

Result

ND

MBLK

R_854

Result

TestCode

TestNo

PQL

0 00020

TestCode

TestNo

PQL

HG_7470_T Units mg/L

SW7470

SPK value SPKRefVal

HG_7470_T Units mg/L

SW7470

SPK value SPKRefVal

Prep Date

Analysis Date

4/30/02

4/30/02


Prep Date

Analysis Date

4/30/02

4/30/02


Run ID SUB-1793

SeqNo 23700

%RPD RPDLimit

Run ID SUB-1793

SeqNo 24307

%RPD RPDLimit

Qual

Qual

Mercury ND 0 00020

Sample ID MB-854

Analyte

SampType MBLK

Batch ID R_854

Result

TestCode HG_7470_T Units mg/L

TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24891

%RPD RPDLimit Qual

Mei cury ND 0 00020

Sample ID MB-854

Analyte

SampType MBLK

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 27231

%RPD RPDLimit Qual

Meicuiy ND 0 00020

Sample ID LCS-854

Analyte

SampType

Batch ID

LCS

R_854

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVal

Piep Date

Analysis Date

4/30/02

4/30/02


Run ID

SeqNo

SUB-1793

23699

%RPD RPDLimit Qual

Mercuiy 0 00492 0 00020 0005 85 115


Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted iccovery limits

J - This concentiation is consideied an estimate due to LCS failuie


Page 24 of 30

Date: 17-May-02

CLIENT: RSSNWork Order: L0204408Project: DI-WATER HG 7470 T



Sample ID LCS-854

Analyte

SampType LCS

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24306

%RPD RPDLimit Qual

Mercury 0 00492 0 00020 0005 984 85 115

Sample ID LCS-854

Analyte

SampType LCS

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24890

%RPD RPDLimit Qual

Meicury 0 00492 0 00020 0005 984 85 115

Sample ID LCS-854

Analyte

SampType LCS

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 27230

%RPD RPDLimit Qual

Mercuiy 0 00492 0 00020 0005 984 85 115


Analyte

SampType MS

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02


%R£C LowLimit HighLimit RPD Ref Val

Run ID SUB-1793

SeqNo 23701

%RPD RPDLimit Qual

Mercui y 0005 0 00020 0005 100 85 115


Analyte

SampType

Batch ID

MS

R_854

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVal

Piep Date

Analysis Date

4/30/02

4/30/02


Run ID

SeqNo

SUB-1793

24308

%RPD RPDLimit Qual

Meicury 0005 0 00020 0005 100 85 115





Page 25 of 30

Date: ll-May-02

CLIENT: RSSN






Analyte

SampType MS

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24892

%RPD RPDLimit Qual

Mercury 0005 0 00020 0005 100 85 115


Analyte

SampType MS

Batch ID R_854

Result


TestNo SW7470


Piep Date 4/30/02



Run ID SUB-1793

SeqNo 27232

%RPD RPDLimit Qual

Meicuiy 0005 0 00020 0005 100 85 115


Analyte

SampType MSD

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 23702

%RPD RPDLimit Qual

Mercuiy 0 00465 0 00020 0005 93


Analyte

SampType MSD

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24309

%RPD RPDLimit Qual

Meicury 0 00465 0 00020 0005 93


Analyte

SampType MSD

Batch ID R_854

Result


TestNo SW7470


Piep Date 4/30/02



Run ID SUB-1793

SeqNo 24893

%RPD RPDLiiTiit Qual

Mercuiy 0 00465 0 00020 0005 93



J - This concentration is considered an estimate due to LCS fai luie


Page 26 of 30

Date: 17-May-02

CLIENT: RSSN






Analyte

SampType MSD

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 27233

%RPD RPDLimit Qual

Mei cury 0 00465 0 00020 0005 93


Analyte

SampType DUP

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 23698

%RPD RPDLimit Qual

Meicuiy ND 0 00020


Analyte

SampType DUP

Batch ID R_854

Result

TestCode HGJ7470_T Units mg/L

TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24305

%RPD RPDLimit Qual

Mercury ND 0 00020


Analyte

SampType DUP

Batch ID R_854

Result


TestNo SW7470


Prep Date 4/30/02



Run ID SUB-1793

SeqNo 24889

%RPD RPDLimit Qual

Meicury ND 0 00020


Analyte

SampType

Batch ID

DUP

R_854

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPK Ref Val

Piep Date

Analysis Date

4/30/02

4/30/02


Run ID

SeqNo

SUB-1793

27229

%RPD RPDLimit Qual

Meicuiy ND 0 00020

Qualifici s: ND - Not Detected at the Repoi ting Limit C - Unspiked sample >5 times the amount spiked




Page 27 of 30

Date: 17-May-02

CLIENT: RSSN


Project: DI-WATER NH3-N W


Test Method: SM4500-NH3 C

Sample ID MB-R2996

Analyte

SampType MBLK

Batch ID R2996

Result

TestCode

TestNo

PQL

NH3-N_W Units mg/L

M4500-NH3 C

SPK. value SPKRefVal

Prep

Analysis

Date

Date 4/30/02


Run ID

SeqNo

L_WC_020430A

23035

%RPD RPDLimit Qual

Ammonia, as N ND 030

Sample ID LCS-R2996 SampType LCS

Analyte

Batch ID R2996

Result

TestCode NH3-N_W Units mg/L

TestNo M4500-NH3C


Piep Date



Run ID L_WC_020430A

SeqNo 23034

%RPD RPDLimit Qual

Ammonia, as N 1 008 030 101 839 117


Analyte

SampType LCSD

Batch ID R2996

Result


TestNo M4500-NH3C


Piep Date



Run ID L_WC_020430A

SeqNo 23037

%RPD RPDLimit Qual

Ammonia, as N 1 01 030 101 839 117 1 008 0198 25

Sample ID L0204322-001BMS

Analyte

SampType MS

Batch ID R2996

Result


TestNo M4500-NH3C


Piep Date



Run ID L_WC_020430A

SeqNo 23036

%RPD RPDLimit Qual

Ammonia, as N 1 12 030 112 764 124



J - This concentration is consideied an estimate due to LCS failure


Page 28 of 30

Date: !7-May-02

CLIENT: RSSN


Project: DI-WATER SULF W


Test Method: SM4500-S D

Sample ID MB-R3137 SampType MBLK

Analyte

Batch ID R3137

Result

TestCode SULF_W Units mg/L

TestNo M4500-SD


Prep Date



Run ID L_SPEC-2_020503A l

SeqNo 24265

%RPD RPDLimit Qual

Sulfide ND 0030

Sample ID LCS-R3137

Analyte

SampType LCS

Batch ID R3137

Result

TestCode SULFJW Units mg/L

TestNo M4500-SD


Prep Date



Run ID L_SPEC-2_020503A

SeqNo 24264

%RPD RPDLimit Qual

Sulfide 0115 0030 0107 107 120

Sample ID LCSD-R3137 SampType LCSD

Analyte

Batch ID R3137

Result


TestNo M4500-SD


Prep Date



Run ID L_SPEC-2_020503A >

SeqNo 24268

%RPD RPDLimit

I

I

Qual '

Sulfide 0 113 0030 0107 106 80 120 0 115 1 75 25

Sample ID L0204408-001BMSD

Analyte

SampType MS

Batch ID R3137

Result


TestNo M4500-SD


Prep Date



Run ID L_SPEC-2_020503A

SeqNo 24267

%RPD RPDLimit Qual

Sulfide 0 119 0030 0107 111 70 130

Sample ID L0204408-001BMS SampType MSD

Analyte

Batch ID R3137

Result

TestCode SULF_\V Units mg/L

TestNo M4500-SD


Prep Date



Run ID L_SPEC-2_020503A !

SeqNo 24266

%RPD RPDLimit Qual

Sulfide 0 116 0030 0107 108 70 130 0119 255 25



J - This concentiation is considered an estimate due to LCS failure


Page 29 of 30

Date: 17-May-02

CLIENT:Work Order:

Project:

RSSNL0204408

DI-WATER TDS W


Test Method: SM2540 C

Sample ID: MB-R3022

Analyte

SampType: MBLK

Batch ID: R3022

Result

TestCode: TDS_W Units- mg/L

TestNo- El 60.1


Prep Date:

Analysis Date: 4/26/02


Run ID: L WC 020426E1

SeqNo: 232191

%RPD RPDLimit Qual

Total Dissolved Solids ND 15.0

Sample ID: LCS-R3022

Analyte

SampType: LCS

Batch ID: R3022

Result

TestCode: TDS_W

TestNo: E160.1

PQL SPK value

Units: mg/L

SPKRefVal

Prep Date:

Analysis Date: 4/26/02


Run ID: L_WC_020426E

SeqNo: 23218

%RPD RPDLimit Qual

j

[

1

Total Dissolved Solids 966 15.0 1000 96.6 80 120


Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits

J - This concentration is considered an estimate due to LCS failure.


Page 30 o/30

Date: 17-May-02

NEL LABORATORIESReno • Las Vegas • Boise

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Analysis

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Box #1 DW - Drinking WaterWW • Waste WaterOL - Oil/Organic Liquid

SD - SolidAQ AqueousA - Air

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D NaOH

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The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received in good condition,including adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceof NEL Standard List Prices for all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples receivsd. at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided above

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