16
0 RE t-34·11·4-108 W'MTI •Atlai Dt....tr •• 1984 Project No . 5727.01 llr. E ..rd L. T11J10r Env1,.ntol Stl'¥1... DhillOn u. S. b¥1-ntol Aglftey I.Utlltlto•. lluttelluntto 02173 Sub.ltct: ReiOlvt Sttt Otto Ytltdltton Colltcttd by CUI>. Drtlttr. McKM IWS Cor!lorotton LaborAtory Dtar llr. T11lor: A laval OM vtltdltton w11 on tilt orttntc anolyttul dltl f,. llltlvt wattr •-.las colltcttcl by c.,, Drtlstr, Mcbt It tilt Relolvt Sttt. NUS Coi'I'Orttton LabOratory tntlyttd tilt IUIPltl for tilt HSL volattltl only. 11o can llllllbtr wa1 tnvolvtd stnu tilt lnt11111 wu not 1clltclultd tllro""' Sill. -var, tilt lab dtd follow tilt CLP tiii'OIIgll312. Tilt dltl WIN t¥11Utttd btnd on tilt following spectral parfoltllnct o 0 dttl o hb0r1tory blinks 0 IU!Togtto IPttll 0 Mtrtx IPikts o ltborltory dupltcttll 0 holding tt•• o tnst,.nt 011tbratton o fttld bltnh 0 fttld dll!llttltll Ttblt 1 1-11111 tilt Vlltdltton ..,_ncllttonl, olltdl tro b11tc1 on tilt foll•tng tnfo,.tton. All tf tilt '"""''"to 1ptkt racovartts aro tcctpttblt. Ltktwtlt tll tf tilt •trta uta rtcOvartts 11 wall " tilt 01trtx 1ptkt dupltuto RPDI aro accaptoblt.

LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

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Page 1: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

0

RE ~EIVEI

t-34middot11middot4-108 WMTI ft~SPONU

COMPU~NCI bullAtlai

Dttr bullbull 1984

Project No 572701

llr Erd L T11J10r Env1ntol Stlyen1 DhillOn u S byen1-ntol Pro~Uon Aglftey IUtlltltobull lluttelluntto 02173

Subltct ReiOlvt Sttt Otto Ytltdltton Colltcttd by CUIgt Drtlttr McKM IWS Corlorotton LaborAtory

Dtar llr T11lor

A laval OM vtltdltton w11 perf~ on tilt orttntc anolyttul dltl f llltlvt wattr bull-las colltcttcl by c Drtlstr Mcbt It tilt Relolvt Sttt NUS CoiIOrttton LabOratory tntlyttd tilt IUIPltl for tilt HSL volattltl only 11o can llllllbtr wa1 tnvolvtd stnu tilt lnt11111 wu not 1clltclultd tllro Sill -var tilt lab dtd follow tilt CLP

=~~~ middot~=~middot1~P~1ct~~~~~ga-a~ltiiiOIIgll312

Tilt dltl WIN tyen11Utttd btnd on tilt following ~~tr-ttrt

spectral parfoltllnct o0 dttl -~middot-middot o hb0r1tory blinks 0 IUTogtto IPttll 0 Mtrtx IPikts o ltborltory dupltcttll 0 holding ttbullbull o tnstnt 011tbratton o fttld bltnh 0 fttld dllllttltll

Ttblt 1 1-11111 tilt Vlltdltton _ncllttonl olltdl tro b11tc1 on tilt follbulltng tnfotton

All tf tilt to 1ptkt racovartts aro tcctpttblt Ltktwtlt tll tf tilt bulltrta uta rtcOvartts 11 wall tilt 01trtx 1ptkt dupltuto RPDI aro accaptoblt

t-34-11-4- 108n Mr Edward L TAyen10r Envlrobullntal Srvlctl DhhlonbullPl~ TliO

Tht Na~nt bhnt contalntd 28 ue1 of Mtllyhno chloride and 24 ue1 of ecotono Tho foll lng c-undbull clotocttd In tht flold blanko Mthylono chloride 3D ug1 trlchlorootheno prtStnt but ltu than 5 ug1 tltrachlorotthtno 8 ueh chlorofON PNiant but lus than 5 ug1 This bull111 rosult In tilt Njoctlon of Mtllylllgtl dllorlclo clota 1111 tllen 60 uefl trlchlorootheno data less than 50 uefl tltrachlorootlltno cloU lou than 16 ug1 dllorofoN data lou 60 uefl end ecotono clota lou then 50 ue1 All other dati for then eoopoundo bull111 bt Jed

All of tht llllgtloo wro rocolvod on 10lt84 Anel1fu occulftd on 102584 end 11784 Tho 11784 1111gtlH hod btln htld for oliDit throe -tl ~ldl w111 Nsult In tile dote btlng Jed

No lnfo-tiOII could bt clotoNlntd froa the fltld dllpllcttll slnct tht1 did not =ntoln eey eoopoundl tbovt tile tRilLs

I htvt onclostd tllo data pochfl so thtt you can Mrk It eppprlato

VII) truly youn

-U _ t-L_ Rldllrd ~ McCracken Projoct Ml~r

cc (IIMII Lindo Paul

I -Y eck-lodge rocolpt end opprovol of tilt IIUSREMPO Level I data velldotlon for the orvanlc bullbullPlt ults for tht above Nforonctd IIIPlH colltcttd by tp Drur -middotend enelyltd bYIIUS torttlon Ltborotol)

Dlpuij PIOltct Off1 cor Rtglonol Sallplo Control tontor

r Tlblt 1 bull Yal1datton Rtcndattons

Swlo Mlllbor 2 ltSL-CIIbullIIlmiddotID1 Amiddot1 ltSL-CII-W1-302 middot RSI-111-115-103 ltSL-1114-104 ltSL-111-IIID-105 ltSL-111-W4-106 ltSL-111-JS-107 ISL-CIImiddotPSmiddotID8 ltSL-11141middot109 ISL-111-Ft-310 ltSL-IIImiddotWll-311 ISI-tlt-1112middot312

Amiddotl Nltct tilt Mtlllltno dll ortdo dote all otlltr ts accoptablo Amiddotl Nltct tilt trtdllorootlltno dote all otlltr to accoptlbh A-3 ~ tilt tr1dllonootlltM and tttradlloroothtnt dote all otlltr t1

acooptlblt A_ Nltct tilt MVIYltnt dllor1do and tr1dl1oroothtnt dote all

all otlltr 11 ocmptlblt A-1 roIKt tilt totradlloroo- and ~ tilt tr1111orootlltno dote tll

all otlltr 11 occa~lo A-6 ~ tilt bullllllltno dllor1do and act- ditt ~11 otlltr 11 KCe~gtttblt A-7 ~ 1M Mlllylono di1Dr1do data all ollltr 11 KC09tlb1t

data allould btmiddot conatdtrod approxtatt

I I I I

Jil1

f--middottbulll ~ftl

I

Tabla 2 bull F1eld Blank bampults

tCEOund Dtgcttd

bullbull_ clllor1dl 72 1bull RSI41middotFCbull306 1 trichl-- It

41111

bull bullthY- clllor1dl 29 11111RSI41~U-311 trichloro- pnt at 411111

o tatradll-- 8 11111

r~fo~~=i ~ ~n

v

~ middotmiddot -- bull

r

nmi To

~~~~~ llevtow of llegton I tontroct Dltll SMO Cut lo- SAS bullo-

Contrac Libu XQd Contract ItoStto N -j~~~tl~~~~~~~~~~~~~~~~~~~~~~ $MO Traffic o a llegton n SAt NO a shyLow Ltvolt_IIH Lno1_Aiifi lno1_soilSOd_llitriWupoundo_

t~ ltltIIICIIt

~a Tl ~u ~~ s-ey of lllto rlftn for tot a taH

1 Dlto Clt-u Ylll~IIII-=-ACID~PUTTCDD_ A bull sslaYl1 bull All t- HltvoiH P bull liilll bull so tt- oot uHOttal for rntn

aN atutogU bull Ubullsseptebh bull S it- 11M1tial for rtv1tw ahi1RJ

II Spoctrtl Porfonco Crttoria YGA (IAlttiiiA (DmPI_

A bull ~ bull All crt torts ott ctrt ofqultty

P bull ~ bull All crttorta not bullt ctrt of reuonulo qultty diU uaoablt for ltlrtlod puIII

U bull IJntssbulletablt bull Cr1tlr1a ut bullt IDICtrt Df poorQral 1ty Uti UftUitabll

UMARG

111 lltot Aotlyota YlllIIII=ACID_IIUT_-nIID_

l bull iW1U1 bull No coot~t~tftlnta abo lrtnt- bullueton 1ta1t no 1nt1rl1rence wtttl _ results

F ~ bull toiIUII1nants DAatnt b~t a1n1a1 1ntTrt bullitll 1111Pll ruultamp

C bull ~sSJptfblt bull ampron ampDfttlll111ai0n too bulletl 1ftttrftnlt to Ult dati hr tttitl CISOftlft11

bull or thl ut1fl frat1oft

bull Sll)tutlo_-__ Contr~et No___

IV Sumgatlto Spfko Rosu1tll VOAlt_tii__AtiD__PtsTnID~ Note StiiP1t dtto neggod on fndlvfdua1 basts

A lodtrfdut1 IIIIP11 naHfng crftltlrft

~ bull All suiTIIgttltl racGrtrfu wttlltn crftltorft JIIUiil bull bl tuiTIIfla raCGrtrfaa outatde crftltorft

Uor ra-rfas of lt101 JubsWtfUed bullbull a atrfa offect

lnn1ff bull MJ rfu of lt101 tlllt 111 IOIIubaWt1attd as a bulltrfa affact

t tua s- A-A~shy lt101 of 1u raported 11 suopoct

gt101 fnlt ltlOI of 1 llporled 11 ffiiiil u bull UnbullssepttlJt- ~~middot-1bullbull raported middotmiddot-tllldor bull111 1aa raporled 11 fnrtlfd

yenOA Q of Jc S1aa SYSpoct i lnnlfd 11 = of = S1aa Suspoct lnvaltd ACID= of $111p1aa Suspoct = Innltd PEST~ of S1as Suspect lnvalfd TtiD = of~ S1as Suspect lnvalfd

Y _ ptlrt Rooultl

~bullto No acton talrtn

A bull AclttllUll bull ElillWmiddot U bull Unmoptab1tshy

VDA_III-=AtiD-=-PIST-=TtDD

on lllltrfa Spfkt rasulta a1ooo

lt101 of _da ouUfdl cntorfa gt101 of lt50S of capoiOidl outJflfo crftarfa gt501 of _ ouUfdt crftltorfa andor bullbull1 racoyentrftl of lt101

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

- I _

r

I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 2: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

t-34-11-4- 108n Mr Edward L TAyen10r Envlrobullntal Srvlctl DhhlonbullPl~ TliO

Tht Na~nt bhnt contalntd 28 ue1 of Mtllyhno chloride and 24 ue1 of ecotono Tho foll lng c-undbull clotocttd In tht flold blanko Mthylono chloride 3D ug1 trlchlorootheno prtStnt but ltu than 5 ug1 tltrachlorotthtno 8 ueh chlorofON PNiant but lus than 5 ug1 This bull111 rosult In tilt Njoctlon of Mtllylllgtl dllorlclo clota 1111 tllen 60 uefl trlchlorootheno data less than 50 uefl tltrachlorootlltno cloU lou than 16 ug1 dllorofoN data lou 60 uefl end ecotono clota lou then 50 ue1 All other dati for then eoopoundo bull111 bt Jed

All of tht llllgtloo wro rocolvod on 10lt84 Anel1fu occulftd on 102584 end 11784 Tho 11784 1111gtlH hod btln htld for oliDit throe -tl ~ldl w111 Nsult In tile dote btlng Jed

No lnfo-tiOII could bt clotoNlntd froa the fltld dllpllcttll slnct tht1 did not =ntoln eey eoopoundl tbovt tile tRilLs

I htvt onclostd tllo data pochfl so thtt you can Mrk It eppprlato

VII) truly youn

-U _ t-L_ Rldllrd ~ McCracken Projoct Ml~r

cc (IIMII Lindo Paul

I -Y eck-lodge rocolpt end opprovol of tilt IIUSREMPO Level I data velldotlon for the orvanlc bullbullPlt ults for tht above Nforonctd IIIPlH colltcttd by tp Drur -middotend enelyltd bYIIUS torttlon Ltborotol)

Dlpuij PIOltct Off1 cor Rtglonol Sallplo Control tontor

r Tlblt 1 bull Yal1datton Rtcndattons

Swlo Mlllbor 2 ltSL-CIIbullIIlmiddotID1 Amiddot1 ltSL-CII-W1-302 middot RSI-111-115-103 ltSL-1114-104 ltSL-111-IIID-105 ltSL-111-W4-106 ltSL-111-JS-107 ISL-CIImiddotPSmiddotID8 ltSL-11141middot109 ISL-111-Ft-310 ltSL-IIImiddotWll-311 ISI-tlt-1112middot312

Amiddotl Nltct tilt Mtlllltno dll ortdo dote all otlltr ts accoptablo Amiddotl Nltct tilt trtdllorootlltno dote all otlltr to accoptlbh A-3 ~ tilt tr1dllonootlltM and tttradlloroothtnt dote all otlltr t1

acooptlblt A_ Nltct tilt MVIYltnt dllor1do and tr1dl1oroothtnt dote all

all otlltr 11 ocmptlblt A-1 roIKt tilt totradlloroo- and ~ tilt tr1111orootlltno dote tll

all otlltr 11 occa~lo A-6 ~ tilt bullllllltno dllor1do and act- ditt ~11 otlltr 11 KCe~gtttblt A-7 ~ 1M Mlllylono di1Dr1do data all ollltr 11 KC09tlb1t

data allould btmiddot conatdtrod approxtatt

I I I I

Jil1

f--middottbulll ~ftl

I

Tabla 2 bull F1eld Blank bampults

tCEOund Dtgcttd

bullbull_ clllor1dl 72 1bull RSI41middotFCbull306 1 trichl-- It

41111

bull bullthY- clllor1dl 29 11111RSI41~U-311 trichloro- pnt at 411111

o tatradll-- 8 11111

r~fo~~=i ~ ~n

v

~ middotmiddot -- bull

r

nmi To

~~~~~ llevtow of llegton I tontroct Dltll SMO Cut lo- SAS bullo-

Contrac Libu XQd Contract ItoStto N -j~~~tl~~~~~~~~~~~~~~~~~~~~~~ $MO Traffic o a llegton n SAt NO a shyLow Ltvolt_IIH Lno1_Aiifi lno1_soilSOd_llitriWupoundo_

t~ ltltIIICIIt

~a Tl ~u ~~ s-ey of lllto rlftn for tot a taH

1 Dlto Clt-u Ylll~IIII-=-ACID~PUTTCDD_ A bull sslaYl1 bull All t- HltvoiH P bull liilll bull so tt- oot uHOttal for rntn

aN atutogU bull Ubullsseptebh bull S it- 11M1tial for rtv1tw ahi1RJ

II Spoctrtl Porfonco Crttoria YGA (IAlttiiiA (DmPI_

A bull ~ bull All crt torts ott ctrt ofqultty

P bull ~ bull All crttorta not bullt ctrt of reuonulo qultty diU uaoablt for ltlrtlod puIII

U bull IJntssbulletablt bull Cr1tlr1a ut bullt IDICtrt Df poorQral 1ty Uti UftUitabll

UMARG

111 lltot Aotlyota YlllIIII=ACID_IIUT_-nIID_

l bull iW1U1 bull No coot~t~tftlnta abo lrtnt- bullueton 1ta1t no 1nt1rl1rence wtttl _ results

F ~ bull toiIUII1nants DAatnt b~t a1n1a1 1ntTrt bullitll 1111Pll ruultamp

C bull ~sSJptfblt bull ampron ampDfttlll111ai0n too bulletl 1ftttrftnlt to Ult dati hr tttitl CISOftlft11

bull or thl ut1fl frat1oft

bull Sll)tutlo_-__ Contr~et No___

IV Sumgatlto Spfko Rosu1tll VOAlt_tii__AtiD__PtsTnID~ Note StiiP1t dtto neggod on fndlvfdua1 basts

A lodtrfdut1 IIIIP11 naHfng crftltlrft

~ bull All suiTIIgttltl racGrtrfu wttlltn crftltorft JIIUiil bull bl tuiTIIfla raCGrtrfaa outatde crftltorft

Uor ra-rfas of lt101 JubsWtfUed bullbull a atrfa offect

lnn1ff bull MJ rfu of lt101 tlllt 111 IOIIubaWt1attd as a bulltrfa affact

t tua s- A-A~shy lt101 of 1u raported 11 suopoct

gt101 fnlt ltlOI of 1 llporled 11 ffiiiil u bull UnbullssepttlJt- ~~middot-1bullbull raported middotmiddot-tllldor bull111 1aa raporled 11 fnrtlfd

yenOA Q of Jc S1aa SYSpoct i lnnlfd 11 = of = S1aa Suspoct lnvaltd ACID= of $111p1aa Suspoct = Innltd PEST~ of S1as Suspect lnvalfd TtiD = of~ S1as Suspect lnvalfd

Y _ ptlrt Rooultl

~bullto No acton talrtn

A bull AclttllUll bull ElillWmiddot U bull Unmoptab1tshy

VDA_III-=AtiD-=-PIST-=TtDD

on lllltrfa Spfkt rasulta a1ooo

lt101 of _da ouUfdl cntorfa gt101 of lt50S of capoiOidl outJflfo crftarfa gt501 of _ ouUfdt crftltorfa andor bullbull1 racoyentrftl of lt101

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

- I _

r

I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 3: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

r Tlblt 1 bull Yal1datton Rtcndattons

Swlo Mlllbor 2 ltSL-CIIbullIIlmiddotID1 Amiddot1 ltSL-CII-W1-302 middot RSI-111-115-103 ltSL-1114-104 ltSL-111-IIID-105 ltSL-111-W4-106 ltSL-111-JS-107 ISL-CIImiddotPSmiddotID8 ltSL-11141middot109 ISL-111-Ft-310 ltSL-IIImiddotWll-311 ISI-tlt-1112middot312

Amiddotl Nltct tilt Mtlllltno dll ortdo dote all otlltr ts accoptablo Amiddotl Nltct tilt trtdllorootlltno dote all otlltr to accoptlbh A-3 ~ tilt tr1dllonootlltM and tttradlloroothtnt dote all otlltr t1

acooptlblt A_ Nltct tilt MVIYltnt dllor1do and tr1dl1oroothtnt dote all

all otlltr 11 ocmptlblt A-1 roIKt tilt totradlloroo- and ~ tilt tr1111orootlltno dote tll

all otlltr 11 occa~lo A-6 ~ tilt bullllllltno dllor1do and act- ditt ~11 otlltr 11 KCe~gtttblt A-7 ~ 1M Mlllylono di1Dr1do data all ollltr 11 KC09tlb1t

data allould btmiddot conatdtrod approxtatt

I I I I

Jil1

f--middottbulll ~ftl

I

Tabla 2 bull F1eld Blank bampults

tCEOund Dtgcttd

bullbull_ clllor1dl 72 1bull RSI41middotFCbull306 1 trichl-- It

41111

bull bullthY- clllor1dl 29 11111RSI41~U-311 trichloro- pnt at 411111

o tatradll-- 8 11111

r~fo~~=i ~ ~n

v

~ middotmiddot -- bull

r

nmi To

~~~~~ llevtow of llegton I tontroct Dltll SMO Cut lo- SAS bullo-

Contrac Libu XQd Contract ItoStto N -j~~~tl~~~~~~~~~~~~~~~~~~~~~~ $MO Traffic o a llegton n SAt NO a shyLow Ltvolt_IIH Lno1_Aiifi lno1_soilSOd_llitriWupoundo_

t~ ltltIIICIIt

~a Tl ~u ~~ s-ey of lllto rlftn for tot a taH

1 Dlto Clt-u Ylll~IIII-=-ACID~PUTTCDD_ A bull sslaYl1 bull All t- HltvoiH P bull liilll bull so tt- oot uHOttal for rntn

aN atutogU bull Ubullsseptebh bull S it- 11M1tial for rtv1tw ahi1RJ

II Spoctrtl Porfonco Crttoria YGA (IAlttiiiA (DmPI_

A bull ~ bull All crt torts ott ctrt ofqultty

P bull ~ bull All crttorta not bullt ctrt of reuonulo qultty diU uaoablt for ltlrtlod puIII

U bull IJntssbulletablt bull Cr1tlr1a ut bullt IDICtrt Df poorQral 1ty Uti UftUitabll

UMARG

111 lltot Aotlyota YlllIIII=ACID_IIUT_-nIID_

l bull iW1U1 bull No coot~t~tftlnta abo lrtnt- bullueton 1ta1t no 1nt1rl1rence wtttl _ results

F ~ bull toiIUII1nants DAatnt b~t a1n1a1 1ntTrt bullitll 1111Pll ruultamp

C bull ~sSJptfblt bull ampron ampDfttlll111ai0n too bulletl 1ftttrftnlt to Ult dati hr tttitl CISOftlft11

bull or thl ut1fl frat1oft

bull Sll)tutlo_-__ Contr~et No___

IV Sumgatlto Spfko Rosu1tll VOAlt_tii__AtiD__PtsTnID~ Note StiiP1t dtto neggod on fndlvfdua1 basts

A lodtrfdut1 IIIIP11 naHfng crftltlrft

~ bull All suiTIIgttltl racGrtrfu wttlltn crftltorft JIIUiil bull bl tuiTIIfla raCGrtrfaa outatde crftltorft

Uor ra-rfas of lt101 JubsWtfUed bullbull a atrfa offect

lnn1ff bull MJ rfu of lt101 tlllt 111 IOIIubaWt1attd as a bulltrfa affact

t tua s- A-A~shy lt101 of 1u raported 11 suopoct

gt101 fnlt ltlOI of 1 llporled 11 ffiiiil u bull UnbullssepttlJt- ~~middot-1bullbull raported middotmiddot-tllldor bull111 1aa raporled 11 fnrtlfd

yenOA Q of Jc S1aa SYSpoct i lnnlfd 11 = of = S1aa Suspoct lnvaltd ACID= of $111p1aa Suspoct = Innltd PEST~ of S1as Suspect lnvalfd TtiD = of~ S1as Suspect lnvalfd

Y _ ptlrt Rooultl

~bullto No acton talrtn

A bull AclttllUll bull ElillWmiddot U bull Unmoptab1tshy

VDA_III-=AtiD-=-PIST-=TtDD

on lllltrfa Spfkt rasulta a1ooo

lt101 of _da ouUfdl cntorfa gt101 of lt50S of capoiOidl outJflfo crftarfa gt501 of _ ouUfdt crftltorfa andor bullbull1 racoyentrftl of lt101

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

- I _

r

I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 4: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

Tabla 2 bull F1eld Blank bampults

tCEOund Dtgcttd

bullbull_ clllor1dl 72 1bull RSI41middotFCbull306 1 trichl-- It

41111

bull bullthY- clllor1dl 29 11111RSI41~U-311 trichloro- pnt at 411111

o tatradll-- 8 11111

r~fo~~=i ~ ~n

v

~ middotmiddot -- bull

r

nmi To

~~~~~ llevtow of llegton I tontroct Dltll SMO Cut lo- SAS bullo-

Contrac Libu XQd Contract ItoStto N -j~~~tl~~~~~~~~~~~~~~~~~~~~~~ $MO Traffic o a llegton n SAt NO a shyLow Ltvolt_IIH Lno1_Aiifi lno1_soilSOd_llitriWupoundo_

t~ ltltIIICIIt

~a Tl ~u ~~ s-ey of lllto rlftn for tot a taH

1 Dlto Clt-u Ylll~IIII-=-ACID~PUTTCDD_ A bull sslaYl1 bull All t- HltvoiH P bull liilll bull so tt- oot uHOttal for rntn

aN atutogU bull Ubullsseptebh bull S it- 11M1tial for rtv1tw ahi1RJ

II Spoctrtl Porfonco Crttoria YGA (IAlttiiiA (DmPI_

A bull ~ bull All crt torts ott ctrt ofqultty

P bull ~ bull All crttorta not bullt ctrt of reuonulo qultty diU uaoablt for ltlrtlod puIII

U bull IJntssbulletablt bull Cr1tlr1a ut bullt IDICtrt Df poorQral 1ty Uti UftUitabll

UMARG

111 lltot Aotlyota YlllIIII=ACID_IIUT_-nIID_

l bull iW1U1 bull No coot~t~tftlnta abo lrtnt- bullueton 1ta1t no 1nt1rl1rence wtttl _ results

F ~ bull toiIUII1nants DAatnt b~t a1n1a1 1ntTrt bullitll 1111Pll ruultamp

C bull ~sSJptfblt bull ampron ampDfttlll111ai0n too bulletl 1ftttrftnlt to Ult dati hr tttitl CISOftlft11

bull or thl ut1fl frat1oft

bull Sll)tutlo_-__ Contr~et No___

IV Sumgatlto Spfko Rosu1tll VOAlt_tii__AtiD__PtsTnID~ Note StiiP1t dtto neggod on fndlvfdua1 basts

A lodtrfdut1 IIIIP11 naHfng crftltlrft

~ bull All suiTIIgttltl racGrtrfu wttlltn crftltorft JIIUiil bull bl tuiTIIfla raCGrtrfaa outatde crftltorft

Uor ra-rfas of lt101 JubsWtfUed bullbull a atrfa offect

lnn1ff bull MJ rfu of lt101 tlllt 111 IOIIubaWt1attd as a bulltrfa affact

t tua s- A-A~shy lt101 of 1u raported 11 suopoct

gt101 fnlt ltlOI of 1 llporled 11 ffiiiil u bull UnbullssepttlJt- ~~middot-1bullbull raported middotmiddot-tllldor bull111 1aa raporled 11 fnrtlfd

yenOA Q of Jc S1aa SYSpoct i lnnlfd 11 = of = S1aa Suspoct lnvaltd ACID= of $111p1aa Suspoct = Innltd PEST~ of S1as Suspect lnvalfd TtiD = of~ S1as Suspect lnvalfd

Y _ ptlrt Rooultl

~bullto No acton talrtn

A bull AclttllUll bull ElillWmiddot U bull Unmoptab1tshy

VDA_III-=AtiD-=-PIST-=TtDD

on lllltrfa Spfkt rasulta a1ooo

lt101 of _da ouUfdl cntorfa gt101 of lt50S of capoiOidl outJflfo crftarfa gt501 of _ ouUfdt crftltorfa andor bullbull1 racoyentrftl of lt101

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

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bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

- I _

r

I I

I I

I I I

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Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 5: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

~ middotmiddot -- bull

r

nmi To

~~~~~ llevtow of llegton I tontroct Dltll SMO Cut lo- SAS bullo-

Contrac Libu XQd Contract ItoStto N -j~~~tl~~~~~~~~~~~~~~~~~~~~~~ $MO Traffic o a llegton n SAt NO a shyLow Ltvolt_IIH Lno1_Aiifi lno1_soilSOd_llitriWupoundo_

t~ ltltIIICIIt

~a Tl ~u ~~ s-ey of lllto rlftn for tot a taH

1 Dlto Clt-u Ylll~IIII-=-ACID~PUTTCDD_ A bull sslaYl1 bull All t- HltvoiH P bull liilll bull so tt- oot uHOttal for rntn

aN atutogU bull Ubullsseptebh bull S it- 11M1tial for rtv1tw ahi1RJ

II Spoctrtl Porfonco Crttoria YGA (IAlttiiiA (DmPI_

A bull ~ bull All crt torts ott ctrt ofqultty

P bull ~ bull All crttorta not bullt ctrt of reuonulo qultty diU uaoablt for ltlrtlod puIII

U bull IJntssbulletablt bull Cr1tlr1a ut bullt IDICtrt Df poorQral 1ty Uti UftUitabll

UMARG

111 lltot Aotlyota YlllIIII=ACID_IIUT_-nIID_

l bull iW1U1 bull No coot~t~tftlnta abo lrtnt- bullueton 1ta1t no 1nt1rl1rence wtttl _ results

F ~ bull toiIUII1nants DAatnt b~t a1n1a1 1ntTrt bullitll 1111Pll ruultamp

C bull ~sSJptfblt bull ampron ampDfttlll111ai0n too bulletl 1ftttrftnlt to Ult dati hr tttitl CISOftlft11

bull or thl ut1fl frat1oft

bull Sll)tutlo_-__ Contr~et No___

IV Sumgatlto Spfko Rosu1tll VOAlt_tii__AtiD__PtsTnID~ Note StiiP1t dtto neggod on fndlvfdua1 basts

A lodtrfdut1 IIIIP11 naHfng crftltlrft

~ bull All suiTIIgttltl racGrtrfu wttlltn crftltorft JIIUiil bull bl tuiTIIfla raCGrtrfaa outatde crftltorft

Uor ra-rfas of lt101 JubsWtfUed bullbull a atrfa offect

lnn1ff bull MJ rfu of lt101 tlllt 111 IOIIubaWt1attd as a bulltrfa affact

t tua s- A-A~shy lt101 of 1u raported 11 suopoct

gt101 fnlt ltlOI of 1 llporled 11 ffiiiil u bull UnbullssepttlJt- ~~middot-1bullbull raported middotmiddot-tllldor bull111 1aa raporled 11 fnrtlfd

yenOA Q of Jc S1aa SYSpoct i lnnlfd 11 = of = S1aa Suspoct lnvaltd ACID= of $111p1aa Suspoct = Innltd PEST~ of S1as Suspect lnvalfd TtiD = of~ S1as Suspect lnvalfd

Y _ ptlrt Rooultl

~bullto No acton talrtn

A bull AclttllUll bull ElillWmiddot U bull Unmoptab1tshy

VDA_III-=AtiD-=-PIST-=TtDD

on lllltrfa Spfkt rasulta a1ooo

lt101 of _da ouUfdl cntorfa gt101 of lt50S of capoiOidl outJflfo crftarfa gt501 of _ ouUfdt crftltorfa andor bullbull1 racoyentrftl of lt101

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

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--_middotr -J Jo(JJgt I

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JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

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no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

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7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 6: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

bull Sll)tutlo_-__ Contr~et No___

IV Sumgatlto Spfko Rosu1tll VOAlt_tii__AtiD__PtsTnID~ Note StiiP1t dtto neggod on fndlvfdua1 basts

A lodtrfdut1 IIIIP11 naHfng crftltlrft

~ bull All suiTIIgttltl racGrtrfu wttlltn crftltorft JIIUiil bull bl tuiTIIfla raCGrtrfaa outatde crftltorft

Uor ra-rfas of lt101 JubsWtfUed bullbull a atrfa offect

lnn1ff bull MJ rfu of lt101 tlllt 111 IOIIubaWt1attd as a bulltrfa affact

t tua s- A-A~shy lt101 of 1u raported 11 suopoct

gt101 fnlt ltlOI of 1 llporled 11 ffiiiil u bull UnbullssepttlJt- ~~middot-1bullbull raported middotmiddot-tllldor bull111 1aa raporled 11 fnrtlfd

yenOA Q of Jc S1aa SYSpoct i lnnlfd 11 = of = S1aa Suspoct lnvaltd ACID= of $111p1aa Suspoct = Innltd PEST~ of S1as Suspect lnvalfd TtiD = of~ S1as Suspect lnvalfd

Y _ ptlrt Rooultl

~bullto No acton talrtn

A bull AclttllUll bull ElillWmiddot U bull Unmoptab1tshy

VDA_III-=AtiD-=-PIST-=TtDD

on lllltrfa Spfkt rasulta a1ooo

lt101 of _da ouUfdl cntorfa gt101 of lt50S of capoiOidl outJflfo crftarfa gt501 of _ ouUfdt crftltorfa andor bullbull1 racoyentrftl of lt101

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

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H 11gt1 ~

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JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

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11--JU tN9~JJ

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Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

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7ltbull-(p UA

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V-17-shygt A~V+6

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NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 7: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

I I I I

Cootratt Lobull~middotJJgtSMO Cut lo___

Yl Dupllutt Spite RaaulU vdtii=_ACJDPESTTCDD_

Abull Amtfkbull bull P bull ~ Ubull ~1

YCIA i of Ill of ACID- of shy=-- =~

-US

ltlSI of bull-uods outsldt crlttro gt S of ltlOS of _ta outaldt crlttrla gtSQI pf cwpiiNia outlict ct1ttria

~middot outside crlttrlt ~middot outaldt crttrlr ~ outaldt crttrll== ~=~=

VII CII_Ufnpllyen vaa_lii_ACID_IIST_n_

Abull ~~ All crlttrla bullt for DOod cll_toerapllyP bull 11119W bull S crlttrla oot oot dati u101bull1bull for1tll1ttd _

Ubull Ynesgptablp Ct1tlrll not bulltbull or Nvtrt taf11nl or Hwtro dllndatoo data f- tftls

ftlctloo bullbullmiddot

m llINI Spite Rasultl VGl_lii_ACID_PEST_ TCIII_

11o splu -ttodl_Spte S-ttod bull Stt attecMd__

middotSWlUl bull P bull Prow1J1pnal bull

Ubull Unasctpttltbull

All _lllldl roporttd alld gtOitnln bull 101 of tllllleud rocobullbulll7middotlo tftln 0111 _uod 8111od ondor lflltlr thla 501 of IIPICttd rl~ftri II -lood gt01t1t otttor facton could bullto tltt diU Ultlblt for llllttd purpoatlloro ttton 0111 -uod lllntltl ondor lUI ~1ft 101 rtCDVIP1 Of Mrl thlfl VM COIIIDOIIftd lftdor tnsaet 1dtftt1f1ci10II of atftllt c~ontnt sp11rtl t alOflt or cgt~~Dintd wtth otntr factors coulc tht dati unYitablt

sro tuaNo____ tontnct Labbl_

r

ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

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SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

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II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

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021

110 n71 12 14

13

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0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

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bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

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J1H JU lmiddotl1middot11_

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bullJ7

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7$ q lfJ

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no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

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ltfJI- middot~I ~ 1

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V-17-shygt A~V+6

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1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 8: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

sro tuaNo____ tontnct Labbl_

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ll 111M llant lllaoltll VOA p 1li~ACID- EST- ltDO shyIll blaat allllllttH_Ilaa~h-SotSiiartal shy

middot-~- bull Elllbull

SU

_ foUId _UId follllf bllt lclofttlflaltl lo lab blsnu refar to lab blaot crltorll for act IIIROP tu~nsntl founcl lnCOIIIIItont wlto Lab bhat aod sho founcl lo IIIIPlts UH blind blaot u blut for case and trut u lab blaot with aloor contoalnttlon amproll tu~oatlbull IOCOftlllttOt wltk lab blut and aho fouod lo bull~lao use bltNI blank as blank fDr cut end tNit u lab blut wtth contPinatlon

~11-1 ) 1 -v ht T ol ~- f~sr

Split 111111 lllaolta VOL__IIli~AtiD_~-ItDD_ lit -1middot~1~-- _

l

A bull WRIlll bull

bull l1211lbull

U Untcctptltlt-

At a coocantntlon of gNitlr than 10 tiMI toa bull1bull1- clltoctlon 11bull1t tilt - _ lcllntlflaltl br tilt COIItract lab and tilt nglonal lab wtth bull1nor d1fftNnCII 1ft contentrat1on

~~~~~~~~~~~ ~~ middot-- wn lcllfttlflacl br tilt connst lib and tilt Nglonal lab with bullJor d1fftNftCII 1n to~~ctfttrat1on Ttst d11crtPinc1ta uuld cauH tlle diU to H uuful onlr for llaltacl purvon1

~~cenJ~~~1 1~ 10 dlffanooos fOgtIId 1bull bull-bull fdlfttbull lflcltiCOII bJ tilt coatnct lab and bull nglonsl lab TIIIIt dlscrepsnclll coold Clt Uti NIUltl for tl11 f11Ct1on to bt UIICI for 11al till purpolll or UftUIIIblt

f1St DltP1JIIl vi llf olma~gt

~ middot~ ~

0

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SliD CampN ________Cclicl allll---shy

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nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

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II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

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I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

- I _

r

I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 9: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

0

I I I I

middot

SliD CampN ________Cclicl allll---shy

mn -LI DATA

nACTICIN COIIOIIIJ CCINCEIITIATICII

Controctor RogtOftl Labf_ LUI_

i

i

I i

J bull lat1bull1R wa1bull A bull Actlll1 value t111 ~hln valbull tbullWift I bull t Ntle1aol bull- to 111nl- lletiRIOft HbullttU T bull Toouthe ta~tftcottao

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

- I _

r

I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 10: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

II II II II I II I I tiMII II II CDrIIII~IIUTIOIWIII IDUTJtUt tciiPOlIDIu fbullbulltl

II UUIIll 1111UitiU r ~middot nu ana unulDIItll mnunn

amplcowmcT bull= llfflll UUIUTI DA11 UUIUttiUftllm U fiD Uti [ flf~~middotmiddotmiddot tl - ItltiWD IPctlllllt amu ru ccc 11 Ill UlttIll ii Ill II bull Ill bullbullltllIll~

llll 1m IIIll~ I IU IIUltiiiCIUUKcashy ttl 6U I

Jlllftlla CIIIIIK Uti U MI ampII

n~ UJ em 11 1n IU

11111 IIIWtllaiJ

I WI 11111-nwl I HI ~ uu middot IllmiddotUt lit

I IJt Illllt-llcanaamiddotmiddotmiddot~ middotII littta- shyttll~ In 111 Ill lilt- miampS8111 Ill atstampm acmn _~ tm IN

IllmiddotIll tulllllooll~ 1_ ua Illmiddot Illllftl shy

UI middot lit 11111~ 711an middot IllKtl l lmiddotlll~

II nUlshy middot ttftlt-1shy_nmma middot _ middot nt

uushy middot an middot Ill II

no II IIna~a--s

middot HI II

middotmiddot~

~--- middot 1 ~

tsl~ l lll tlntrIIIUa middottn n tlllbull t tu 11n II llfU num middot au

tttu bull um1 unaatn ll 111 Ulllll or Rm _tllf tftltGt wbullt rampmll lftt bull ltlftl PDfDIRIIt rnl tMCieliU

II IUD bull fDta ULlTft SUDampID Jnlll It rov 111

U ISirlU lUI bull Cft filM U 111 LW 11m bullm ftampUUIIU II L~l nr

1---=middot

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

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hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

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bull)

7$ q lfJ

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Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 11: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

I I I I

I I II II II II bull II I II I III II IJillCCIItJII tampIIUT1CI Ula II IOUTJ~tUL~~I f

Imiddot

Imiddott~lII () IIW l llll CUIIIITJbull Jampft UIIIIU

11~ Till UIOUTR1 JD tmtUut

t~lllll lltlbullnn amut

Jill

llrTUI tlUWTI tlft IIUIU [~JmiddotaubullbullrMceampllll

U i u u

II tlllla ii tbull IPU II l ltl

Ill UI Ill ~ It _ 1111

1117 middotIIUltllll CIUIIII Ill II~ II

11aal aullll IU middotlit IISfl~ uu I JU IIIU~tUNIK 1

11111 11111~

I HI middottUf II I ampU II

ltlca-w ~

II

Ultmiddot anbull II

II II - middotmiddotmiddotl$7 ltlttMII~

II Ill IIII1Caii81IIDCIIa1K IIuanmwrm 711

11111bull11 - lll_l_ middot I IImiddotIll

Ill II I

11-IWIshy middot 111111 Ill middotm II14111--rllll bulln11t Mlnabullmus Ill an I

u shy n middot II IIU lfiCUtWUIIIIDfltlll IIaas--mtnrem middot II

Ill II 11

Jtl- shy middotan m 111~ Ult__ UI Ill tiTC IIn m

I IImiddotUittaa ~ - II- 1middot111 unmiddot I~- IllnmICIII

141 atu u11ftliIBI ntiTftlll UI middot

I I

Ulr bull ~~ Ua tiiIICII~ U 1ll uetr ll Rltl ca bull WIILI~la RIQ CIJogtlttl

Ill_ltlf bull ftllCI ltltbulll U~ IPC bull ltiTIP PRrtiiMCI CIICI CMiallttl bull~UB raa uurrn rtiOW tnnrrbull

u u hlrJt ISirtU IUtt bull tfl filii ll rot Ul Lm~ Wlll DUitiUIIU Of UDl Plr

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

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J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

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Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

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I I

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I I I

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Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 12: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

( bull ftl1amp11 iitUU~middotU~IIk61~ ) lltVvbull_ vv-bullbullbullbullbullbullbullbull bull bull bull )

c-____________ c-__ ___bull-middot------- No----shyc-c~

----~~-~---~-----~-rmiddot~-~-~~~middot~-~middot-----~---- --------rmiddot~-~r~-~-~middotr=~~-WL~A~~=rbull~ middot--middot~------r-middot---------r--- -~-~-~-~-~-T--~-~------T-----------middot-1~~~middot~middot~~~---- -- middot-=middot -= =--middot --=-middot bull-- ~ =middotmiddot ----------l-----~~---~----~1----~-----~---~-~--~-----l------- ~-- ~

at -1 9ii 101 91 ------- shyJL- 011-11] 301 Ill 1011 11lt1 _

middotmiddotl-011-117 R-lliO _lJII_ U__I-----1----1----1----1---- --- ==--shy~t-011-MS ]Q] 1(14 Jill 1-1111- ]IM - -----------middot -- shy-=- =--------t-~-1---11---t---l------------- shy1- 0IIJOS middot 90 9L or ---1-1~-middot---middotbullmiddot~~ ----------- shymiddot-~~ M M 95 ----1- -----shyimiddot~-011-li ~--raquo--- ---- shymiddotL-011-PS 111115 tno

~~~ 3011t~l -----------------_- -------middot- ------- shymiddot~L-011-011 bullJOI 100 __]JI)___-- ------ - shyIKL-011-rc liO 96 95 M -------shy

~~ llLi~---11_==1=~=+==~==~~===+==~===1=== 1- 011- VI 312 1110 911 __lL__~---f----l---f----f----~---1-----~ - -1----l---t---1---l---l--+---l---11-- ------shy--t----1----t---t----t---- ----- ----middot---ll---l---l------ shyl--l--~---l---l---l---l---+---~--+---1--~------ 1--------- shy

1-- r-------shyl--l---1--l---l----1--l---l--1-------- shy--+---+--+---l---1--- ----1- ---1--~~--1---i--

YAIOCS - IJUTiliiE CF CIJNTRACT MCIUIIpound0 OC lloiTS -- __lL_JL roc- -LMTSIHY ------ oo1 _____ or oc -middot __ __ roc-middot

~ ---------------------------------------------------------------shy

ltitfo~~ ~IJWtUSINIWGW middot~r 31105-~

J middotmiddot~ --OOAIO~A q P II ~ Hpou ---_ bull1u bulllA M iiIWIII------- ---shy

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

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bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

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I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 13: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

( WIITIR MATRIX SPIKEIIATRIJI ( )IKI DUPLICATE RECOVERY l tObullbullbull t _ _____IlL~-- c _________

cbullbullmiddotmiddot ---rt-------shyfiiACTshy- - COftC -o =middotu CIIOIC

OIS r ocimiddot MC jf ~nv-

SMO SA_IMO

~-011-PS-

middot~---shyT_ n o

n ngtn

021

110 n71 12 14

13

-m~

0-25 n JIM 027 lOll 4 21

5_

31middot11 41middot111

_ SAW(110

bull ACID

114middot 1~

middotmiddot~shy NMttmiddotDIbull 14middot0~

middot~~~middot-

ll ll

u

21middotmiddot~r--41-11_

J~t_LOiil

SNIMU NO

IEST middotOtlerbull3-MI_ __ ~

_ u

bullbull

21middot1 3 23-ll

bullun___ WWo-shy-1shy

SAMIlENObull middotvor

_ II I

21

12middotUI

JImiddotU7

_________L__ ____ -ocshy_____ lliCOYEfiY -L-oll oc _______ CID__

Nsr__ oc-ocshy-oc--oc--oc--ocshy~------------~-----------------------------~-

~~ ~Ilwtf1SIHlwcJil bull lfllt 3Al05-~

---shy

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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I I

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I I I

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Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 14: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

----

c REAGENT BLALlt SUMMARY

____-___________ Ceooctbullbull-~-----bullbull --middotl~lm---

pound ~-_

mfi -middot~middot -shytll-1 Jnllamp -middotshy middotshy111-1 1025R 1M wter low 1111130 67-64-1 141-1 117M WOo bullter law IIIII3ZIII 75-ot-2 111-1 11764 WOo wter low lm3201 67-64-1

- -

-

-

___

__ shyu_l _lertdo-shy

-middot 6R

24 28

22

--middot JIIlL_ _s_

-l9lL _1_0_ ug1 ~ ug1 10

-shy---shy-shy-shy-shy--shy-shy-shy1shy-shy

- -- - -shy-shy--shy- - -shy-shy-shy- shy -shy

cRio~~ ~IL~SINIWltJW middot~t 31-QS-~

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 15: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

Bromofluorobenzene (aFa)

No ampp orelt Comracror _ vr_____ Conuoct No

fl--ID~ DIU __IQbullofmiddotl~J____ 111111--3middot1J____

bulllt liON UUNDANCI CRITIJUA UILATIYIMUNOANCI

10 110 ~ fQft pull middot 79 71 JDD middotltO puk i-1-U

bull bullmiddot 1005 tn 100 II UbulllfteflftiMaJUII 5W

171 _ftn1JalflhiiMbullIiiiM bullltJtJ 17 _tflllniOAMebutk Mi 171 ~ middotbull of - -~ (JJ)1

171 bull ttft na ~ 101a ( JJ cw-n 1

177 UmiddotI11Sol-171 4middot1gt4 middotcn 2

1VUIRW IIbullbull nbull 2vto~o-middot- 171

TMII PIOOOMANCI TUNI ALIII TO THI OLLOWING ampAM~II ILAIIU AND ITANOAODL

IAWLIID

~IIA

AlPbull ~~ -~IN fl ft

- -J1v ~Lmiddott)lh5middot3d ~( ~Mo IJ4

~--middot _ 1 middotNmiddot oAlmiddot SOj 1fl bull 111- rlt- d J-~ JJ A Jt gti olt(

--_middotr -J Jo(JJgt I

LAIID

1J~Ifi

hAbullbullJ bullJIJIJ61

H 11gt1 ~

~ lj ltt ~ I~IJ 41 IMI -1011117

JJIIJ

Jill 69 1IJIJ9 lflf(lt Nibil IIITJ

OATl 01 ANALVIII

11--JU tN9~JJ

LHmiddotJil HJ-~~ - 11 ~M-Jf_

IDmiddotRmiddotid )middot IJjj

-~-JJ tl~t-JJ )v JI

J1H JU lmiddotl1middot11_

TIMI 0 ANALYIII

I(

bullJ7

bull)

7$ q lfJ

-~-~ gtbullIn ~bull11~

middotn )

I

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

--toJ 7o tJ I If

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I I

I I

I I I

I I I I

Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950
Page 16: LETTER REGARDING DATA VALIDATION REPORTS · 2020. 9. 2. · All of tht llll>loo . wro roc:olvod on 10/lt/84. Anel1fu oc:culftd on 10/25/84 end 11/7/84. Tho 11/7/84 1111>lH hod btln

Bromofluorobenzene (SFS)

no No ~FZrf( Connctor _ _~lt4opound_____ Conuoct No ---- shy

bull_ ID C~ Doto IImiddot Z4J TIIN tt4(

Dou Rolu11 AUIIIoriJod~ ------------ shy

UIampATIIIUUNDAHCI

10 111 middotaal lbl u pt XIO middot IDDIIof __

71 4~-1

bull bullk ralatiw llluNSinbull ttJOI II LO bull tCN et mt 111M pull 91 173 1amp - pnk bull1middot4b

ar INft IOft et 1111 nbull a-u 171 t-Omiddot)ftof_ JSI ~)

middot~

171 arer INft ft~ M Will 10lDI Di IMa 17 fa)19middot 7 IDmiddotIftof- 171 7) 2r-m -f-I

v~ bull 2vaiutlrl~bullbull bull171

THII IRORCI TUNIALIII TO THI 0LLOW1NG IAMILll ILANKI ANO ITANOAROL

IIAWUIO

_-A- (

7ltbull-(p UA

ltfJI- middot~I ~ 1

10

V-17-shygt A~V+6

NL 1)

NI~Amiddot ~~ ~ k

I DATI 0 ANALVSII

1-middoti+ I middot7-IY 7middot middot7middot11

bull 7middot1yen IImiddot 7middot 1

TlMl OF ANALVIII

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I I I

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Ji-llfJ irI It_ fflbullbull

I

  1. barcode 553950
  2. barcodetext SDMS Doc ID 553950