Letter ofTransmittal

ED BARBER & ASSOCIATES Wildewood Professional3639 Cortez Road West, .:lUlilN:.L

Bradenton, Florida 34210Tel: 941-739-3903 Fax: 94 ~l?!39_3~~~CE:::IVea

Date: May 11, 2000

Letter of Transmittal

To: Theresa Connor / Sarasota County Storm Water

Project Name: Phillippi Cr. Navigation Dredging

Project No.: 01-07

The following items are transmitted:

_ For Approval X. For Your Use X As Requested For Review Please Return

1. Analytical data collected to support the applications to FDEP for authorization to dredge thecreek. (Note that the detail sheets for sieve analysis are not quite complete. Will provide assoon as we get a complete set together.)

2. Map illustrating sampling locations.

Remarks:

~I

igned: /?-l~~- '4

'-

s

Cc:

~ryv\ L--yf:i,-.(

WCIND Phillippi CreekDredging Project

PUBLIC WORKS

STORMWATER

"

•__ APPROXIMATE MAINTENANCE DREDGING LOCATIONS

I,-=~I~1...- /r'

===l'}=~1

C::====:;1---; I

wc.rNlJTEMPORARY DISPOSAL LOCATIONS

A c.,.1 ... _-...~ =® CorporationEnvironmental Quality Laboratory

October 15, 1998

ED BARBER & ASSOC. (Philippi Creek)3639 CORTEZ ROADSUITE 106BR~DSNTON FL 34210 Cust. Froj :?HILIPPI CREEK SOIL SAMPLI~G

Attached are the results from 7 sa~ple(s) received bythe EnvirOi:mental Quality Laboratory for analysis.The EQ Lab identification nuwber is 98/4002/ 6528; please refer tothis number when requesting information regarding these data.Also, this letter should be attached to any data submitted by youto regulatory agencies.

I

The Laboratory has a~ approved FDEP Comprehensive QualltyAssurance Plan (#870264) which specifies the proced~res used inthe analyses of the above referenced samples. In addition, theLaboratory is certified by FDOH for the analysis of environmentaland dl:-:'nk:;.ng "..rater samples (#E85086 & 85116) respect:ivel:i. Thesecertification numbers should be referenced when attescing tQr:egulatory agencies regarding the protocols of the analyticc.lprocedures used.

The Environmental Quality Laboratory is pleased to have served youc.nd hopes to meet any future laboratory r:eeds you may have.

SinceI'ely I

q(Y./l.l r L- Irdirt Kondel /_Laboratorvioperations Mana~_':er./ .

Laboratory Testing & Environmental Services,

1009 TAMIAMI TRAIL, PORT CHARLOTTE, FLORIDA 33953 • PH 941-625-3137 • TOLL FREE 1-877-452-2712FX 941-629-7467 • EMAIL: [email protected] • WEBSITE: www.ascicorp.com

a Crt.... _ -...~ =@ CorporationEnvironmental Quality Laboratory

ORGANIC SAMPLE ANALYSIS

Customer: ED BARBER & ASSOC. (Philippi Creek)

Customer Project: PHILIPPI CREEK SOIL SAMPLING

Page: 1Date:lO/15/1998

Lab ID :98/4002/ 6528Sample#: 11900

Station#/Location: 1 STATION #3

Sample Date: 09/09/1998

ParameterName

Analysis AnalysisResult Method

A!lalysisDate

Det.Lt. *DQUsed

ORGANOCHLORINE PESTICIDES (Soil)Extraction Date: 09/23/1998

ug/Kg

a-BHCb-BHCd-BHCEndosulfan IEndosulfan II

Endosulfan Sulfate4,4' -DDE

4,4' -DDD

4,4' -DDT

Endrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-1016PCB-l221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Chlordane

< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C<1000.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C< 60.0000 EPA 8270C

10/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98J.a/06/S'8

60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U

1000 U60.0000 U60.0000 U60.0000 U60.0000 U

1240 U1240 U1240 U1240 U1240 U1240 U1240 U

60.0000 U

NOTE: Reported Results not valid without accompanying signature page.* See attached Data Qualifier Codes

Laboratory Testing & Environmental Services1009 TAMIAMI TRAIL, PORT CHARLOTTE, FLORIDA 33953 • PH 941-625-3137 • TOLL FREE 1-877-452-2712

FX 941-629-7467 • EMAIL: [email protected] • WEBSITE: www.ascicorp.com

A c.-I ... _ .........~ =® CorporatIonEnvironmental Quality Laboratory

ORGANIC SAMPLE M~ALYSIS



Page: 2Date:10/15/1998

Lab ID :98/4002/ 6528Samp 1 e # : 119 01



ParameterName


AnalysisDate

Det.Lt. *DQUsed


UglKg

a-BHCb-BHCd-BHCEndosulfan IEndosulfan IIEndosulfan Sulfate4,4'-DDE4,4' -DDD4,4'-DDTEndrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Chlordane

< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA S270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C<1000.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C< 60.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C<1240.0000 EPA 8270C< 60.0000 EPA 8270C

10/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98lO/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98;.0/06/98

60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U60.0000 U

1000 U60.0000 U60.0000 U60.0000 U60.0000 U

1240 U1240 U1240 U1240 U1240 U1240 U1240 U

60.0000 U


Laboratory Testing & Environmental Services1009 TAMIAMI TRAIl., PORT CHARl.OTTE, FLORIDA 33953 • PH 941-625-3137 • TOLl. FREE 1-877-452-2712

FX 941-629-7467 • EMAIl.:[email protected] • WEBSITE: www.ascicorp.com

ae.-I.. _~~ -® CorporationEnvironmental Quality Laboratory




Page: 3Date:10/15/1998

Lab ID :98/4002/ 6528Samp1e#: 11902



ParameterName


AnalysisDate

Det.Lt. *DQUsed


ug,/Kg


Endosulfan Sulfate4,4' -DDE4,4' -DDD4,4' -DDTEndrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-1016PCB-1221PCB-1232PCB-1242PCB 1248PCB-1254PCB-1260Chlordane

< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C<1040.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C< 65.0000 EPA 8270C<1300.0000 EPA 8270C<1300.0000 EPA 8270C<1300.0000 EPA 8270C<1300.0000 EPA 8270C<1300.0000 EPA 8270C<1300.0000 EPA 8270C<1300.0000 EPA 8270C< 65.0000 EPA 827GC

::"0/06/9810/06/9810/06/9810/06/98::"0/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98

65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U65.0000 U

1040 U65.0000 U65.0000 U65.0000 U65.0000 U

1300 U

1300 U

1300 U

1300 U

1300 U

1300 U

1300 U

65.0000 U



FX 941-629-7467 • EMAIL: [email protected] • WE8SITE: www.ascicorp.com

Ac..1.... _ -....~ =® CorporationEnvironmental Quality Laboratory




Page: 4Date:10/15/1998

Lab ID :98/4002/ 6528Samp1e#: 11903



ParameterName


AnalysisDate

Det.Lt. *DQUsed


ug/Kg


Endosulfan Sulfate4,4' -DDE4,4' -DDD4,4' -DDTEndrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-10l6PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Chlordane

< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 827~C

< 59.0000 EPA 8270C< 940.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C< 59.0000 EPA 8270C<1170.0000 EPA 8270C<1170.0000 EPA 8270C<1170.0000 EPA 8270C<1170.0000 EPA 8270C<1170.0000 EPA 8270C<1170.0000 EPA 8270C<1170.0000 EPA 8270C< 59.0000 EPA 8270C

10/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98

59.000059.000059.000059.000059.000059.000059.000059.000059.000059.000059.000059.0000

940.000059.000059.000059.000059.0000

1170117011701170117011701170

59.0000

uuuuuuuuuuuuuuuuuuuuuuuuu




ac:..1.. _ ............-. =® CorporationEnvironmental Quality Laboratory




Page: 5Date:10/15/1998

Lab ID :98/4002/ 6528Sample#: 11904



ParameterName


AnalysisDate

Det.Lt. *DQUsed


ug/Kg

a-BHCb-BHCd-BHCEndosulfan IEndosulfan IIEndosulfan Sulfate4,4' -DDE4,4' -DDD4,4' -DDTEndrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Chlordane

< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C<2500.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C< 160.0000 EPA 8270C<3100.0000 EPA 8270C<3100.0000 EPA 8270C<3100.0000 EPA 8270C<3100.0000 EPA 8270C<3100.0000 EPA 8270C<3100.0000 EPA 8270C<3100.0000 EPA 8270C

543.0000 EPA 8270C

10/06/9810/06/9810/06/9810/06/9810/06/9810/06/98:i.0/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98

160.0000160.0000160.0000160.0000160.0000160.0000160.0000160.0000160.0000160.0000160.0000160.0000

2500160.0000160.0000160.0000160.0000

3100310031003100310031003100

160.0000

uuuuuuuuuuuuuuuuuuuuuuuu




A e.-I .... ... ............-. -. CorporatIon

. <Ill

Environmental Quality Laboratory




Page: 6Date:10/15/1998

Lab ID :98/4002/ 6528Samp1e#: 11905



ParameterName


AnalysisDate

Det .Lt. *DQUsed


a-BHCb-BHCd-BHCEndosulfan IEndosulfan IIEndosulfan Sulfate4 / 4 / -DDE4 / 4 / -DDD4 / 4 / -DDTEndrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Chlordane

< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C<1500.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C< 95.0000 EPA 8270C<1900.0000 EPA 8270C<1900.0000 EPA 8270C<1900.0000 EPA 8270C<1900.0000 EPA 8270C<1900.0000 EPA 8270C<1900.0000 EPA 8270C<1900.0000 EPA 8270C< 95.0000 EPA 8270C

10/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/9810/07/98

95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U95.0000 U

1500 U95.0000 U95.0000 U95.0000 U95.0000 U

1900 U1900 U1900 U1900 U1900 U1900 U1900 U

95.0000 U


Laboratory Testing & Environmental Services1009 TAMIAMI TRAIL, PORT CHARLOTTE, FLORIDA 33953 • PH 941-625-3137! TOLL FREE 1-877-452-2712


II e.-I ... _~~ =® CorporationEnvironmental Quality Laboratory




Page: 7Date:10/15/1998

Lab ID :98/4002/ 6528Sample#: 11906

Station#/Location: 7 EQUIPMENT BLANK

Spmple Date: 09/09/1998

ParameterName


AnalysisDate

Det.Lt. *DQUsed

ORGANOCHLORINE PESTICIDES[EPA 608] ug/LExtraction Date: 09/23/1998

a-BHCb-BHCd-BHCEndosulfan I

Endosulfan II

Endosulfan Sulfate4,4'-DDE4,4' -DDD4,4' -DDTEndrin AldehydeEndrinLindane (gamma-BHC)ToxapheneHeptachlorHeptachlor EpoxideAldrinDieldrinPCB-1016PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260Chlordane

< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 10.0000 EPA 8270C< 1.0000 EPA 8270C< 1.0000 EPA 8270C< 2.0000 EPA 8270C< 2.0000 EPA 8270C< 10.0000 EPA 8270C< 10.0000 EPA ~270C

< 10.0000 EPA 8270C< 10.0000 EPA 8270C< 10.0000 EPA 8270C< 10.0000 EPA 8270C< 10.0000 EPA 8270C< 1.0000 EPA 8270C

10/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/9810/06/98

1. 0000 U1. 0000 U

1. 0000 U

1. 0000 U

1.0000 U1. 0000 U

1. 0000 U

1. 0000 U

1.0000 U1. 0000 U1.0000 U1. 0000 U

10.0000 U1. 0000 U1. 0000 U2.0000 U2.0000 U

10.0000 U10.0000 U10.0000 U10.0000 U10.0000 U10.0000 U10.0000 U1. 0000 U




.1~15•

Phone (941)625-3137Fax (941) 629-7467

page-lof-!-

~NOCollection

Date

HRS Form?

oYes

FAX:

Phone:

Sample Description

qrl,\ L\(XJ~ V;C'

EOlSample No.

Client: Bl.\j\.\\''Q~( ~

Project: - \N\ ~ \ \ ~ CO\ ('! f:I-;Labid:

Address:

Environmental Quality Laboratory, Inc.1009 Tamiami Trail Port Charlotte, FL 33953

Samole Informatio

Commenls: 'J.u(\ v..>;Chain of Custody Total 1# of Containers. I

Transfer Released by: Dale Time Iwl~ive1&>Y: /l a I1st Steuo (Sample collector) 19-"1-nr- /(.::>-0 "~'\INI~~ JIQIM{Jj1JV2nd \ \" ....,

-I---

.lIh 1(\, 1

1""")-,~

Report Date: 10/23/98

BENCHMARK Page: 1 of 7Reference No.: 98090036

EnviroAnalytical, Inc. Date Received: 09/09/98Time Received: 1540

FDHRS Cor<ificotia> .fEB.4167 and #844.1.1FOER Qualley ...........,. R7O.l94G

Applied Technology & Management, Inc. Date Collected: 09/09/98677 N. Washington Blvd., Suite 41 Collected By: client - SL

Sarasota, FI 34236-4241 Sample Type: grab; EstuarineSediment

Project Name: Phillippi Creek Project

Parameter Result Units MDL Procedure Analyzed Analyst

St8tion #2 • 0910

Percent Solid 79.8 % 0.0 SM 2540 G 09/16/98 RK

Alumminum. 8S AI 546.4 MGIKG 7.86 7020 09/24/98 RK

Arsenic. 85 As 0.72 MGIKG 0.16 7060 A 10/02/98 RK

Cadmium, 8S Cd 0.04 MG/KG 0.01 7131 A '10/02/98 RK

Copper. 8S CU , 1.80 MG/KG 0.05 7211 10/01198 RK

Le8d. 8S Pb 1.69 MGIKG 0.03 7421 10/01/98 RK

Mercury. 8S Hg < 0.08 MG/KG 0.08 7471 A 09/26/98 DD

Zinc. 8S Zn 7.86 MG/KG 0.20 7950 09/24/98 RK

St8tion #3 • 0945


Alumminum, 8S AI 358.1 MG/KG 7.19 7020 09/24/98 RK

Arsenic. 85 As 0.88 MG/KG 0.16 7060 A 10/02/98 RK

Cadmium, 85 Cd 0.04 MGIKG 0.01 7131 A 10102/98 RK

Copper, 88 Cu ' 1.23 MG/KG 0.05 7211 10101/98 RK

Lead, 85 Pb 1.05 MGIKG 0.03 7421 10/01/98 RK

Mercury, 85 Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DD

Zinc, 85 Zn 6.59 MG/KG 0.18 7950 09/24/98 RK

St8tion 14 - 1015


Alumminum, 85 AI 2923 MG/KG 8.90 7020 09/24/98 RK

Arsenic, 8S As 1.92 MGIKG 0.18 7060 A 10/02/98 RK

C8dmium. 8S Cd 0.19 MGIKG 0.01 7131 A 10102/98 RK

Copper, 85 Cu 11.87 MGIKG 1.19 7210 09/15/98 RK

Le8d. 85 Pb 12.53 MG/KG 0.03 7421 10/01/98 RK

Mercury. 8S Hg < 0.08 MGIKG 0.08 7471 A 09/26198 DO

Zinc, 85 Zn 25.97 MGIKG 0.22 7950 09/24/98 RK

653 Tenth Street East • Palmetto, FL 34221 • PHONE (941)723-9986 • FAX (941)723-6061

'.




FDHItS e-IIIcoUaa 1EJ.4161 aal il644S5F'DER~_~


Sarasota, FI 34236-4241 , Sample Type: grab; EstuarineSediment



Station #5 - 1032

Peroent Solid 25.2 % 0.0 SM 2540 G 09/16/98 RK

Alumminum. as AI 8240 MGIKG 20.2 7020 09/24/98 RK

Arsanio. as As 7.36 MG/KG 0.54 7060 A 10/02/98 RK

Cadmium. as Cd 1.05 MGIKG 0.04 7131 A 10/02/98 ' RK

Coppar. as Co. 91.0 MG/KG 2.70 7210 09/15/98 RK

Lead. as Pb 67.4 MG/KG 11.8 7420 09/16/98 RK

Meroury. a8 Hg 0.21 MG/KG 0.09 7471 A 09/26/98 DO

Zino. as Zn 118.8 MGIKG 0.50 7950 09/24/98 RK

Station #6 • 1045


Alumminum. as AI 497.2 MG/KG 8.10 7020 09/24/98 RK

Arsenio, as As 0.54 MGIKG 0.16 7060 A 10/02/98 RK

Cadmium. as Cd 0.05 MGIKG 0.01 7131 A 10/02/98 RK

Coppar. as Cu 1.74 MG/KG 0.05 7211 10/01/98 RK

Lead. as Pb 1.56 MG/KG 0.03 7421 10/01/98 RK

Meroury. a8 Hg < 0.08 MGIKG 0.08 7471 A 09/26/98 DO

Zino, as Zn 7.40 MGIKG 0.20 7950 09/24/98 RK

Station 17· 1057


Alumminum, as AI 493.9 MG/KG 7.90 7020 09/24/98 RK

Arsenio. as As 0.61 MGIKG 0.14 7060 A 10102/98 RK

Cadmium, as Cd 0.46 MGIKG 0.01 7131 A 10/02/98 RK

Copper, as Cu 1.63 MGIKG 0.05 7211 10/01/98 RK

Lead, as Pb 1.60 MGIKG 0.03 7421 10/01/98 RK

Meroury, as Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DO

Zino, as Zn 6.58 MG/KG 0.20 7950 09/24/98 RK

653 Tenth Street East • Palmetto, FL 34221 • PHONE (941 )723-9986 • FAX (941 )723-6061




FDHRS e-IIkaIIca ~167 ond IS4455FOD Q\&llly~ AlI7Q594G




Parameter Result Units MOL Procedure Analyzed Analyst

Station 18 • 1105


Alumm;num, as AI 1190 MG/KG 7.10 7020 09/24/98 RK

Arsenic. as As 1.21 MGIKG 0.17 7060 A 10/02/98 RK


Coppar, as Cut 4.03 MGIKG 0.06 7211 10/01/98 RK


Mercury, as Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DO

Zinc, as Zn 10.12 MGIKG 0.18 7950 09/24/98 RK

Station 19 • 1115



Arsenic, es As 0.85 MGIKG 0.15 7060 A 10/02/98 RK


Copper, as Cu 1.35 MGIKG 0.07 7211 10101/98 RK

Lead, as Pb 1.38 MG/KG 0.03 7421 10/01/98 RK


Zinc. as Zn 8.57 MGIKG 0.17 7950 09/24/98 RK

Station 110- 1128


Alumminum, as AI 498 MGIKG 7.46 7020 09/24/98 RK

Arsenic. as As 0.50 MGIKG 0.25 7060 A 10/02/98 RK



Lead, 8S Pb 1.25 MGIKG 0.03 7421 10/01/98 RK

Mercury, 8,8 Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DO





EnviroAnalytical, Inc. Date Received; 09/09/98Time Received: 1540

F'DHIU~ 1EIl4167 ODd~FOEll Quo1IIy~ I8iOS94G

Applied Technology & Management, Inc. Date Collected: 09/09/98677 N. Washington Blvd., Suite 41 Collected By: client - SLSarasota, FI 34236-4241 Sample Type: grab; Estuarine

Sediment



Station #11 - 1157


Alumminum, as AI 836.5 MGIKG 6.81 7020 09/24/98 RK

Arsenic, as As 2.80 MG/KG 0.15 7060 A 10/02/98 RK

Cadmium, as Cd 0.08 MGIKG 0.01 7131 A . 10102/98 RK

Copper, as CU' 1.19 MGIKG 0.06 7211 10/01/98 RK

Laad, as Pb 1.25 MGIKG 0.03 7421 10/01/98 RK

Mercury, as Hg < 0.07 MG/KG 0.07 7471 A 09/26/98 DO


Station #12· 1229




Cadmium, as Cd 0.09 MG/KG 0.01 7131 A 10/02/98 RK

Copper, as Cu 2.94 MGIKG 0.07 7211 10101/98 RK

Lead, as Pb 1.36 MG/KG 0.03 7421 10/01/98 RK



Station #13 - 1243


Alumminum, as Al 779.2 MG/KG 6.87 7020 09/24/98 RK

Arsenic, 8S As 0.76 MG/KG 0.15 7060 A 10/02/98 RK

Cadmium, 8S Cd 0.08 MGIKG 0.01 7131 A 10102/98 RK

Copper, 8S CU 2.21 MGIKG 0.06 7211 10/01/98 RK

Lead, 8S Pb 1.74 MG/KG 0.03 7421 10101/98 RK

Mercury, 88 Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DO

Zinc, 8S Zn 9.15 MGIKG 0.17 7950 09/24/98 RK



"BENCHMARK Page: 5 of 7Reference No.: 98090036


FIlHIU ConIIiaotioD 1Ell-4167 OPCI 184455FDEJl QwJily -..... NlO594O

Applied Technology & Management, Inc. Date Collected: 09/09/98677 N. Washington Blvd., Suite 41 Collected By: client - SLSarasota, FI 34236-4241 Sample Type: grab; Estuarine

Sediment



Stetion 114 • 1257




Cedmium, a6 Cd 0.06 MGIKG 0.01 7131 A . 10/02/98 RK

Copper. as Cu, 1.50 MGIKG 0.06 7211 10/01/98 RK

Lead, as Pb 1.63 MG/KG 0.03 7421 10/01/98 RK

Mercury, 8S Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DO


Station 115 - 1306


Alumminum. 8S AI 595.5 MG/KG 5.89 7020 09/24/98 RK


Cedmium. 8S Cd 0.07 MGIKG 0.01 7131 A 10102/98 RK

Copper, 8S CU 0.98 MGIKG 0.06 7211 10/01198 RK

Leed. 86 Pb 3.09 MGIKG 0.03 7421 10101/98 RK

Mercury, 8S Hg < 0.09 MGIKG 0.09 7471 A 09/26/98 DO


Station 116 • 1313


Alunvninum, 86 AI 1122 MGIKG 7.48 7020 09/24/98 RK

Arsenic. 8S As 2.15 MG/KG 0.14 7060 A 10102/98 RK

Cedmium, 8S Cd 0.12 MG/KG 0.01 7131 A 10/02/98 RK

Copper. as Cu 1.60 MGIKG 0.05 7211 10101/98 RK

Laed. a6 Pb 2.17 MG/KG 0.03 7421 10101/98 RK

Mercury. a6 Hg <: 0.08 MGIKG 0.08 7471 A 09/26198 DO

Zinc, 86 Zn 6.85 MGIKG 0.19 7950 09/24/98 RK



BENCHMARK Page: 6 of 7, Reference No.: 98090036


FOHRS CcrtificalioollEll-4167 and .Ml445.'lFDER QuaJiIy "--'"~





Station 117 - 1334


Alumminum, as AI 1583 MG/KG 6.82 7020 09/24/98 RK

Arsenic, as As 1.86 MGIKG 0.18 7060 A 10/02198 RK


Copper, as Cu: 4.54 MGIKG 0.91 7210 09/15/98 RK




Station #18·1351




Cadmium, as Cd 0.46 MGIKG 0.02 7131 A 10102/98 RK

Copper, as Cu 23.2 MG/KG 1.28 7210 09/15/98 RK




Station #19 • 1409


Alumminum, as AI 6925 MGIKG 7.96 7020 09/24/98 RK

Arsenic, as As 12.04 MGIKG 0.19 7060 A 10/02/98 RK

Cadmium, as Cd 1.18 MG/KG 0.01 7131 A 10/02/98 RK



Mercury, as Hg 0.048 MGIKG 0.02 7471 A 09/26/98 DO



BENCHMARKEnviroAnalytical, Inc.

Report Date:Page:Reference No.:Date Received:Time Received:

10/23/987 of 79809003609/09/981540

FDtUU Cortlficotloo fE&.4167 and iIll4<5SFOEll. QuoII\)' ............. WlOS~

Applied Technology & Management, Inc.677 N. Washington Blvd., Suite 41Sarasota, FI 34236-4241

Date Collected:Collected By:Sample Type:

09/09/98client - SLgrab; EstuarineSediment



Station #20 - 1427


Alumminum. as AI 1084 MG/KG 8.20 7020 ·09/24/98 RK

Arsenic, as As. 0.87 MGIKG 0.18 7060 A 10/02/98 RK


Coppar, as Cu 4.09 MGIKG 1.09 7210 09/15/98 RK

Lead. as Pb 3.78 MG/KG 0.03 7421 10/01/98 RK



Station #21 - 1443





Coppar, as Cu 65.04 MGIKG 1.71 7210 09/15/98 RK


Mercury, as Hg 0.104 MG/KG 0.02 7471 A 09/26/98 DO


((~·i. L'~U~~~Laboratory Director

AU~ potfotmod loa llOCOIIIoDco will> 1ho __ 0flP"0"'ld <diu.- 0( Sundanl Melhodo rOi \he Eumino'kln

0( w.1IIJ' and wU\OW!"" and Me!hod! rOi CbtmkaJ Ano!yola 0( WI"" and wu........... OIbotwile DOled.

653 Tenth Street East • Palmetto, FL 34221 • PHONE (941)723-9986· FAX (941)723-6061

Sieve Analvsis & Classification~ c>

Date Sampled September 09, 1998Date Sieved _~S~e~p~te=::.m~b=e=r~1~6.1-'1~9;.,::9~8_

Project Name: Cust# 4002 LABID 6528

Sample #: Sample Location: __S~t~a~ti~o~n~#.:::.3 _

Material Description: Pale brown fine sand / shell fra~mentsWeight of Oven Dry Sample: _----=2=0=5;.:.:.1=-- _

Weight of Sample After Wash: _-=2=0=3=.8'-- _

..... '

. ..... ..... .'..... '.

U:S>Sieve ..... .Weight (Acc.)gms '>%Retained % Passing

3/8" 1.0 0.5 99.5

1/4" 1.2 0.6 99.4

No. 16 6.0 2.9 97.1

No. 20 9.0 4.4 95.6

No. 60 155.6 75.9 24.1

No. 100 198.5 96.8 3.2

No. 200 203.2 99.1 0.9

PAN 203.8

P-200 = 205.1 - 203.8 = 1.3 / 205.1 = JhL 0/0

Dry weight Wash weight Loss Dry weight P-200

(gm) (gm) (gm) (gm)

% Moisture =260.6 205.1 = 55.5 / 205.1 = 27.1 %

Wet weight Dry weight Loss Dry weight % Moisture

(gm) (gm) (gm) (gm) Content

Technician Initial EL

Sieve Analvsis & Classification• cr

Date Sampled September 09, 1998

Date Sieved _....:S=e::.&'p=te=m=b=e::..:..r-"1=6,,--,,1,,-,,9~9=8_


Sample #: Sample Location: _-,S=t=a=ti=on~#=6 _

Material Description: Pale brown fine sand / shell fra2ments

Weight of Oven Dry Sample: _~2~2~5~,7:.....-. _

Weight of Sample After Wash: _-=2~3=5.:...:4 _

u.S. Sieve

3/8"

1/4"

No. 16

No. 20

No. 60

No. 100

No. 200

PAN

0.0 0.0

0.0 0.0

0.0 0.0

0.02 0.0

66.7 28.3

227.1 96.3

235.2 99.8

235.4 99.9

% Passing

0.0

0.0

0.0

0.0

71.7

71.7

0.2

P-200 = 235.7 - 235.4 = 0.3 / 235.7 = JhL %


(gm) (gm) (gm) (gm)

% Moisture =296.7 235.7 = 61.0 / 235.7 = 25.9 %




Sieve Analvsis & Classification.- ....


Date Sieved _--,S=e"",p=te=m=b=e=r--"I~6.L.'1"",9'-'09=8_


Sample #: Sample Location: _--,S=t=a=ti=on=...:.:.#~9 _

Material Description: Pale brown fine sand I trace shell fra~ments

Weight of Oven Dry Sample: _--=3~7~3~.2~ _

Weight of Sample Mter Wash: _ ....3:...!,.7.=2.:,:::3 _

>.·••••.••·.··i •••·•....... . .. .. . ..... i>

.... ., .. U.S•. Sieve I .Weight(Acc.)gms % Retained % Passing

3/8" 0.0 0.0 0.0

1/4" 0.0 0.0 0.0--

) No. 16 2.4 0.6 99.3

No. 20 3.5 0.9 99.1

No. 60 283.1 75.9 24.1

No. 100 369.4 99.0 1.0

No. 200 372.2 99.7

PAN 372.3 99.8_.

-

P-200 = 373.2 - 372.3 = 0.9 I 373.2 = J!:.L %


(gm) (gm) (gm) (gm)

% Moisture =480.3 373.2 =107.1 I 373.2 = 28.7 0/0

Wet weight Dry weight Loss Dry weight % Moisture,



Sieve Analvsis & Classification• u


Date Sieved _--,S:;:.;e"&,p:..:.;te=m=b=e=r-=I",,,,6,L.'1=9:...::;9=8_


Sample #: Sample Location: __S::::..t=a=ti=o=n..:.:,#-"'13""- _

Material Description: Pale brown fine sand / trace shell fra~ments

Weight or Oven Dry Sample: _----:4~2~3~.7~ _

Weight of Sample After Wash: _--'4~2_"'1.:...:4 _

.'....:'...."..:'.:.: .. .. .. ..

·:·W~i;l1t(i\.c~hgms '..:.:.: . .... .

(U.S. Sieve % Retained % Passing

3/8" 0.0 0.0 0.0

1/4" 0.0 0.0 0.0

No. 16 9.4 2.2 97.8

No. 20 23.1 5.4 94.6

No. 60 381.7 90.1 9.9~

No. 100 419.4 99.0 1.0

No. 200 421.1 99.4 0.6

PAN 421.4 99.5

P-200 = 423.7 - 421.4 = 2.3 / 423.7 = J!:L 0/0


(gm) (gm) (gm) (gm)

% Moisture =529.1 423.7 = 105.4 / 423.7 = 24.9 0/0




Sieve Analvsis & Classification~ '"

Date Sampled September 09,1998

Date Sieved _~S~e~p~te~m~b~e~r~1~6.l..'~19~9~8_


Sa~ple #: Sample Location: _---::::.St.l:.::a~ti~o~n...:.:#..:=:.1~5 _


Weight of Oven Dry Sample: _--,2=.::3~3:..:.::.3,-- _

Weight of Sample After Wash: _....::2=3=2::..,:.4'-- _

3/8" 2.9 1.2

1/4" 5.3 2.3

) No. 16 17.9 7.7

No. 20 24.1 10.3

No. 60 200.3 85.9

No. 100 230.9 99.0

No. 200 231.8 . 99.4

PAN 232.4 99.6

% Passing

98.8

97.7

92.3

89.7

14.1

1.0

0.6

P-200 = 233.3 - 232.4 = 0.9 / 233.3 = ..M.- 0/0


(gm) (gm) (gm) (gm)

0/0 Moisture =299.2 233.3 = 65.9 / 233.3 = 28.2 0/0




.-......~........ _ n"",",,-'~" f', .......

Sieve Analvsis & Classification• cr


Date Sieved _....:S~e~p~te=m=b=e=r~1~61..,1~9:....<:9~8_


Sa~ple #: Sample Location: _--=St=a=ti:..:<;o.:=.n...:.:#......1....8 _

Material Description: Pale brown fine sand I trace shell fra2ments

Weight of Oven Dry Sample: _~2~6~3:.:.:.2"-- _

Weight of Sample After Wash: _-=2~5=2=.0'-- _

3/8'1 2.2

1/4" 3.1

No. 16 13.6

No. 20 17.4

No. 60 107.0

No. 100 209.1

No. 200 I 248.2

PAN 252.0

%J~etained % Passing

0.8 99.2

1.2 98.8

5.2 94.8

6.6 93.4

40.7 59.3

79.4 20.6

94.3 5.7

95.7

P-200 = 263.2 - 252.0 = 11.2 I 263.2 = ..1:L %


(gm) (gm) (gm) (gm)

0/0 Moisture =443.7 263.2 = 18055 I 263.2 = 68.6 %




Sieve Analvsis & Classification..- cr


Date Sieved _......:S~e~p~te=m~b~e:::..r~I~6.1..,1~9:....:::9~8_


Sa~ple #: Sample Location: _--'S::::;.;t=a=ti=ono=.....:.:.:#2=1::..- _


Weight of Oven Dry Sample: _---==3~4:...!.7~.1'-- _

Weight of Sample After Wash: _-"3:,.=2=2.=2 _

3/8"

1/4"

) No. 16

No. 20

No. 60

No. 100

No. 200

PAN

0.0

0.0

3.2

4.9

25.7

143.0

315.0

322.2

% Retained

0.0

0.0

0.9

1.4

7.4

41.2

90.7

92.8

% Passing

0.0

0.0

99.1

98.6

92.6

58.8

9.3

P-200 = 347.1 - 322.2 = 24.9 /

Dry weight Wash weight Loss

(gm) (gm) (gm) (gm)

347.1 =

Dry weight

~%

P-200

0/0 Moisture = 584.0

Wet weight

(gm)


347.1 = 236.9 /

Dry weight Loss

(gm) (gm)

347.1 =Dry weight

(gm)

68.3 %

% Moisture

Content

DH

Environmental Quality Laboratory

roject Name: Cust# 4002 LARID 6528

Project # 9578490.01

T- .: .T7J'>' ....• .\/

Dry.Weight{gm) % Moisture·rY""5""~ ..........ii Content

••••.... ...

Station #2 46.9 35.1 33.6

Station #3 260.6 205.1 27.1

Station #4 308.5 222.1 38.9

Station #5 252.8 100.2 152.3

Station #6 296.7 235.7 25.9

Station #7 299.3 236.4 26.6

Station #8 339.9 262.7 29.4

Station #9 480.3 373.2 28.7

Station #10 193.6 147.0 31.7

Station #11 60.2 48.9 23.1

Station #12 33.2 26.5 25.9

Station #13 529.1 423.7 24.9

Station #14 72.7 60.2 20.8

Station #15 299.3 233.3 28.2

Station #16 333.4 258.8 28.8

Station #17 402.5 276.3 45.7

Station #18 443.7 263.2 68.6

Station #19 179.8 140.7 27.8

Station #20 444.1 218.8 103.0

Station #21 584.0 347.1 68.3

DH

Documents

Letter ofTransmittal