LIMITED PHASE II ENVIRONMENTAL - NDEP · 5.3 Analytical Testing The soil sample was delivered under chain-of-custody protocol toAsset Laboratories located in Las Vegas, Nevada. The

LIMITED PHASE II ENVIRONMENTAL

SITE ASSESSMENT

DEW DROP INN MAIN STREET

APN 002-053-04 SILVER PEAK

ESMERALDA COUNTY NEVADA

Contract DEP14-008 Task Number M20-17

Prepared for:

State of Nevada Department of Conservation & Natural Resources

Division of Environmental Protection 901 South Stewart Street, Suite 3005

Carson City, Nevada 89701

ATTN: Mr. David Friedman

August 24, 2017

Reno 815 Maestro Drive Reno, Nevada 89511 Ph: 775.829.2245

Las Vegas 1915 N. Green Valley Parkway Suite 200 Henderson, Nevada 89074 Ph: 702.260.4961

www.mcgin.com

| Site Remediation

| Soil & Groundwater Investigations

| Closure Optimization

| Air Quality Permitting & Modeling

| Brownfields Redevelopment

| Permitting & Compliance

| NEPA Studies

| Phase I Assessments

| Indoor Air Quality

| Storm Water & Spill Plans

| Underground Tank Services

| Toxics Release Inventory

| Geographic Information Systems

| Groundwater Modeling

| Litigation Support & Expert Witness

| Mining Plans of Operations

| Mining Exploration Notices

| Abandoned Mine Lands

Limited Phase II ESA: APN 002-053-04, Main Street, Silver Peak, Nevada i

V:\\Projects\BRN\BRN041\ McGinley & Associates, Inc.

TABLE OF CONTENTS

1. INTRODUCTION ....................................................................................................... 1

2. BACKGROUND ......................................................................................................... 1

3. OBJECTIVES ............................................................................................................ 1

4. SCOPE OF SERVICES ............................................................................................. 2

5. ENVIRONMENTAL INVESTIGATION ....................................................................... 2

5.1 Trenching ......................................................................................................... 2 5.1.1 55-Gallon Drum Area ................................................................................................ 2 5.1.2 Extruding Pipe Area .................................................................................................. 2

5.2 Air Survey ......................................................................................................... 3 5.3 Analytical Testing ............................................................................................. 3 5.4 Analytical results .............................................................................................. 3

6. DATA QUALITY ......................................................................................................... 4

6.1 Soil Sampling ................................................................................................... 4 6.2 Laboratory Analytical Data ............................................................................... 4

7. SUMMARY OF FIELD ACTIVITIES ........................................................................... 4

8. FINDINGS AND CONCLUSIONS .............................................................................. 5

9. RECOMMENDATIONS ............................................................................................. 5

10. LIMITATIONS ............................................................................................................ 5

11. CLOSING .................................................................................................................. 6

12. REFERENCES .......................................................................................................... 7

TABLES

Table 1A Summary of Soil Analytical Results Table 1B Summary of Liquid Analytical Results

FIGURES Figure 1 Project Location Map Figure 2 Site Map - Showing Soil Sample Locations and Analytical Results

APPENDICES Appendix A Chain-of-Custody Records and Laboratory Reports for Soil Samples

Limited Phase II ESA: APN 002-053-04, Main Street, Silver Peak, Nevada 1


1. INTRODUCTION

McGinley & Associates (MGA) conducted a Limited Phase II Environmental Site Assessment(ESA) at the subject property located on Main Street in Silver Peak, NV. These assessmentactivities were conducted on behalf of Nye County and the Rural Desert SouthwestBrownfields Coalition (RDSBC) for the Nevada Division of Environmental Protection (NDEP)utilizing funding provided by the State of Nevada Brownfields Program (NBP), ContractDEP14-008, Task Number M20-17. MGA conducted this investigation for the purpose ofinvestigating previously identified recognized environmental conditions (RECs) on the subjectproperty. The site location is indicated in Figure 1.

2. BACKGROUND

A Phase I ESA of the Subject Property was conducted by BEC Environmental, Inc. for NDEPon behalf of Nye County and the RDSBC and dated December 22, 2016. The Phase I ESAreport concluded that the assessment revealed no evidence of recognized environmentalconditions (REC) or conditional recognized environmental conditions (CREC) in connectionwith the property except for the following:

1. Based on the historic and current mining activity in the vicinity of Silver Peak and thepresence of a mine access in the cellar of the Dew Drop Inn, the potential exists for vaporintrusion from the subsurface into the building.

2. Based on the presence of one closed, buried 55-gallon drum and one open 55-gallon drumwith an access to a larger space below ground surface, the potential exists for unidentifiedhazardous chemicals stored on site.

3. A possible vent-pipe was observed on the northwest exterior of the Dew Drop Inn building,potentially indicative of an underground storage tank (UST) on the subject site.

4. A tar-like, highly viscous substance was observed seeping from beneath a wooden palleton the subject site, indicative of the potential release of petroleum hydrocarbons on thesubject site.

5. Based on the age of the buildings, the potential exists for asbestos-containing materials inthe Dew Drop Inn, the Shifting Sands Bar, and in two piles of drywall and shingles on theexterior portion of the subject site.

3. OBJECTIVES

The objectives of the ESA activities were to address the RECs identified during in the previousPhase I ESA (Section 2) and to assess for the presence of regulated, hazardous, or potentiallyhazardous chemical constituents in the soils located on the subject property. As required by theState of Nevada Administrative Code (NAC) 459, all MGA services were supervised andreviewed by a Nevada Certified Environmental Manager (CEM).



4. SCOPE OF SERVICES

The field activities performed by MGA for the limited Phase II ESA were conducted in accordance with EPA and MGA Standard Operating Procedures (SOP) and the site-specific Health and Safety Plan (HASP). On site activities consisted of the following:

• Trenching in two areas onsite (near two abandoned 55-gallon drums and next to an open metal pipe end extruding from the ground);

• Collecting one soil sample and one liquid sample;

• Conducting an air survey in the basement of the Dew Drop Inn using a photoionizing detector (PID)

• Analytical testing of the soil and liquid sample; and

• Preparing a technical report complete with findings and recommendations.

5. ENVIRONMENTAL INVESTIGATION

Limited Phase II ESA field activities were performed by MGA on June 20, 2017. At the time of the assessment, the wood pallet with a tar-like substance, as characterized as a REC in the Phase I ESA, appeared to be de minimis in nature. Therefore, this REC was not investigated as part of this assessment.

5.1 Trenching In order to assess two of the RECs identified in Section 2, trenches were excavated with a backhoe in the vicinity of the two 55-gallon drums and proximal to a four-inch steel pipe extruding from the ground.

5.1.1 55-Gallon Drum Area Upon examination of the semi-buried 55-gallon drums (REC #2), it was determined that the pit below the drum openings (as seen through the top of the drums) appeared to be consistent with a former grease trap or otherwise analogous waste liquid storage vessel. Due to overhead wires, a tree growing in the vicinity, the building close by, and an effort to limit damage to, or potential leakage of, the underground storage vessel, the excavator dug one trench (T-1) to the west of the 55-gallon barrels and just north of the former Shifting Sands Bar to characterize the soil adjacent to the drums. Due to the existing site conditions, approximately two, one-foot wide bucket loads were removed from this area and one representative soil sample was collected. This soil sample was collected directly from the trench and subsequently placed into laboratory provided glass jars. Additionally, a liquid sample was collected from the water-sludge mixture contained within the pit below one of the drum openings. The purpose of collecting the liquid sample for analysis was to provide a contaminant profile for future removal and disposal. The sample locations are shown on Figure 2.

5.1.2 Extruding Pipe Area The “vent pipe” described in the Phase I ESA as a vent for a possible underground storage tank (REC #3) was observed to be constructed of plastic and appeared to be associated with a freezer room located within the former Shifting Sands Bar. Based on these observations, it was determined that this pipe did not appear to be a vent pipe associated with an UST. However, a separate four-inch steel vent pipe located on the northwest side of the Dew Drop Inn building



was discovered. Due to the pipe being constructed of steel and open to the air above the roof-line of the building, a possibility existed that the pipe was associated with an UST or a tunnel. Therefore, a trench (T-2) was excavated in this location between the former Dew Drop Inn and Shifting Sands Bar buildings and proximal to the pipe. The trench uncovered an underground tunnel trending north-south and it appeared that the tunnel was constructed as if it was an underground mine shaft. The purpose of the tunnel is unknown. Based on these findings, it appeared that the four-inch steel pipe was possibly an air pipe for the tunnel. No soil samples were collected for environmental analysis.

5.2 Air Survey A photoionization detector (PID) was used to determine if the “mine access tunnel” in the cellar of the Dew Drop Inn was a potential source of volatile organic compounds (VOCs). Upon inspection of the cellar and based on an interview with the property owner, it was determined that the “mine access tunnel” is an 80-foot deep hand-dug well that is no longer in use. Although it did not appear that a mine tunnel existed within the cellar, the PID was used for several minutes and there was no indication of the presence of VOCs in the cellar.

5.3 Analytical Testing The soil sample was delivered under chain-of-custody protocol to Asset Laboratories located in Las Vegas, Nevada. The soil sample was analyzed for volatile organic compounds (VOC) by EPA Method 8260, polycyclic aromatic hydrocarbons (PAH) via EPA Method 8270CSIM, total petroleum hydrocarbons (TPH) in the diesel range (DRO), oil range (ORO), and gasoline range (GRO) by EPA Method 8015B, and total metals including lead, cadmium, and chromium by EPA Method 6010B. The liquid sample (“Sludge”) was a characterization sample to determine hazardous/non-hazardous status and was analyzed for pH by EPA Method 9040B, ignitability by EPA Method 1020A, VOCs by EPA Method 8260B, GRO by EPA Method 8015B, and RCRA 8 Metals by EPA 6010B for arsenic, barium, cadmium, chromium, lead, selenium, and silver, and EPA Method 7470A for total mercury by cold vapor technique. A copy of the chain-of-custody records for the soil and liquid samples are provided in Appendix A.

5.4 Analytical results The analytical results for the soil sample are presented in Table 1A and summarized below: • No detectable concentrations of TPH in the gasoline range (GRO), VOCs, or total cadmium

were reported above laboratory reporting limits; • The concentration of TPH in the diesel range (DRO) was reported to be 12 mg/kg; • The concentration of TPH in the oil range (ORO) was reported to be 29 mg/kg; • The chrysene concentration was reported to be 7.0 mg/kg; • The fluoranthene concentration was reported to be 6.5 mg/kg; • The pyrene concentration was reported to be 6.5 mg/kg; • The chromium concentration was reported to be 14.0 mg/kg; and • The lead concentration was reported to be 110 mg/kg. The analytical results for the liquid sample is presented in Table 1B and summarized below: • The pH of the liquid was reported to be 8.4 • No detectable concentrations of TPH, VOCs, PAHs, or cadmium were reported for the



sample. • The ignitability of the sample was reported to be greater than 212 degrees Fahrenheit; • The arsenic concentration was reported to be 0.055 mg/L; • The barium concentration was reported to be 0.11 mg/L; • The chromium concentration was reported to be 0.0062 mg/L; and • The lead concentration was reported to be 0.0055 mg/L.

6. DATA QUALITY

6.1 Soil Sampling The soil sample was collected in accordance with EPA and MGA SOPs. Care was taken to minimize sample disturbance. Soil and liquid samples were preserved in a cooler and transported under proper chain-of-custody protocol until they were received by the laboratory (see chain-of-custody records provided in Appendix A).

6.2 Laboratory Analytical Data The laboratory analytical data for the soil sample was in compliance with the data quality objectives established in the laboratory’s SOP.

7. SUMMARY OF FIELD ACTIVITIES

• Two trenches were excavated by the property owner using a backhoe. One trench was located proximal to two uncovered 55-gallon drums and one trench was located proximal to a four-inch steel pipe extruding from the ground and extending above the roof-line of the Dew Drop Inn;

• One soil sample was collected at 1.0 feet bgs within the trench located proximal to the two 55-gallon drums;

• One liquid sample was collected from the pit located below one of the two 55-gallon drums. The purpose of the liquid sample was to characterize the liquid for future removal and disposal;

• An investigation of the possible underground storage tank (UST) near the former Shifting Sands Bar concluded that a potential vent pipe did not appear to be associated with a UST. The vent pipe was plastic and appeared to lead to a freezer room located within the Shifting Sands structure. Therefore, it was concluded that no environmental hazards appeared to exist and no soil samples were collected proximal to the plastic pipe extruding from the ground.

• An investigation into the steel four-inch pipe extruding from the ground proximal to the Dew Drop Inn structure was conducted by trenching adjacent to the pipe and towards the Shifting Sands structure. The trench discovered an underground tunnel running in a north-south direction and it was determined that the steel pipe appeared to be used for supplying air to the tunnel. Therefore, no soil samples were collected from this trench or the area proximal to the extruding steel pipe; and

• An air survey using a PID instrument was conducted within the cellar of the Dew Drop Inn proximal to a large opening that was determined to be an 80-foot deep hand-dug well.



8. FINDINGS AND CONCLUSIONS

McGinley & Associates (MGA) performed a Limited Phase II ESA of the former Dew Drop Inn property located on Main Street in Silver Peak, NV. These assessment activities were conducted on behalf of Nye County and the RDSBC for the Nevada Division of Environmental Protection (NDEP). MGA conducted this investigation for the purpose of investigating previously identified recognized environmental conditions (RECs) on the subject property. The following are findings from the assessment: • None of the constituents analyzed for in the soil sample were reported to have

concentrations greater than EPA Region 9 RSLs or State of Nevada Reportable Concentrations.

• No VOCs were discovered emanating from the 80-foot deep hand-dug well. • The liquid sample collected from the pit beneath one of the 55-gallon drums is non-

hazardous.

9. RECOMMENDATIONS

Based on the results of the assessment activities, the following recommendations are provided: • Based on the analytical laboratory data for the collected soil sample and the determination

that heating oil tanks are likely not present on the property, MGA is of the opinion that no further assessment for the Subject Property, with regards to potential surface soil contamination, is warranted at this time.

• Based on the results reported for the liquid sample collected from the pit located below one of the two 55-gallon drums, it appears that the liquid can be characterized as non-hazardous. The liquid should be disposed of as such in accordance with local, state, and federal regulations. It is recommended that this be conducted prior to removing the below ground appurtenances. Upon removal of the below ground appurtenances, it is recommended that additional assessment of the soil below the grease trap be assessed at that time.

10. LIMITATIONS

The conclusions presented herein are based on analytical data and observations. MGA makes no warranties or guarantees as to the accuracy or completeness of information provided or compiled by others. The results reported herein are applicable to the time the sampling occurred. Changes in site conditions may occur as a result of illegal dumping practices, prevailing winds, rainfall, or other factors. It should be recognized that definition and evaluation of environmental conditions is a difficult and inexact science. Judgments and opinions leading to conclusions and recommendations are generally made with an incomplete knowledge of the conditions present. More extensive studies, including additional environmental investigations, can tend to reduce the inherent uncertainties associated with such studies. Additional information not found or unavailable to MGA at the time of writing this report may result in a modification to the conclusions and recommendations contained herein. This report is not a legal opinion. The services performed by MGA have been conducted in a manner consistent with the level of care ordinarily exercised by members of our profession



currently practicing under similar conditions. No other warranty, expressed or implied, is made. The use of the word "certify" in this document constitutes an expression of professional opinion regarding those facts or findings which are the subject of the certification and does not constitute a warranty or guarantee, either expressed or implied.

11. CLOSING

Should you have any questions regarding this report please contact Brett Bottenberg at (702) 260-4961 or via email at [email protected]. Respectfully submitted, McGinley and Associates, Inc.

Jonathan T. Payne Staff Geologist Reviewed by: I hereby certify that I am responsible for the services described in this document and for the preparation of this document. The services described in this document have been provided in a manner consistent with the current standards of the profession and to the best of my knowledge comply with all applicable federal, state and local statutes, regulations, and ordinances. Brett C. Bottenberg, C.E.M. #1690, Exp. 10/07/17 Senior Project Manager



12. REFERENCES

BEC Environmental, “Phase I Environmental Site Assessment”, December 2016.

MGA, “Standard Operating Procedures”, March 1, 2001. US EPA, “Soil Sampling Standard Operating Procedure”, August 19

VO

Cs (

mg/

kg)

GR

O (T

PH-P

)D

RO

OR

OT

PH-E

Chr

ysen

eFl

uora

nthe

nePy

rene

Cad

miu

mC

hrom

ium

Lea

dN

one

Det

ecte

d

SS-1

2Tr

ench

1.0

20-J

un-1

7N

D12

2941

7.0

6.5

6.5

ND

1411

0-

100

100

100

100

2,10

030

,000

23,0

008

3880

0-

* EP

A Re

gion

9 R

SL -

Indu

stria

l - (b

lue

text

)*

Stat

e of

Nev

ada

Repo

rtab

le C

once

ntra

tion

(red

text

) - if

EPA

RSL

not

ava

ilabl

e

Tab

le 1

A.

Sum

mar

y of

Soi

l Ana

lytic

al R

esul

tsPA

H-S

IM (m

g/kg

)R

CR

A M

etal

s (m

g/kg

)

Scre

enin

g L

evel

*

Sam

ple

ID

TPH

(mg/

kg)

Dat

eD

epth

(fbg

s)L

ocat

ion

TPH

-P (m

g/L

)Ig

nita

bilit

ypH

VO

Cs (

mg/

L)

PAH

s (m

g/L

)

GR

Ode

g. F

S.U

.A

rsen

icB

ariu

mC

adm

ium

Chr

omiu

mL

ead

Non

e D

etec

ted

Non

e D

etec

ted

SLU

DG

E-1

Pit

1.5

20-J

un-1

7N

D>2

128.

40.

055

0.11

ND

0.00

620.

0055

ND

ND

* EP

A Re

gion

9 R

SL -

Indu

stria

l - (b

lue

text

)*

Stat

e of

Nev

ada

Repo

rtab

le C

once

ntra

tion

(red

text

) - if

EPA

RSL

not

ava

ilabl

e

Tab

le 1

B.

Sum

mar

y of

Liq

uid

Ana

lytic

al R

esul

ts

Sam

ple

IDL

ocat

ion

Dep

th (f

bgs)

Dat

e

RC

RA

Met

als (

mg/

L)

!!!!!

PROJECT LOCATION MAP-SHOWING-

EXTENT OF EXCAVATIONSAMPLE LOCATIONS

SILVER PEAK, NV

REF. DESIGNED

DRAWNCHECKEDAPPROVED

HCHC

JPJP

Fig 1 - Project Location Map

NAD 1983 UTM Zone 11N

FILE:

COORDINATE SYSTEM:

7/3/2017

TITLE:

REVISION:BRN041JOB NO.:

FIGURE 1

DATE:

-

±

0 450

Feet

LegendSubject Property

!!SS - 12

@1'

Sludge - 1

!!!!!

SITE MAP-SHOWING-

EXTENT OF EXCAVATIONSAMPLE LOCATIONS

SILVER PEAK, NV

REF. DESIGNED

DRAWNCHECKEDAPPROVED

HCHC

JPJP

Fig 2 - Site Map

NAD 1983 UTM Zone 11N

FILE:

COORDINATE SYSTEM:

7/3/2017

TITLE:

REVISION:BRN041JOB NO.:

FIGURE 2

DATE:

-

±

0 30

Feet

Legend! Sludge! Soil Sample Location

BarrelGrease PitBuilding Footprint

State Rout

e 265

APPENDIX A Chain-of-Custody Records and Laboratory Reports for Soil Samples

NEVADA|P:702.307.2659 F:702.307.2691 3151 W. Post Rd., Las Vegas, NV 89118 ELAP Cert 2676 | NV Cert NV00922

ORELAP/NELAP Cert 4046 “Serving Clients with Passion and Professionalism”

CALIFORNIA|P:562.219.7435 F:562.219.7436 11110 Artesia Blvd., Ste B, Cerritos, CA 90703

ELAP Cert 2921 EPA ID CA01638

July 03, 2017

Mc.Ginley and AssociatesBrett Bottenberg

Attention: Brett Bottenberg

RE: SILVER PEAK SOIL, BRN041

Workorder No.: N024683FAX: (702) 260-4968TEL: (702) 260-4961

6280 S. Valley View Blvd. Suite 604Las Vegas, NV 89118

This is an amended report. Please disregard all previous documentation that corresponds to the page(s) enclosed.

Thank you for the opportunity to service the needs of your company.

Please feel free to call me at (702) 307-2659 if I can be of further assistance to your company.

Sincerely,

Puri Romualdo

Laboratory Director

Enclosed are the results for sample(s) received on June 21, 2017 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications.

The cover letter is an integral part of this analytical report. This Laboratory Report cannot be reproduced in part or in its entirety without written permission from the client and Advanced Technology Laboratories - Las Vegas.

1 of 44





03-Jul-17Date:ASSET Laboratories

Project: SILVER PEAK SOIL, BRN041CLIENT: Mc.Ginley and Associates

Lab Order: N024683CASE NARRATIVE

SAMPLE RECEIVING/GENERAL COMMENTS:

Samples were received intact with proper chain of custody documentation.

Cooler temperature and sample preservation were verified upon receipt of samples if applicable.

Information on sample receipt conditions including discrepancies can be found in attached Sample Receipt Checklist Form.

Samples were analyzed within method holding time.

Analytical Comments for EPA 6010B (Soil):

Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are outside recovery criteria for Lead possibly due to matrix interference. The associated Laboratory Control Sample (LCS) recovery was acceptable.

Analytical Comments for EPA 8270C_SIM (Soil):

Some analytes were reported non-detect (ND) with dilution on sample N024683-001 due to associated internal standard not meeting method criteria possibly due to matrix interference. Sample was analyzed with dilution and internal standard met method criteria. Affected analyte for this failed internal standard was reported at dilution that meet internal standard recovery limit.

RPD for Matrix Spike (MS)/Matrix Spike Duplicate (MSD) is outside criteria for Benzo(k)fluoranthene; however, the analytical batch was validated by the Laboratory Control Sample (LCS).

Analytical Comments for EPA 8260B (Soil):

RPD for Matrix Spike (MS)/Matrix Spike Duplicate (MSD) is outside criteria for 1,1,2,2-Tetrachloroethane; however, the analytical batch was validated by the Laboratory Control Sample (LCS).

Analytical Comments for EPA 8260B (Water):

Page 1 of 2

2 of 44






Lab Order: N024683CASE NARRATIVE

Dilution was necessary due to matrix.

Page 2 of 2

3 of 44







Lab Order: N024683Work Order Sample Summary

Lab Sample ID Client Sample ID Collection DateMatrix Date Received

Contract No:

Date Reported

N024683-001A SS-12 6/20/2017 11:15:00 AM 6/21/2017 6/30/2017Soil

N024683-001B SS-12 6/20/2017 11:15:00 AM 6/21/2017 6/30/2017Soil

N024683-002A SLUDGE-1 6/20/2017 11:00:00 AM 6/21/2017 6/30/2017Water

N024683-002B SLUDGE-1 6/20/2017 11:00:00 AM 6/21/2017 6/30/2017Water

N024683-002C SLUDGE-1 6/20/2017 11:00:00 AM 6/21/2017 6/30/2017Water

N024683-002D SLUDGE-1 6/20/2017 11:00:00 AM 6/21/2017 6/30/2017Water

Page 1 of 1

4 of 44





Project: SILVER PEAK SOIL, BRN041

Client Sample ID: SS-12Collection Date: 6/20/2017 11:15:00 AM

Matrix: SOIL

Analyses Result Qual Units Date Analyzed

CLIENT: Mc.Ginley and AssociatesLab Order: N024683

DF

Lab ID: N024683-001

ASSET Laboratories Print Date: 03-Jul-17

PQL

ANALYTICAL RESULTS

SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS-SIMEPA 8270CSIM

Analyst: JJS

EPA 3546

RunID: NV00922-MS9_170625A 62632QC Batch: PrepDate 6/23/2017

1-Methylnaphthalene 6/26/2017 06:12 AM5.0 µg/Kg 1ND2-Methylnaphthalene 6/26/2017 06:12 AM5.0 µg/Kg 1NDAcenaphthene 6/26/2017 06:12 AM5.0 µg/Kg 1NDAcenaphthylene 6/26/2017 06:12 AM5.0 µg/Kg 1NDAnthracene 6/26/2017 06:12 AM5.0 µg/Kg 1NDBenzo(a)anthracene 6/26/2017 06:12 AM5.0 µg/Kg 1NDBenzo(a)pyrene 6/26/2017 04:19 AM50 µg/Kg 10NDBenzo(b)fluoranthene 6/26/2017 04:19 AM50 µg/Kg 10NDBenzo(g,h,i)perylene 6/26/2017 04:19 AM50 µg/Kg 10NDBenzo(k)fluoranthene 6/26/2017 04:19 AM50 µg/Kg 10NDChrysene 6/26/2017 06:12 AM5.0 µg/Kg 17.0Dibenz(a,h)anthracene 6/26/2017 04:19 AM50 µg/Kg 10NDFluoranthene 6/26/2017 06:12 AM5.0 µg/Kg 16.5Fluorene 6/26/2017 06:12 AM5.0 µg/Kg 1NDIndeno(1,2,3-cd)pyrene 6/26/2017 04:19 AM50 µg/Kg 10NDNaphthalene 6/26/2017 06:12 AM5.0 µg/Kg 1NDPhenanthrene 6/26/2017 06:12 AM5.0 µg/Kg 1NDPyrene 6/26/2017 06:12 AM5.0 µg/Kg 16.5 Surr: 1,2-Dichlorobenzene-d4 6/26/2017 06:12 AM25-130 %REC 161.0 Surr: 2-Fluorobiphenyl 6/26/2017 06:12 AM23-130 %REC 182.0 Surr: 4-Terphenyl-d14 6/26/2017 06:12 AM24-130 %REC 195.0 Surr: Nitrobenzene-d5 6/26/2017 06:12 AM22-130 %REC 191.0

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: RBRunID: NV00922-MS5_170623A P17VS072QC Batch: PrepDate

1,1,1,2-Tetrachloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,1,1-Trichloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,1,2,2-Tetrachloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,1,2-Trichloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,1-Dichloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,1-Dichloroethene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,1-Dichloropropene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2,3-Trichlorobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2,3-Trichloropropane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2,4-Trichlorobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2,4-Trimethylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation rangeH Holding times for preparation or analysis exceeded ND Not Detected at the Reporting LimitS Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified

DO Surrogate Diluted Out

5 of 44







Matrix: SOIL



DF

Lab ID: N024683-001


PQL

ANALYTICAL RESULTS



1,2-Dibromo-3-chloropropane 6/24/2017 03:01 AM10 µg/Kg 1ND1,2-Dibromoethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2-Dichlorobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2-Dichloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,2-Dichloropropane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,3,5-Trimethylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,3-Dichlorobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,3-Dichloropropane 6/24/2017 03:01 AM5.0 µg/Kg 1ND1,4-Dichlorobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1ND2,2-Dichloropropane 6/24/2017 03:01 AM5.0 µg/Kg 1ND2-Butanone 6/24/2017 03:01 AM50 µg/Kg 1ND2-Chlorotoluene 6/24/2017 03:01 AM5.0 µg/Kg 1ND4-Chlorotoluene 6/24/2017 03:01 AM5.0 µg/Kg 1ND4-Isopropyltoluene 6/24/2017 03:01 AM5.0 µg/Kg 1NDBenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDBromobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDBromodichloromethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDBromoform 6/24/2017 03:01 AM5.0 µg/Kg 1NDBromomethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDCarbon tetrachloride 6/24/2017 03:01 AM5.0 µg/Kg 1NDChlorobenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDChloroethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDChloroform 6/24/2017 03:01 AM5.0 µg/Kg 1NDChloromethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDcis-1,2-Dichloroethene 6/24/2017 03:01 AM5.0 µg/Kg 1NDcis-1,3-Dichloropropene 6/24/2017 03:01 AM5.0 µg/Kg 1NDDibromochloromethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDDibromomethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDDichlorodifluoromethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDEthylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDFreon-113 6/24/2017 03:01 AM5.0 µg/Kg 1NDHexachlorobutadiene 6/24/2017 03:01 AM5.0 µg/Kg 1NDIsopropylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDm,p-Xylene 6/24/2017 03:01 AM10 µg/Kg 1NDMethylene chloride 6/24/2017 03:01 AM5.0 µg/Kg 1NDMTBE 6/24/2017 03:01 AM5.0 µg/Kg 1ND



6 of 44







Matrix: SOIL



DF

Lab ID: N024683-001


PQL

ANALYTICAL RESULTS



n-Butylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDn-Propylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDNaphthalene 6/24/2017 03:01 AM5.0 µg/Kg 1NDo-Xylene 6/24/2017 03:01 AM5.0 µg/Kg 1NDsec-Butylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDStyrene 6/24/2017 03:01 AM5.0 µg/Kg 1NDtert-Butylbenzene 6/24/2017 03:01 AM5.0 µg/Kg 1NDTetrachloroethene 6/24/2017 03:01 AM5.0 µg/Kg 1NDToluene 6/24/2017 03:01 AM5.0 µg/Kg 1NDtrans-1,2-Dichloroethene 6/24/2017 03:01 AM5.0 µg/Kg 1NDTrichloroethene 6/24/2017 03:01 AM5.0 µg/Kg 1NDTrichlorofluoromethane 6/24/2017 03:01 AM5.0 µg/Kg 1NDVinyl chloride 6/24/2017 03:01 AM5.0 µg/Kg 1ND Surr: 1,2-Dichloroethane-d4 6/24/2017 03:01 AM71-154 %REC 1123 Surr: 4-Bromofluorobenzene 6/24/2017 03:01 AM80-125 %REC 1102 Surr: Dibromofluoromethane 6/24/2017 03:01 AM80-128 %REC 1110 Surr: Toluene-d8 6/24/2017 03:01 AM80-120 %REC 1102

DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FIDEPA 8015B

Analyst: QCE

EPA 3550B

RunID: NV00922-GC1_170627A 62664QC Batch: PrepDate 6/27/2017

DRO 6/27/2017 02:07 PM10 mg/Kg 112ORO 6/27/2017 02:07 PM10 mg/Kg 129 Surr: p-Terphenyl 6/27/2017 02:07 PM38-152 %REC 174.8

GASOLINE RANGE ORGANICS BY GC/FIDEPA 8015B

Analyst: RBRunID: NV00922-GC4_170623A E17VS110QC Batch: PrepDate

GRO 6/23/2017 04:55 PM1.0 mg/Kg 1ND Surr: Chlorobenzene - d5 6/23/2017 04:55 PM46-157 %REC 1134

TOTAL METALS BY ICPEPA 6010B

Analyst: CEI

EPA 3050B

RunID: NV00922-ICP2_170623D 62615QC Batch: PrepDate 6/22/2017

Cadmium 6/23/2017 06:43 PM1.0 mg/Kg 1NDChromium 6/23/2017 06:43 PM1.0 mg/Kg 114Lead 6/23/2017 06:43 PM1.0 mg/Kg 1110



7 of 44






Client Sample ID: SLUDGE-1Collection Date: 6/20/2017 11:00:00 AM

Matrix: WATER



DF

Lab ID: N024683-002


PQL

ANALYTICAL RESULTS

PHEPA 9040B

Analyst: LRRunID: NV00922-WC_170621C R115907QC Batch: PrepDate

pH 6/21/2017 04:20 PM0.10 pH Units 18.4Temp. at time of pH Analysis 6/21/2017 04:20 PM0 °C 126

IGNITABILITY BY SETAFLASH CLOSED-CUPEPA 1020A

Analyst: RBRunID: NV00922-WC_170625A R115948QC Batch: PrepDate

Ignitability 6/25/20170 DEG F 1>212VOLATILE ORGANIC COMPOUNDS BY GC/MS

EPA 8260B

Analyst: RBRunID: NV00922-MS5_170622B P17VW102QC Batch: PrepDate

1,1,1,2-Tetrachloroethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,1,1-Trichloroethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,1,2,2-Tetrachloroethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,1,2-Trichloroethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,1-Dichloroethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,1-Dichloroethene 6/23/2017 06:43 AM2.5 µg/L 5ND1,1-Dichloropropene 6/23/2017 06:43 AM2.5 µg/L 5ND1,2,3-Trichlorobenzene 6/23/2017 06:43 AM2.5 µg/L 5ND1,2,3-Trichloropropane 6/23/2017 06:43 AM2.5 µg/L 5ND1,2,4-Trichlorobenzene 6/23/2017 06:43 AM2.5 µg/L 5ND1,2,4-Trimethylbenzene 6/23/2017 06:43 AM2.5 µg/L 5ND1,2-Dibromo-3-chloropropane 6/23/2017 06:43 AM5.0 µg/L 5ND1,2-Dibromoethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,2-Dichlorobenzene 6/23/2017 06:43 AM2.5 µg/L 5ND1,2-Dichloroethane 6/23/2017 06:43 AM2.5 µg/L 5ND1,2-Dichloropropane 6/23/2017 06:43 AM2.5 µg/L 5ND1,3,5-Trimethylbenzene 6/23/2017 06:43 AM2.5 µg/L 5ND1,3-Dichlorobenzene 6/23/2017 06:43 AM2.5 µg/L 5ND1,3-Dichloropropane 6/23/2017 06:43 AM2.5 µg/L 5ND1,4-Dichlorobenzene 6/23/2017 06:43 AM2.5 µg/L 5ND2,2-Dichloropropane 6/23/2017 06:43 AM2.5 µg/L 5ND2-Butanone 6/23/2017 06:43 AM25 µg/L 5ND2-Chlorotoluene 6/23/2017 06:43 AM2.5 µg/L 5ND4-Chlorotoluene 6/23/2017 06:43 AM2.5 µg/L 5ND4-Isopropyltoluene 6/23/2017 06:43 AM2.5 µg/L 5NDBenzene 6/23/2017 06:43 AM2.5 µg/L 5ND



8 of 44







Matrix: WATER



DF

Lab ID: N024683-002


PQL

ANALYTICAL RESULTS



Bromobenzene 6/23/2017 06:43 AM2.5 µg/L 5NDBromodichloromethane 6/23/2017 06:43 AM2.5 µg/L 5NDBromoform 6/23/2017 06:43 AM2.5 µg/L 5NDBromomethane 6/23/2017 06:43 AM5.0 µg/L 5NDCarbon tetrachloride 6/23/2017 06:43 AM2.5 µg/L 5NDChlorobenzene 6/23/2017 06:43 AM2.5 µg/L 5NDChloroethane 6/23/2017 06:43 AM5.0 µg/L 5NDChloroform 6/23/2017 06:43 AM2.5 µg/L 5NDChloromethane 6/23/2017 06:43 AM2.5 µg/L 5NDcis-1,2-Dichloroethene 6/23/2017 06:43 AM2.5 µg/L 5NDcis-1,3-Dichloropropene 6/23/2017 06:43 AM2.5 µg/L 5NDDibromochloromethane 6/23/2017 06:43 AM2.5 µg/L 5NDDibromomethane 6/23/2017 06:43 AM2.5 µg/L 5NDDichlorodifluoromethane 6/23/2017 06:43 AM2.5 µg/L 5NDEthylbenzene 6/23/2017 06:43 AM2.5 µg/L 5NDFreon-113 6/23/2017 06:43 AM2.5 µg/L 5NDHexachlorobutadiene 6/23/2017 06:43 AM2.5 µg/L 5NDIsopropylbenzene 6/23/2017 06:43 AM2.5 µg/L 5NDm,p-Xylene 6/23/2017 06:43 AM5.0 µg/L 5NDMethylene chloride 6/23/2017 06:43 AM10 µg/L 5NDMTBE 6/23/2017 06:43 AM2.5 µg/L 5NDn-Butylbenzene 6/23/2017 06:43 AM2.5 µg/L 5NDn-Propylbenzene 6/23/2017 06:43 AM2.5 µg/L 5NDNaphthalene 6/23/2017 06:43 AM2.5 µg/L 5NDo-Xylene 6/23/2017 06:43 AM2.5 µg/L 5NDsec-Butylbenzene 6/23/2017 06:43 AM2.5 µg/L 5NDStyrene 6/23/2017 06:43 AM2.5 µg/L 5NDtert-Butylbenzene 6/23/2017 06:43 AM2.5 µg/L 5NDTetrachloroethene 6/23/2017 06:43 AM2.5 µg/L 5NDToluene 6/23/2017 06:43 AM2.5 µg/L 5NDtrans-1,2-Dichloroethene 6/23/2017 06:43 AM2.5 µg/L 5NDTrichloroethene 6/23/2017 06:43 AM2.5 µg/L 5NDTrichlorofluoromethane 6/23/2017 06:43 AM2.5 µg/L 5NDVinyl chloride 6/23/2017 06:43 AM2.5 µg/L 5ND Surr: 1,2-Dichloroethane-d4 6/23/2017 06:43 AM73-127 %REC 591.9 Surr: 4-Bromofluorobenzene 6/23/2017 06:43 AM80-120 %REC 591.9



9 of 44







Matrix: WATER



DF

Lab ID: N024683-002


PQL

ANALYTICAL RESULTS



Surr: Dibromofluoromethane 6/23/2017 06:43 AM80-121 %REC 593.8 Surr: Toluene-d8 6/23/2017 06:43 AM80-120 %REC 599.7

GASOLINE RANGE ORGANICS BY GC/FIDEPA 8015B

Analyst: QBMRunID: NV00922-GC4_170626A E17VW059QC Batch: PrepDate

GRO 6/26/2017 02:59 PM0.050 mg/L 1ND Surr: Chlorobenzene - d5 6/26/2017 02:59 PM72-143 %REC 1113

TOTAL MERCURY BY COLD VAPOR TECHNIQUEEPA 7470A

Analyst: CEIRunID: NV00922-AA1_170623C 62626QC Batch: PrepDate 6/23/2017

Mercury 6/23/2017 11:59 AM0.20 µg/L 1ND

TOTAL METALS BY ICPEPA 6010B

Analyst: CEI

EPA 3010A

RunID: NV00922-ICP2_170624A 62625QC Batch: PrepDate 6/23/2017

Arsenic 6/24/2017 10:38 AM0.010 mg/L 10.055Barium 6/23/2017 04:08 PM0.0030 mg/L 10.11Cadmium 6/23/2017 04:08 PM0.0030 mg/L 1NDChromium 6/24/2017 10:38 AM0.0030 mg/L 10.0062Lead 6/23/2017 04:08 PM0.0050 mg/L 10.0055Selenium 6/23/2017 04:08 PM0.010 mg/L 1NDSilver 6/23/2017 04:08 PM0.0030 mg/L 1ND



10 of 44







CLIENT: Mc.Ginley and AssociatesWork Order: N024683

ANALYTICAL QC SUMMARY REPORTTestCode: 1020a

Sample ID LCS-R115948

Batch ID: R115948 TestNo: EPA 1020A Analysis Date: 6/25/2017

Prep Date:

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: DEG F

PQL

Client ID: LCSW

RunNo: 115948

SeqNo: 2674030

LCSSampType: TestCode: 1020a

Ignitability 81.00 100 85 1150 081.000

Sample ID LCSD-R115948


Prep Date:


Units: DEG F

PQL

Client ID: LCSS02

RunNo: 115948

SeqNo: 2674031

LCSDSampType: TestCode: 1020a

Ignitability 81.00 100 85 115 100 0 81.00 081.000

Sample ID N024683-002C-DUP


Prep Date:


Units: DEG F

PQL

Client ID: ZZZZZZ

RunNo: 115948

SeqNo: 2674033

DUPSampType: TestCode: 1020a

Ignitability 100 0 0>212



Prep Date:


Units: DEG F

PQL

Client ID: ZZZZZZ

RunNo: 115948

SeqNo: 2674035





Prep Date:


Units: DEG F

PQL

Client ID: ZZZZZZ

RunNo: 115948

SeqNo: 2674037



Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interferenceDO Surrogate Diluted Out Calculations are based on raw values

11 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 6010_S

Sample ID MB-62615

Batch ID: 62615 TestNo: EPA 6010B Analysis Date: 6/23/2017

Prep Date: 6/22/2017


Units: mg/Kg

PQL

Client ID: PBS

RunNo: 115938

SeqNo: 2673384

MBLKSampType: TestCode: 6010_S

EPA 3050B

Arsenic 1.0NDBarium 1.0NDCadmium 1.0NDChromium 1.0NDLead 1.0NDSelenium 1.0NDSilver 1.0ND

Sample ID LCS-62615




Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 115938

SeqNo: 2673385

LCSSampType: TestCode: 6010_S

EPA 3050B

Arsenic 25.00 100 80 1201.0 025.010Barium 25.00 101 80 1201.0 025.252Cadmium 25.00 101 80 1201.0 025.232Chromium 25.00 101 80 1201.0 025.177Lead 25.00 101 80 1201.0 025.310Selenium 25.00 98.8 80 1201.0 024.690Silver 25.00 103 80 1201.0 025.723

Sample ID N024682-001B-MS




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115938

SeqNo: 2673397

MSSampType: TestCode: 6010_S

EPA 3050B

Barium 24.89 149 75 125 S1.0 96.07133.166Cadmium 24.89 87.0 75 1251.0 0.947622.593Chromium 24.89 78.5 75 1251.0 11.3530.892Lead 24.89 152 75 125 S1.0 110.9148.699Selenium 24.89 81.9 75 1251.0 020.378Silver 24.89 80.6 75 1251.0 0.810420.879



12 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 6010_S

Sample ID N024682-001B-MSD




Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115938

SeqNo: 2673398

MSDSampType: TestCode: 6010_S

EPA 3050B

Barium 24.99 152 75 125 20 S1.0 96.07 133.2 0.680134.075Cadmium 24.99 87.3 75 125 201.0 0.9476 22.59 0.75422.764Chromium 24.99 79.1 75 125 201.0 11.35 30.89 0.71931.115Lead 24.99 157 75 125 20 S1.0 110.9 148.7 0.951150.120Selenium 24.99 81.1 75 125 201.0 0 20.38 0.58920.259Silver 24.99 81.0 75 125 201.0 0.8104 20.88 0.82921.053





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115938

SeqNo: 2673705

MSSampType: TestCode: 6010_S

EPA 3050B

Arsenic 24.89 133 75 125 S1.0 32.0065.149





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115938

SeqNo: 2673706

MSDSampType: TestCode: 6010_S

EPA 3050B

Arsenic 24.99 134 75 125 20 S1.0 32.00 65.15 0.50465.478



13 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 6010_W

Sample ID MB-62625




Units: mg/L

PQL

Client ID: PBW

RunNo: 115936

SeqNo: 2673174

MBLKSampType: TestCode: 6010_W

EPA 3010A

Arsenic 0.010NDBarium 0.00300.00015Cadmium 0.0030NDChromium 0.00300.000536Lead 0.0050NDSelenium 0.010NDSilver 0.0030ND

Sample ID LCS-62625




Units: mg/L

PQL

Client ID: LCSW

RunNo: 115936

SeqNo: 2673175

LCSSampType: TestCode: 6010_W

EPA 3010A

Arsenic 0.5000 101 85 1150.010 00.505Barium 0.5000 101 85 1150.0030 00.506Cadmium 0.5000 101 85 1150.0030 00.507Chromium 0.5000 101 85 1150.0030 00.504Lead 0.5000 102 85 1150.0050 00.510Selenium 0.5000 102 85 1150.010 00.508Silver 0.5000 103 85 1150.0030 00.514

Sample ID N024683-002D-MS




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 115936

SeqNo: 2673179

MSSampType: TestCode: 6010_W

EPA 3010A

Barium 0.5000 84.2 75 1250.0030 0.11160.532Cadmium 0.5000 98.9 75 1250.0030 0.00067990.495Lead 0.5000 80.7 75 1250.0050 0.0054660.409Selenium 0.5000 89.6 75 1250.010 00.448Silver 0.5000 81.6 75 1250.0030 0.0011210.409



14 of 44








Sample ID N024683-002D-MSD




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 115936

SeqNo: 2673180

MSDSampType: TestCode: 6010_W

EPA 3010A

Barium 0.5000 84.2 75 125 200.0030 0.1116 0.5325 0.007900.533Cadmium 0.5000 98.9 75 125 200.0030 0.0006799 0.4951 0.02440.495Lead 0.5000 80.3 75 125 200.0050 0.005466 0.4092 0.5870.407Selenium 0.5000 90.0 75 125 200.010 0 0.4480 0.4940.450Silver 0.5000 81.7 75 125 200.0030 0.001121 0.4091 0.06890.409

Sample ID N024683-002D-MS




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 115936

SeqNo: 2673511


EPA 3010A

Arsenic 0.5000 90.6 75 1250.010 0.055500.508Chromium 0.5000 83.5 75 1250.0030 0.0062320.424

Sample ID N024683-002D-MSD




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 115936

SeqNo: 2673512


EPA 3010A

Arsenic 0.5000 90.0 75 125 200.010 0.05550 0.5084 0.6060.505Chromium 0.5000 83.6 75 125 200.0030 0.006232 0.4237 0.1570.424



15 of 44








Sample ID MB-62626

Batch ID: 62626 TestNo: EPA 7470A Analysis Date: 6/23/2017



Units: µg/L

PQL

Client ID: PBW

RunNo: 115929

SeqNo: 2672980

MBLKSampType: TestCode: 7470_W

Mercury 0.20ND

Sample ID LCS-62626




Units: µg/L

PQL

Client ID: LCSW

RunNo: 115929

SeqNo: 2672981

LCSSampType: TestCode: 7470_W

Mercury 5.000 96.7 85 1150.20 04.834

Sample ID N024691-003G-MS




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115929

SeqNo: 2672982


Mercury 5.000 95.8 75 1250.20 04.790

Sample ID N024691-003G-MSD




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115929

SeqNo: 2672983


Mercury 5.000 94.4 75 125 200.20 0 4.790 1.514.718



16 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 8015_S_DM H

Sample ID LCS-62664




Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 115995

SeqNo: 2677457

LCSSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 1000 91.9 67 11910 0918.878 Surr: p-Terphenyl 80.00 76.2 38 15260.932

Sample ID MB-62664




Units: mg/Kg

PQL

Client ID: PBS

RunNo: 115995

SeqNo: 2677458

MBLKSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 10NDORO 107.336 Surr: p-Terphenyl 80.00 75.4 38 15260.343





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115995

SeqNo: 2677563

MSSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 999.0 87.4 46 14310 7.549880.716 Surr: p-Terphenyl 79.92 72.8 38 15258.211





Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115995

SeqNo: 2677564

MSDSampType: TestCode: 8015_S_DM

EPA 3550B

DRO 999.0 89.3 46 143 2010 7.549 880.7 2.17900.005 Surr: p-Terphenyl 79.92 79.0 38 152 063.114



17 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 8015GAS_S

Sample ID E170623LCS

Batch ID: E17VS110 TestNo: EPA 8015B Analysis Date: 6/23/2017

Prep Date:


Units: mg/Kg

PQL

Client ID: LCSS

RunNo: 115949

SeqNo: 2674038

LCSSampType: TestCode: 8015GAS_S

GRO 5.000 127 74 1271.0 06.347 Surr: Chlorobenzene - d5 100.0 112 46 157112.297

Sample ID E170623MB1


Prep Date:


Units: mg/Kg

PQL

Client ID: PBS

RunNo: 115949

SeqNo: 2674039

MBLKSampType: TestCode: 8015GAS_S

GRO 1.00.068 Surr: Chlorobenzene - d5 100.0 124 46 157124.356

Sample ID N024682-006AMS


Prep Date:


Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115949

SeqNo: 2674041

MSSampType: TestCode: 8015GAS_S

GRO 5.000 111 27 1441.0 0.063005.626 Surr: Chlorobenzene - d5 100.0 118 46 157118.208

Sample ID N024682-006AMSD


Prep Date:


Units: mg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115949

SeqNo: 2674042

MSDSampType: TestCode: 8015GAS_S

GRO 5.000 118 27 144 201.0 0.06300 5.626 6.205.986 Surr: Chlorobenzene - d5 100.0 107 46 157 0107.265



18 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 8015GAS_WP

Sample ID E170626LCS

Batch ID: E17VW059 TestNo: EPA 8015B Analysis Date: 6/26/2017

Prep Date:


Units: mg/L

PQL

Client ID: LCSW

RunNo: 115977

SeqNo: 2675094

LCSSampType: TestCode: 8015GAS_W

GRO 1.000 122 74 1330.050 01.223 Surr: Chlorobenzene - d5 50.00 119 72 14359.304

Sample ID E170626MB1


Prep Date:


Units: mg/L

PQL

Client ID: PBW

RunNo: 115977

SeqNo: 2675095

MBLKSampType: TestCode: 8015GAS_W

GRO 0.050ND Surr: Chlorobenzene - d5 50.00 121 72 14360.263



Prep Date:


Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 115977

SeqNo: 2675103

MSSampType: TestCode: 8015GAS_W

GRO 1.000 101 74 1330.050 01.010 Surr: Chlorobenzene - d5 50.00 93.2 72 14346.609



Prep Date:


Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 115977

SeqNo: 2675104

MSDSampType: TestCode: 8015GAS_W

GRO 1.000 104 74 133 300.050 0 1.010 3.411.045 Surr: Chlorobenzene - d5 50.00 101 72 143 050.290



19 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 8260SOIL

Sample ID P170623LCS

Batch ID: P17VS072 TestNo: EPA 8260B Analysis Date: 6/24/2017

Prep Date:


Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 115944

SeqNo: 2674429

LCSSampType: TestCode: 8260SOIL

1,1,1,2-Tetrachloroethane 40.00 94.5 79 1235.0 037.8101,1,1-Trichloroethane 40.00 92.2 77 1265.0 036.8901,1,2,2-Tetrachloroethane 40.00 91.9 75 1275.0 036.7401,1,2-Trichloroethane 40.00 84.6 78 1165.0 033.8201,1-Dichloroethane 40.00 88.4 60 1345.0 035.3801,1-Dichloroethene 40.00 89.4 67 1295.0 035.7601,1-Dichloropropene 40.00 94.1 84 1325.0 037.6201,2,3-Trichlorobenzene 40.00 95.9 77 1275.0 038.3501,2,3-Trichloropropane 40.00 88.0 72 1255.0 035.2201,2,4-Trichlorobenzene 40.00 96.2 72 1285.0 038.4701,2,4-Trimethylbenzene 40.00 93.5 87 1305.0 037.4101,2-Dibromo-3-chloropropane 40.00 85.2 70 12810 034.0901,2-Dibromoethane 40.00 86.7 81 1215.0 034.6801,2-Dichlorobenzene 40.00 93.6 83 1265.0 037.4201,2-Dichloroethane 40.00 90.1 78 1195.0 036.0501,2-Dichloropropane 40.00 91.4 81 1205.0 036.5401,3,5-Trimethylbenzene 40.00 95.1 89 1295.0 038.0501,3-Dichlorobenzene 40.00 90.9 83 1245.0 036.3601,3-Dichloropropane 40.00 97.6 83 1235.0 039.0401,4-Dichlorobenzene 40.00 92.7 80 1255.0 037.0902,2-Dichloropropane 40.00 84.2 64 1355.0 033.6902-Butanone 400.0 84.5 20 16850 0338.0202-Chlorotoluene 40.00 91.8 83 1235.0 036.7304-Chlorotoluene 40.00 93.6 84 1285.0 037.4404-Isopropyltoluene 40.00 95.0 86 1365.0 038.000Benzene 40.00 89.2 83 1205.0 035.680Bromobenzene 40.00 89.3 81 1205.0 035.730Bromodichloromethane 40.00 92.3 81 1205.0 036.930Bromoform 40.00 88.7 72 1295.0 035.480Bromomethane 40.00 98.7 32 1525.0 039.480



20 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 115944

SeqNo: 2674429


Carbon tetrachloride 40.00 94.1 74 1355.0 037.650Chlorobenzene 40.00 93.9 84 1235.0 037.570Chloroethane 40.00 104 69 1535.0 041.780Chloroform 40.00 89.2 76 1165.0 035.670Chloromethane 40.00 98.3 47 1355.0 039.310cis-1,2-Dichloroethene 40.00 90.0 80 1195.0 035.990cis-1,3-Dichloropropene 40.00 95.6 82 1275.0 038.230Dibromochloromethane 40.00 93.6 81 1275.0 037.420Dibromomethane 40.00 91.1 79 1175.0 036.450Dichlorodifluoromethane 40.00 95.4 26 1885.0 038.140Ethylbenzene 40.00 91.9 84 1235.0 036.740Freon-113 40.00 80.2 48 1305.0 032.090Hexachlorobutadiene 40.00 93.7 77 1345.0 037.490Isopropylbenzene 40.00 78.6 66 1295.0 031.450m,p-Xylene 80.00 94.8 86 12610 075.850Methylene chloride 40.00 92.1 65 1315.0 036.850MTBE 40.00 88.8 70 1145.0 035.530n-Butylbenzene 40.00 93.0 79 1385.0 037.200n-Propylbenzene 40.00 95.7 86 1325.0 038.290Naphthalene 40.00 99.7 69 1245.0 039.860o-Xylene 40.00 96.7 87 1275.0 038.680sec-Butylbenzene 40.00 94.4 87 1345.0 037.770Styrene 40.00 92.2 88 1245.0 036.880tert-Butylbenzene 40.00 96.0 87 1345.0 038.390Tetrachloroethene 40.00 91.8 82 1275.0 036.710Toluene 40.00 84.8 78 1185.0 033.930trans-1,2-Dichloroethene 40.00 91.6 74 1245.0 036.630Trichloroethene 40.00 91.2 82 1235.0 036.500Trichlorofluoromethane 40.00 97.4 68 1485.0 038.970Vinyl chloride 40.00 104 61 1375.0 041.650



21 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 115944

SeqNo: 2674429


Surr: 1,2-Dichloroethane-d4 50.00 97.1 71 15448.570 Surr: 4-Bromofluorobenzene 50.00 103 80 12551.410 Surr: Dibromofluoromethane 50.00 104 80 12852.060 Surr: Toluene-d8 50.00 102 80 12050.880

Sample ID P170623MB3


Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 115944

SeqNo: 2674430

MBLKSampType: TestCode: 8260SOIL

1,1,1,2-Tetrachloroethane 5.0ND1,1,1-Trichloroethane 5.0ND1,1,2,2-Tetrachloroethane 5.0ND1,1,2-Trichloroethane 5.0ND1,1-Dichloroethane 5.0ND1,1-Dichloroethene 5.0ND1,1-Dichloropropene 5.0ND1,2,3-Trichlorobenzene 5.0ND1,2,3-Trichloropropane 5.0ND1,2,4-Trichlorobenzene 5.0ND1,2,4-Trimethylbenzene 5.0ND1,2-Dibromo-3-chloropropane 10ND1,2-Dibromoethane 5.0ND1,2-Dichlorobenzene 5.0ND1,2-Dichloroethane 5.0ND1,2-Dichloropropane 5.0ND1,3,5-Trimethylbenzene 5.0ND1,3-Dichlorobenzene 5.0ND1,3-Dichloropropane 5.0ND1,4-Dichlorobenzene 5.0ND2,2-Dichloropropane 5.0ND



22 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 115944

SeqNo: 2674430


2-Butanone 50ND2-Chlorotoluene 5.0ND4-Chlorotoluene 5.0ND4-Isopropyltoluene 5.0NDBenzene 5.0NDBromobenzene 5.0NDBromodichloromethane 5.0NDBromoform 5.0NDBromomethane 5.0NDCarbon tetrachloride 5.0NDChlorobenzene 5.0NDChloroethane 5.0NDChloroform 5.0NDChloromethane 5.0NDcis-1,2-Dichloroethene 5.0NDcis-1,3-Dichloropropene 5.0NDDibromochloromethane 5.0NDDibromomethane 5.0NDDichlorodifluoromethane 5.0NDEthylbenzene 5.0NDFreon-113 5.0NDHexachlorobutadiene 5.0NDIsopropylbenzene 5.0NDm,p-Xylene 10NDMethylene chloride 5.0NDMTBE 5.0NDn-Butylbenzene 5.0NDn-Propylbenzene 5.0NDNaphthalene 5.0NDo-Xylene 5.0ND



23 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: PBS

RunNo: 115944

SeqNo: 2674430


sec-Butylbenzene 5.0NDStyrene 5.0NDtert-Butylbenzene 5.0NDTetrachloroethene 5.0NDToluene 5.0NDtrans-1,2-Dichloroethene 5.0NDTrichloroethene 5.0NDTrichlorofluoromethane 5.0NDVinyl chloride 5.0ND Surr: 1,2-Dichloroethane-d4 50.00 106 71 15453.010 Surr: 4-Bromofluorobenzene 50.00 103 80 12551.320 Surr: Dibromofluoromethane 50.00 110 80 12854.970 Surr: Toluene-d8 50.00 105 80 12052.510



Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674441

MSSampType: TestCode: 8260SOIL

1,1,1,2-Tetrachloroethane 40.00 73.3 51 1295.0 029.3301,1,1-Trichloroethane 40.00 81.1 56 1285.0 032.4501,1,2,2-Tetrachloroethane 40.00 76.9 35 1705.0 030.7501,1,2-Trichloroethane 40.00 84.0 63 1345.0 033.5801,1-Dichloroethane 40.00 76.5 50 1235.0 030.5901,1-Dichloroethene 40.00 87.9 54 1265.0 035.1701,1-Dichloropropene 40.00 84.2 63 1315.0 033.6701,2,3-Trichlorobenzene 40.00 61.0 13 1475.0 024.3901,2,3-Trichloropropane 40.00 86.6 51 1585.0 034.6501,2,4-Trichlorobenzene 40.00 55.2 19 1345.0 022.0701,2,4-Trimethylbenzene 40.00 65.3 40 1455.0 026.1301,2-Dibromo-3-chloropropane 40.00 95.6 52 17110 038.240



24 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674441


1,2-Dibromoethane 40.00 89.6 65 1455.0 035.8201,2-Dichlorobenzene 40.00 65.5 44 1345.0 026.2101,2-Dichloroethane 40.00 81.5 62 1295.0 032.6001,2-Dichloropropane 40.00 76.9 58 1265.0 030.7701,3,5-Trimethylbenzene 40.00 66.6 44 1425.0 026.6501,3-Dichlorobenzene 40.00 62.5 41 1305.0 025.0101,3-Dichloropropane 40.00 88.2 64 1425.0 035.3001,4-Dichlorobenzene 40.00 63.3 42 1285.0 025.3202,2-Dichloropropane 40.00 72.8 45 1365.0 029.1302-Butanone 400.0 165 3 22750 0659.8402-Chlorotoluene 40.00 64.9 42 1325.0 025.9404-Chlorotoluene 40.00 65.7 43 1355.0 026.2804-Isopropyltoluene 40.00 66.5 43 1445.0 026.600Benzene 40.00 77.6 58 1225.0 031.030Bromobenzene 40.00 68.0 44 1305.0 027.220Bromodichloromethane 40.00 79.7 58 1255.0 031.890Bromoform 40.00 82.1 50 1545.0 032.830Bromomethane 40.00 90.9 40 1205.0 036.360Carbon tetrachloride 40.00 81.8 56 1315.0 032.740Chlorobenzene 40.00 72.4 56 1235.0 028.980Chloroethane 40.00 99.0 30 1465.0 039.590Chloroform 40.00 76.8 56 1195.0 030.730Chloromethane 40.00 89.2 39 1315.0 035.680cis-1,2-Dichloroethene 40.00 78.1 34 1415.0 031.250cis-1,3-Dichloropropene 40.00 78.9 53 1395.0 031.570Dibromochloromethane 40.00 79.5 59 1405.0 031.810Dibromomethane 40.00 86.2 64 1345.0 034.500Dichlorodifluoromethane 40.00 93.6 12 2005.0 037.440Ethylbenzene 40.00 71.4 54 1255.0 028.560Freon-113 40.00 78.5 34 1285.0 031.390



25 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674441


Hexachlorobutadiene 40.00 60.4 33 1275.0 024.150Isopropylbenzene 40.00 59.2 25 1415.0 023.690m,p-Xylene 80.00 71.5 52 13010 057.210Methylene chloride 40.00 81.4 53 1235.0 032.560MTBE 40.00 87.5 59 1285.0 034.990n-Butylbenzene 40.00 61.8 31 1425.0 024.730n-Propylbenzene 40.00 70.4 47 1385.0 028.180Naphthalene 40.00 75.9 30 1545.0 030.370o-Xylene 40.00 72.4 54 1305.0 028.940sec-Butylbenzene 40.00 70.4 49 1395.0 028.150Styrene 40.00 69.1 50 1275.0 027.650tert-Butylbenzene 40.00 71.2 48 1405.0 028.480Tetrachloroethene 40.00 74.6 56 1255.0 029.840Toluene 40.00 70.2 54 1195.0 028.080trans-1,2-Dichloroethene 40.00 80.3 60 1165.0 032.120Trichloroethene 40.00 87.3 33 1535.0 034.930Trichlorofluoromethane 40.00 96.3 30 1615.0 038.520Vinyl chloride 40.00 102 43 1405.0 040.990 Surr: 1,2-Dichloroethane-d4 50.00 126 71 15462.780 Surr: 4-Bromofluorobenzene 50.00 106 80 12552.830 Surr: Dibromofluoromethane 50.00 112 80 12855.890 Surr: Toluene-d8 50.00 104 80 12051.890



Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674442

MSDSampType: TestCode: 8260SOIL

1,1,1,2-Tetrachloroethane 40.00 67.4 51 129 205.0 0 29.33 8.4926.9401,1,1-Trichloroethane 40.00 79.3 56 128 205.0 0 32.45 2.3131.7101,1,2,2-Tetrachloroethane 40.00 60.0 35 170 20 R5.0 0 30.75 24.723.980



26 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674442


1,1,2-Trichloroethane 40.00 74.6 63 134 205.0 0 33.58 11.829.8501,1-Dichloroethane 40.00 74.6 50 123 205.0 0 30.59 2.5229.8301,1-Dichloroethene 40.00 85.5 54 126 205.0 0 35.17 2.8334.1901,1-Dichloropropene 40.00 80.6 63 131 205.0 0 33.67 4.4032.2201,2,3-Trichlorobenzene 40.00 60.6 13 147 205.0 0 24.39 0.69924.2201,2,3-Trichloropropane 40.00 77.8 51 158 205.0 0 34.65 10.831.1001,2,4-Trichlorobenzene 40.00 56.0 19 134 205.0 0 22.07 1.3922.3801,2,4-Trimethylbenzene 40.00 63.1 40 145 205.0 0 26.13 3.5025.2301,2-Dibromo-3-chloropropane 40.00 86.4 52 171 2010 0 38.24 10.134.5701,2-Dibromoethane 40.00 79.3 65 145 205.0 0 35.82 12.231.7101,2-Dichlorobenzene 40.00 66.1 44 134 205.0 0 26.21 0.79826.4201,2-Dichloroethane 40.00 76.6 62 129 205.0 0 32.60 6.1730.6501,2-Dichloropropane 40.00 74.5 58 126 205.0 0 30.77 3.2029.8001,3,5-Trimethylbenzene 40.00 64.5 44 142 205.0 0 26.65 3.2425.8001,3-Dichlorobenzene 40.00 60.9 41 130 205.0 0 25.01 2.6324.3601,3-Dichloropropane 40.00 79.8 64 142 205.0 0 35.30 10.131.9101,4-Dichlorobenzene 40.00 62.4 42 128 205.0 0 25.32 1.3524.9802,2-Dichloropropane 40.00 73.8 45 136 205.0 0 29.13 1.3329.5202-Butanone 400.0 149 3 227 2050 0 659.8 10.4594.8702-Chlorotoluene 40.00 63.4 42 132 205.0 0 25.94 2.3025.3504-Chlorotoluene 40.00 63.4 43 135 205.0 0 26.28 3.5225.3704-Isopropyltoluene 40.00 64.8 43 144 205.0 0 26.60 2.5525.930Benzene 40.00 71.4 58 122 205.0 0 31.03 8.2928.560Bromobenzene 40.00 63.7 44 130 205.0 0 27.22 6.6425.470Bromodichloromethane 40.00 73.5 58 125 205.0 0 31.89 8.0929.410Bromoform 40.00 75.1 50 154 205.0 0 32.83 8.9130.030Bromomethane 40.00 89.0 40 120 205.0 0 36.36 2.1735.580Carbon tetrachloride 40.00 77.9 56 131 205.0 0 32.74 4.9831.150Chlorobenzene 40.00 67.3 56 123 205.0 0 28.98 7.3726.920Chloroethane 40.00 95.7 30 146 205.0 0 39.59 3.3438.290



27 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674442


Chloroform 40.00 72.9 56 119 205.0 0 30.73 5.3129.140Chloromethane 40.00 88.8 39 131 205.0 0 35.68 0.47835.510cis-1,2-Dichloroethene 40.00 72.9 34 141 205.0 0 31.25 6.9229.160cis-1,3-Dichloropropene 40.00 71.9 53 139 205.0 0 31.57 9.3528.750Dibromochloromethane 40.00 71.2 59 140 205.0 0 31.81 11.128.460Dibromomethane 40.00 77.9 64 134 205.0 0 34.50 10.231.150Dichlorodifluoromethane 40.00 93.4 12 200 205.0 0 37.44 0.24137.350Ethylbenzene 40.00 67.1 54 125 205.0 0 28.56 6.2126.840Freon-113 40.00 74.5 34 128 205.0 0 31.39 5.2029.800Hexachlorobutadiene 40.00 60.2 33 127 205.0 0 24.15 0.24924.090Isopropylbenzene 40.00 55.8 25 141 205.0 0 23.69 5.9622.320m,p-Xylene 80.00 66.0 52 130 2010 0 57.21 8.0752.770Methylene chloride 40.00 78.6 53 123 205.0 0 32.56 3.4731.450MTBE 40.00 80.9 59 128 205.0 0 34.99 7.7832.370n-Butylbenzene 40.00 62.0 31 142 205.0 0 24.73 0.20224.780n-Propylbenzene 40.00 68.0 47 138 205.0 0 28.18 3.6127.180Naphthalene 40.00 79.3 30 154 205.0 0 30.37 4.3531.720o-Xylene 40.00 67.8 54 130 205.0 0 28.94 6.4227.140sec-Butylbenzene 40.00 67.7 49 139 205.0 0 28.15 3.8427.090Styrene 40.00 64.7 50 127 205.0 0 27.65 6.5725.890tert-Butylbenzene 40.00 68.5 48 140 205.0 0 28.48 3.9027.390Tetrachloroethene 40.00 69.0 56 125 205.0 0 29.84 7.8427.590Toluene 40.00 65.7 54 119 205.0 0 28.08 6.5826.290trans-1,2-Dichloroethene 40.00 77.7 60 116 205.0 0 32.12 3.2931.080Trichloroethene 40.00 90.2 33 153 205.0 0 34.93 3.2436.080Trichlorofluoromethane 40.00 94.6 30 161 205.0 0 38.52 1.7337.860Vinyl chloride 40.00 99.7 43 140 205.0 0 40.99 2.7239.890 Surr: 1,2-Dichloroethane-d4 50.00 124 71 154 062.130 Surr: 4-Bromofluorobenzene 50.00 104 80 125 052.000 Surr: Dibromofluoromethane 50.00 113 80 128 056.490



28 of 44










Prep Date:


Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115944

SeqNo: 2674442


Surr: Toluene-d8 50.00 102 80 120 050.980



29 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 8260WATERP


Batch ID: P17VW102 TestNo: EPA 8260B Analysis Date: 6/22/2017

Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 115920

SeqNo: 2672387

LCSSampType: TestCode: 8260WATER

1,1,1,2-Tetrachloroethane 20.00 94.7 80 1220.50 018.9401,1,1-Trichloroethane 20.00 88.8 80 1250.50 017.7501,1,2,2-Tetrachloroethane 20.00 97.7 76 1240.50 019.5401,1,2-Trichloroethane 20.00 99.4 80 1200.50 019.8701,1-Dichloroethane 20.00 85.1 67 1280.50 017.0201,1-Dichloroethene 20.00 110 66 1310.50 021.9601,1-Dichloropropene 20.00 98.3 80 1320.50 019.6601,2,3-Trichlorobenzene 20.00 102 76 1220.50 020.4401,2,3-Trichloropropane 20.00 96.0 75 1210.50 019.2101,2,4-Trichlorobenzene 20.00 103 73 1210.50 020.5101,2,4-Trimethylbenzene 20.00 99.4 80 1250.50 019.8801,2-Dibromo-3-chloropropane 20.00 87.5 66 1291.0 017.5001,2-Dibromoethane 20.00 97.5 80 1200.50 019.5001,2-Dichlorobenzene 20.00 102 80 1200.50 020.3701,2-Dichloroethane 20.00 89.0 80 1200.50 017.7901,2-Dichloropropane 20.00 89.8 80 1200.50 017.9601,3,5-Trimethylbenzene 20.00 96.9 80 1280.50 019.3801,3-Dichlorobenzene 20.00 100 80 1200.50 020.0901,3-Dichloropropane 20.00 95.9 80 1200.50 019.1701,4-Dichlorobenzene 20.00 103 80 1200.50 020.5902,2-Dichloropropane 20.00 86.1 69 1360.50 017.2202-Butanone 200.0 73.2 10 1715.0 0146.4302-Chlorotoluene 20.00 94.2 80 1200.50 018.8404-Chlorotoluene 20.00 97.2 80 1220.50 019.4304-Isopropyltoluene 20.00 101 80 1330.50 020.140Benzene 20.00 96.2 80 1200.50 019.240Bromobenzene 20.00 102 80 1200.50 020.350Bromodichloromethane 20.00 89.4 80 1200.50 017.890Bromoform 20.00 81.0 67 1300.50 016.210Bromomethane 20.00 120 21 1481.0 023.960



30 of 44










Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 115920

SeqNo: 2672387


Carbon tetrachloride 20.00 91.1 76 1380.50 018.210Chlorobenzene 20.00 100 80 1200.50 020.090Chloroethane 20.00 109 67 1551.0 021.750Chloroform 20.00 84.9 79 1200.50 016.980Chloromethane 20.00 90.6 33 1450.50 018.110cis-1,2-Dichloroethene 20.00 91.4 80 1200.50 018.290cis-1,3-Dichloropropene 20.00 91.0 80 1210.50 018.200Dibromochloromethane 20.00 91.2 77 1310.50 018.250Dibromomethane 20.00 90.8 80 1200.50 018.150Dichlorodifluoromethane 20.00 141 40 1690.50 028.180Ethylbenzene 20.00 96.2 80 1210.50 019.240Freon-113 20.00 93.8 47 1320.50 018.770Hexachlorobutadiene 20.00 98.4 80 1320.50 019.670Isopropylbenzene 20.00 83.6 59 1280.50 016.710m,p-Xylene 40.00 97.2 80 1241.0 038.880Methylene chloride 20.00 73.5 68 1262.0 014.700MTBE 20.00 82.1 65 1200.50 016.420n-Butylbenzene 20.00 100 74 1390.50 020.090n-Propylbenzene 20.00 99.5 80 1290.50 019.900Naphthalene 20.00 99.4 67 1230.50 019.880o-Xylene 20.00 97.0 80 1230.50 019.390sec-Butylbenzene 20.00 99.5 80 1330.50 019.900Styrene 20.00 96.6 80 1220.50 019.310tert-Butylbenzene 20.00 99.9 80 1300.50 019.980Tetrachloroethene 20.00 98.4 80 1290.50 019.690Toluene 20.00 96.8 80 1200.50 019.360trans-1,2-Dichloroethene 20.00 90.3 75 1220.50 018.060Trichloroethene 20.00 101 80 1200.50 020.270Trichlorofluoromethane 20.00 123 71 1490.50 024.510Vinyl chloride 20.00 108 53 1460.50 021.550



31 of 44










Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 115920

SeqNo: 2672387


Surr: 1,2-Dichloroethane-d4 25.00 84.2 73 12721.060 Surr: 4-Bromofluorobenzene 25.00 93.2 80 12023.300 Surr: Dibromofluoromethane 25.00 93.8 80 12123.460 Surr: Toluene-d8 25.00 94.2 80 12023.560



Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 115920

SeqNo: 2672390

MBLKSampType: TestCode: 8260WATER

1,1,1,2-Tetrachloroethane 0.50ND1,1,1-Trichloroethane 0.50ND1,1,2,2-Tetrachloroethane 0.50ND1,1,2-Trichloroethane 0.50ND1,1-Dichloroethane 0.50ND1,1-Dichloroethene 0.50ND1,1-Dichloropropene 0.50ND1,2,3-Trichlorobenzene 0.50ND1,2,3-Trichloropropane 0.50ND1,2,4-Trichlorobenzene 0.50ND1,2,4-Trimethylbenzene 0.50ND1,2-Dibromo-3-chloropropane 1.0ND1,2-Dibromoethane 0.50ND1,2-Dichlorobenzene 0.50ND1,2-Dichloroethane 0.50ND1,2-Dichloropropane 0.50ND1,3,5-Trimethylbenzene 0.50ND1,3-Dichlorobenzene 0.50ND1,3-Dichloropropane 0.50ND1,4-Dichlorobenzene 0.50ND2,2-Dichloropropane 0.50ND



32 of 44










Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 115920

SeqNo: 2672390


2-Butanone 5.0ND2-Chlorotoluene 0.50ND4-Chlorotoluene 0.50ND4-Isopropyltoluene 0.50NDBenzene 0.50NDBromobenzene 0.50NDBromodichloromethane 0.50NDBromoform 0.50NDBromomethane 1.0NDCarbon tetrachloride 0.50NDChlorobenzene 0.50NDChloroethane 1.0NDChloroform 0.50NDChloromethane 0.50NDcis-1,2-Dichloroethene 0.50NDcis-1,3-Dichloropropene 0.50NDDibromochloromethane 0.50NDDibromomethane 0.50NDDichlorodifluoromethane 0.50NDEthylbenzene 0.50NDFreon-113 0.50NDHexachlorobutadiene 0.50NDIsopropylbenzene 0.50NDm,p-Xylene 1.0NDMethylene chloride 2.0NDMTBE 0.50NDn-Butylbenzene 0.50NDn-Propylbenzene 0.50NDNaphthalene 0.50NDo-Xylene 0.50ND



33 of 44










Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 115920

SeqNo: 2672390


sec-Butylbenzene 0.50NDStyrene 0.50NDtert-Butylbenzene 0.50NDTetrachloroethene 0.50NDToluene 0.50NDtrans-1,2-Dichloroethene 0.50NDTrichloroethene 0.50NDTrichlorofluoromethane 0.50NDVinyl chloride 0.50ND Surr: 1,2-Dichloroethane-d4 25.00 83.9 73 12720.970 Surr: 4-Bromofluorobenzene 25.00 92.6 80 12023.160 Surr: Dibromofluoromethane 25.00 91.0 80 12122.760 Surr: Toluene-d8 25.00 95.6 80 12023.910



Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672393

MSSampType: TestCode: 8260WATER

1,1,1,2-Tetrachloroethane 20.00 92.5 79 1230.50 018.4901,1,1-Trichloroethane 20.00 92.2 76 1330.50 018.4301,1,2,2-Tetrachloroethane 20.00 98.0 72 1240.50 019.6101,1,2-Trichloroethane 20.00 93.8 76 1200.50 018.7601,1-Dichloroethane 20.00 83.7 67 1300.50 016.7401,1-Dichloroethene 20.00 122 63 1350.50 024.3601,1-Dichloropropene 20.00 104 80 1390.50 020.8001,2,3-Trichlorobenzene 20.00 95.4 71 1220.50 019.0901,2,3-Trichloropropane 20.00 94.3 69 1200.50 018.8601,2,4-Trichlorobenzene 20.00 99.2 66 1250.50 019.8501,2,4-Trimethylbenzene 20.00 102 67 1390.50 020.4101,2-Dibromo-3-chloropropane 20.00 81.1 65 1201.0 016.220



34 of 44










Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672393


1,2-Dibromoethane 20.00 93.4 78 1200.50 018.6701,2-Dichlorobenzene 20.00 102 80 1200.50 020.3201,2-Dichloroethane 20.00 88.0 78 1200.50 017.6101,2-Dichloropropane 20.00 90.1 79 1200.50 018.0201,3,5-Trimethylbenzene 20.00 100 57 1540.50 020.0401,3-Dichlorobenzene 20.00 101 80 1200.50 020.2001,3-Dichloropropane 20.00 94.1 80 1200.50 018.8101,4-Dichlorobenzene 20.00 103 80 1200.50 020.5502,2-Dichloropropane 20.00 90.6 61 1440.50 018.1202-Butanone 200.0 66.0 9 1205.0 0131.9502-Chlorotoluene 20.00 97.6 78 1260.50 019.5204-Chlorotoluene 20.00 97.5 80 1280.50 019.4904-Isopropyltoluene 20.00 105 78 1420.50 020.940Benzene 20.00 99.6 56 1450.50 019.910Bromobenzene 20.00 102 80 1200.50 020.320Bromodichloromethane 20.00 89.2 80 1200.50 017.830Bromoform 20.00 78.7 64 1260.50 015.730Bromomethane 20.00 145 13 1571.0 028.940Carbon tetrachloride 20.00 97.9 72 1430.50 019.580Chlorobenzene 20.00 101 80 1200.50 020.140Chloroethane 20.00 116 62 1721.0 023.230Chloroform 20.00 84.6 73 1200.50 016.930Chloromethane 20.00 92.2 33 1460.50 018.430cis-1,2-Dichloroethene 20.00 92.8 74 1240.50 018.550cis-1,3-Dichloropropene 20.00 89.5 80 1230.50 017.900Dibromochloromethane 20.00 89.1 75 1260.50 017.820Dibromomethane 20.00 88.7 79 1200.50 017.740Dichlorodifluoromethane 20.00 158 29 1840.50 031.640Ethylbenzene 20.00 98.8 80 1260.50 019.750Freon-113 20.00 105 49 1350.50 020.940



35 of 44










Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672393


Hexachlorobutadiene 20.00 102 76 1360.50 020.340Isopropylbenzene 20.00 89.2 56 1350.50 017.840m,p-Xylene 40.00 97.2 80 1301.0 038.880Methylene chloride 20.00 70.3 0 1872.0 014.060MTBE 20.00 79.6 61 1200.50 015.920n-Butylbenzene 20.00 104 67 1480.50 020.710n-Propylbenzene 20.00 104 80 1390.50 020.740Naphthalene 20.00 90.8 54 1250.50 018.150o-Xylene 20.00 97.0 80 1290.50 019.410sec-Butylbenzene 20.00 105 80 1440.50 020.920Styrene 20.00 94.2 33 1530.50 018.830tert-Butylbenzene 20.00 105 80 1400.50 020.940Tetrachloroethene 20.00 103 69 1460.50 020.570Toluene 20.00 97.8 76 1200.50 0.370019.920trans-1,2-Dichloroethene 20.00 96.0 69 1280.50 019.210Trichloroethene 20.00 106 72 1320.50 021.150Trichlorofluoromethane 20.00 133 66 1600.50 026.650Vinyl chloride 20.00 120 44 1590.50 024.080 Surr: 1,2-Dichloroethane-d4 25.00 86.4 73 12721.590 Surr: 4-Bromofluorobenzene 25.00 92.0 80 12023.000 Surr: Dibromofluoromethane 25.00 92.8 80 12123.200 Surr: Toluene-d8 25.00 96.4 80 12024.110



Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672394

MSDSampType: TestCode: 8260WATER

1,1,1,2-Tetrachloroethane 20.00 95.2 79 123 200.50 0 18.49 2.8819.0301,1,1-Trichloroethane 20.00 92.0 76 133 200.50 0 18.43 0.10918.4101,1,2,2-Tetrachloroethane 20.00 98.2 72 124 200.50 0 19.61 0.20419.650



36 of 44










Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672394


1,1,2-Trichloroethane 20.00 98.2 76 120 200.50 0 18.76 4.6319.6501,1-Dichloroethane 20.00 86.2 67 130 200.50 0 16.74 3.0017.2501,1-Dichloroethene 20.00 119 63 135 200.50 0 24.36 2.2823.8101,1-Dichloropropene 20.00 102 80 139 200.50 0 20.80 1.8420.4201,2,3-Trichlorobenzene 20.00 102 71 122 200.50 0 19.09 6.4420.3601,2,3-Trichloropropane 20.00 95.6 69 120 200.50 0 18.86 1.3719.1201,2,4-Trichlorobenzene 20.00 102 66 125 200.50 0 19.85 2.7320.4001,2,4-Trimethylbenzene 20.00 103 67 139 200.50 0 20.41 0.53820.5201,2-Dibromo-3-chloropropane 20.00 83.8 65 120 201.0 0 16.22 3.2716.7601,2-Dibromoethane 20.00 99.7 78 120 200.50 0 18.67 6.5819.9401,2-Dichlorobenzene 20.00 104 80 120 200.50 0 20.32 1.9020.7101,2-Dichloroethane 20.00 88.7 78 120 200.50 0 17.61 0.73617.7401,2-Dichloropropane 20.00 92.2 79 120 200.50 0 18.02 2.3018.4401,3,5-Trimethylbenzene 20.00 100 57 154 200.50 0 20.04 0.099820.0601,3-Dichlorobenzene 20.00 102 80 120 200.50 0 20.20 0.93620.3901,3-Dichloropropane 20.00 100 80 120 200.50 0 18.81 6.4820.0701,4-Dichlorobenzene 20.00 105 80 120 200.50 0 20.55 2.3121.0302,2-Dichloropropane 20.00 87.7 61 144 200.50 0 18.12 3.2517.5402-Butanone 200.0 70.2 9 120 205.0 0 132.0 6.18140.3702-Chlorotoluene 20.00 97.6 78 126 200.50 0 19.52 0.051219.5304-Chlorotoluene 20.00 99.0 80 128 200.50 0 19.49 1.5819.8004-Isopropyltoluene 20.00 104 78 142 200.50 0 20.94 0.67120.800Benzene 20.00 99.0 56 145 200.50 0 19.91 0.55419.800Bromobenzene 20.00 101 80 120 200.50 0 20.32 0.29620.260Bromodichloromethane 20.00 91.0 80 120 200.50 0 17.83 2.0518.200Bromoform 20.00 81.2 64 126 200.50 0 15.73 3.1316.230Bromomethane 20.00 137 13 157 201.0 0 28.94 5.7627.320Carbon tetrachloride 20.00 98.9 72 143 200.50 0 19.58 1.0219.780Chlorobenzene 20.00 102 80 120 200.50 0 20.14 1.3820.420Chloroethane 20.00 109 62 172 201.0 0 23.23 6.3121.810



37 of 44










Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672394


Chloroform 20.00 86.0 73 120 200.50 0 16.93 1.5817.200Chloromethane 20.00 94.0 33 146 200.50 0 18.43 1.9318.790cis-1,2-Dichloroethene 20.00 95.6 74 124 200.50 0 18.55 2.9719.110cis-1,3-Dichloropropene 20.00 93.6 80 123 200.50 0 17.90 4.5318.730Dibromochloromethane 20.00 90.8 75 126 200.50 0 17.82 1.8318.150Dibromomethane 20.00 93.4 79 120 200.50 0 17.74 5.1618.680Dichlorodifluoromethane 20.00 149 29 184 200.50 0 31.64 6.0229.790Ethylbenzene 20.00 99.2 80 126 200.50 0 19.75 0.45519.840Freon-113 20.00 102 49 135 200.50 0 20.94 2.9620.330Hexachlorobutadiene 20.00 103 76 136 200.50 0 20.34 1.2220.590Isopropylbenzene 20.00 87.0 56 135 200.50 0 17.84 2.5017.400m,p-Xylene 40.00 101 80 130 201.0 0 38.88 3.3440.200Methylene chloride 20.00 71.9 0 187 202.0 0 14.06 2.2514.380MTBE 20.00 82.8 61 120 200.50 0 15.92 4.0016.570n-Butylbenzene 20.00 103 67 148 200.50 0 20.71 0.24220.660n-Propylbenzene 20.00 103 80 139 200.50 0 20.74 0.48320.640Naphthalene 20.00 98.6 54 125 200.50 0 18.15 8.3419.730o-Xylene 20.00 99.0 80 129 200.50 0 19.41 1.9419.790sec-Butylbenzene 20.00 104 80 144 200.50 0 20.92 1.0120.710Styrene 20.00 94.4 33 153 200.50 0 18.83 0.21218.870tert-Butylbenzene 20.00 102 80 140 200.50 0 20.94 2.6120.400Tetrachloroethene 20.00 106 69 146 200.50 0 20.57 3.2521.250Toluene 20.00 96.8 76 120 200.50 0.3700 19.92 1.0119.720trans-1,2-Dichloroethene 20.00 94.4 69 128 200.50 0 19.21 1.6818.890Trichloroethene 20.00 105 72 132 200.50 0 21.15 0.33221.080Trichlorofluoromethane 20.00 129 66 160 200.50 0 26.65 3.0125.860Vinyl chloride 20.00 117 44 159 200.50 0 24.08 2.6523.450 Surr: 1,2-Dichloroethane-d4 25.00 87.7 73 127 021.930 Surr: 4-Bromofluorobenzene 25.00 93.5 80 120 023.380 Surr: Dibromofluoromethane 25.00 93.4 80 121 023.350



38 of 44










Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 115920

SeqNo: 2672394


Surr: Toluene-d8 25.00 97.1 80 120 024.280



39 of 44







ANALYTICAL QC SUMMARY REPORTTestCode: 8270SOILSIM_M

Sample ID LCS-62632

Batch ID: 62632 TestNo: EPA 8270CSI Analysis Date: 6/25/2017



Units: µg/Kg

PQL

Client ID: LCSS

RunNo: 115963

SeqNo: 2674419

LCSSampType: TestCode: 8270SOILSIM

EPA 3546

1-Methylnaphthalene 50.00 68.0 44 1095.0 034.0002-Methylnaphthalene 50.00 70.0 42 1175.0 035.000Acenaphthene 50.00 68.0 46 1095.0 034.000Acenaphthylene 50.00 69.0 45 1145.0 034.500Anthracene 50.00 71.0 45 1015.0 035.500Benzo(a)anthracene 50.00 70.0 38 1195.0 035.000Benzo(a)pyrene 50.00 70.0 43 1035.0 035.000Benzo(b)fluoranthene 50.00 59.0 31 1265.0 029.500Benzo(g,h,i)perylene 50.00 91.0 26 1185.0 045.500Benzo(k)fluoranthene 50.00 66.0 42 1235.0 033.000Chrysene 50.00 66.0 45 1095.0 033.000Dibenz(a,h)anthracene 50.00 82.0 33 1185.0 041.000Fluoranthene 50.00 70.0 48 1115.0 035.000Fluorene 50.00 70.0 47 1125.0 035.000Indeno(1,2,3-cd)pyrene 50.00 83.0 31 1195.0 041.500Naphthalene 50.00 68.0 43 1095.0 034.000Phenanthrene 50.00 69.0 39 1145.0 034.500Pyrene 50.00 70.0 48 1135.0 035.000 Surr: 1,2-Dichlorobenzene-d4 50.00 55.0 25 13027.500 Surr: 2-Fluorobiphenyl 50.00 76.0 23 13038.000 Surr: 4-Terphenyl-d14 50.00 79.0 24 13039.500 Surr: Nitrobenzene-d5 50.00 79.0 22 13039.500

Sample ID MB-62632




Units: µg/Kg

PQL

Client ID: PBS

RunNo: 115963

SeqNo: 2674420

MBLKSampType: TestCode: 8270SOILSIM

EPA 3546

1-Methylnaphthalene 5.0ND2-Methylnaphthalene 5.0NDAcenaphthene 5.0ND



40 of 44








Sample ID MB-62632




Units: µg/Kg

PQL

Client ID: PBS

RunNo: 115963

SeqNo: 2674420

MBLKSampType: TestCode: 8270SOILSIM

EPA 3546

Acenaphthylene 5.0NDAnthracene 5.0NDBenzo(a)anthracene 5.0NDBenzo(a)pyrene 5.0NDBenzo(b)fluoranthene 5.0NDBenzo(g,h,i)perylene 5.0NDBenzo(k)fluoranthene 5.0NDChrysene 5.0NDDibenz(a,h)anthracene 5.0NDFluoranthene 5.0NDFluorene 5.0NDIndeno(1,2,3-cd)pyrene 5.0NDNaphthalene 5.0NDPhenanthrene 5.0NDPyrene 5.0ND Surr: 1,2-Dichlorobenzene-d4 50.00 54.0 25 13027.000 Surr: 2-Fluorobiphenyl 50.00 75.0 23 13037.500 Surr: 4-Terphenyl-d14 50.00 77.0 24 13038.500 Surr: Nitrobenzene-d5 50.00 77.0 22 13038.500





Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115963

SeqNo: 2674422

MSSampType: TestCode: 8270SOILSIM

EPA 3546

1-Methylnaphthalene 200.2 52.0 44 1095.0 1.493105.6062-Methylnaphthalene 200.2 56.0 42 1175.0 2.489114.615Acenaphthene 200.2 55.5 46 1095.0 0111.111Acenaphthylene 200.2 56.8 45 1145.0 0113.614Anthracene 200.2 59.8 45 1015.0 0119.620Benzo(a)anthracene 200.2 63.5 38 1195.0 1.493128.629



41 of 44












Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115963

SeqNo: 2674422

MSSampType: TestCode: 8270SOILSIM

EPA 3546

Benzo(a)pyrene 200.2 63.5 43 1035.0 0127.127Benzo(b)fluoranthene 200.2 71.0 31 1265.0 1.991144.144Benzo(g,h,i)perylene 200.2 40.8 26 1185.0 15.9397.598Benzo(k)fluoranthene 200.2 56.3 42 1235.0 0112.613Chrysene 200.2 58.5 45 1095.0 0117.117Dibenz(a,h)anthracene 200.2 49.8 33 1185.0 099.600Fluoranthene 200.2 63.3 48 1115.0 1.493128.128Fluorene 200.2 61.3 47 1125.0 0122.623Indeno(1,2,3-cd)pyrene 200.2 48.5 31 1195.0 1.49398.599Naphthalene 200.2 50.8 43 1095.0 1.493103.103Phenanthrene 200.2 56.0 39 1145.0 0.9955113.113Pyrene 200.2 63.3 48 1135.0 1.493128.128 Surr: 1,2-Dichlorobenzene-d4 50.05 41.0 25 13020.521 Surr: 2-Fluorobiphenyl 50.05 62.0 23 13031.031 Surr: 4-Terphenyl-d14 50.05 70.0 24 13035.035 Surr: Nitrobenzene-d5 50.05 59.0 22 13029.530





Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115963

SeqNo: 2674423

MSDSampType: TestCode: 8270SOILSIM

EPA 3546

1-Methylnaphthalene 199.0 58.7 44 109 205.0 1.493 105.6 11.4118.4082-Methylnaphthalene 199.0 60.5 42 117 205.0 2.489 114.6 6.97122.886Acenaphthene 199.0 60.0 46 109 205.0 0 111.1 7.19119.403Acenaphthylene 199.0 57.5 45 114 205.0 0 113.6 0.714114.428Anthracene 199.0 63.3 45 101 205.0 0 119.6 5.09125.871Benzo(a)anthracene 199.0 68.0 38 119 205.0 1.493 128.6 6.17136.816Benzo(a)pyrene 199.0 68.5 43 103 205.0 0 127.1 6.98136.318Benzo(b)fluoranthene 199.0 76.5 31 126 205.0 1.991 144.1 6.76154.229Benzo(g,h,i)perylene 199.0 41.0 26 118 205.0 15.93 97.60 0.087397.512



42 of 44












Units: µg/Kg

PQL

Client ID: ZZZZZZ

RunNo: 115963

SeqNo: 2674423

MSDSampType: TestCode: 8270SOILSIM

EPA 3546

Benzo(k)fluoranthene 199.0 81.2 42 123 20 R5.0 0 112.6 35.8161.692Chrysene 199.0 62.3 45 109 205.0 0 117.1 5.61123.881Dibenz(a,h)anthracene 199.0 50.3 33 118 205.0 0 99.60 0.401100.000Fluoranthene 199.0 62.7 48 111 205.0 1.493 128.1 1.38126.368Fluorene 199.0 66.3 47 112 205.0 0 122.6 7.25131.841Indeno(1,2,3-cd)pyrene 199.0 48.2 31 119 205.0 1.493 98.60 1.1197.512Naphthalene 199.0 56.7 43 109 205.0 1.493 103.1 10.4114.428Phenanthrene 199.0 61.0 39 114 205.0 0.9955 113.1 7.88122.388Pyrene 199.0 63.0 48 113 205.0 1.493 128.1 0.990126.866 Surr: 1,2-Dichlorobenzene-d4 49.75 49.0 25 130 024.378 Surr: 2-Fluorobiphenyl 49.75 70.0 23 130 034.826 Surr: 4-Terphenyl-d14 49.75 69.0 24 130 034.328 Surr: Nitrobenzene-d5 49.75 75.0 22 130 037.313



43 of 44








Sample ID N024683-002CDUP

Batch ID: R115907 TestNo: EPA 9040B Analysis Date: 6/21/2017

Prep Date:


Units: pH Units

PQL

Client ID: ZZZZZZ

RunNo: 115907

SeqNo: 2671914

DUPSampType: TestCode: 9040_W

pH 100.10 8.380 0.4768.420Temp. at time of pH Analysis 00 25.90 025.900



44 of 44

N024683 - 01- 02

ASSET LaboratoriesPlease review the checklist below. Any NO signifies non-compliance. Any non-compliance will be noted and must be understood as having an impact on the quality of the data. All tests will be performed as requested regardless of any compliance issues.

If you have any questions or further instruction, please contact our Project Coordinator at (702) 307-2659.

Carrier name: Walk-In

Cooler Received/Opened On: 6/21/2017

Rep sample Temp (Deg C): 2.7 IR Gun ID: 1

Temp Blank: Yes No

Last 4 digits of Tracking No.: NA

Cooling process: Ice Ice Pack Dry Ice Other None

Packing Material Used: None

Workorder: N024683

Sample Receipt Checklist

4. Chain of custody present? Yes No

6. Chain of custody signed when relinquished and received? Yes No

7. Chain of custody agrees with sample labels? Yes No

8. Samples in proper container/bottle? Yes No

9. Sample containers intact? Yes No

10. Sufficient sample volume for indicated test? Yes No

11. All samples received within holding time? Yes No

Yes No NA13. Water - VOA vials have zero headspace?

14. Water - pH acceptable upon receipt? Yes No NAExample: pH > 12 for (CN,S); pH<2 for Metals

1. Shipping container/cooler in good condition? Yes No Not Present

2. Custody seals intact, signed, dated on shippping container/cooler? Yes No Not Present

3. Custody seals intact on sample bottles? Yes No Not Present

5. Sampler's name present in COC? Yes No

12. Temperature of rep sample or Temp Blank within acceptable limit? Yes No NA

Yes No NA15. Did the bottle labels indicate correct preservatives used?

16. Were there Non-Conformance issues at login? Yes No NAWas Client notified? Yes No NA

Comments: Sample for Metals was received @ pH 8 and adjusted to pH < 2 with HNO3.See Correspondence.

Checklist Completed By: FR Reviewed By:

Sample ID Client Sample ID Date Collected

Date Received:

Date Due Matrix Test No

WORK ORDER Summary 03-Jul-17

WorkOrder: N024683

Comments:

Client ID: MCGAS01Project: SILVER PEAK SOIL, BRN041 QC Level: RTNE

Hld MS Sub

6/21/2017

Test Name

ASSET Laboratories

Storage

N024683-001A SS-12 6/20/2017 11:15:00 AM 6/28/2017 Soil EPA 8015B GASOLINE RANGE ORGANICS BY GC/FID

RB

6/28/2017 EPA 8260B VOLATILE ORGANIC COMPOUNDS BY GC/MS

RB

N024683-001B 6/28/2017 EPA 3050B SOPREP TOTAL METALS WS

6/28/2017 EPA 3546 Microwave Extraction WS

6/28/2017 EPA 6010B TOTAL METALS BY ICP WS

6/28/2017 EPA 8015B DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

WS

6/28/2017 EPA 8270CSIM SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS-SIM

WS

6/28/2017 EPA 3550B SHAKE-OUT METHOD: EXTRACTABLE FUELS

WS

N024683-002A SLUDGE-1 6/20/2017 11:00:00 AM 6/28/2017 Water EPA 8015B GASOLINE RANGE ORGANICS BY GC/FID

VW

6/28/2017 EPA 8260B VOLATILE ORGANIC COMPOUNDS BY GC/MS

VW

N024683-002B 6/28/2017 EPA 3510C SEPARATORY FUNNEL EXTRACTION: EXTRACTABLE FUELS

WW

6/28/2017 EPA 3510C SEPARATORY FUNNEL EXTRACTION: 8270C - SIM

WW

6/28/2017 EPA 8015B DIESEL & MOTOR OIL RANGE ORGANICS BY GC/FID

WW

6/28/2017 EPA 8270CSIM SEMIVOLATILE ORGANIC COMPOUNDS BY GC/MS-SIM

WW

N024683-002C 6/28/2017 EPA 1020A IGNITABILITY BY SETAFLASH CLOSED-CUP

WW

6/28/2017 EPA 9040B pH WW

N024683-002D 6/28/2017 EPA 3010A AQPREP TOTAL METALS: ICP, FLAA WW

6/28/2017 EPA 6010B TOTAL METALS BY ICP WW

1 of 2Page

Sample ID Client Sample ID Date Collected

Date Received:

Date Due Matrix Test No

WORK ORDER Summary 03-Jul-17

WorkOrder: N024683

Comments:

Client ID: MCGAS01Project: SILVER PEAK SOIL, BRN041 QC Level: RTNE

Hld MS Sub

6/21/2017

Test Name

ASSET Laboratories

Storage

N024683-002D SLUDGE-1 6/20/2017 11:00:00 AM 6/28/2017 Water MERCURY PREP WW

6/28/2017 EPA 7470A TOTAL MERCURY BY COLD VAPOR TECHNIQUE

WW

N024683-003A FOLDER 6/28/2017 6/28/2017 Folder Folder LAB

6/28/2017 Folder Folder LAB

2 of 2Page

Yoandra Rodriguez

From: Brett Bottenberg [[email protected]]Sent: Thursday, June 22, 2017 8:28 AMTo: Yoandra RodriguezCc: Marlon B. Cartin; Quennie Manimtim; Fernando Rivera; Sonny. Lorenzo; Andreafe. GallardoSubject: Re: SILVER PEAR SOIL, BRN041 (Asset Labs No, N024683)

Page 1 of 2

6/22/2017

Hi Yoandra, Please run the TPH gas, VOCs, pH, Ignitability and Metals..... thank you, Brett Brett Bottenberg, CEM Operations Manager - Las Vegas Office D 702.260.4961 ext. 201 C 702.232.5247 E [email protected] McGinley & Associates, Inc. 1915 N. Green Valley Parkway, Suite 200 Henderson, NV 89074 __________________________________________________________________________________ On Wed, Jun 21, 2017 at 6:23 PM, Yoandra Rodriguez <[email protected]> wrote:

Hello Brett, We received 3 VOAs and two 4 oz jars for sample "Slugde-1" (water). There's no enough volumen to run all the test requested on COC. TPH gas, VOCs, pH, Ignitability and Metals could be performed but we need more sample (at least 1 L) for TPH DM and PAHs. Please kindly advise which tests to prioritize. Thanks, Yoandra Rodriguez Sample Control Officer California: 11110 Artesia Blvd., Ste. B, Cerritos, CA 90703 I P: 562.219.7435 I F: 562.219.7436 Nevada: 3151 W. Post Road, Las Vegas, NV 89118 I P: 702.307.2659 Ext. 411 I F: 702.307.2691 I www.assetlaboratories.com ASSET LABORATORIES - Serving Clients with Passion and Professionalism This message is intended for the use of the individual or entity to which it is addressed. This may contain information that is privileged, confidential, and exempt from disclosure under applicable law. If the reader of this

mailto:[email protected]



http://www.assetlaboratories.com

message is not the intended recipient, or the employee or agent responsible for delivering the message to the intended recipient, you are hereby notified that any dissemination, distribution or copying of this communication is strictly prohibited. If you have received this communication in error, please notify us immediately by telephone and delete the original message. Thank you.

Page 2 of 2

6/22/2017

Subject: Re: Silver Pear Soil, BRN042 (Asset Labs No. N024682)

From: Bre� Bo�enberg <bbo�[email protected]>

Date: 07/03/17 7:32 AM

To: Reports ASSET Laboratories <[email protected]>

CC: "Marlon B. Car/n" <[email protected]>

Fern,

Can you please change the project to "Silver Peak" from Silver Pear? Please do this for allreports and invoices and please make sure the date stays the same.

Thank you,Brett

Brett Bottenberg, CEMOperations Manager - Las Vegas OfficeD 702.260.4961 ext. 201

C 702.232.5247

E [email protected]

McGinley & Associates, Inc.

1915 N. Green Valley Parkway, Suite 200

Henderson, NV 89074

__________________________________________________________________________________

On Fri, Jun 30, 2017 at 10:37 PM, Reports ASSET Laboratories <[email protected]> wrote:

Enclosed is the final report for the above project.

Thanks,

Fern Rivera

Nevada: 3151 W. Post Road, Las Vegas, NV 89118 I P: 702.307.2659 I F: 702.307.2691 I

California: 11110 Artesia Blvd., Ste. C, Cerritos, CA 90703 I P: 562.219.7435 I F: 562.219.7436

www.assetlaboratories.com

Re:SilverPearSoil,BRN042(AssetLabsNo.N024682)

1of2

ASSET LABORATORIES - Serving Clients with Passion and Professionalism

This message is intended for the use of the individual or en/ty to which it is addressed. This may

contain informa/on that is privileged, confiden/al, and exempt from disclosure under applicable law. If

the reader of this message is not the intended recipient, or the employee or agent responsible for

delivering the message to the intended recipient, you are hereby no/fied that any dissemina/on,

distribu/on or copying of this communica/on is strictly prohibited. If you have received this

communica/on in error, please no/fy us immediately by telephone and delete the original message.

Thank you.

Virus-free. www.avast.com

Re:SilverPearSoil,BRN042(AssetLabsNo.N024682)

2of2

Documents

LIMITED PHASE II ENVIRONMENTAL - NDEP · 5.3 Analytical Testing The soil sample was delivered under chain-of-custody protocol toAsset Laboratories located in Las Vegas, Nevada. The