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31-12 24 TH AVENUE QUEENS, NEW YORK Limited Remedial Investigation Report NYC VCP Site Number: TBD OER Project Number: 11EHAZ215Q Prepared for: Tres Construction, LLC 24-08 32 nd Street Queens, New York 11102 [email protected] Prepared by: 4509 Greenpoint Avenue, Queens, NY 11104 [email protected] (718) 7847490 MAY 2015

Limited Remedial Investigation Report - Welcome to … Project Number: 11EHAZ215Q ... 1.2 Proposed Redevelopment Plan ... developed with various commercial uses including lamp shade

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31-12 24TH AVENUE

QUEENS, NEW YORK

Limited Remedial Investigation Report

NYC VCP Site Number: TBD

OER Project Number: 11EHAZ215Q

Prepared for:

Tres Construction, LLC 24-08 32nd Street

Queens, New York 11102 [email protected]

Prepared by:

45‐09 Greenpoint Avenue, Queens, NY 11104

[email protected]

(718) 784‐7490

MAY 2015

i

TABLE OF CONTENTS

TABLE OF CONTENTS ......................................................................................................... i 

LIST OF ACRONYMS .......................................................................................................... iii 

CERTIFICATION .................................................................................................................. iv 

EXECUTIVE SUMMARY ..................................................................................................... 1 

REMEDIAL INVESTIGATION REPORT ............................................................................ 5 

1.0   SITE BACKGROUND................................................................................................. 5 

1.1   Site Location and Current Usage .............................................................................. 5 

1.2  Proposed Redevelopment Plan ................................................................................. 5 

1.3   Description of Surrounding Property ........................................................................ 6 

2.0   SITE HISTORY ........................................................................................................... 7 

2.1   Past Uses and Ownership .......................................................................................... 7 

2.2   Previous Investigations ............................................................................................. 7 

2.3   Site Inspection ........................................................................................................... 7 

2.4   Areas of Concern ...................................................................................................... 7 

3.0   PROJECT MANAGEMENT ....................................................................................... 8 

3.1   Project Organization ................................................................................................. 8 

3.2   Health and Safety ...................................................................................................... 8 

3.3  Materials Management .............................................................................................. 8 

4.0   REMEDIAL INVESTIGATION ACTIVITIES ........................................................... 9 

4.1   Geophysical Investigation ......................................................................................... 9 

4.2   Borings and Monitoring Wells .................................................................................. 9 

4.3   Sample Collection and Chemical Analysis ............................................................. 10 

5.0   ENVIRONMENTAL EVALUATION....................................................................... 14 

5.1  Geological and Hydrogeological Conditions .......................................................... 14 

5.2   Soil Chemistry ........................................................................................................ 14 

5.3   Groundwater Chemistry .......................................................................................... 15 

5.4   Soil Vapor Chemistry ............................................................................................. 15 

5.5   Prior Activity .......................................................................................................... 15 

5.6   Impediments to Remedial Action ........................................................................... 15 

ii

FIGURES

Figure-1: Site Location Map Figure-2: Site Boundary Map Figure-3: Proposed Redevelopment Plan Figure-4: Areas of Concern Figure-5: Sampling Plan Figure-6: Diagram of Exceedances in Soil Samples

TABLES

Table-1: Soil Samples Analytical Results for VOCs (showing exceedances of Track 1 SCOs)

Table-2: Soil Samples Analytical Results for SVOCs (showing exceedances of Track 1 SCOs)

Table-3: Soil Samples Analytical Results for Pesticides/PCBs (showing exceedances of Track 1 SCOs) Table-4: Soil Samples Analytical Results for Metals (showing exceedances of Track 1

SCOs) Table-5: Soil Vapor Analytical Data Summary (showing exceedances of NYS

DOH Soil Vapor Intrusion Guidance)

APPENDICES

Appendix A: Phase I ESA Report Appendix B: Photo Log Appendix C: GPR Report Appendix D: Boring Logs Appendix E: Soil Vapor Sampling Log Appendix F: Laboratory Analytical Results for Soil Samples Appendix G: Laboratory Analytical Results for Soil Vapor Samples

iii

LIST OF ACRONYMS

Acronym Definition

AOC Area of Concern

CAMP Community Air Monitoring Plan

COC Contaminant of Concern

CPP Citizen Participation Plan

CSM Conceptual Site Model

DER-10 New York State Department of Environmental Conservation Technical Guide 10

FID Flame Ionization Detector

GPS Global Positioning System

HASP Health and Safety Plan

HAZWOPER Hazardous Waste Operations and Emergency Response

IRM Interim Remedial Measure

NAPL Non-aqueous Phase Liquid

NYC VCP New York City Voluntary Cleanup Program

NYC DOHMH New York City Department of Health and Mental Hygiene

NYC OER New York City Office of Environmental Remediation

NYS DOH ELAP

New York State Department of Health Environmental Laboratory Accreditation Program

OSHA Occupational Safety and Health Administration

PID Photoionization Detector

QEP Qualified Environmental Professional

RI Remedial Investigation

RIR Remedial Investigation Report

SCO Soil Cleanup Objective

SPEED Searchable Property Environmental Electronic Database

1

EXECUTIVE SUMMARY

The Remedial Investigation Report (RIR) provides sufficient information for establishment

of remedial action objectives, evaluation of remedial action alternatives, and selection of a

remedy pursuant to RCNY§ 43-1407(f). The remedial investigation (RI) described in this

document is consistent with applicable guidance.

Site Location and Current Usage

The Site is located at 31-12 to 31-18 24th Avenue and 24-08 32nd Street in the Astoria section

of Queens, New York and is identified as Block 837 and Lot 50 on the New York City Tax Map

(Please note that the Site was recently merged from Lots 50 and 52 into a single Lot 50). Figure

1 shows the Site location. The Site is 7,500-square feet and is bounded by 24th Avenue to the

north, a 3-story residential structure to the south, 32nd Street to the east, and several residential

structures and a commercial deli to the west. A map of the site boundary is shown in Figure 2.

Currently, the Site is used for storage and office space for a commercial construction business

and contains one 2-story structure with a partial basement and one 1-story structure. The two

buildings are interconnected at grade level.

Proposed Redevelopment Plan

The proposed future use of the Site will consist of a 6-story mixed use commercial and

residential building with cellar and sub-cellar which will occupy the entire footprint of the Site.

The total gross square footage of the proposed building will be approximately 37,049 square feet,

including approximately 22,648 square feet of residential units and 7,781 of commercial space

with the 7,483 square foot sub-cellar utilized for parking and mechanical rooms. The cellar will

also be utilized for parking along with commercial as well as commercial space and residential

lobby. The first floor will consist of commercial occupancy and a small open area used for

bicycle parking. The floors above (2nd through 6th) will be utilized as residential units. As part of

development, the entire Site is expected to be excavated to approximately 12-13 feet below

current grade. The total amount of soil expected to be removed for excavation of the cellar levels

is approximately 3,600 cubic yards. The groundwater table is assumed to be at approximately 25

feet bgs at the Site. Layout of the proposed site development is presented in Figure 3. The

current zoning designation is C4-3 (R6 equivalent). The proposed use is consistent with existing

zoning for the property.

2

Summary of Past Uses of Site and Areas of Concern

A Phase I Environmental Site Assessment was performed by Athenica in May 2015.

Historical Sanborn maps show the Site was developed from at least 1915. The Site was shown as

developed with various commercial uses including lamp shade manufacturing and as an

unspecified use warehouse. Portions of the Site are also shown as developed with small

structures designated as “auto” which were most likely former parking garages. Historical City

Directories also list several commercial occupants of the Site including: Terrazzo Flooring Co,

Kovar Products Co, Astoria Novelty Co, C&L Cabinets & Woodturning, Greenlight Energy

Incorporated and Tres Construction.

The AOCs identified for this site include:

1. Presence of urban fill from approximately grade level to 4 feet bgs.

Summary of the Work Performed under the Remedial Investigation

The scope of work implemented in May of 2015 by Athenica included:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e. structures,

buildings, etc.);

2. Performed a ground penetrating radar (GPR) survey;

3. Installed four (4) soil borings across the entire project Site, and collected nine (9) soil

samples for chemical analysis from the soil borings to evaluate soil quality;

4. Monitoring wells could not be installed at the Site due to the Site conditions. Monitoring

wells will be completed after the demolition of the on Site structures and groundwater

quality beneath the Site will be evaluated.

5. Installed two (2) soil vapor probes around Site perimeter and collected two (2) samples

for chemical analysis.

Summary of Environmental Findings

1. Elevation of the property ranges from 52.54 to 60.23 feet.

3

2. Groundwater depth could not be determined since monitoring wells could not be installed

during the Remedial Investigation (RI). The monitoring wells will be installed after the

demolition of the buildings is completed at the Site.

3. Groundwater flow could not be determined since monitoring wells could not be installed

during the RI. The regional groundwater flow direction is towards west in the vicinity of

the Site.

4. Bedrock was not encountered during the RI.

5. The stratigraphy of the Site, from the surface down, consists of approximately 2 to 4 feet

of medium sand with urban fill, underlain by 6 feet of medium sand with pebbles and

beneath 10 feet below grade surface underlain by 5 feet of coarse sand and pebbles.

6. Soil/fill samples collected during the limited RI were compared to NYSDEC 6NYCRR

Part 375-6.8 Unrestricted Use Soil Cleanup Objectives (SCOs) and Restricted Residential

Use SCOs. Soil/fill sampling collected during the RI showed trace concentrations of a

few VOCs including acetone and methylene chloride, both common lab contaminants.

Three (3) Polycyclic Aromatic Hydrocarbon (PAH) SVOCs including benz(a)anthracene

(1.34 ppm), benzo(k)fluoranthene (0.84 ppm), and chrysene (1.25 ppm) were detected in

one shallow soil sample (0’-2’) at SB-2 exceeding their respective Unrestricted Use

SCOs . Of these only benz(a)anthracene exceeded its respective Restricted Residential

Use SCO. One Pesticide; 4,4’DDT (max. of 0.0082 ppm) was detected above its

Unrestricted Use SCO in one shallow (0’-2’) and one deeper (4’-6’) soil sample. Total

PCBs was detected in one shallow sample at 0.088 ppm, below its Unrestricted Use SCO.

Two (2) metals, including lead (max. of 80.7 ppm) and zinc (113 ppm) were detected

above their respective Unrestricted Use SCOs, but below their respective Restricted

Residential Use SCOs. The results are indicative of historic fill material and they are

contained in the shallow soil beneath the Site. A summary table of data for chemical

analyses performed on soil samples is included in Table 1 through 4.

7. Soil vapor samples collected during the RI were compared to the compounds listed in

Vapor Intrusion Matrices in the New York State Department of Health (NYSDOH) Final

Guidance for Evaluating Soil Vapor Intrusion, dated October 2006. Soil vapor sample

results detected trace levels of petroleum compounds and chlorinated VOCs. The total

concentration of petroleum-related VOCs (BTEX) was 27 µg/m3. Chlorinated compound

4

including 1,1,1-trichloroethane, carbon tetrachloride and trichloroethylene (TCE) were

not detected in any of the samples. Tetrachloroethylene (PCE) was detected in one

sample at a concentration of 17 µg/m3. All chlorinated compounds were below the

monitoring and mitigation levels established by NYSDOH matrix. A summary table of

data for chemical analyses performed on soil vapor samples is included in Table 5.

5

REMEDIAL INVESTIGATION REPORT

1.0 SITE BACKGROUND

Tres Construction LLC has applied to enroll in the New York City Voluntary Cleanup

Program (NYC VCP) to investigate and remediate a 0.172-acre site located at 31-12 to 31-18

24th Avenue and 24-08 32nd Street in the Astoria section of Queens, New York. Mixed

commercial residential use is proposed for the property. The RI work was performed between

May 11 and May 12, 2015. This RIR summarizes the nature and extent of contamination and

provides sufficient information for establishment of remedial action objectives, evaluation of

remedial action alternatives, and selection of a remedy that is protective of human health and the

environment consistent with the use of the property pursuant to RCNY§ 43-1407(f).

1.1 Site Location and Current Usage

The Site is located at 31-12 to 31-18 24th Avenue and 24-08 32nd Street in the Astoria section

of Queens, New York and is identified as Block 837 and Lot 50 on the New York City Tax Map

(Please note that the Site was recently merged from Lots 50 and 52 into a single Lot 50). Figure

1 shows the Site location. The Site is 7,500-square feet and is bounded by 24th Avenue to the

north, a 3-story residential structure to the south, 32nd Street to the east, and several residential

structures and a commercial deli to the west. A map of the site boundary is shown in Figure 2.

Currently, the Site is used for storage and office space for a commercial construction business

and contains one 2-story structure with a partial basement and one 1-story structure. The two

buildings are interconnected at grade level.

1.2 Proposed Redevelopment Plan

The proposed future use of the Site will consist of a 6-story mixed use commercial and retail

building with cellar and sub-cellar which will occupy the entire footprint of the Site. The total

gross square footage of the proposed building will be approximately 37,049 square feet,

including approximately 22,648 square feet of residential units and 7,781 of commercial space

with the 7,483 square foot sub-cellar utilized for parking and mechanical rooms. The cellar will

also be utilized for parking along with commercial as well as commercial space and residential

lobby. The first floor will consist of commercial occupancy and a small open area used for

bicycle parking. The floors above (2nd through 6th) will be utilized as residential units. As part of

development, the entire Site is expected to be excavated to approximately 12-13 feet below

6

current grade. The total amount of soil expected to be removed for excavation of the celllar leves

is approximately 3,600 cubic yards. The groundwater table is assumed to be at approximately 25

feet bgs at the Site. Layout of the proposed site development is presented in Figure 3. The

current zoning designation is C4-3 (R6 equivalent). The proposed use is consistent with existing

zoning for the property.

1.3 Description of Surrounding Property

The Site is located within a primarily mixed use residential and commercial area of Queens,

New York. The Site is bounded by 24th Avenue to the north, a 3-story residential structure to the

south, 32nd Street to the east, and several residential structures and a commercial deli to the west.

According to the OER Searchable Property Environmental E-Database (SPEED), there is one

sensitive receptor (such as schools, hospitals and day-care facilities) within a 500-foot radius of

the Site. P.S. 85 Judge Charles Vallone is located approximately 250 feet to the north of the Site

at 23-70 31st St.

Figure 2 shows the surrounding land usage.

7

2.0 SITE HISTORY

2.1 Past Uses and Ownership

A Phase I Environmental Site Assessment was performed by Athenica in May 2015.

Historical Sanborn maps show the Site was developed from at least 1915. The Site was shown as

developed with various commercial uses including lamp shade manufacturing and as an

unspecified use warehouse. Portions of the Site are also shown as developed with small

structures designated as “auto” which were most likely former parking garages. Historical City

Directories also list several commercial occupants of the Site including: Terrazzo Flooring Co,

Kovar Products Co, Astoria Novelty Co, C&L Cabinets & Woodturning, Greenlight Energy

Incorporated and Tres Construction.

2.2 Previous Investigations

No previous investigations were performed at the Site except for a geotechnical investigation

dated November 26, 2007 and revised on April 28, 2014. The geotechnical investigation report

was previously submitted to OER.

2.3 Site Inspection

Ms. Ezgi Karayel and Mr. Ethan Rainey of Athenica performed a Site inspection on May 5,

2015. The Site reconnaissance consisted of observing conditions throughout accessible areas of

the Site and around the perimeter of the Site. At the date of the inspection, the Site consisted of

one 2-story building with a partial basement and one 1-story building with no basement. The

buildings were connected internally at the grade level. A concrete covered back yard was located

to the west and a concrete covered front yard was located to the east of the Site.

2.4 Areas of Concern

The AOCs identified for this site include:

1. Presence of urban fill from approximately grade level to 4 feet bgs.

Phase 1 Report is presented in Appendix A. A map showing areas of concern is presented in

Figure 4.

8

3.0 PROJECT MANAGEMENT

3.1 Project Organization

The Qualified Environmental Profession (QEP) responsible for preparation of this RIR is

William Silveri.

3.2 Health and Safety

All work described in this RIR was performed in full compliance with applicable laws and

regulations, including Site and OSHA worker safety requirements and HAZWOPER

requirements.

3.3 Materials Management

All material encountered during the RI was managed in accordance with applicable laws and

regulations.

9

4.0 REMEDIAL INVESTIGATION ACTIVITIES

Athenica performed the following scope of work on behalf of Tres Construction LLC in May

of 2015:

1. Conducted a Site inspection to identify AOCs and physical obstructions (i.e.

structures, buildings, etc.);

2. Performed a ground penetrating radar (GPR) survey;

3. Installed four (4) soil borings across the entire project Site, and collected nine (9) soil

samples for chemical analysis from the soil borings to evaluate soil quality;

4. Monitoring wells could not be installed at the Site due to the Site conditions.

Monitoring wells will be completed after the demolition of the on Site structures and

groundwater quality beneath the Site will be evaluated.

5. Installed two (2) soil vapor probes around Site perimeter and collected two (2)

samples for chemical analysis.

Fieldwork was photo documented. Appendix B provides the investigation photographs.

4.1 Geophysical Investigation

Athenica contracted Ground Penetrating Radar Systems (GPRS) to conduct a geophysical

survey across the Site on May 11, 2015. The purpose of the GPR was to determine if any

anomalies were present at the Site and to clear all sampling locations of any potential subsurface

obstructions. GPRS utilized a 400 MHZ ground penetrating radar (GPR) instrument along

transects approximately two feet apart. The survey was performed in all accessible portions of

the Site. The geophysical survey did not identify any anomalies indicative of an underground

storage tank (UST) at the Site. A copy of the geophysical survey report describing the

methodologies and findings is included in Appendix C.

4.2 Borings and Monitoring Wells

Drilling and Soil Logging

A total of four (4) soil borings were installed using a direct-push drill rig. The borings were

designated SB-1 through SB-4. All the soil borings were installed to 15 feet bgs.

10

From each of the direct-push soil borings, soil samples were continuously collected from

grade to the boring termination depth and screened for evidence of contamination utilizing field

observations (odor and/or staining) and a photoionization detector (PID). A PID makes use of the

principle of photoionization for the detection and qualitative measurement of organic vapors. A

PID does not respond to all compounds similarly, rather, each compound has its own response

factor relative to its calibration. For this investigation, the PID was calibrated to the compound

isobutylene, as published by the manufacturer. No staining or odors were observed in any of the

borings. Only one elevated PID reading of 77.9 ppm was identified in 4 to 6 feet interval at SB-

4. Therefore an additional soil samples is collected from this interval. No other elevated PID

readings were identified at any other soil borings.

Boring logs were prepared by a geologist and are attached in Appendix D. A map showing

the location of soil borings is provided in Figure 5.

Groundwater Monitoring Well Construction

Groundwater monitoring wells could not be installed during the RI due to the Site conditions.

Groundwater monitoring wells will be installed followed by the completion of demolition at the

Site with a special rig. Survey

The locations of soil and soil vapor borings were field measured. Since groundwater

monitoring wells could not be installed during the RI, a land survey is not performed.

Water Level Measurement

Water level could not be measured since monitoring wells could not be installed during the

RI. Water level will be measured upon installation of monitoring wells at the Site followed by

the demolition work. Groundwater depth beneath the Site will be provided to OER upon

determination.

4.3 Sample Collection and Chemical Analysis

Sampling performed as part of the field investigation was conducted for all Areas of Concern

and also considered other means for bias of sampling based on professional judgment, area

history, discolored soil, stressed vegetation, drainage patterns, field instrument measurements,

odor, or other field indicators. All media including soil, groundwater and soil vapor have been

sampled and evaluated in the RIR. Discrete (grab) samples have been used for final delineation

of the nature and extent of contamination and to determine the impact of contaminants on public

11

health and the environment. The sampling performed and presented in this RIR provides

sufficient basis for evaluation of remedial action alternatives, establishment of a qualitative

human health exposure assessment, and selection of a final remedy.

Soil Sampling

A total of nine (9) soil samples were collected for chemical analysis during this RI. One

shallow and one deeper sample were collected from all of the soil borings. One additional soil

sample was collected from SB-4 due to the elevated PID reading of 77 ppm identified at 4 to 6

feet interval. Two more soil borings will be installed followed by the completion of demolition

activities at the Site and minimum of four more soil samples will be collected. Data on soil

sample collection for chemical analyses, including dates of collection and sample depths, is

reported in Tables 1 through 4. Figure 5 shows the location of samples collected in this

investigation. Laboratories and analytical methods are shown below. Soil samples were collected

in pre-cleaned, laboratory supplied glassware, stored in a chilled cooler (4º C) and submitted for

analysis. Soil samples were analyzed at New York State Department of Health ELAP-certified

laboratories. All soil samples were analyzed for the presence of volatile organic compounds

(VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by EPA Method

8270, pesticides/PCBs by EPA Methods 8081/8082, and target analyte list (TAL) metals as well

as trivalent and hexavalent chromium. All samples were transmitted under proper chain of

custody procedures to York Analytical Laboratories, a State-certified (ELAP) laboratory for

confirmatory laboratory analyses.

Groundwater Sampling

Groundwater samples are not collected during this RI since groundwater monitoring wells

could not be installed. Groundwater monitoring wells will be installed and groundwater samples

will be collected followed by the demolition of the on Site structures. Groundwater samples will

be collected utilizing low-flow purging and sampling methods. The groundwater wells will be

purged until water quality parameters, such as turbidity, conductivity, pH, and dissolved oxygen

are stabilized over three consecutive measurements while draw-down during purging is kept to a

minimum (0.3 feet or less). The groundwater samples will be analyzed for the same parameters

as soil samples.

12

Soil Vapor Sampling

Two (2) soil vapor probes were installed and two (2) soil vapor samples were collected for

chemical analysis during this RI. Two (2) more soil vapor borings will be installed and two (2)

more soil vapor samples will be collected followed by the completion of the demolition activities

at the Site. Soil vapor sampling locations are shown in Figure 5. Soil vapor sample collection

data is reported in Table 5. Soil vapor sampling logs are included in Appendix E. Methodologies

used for soil vapor assessment conform to the NYS DOH Final Guidance on Soil Vapor

Intrusion, October 2006.

The soil vapor probes were connected to ¼-inch outer diameter inert Teflon-lined

polyethylene tubing which extended above ground surface to allow for purging and sampling. 72

hours following the installation, approximately three volumes of air was purged from each vapor

probe at a flow rate less than 200 milliliters per minute, and a representative vapor sample was

collected over a four-hour period for laboratory analysis utilizing a 6-liter pre-cleaned SUMMA

canisters. After vapor sampling, each SUMMA cannister was labeled and sent to a laboratory

certified to perform air analysis in New York State and analyzed for VOCs via EPA TO-15.

Chemical Analysis

Chemical analytical work presented in this RIR has been performed in the following manner:

Factor Description

Quality Assurance Officer The chemical analytical quality assurance is directed by William

Silveri

Chemical Analytical

Laboratory

Chemical analytical laboratory used in the RI is NYS ELAP

certified and was York Analytical Laboratories

Chemical Analytical

Methods

Soil analytical methods:

TAL Metals by EPA Method 6010C (rev. 2007);

VOCs by EPA Method 8260C (rev. 2006);

13

SVOCs by EPA Method 8270D (rev. 2007);

Pesticides by EPA Method 8081B (rev. 2000);

PCBs by EPA Method 8082A (rev. 2000);

Soil vapor analytical methods:

VOCs by TO-15 VOC parameters..

Results of Chemical Analyses

Laboratory data for soil and soil vapor are summarized in Tables 1 through 5, respectively.

Laboratory data deliverables for all samples evaluated in this RIR are provided in digital form in

Appendix F and Appendix G.

14

5.0 ENVIRONMENTAL EVALUATION

5.1 Geological and Hydrogeological Conditions

Stratigraphy

The stratigraphy of the Site, from the surface down, consists of approximately 2 to 4 feet of

medium sand with urban fill, underlain by 6 feet of medium sand with pebbles and beneath 10

feet below grade surface underlain by 5 feet of coarse sand and pebbles.

Hydrogeology

Based on the available groundwater data for the vicinity of the Site, the average depth to groundwater is approximately 25 feet bgs and the regional groundwater direction is towards west.

5.2 Soil Chemistry

Soil/fill samples collected during the RI were compared to 6NYCRR Part 375-6.8 Track 1

Unrestricted Soil Cleanup Objectives (SCOs) and Track 2 Restricted Residential Use SCOs. Soil

sampling results showed that there were no detectable concentrations of VOCs except for

acetone, and methylene chloride, both common lab contaminants. Three (3) Polycyclic Aromatic

Hydrocarbon (PAH) SVOCs were detected in one shallow soil (0’-2’) at SB-2 above their

respective Unrestricted Use SCOs and included benzo(a)anthracene (1.34 ppm),

benzo(k)fluoranthene (0.84 ppm), and chrysene (1.25 ppm). Of these only benzo(a)anthracene

exceeded its respective Restricted Residential Use SCO. One Pesticide; 4,4’DDT (max. of

0.0082 ppm) was detected above its Unrestricted Use SCO in one shallow (0’-2’) and one deeper

(4’-6’) soil sample. Total PCBs was detected in one shallow sample at 0.088 ppm, below its

Unrestricted Use SCO. Two (2) metals, including lead (max. of 80.7 ppm) and zinc (119 ppm)

were detected above their respective Unrestricted Use SCOs, but below their respective

Restricted Residential Use SCOs. The results are indicative of historic fill material and they are

contained in the shallow soil beneath the Site.

Data collected during the RI is sufficient to delineate the vertical and horizontal distribution

of contaminants in soil/fill at the Site. A summary table of data for chemical analyses performed

on soil samples is included in Tables 1 through 4. Figure 6 shows the location and posts the

values for soil/fill that exceed the 6NYCRR Part 375-6.8 Track 2 Soil Cleanup Objectives.

15

5.3 Groundwater Chemistry

Groundwater samples could not be collected during the RI and therefore

groundwater chemistry could not be determined. Groundwater quality beneath the Site

will be evaluated upon installation of groundwater monitoring wells followed by the

completion of demolition activities at the Site.

5.4 Soil Vapor Chemistry

Soil vapor samples collected during the RI were compared to the compounds listed in

Vapor Intrusion Matrices in the New York State Department of Health (NYSDOH) Final

Guidance for Evaluating Soil Vapor Intrusion, dated October 2006. Soil vapor results detected

trace levels of petroleum compounds and chlorinated VOCs. Samples did not detect 1,1,1-

trichloroethane, carbon tetrachloride and trichloroethylene (TCE). Tetrachloroethylene (PCE)

was detected in one sample at a concentration of 17 µg/m3. All chlorinated compounds were

below the monitoring and mitigation levels established by NYSDOH matrix. Data collected

during the RI is sufficient to delineate the distribution of contaminants in soil vapor at the Site. A

summary table of data for chemical analyses performed on soil vapor samples is included in

Table 5.

5.5 Prior Activity

Based on an evaluation of the data and information from the RIR, disposal of significant

amounts of hazardous waste is not suspected at this site.

5.6 Impediments to Remedial Action

There are no known impediments to remedial action at this property.

FIGURES

Date:

Drawn by:

Checked by:

Drawing Scale:

Project No.:

MAY 7, 2015

ETHAN RAINEY

EZGI KARAYEL

Site map:

Figure:

Title:

Legend:

15-133-0436

NOT TO SCALE

31-12 24TH AVENUE

QUEENS, NY 11102

1

REMEDIAL INVESTIGATION REPORT

SITE LOCATION MAP

SITE LOCATION

SITE LOCATION

Date:

Drawn by:

Checked by:

Drawing Scale:

Project No.:

MAY 13, 2015

ETHAN RAINEY

EZGI KARAYEL

Site map:

Figure:

Title:

15-133-0436

NOT TO SCALE

31-12 24TH AVENUE

QUEENS, NY 11102

2

REMEDIAL INVESTIGATION REPORT

SITE BOUNDARY MAP

RESIDENTIAL

RESIDENTIAL

RESIDENTIAL

RESIDENTIAL

RESIDENTIAL

SITE

Date:

Drawn by:

Checked by:

Drawing Scale:

Project No.:

MAY 8, 2015

ETHAN RAINEY

EZGI KARAYEL

Site map:

Figure:

Title:

15-133-0436

N.T.S.

31-12 24th Avenue

Queens, NY 11102

3

REMEDIAL INVESTIGATION REPORT

PROPOSED SITE DEVELOPMENT

Date:

Drawn by:

Checked by:

Drawing Scale:

Project No.:

MAY 13, 2015

EZGI KARAYEL

WILLIAM SILVERI

Site map:

Figure:

Title:

Legend:

15-133-0436

N.T.S.

31-12 24TH AVENUE

QUEENS, NY 11102

4

AREAS OF CONCERN

Scale:

32ND STREET

24TH

AVE

NUE

LOT 52

LOT 50

1 Story Building

2 Story Buildingwith a Basement

Existing partial basementfootprint beneath the building

Existing on Site buildings

PRESUMED GROUNDWATER

FLOW DIRECTION

BORING LOCATIONSN.T.S.

Basement

Urban fill from grade level toapproximately 4 feet bgs

Date:

Drawn by:

Checked by:

Drawing Scale:

Project No.:

MAY 13, 2015

EZGI KARAYEL

WILLIAM SILVERI

Site map:

Figure:

Title:

Legend:

15-133-0436

N.T.S.

31-12 24TH AVENUE

QUEENS, NY 11102

5

SAMPLING PLAN

Scale:

32ND STREET

24TH

AVE

NUE

LOT 52

LOT 50

1 Story Building

2 Story Buildingwith a Basement

Existing partial basement beneath the building

Existing on Site buildings

SB-1 / MW-X

SB-4 / MW-X

SB-2 / MW-X

SV-1

SV-2

SB-3

Soil Boring Location and Number

Soil Boring and Monitoring WellLocation and Number

Soil Vapor Boring Location and Number

PRESUMED GROUNDWATER

FLOW DIRECTION

BORING LOCATIONSN.T.S.

Basement

Date:

Drawn by:

Checked by:

Drawing Scale:

Project No.:

MAY 13, 2015

EZGI KARAYEL

WILLIAM SILVERI

Site map:

Figure:

Title:

Notes:

15-133-0436

N.T.S.

31-12 24TH AVENUE

QUEENS, NY 11102

6

EXCEEDANCES IN SOIL SAMPLES

Scale:

32ND STREET

24TH

AVE

NUE

LOT 52

LOT 50

1 Story Building

2 Story Building with aBasement SB-1 / MW-X

SB-4 / MW-X

SB-2 / MW-X

SB-3

BORING LOCATIONSN.T.S.

Basement

Gray highlighted concentrations indicate Track 1 Unrestricted Use SCOExceedances

Orange highlighted concentrations indicate Track 2 Restricted Residential Use SCOExceedances

TABLES

Table 1VOCs in Soil Samples

31-12 24th Avenue, Queens, NY

Sample IDSample DepthLab Sample IDSampling DateDilution FactorSample MatrixUnit of Measure mg/kg mg/kg1,1,1,2‐Tetrachloroethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,1,1‐Trichloroethane 0.68 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,1,2,2‐Tetrachloroethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,1,2‐Trichloro‐1,2,2‐trifluoroethane (Freon 113) NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,1,2‐Trichloroethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,1‐Dichloroethane 0.27 26 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,1‐Dichloroethylene 0.33 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2,3‐Trichlorobenzene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2,3‐Trichloropropane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2,4‐Trichlorobenzene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2,4‐Trimethylbenzene 3.6 52 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2‐Dibromo‐3‐chloropropane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2‐Dibromoethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2‐Dichlorobenzene 1.1 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2‐Dichloroethane 0.02 3.1 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,2‐Dichloropropane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,3,5‐Trimethylbenzene 8.4 52 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,3‐Dichlorobenzene 2.4 49 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,4‐Dichlorobenzene 1.8 13 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND1,4‐Dioxane 0.1 13 0.049 ND 0.050 ND 0.054 ND 0.049 ND 0.044 ND 0.034 ND 0.047 ND 0.045 ND 0.046 ND2‐Butanone 0.12 100 0.0024 ND 0.0025 ND 0.0037 J 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND2‐Hexanone NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 ND4‐Methyl‐2‐pentanone NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDAcetone 0.05 100 0.0050 J 0.0050 ND 0.033 0.0065 J 0.0044 ND 0.0034 ND 0.0070 J 0.011 0.0092Acrolein NC NC 0.0049 ND 0.0050 ND 0.0054 ND 0.0049 ND 0.0044 ND 0.0034 ND 0.0047 ND 0.0045 ND 0.0046 NDAcrylonitrile NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDBenzene 0.06 4.8 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDBromochloromethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDBromodichloromethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDBromoform NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDBromomethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDCarbon disulfide NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDCarbon tetrachloride 0.76 2.4 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDChlorobenzene 1.1 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDChloroethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDChloroform 0.37 49 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDChloromethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDcis‐1,2‐Dichloroethylene 0.25 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDcis‐1,3‐Dichloropropylene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDCyclohexane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDDibromochloromethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDDibromomethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDDichlorodifluoromethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDEthyl Benzene 1 41 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDHexachlorobutadiene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDIsopropylbenzene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDMethyl acetate NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDMethyl tert‐butyl ether (MTBE) 0.93 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDMethylcyclohexane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDMethylene chloride 0.05 100 0.0049 ND 0.0050 ND 0.0089 J 0.0049 ND 0.0044 ND 0.0034 ND 0.0047 ND 0.0045 ND 0.0046 NDn‐Butylbenzene 12 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDn‐Propylbenzene 3.9 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDo‐Xylene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDp‐ & m‐ Xylenes NC NC 0.0049 ND 0.0050 ND 0.0054 ND 0.0049 ND 0.0044 ND 0.0034 ND 0.0047 ND 0.0045 ND 0.0046 NDp‐Isopropyltoluene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDsec‐Butylbenzene 11 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDStyrene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDtert‐Butyl alcohol (TBA) NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDtert‐Butylbenzene 5.9 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDTetrachloroethylene 1.3 19 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDToluene 0.7 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDtrans‐1,2‐Dichloroethylene 0.19 100 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDtrans‐1,3‐Dichloropropylene NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDTrichloroethylene 0.47 21 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDTrichlorofluoromethane NC NC 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDVinyl Chloride 0.02 0.9 0.0024 ND 0.0025 ND 0.0027 ND 0.0025 ND 0.0022 ND 0.0017 ND 0.0023 ND 0.0023 ND 0.0023 NDXylenes, Total 0.26 100 0.0073 ND 0.0075 ND 0.0082 ND 0.0074 ND 0.0066 ND 0.0051 ND 0.0070 ND 0.0068 ND 0.0069 ND

Legendmg/kg - milligrams per kilograms

B ‐ Analyte found in the analysis batch blank

Gray bold and shaded values exceed the Part 375 Unrestricted Use Soil Cleanup Objectives

Notes

0'-2'15E0465‐05

5/12/20151

Soil

13'-15'15E0465‐06

5/12/20151

Soil

5/12/2015 5/12/2015 5/12/2015

1. Evaluation criteria for soil sample results is the NYSDEC Part 375 Value for Unrestricted Use Soil Cleanup Objective and Restricted Residential SCOs

D- Result is from an analysis that required a dilution

J - Analyte detected at or above the method detection limit (MDL)

Soilmg/kg

NC - No criterion for evaluation of analytical parameter

SB‐2

13'-15'15E0465‐04

5/12/20151

15E0465‐07 15E0465‐08 15E0465‐090'-2' 4'-6' 13'-15'

SB‐3 SB‐3 SB‐4 SB‐4 SB‐4

mg/kg mg/kg mg/kgmg/kg mg/kg

1Soil

1Soil

1Soil

5/11/2015

Soil

SB‐1

15E0465‐02

5/11/2015

Soil

0'-2' 13'-15'

ND - Analyte not detected at or above the indicated (reporting limit, method detection limit)

NYSDEC Part 375 Unrestricted Use

Soil Cleanup Objectives

NYSDEC Part 375 Restricted Use Soil Cleanup Objectives -

Restricted Residential

0'-2'

1 1 1

mg/kg mg/kg mg/kg

SB‐2

15E0465‐03

5/12/2015

Soil

SB‐1

15E0465‐01

Table 2SVOCs in Soil Samples

31-12 24th Avenue, Queens, NY

Sample IDSample DepthLab Sample IDSampling DateDilution FactorSample MatrixUnit of Measure mg/kg mg/kg1,1'‐Biphenyl NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND1,2,4,5‐Tetrachlorobenzene NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND1,2,4‐Trichlorobenzene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND1,2‐Dichlorobenzene 1.1 100 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND1,2‐Diphenylhydrazine (as Azobenzene) NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND1,3‐Dichlorobenzene 2.4 49 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND1,4‐Dichlorobenzene 1.8 13 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2,3,4,6‐Tetrachlorophenol NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND2,4,5‐Trichlorophenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2,4,6‐Trichlorophenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2,4‐Dichlorophenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2,4‐Dimethylphenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2,4‐Dinitrophenol NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND2,4‐Dinitrotoluene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2,6‐Dinitrotoluene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2‐Chloronaphthalene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2‐Chlorophenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2‐Methylnaphthalene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2‐Methylphenol 0.33 100 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND2‐Nitroaniline NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND2‐Nitrophenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND3‐ & 4‐Methylphenols NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND3,3'‐Dichlorobenzidine NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND3‐Nitroaniline NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND4,6‐Dinitro‐2‐methylphenol NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND4‐Bromophenyl phenyl ether NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND4‐Chloro‐3‐methylphenol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND4‐Chloroaniline NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND4‐Chlorophenyl phenyl ether NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 ND4‐Nitroaniline NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 ND4‐Nitrophenol NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 NDAcenaphthene 20 100 0.11 ND 0.022 ND 0.14 D 0.022 ND 0.11 ND 0.022 ND 0.076 JD 0.046 ND 0.022 NDAcenaphthylene 100 100 0.11 ND 0.022 ND 0.13 D 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDAcetophenone NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDAniline NC NC 0.44 ND 0.086 ND 0.18 ND 0.087 ND 0.43 ND 0.086 ND 0.19 ND 0.18 ND 0.087 NDAnthracene 100 100 0.11 ND 0.022 ND 0.73 D 0.022 ND 0.11 ND 0.022 ND 0.13 D 0.046 ND 0.022 NDAtrazine NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBenzaldehyde NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBenzidine NC NC 0.44 ND 0.086 ND 0.18 ND 0.087 ND 0.43 ND 0.086 ND 0.19 ND 0.18 ND 0.087 NDBenzo(a)anthracene 1 1 0.11 ND 0.022 ND 1.34 D 0.022 ND 0.11 ND 0.022 ND 0.32 D 0.046 ND 0.022 NDBenzo(a)pyrene 1 1 0.11 ND 0.022 ND 0.76 D 0.022 ND 0.11 ND 0.022 ND 0.11 D 0.046 ND 0.022 NDBenzo(b)fluoranthene 1 1 0.11 ND 0.022 ND 0.67 D 0.022 ND 0.11 ND 0.022 ND 0.12 D 0.046 ND 0.022 NDBenzo(g,h,i)perylene 100 100 0.11 ND 0.022 ND 0.33 D 0.022 ND 0.11 ND 0.022 ND 0.097 D 0.046 ND 0.022 NDBenzo(k)fluoranthene 0.8 3.9 0.11 ND 0.022 ND 0.84 D 0.022 ND 0.11 ND 0.022 ND 0.13 D 0.046 ND 0.022 NDBenzoic acid NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBenzyl alcohol NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBenzyl butyl phthalate NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBis(2‐chloroethoxy)methane NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBis(2‐chloroethyl)ether NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBis(2‐chloroisopropyl)ether NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDBis(2‐ethylhexyl)phthalate NC NC 0.11 ND 0.041 J 0.59 D 0.025 J 0.13 JD 0.042 J 0.34 D 0.054 JD 0.042 JCaprolactam NC NC 0.22 ND 0.043 ND 0.089 ND 0.043 ND 0.21 ND 0.043 ND 0.095 ND 0.091 ND 0.044 NDCarbazole NC NC 0.11 ND 0.022 ND 0.21 D 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDChrysene 1 3.9 0.17 JD 0.022 ND 1.25 D 0.022 ND 0.15 JD 0.022 ND 0.33 D 0.17 D 0.022 NDDibenzo(a,h)anthracene 0.33 0.33 0.11 ND 0.022 ND 0.17 D 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDDibenzofuran 7 59 0.11 ND 0.022 ND 0.11 D 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDDiethyl phthalate NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDDimethyl phthalate NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDDi‐n‐butyl phthalate NC NC 0.11 ND 0.022 ND 0.69 D 0.038 J 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.12Di‐n‐octyl phthalate NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDFluoranthene 100 100 0.16 JD 0.022 ND 2.62 D 0.022 ND 0.16 JD 0.022 ND 0.76 D 0.25 D 0.022 NDFluorene 30 100 0.11 ND 0.026 J 0.31 D 0.022 ND 0.11 ND 0.022 ND 0.082 JD 0.046 ND 0.022 NDHexachlorobenzene 0.33 1.2 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDHexachlorobutadiene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDHexachlorocyclopentadiene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDHexachloroethane NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDIndeno(1,2,3‐cd)pyrene 0.5 0.5 0.11 ND 0.022 ND 0.38 D 0.022 ND 0.11 ND 0.022 ND 0.075 JD 0.046 ND 0.022 NDIsophorone NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDNaphthalene 12 100 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDNitrobenzene NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDN‐Nitrosodimethylamine NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDN‐nitroso‐di‐n‐propylamine NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDN‐Nitrosodiphenylamine NC NC 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDPentachlorophenol 0.8 6.7 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDPhenanthrene 100 100 0.11 ND 0.022 ND 2.21 D 0.022 ND 0.11 ND 0.022 ND 0.52 D 0.22 D 0.022 NDPhenol 0.33 100 0.11 ND 0.022 ND 0.045 ND 0.022 ND 0.11 ND 0.022 ND 0.048 ND 0.046 ND 0.022 NDPyrene 100 100 0.15 JD 0.022 ND 2.18 D 0.022 ND 0.13 JD 0.022 ND 0.82 D 0.21 D 0.022 ND

Legendmg/kg - milligrams per kilograms

Gray bold and shaded values exceed the Part 375 Unrestricted Use Soil Cleanup ObjectivesOrange bold and shaded values exceed the Part 375 Restricted Residential Soil Cleanup ObjectivesNotes

Soil Soil Soilmg/kg

1. Evaluation criteria for soil sample results is the NYSDEC Part 375 Value for Unrestricted Use Soil Cleanup Objective and Restricted Residential SCOs

D- Result is from an analysis that required a dilution

mg/kg mg/kg mg/kg mg/kg mg/kgSoil Soil Soil

15E0465‐09

5/12/2015 5/12/2015 5/12/2015 5/12/2015 5/12/2015 5/12/201515E0465‐04 15E0465‐05 15E0465‐06 15E0465‐07 15E0465‐08

SB‐4

13'-15' 0'-2' 13'-15' 0'-2' 4'-6' 13'-15'SB‐2 SB‐3 SB‐3 SB‐4 SB‐4

5/11/2015 5/12/2015

13'-15' 0'-2'15E0465‐01 15E0465‐02 15E0465‐03

NC - No criterion for evaluation of analytical parameter

ND - Analyte not detected at or above the indicated (reporting limit, method detection limit)

J - Analyte detected at or above the method detection limit (MDL)

Soil Soil Soilmg/kg mg/kg mg/kg

NYSDEC Part 375 Unrestricted Use

Soil Cleanup Objectives

NYSDEC Part 375 Restricted Use Soil

Cleanup Objectives -Restricted Residential

SB‐1 SB‐1 SB‐2

0'-2'

5/11/20151 2 2 15 1 2 1 5

Table 3Pesticides and PCBs in Soil Samples

31-12 24th Avenue, Queens, NY

Sample IDSample DepthLab Sample IDSampling DateDilution FactorSample MatrixUnit of Measure mg/kg mg/kg4,4'‐DDD 0.0033 13 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 ND4,4'‐DDE 0.0033 8.9 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0025 D 0.0021 D 0.0017 ND4,4'‐DDT 0.0033 7.9 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0082 D 0.0039 D 0.0017 NDAldrin 0.005 0.097 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDalpha‐BHC 0.02 0.48 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDalpha‐Chlordane 0.094 4.2 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0064 D 0.0023 D 0.0017 NDbeta‐BHC 0.036 0.36 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDChlordane, total NC NC 0.070 ND 0.068 ND 0.071 ND 0.069 ND 0.068 ND 0.068 ND 0.075 ND 0.072 ND 0.069 NDdelta‐BHC 0.04 100 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDDieldrin 0.005 0.2 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDEndosulfan I 2.4 24 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDEndosulfan II 2.4 24 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDEndosulfan sulfate 2.4 24 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDEndrin 0.014 11 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDEndrin aldehyde NC NC 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDEndrin ketone NC NC 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDgamma‐BHC (Lindane) 0.1 1.3 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDgamma‐Chlordane NC NC 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0082 D 0.0039 D 0.0017 NDHeptachlor 0.042 2.1 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDHeptachlor epoxide NC NC 0.0018 ND 0.0017 ND 0.0018 ND 0.0017 ND 0.0017 ND 0.0017 ND 0.0019 ND 0.0018 ND 0.0017 NDMethoxychlor NC NC 0.0087 ND 0.0085 ND 0.0088 ND 0.0086 ND 0.0085 ND 0.0085 ND 0.0094 ND 0.0090 ND 0.0086 NDToxaphene NC NC 0.088 ND 0.086 ND 0.089 ND 0.087 ND 0.086 ND 0.086 ND 0.095 ND 0.091 ND 0.087 NDDilution FactorAroclor 1016 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.026 0.018 ND 0.017 NDAroclor 1221 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.019 ND 0.018 ND 0.017 NDAroclor 1232 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.019 ND 0.018 ND 0.017 NDAroclor 1242 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.019 ND 0.018 ND 0.017 NDAroclor 1248 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.019 ND 0.018 ND 0.017 NDAroclor 1254 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.062 0.018 ND 0.017 NDAroclor 1260 NC NC 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.019 ND 0.018 ND 0.017 NDTotal PCBs 0.1 1 0.018 ND 0.017 ND 0.018 ND 0.017 ND 0.017 ND 0.017 ND 0.088 0.018 ND 0.017 NDLegendmg/kg - milligrams per kilograms

NotesGray bold and shaded values exceed the Part 375 Unrestricted Use Soil Cleanup Objectives

5 5

1 1 1 1

mg/kgSoil

mg/kg mg/kg mg/kg mg/kg mg/kgSoilSoil Soil Soil

5 5 5 5 5

1 1 1 1 1

Soil

15E0465‐09

5/12/2015 5/12/2015 5/12/2015 5/12/2015 5/12/2015 5/12/201515E0465‐04 15E0465‐05 15E0465‐06 15E0465‐07 15E0465‐08

5SoilSoil

SB‐4

13'-15' 0'-2' 13'-15' 0'-2' 4'-6' 13'-15'SB‐2 SB‐3 SB‐3 SB‐4 SB‐4

Soil

1. Evaluation criteria for soil sample results is the NYSDEC Part 375 Value for Unrestricted Use Soil Cleanup Objective and Restricted Residential SCOs

15E0465‐03

5/11/2015 5/11/2015 5/12/2015

NYSDEC Part 375 Unrestricted Use

Soil Cleanup Objectives

NYSDEC Part 375 Restricted Use Soil Cleanup Objectives -

Restricted Residential

SB‐1 SB‐1 SB‐2

0'-2' 13'-15' 0'-2'15E0465‐01 15E0465‐02

5

NC - No criterion for evaluation of analytical parameter

ND - Analyte not detected at or above the indicated (reporting limit, method detection limit)

mg/kg mg/kg mg/kg

Table 4TAL Metals in Soil Samples

31-12 24th Avenue, Queens, NY

Sample IDSample DepthLab Sample IDSampling DateDilution FactorSample MatrixUnit of Measure mg/kg mg/kgAluminum NC NC 5,080 4,990 7,160 6,650 6,410 3,480 6,720 5,060 5,520Antimony NC NC 1.11 0.52 ND 0.53 ND 0.52 ND 0.51 ND 0.52 ND 0.61 0.55 ND 0.52 NDArsenic 13 16 1.86 1.58 2.60 2.13 2.33 1.29 4.03 1.93 1.48Barium 350 400 56 29.40 57.50 45.50 62.50 25 71.50 67.40 46.10Beryllium 7.2 72 0.11 ND 0.10 ND 0.11 ND 0.10 ND 0.10 ND 0.10 ND 0.11 ND 0.11 ND 0.11 NDCadmium 2.5 4.3 0.34 0.31 ND 0.32 ND 0.31 ND 0.31 ND 0.31 ND 0.44 0.33 ND 0.31 NDCalcium NC NC 16,400 2,190 16,900 3,160 4,560 1,090 44,600 20,200 2,420Chromium NC NC 14 17 18.50 23.30 14.10 9.87 15.40 14.50 15.80Chromium, Hexavalent 1 110 0.53 ND 0.52 ND 0.53 ND 0.52 ND 0.51 ND 0.52 ND 0.57 ND 0.55 ND 0.52 NDChromium, Trivalent 30 180 14 17 18.50 23.30 14.10 9.87 15.40 14.50 15.80Cobalt NC NC 4.79 5.42 6.26 7.09 7.08 4.11 5.31 4.95 5.87Copper 50 270 34 25.50 29.10 24 38.90 12.60 34.30 29.50 35.60Iron NC NC 11,300 11,500 14,300 14,400 16,300 9,730 12,800 13,100 13,000Lead 63 400 80.70 2.63 50.70 4.79 55.20 2.53 69.50 79.90 4.10Magnesium NC NC 7,290 2,300 3,050 2,840 3,260 1,970 7,350 3,050 2,400Manganese 1,600 2,000 254 193 291 249 326 182 205 232 357Mercury 0.18 0.81 0.11 0.031 ND 0.042 0.031 ND 0.031 ND 0.031 ND 0.050 0.033 ND 0.031 NDNickel 30 310 13.60 11 14 12.90 12 9.49 13.90 12.40 10.60Potassium NC NC 721 781 1,110 1,040 1,310 543 696 831 1,070Selenium 3.9 180 1.65 1.09 1.93 2.33 1.62 1.03 ND 1.96 1.99 1.49Silver 2 180 0.53 ND 0.52 ND 0.53 ND 0.52 ND 0.51 ND 0.52 ND 0.57 ND 0.55 ND 0.52 NDSodium NC NC 236 360 214 437 280 110 245 173 325Thallium NC NC 1.06 ND 1.03 ND 1.07 ND 1.04 ND 1.03 ND 1.03 ND 1.14 ND 1.10 ND 1.05 NDVanadium NC NC 24.40 28.20 33.30 28.50 34.20 16.60 31.80 26.60 27Zinc 109 10,000 84 15.90 90.10 35 69.30 23.10 113 51.40 23.30Legendmg/kg - milligrams per kilograms

Gray bold and shaded values exceed the Part 375 Unrestricted Use Soil Cleanup ObjectivesNotes1. Evaluation criteria for soil sample results is the NYSDEC Part 375 Value for Unrestricted Use Soil Cleanup Objective and Restricted Residential SCOs

mg/kg

NC - No criterion for evaluation of analytical parameter

ND - Analyte not detected at or above the indicated (reporting limit, method detection limit)

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgSoil

1 1 1 1 1Soil Soil Soil Soil Soil

5/12/201515E0465‐04 15E0465‐05 15E0465‐06 15E0465‐07 15E0465‐08

SB‐4 SB‐4

5/12/2015 5/12/2015 5/12/2015 5/12/2015 5/12/20151 1

15E0465‐01 15E0465‐02

SB‐4

15E0465‐09

1

13'-15' 0'-2' 13'-15' 0'-2' 4'-6' 13'-15'SB‐2 SB‐3 SB‐3

NYSDEC Part 375 Unrestricted Use

Soil Cleanup Objectives

NYSDEC Part 375 Restricted Use Soil

Cleanup Objectives -Restricted Residential

SB‐1 SB‐1 SB‐2

0'-2' 13'-15' 0'-2'

Soil Soil Soil

15E0465‐03

5/11/2015 5/11/2015 5/12/20151

Table 5VOCs in Soil Vapor Samples

31‐12 24th Avenue, Queens, NY

Sample IDLab Sample IDSampling DateDilution FactorSample MatrixUnit of Measure1,1,1,2‐Tetrachloroethane NC 14 ND 17 ND1,1,1‐Trichloroethane 100 11 ND 13 ND1,1,2,2‐Tetrachloroethane NC 14 ND 17 ND1,1,2‐Trichloro‐1,2,2‐trifluoroethane (Freon 113) NC 15 ND 19 ND1,1,2‐Trichloroethane NC 11 ND 13 ND1,1‐Dichloroethane NC 8.20 ND 10 ND1,1‐Dichloroethylene NC 8 ND 9.70 ND1,2,4‐Trichlorobenzene NC 15 ND 18 ND1,2,4‐Trimethylbenzene NC 9.90 ND 12 ND1,2‐Dibromoethane NC 15 ND 19 ND1,2‐Dichlorobenzene NC 12 ND 15 ND1,2‐Dichloroethane NC 8.20 ND 10 ND1,2‐Dichloropropane NC 9.30 ND 11 ND1,2‐Dichlorotetrafluoroethane NC 14 ND 17 ND1,3,5‐Trimethylbenzene NC 9.90 ND 12 ND1,3‐Butadiene NC 8.70 ND 170 D1,3‐Dichlorobenzene NC 12 ND 15 ND1,3‐Dichloropropane NC 9.30 ND 11 ND1,4‐Dichlorobenzene NC 12 ND 180 D1,4‐Dioxane NC 7.30 ND 8.90 ND2‐Butanone NC 120 D 250 D2‐Hexanone NC 17 ND 44 D3‐Chloropropene NC 6.30 ND 7.70 ND4‐Methyl‐2‐pentanone NC 8.30 ND 10 NDAcetone NC 960 D 5,000 DEAcrylonitrile NC 4.40 ND 5.30 NDBenzene NC 6.40 ND 16 DBenzyl chloride NC 10 ND 13 NDBromodichloromethane NC 13 ND 15 NDBromoform NC 21 ND 25 NDBromomethane NC 7.80 ND 9.50 NDCarbon disulfide NC 6.30 ND 12 DCarbon tetrachloride 5 3.20 ND 3.90 NDChlorobenzene NC 9.30 ND 11 NDChloroethane NC 5.30 ND 6.50 NDChloroform NC 9.80 ND 13 DChloromethane NC 17 D 5.10 NDcis‐1,2‐Dichloroethylene NC 8 ND 9.70 NDcis‐1,3‐Dichloropropylene NC 9.10 ND 11 NDCyclohexane NC 6.90 ND 8.50 NDDibromochloromethane NC 16 ND 20 NDDichlorodifluoromethane NC 10 ND 12 NDEthyl acetate NC 15 ND 18 NDEthyl Benzene NC 8.80 ND 11 NDHexachlorobutadiene NC 22 ND 26 NDIsopropanol NC 9.90 ND 36 DMethyl Methacrylate NC 8.30 ND 10 NDMethyl tert‐butyl ether (MTBE) NC 7.30 ND 8.90 NDMethylene chloride NC 14 ND 17 NDn‐Heptane NC 8.30 ND 29 Dn‐Hexane NC 7.10 ND 47 Do‐Xylene NC 8.80 ND 11 NDp‐ & m‐ Xylenes NC 18 ND 21 NDp‐Ethyltoluene NC 9.90 ND 12 NDPropylene NC 79 D 850 DStyrene NC 8.60 ND 10 NDTetrachloroethylene 100 3.40 ND 17 DTetrahydrofuran NC 61 D 80 DToluene NC 7.60 ND 11 Dtrans‐1,2‐Dichloroethylene NC 8 ND 9.70 NDtrans‐1,3‐Dichloropropylene NC 9.10 ND 11 NDTrichloroethylene 5 2.70 ND 3.30 NDTrichlorofluoromethane (Freon 11) NC 11 ND 14 NDVinyl acetate NC 7.10 ND 8.70 NDVinyl bromide NC 8.80 ND 11 NDVinyl Chloride NC 1.30 ND 1.60 NDLegendNC ‐ No criterion for evaluation of analytical parameterND ‐ Analyte not detected at or above the level indicatedD ‐ Result is from an analysis that required a dilution

Note:Evaluation criteria for soil vapor is the sub‐slub vapor concentration for the Matrix 1 and Matrix 2 compounds presented in the NYSDOH Soil Vapor Intrusion Guidance document dated October 2006

NYS DOH Sub‐Slab and Soil Vapor 

Evaluation Criteria20.16 24.59

Soil Vapor Soil Vaporug/m3 ug/m3

SV‐115E0464‐015/12/2015

SV‐215E0464‐025/12/2015

APPENDICES

APPENDIX A

PHASE I ESA REPORT

APPENDIX B

PHOTOGRAPHS

APPENDIX C

GPR REPORT

Page | 1 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

May 12, 2015

ATTN: Ezgi Karayel

Athenica Environmental Services, INC.

45-09 Greenpoint Avenue

Long Island City, New York 11104

(718)-784-7490

Subject: Ground Penetrating Radar (GPR) scanning of 31-12 24th

Ave. Queens, NY

Lead Technician: Josh Elam

Project Manager of NY/NJ/CT Tri-State Region

Ground Penetrating Radar Systems, Inc.

New York/Long Island (631)-241-2261

[email protected]

Table of Contents

1. Overview of GPR

2. Equipment & Capabilities

3. Site Description

4. Inspection Methods

5. Findings

6. Qualifications

7. Closing

Page | 2 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

1. Overview of GPR Ground Penetrating Radar (GPR) is a non-destructive testing technology that sends a

series of radar pulses into the surface which reflect back off of anomalies below. As the radar

pulses through the ground, the waves bend slightly when encountering a material with differing

physical properties, particularly density and conductivity. Thousands of pulses are sent and

received in a small area, and the received signals are combined to form a real-time image of what

is in the ground. The various places where the radar waves bend are displayed as anomalies

which can be interpreted as utilities, steel pipes, PVC conduits, underground storage tanks, voids,

foundations, etc. One of the many advantages of the technology is the ability to locate metal and

non-metallic objects as well as determining depth to the object. GPR data acquisition is very fast

and results are available immediately, allowing any discovered anomalies to be marked directly

in the field. Although confused with X-Ray, GPR uses less than 1% of your cell phones

radiation emissions and is safe to work with human presence in close proximity.

2. Equipment and Capabilities Ground Penetrating Radar (GPR)

GSSI SIR-3000

-GPRS uses a Geophysical Survey Systems Inc. (GSSI) SIR-3000 radar unit. This is the most

advanced GPR available. It allows for on-site interpretation, as well as stored data for later

processing. This equipment is self-calibrating, allowing more precise depth and location

measurements.

-GSSI is the world’s leading GPR designer and manufacturer. Information can be found at

www.geophysical.com.

400 MHZ GSSI Antenna

-For utility locating, we use a 400MHz antenna with the SIR-3000 GPR head unit. This antenna

allows data collection to a maximum depth of approximately 5-8 feet, depending on soil

conditions.

3. Site Description At 31-24 24

th Ave. Queens, NY the primary objective was to scan and clear 10 soil boring

locations. The soil boring locations were located in the exterior and interior of the facility.

4. Inspection Methods Since the surface was outside and the scans were performed every two feet, our 400MHz antenna

was utilized. When scanning the concerned locations, we performed North-South and East-West

scans to ensure the locations that each was soil boring location was cleared of any utilities or

other obstructions.

Page | 3 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

5. Findings When scanning the site, the depth penetration of the radar was limited to 4 feet. The 10 areas of

concern were identified, marked, and cleared of any utilities or other obstructions. Each soil

boring location was marked with a white dot and numbered. Below is a screen shot taken from

the SIR-3000 and photographs taken on site.

The above screen shot and corresponding photo was taken from the SIR-3000 with the 400MHZ

antenna from the site showing no signs of any obstructions and a depth of approximately 4ft.

There are 2 gauges in each screen shot. The left side gives the technician the depth of each

obstruction while the top allows you to see the distance of each scan performed.

Page | 4 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

Page | 5 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

Page | 6 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

Page | 7 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

Page | 8 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

Page | 9 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

6. Qualifications Ground Penetrating Radar Systems, Inc. (GPRS) was founded in October 2001 by Matt

Aston, who engrained a philosophy of client service and data accuracy. Matt’s primary intent in

starting the business was to give contractors a reliable way to scan into concrete and foundational

slabs in order to avoid cutting embedded electrical conduits and critical reinforcing steel. These

are immensely important services in the construction business as it helps to maintain structural

integrity and avoid major human error leading to increasing costs and man hours. Obviously, in

a field with such dramatic implications, reliability and credibility are the cornerstones. While

GPRS performs this type work on a regular basis, there are many other applications in which our

services can be deployed and as we have grown over the past decade, we have become industry

leaders in the nuances of GPR in specific circumstances, including the scanning of cemeteries

and burial plots.

Since our inception, GPRS has grown to a nationwide enterprise and has completed over six

thousand projects. This success is due to our high level of customer service coupled with our

unique market position. Unlike many other companies that provide GPR services, GPRS offers

no ancillary services and therefore our field operators are able to dedicate 100% of their time and

effort in perfecting this particular tradecraft. Indicative of our dedication to this function is the

fact that we are the only national GPR Company specializing solely in this service. We perform

GPR services every day in a variety of complex and often unique environments. This gives us

familiarity with environments and in situations that other firms would find foreign. Further, this

is not something we do once in a while; our technicians are in the field every day. We are very

proud of this dedication to our craft and of our performance record. Additionally, in our twelve

years in business we have maintained a record of zero recordables (essentially remaining

incident free). To statistically quantify our reliability, we have had a reported incident of error

on less than one percent of the projects we have completed. Our customers have expressed a

high level of satisfaction, as evidenced by the fact that in 2012 nearly 80% of our business was

either repeat clients or referred by our customers. To demonstrate our environmental experience,

GPRS has been involved in projects ranging from small residential jobs to major construction

projects with values in excess of $4 Billion.

Every one of our technicians is required to undergo over five months of both classroom and

apprentice training to ensure that they are highly proficient in the scanning process and in the

interpretation of results. Each member of our team is intensely scrutinized prior to independent

field deployment and those individuals who do not meet our standards are not permitted to

operate our equipment nor analyze field results. Additionally, we include an internal audit

process involving other analysts when dealing with a particularly sensitive job. This is to

maintain our high level of standards and ensure the continuing credibility of our services.

Page | 10 Josh Elam Ground Penetrating Radar Systems

631-241-2261

[email protected]

7. Closing Thank you for the opportunity to serve you on this project. I hope this report has answered all

the questions you had regarding this survey. However if there is anything you have questions

about or feel was omitted, please do not hesitate to contact me.

Thank you,

Josh Elam

Project Manager of the NY/NJ/CT Tristate Region

Ground Penetrating Radar Systems, Inc.

New York/Long Island 631-241-22

[email protected]

APPENDIX D

SOIL BORING LOGS

Client:   Boring Number: SB‐1Tres Construction, LLCJob Name:  31‐12 24th Avenue Boring Location:

Job Number:  15‐133‐0436

Field Representatives:

Groundwater Observations: Casing Sampler Type: Date Start: 05/11/2015Geoprobe 6712 Date Completed: 05/11/2015

Depth (bgs)Recovery 

(in.)Density or Moist

PID (ppm)

0' 6" ‐ Asphalt18" ‐ Black SAND some ash some gravel (Historic Fill)

2' Light brown medium grained SAND (Native)

4'

6'

8'

10'

12'

14'

15' (boring termination depth)G = Grab sample collected for analysisbgs = Below Ground Surface

=samples submitted to laboratory for analysis

Northern portion of the Site45‐09 Greenpoint Avenue                                                                             Long Island City, New York, 11104Phone: 718‐784‐7490  Fax: 718‐784‐4085

Location:   31‐12 24th Avenue, Queens, NY, 11102

Ethan Rainey

No

Sample Number   Type

Field Identification of Soil / Remarks

SB‐1 (0'‐2') G 24" Dry 0.0

Same as above

SB‐1 (2'‐4') 24" Dry 0.0

SB‐1 (4'‐6') 24" Dry 0.0

Dark brown coarse SAND some pebbles

SB‐1 (6'‐8') 24" Dry 0.0

Same as above

SB‐1 (8'‐10') 24" Dry 0.0

Light brown coarse SAND and pebbles

*Grab sample from 13' ‐ 15'

SB‐1 (10'‐12') 24" Dry 0.0

Same as above

SB‐1 (12'‐14') G 24" Dry 0.0

Same as above

SB‐1 (14'‐15') G 24" Dry 0.0

Client:   Boring Number: SB‐2Tres Construction, LLCJob Name:  31‐12 24th Avenue Boring Location:

Job Number:  15‐133‐0436

Field Representatives:

Groundwater Observations: Casing Sampler Type: Date Start: 05/12/2015Geoprobe 6712 Date Completed: 05/12/2015

Depth (bgs)Recovery 

(in.)Density or Moist

PID (ppm)

0' 6" ‐ Concrete18" ‐ Dark brown medium grained SAND (native)

2' Same as above

4'

6'

8'

10'

12'

14'

15' (boring termination depth)G = Grab sample collected for analysisbgs = Below Ground Surface

=samples submitted to laboratory for analysis

Same as above

SB‐2 (12'‐14') G 24" Dry 0.0

Light brown coarse SAND and pebbles

*Grab sample from 13' ‐ 15'

SB‐2 (14'‐15') G 24" Dry 0.0

Same as above

SB‐2 (8'‐10') 24" Dry 0.0

Dark brown coarse SAND some pebbles

SB‐2 (10'‐12') 24" Dry 0.0

Same as above

SB‐2 (4'‐6') 24" Dry 0.0

Same as above

SB‐2 (6'‐8') 24" Dry 0.0

No

Sample Number   Type

Field Identification of Soil / Remarks

SB‐2 (0'‐2') G 24" Dry 0.0

SB‐2 (2'‐4') 24" Dry 0.0

South western portion of the Site45‐09 Greenpoint Avenue                                                                             Long Island City, New York, 11104Phone: 718‐784‐7490  Fax: 718‐784‐4085

Location:   31‐12 24th Avenue, Queens, NY, 11102

Ethan Rainey

Client:   Boring Number: SB‐3Tres Construction, LLCJob Name:  31‐12 24th Avenue Boring Location:

Job Number:  15‐133‐0436

Field Representatives:

Groundwater Observations: Casing Sampler Type: Date Start: 05/12/2015Geoprobe 6712 Date Completed: 05/12/2015

Depth (bgs)Recovery 

(in.)Density or Moist

PID (ppm)

0' Black medium grained SAND some ash some gravel (Historic fill)

2' Light brown medium SAND some pebbles (Native)

4'

6'

8'

10'

12'

14'

15' (boring termination depth)G = Grab sample collected for analysisbgs = Below Ground Surface

=samples submitted to laboratory for analysis

Eastern portion of the Site45‐09 Greenpoint Avenue                                                                             Long Island City, New York, 11104Phone: 718‐784‐7490  Fax: 718‐784‐4085

Location:   31‐12 24th Avenue, Queens, NY, 11102

Ethan Rainey

No

Sample Number   Type

Field Identification of Soil / Remarks

SB‐3 (0'‐2') G 24" Dry 0.0

SB‐3 (2'‐4') 24" Dry 0.0

Brown SAND some silt some pebbles

SB‐3 (4'‐6') 24" Dry 0.0

Same as above

SB‐3 (6'‐8') 24" Dry 0.0

Light brown coarse SAND and pebbles

SB‐3 (8'‐10') 24" Dry 0.0

Same as above

SB‐3 (10'‐12') 24" Dry 0.0

Same as above

SB‐3 (12'‐14') G 24" Dry 0.0

Same as above

*Grab sample from 13' ‐ 15'

SB‐3 (14'‐15') G 24" Dry 0.0

Client:   Boring Number: SB‐4Tres Construction, LLCJob Name:  31‐12 24th Avenue Boring Location:

Job Number:  15‐133‐0436

Field Representatives:

Groundwater Observations: Casing Sampler Type: Date Start: 05/12/2015Geoprobe 6712 Date Completed: 05/12/2015

Depth (bgs)Recovery 

(in.)Density or Moist

PID (ppm)

0' Black medium grained SAND some ash some gravel (Historic fill)

2' Same as above

4'

6'

8'

10'

12'

14'

15' (boring termination depth)G = Grab sample collected for analysisbgs = Below Ground Surface

=samples submitted to laboratory for analysis

Eastern portion of the Site45‐09 Greenpoint Avenue                                                                             Long Island City, New York, 11104Phone: 718‐784‐7490  Fax: 718‐784‐4085

Location:   31‐12 24th Avenue, Queens, NY, 11102

Ethan Rainey

No

Sample Number   Type

Field Identification of Soil / Remarks

SB‐4 (0'‐2') G 24" Dry 0.0

SB‐4 (2'‐4') 24" Dry 0.0

Same as above

SB‐4 (4'‐6') G 24" Dry 77.9

Light brown medium SAND some pebbles (Native)

SB‐4 (6'‐8') 24" Dry 0.0

Light brown coarse SAND and pebbles 

SB‐4 (8'‐10') 24" Dry 0.0

Same as above

SB‐4 (10'‐12') 24" Dry 0.0

Same as above

SB‐4 (12'‐14') G 24" Dry 0.0

Same as above

*Grab sample from 13' ‐ 15'

SB‐4 (14'‐15') G 24" Dry 0.0

APPENDIX E

SOIL VAPOR SAMPLING LOG

E‐Designation Remedial Investigation ‐ Soil Vapor Log31‐12 24th Avenue, Queens, NY 

Start Sampling Time

‐30

Canister Pressure in Field ("Hg") (Stop)

‐30

Stop Sampling Time

Canister Pressure in Field ("Hg") (Start)

Sample ID Sample DateFlow 

Controller Readout 

SV‐1 (22)

‐10

< 0.2 L/min

5/12/2015 < 0.2 L/min 11:15

‐710:15 14:30

15:00

5/12/2015

SV‐2 (S13)

APPENDIX F

LABORATORY ANALYTICAL RESULTS FOR SOIL SAMPLES

Technical Report

prepared for:

Athenica Environmental Services, Inc.45-09 Greenpoint Avenue

Long Island City NY, 11104

Attention: Ezgi Karayel

Report Date: 05/13/2015

Client Project ID: 15-133-0436 / 31-12 24th Ave.

York Project (SDG) No.: 15E0465

CT Cert. No. PH-0723 New Jersey Cert. No. CT-005 New York Cert. No. 10854 PA Cert. No. 68-04440

120 RESEARCH DRIVE FAX (203) 357-0166(203) 325-1371STRATFORD, CT 06615

Page 1 of 104

Client Sample IDYork Sample ID Matrix Date Collected Date Received

SB-1 (0-2')15E0465-01 Soil 05/11/2015 05/12/2015

SB-1 (13'-15')15E0465-02 Soil 05/11/2015 05/12/2015

SB-2 (0'-2')15E0465-03 Soil 05/12/2015 05/12/2015

SB-2 (13'-15')15E0465-04 Soil 05/12/2015 05/12/2015

SB-3 (0'-2')15E0465-05 Soil 05/12/2015 05/12/2015

SB-3 (13'-15')15E0465-06 Soil 05/12/2015 05/12/2015

SB-4 (0'-2')15E0465-07 Soil 05/12/2015 05/12/2015

SB-4 (4'-6')15E0465-08 Soil 05/12/2015 05/12/2015

SB-4 (13'-15')15E0465-09 Soil 05/12/2015 05/12/2015

Client Project ID: 15-133-0436 / 31-12 24th Ave.

York Project (SDG) No.: 15E0465

Report Date: 05/13/2015

Attention: Ezgi Karayel

Long Island City NY, 11104

45-09 Greenpoint Avenue

Athenica Environmental Services, Inc.

Purpose and Results

This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory

on May 12, 2015 and listed below. The project was identified as your project: 15-133-0436 / 31-12 24th Ave..

The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data

summary tables.

All samples were received in proper condition meeting the customary acceptance requirements for environmental samples

except those indicated under the Notes section of this report.

All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,

the meaning of which are explained in the attachment to this report, and case narrative if applicable.

The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the

following pages.

Please contact Client Services at 203.325.1371 with any questions regarding this report.

[TOC_1] Introduction and Sample Cross Reference [

Page 2 of 104

General Notes for York Project (SDG) No.: 15E0465

1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to

the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest

standard utilized for the calibration where applicable.

2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.

3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .

4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.

5. All samples were received in proper condition for analysis with proper documentation, unless otherwise noted.

6. All analyses conducted met method or Laboratory SOP requirements. See the Qualifiers and/or Narrative sections for further information.

7. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.

8. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.

Approved By:

Laboratory Director

Date: 05/13/2015

Benjamin Gulizia

OC_2]General Notes Relating to this Report[TOC]

Page 3 of 104

SB-1 (0-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-1 (0-2')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 SS05/13/2015 08:42 05/13/2015 12:029749 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_1]Sample Results[TOC]

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 4 of 104

SB-1 (0-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1591-78-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

5.0 ug/kg dry 167-64-1 SS05/13/2015 08:42 05/13/2015 12:029.74.9 EPA 8260CAcetone J

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 SS05/13/2015 08:42 05/13/2015 12:029.74.9 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 5 of 104

SB-1 (0-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1100-41-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 SS05/13/2015 08:42 05/13/2015 12:029.74.9 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 SS05/13/2015 08:42 05/13/2015 12:029.74.9 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 6 of 104

SB-1 (0-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 175-01-4 SS05/13/2015 08:42 05/13/2015 12:024.92.4 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 SS05/13/2015 08:42 05/13/2015 12:02157.3 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-125100 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-120110 %Surrogate: Toluene-d82037-26-5

76-13096.7 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 583-32-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5208-96-8 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 598-86-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 562-53-3 SR05/12/2015 19:15 05/13/2015 11:54883442 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5120-12-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51912-24-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5100-52-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 592-87-5 SR05/12/2015 19:15 05/13/2015 11:54883442 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 556-55-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-32-8 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5205-99-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5191-24-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 565-85-0 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5207-08-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5100-51-6 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 7 of 104

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15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 585-68-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 592-52-4 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5101-55-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5105-60-2 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 586-74-8 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 559-50-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5106-47-8 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5111-91-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5111-44-4 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5108-60-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 591-58-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-57-8 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57005-72-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

167 ug/kg dry 5218-01-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DChrysene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553-70-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5132-64-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 584-74-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-50-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 5541-73-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 5106-46-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 591-94-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5120-83-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 8 of 104

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York Project (SDG) No.

15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 584-66-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5105-67-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5131-11-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5534-52-1 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 551-28-5 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5121-14-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5606-20-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5117-84-0 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5122-66-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5117-81-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DBis(2-ethylhexyl)phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

164 ug/kg dry 5206-44-0 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DFluoranthene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 586-73-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5118-74-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 587-68-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 577-47-4 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 567-72-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5193-39-5 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 578-59-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 591-57-6 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 595-48-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 565794-96-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 591-20-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 9 of 104

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15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 5100-01-6 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 588-74-4 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 599-09-2 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 598-95-3 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 588-75-5 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5100-02-7 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5621-64-7 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 562-75-9 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 586-30-6 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 587-86-5 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 585-01-8 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5108-95-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

145 ug/kg dry 5129-00-0 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270DPyrene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-94-3 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 558-90-2 SR05/12/2015 19:15 05/13/2015 11:54441221 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5120-82-1 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 588-06-2 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-95-4 SR05/12/2015 19:15 05/13/2015 11:54221111 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9565.5 %Surrogate: 2-Fluorophenol367-12-4

10-10776.5 %Surrogate: Phenol-d54165-62-2

10-9552.4 %Surrogate: Nitrobenzene-d54165-60-0

10-9787.7 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10349.5 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9966.2 %Surrogate: Terphenyl-d14 1718-51-0

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 10 of 104

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15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 12:3769.869.8 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 12:371.751.75 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 12:378.738.73 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 12:3788.388.3 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14032.7 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14033.2 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 11:540.01760.0176 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14038.4 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14055.2 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

5080 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 10:545.295.29 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.11 mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1.86 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 10:541.061.06 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

56.0 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 10:541.061.06 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 10:540.1060.106 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

0.344 mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 10:540.3170.317 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

16400 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 10:545.290.529 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

14.0 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

4.79 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

34.0 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

11300 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 10:542.122.12 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

80.7 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 10:540.3170.317 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

7290 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 10:545.295.29 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

254 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

13.6 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

721 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 10:545.295.29 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.65 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 10:541.061.06 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 10:540.5290.529 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

236 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 10:5410.610.6 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 10:541.061.06 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

24.4 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 10:541.061.06 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

84.0 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 10:541.061.06 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

0.107 mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 11:190.03170.0317 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids Sample Notes:Log-in Notes:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 13 of 104

SB-1 (0-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-01

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Miscellaneous Physical Parameters[TOC]

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

LOD/MDL LOQ

Reported to

94.5 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5290.370 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

14.0 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-1 (13'-15')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 14 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 187-61-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 SS05/13/2015 08:42 05/13/2015 12:3210050 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 167-64-1 SS05/13/2015 08:42 05/13/2015 12:32105.0 EPA 8260CAcetone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 SS05/13/2015 08:42 05/13/2015 12:32105.0 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 15 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 175-25-2 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 SS05/13/2015 08:42 05/13/2015 12:32105.0 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 16 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1103-65-1 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 SS05/13/2015 08:42 05/13/2015 12:32105.0 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 SS05/13/2015 08:42 05/13/2015 12:325.02.5 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 SS05/13/2015 08:42 05/13/2015 12:32157.5 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-12599.4 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-120107 %Surrogate: Toluene-d82037-26-5

76-13097.6 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 183-32-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 17 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1208-96-8 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-86-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 162-53-3 SR05/12/2015 19:15 05/13/2015 10:2117386.3 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-12-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11912-24-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-52-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 192-87-5 SR05/12/2015 19:15 05/13/2015 10:2117386.3 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 156-55-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 150-32-8 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1205-99-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1191-24-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165-85-0 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1207-08-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-51-6 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-68-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 192-52-4 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1101-55-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-60-2 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 186-74-8 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 159-50-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-47-8 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1111-91-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 18 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1111-44-4 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-60-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-58-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-57-8 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 17005-72-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1218-01-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 153-70-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1132-64-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 184-74-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-50-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1541-73-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1106-46-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 191-94-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-83-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 184-66-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-67-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1131-11-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1534-52-1 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 151-28-5 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1121-14-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1606-20-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1117-84-0 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 19 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1122-66-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

40.7 ug/kg dry 1117-81-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DBis(2-ethylhexyl)phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1206-44-0 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

26.2 ug/kg dry 186-73-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DFluorene J

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1118-74-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 177-47-4 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-72-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1193-39-5 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-59-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-57-6 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-48-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165794-96-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 191-20-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-01-6 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-74-4 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 199-09-2 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-95-3 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-75-5 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-02-7 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1621-64-7 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 162-75-9 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 20 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 186-30-6 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 187-86-5 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-01-8 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-95-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1129-00-0 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-94-3 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 158-90-2 SR05/12/2015 19:15 05/13/2015 10:2186.143.1 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-06-2 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-95-4 SR05/12/2015 19:15 05/13/2015 10:2143.121.6 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9575.0 %Surrogate: 2-Fluorophenol367-12-4

10-10775.2 %Surrogate: Phenol-d54165-62-2

10-9557.9 %Surrogate: Nitrobenzene-d54165-60-0

10-9780.9 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10348.2 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9966.5 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 21 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 10:3268.268.2 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 10:321.711.71 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 10:328.538.53 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 10:3286.386.3 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14025.2 %Surrogate: Tetrachloro-m-xylene877-09-8 GC-Sur

r

30-14053.2 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 22 of 104

SB-1 (13'-15')

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15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 12:090.01720.0172 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14026.1 %Surrogate: Tetrachloro-m-xylene877-09-8 GC-Sur

r

30-14046.3 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

4990 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 10:595.175.17 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1.58 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 10:591.031.03 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

29.4 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 10:591.031.03 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 10:590.1030.103 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 10:590.3100.310 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2190 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 10:595.170.517 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

17.0 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

5.42 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 23 of 104

SB-1 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

25.5 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

11500 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 10:592.072.07 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

2.63 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 10:590.3100.310 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2300 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 10:595.175.17 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

193 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

11.0 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

781 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 10:595.175.17 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.09 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 10:591.031.03 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 10:590.5170.517 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

360 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 10:5910.310.3 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 10:591.031.03 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

28.2 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 10:591.031.03 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

15.9 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 10:591.031.03 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 11:280.03100.0310 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

96.7 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent Sample Notes:Log-in Notes:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 24 of 104

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York Sample ID: 15E0465-02

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 11, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Wet Chemistry Parameters[TOC]

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5170.362 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

17.0 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-2 (0'-2')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 25 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 196-12-8 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 SS05/13/2015 08:42 05/13/2015 13:0211054 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

3.7 ug/kg dry 178-93-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C2-Butanone J

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

33 ug/kg dry 167-64-1 SS05/13/2015 08:42 05/13/2015 13:02115.4 EPA 8260CAcetone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 SS05/13/2015 08:42 05/13/2015 13:02115.4 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 26 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1108-90-7 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

8.9 ug/kg dry 175-09-2 SS05/13/2015 08:42 05/13/2015 13:02115.4 EPA 8260CMethylene chloride J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 SS05/13/2015 08:42 05/13/2015 13:02115.4 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 27 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1135-98-8 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 SS05/13/2015 08:42 05/13/2015 13:025.42.7 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 SS05/13/2015 08:42 05/13/2015 13:02168.2 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-125102 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-120104 %Surrogate: Toluene-d82037-26-5

76-13096.7 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

139 ug/kg dry 283-32-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

130 ug/kg dry 2208-96-8 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-86-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 262-53-3 KH05/12/2015 19:15 05/13/2015 12:31357178 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

728 ug/kg dry 2120-12-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 28 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 21912-24-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2100-52-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 292-87-5 KH05/12/2015 19:15 05/13/2015 12:31357178 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

1340 ug/kg dry 256-55-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

760 ug/kg dry 250-32-8 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

670 ug/kg dry 2205-99-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

332 ug/kg dry 2191-24-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265-85-0 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

844 ug/kg dry 2207-08-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-51-6 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 285-68-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 292-52-4 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2101-55-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-60-2 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

207 ug/kg dry 286-74-8 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 259-50-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2106-47-8 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-91-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-44-4 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-60-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-58-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-57-8 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 29 of 104

SB-2 (0'-2')

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15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 27005-72-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1250 ug/kg dry 2218-01-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

165 ug/kg dry 253-70-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

112 ug/kg dry 2132-64-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

690 ug/kg dry 284-74-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-50-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 2541-73-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 2106-46-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 291-94-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-83-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 284-66-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-67-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2131-11-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2534-52-1 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 251-28-5 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2121-14-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2606-20-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2117-84-0 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2122-66-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

588 ug/kg dry 2117-81-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DBis(2-ethylhexyl)phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2620 ug/kg dry 2206-44-0 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

312 ug/kg dry 286-73-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 30 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 2118-74-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-68-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 277-47-4 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 267-72-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

378 ug/kg dry 2193-39-5 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 278-59-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-57-6 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 295-48-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265794-96-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 291-20-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 2100-01-6 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-74-4 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 299-09-2 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-95-3 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-75-5 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-02-7 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2621-64-7 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-75-9 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 286-30-6 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 287-86-5 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2210 ug/kg dry 285-01-8 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-95-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

2180 ug/kg dry 2129-00-0 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-94-3 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 258-90-2 KH05/12/2015 19:15 05/13/2015 12:3117889.1 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2120-82-1 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-06-2 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-95-4 KH05/12/2015 19:15 05/13/2015 12:3189.144.7 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9516.3 %Surrogate: 2-Fluorophenol367-12-4

10-10743.1 %Surrogate: Phenol-d54165-62-2

10-9554.9 %Surrogate: Nitrobenzene-d54165-60-0

10-9748.0 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10315.3 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9962.3 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 12:5270.570.5 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 12:521.761.76 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 12:528.818.81 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 12:5289.289.2 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14045.6 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14054.5 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 33 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 12:260.01780.0178 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14059.6 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14096.5 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

7160 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:045.345.34 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.60 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:041.071.07 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

57.5 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:041.071.07 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:040.1070.107 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:040.3210.321 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

16900 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:045.340.534 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

18.5 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

6.26 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

29.1 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

14300 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:042.142.14 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

50.7 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:040.3210.321 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

3050 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:045.345.34 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

291 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 34 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

14.0 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1110 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:045.345.34 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.93 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:041.071.07 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:040.5340.534 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

214 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:0410.710.7 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:041.071.07 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

33.3 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:041.071.07 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

90.1 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:041.071.07 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

0.0416 mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 11:370.03210.0321 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

93.6 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5340.374 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

18.5 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 35 of 104

SB-2 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-03

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-2 (13'-15')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 36 of 104

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1541-73-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 SS05/13/2015 08:42 05/13/2015 13:339849 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

6.5 ug/kg dry 167-64-1 SS05/13/2015 08:42 05/13/2015 13:339.84.9 EPA 8260CAcetone J

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 SS05/13/2015 08:42 05/13/2015 13:339.84.9 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 37 of 104

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1110-82-7 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 SS05/13/2015 08:42 05/13/2015 13:339.84.9 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 SS05/13/2015 08:42 05/13/2015 13:339.84.9 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 38 of 104

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1156-60-5 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 SS05/13/2015 08:42 05/13/2015 13:334.92.5 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 SS05/13/2015 08:42 05/13/2015 13:33157.4 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-12597.8 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-120104 %Surrogate: Toluene-d82037-26-5

76-13092.5 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 183-32-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1208-96-8 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-86-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 162-53-3 KH05/12/2015 19:15 05/13/2015 12:0017386.6 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-12-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11912-24-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-52-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 192-87-5 KH05/12/2015 19:15 05/13/2015 12:0017386.6 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 156-55-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 150-32-8 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1205-99-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 39 of 104

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15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1191-24-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165-85-0 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1207-08-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-51-6 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-68-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 192-52-4 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1101-55-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-60-2 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 186-74-8 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 159-50-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-47-8 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1111-91-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1111-44-4 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-60-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-58-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-57-8 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 17005-72-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1218-01-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 153-70-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1132-64-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

38.0 ug/kg dry 184-74-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DDi-n-butyl phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-50-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 40 of 104

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1541-73-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1106-46-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 191-94-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-83-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 184-66-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-67-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1131-11-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1534-52-1 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 151-28-5 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1121-14-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1606-20-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1117-84-0 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1122-66-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

24.6 ug/kg dry 1117-81-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DBis(2-ethylhexyl)phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1206-44-0 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 186-73-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1118-74-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 177-47-4 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-72-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1193-39-5 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-59-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 41 of 104

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 191-57-6 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-48-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165794-96-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 191-20-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-01-6 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-74-4 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 199-09-2 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-95-3 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-75-5 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-02-7 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1621-64-7 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 162-75-9 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 186-30-6 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 187-86-5 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-01-8 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-95-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1129-00-0 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-94-3 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 158-90-2 KH05/12/2015 19:15 05/13/2015 12:0086.443.3 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-06-2 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-95-4 KH05/12/2015 19:15 05/13/2015 12:0043.321.7 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 42 of 104

SB-2 (13'-15')

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15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

Surrogate Recoveries Result Acceptance Range

10-9542.6 %Surrogate: 2-Fluorophenol367-12-4

10-10747.5 %Surrogate: Phenol-d54165-62-2

10-9554.8 %Surrogate: Nitrobenzene-d54165-60-0

10-9743.9 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10371.2 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9945.9 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 10:4468.568.5 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 43 of 104

SB-2 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 10:441.711.71 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 10:448.568.56 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 10:4486.686.6 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14028.3 %Surrogate: Tetrachloro-m-xylene877-09-8 GC-Sur

r

30-14041.4 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 12:450.01730.0173 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14031.0 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14054.7 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

6650 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:085.195.19 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.13 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:081.041.04 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

45.5 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:081.041.04 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:080.1040.104 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:080.3110.311 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

3160 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:085.190.519 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

23.3 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

7.09 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

24.0 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

14400 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:082.082.08 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

4.79 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:080.3110.311 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2840 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:085.195.19 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

249 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

12.9 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1040 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:085.195.19 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

2.33 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:081.041.04 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:080.5190.519 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

437 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:0810.410.4 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:081.041.04 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

28.5 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:081.041.04 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

35.0 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:081.041.04 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Project (SDG) No.

15E0465

York Sample ID: 15E0465-04

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 11:460.03110.0311 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

96.4 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5190.363 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

23.3 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-3 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-3 (0'-2')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-3 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 176-13-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 SS05/13/2015 08:42 05/13/2015 14:038744 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 167-64-1 SS05/13/2015 08:42 05/13/2015 14:038.74.4 EPA 8260CAcetone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 SS05/13/2015 08:42 05/13/2015 14:038.74.4 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 47 of 104

SB-3 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1107-13-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 48 of 104

SB-3 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 11634-04-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 SS05/13/2015 08:42 05/13/2015 14:038.74.4 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 SS05/13/2015 08:42 05/13/2015 14:038.74.4 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 SS05/13/2015 08:42 05/13/2015 14:034.42.2 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 SS05/13/2015 08:42 05/13/2015 14:03136.6 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-125104 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-120101 %Surrogate: Toluene-d82037-26-5

76-13093.5 %Surrogate: p-Bromofluorobenzene460-00-4

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 583-32-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5208-96-8 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 598-86-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 562-53-3 SR05/12/2015 19:15 05/13/2015 12:57857428 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5120-12-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51912-24-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5100-52-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 592-87-5 SR05/12/2015 19:15 05/13/2015 12:57857428 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 556-55-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-32-8 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5205-99-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5191-24-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 565-85-0 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5207-08-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5100-51-6 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 585-68-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 592-52-4 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5101-55-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5105-60-2 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 586-74-8 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 559-50-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 5106-47-8 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5111-91-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5111-44-4 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5108-60-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 591-58-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-57-8 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57005-72-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

154 ug/kg dry 5218-01-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DChrysene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553-70-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5132-64-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 584-74-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-50-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 5541-73-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 5106-46-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 591-94-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5120-83-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 584-66-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5105-67-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5131-11-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5534-52-1 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 551-28-5 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5121-14-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 5606-20-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5117-84-0 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5122-66-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

127 ug/kg dry 5117-81-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DBis(2-ethylhexyl)phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

157 ug/kg dry 5206-44-0 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DFluoranthene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 586-73-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5118-74-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 587-68-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 577-47-4 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 567-72-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5193-39-5 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 578-59-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 591-57-6 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 595-48-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 565794-96-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 591-20-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 5100-01-6 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 588-74-4 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 599-09-2 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 598-95-3 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 588-75-5 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5100-02-7 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 5621-64-7 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 562-75-9 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 586-30-6 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 587-86-5 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 585-01-8 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5108-95-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

125 ug/kg dry 5129-00-0 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270DPyrene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-94-3 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 558-90-2 SR05/12/2015 19:15 05/13/2015 12:57427214 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5120-82-1 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 588-06-2 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 595-95-4 SR05/12/2015 19:15 05/13/2015 12:57214107 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9557.6 %Surrogate: 2-Fluorophenol367-12-4

10-10762.3 %Surrogate: Phenol-d54165-62-2

10-9543.3 %Surrogate: Nitrobenzene-d54165-60-0

10-9772.9 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10340.2 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9944.8 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 13:0767.767.7 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 13:071.691.69 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 13:078.468.46 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 13:0785.785.7 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14030.7 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14034.1 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB) Sample Notes:Log-in Notes:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 13:010.01710.0171 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14042.9 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14060.7 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

6410 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:135.135.13 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.33 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:131.031.03 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

62.5 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:131.031.03 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:130.1030.103 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:130.3080.308 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

4560 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:135.130.513 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

14.1 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

7.08 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

38.9 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

16300 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:132.052.05 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

55.2 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:130.3080.308 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

3260 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:135.135.13 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

326 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

12.0 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1310 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:135.135.13 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.62 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:131.031.03 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:130.5130.513 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

280 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:1310.310.3 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:131.031.03 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

34.2 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:131.031.03 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

69.3 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:131.031.03 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 11:550.03080.0308 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

97.5 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-05

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5130.359 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

14.1 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-3 (13'-15')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 195-63-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 SS05/13/2015 08:42 05/13/2015 14:336834 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 167-64-1 SS05/13/2015 08:42 05/13/2015 14:336.83.4 EPA 8260CAcetone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 SS05/13/2015 08:42 05/13/2015 14:336.83.4 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 156-23-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 SS05/13/2015 08:42 05/13/2015 14:336.83.4 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 SS05/13/2015 08:42 05/13/2015 14:336.83.4 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 199-87-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 SS05/13/2015 08:42 05/13/2015 14:333.41.7 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 SS05/13/2015 08:42 05/13/2015 14:33105.1 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-125106 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-120107 %Surrogate: Toluene-d82037-26-5

76-13095.0 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 183-32-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1208-96-8 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-86-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 162-53-3 SR05/12/2015 19:15 05/13/2015 10:5217386.3 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 60 of 104

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York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1120-12-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11912-24-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-52-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 192-87-5 SR05/12/2015 19:15 05/13/2015 10:5217386.3 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 156-55-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 150-32-8 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1205-99-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1191-24-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165-85-0 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1207-08-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-51-6 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-68-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 192-52-4 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1101-55-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-60-2 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 186-74-8 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 159-50-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-47-8 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1111-91-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1111-44-4 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-60-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-58-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 61 of 104

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 195-57-8 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 17005-72-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1218-01-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 153-70-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1132-64-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 184-74-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-50-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1541-73-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1106-46-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 191-94-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-83-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 184-66-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-67-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1131-11-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1534-52-1 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 151-28-5 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1121-14-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1606-20-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1117-84-0 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1122-66-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

42.4 ug/kg dry 1117-81-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DBis(2-ethylhexyl)phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1206-44-0 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 62 of 104

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 186-73-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1118-74-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 177-47-4 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-72-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1193-39-5 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-59-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-57-6 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-48-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165794-96-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 191-20-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-01-6 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-74-4 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 199-09-2 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-95-3 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-75-5 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-02-7 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1621-64-7 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 162-75-9 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 186-30-6 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 187-86-5 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-01-8 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 63 of 104

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1108-95-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1129-00-0 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-94-3 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 158-90-2 SR05/12/2015 19:15 05/13/2015 10:5286.043.1 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-06-2 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-95-4 SR05/12/2015 19:15 05/13/2015 10:5243.121.6 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9541.1 %Surrogate: 2-Fluorophenol367-12-4

10-10753.2 %Surrogate: Phenol-d54165-62-2

10-9539.3 %Surrogate: Nitrobenzene-d54165-60-0

10-9760.6 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10338.2 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9956.4 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 10:5868.268.2 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 64 of 104

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 10:581.701.70 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 10:588.528.52 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 10:5886.386.3 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14048.4 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14066.6 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 65 of 104

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 13:180.01720.0172 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14047.8 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14064.7 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

3480 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:185.165.16 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1.29 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:181.031.03 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

25.0 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:181.031.03 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:180.1030.103 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:180.3100.310 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1090 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:185.160.516 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

9.87 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

4.11 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

12.6 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

9730 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:182.072.07 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

2.53 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:180.3100.310 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1970 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:185.165.16 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

182 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

9.49 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

543 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:185.165.16 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:181.031.03 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:180.5160.516 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

110 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:1810.310.3 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:181.031.03 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

16.6 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:181.031.03 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

23.1 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:181.031.03 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 12:040.03100.0310 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

96.8 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5160.362 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 67 of 104

SB-3 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-06

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

9.87 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-4 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-4 (0'-2')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 68 of 104

SB-4 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1107-06-2 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 BK05/13/2015 09:23 05/13/2015 12:269347 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

7.0 ug/kg dry 167-64-1 BK05/13/2015 09:23 05/13/2015 12:269.34.7 EPA 8260CAcetone SCAL-

E, J Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 BK05/13/2015 09:23 05/13/2015 12:269.34.7 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 69 of 104

SB-4 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 174-87-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 BK05/13/2015 09:23 05/13/2015 12:269.34.7 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 BK05/13/2015 09:23 05/13/2015 12:269.34.7 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 70 of 104

SB-4 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 198-06-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 BK05/13/2015 09:23 05/13/2015 12:264.72.3 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 BK05/13/2015 09:23 05/13/2015 12:26147.0 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-12595.7 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-12097.1 %Surrogate: Toluene-d82037-26-5

76-130105 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

75.7 ug/kg dry 283-32-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DAcenaphthene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2208-96-8 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-86-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 262-53-3 KH05/12/2015 19:15 05/13/2015 13:02379190 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

128 ug/kg dry 2120-12-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 21912-24-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2100-52-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 292-87-5 KH05/12/2015 19:15 05/13/2015 13:02379190 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

321 ug/kg dry 256-55-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

109 ug/kg dry 250-32-8 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

122 ug/kg dry 2205-99-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

96.9 ug/kg dry 2191-24-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265-85-0 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

131 ug/kg dry 2207-08-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-51-6 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 285-68-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 292-52-4 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2101-55-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-60-2 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 286-74-8 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 259-50-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2106-47-8 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-91-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-44-4 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-60-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-58-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-57-8 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 27005-72-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

332 ug/kg dry 2218-01-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 253-70-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (0'-2')

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York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 2132-64-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 284-74-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-50-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 2541-73-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 2106-46-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 291-94-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-83-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 284-66-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-67-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2131-11-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2534-52-1 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 251-28-5 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2121-14-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2606-20-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2117-84-0 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2122-66-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

335 ug/kg dry 2117-81-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DBis(2-ethylhexyl)phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

756 ug/kg dry 2206-44-0 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

81.7 ug/kg dry 286-73-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DFluorene J

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2118-74-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-68-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 277-47-4 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (0'-2')

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York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 267-72-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

74.9 ug/kg dry 2193-39-5 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DIndeno(1,2,3-cd)pyrene J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 278-59-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-57-6 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 295-48-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265794-96-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 291-20-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 2100-01-6 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-74-4 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 299-09-2 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-95-3 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-75-5 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-02-7 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2621-64-7 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-75-9 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 286-30-6 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 287-86-5 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

518 ug/kg dry 285-01-8 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-95-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

820 ug/kg dry 2129-00-0 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-94-3 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 258-90-2 KH05/12/2015 19:15 05/13/2015 13:0218994.7 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 2120-82-1 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-06-2 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-95-4 KH05/12/2015 19:15 05/13/2015 13:0294.747.5 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9528.4 %Surrogate: 2-Fluorophenol367-12-4

10-10741.0 %Surrogate: Phenol-d54165-62-2

10-9545.2 %Surrogate: Nitrobenzene-d54165-60-0

10-9743.9 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10325.1 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9970.0 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.54 ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

8.20 ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 13:2274.974.9 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

8.16 ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (0'-2')

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York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

6.42 ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 13:221.871.87 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 13:229.379.37 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 13:2294.894.8 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14039.2 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14039.4 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

0.0257 mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

0.0618 mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

0.0875 mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 13:370.01890.0189 EPA 8082A* Total PCBs

Certifications:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

Surrogate Recoveries Result Acceptance Range

30-14045.8 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14073.1 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

6720 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:485.685.68 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

0.612 mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

4.03 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:481.141.14 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

71.5 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:481.141.14 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:480.1140.114 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

0.440 mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:480.3410.341 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

44600 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:485.680.568 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

15.4 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

5.31 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

34.3 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

12800 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:482.272.27 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

69.5 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:480.3410.341 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

7350 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:485.685.68 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

205 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

13.9 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

696 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:485.685.68 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.96 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:481.141.14 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:480.5680.568 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

245 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:4811.411.4 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (0'-2')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-07

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:481.141.14 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

31.8 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:481.141.14 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

113 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:481.141.14 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

0.0498 mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 12:130.03410.0341 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

88.1 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5680.397 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

15.4 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-4 (4'-6')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-4 (4'-6')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (4'-6')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-4 (4'-6')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-61-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 BK05/13/2015 09:23 05/13/2015 13:029145 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (4'-6')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1591-78-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

11 ug/kg dry 167-64-1 BK05/13/2015 09:23 05/13/2015 13:029.14.5 EPA 8260CAcetone SCAL-

E Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 BK05/13/2015 09:23 05/13/2015 13:029.14.5 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-25-2 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (4'-6')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1100-41-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 BK05/13/2015 09:23 05/13/2015 13:029.14.5 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1103-65-1 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 BK05/13/2015 09:23 05/13/2015 13:029.14.5 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 175-01-4 BK05/13/2015 09:23 05/13/2015 13:024.52.3 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 BK05/13/2015 09:23 05/13/2015 13:02146.8 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-12596.8 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-12095.5 %Surrogate: Toluene-d82037-26-5

76-130105 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 283-32-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2208-96-8 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-86-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 262-53-3 SR05/12/2015 19:15 05/13/2015 12:25366183 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-12-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 21912-24-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2100-52-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 292-87-5 SR05/12/2015 19:15 05/13/2015 12:25366183 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 256-55-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 250-32-8 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2205-99-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2191-24-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265-85-0 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2207-08-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-51-6 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 285-68-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 292-52-4 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2101-55-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-60-2 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 286-74-8 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 259-50-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2106-47-8 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-91-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2111-44-4 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-60-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-58-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-57-8 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 27005-72-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

172 ug/kg dry 2218-01-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 253-70-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2132-64-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 284-74-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-50-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 2541-73-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 2106-46-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 291-94-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2120-83-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (4'-6')

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York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 284-66-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2105-67-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2131-11-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2534-52-1 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 251-28-5 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2121-14-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2606-20-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2117-84-0 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2122-66-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

54.0 ug/kg dry 2117-81-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DBis(2-ethylhexyl)phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

250 ug/kg dry 2206-44-0 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 286-73-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2118-74-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 287-68-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 277-47-4 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 267-72-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2193-39-5 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 278-59-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 291-57-6 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 295-48-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 265794-96-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 291-20-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (4'-6')

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15E0465

York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 2100-01-6 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-74-4 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 299-09-2 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 298-95-3 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-75-5 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2100-02-7 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2621-64-7 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 262-75-9 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 286-30-6 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 287-86-5 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

215 ug/kg dry 285-01-8 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 2108-95-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

207 ug/kg dry 2129-00-0 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-94-3 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 258-90-2 SR05/12/2015 19:15 05/13/2015 12:2518291.3 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 2120-82-1 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 288-06-2 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 295-95-4 SR05/12/2015 19:15 05/13/2015 12:2591.345.8 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9525.0 %Surrogate: 2-Fluorophenol367-12-4

10-10753.0 %Surrogate: Phenol-d54165-62-2

10-9537.6 %Surrogate: Nitrobenzene-d54165-60-0

10-9764.2 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10311.2 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9945.0 %Surrogate: Terphenyl-d14 1718-51-0

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (4'-6')

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York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.07 ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

3.92 ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 13:3772.372.3 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

3.90 ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2.34 ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 13:371.811.81 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 13:379.039.03 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 13:3791.491.4 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-08

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

Surrogate Recoveries Result Acceptance Range

30-14036.0 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14039.4 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 13:560.01820.0182 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14043.8 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14066.2 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

5060 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:535.485.48 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1.93 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:531.101.10 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

67.4 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:531.101.10 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:530.1100.110 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

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Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:530.3290.329 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

20200 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:535.480.548 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

14.5 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

4.95 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

29.5 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

13100 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:532.192.19 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

79.9 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:530.3290.329 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

3050 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:535.485.48 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

232 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

12.4 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

831 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:535.485.48 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.99 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:531.101.10 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:530.5480.548 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

173 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:5311.011.0 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:531.101.10 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

26.6 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:531.101.10 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

51.4 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:531.101.10 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 12:220.03290.0329 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids Sample Notes:Log-in Notes:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Miscellaneous Physical Parameters[TOC]

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

LOD/MDL LOQ

Reported to

91.3 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5480.383 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

14.5 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_2]SB-4 (13'-15')[TOC]

[TOC_3]Volatile Organic Compounds by GC/MS[TOC]

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1630-20-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1,1,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-55-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1,1-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-34-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1,2,2-Tetrachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 176-13-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-00-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1,2-Trichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-34-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-35-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,1-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 187-61-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2,3-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 196-18-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2,3-Trichloropropane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2,4-Trichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 195-63-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2,4-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 196-12-8 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2-Dibromo-3-chloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1106-93-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2-Dibromoethane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-50-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1107-06-2 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2-Dichloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-87-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,2-Dichloropropane

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-67-8 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,3,5-Trimethylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1541-73-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,3-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-46-7 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C1,4-Dichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1123-91-1 BK05/13/2015 09:23 05/13/2015 13:389246 EPA 8260C1,4-Dioxane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 178-93-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C2-Butanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1591-78-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C2-Hexanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-10-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260C4-Methyl-2-pentanone

Certifications: CTDOH,NELAC-NY10854,NJDEP

9.2 ug/kg dry 167-64-1 BK05/13/2015 09:23 05/13/2015 13:389.24.6 EPA 8260CAcetone SCAL-

E Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-02-8 BK05/13/2015 09:23 05/13/2015 13:389.24.6 EPA 8260CAcrolein

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1107-13-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CAcrylonitrile

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 171-43-2 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CBenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-97-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CBromochloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-27-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CBromodichloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

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York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 175-25-2 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CBromoform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-83-9 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CBromomethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-15-0 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CCarbon disulfide

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 156-23-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CCarbon tetrachloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-90-7 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CChlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-00-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CChloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-66-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CChloroform

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-87-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CChloromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-59-2 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Ccis-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-01-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Ccis-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1110-82-7 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CCyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1124-48-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CDibromochloromethane

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 174-95-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CDibromomethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-71-8 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CDichlorodifluoromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-41-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CEthyl Benzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CHexachlorobutadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-82-8 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CIsopropylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 179-20-9 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CMethyl acetate

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 11634-04-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CMethyl tert-butyl ether (MTBE)

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1108-87-2 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CMethylcyclohexane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 175-09-2 BK05/13/2015 09:23 05/13/2015 13:389.24.6 EPA 8260CMethylene chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1104-51-8 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Cn-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 91 of 104

SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Volatile Organics, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 5035A

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1103-65-1 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Cn-Propylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-47-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Co-Xylene

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 1179601-23-1 BK05/13/2015 09:23 05/13/2015 13:389.24.6 EPA 8260Cp- & m- Xylenes

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 199-87-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Cp-Isopropyltoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1135-98-8 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Csec-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-42-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CStyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 175-65-0 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Ctert-Butyl alcohol (TBA)

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 198-06-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Ctert-Butylbenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1127-18-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CTetrachloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-88-3 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CToluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1156-60-5 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Ctrans-1,2-Dichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 110061-02-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260Ctrans-1,3-Dichloropropylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 179-01-6 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CTrichloroethylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-69-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CTrichlorofluoromethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 175-01-4 BK05/13/2015 09:23 05/13/2015 13:384.62.3 EPA 8260CVinyl Chloride

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11330-20-7 BK05/13/2015 09:23 05/13/2015 13:38146.9 EPA 8260CXylenes, Total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

Surrogate Recoveries Result Acceptance Range

77-12595.0 %Surrogate: 1,2-Dichloroethane-d417060-07-0

85-12096.0 %Surrogate: Toluene-d82037-26-5

76-130104 %Surrogate: p-Bromofluorobenzene460-00-4

[TOC_3]Semivolatile Organic Compounds by GC/MS[TOC]

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 183-32-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DAcenaphthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 92 of 104

SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1208-96-8 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DAcenaphthylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-86-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DAcetophenone

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 162-53-3 KH05/12/2015 19:15 05/13/2015 11:2817587.4 EPA 8270DAniline

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-12-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DAnthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 11912-24-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DAtrazine

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1100-52-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzaldehyde

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 192-87-5 KH05/12/2015 19:15 05/13/2015 11:2817587.4 EPA 8270DBenzidine

Certifications: CTDOH,NELAC-NY10854

ND ug/kg dry 156-55-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzo(a)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 150-32-8 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzo(a)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1205-99-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzo(b)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1191-24-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzo(g,h,i)perylene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165-85-0 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzoic acid

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1207-08-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzo(k)fluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-51-6 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzyl alcohol

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-68-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBenzyl butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 192-52-4 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D1,1'-Biphenyl

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1101-55-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D4-Bromophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-60-2 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270DCaprolactam

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 186-74-8 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DCarbazole

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 159-50-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D4-Chloro-3-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1106-47-8 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D4-Chloroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1111-91-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBis(2-chloroethoxy)methane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 93 of 104

SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1111-44-4 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBis(2-chloroethyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-60-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBis(2-chloroisopropyl)ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-58-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2-Chloronaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-57-8 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2-Chlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 17005-72-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D4-Chlorophenyl phenyl ether

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1218-01-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DChrysene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 153-70-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DDibenzo(a,h)anthracene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1132-64-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DDibenzofuran

Certifications: CTDOH,NELAC-NY10854,NJDEP

124 ug/kg dry 184-74-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DDi-n-butyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-50-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D1,2-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1541-73-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D1,3-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 1106-46-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D1,4-Dichlorobenzene

Certifications: NELAC-NY10854

ND ug/kg dry 191-94-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D3,3'-Dichlorobenzidine

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1120-83-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2,4-Dichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 184-66-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DDiethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1105-67-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2,4-Dimethylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1131-11-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DDimethyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1534-52-1 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D4,6-Dinitro-2-methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 151-28-5 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D2,4-Dinitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1121-14-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2,4-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1606-20-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2,6-Dinitrotoluene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1117-84-0 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DDi-n-octyl phthalate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (13'-15')

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15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 1122-66-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D1,2-Diphenylhydrazine (as

Azobenzene) Certifications: NELAC-NY10854,NJDEP

41.9 ug/kg dry 1117-81-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DBis(2-ethylhexyl)phthalate J

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1206-44-0 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DFluoranthene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 186-73-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DFluorene

Certifications: NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1118-74-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DHexachlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 187-68-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DHexachlorobutadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 177-47-4 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DHexachlorocyclopentadiene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 167-72-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DHexachloroethane

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1193-39-5 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DIndeno(1,2,3-cd)pyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 178-59-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DIsophorone

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 191-57-6 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2-Methylnaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 195-48-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2-Methylphenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 165794-96-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D3- & 4-Methylphenols

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 191-20-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DNaphthalene

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 1100-01-6 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D4-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-74-4 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D2-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 199-09-2 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D3-Nitroaniline

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 198-95-3 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DNitrobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-75-5 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1100-02-7 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D4-Nitrophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1621-64-7 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DN-nitroso-di-n-propylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 162-75-9 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DN-Nitrosodimethylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 95 of 104

SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Semi-Volatiles, NJDEP/TCL/Part 375 List

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL

Reported to

LOQ

ND ug/kg dry 186-30-6 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DN-Nitrosodiphenylamine

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 187-86-5 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DPentachlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 185-01-8 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DPhenanthrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1108-95-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DPhenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 1129-00-0 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270DPyrene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-94-3 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D1,2,4,5-Tetrachlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 158-90-2 KH05/12/2015 19:15 05/13/2015 11:2887.243.7 EPA 8270D2,3,4,6-Tetrachlorophenol

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 1120-82-1 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D1,2,4-Trichlorobenzene

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 188-06-2 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2,4,6-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 195-95-4 KH05/12/2015 19:15 05/13/2015 11:2843.721.9 EPA 8270D2,4,5-Trichlorophenol

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

10-9543.0 %Surrogate: 2-Fluorophenol367-12-4

10-10749.0 %Surrogate: Phenol-d54165-62-2

10-9555.6 %Surrogate: Nitrobenzene-d54165-60-0

10-9743.7 %Surrogate: 2-Fluorobiphenyl321-60-8

10-10372.4 %Surrogate: 2,4,6-Tribromophenol118-79-6

19-9949.9 %Surrogate: Terphenyl-d14 1718-51-0

[TOC_3]Organochlorine Pesticides by GC/ECD[TOC]

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 572-54-8 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081B4,4'-DDD

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-55-9 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081B4,4'-DDE

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 550-29-3 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081B4,4'-DDT

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5309-00-2 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BAldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5319-84-6 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081Balpha-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Pesticides, 8081 target list

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND ug/kg dry 5319-85-7 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081Bbeta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 557-74-9 JW05/12/2015 20:59 05/13/2015 11:2269.169.1 EPA 8081BChlordane, total

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-74-2 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081Bgamma-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 5319-86-8 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081Bdelta-BHC

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 560-57-1 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BDieldrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 5959-98-8 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BEndosulfan I

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 533213-65-9 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BEndosulfan II

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51031-07-8 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BEndosulfan sulfate

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 572-20-8 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BEndrin

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 57421-93-4 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BEndrin aldehyde

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 553494-70-5 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BEndrin ketone

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND ug/kg dry 558-89-9 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081Bgamma-BHC (Lindane)

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 576-44-8 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BHeptachlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 51024-57-3 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081BHeptachlor epoxide

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 55103-71-9 JW05/12/2015 20:59 05/13/2015 11:221.731.73 EPA 8081Balpha-Chlordane

Certifications: NELAC-NY10854,NJDEP

ND ug/kg dry 572-43-5 JW05/12/2015 20:59 05/13/2015 11:228.648.64 EPA 8081BMethoxychlor

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND ug/kg dry 58001-35-2 JW05/12/2015 20:59 05/13/2015 11:2287.487.4 EPA 8081BToxaphene

Certifications: CTDOH,NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

30-14052.1 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14064.4 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Polychlorinated Biphenyls by GC/ECD[TOC]

Polychlorinated Biphenyls (PCB)

Sample Prepared by Method: EPA 3550C

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 112674-11-2 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1016

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111104-28-2 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1221

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111141-16-5 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1232

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 153469-21-9 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1242

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 112672-29-6 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1248

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111097-69-1 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1254

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 111096-82-5 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082AAroclor 1260

Certifications: NELAC-NY10854,CTDOH,NJDEP,PADEP

ND mg/kg dry 11336-36-3 AMC05/12/2015 20:59 05/13/2015 14:160.01740.0174 EPA 8082A* Total PCBs

Certifications:

Surrogate Recoveries Result Acceptance Range

30-14052.7 %Surrogate: Tetrachloro-m-xylene877-09-8

30-14076.1 %Surrogate: Decachlorobiphenyl2051-24-3

[TOC_3]Metals by ICP[TOC]

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

5520 mg/kg dry 17429-90-5 MW05/13/2015 08:29 05/13/2015 11:585.235.23 EPA 6010CAluminum

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-36-0 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CAntimony

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1.48 mg/kg dry 17440-38-2 MW05/13/2015 08:29 05/13/2015 11:581.051.05 EPA 6010CArsenic

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

46.1 mg/kg dry 17440-39-3 MW05/13/2015 08:29 05/13/2015 11:581.051.05 EPA 6010CBarium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-41-7 MW05/13/2015 08:29 05/13/2015 11:580.1050.105 EPA 6010CBeryllium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-43-9 MW05/13/2015 08:29 05/13/2015 11:580.3140.314 EPA 6010CCadmium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2420 mg/kg dry 17440-70-2 MW05/13/2015 08:29 05/13/2015 11:585.230.523 EPA 6010CCalcium

Certifications: CTDOH,NELAC-NY10854,NJDEP

15.8 mg/kg dry 17440-47-3 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CChromium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

5.87 mg/kg dry 17440-48-4 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CCobalt

Certifications: CTDOH,NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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SB-4 (13'-15')

York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

Metals, Target Analyte

Sample Prepared by Method: EPA 3050B

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

35.6 mg/kg dry 17440-50-8 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CCopper

Certifications: CTDOH,NELAC-NY10854,NJDEP

13000 mg/kg dry 17439-89-6 MW05/13/2015 08:29 05/13/2015 11:582.092.09 EPA 6010CIron

Certifications: CTDOH,NELAC-NY10854,NJDEP

4.10 mg/kg dry 17439-92-1 MW05/13/2015 08:29 05/13/2015 11:580.3140.314 EPA 6010CLead

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

2400 mg/kg dry 17439-95-4 MW05/13/2015 08:29 05/13/2015 11:585.235.23 EPA 6010CMagnesium

Certifications: CTDOH,NELAC-NY10854,NJDEP

357 mg/kg dry 17439-96-5 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CManganese

Certifications: CTDOH,NELAC-NY10854,NJDEP

10.6 mg/kg dry 17440-02-0 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CNickel

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

1070 mg/kg dry 17440-09-7 MW05/13/2015 08:29 05/13/2015 11:585.235.23 EPA 6010CPotassium

Certifications: CTDOH,NELAC-NY10854,NJDEP

1.49 mg/kg dry 17782-49-2 MW05/13/2015 08:29 05/13/2015 11:581.051.05 EPA 6010CSelenium

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

ND mg/kg dry 17440-22-4 MW05/13/2015 08:29 05/13/2015 11:580.5230.523 EPA 6010CSilver

Certifications: CTDOH,NELAC-NY10854,NJDEP,PADEP

325 mg/kg dry 17440-23-5 MW05/13/2015 08:29 05/13/2015 11:5810.510.5 EPA 6010CSodium

Certifications: CTDOH,NELAC-NY10854,NJDEP

ND mg/kg dry 17440-28-0 MW05/13/2015 08:29 05/13/2015 11:581.051.05 EPA 6010CThallium

Certifications: CTDOH,NELAC-NY10854,NJDEP

27.0 mg/kg dry 17440-62-2 MW05/13/2015 08:29 05/13/2015 11:581.051.05 EPA 6010CVanadium

Certifications: CTDOH,NELAC-NY10854,NJDEP

23.3 mg/kg dry 17440-66-6 MW05/13/2015 08:29 05/13/2015 11:581.051.05 EPA 6010CZinc

Certifications: CTDOH,NELAC-NY10854,NJDEP

[TOC_3]Mercury by EPA 7000/200 Series Methods[TOC]

Mercury by 7473

Sample Prepared by Method: EPA 7473 soil

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

ND mg/kg dry 17439-97-6 ALD05/13/2015 07:01 05/13/2015 12:300.03140.0314 EPA 7473Mercury

Certifications: CTDOH,NJDEP,NELAC-NY10854,PADEP

[TOC_3]Miscellaneous Physical Parameters[TOC]

Total Solids

Sample Prepared by Method: % Solids Prep

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

95.5 % 1solids SCA05/13/2015 10:10 05/13/2015 14:570.1000.100 SM 2540G* % Solids

Certifications: CTDOH

[TOC_3]Wet Chemistry Parameters[TOC]

Chromium, Hexavalent Sample Notes:Log-in Notes:

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York Project (SDG) No.

15E0465

York Sample ID: 15E0465-09

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil15-133-0436 / 31-12 24th Ave.

[TOC_3]Wet Chemistry Parameters[TOC]

Sample Prepared by Method: EPA SW846-3060

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

LOD/MDL LOQ

Reported to

ND mg/kg dry 118540-29-9 SC05/13/2015 07:42 05/13/2015 14:480.5230.366 EPA 7196AChromium, Hexavalent

Certifications: NJDEP,CTDOH,NELAC-NY10854

Chromium, Trivalent

Sample Prepared by Method: Analysis Preparation

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOD/MDL LOQ

Reported to

15.8 mg/kg 116065-83-1 SC05/13/2015 07:39 05/13/2015 14:500.5000.250 Calculation* Chromium, Trivalent

Certifications:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 100 of 104

Volatile Analysis Sample Containers

Volatile Sample ContainerClient Sample IDLab ID

15E0465-01 40mL Vial with Stir Bar-Cool 4° CSB-1 (0-2')

15E0465-02 40mL Vial with Stir Bar-Cool 4° CSB-1 (13'-15')

15E0465-03 40mL Vial with Stir Bar-Cool 4° CSB-2 (0'-2')

15E0465-04 40mL Vial with Stir Bar-Cool 4° CSB-2 (13'-15')

15E0465-05 40mL Vial with Stir Bar-Cool 4° CSB-3 (0'-2')

15E0465-06 40mL Vial with Stir Bar-Cool 4° CSB-3 (13'-15')

15E0465-07 40mL Vial with Stir Bar-Cool 4° CSB-4 (0'-2')

15E0465-08 40mL Vial with Stir Bar-Cool 4° CSB-4 (4'-6')

15E0465-09 40mL Vial with Stir Bar-Cool 4° CSB-4 (13'-15')

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Notes and Definitions [TOC_1]Notes and Specific Data Flags[

SCAL-E The value reported is ESTIMATED. The value is estimated due to its behavior during initial calibration (average Rf>20%).

QL-02 This LCS analyte is outside Laboratory Recovery limits due the analyte behavior using the referenced method. The reference method

has certain limitations with respect to analytes of this nature.

M-MISpk The spike recovery was outside acceptance limits for the MS and/or MSD due to matrix interference. The SRM was within acceptance

limits, therefore data are acceptable.

M-HCSpk Sample conc. >10 X spike conc.

J Detected below the Reporting Limit but greater than or equal to the Method Detection Limit (MDL/LOD) or in the case of a TIC, the

result is an estimated concentration.

GC-Surr Surrogate recovery outside of control limits. The data was accepted based on valid recovery of the alternate surrogate.

CCV-E The value reported is ESTIMATED. The value is estimated due to its behavior during continuing calibration verification (>20%

Difference for average Rf or >20% Drift for quadratic fit).

Relative Percent DifferenceRPD

Not reportedNR

NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND

Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note

that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias

conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.

Low Bias

High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take

note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias

conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.

High Bias

Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is

outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high

due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.

Wet The data has been reported on an as-received (wet weight) basis

REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.

METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a

99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA

600 and 200 series methods.

RL

MDL

If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet

and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two.

For this reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as

Diphenylamine.

*

LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the

lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is

based upon NELAC 2009 Standards and applies to all analyses.

LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably

detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.

Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located

above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and

semi-volatile target compounds only.

Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 102 of 104

If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and

1268 which are non-target aroclors for some regulatory lists.

2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user

should take note.

Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.

Certification for pH is no longer offered by NYDOH ELAP.

For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a

verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

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Page 104 of 104

APPENDIX G

LABORATORY ANALYTICAL REPORTS FOR SOIL VAPOR SAMPLES

Technical Report

prepared for:

Athenica Environmental Services, Inc.45-09 Greenpoint Avenue

Long Island City NY, 11104

Attention: Ezgi Karayel

Report Date: 05/14/2015

Client Project ID: 15-133-0436 / 31-12 24th Ave

York Project (SDG) No.: 15E0464

CT Cert. No. PH-0723 New Jersey Cert. No. CT-005 New York Cert. No. 10854 PA Cert. No. 68-04440

120 RESEARCH DRIVE FAX (203) 357-0166(203) 325-1371STRATFORD, CT 06615

Page 1 of 13

Client Sample IDYork Sample ID Matrix Date Collected Date Received

SV-115E0464-01 Soil Vapor 05/12/2015 05/12/2015

SV-215E0464-02 Soil Vapor 05/12/2015 05/12/2015

Client Project ID: 15-133-0436 / 31-12 24th Ave

York Project (SDG) No.: 15E0464

Report Date: 05/14/2015

Attention: Ezgi Karayel

Long Island City NY, 11104

45-09 Greenpoint Avenue

Athenica Environmental Services, Inc.

Purpose and Results

This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory

on May 12, 2015 and listed below. The project was identified as your project: 15-133-0436 / 31-12 24th Ave.

The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data

summary tables.

All samples were received in proper condition meeting the customary acceptance requirements for environmental samples

except those indicated under the Notes section of this report.

All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags,

the meaning of which are explained in the attachment to this report, and case narrative if applicable.

The results of the analyses, which are all reported on dry weight basis (soils) unless otherwise noted, are detailed in the

following pages.

Please contact Client Services at 203.325.1371 with any questions regarding this report.

[TOC_1] Introduction and Sample Cross Reference [

General Notes for York Project (SDG) No.: 15E0464

1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to

the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest

standard utilized for the calibration where applicable.

2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.

3. York's liability for the above data is limited to the dollar value paid to York for the referenced project .

4. This report shall not be reproduced without the written approval of York Analytical Laboratories , Inc.

5. All samples were received in proper condition for analysis with proper documentation, unless otherwise noted.

6. All analyses conducted met method or Laboratory SOP requirements. See the Qualifiers and/or Narrative sections for further information.

7. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.

8. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.

Approved By:

Laboratory Director

Date: 05/14/2015

Benjamin Gulizia

OC_2]General Notes Relating to this Report[TOC]

Page 2 of 13

SV-1

York Project (SDG) No.

15E0464

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil Vapor15-133-0436 / 31-12 24th Ave

[TOC_2]SV-1[TOC]

15E0464-01

[TOC_3]Volatile Organic Compounds in Air by GC/MS[TOC]

Volatile Organics, EPA TO15 Full List

Sample Prepared by Method: EPA TO15 PREP

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOQ

Reported to

LOD/MDL

ND ug/m³ 20.16630-20-6 ALD05/13/2015 23:31 05/13/2015 23:31146.9 EPA TO-15* 1,1,1,2-TetrachloroethaneCertifications:

ND ug/m³ 20.1671-55-6 ALD05/13/2015 23:31 05/13/2015 23:311111 EPA TO-151,1,1-TrichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1679-34-5 ALD05/13/2015 23:31 05/13/2015 23:311414 EPA TO-151,1,2,2-TetrachloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1676-13-1 ALD05/13/2015 23:31 05/13/2015 23:311515 EPA TO-151,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1679-00-5 ALD05/13/2015 23:31 05/13/2015 23:311111 EPA TO-151,1,2-TrichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-34-3 ALD05/13/2015 23:31 05/13/2015 23:318.28.2 EPA TO-151,1-DichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-35-4 ALD05/13/2015 23:31 05/13/2015 23:318.08.0 EPA TO-151,1-DichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16120-82-1 ALD05/13/2015 23:31 05/13/2015 23:311515 EPA TO-151,2,4-TrichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1695-63-6 ALD05/13/2015 23:31 05/13/2015 23:319.99.9 EPA TO-151,2,4-TrimethylbenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16106-93-4 ALD05/13/2015 23:31 05/13/2015 23:311515 EPA TO-151,2-DibromoethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1695-50-1 ALD05/13/2015 23:31 05/13/2015 23:311212 EPA TO-151,2-DichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16107-06-2 ALD05/13/2015 23:31 05/13/2015 23:318.28.2 EPA TO-151,2-DichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1678-87-5 ALD05/13/2015 23:31 05/13/2015 23:319.39.3 EPA TO-151,2-DichloropropaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1676-14-2 ALD05/13/2015 23:31 05/13/2015 23:311414 EPA TO-151,2-DichlorotetrafluoroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16108-67-8 ALD05/13/2015 23:31 05/13/2015 23:319.99.9 EPA TO-151,3,5-TrimethylbenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16106-99-0 ALD05/13/2015 23:31 05/13/2015 23:318.78.7 EPA TO-151,3-ButadieneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16541-73-1 ALD05/13/2015 23:31 05/13/2015 23:311212 EPA TO-151,3-DichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16142-28-9 ALD05/13/2015 23:31 05/13/2015 23:319.39.3 EPA TO-15* 1,3-DichloropropaneCertifications:

ND ug/m³ 20.16106-46-7 ALD05/13/2015 23:31 05/13/2015 23:311212 EPA TO-151,4-DichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16123-91-1 ALD05/13/2015 23:31 05/13/2015 23:317.37.3 EPA TO-151,4-DioxaneCertifications: NELAC-NY10854,NJDEP

120 ug/m³ 20.1678-93-3 ALD05/13/2015 23:31 05/13/2015 23:315.95.9 EPA TO-152-Butanone

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16591-78-6 ALD05/13/2015 23:31 05/13/2015 23:311717 EPA TO-15* 2-HexanoneCertifications:

ND ug/m³ 20.16107-05-1 ALD05/13/2015 23:31 05/13/2015 23:316.36.3 EPA TO-15* 3-ChloropropeneCertifications:

[TOC_1]Sample Results[TOC]

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 3 of 13

SV-1

York Project (SDG) No.

15E0464

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil Vapor15-133-0436 / 31-12 24th Ave

15E0464-01

Volatile Organics, EPA TO15 Full List

Sample Prepared by Method: EPA TO15 PREP

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOQ

Reported to

LOD/MDL

ND ug/m³ 20.16108-10-1 ALD05/13/2015 23:31 05/13/2015 23:318.38.3 EPA TO-154-Methyl-2-pentanoneCertifications: NELAC-NY10854,NJDEP

960 ug/m³ 20.1667-64-1 ALD05/13/2015 23:31 05/13/2015 23:314.84.8 EPA TO-15Acetone

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16107-13-1 ALD05/13/2015 23:31 05/13/2015 23:314.44.4 EPA TO-15* AcrylonitrileCertifications:

ND ug/m³ 20.1671-43-2 ALD05/13/2015 23:31 05/13/2015 23:316.46.4 EPA TO-15BenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16100-44-7 ALD05/13/2015 23:31 05/13/2015 23:311010 EPA TO-15Benzyl chlorideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-27-4 ALD05/13/2015 23:31 05/13/2015 23:311313 EPA TO-15BromodichloromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-25-2 ALD05/13/2015 23:31 05/13/2015 23:312121 EPA TO-15BromoformCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1674-83-9 ALD05/13/2015 23:31 05/13/2015 23:317.87.8 EPA TO-15BromomethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-15-0 ALD05/13/2015 23:31 05/13/2015 23:316.36.3 EPA TO-15Carbon disulfideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1656-23-5 ALD05/13/2015 23:31 05/13/2015 23:313.23.2 EPA TO-15Carbon tetrachlorideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16108-90-7 ALD05/13/2015 23:31 05/13/2015 23:319.39.3 EPA TO-15ChlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-00-3 ALD05/13/2015 23:31 05/13/2015 23:315.35.3 EPA TO-15ChloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1667-66-3 ALD05/13/2015 23:31 05/13/2015 23:319.89.8 EPA TO-15ChloroformCertifications: NELAC-NY10854,NJDEP

17 ug/m³ 20.1674-87-3 ALD05/13/2015 23:31 05/13/2015 23:314.24.2 EPA TO-15Chloromethane

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16156-59-2 ALD05/13/2015 23:31 05/13/2015 23:318.08.0 EPA TO-15cis-1,2-DichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1610061-01-5 ALD05/13/2015 23:31 05/13/2015 23:319.19.1 EPA TO-15cis-1,3-DichloropropyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16110-82-7 ALD05/13/2015 23:31 05/13/2015 23:316.96.9 EPA TO-15CyclohexaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16124-48-1 ALD05/13/2015 23:31 05/13/2015 23:311616 EPA TO-15DibromochloromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-71-8 ALD05/13/2015 23:31 05/13/2015 23:311010 EPA TO-15DichlorodifluoromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16141-78-6 ALD05/13/2015 23:31 05/13/2015 23:311515 EPA TO-15* Ethyl acetateCertifications:

ND ug/m³ 20.16100-41-4 ALD05/13/2015 23:31 05/13/2015 23:318.88.8 EPA TO-15Ethyl BenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1687-68-3 ALD05/13/2015 23:31 05/13/2015 23:312222 EPA TO-15HexachlorobutadieneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1667-63-0 ALD05/13/2015 23:31 05/13/2015 23:319.99.9 EPA TO-15IsopropanolCertifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 4 of 13

SV-1

York Project (SDG) No.

15E0464

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil Vapor15-133-0436 / 31-12 24th Ave

15E0464-01

Volatile Organics, EPA TO15 Full List

Sample Prepared by Method: EPA TO15 PREP

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOQ

Reported to

LOD/MDL

ND ug/m³ 20.1680-62-6 ALD05/13/2015 23:31 05/13/2015 23:318.38.3 EPA TO-15Methyl MethacrylateCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.161634-04-4 ALD05/13/2015 23:31 05/13/2015 23:317.37.3 EPA TO-15Methyl tert-butyl ether (MTBE)Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-09-2 ALD05/13/2015 23:31 05/13/2015 23:311414 EPA TO-15Methylene chlorideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16142-82-5 ALD05/13/2015 23:31 05/13/2015 23:318.38.3 EPA TO-15n-HeptaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16110-54-3 ALD05/13/2015 23:31 05/13/2015 23:317.17.1 EPA TO-15n-HexaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1695-47-6 ALD05/13/2015 23:31 05/13/2015 23:318.88.8 EPA TO-15o-XyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16179601-23-1 ALD05/13/2015 23:31 05/13/2015 23:311818 EPA TO-15p- & m- XylenesCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16622-96-8 ALD05/13/2015 23:31 05/13/2015 23:319.99.9 EPA TO-15* p-EthyltolueneCertifications:

79 ug/m³ 20.16115-07-1 ALD05/13/2015 23:31 05/13/2015 23:313.53.5 EPA TO-15* Propylene

Certifications:

ND ug/m³ 20.16100-42-5 ALD05/13/2015 23:31 05/13/2015 23:318.68.6 EPA TO-15StyreneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16127-18-4 ALD05/13/2015 23:31 05/13/2015 23:313.43.4 EPA TO-15TetrachloroethyleneCertifications: NELAC-NY10854,NJDEP

61 ug/m³ 20.16109-99-9 ALD05/13/2015 23:31 05/13/2015 23:315.95.9 EPA TO-15* Tetrahydrofuran

Certifications:

ND ug/m³ 20.16108-88-3 ALD05/13/2015 23:31 05/13/2015 23:317.67.6 EPA TO-15TolueneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16156-60-5 ALD05/13/2015 23:31 05/13/2015 23:318.08.0 EPA TO-15trans-1,2-DichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1610061-02-6 ALD05/13/2015 23:31 05/13/2015 23:319.19.1 EPA TO-15trans-1,3-DichloropropyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1679-01-6 ALD05/13/2015 23:31 05/13/2015 23:312.72.7 EPA TO-15TrichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-69-4 ALD05/13/2015 23:31 05/13/2015 23:311111 EPA TO-15Trichlorofluoromethane (Freon 11)Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16108-05-4 ALD05/13/2015 23:31 05/13/2015 23:317.17.1 EPA TO-15Vinyl acetateCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.16593-60-2 ALD05/13/2015 23:31 05/13/2015 23:318.88.8 EPA TO-15Vinyl bromideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 20.1675-01-4 ALD05/13/2015 23:31 05/13/2015 23:311.31.3 EPA TO-15Vinyl ChlorideCertifications: NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

72-11894.1 %Surrogate: p-Bromofluorobenzene460-00-4

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 5 of 13

SV-2

York Project (SDG) No.

15E0464

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil Vapor15-133-0436 / 31-12 24th Ave

[TOC_2]SV-2[TOC]

15E0464-02

Volatile Organics, EPA TO15 Full List

Sample Prepared by Method: EPA TO15 PREP

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOQ

Reported to

LOD/MDL

ND ug/m³ 24.59630-20-6 ALD05/14/2015 00:21 05/14/2015 00:21178.4 EPA TO-15* 1,1,1,2-TetrachloroethaneCertifications:

ND ug/m³ 24.5971-55-6 ALD05/14/2015 00:21 05/14/2015 00:211313 EPA TO-151,1,1-TrichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5979-34-5 ALD05/14/2015 00:21 05/14/2015 00:211717 EPA TO-151,1,2,2-TetrachloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5976-13-1 ALD05/14/2015 00:21 05/14/2015 00:211919 EPA TO-151,1,2-Trichloro-1,2,2-trifluoroethane

(Freon 113) Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5979-00-5 ALD05/14/2015 00:21 05/14/2015 00:211313 EPA TO-151,1,2-TrichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-34-3 ALD05/14/2015 00:21 05/14/2015 00:211010 EPA TO-151,1-DichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-35-4 ALD05/14/2015 00:21 05/14/2015 00:219.79.7 EPA TO-151,1-DichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59120-82-1 ALD05/14/2015 00:21 05/14/2015 00:211818 EPA TO-151,2,4-TrichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5995-63-6 ALD05/14/2015 00:21 05/14/2015 00:211212 EPA TO-151,2,4-TrimethylbenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59106-93-4 ALD05/14/2015 00:21 05/14/2015 00:211919 EPA TO-151,2-DibromoethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5995-50-1 ALD05/14/2015 00:21 05/14/2015 00:211515 EPA TO-151,2-DichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59107-06-2 ALD05/14/2015 00:21 05/14/2015 00:211010 EPA TO-151,2-DichloroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5978-87-5 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-151,2-DichloropropaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5976-14-2 ALD05/14/2015 00:21 05/14/2015 00:211717 EPA TO-151,2-DichlorotetrafluoroethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59108-67-8 ALD05/14/2015 00:21 05/14/2015 00:211212 EPA TO-151,3,5-TrimethylbenzeneCertifications: NELAC-NY10854,NJDEP

170 ug/m³ 24.59106-99-0 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-151,3-Butadiene

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59541-73-1 ALD05/14/2015 00:21 05/14/2015 00:211515 EPA TO-151,3-DichlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59142-28-9 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15* 1,3-DichloropropaneCertifications:

180 ug/m³ 24.59106-46-7 ALD05/14/2015 00:21 05/14/2015 00:211515 EPA TO-151,4-Dichlorobenzene

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59123-91-1 ALD05/14/2015 00:21 05/14/2015 00:218.98.9 EPA TO-151,4-DioxaneCertifications: NELAC-NY10854,NJDEP

250 ug/m³ 24.5978-93-3 ALD05/14/2015 00:21 05/14/2015 00:217.37.3 EPA TO-152-Butanone

Certifications: NELAC-NY10854,NJDEP

44 ug/m³ 24.59591-78-6 ALD05/14/2015 00:21 05/14/2015 00:212020 EPA TO-15* 2-Hexanone

Certifications:

ND ug/m³ 24.59107-05-1 ALD05/14/2015 00:21 05/14/2015 00:217.77.7 EPA TO-15* 3-ChloropropeneCertifications:

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 6 of 13

SV-2

York Project (SDG) No.

15E0464

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil Vapor15-133-0436 / 31-12 24th Ave

15E0464-02

Volatile Organics, EPA TO15 Full List

Sample Prepared by Method: EPA TO15 PREP

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOQ

Reported to

LOD/MDL

ND ug/m³ 24.59108-10-1 ALD05/14/2015 00:21 05/14/2015 00:211010 EPA TO-154-Methyl-2-pentanoneCertifications: NELAC-NY10854,NJDEP

5000 ug/m³ 24.5967-64-1 ALD05/14/2015 00:21 05/14/2015 00:215.85.8 EPA TO-15Acetone E

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59107-13-1 ALD05/14/2015 00:21 05/14/2015 00:215.35.3 EPA TO-15* AcrylonitrileCertifications:

16 ug/m³ 24.5971-43-2 ALD05/14/2015 00:21 05/14/2015 00:217.97.9 EPA TO-15Benzene

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59100-44-7 ALD05/14/2015 00:21 05/14/2015 00:211313 EPA TO-15Benzyl chlorideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-27-4 ALD05/14/2015 00:21 05/14/2015 00:211515 EPA TO-15BromodichloromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-25-2 ALD05/14/2015 00:21 05/14/2015 00:212525 EPA TO-15BromoformCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5974-83-9 ALD05/14/2015 00:21 05/14/2015 00:219.59.5 EPA TO-15BromomethaneCertifications: NELAC-NY10854,NJDEP

12 ug/m³ 24.5975-15-0 ALD05/14/2015 00:21 05/14/2015 00:217.77.7 EPA TO-15Carbon disulfide

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5956-23-5 ALD05/14/2015 00:21 05/14/2015 00:213.93.9 EPA TO-15Carbon tetrachlorideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59108-90-7 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15ChlorobenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-00-3 ALD05/14/2015 00:21 05/14/2015 00:216.56.5 EPA TO-15ChloroethaneCertifications: NELAC-NY10854,NJDEP

13 ug/m³ 24.5967-66-3 ALD05/14/2015 00:21 05/14/2015 00:211212 EPA TO-15Chloroform

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5974-87-3 ALD05/14/2015 00:21 05/14/2015 00:215.15.1 EPA TO-15ChloromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59156-59-2 ALD05/14/2015 00:21 05/14/2015 00:219.79.7 EPA TO-15cis-1,2-DichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5910061-01-5 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15cis-1,3-DichloropropyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59110-82-7 ALD05/14/2015 00:21 05/14/2015 00:218.58.5 EPA TO-15CyclohexaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59124-48-1 ALD05/14/2015 00:21 05/14/2015 00:212020 EPA TO-15DibromochloromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-71-8 ALD05/14/2015 00:21 05/14/2015 00:211212 EPA TO-15DichlorodifluoromethaneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59141-78-6 ALD05/14/2015 00:21 05/14/2015 00:211818 EPA TO-15* Ethyl acetateCertifications:

ND ug/m³ 24.59100-41-4 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15Ethyl BenzeneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5987-68-3 ALD05/14/2015 00:21 05/14/2015 00:212626 EPA TO-15HexachlorobutadieneCertifications: NELAC-NY10854,NJDEP

36 ug/m³ 24.5967-63-0 ALD05/14/2015 00:21 05/14/2015 00:211212 EPA TO-15Isopropanol

Certifications: NELAC-NY10854,NJDEP

120 RESEARCH DRIVE STRATFORD, CT 06615 (203) 325-1371 FAX (203) 357-0166

Page 7 of 13

SV-2

York Project (SDG) No.

15E0464

York Sample ID:

Sample Information

Client Project ID

Client Sample ID:

Matrix Collection Date/Time Date Received

May 12, 2015 3:00 pm 05/12/2015Soil Vapor15-133-0436 / 31-12 24th Ave

15E0464-02

Volatile Organics, EPA TO15 Full List

Sample Prepared by Method: EPA TO15 PREP

Parameter Result Prepared AnalyzedReference MethodFlag DilutionUnitsCAS No. AnalystDate/Time Date/Time

Sample Notes:Log-in Notes:

LOQ

Reported to

LOD/MDL

ND ug/m³ 24.5980-62-6 ALD05/14/2015 00:21 05/14/2015 00:211010 EPA TO-15Methyl MethacrylateCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.591634-04-4 ALD05/14/2015 00:21 05/14/2015 00:218.98.9 EPA TO-15Methyl tert-butyl ether (MTBE)Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-09-2 ALD05/14/2015 00:21 05/14/2015 00:211717 EPA TO-15Methylene chlorideCertifications: NELAC-NY10854,NJDEP

29 ug/m³ 24.59142-82-5 ALD05/14/2015 00:21 05/14/2015 00:211010 EPA TO-15n-Heptane

Certifications: NELAC-NY10854,NJDEP

47 ug/m³ 24.59110-54-3 ALD05/14/2015 00:21 05/14/2015 00:218.78.7 EPA TO-15n-Hexane

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5995-47-6 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15o-XyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59179601-23-1 ALD05/14/2015 00:21 05/14/2015 00:212121 EPA TO-15p- & m- XylenesCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59622-96-8 ALD05/14/2015 00:21 05/14/2015 00:211212 EPA TO-15* p-EthyltolueneCertifications:

850 ug/m³ 24.59115-07-1 ALD05/14/2015 00:21 05/14/2015 00:214.24.2 EPA TO-15* Propylene

Certifications:

ND ug/m³ 24.59100-42-5 ALD05/14/2015 00:21 05/14/2015 00:211010 EPA TO-15StyreneCertifications: NELAC-NY10854,NJDEP

17 ug/m³ 24.59127-18-4 ALD05/14/2015 00:21 05/14/2015 00:214.24.2 EPA TO-15Tetrachloroethylene

Certifications: NELAC-NY10854,NJDEP

80 ug/m³ 24.59109-99-9 ALD05/14/2015 00:21 05/14/2015 00:217.37.3 EPA TO-15* Tetrahydrofuran

Certifications:

11 ug/m³ 24.59108-88-3 ALD05/14/2015 00:21 05/14/2015 00:219.39.3 EPA TO-15Toluene

Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59156-60-5 ALD05/14/2015 00:21 05/14/2015 00:219.79.7 EPA TO-15trans-1,2-DichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5910061-02-6 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15trans-1,3-DichloropropyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5979-01-6 ALD05/14/2015 00:21 05/14/2015 00:213.33.3 EPA TO-15TrichloroethyleneCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-69-4 ALD05/14/2015 00:21 05/14/2015 00:211414 EPA TO-15Trichlorofluoromethane (Freon 11)Certifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59108-05-4 ALD05/14/2015 00:21 05/14/2015 00:218.78.7 EPA TO-15Vinyl acetateCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.59593-60-2 ALD05/14/2015 00:21 05/14/2015 00:211111 EPA TO-15Vinyl bromideCertifications: NELAC-NY10854,NJDEP

ND ug/m³ 24.5975-01-4 ALD05/14/2015 00:21 05/14/2015 00:211.61.6 EPA TO-15Vinyl ChlorideCertifications: NELAC-NY10854,NJDEP

Surrogate Recoveries Result Acceptance Range

72-11890.9 %Surrogate: p-Bromofluorobenzene460-00-4

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Analytical Batch Summary

OC_1]Quality Batch Summary[TOC]

Batch ID: Preparation Method: Prepared By:BE50440 EPA TO15 PREP ALD

YORK Sample ID Client Sample ID Preparation Date

15E0464-01 SV-1 05/13/15

15E0464-02 SV-2 05/14/15

BE50440-BLK1 Blank 05/13/15

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OC_1]QA/QC Summary Data[TOC]

Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Volatile Organic Compounds in Air by GC/MS - Quality Control Data

York Analytical Laboratories, Inc.

Flag

olatile Organic Compounds in Air by GC/MS EPA TO-15[TOC]

Batch BE50440 - EPA TO15 PREP

Blank (BE50440-BLK1) Prepared & Analyzed: 05/13/2015

ug/m³ND 0.691,1,1,2-Tetrachloroethane

"ND 0.551,1,1-Trichloroethane

"ND 0.691,1,2,2-Tetrachloroethane

"ND 0.771,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)

"ND 0.551,1,2-Trichloroethane

"ND 0.401,1-Dichloroethane

"ND 0.401,1-Dichloroethylene

"ND 0.741,2,4-Trichlorobenzene

"ND 0.491,2,4-Trimethylbenzene

"ND 0.771,2-Dibromoethane

"ND 0.601,2-Dichlorobenzene

"ND 0.401,2-Dichloroethane

"ND 0.461,2-Dichloropropane

"ND 0.701,2-Dichlorotetrafluoroethane

"ND 0.491,3,5-Trimethylbenzene

"ND 0.431,3-Butadiene

"ND 0.601,3-Dichlorobenzene

"ND 0.461,3-Dichloropropane

"ND 0.601,4-Dichlorobenzene

"ND 0.361,4-Dioxane

"ND 0.292-Butanone

"ND 0.822-Hexanone

"ND 0.313-Chloropropene

"ND 0.414-Methyl-2-pentanone

"ND 0.24Acetone

"ND 0.22Acrylonitrile

"ND 0.32Benzene

"ND 0.52Benzyl chloride

"ND 0.62Bromodichloromethane

"ND 1.0Bromoform

"ND 0.39Bromomethane

"ND 0.31Carbon disulfide

"ND 0.16Carbon tetrachloride

"ND 0.46Chlorobenzene

"ND 0.26Chloroethane

"ND 0.49Chloroform

"ND 0.21Chloromethane

"ND 0.40cis-1,2-Dichloroethylene

"ND 0.45cis-1,3-Dichloropropylene

"ND 0.34Cyclohexane

"ND 0.80Dibromochloromethane

"ND 0.49Dichlorodifluoromethane

"ND 0.72Ethyl acetate

"ND 0.43Ethyl Benzene

"ND 1.1Hexachlorobutadiene

"ND 0.49Isopropanol

"ND 0.41Methyl Methacrylate

"ND 0.36Methyl tert-butyl ether (MTBE)

"ND 0.69Methylene chloride

"ND 0.41n-Heptane

"ND 0.35n-Hexane

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Result Limit

Reporting

Units Level

Spike

Result

Source*

%REC

%REC

Limits RPD

RPD

Limit Flag Analyte

Volatile Organic Compounds in Air by GC/MS - Quality Control Data

York Analytical Laboratories, Inc.

Flag

Batch BE50440 - EPA TO15 PREP

Blank (BE50440-BLK1) Prepared & Analyzed: 05/13/2015

ug/m³ND 0.43o-Xylene

"ND 0.87p- & m- Xylenes

"ND 0.49p-Ethyltoluene

"ND 0.17Propylene

"ND 0.43Styrene

"ND 0.17Tetrachloroethylene

"ND 0.29Tetrahydrofuran

"ND 0.38Toluene

"ND 0.40trans-1,2-Dichloroethylene

"ND 0.45trans-1,3-Dichloropropylene

"ND 0.13Trichloroethylene

"ND 0.56Trichlorofluoromethane (Freon 11)

"ND 0.35Vinyl acetate

"ND 0.44Vinyl bromide

"ND 0.064Vinyl Chloride

ppbv 10.4 72-118Surrogate: p-Bromofluorobenzene 88.79.22

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Notes and Definitions [TOC_1]Notes and Specific Data Flags[

E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered

an estimate.

Relative Percent DifferenceRPD

Not reportedNR

NOT DETECTED - the analyte is not detected at the Reported to level (LOQ/RL or LOD/MDL)ND

Low Bias flag indicates that the recovery of the flagged analyte is below the laboratory or regulatory lower control limit. The data user should take note

that this analyte may be biased low but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias

conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.

Low Bias

High Bias flag indicates that the recovery of the flagged analyte is above the laboratory or regulatory upper control limit. The data user should take

note that this analyte may be biased high but should evaluate multiple lines of evidence including the LCS and site-specific MS/MSD data to draw bias

conclusions. In cases where no site-specific MS/MSD was requested, only the LCS data can be used to evaluate such bias.

High Bias

Non-Dir. Non-dir. flag (Non-Directional Bias ) indicates that the Relative Percent Difference (RPD) (a measure of precision) among the MS and MSD data is

outside the laboratory or regulatory control limit. This alerts the data user where the MS and MSD are from site-specific samples that the RPD is high

due to either non-homogeneous distribution of target analyte between the MS/MSD or indicates poor reproducibility for other reasons.

Wet The data has been reported on an as-received (wet weight) basis

REPORTING LIMIT - the minimum reportable value based upon the lowest point in the analyte calibration curve.

METHOD DETECTION LIMIT - a statistically derived estimate of the minimum amount of a substance an analytical system can reliably detect with a

99% confidence that the concentration of the substance is greater than zero. This is based upon 40 CFR Part 136 Appendix B and applies only to EPA

600 and 200 series methods.

RL

MDL

If EPA SW-846 method 8270 is included herein it is noted that the target compound N-nitrosodiphenylamine (NDPA) decomposes in the gas chromatographic inlet

and cannot be separated from diphenylamine (DPA). These results could actually represent 100% DPA, 100% NDPA or some combination of the two.

For this reason, York reports the combined result for n-nitrosodiphenylamine and diphenylamine for either of these compounds as a combined concentration as

Diphenylamine.

If Total PCBs are detected and the target aroclors reported are "Not detected", the Total PCB value is reported due to the presence of either or both Aroclors 1262 and

1268 which are non-target aroclors for some regulatory lists.

2-chloroethylvinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user

should take note.

Semi-Volatile and Volatile analyses are reported down to the LOD/MDL, with values between the LOD/MDL and the LOQ being "J" flagged as estimated results.

Certification for pH is no longer offered by NYDOH ELAP.

*

LOQ LIMIT OF QUANTITATION - the minimum concentration of a target analyte that can be reported within a specified degree of confidence . This is the

lowest point in an analyte calibration curve that has been subjected to all steps of the processing/analysis and verified to meet defined criteria. This is

based upon NELAC 2009 Standards and applies to all analyses.

LOD LIMIT OF DETECTION - a verified estimate of the minimum concentration of a substance in a given matrix that an analytical process can reliably

detect. This is based upon NELAC 2009 Standards and applies to all analyses conducted under the auspices of EPA SW-846.

Reported to This indicates that the data for a particular analysis is reported to either the LOD/MDL, or the LOQ/RL. In cases where the "Reported to" is located

above the LOD/MDL, any value between this and the LOQ represents an estimated value which is "J" flagged accordingly. This applies to volatile and

semi-volatile target compounds only.

Analyte is not certified or the state of the samples origination does not offer certification for the Analyte .

For analyses by EPA SW-846-8270D, the Limit of Quantitation (LOQ) reported for benzidine is based upon the lowest standard used for calibration and is not a

verified LOQ due to this compound's propensity for oxidative losses during extraction/concentration procedures and non-reproducible chromatographic performance.

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