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Proceso productivo de calidad - aceite de palma
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INTRODUCTION TO PRODUCTION,
PROCESSING AND QUALITY OF PALM
AND PALM KERNEL PRODUCTS
Chong Chiew Let
Head
Analytical & Quality Development Unit
Product development and Advisory Services Division
Malaysian Palm Oil Board (MPOB)
Kementerian Produk Peladang dan Komoditi (KPPK)
Palm Oil Familiarization Programme
2009 Kuala Lumpur
INTRODUCTION
Oil palm is a tree crop which bears fruit three years after planting
INTRODUCTION (con’t)
Palm oil: from mesocarp of the palm fruit
Palm kernel oil: from kernel inside the fruit
Palm kernel oil is meant for propagation of the specie
Five
major sectors of
Malaysian PO
industry
Plantation sector Milling sector
Refining sector
Oleochemical sectorKernel crushing
sector
Effect of Plantation Practices on the
Quality of CPO
Bunch ripeness
Bruising of fruits during
harvesting
Transportation of ffb to
mill as soon as possible
B) Sterilization
Objectives of bunch sterilization are:-
• Deactivation of enzymes to prevent further rise in FFB
• Facilitate stripping of fruits
• Preparation of fruit mesocarp by coagulating mucilaginous material which facilitates oil cell rupturing
• Reconditioning of nuts to minimise kernel breakages during pressing and nut cracking
Sterilization (cont)
•Horizontal sterilizers are generally used
•FFB is subjected to steam-heat
treatment
•Saturated steam at a pressure of 3
kg/cm2 is used for heating
•3 peak sterilization cycle used
•Sterilizing cycle time: 75 to 90 minutes
C) Stripping
“cooked” FFB are fed into a rotary drum thresher for
separation of fruits from bunch stalk
As drum stripper rotates, bunches are lifted up and then
dropped repeatedly as the bunches travel along the stripper
The fruits are knocked off the bunch by impact action
Detached fruits pass through the bar screen and are collected
underneath by conveyors and discharged into digester
Empty bunches (EFB) are discharged at the end of the
stripper continuously
D) Digestion
Sterilized fruit mesocarp must be
loosened from the nuts in preparation
for mesocarp pressing
Digestion involves mashing of palm
fruits heated conditions
Heating : by steam jacket around
digester or live steam injection
The digester is a vertical cylindrical
vessel fitted with a rotating shaft fitted
with a number of stirring arms
Fruits are mashed and heating will
rupture oil bearing cells
E) Pressing
CPO is extracted by means of a twin screw press
Hot water added to assist oil flow when necessary
CPO slurry is collected in crude oil tank for purification
Press cake is conveyed to a depericarper for separation
The press is operated to press out oil without breaking any nuts
Possible to reduce nut breakages by employing double pressing
which is practiced by a number of palm oil mills in the country
F) Clarification and Purification of CPO
Oil is sent to a vibrating screen of 30-40 mesh to remove fibres and residues
It is then pumped to a continuous horizontal or vertical clarification tank for
oil separation
Temperature of clarification: 90°C to enhance oil separation by density
differences
Clarified oil is centrifuged to remove impurities
Cleaned oil is then vacuum dried and cooled to 45°C before storage
CPO: moisture and dirt content of below 0.2% and 0.025% respectively.
G) Depericarping
Press cake consists of a moist and oily fibres and nuts
mixture
Mixture is conveyed to a depericarper for nut and fibre
separation
Fibre, separated from by winnowing, is sent to boiler
house for boiler fuel
Nuts are sent to a rotating drum where remaining fibre is
removed by attrition before being sent to a nut cracker
H) Kernel Extraction
Nuts are dried and cooled to loosen kernel from shell
before cracking : “conditioning”
Nuts are cracked in a nut cracker by impact
The shell and kernel are separated by winnowing
followed by a clay bath or hydrocyclone
Kernel is then dried in a kernel silo dryer to reduce
moisture to below 7% to prevent mould growth
Palm oil milling process
Steriliser
Loading ramp
Stripping
Digester
Press
Nut/fiber
separationOil/water
separation
Fresh fruit bunches (ffb)
Empty fruit bunches
crude oil storage heating fiber for fertilising
nuts to storage
bruising
Iron
Milling Practices
that can affect
the quality of
CPO:
Quality of Crude Palm Oil
The sale specifications of
crude palm oil within
Malaysia are (MPOA):-
FFA 5.0% max
M & L 0.25% max
DOBI 2.3 min
Quality of Palm Kernel
MEOMA
Dirt & Shell (%) 6% max 10%
rejectable
Moisture (%) 7% max 10%
rejectable
FFA (%) 5% max
(as lauric acid)
PALM KERNEL CRUSHING SECTOR
Extraction Process
Three types of extraction processes are
used:
Mechanical Extraction using high
pressure screw press
Direct solvent exraction
Prepressing followed by solvent
extraction
Mainly mechanical extraction used
Palm Kernel Oil Extraction: Pretreatment
Feed kernels are cleaned using magnetic traps to remove
metal debris
Vibrating screens for sieving out sand, stones/other
undesirable materials
Kernels are than broken into small fragments to facilitate
flaking by roller mill
Roller mill roll kernel into flakes of 0.25 – 0.4mm thick
Kernel flakes are then steam conditioning in stack
steamer to, rupture cell wall
Screw Pressing
Cooked kernel meal is fed into a screw-press
Expelled oil is drained through perforations cage
Oil Clarification
Expelled palm kernel oil is decanted or screened to
remove fines and foot
A filter press is also used in order to produce a clean
oil prior to storage
The cake discharged from the press is conveyed for
storage in a silo
Quality of Crude Palm
Kernel Oil
FFA 5.0% max
M&I 0.5% max
IV 19 max
PALM OIL REFINING
Removal of
odoriferous materials
Reduction of ffa
Reduction of oil colour
Preservation of minor
components
Objectives of refining
palm oil products
REFINING OF PALM OIL
Two type of processes
• chemical (alkali)
• physical refining
Chemical Refining
Chemical Refining consists of degumming,
neutralising, bleaching and deodorising
High operating costs and high refining losses,
problems of pollution due to soapstocks
ALKALI REFINING
DEGUMMING
NEUTRALISATION
PRETREATMENT
BLEACHING
DEODORIZATION
DEGUMMING
DEACIDIFICATION/
DEODORIZATION
PHYSICAL
REFINING
NBD RBD
PRETREATMENT
BLEACHING
Malaysia:Mainly physical refining
Physical Refining
Physical refining process involves only
degumming, bleaching and deodorisation
In the deodoriser, stripping steam is used
to deacidify the oil under vacuum
Refining losses and costs are much lower
Physical refining is most widely used in
Malaysian palm oil refining industry
PRETREATMENT: DEGUMMING and BLEACHING
DEGUMMING
Phosphoric acid is added to degum the oil
Conditions phospholipids and trace metals prior
to earth bleaching
BLEACHING
Bleaching : non-activated clay, activated carbon
and silica are generally used
Acid activated bleaching earth is sometimes used
Pretreatment bleaching……
The most important property is the
catalytic decomposition of the
hydroperoxides in the oil
The primary function of the bleaching
earths during pretreatment is the
removal of peroxides and secondary
oxidation products
The secondary function is to clean up
traces of soap, phosphatides, trace
metals and pigments in the oil
PRETREATMENT BLEACHING
DEGUMMING
VACUUM BLEACHING
FILTRATION
SECURITY FILTRATION
PHOSPHORIC ACID
BLEACHING EARTH
CRUDE PALM OIL
DEG BL PO
Vertical Leaf Filter
DEODORISATION
The last step in the refining process is deodorisation
Oil is heated to 260°C under vacuum to remove undesired
odours in chemical refining
For physical refining, main aim is removal of FFA with
injected steam
Deodorization removes:
free fatty acids carotenoids break down
ketones & aldehydes other volatiles
pesticides & other HC volatile oxidation products
PORAM Standard Specifications
For NBD/RBD Palm Oil
FFA (as palmitic) 0.1% max
M&I 0.1% max
IV (Wijs) 50-55
MP/oC 33-39
(AOCS Cc3-25)
Colour (51/4”cell) 3 or 6 Red max
NBD/RBD Palm Kernel Oil
Specifications For Export
FFA (as lauric) 0.1% max
M&I 0.1% max
IV (wijs) 19 max (shipment time)
Colour (51/4”cell) Red 1.5 max
FRACTIONATION
Three fractionation methods used:
Crystallisation of PO; separation by filtration (Dry
Fractionation)
Crystallisation of PO in solvent; filtration (Solvent
Fractionation)
Partial Crystallisation of PO and mixing with surface
active agent (sodium lauryl sulphate) ; centrifuging
(Detergent Fractionation)
Liquid fraction: olein Solid fraction: stearin
Liquid fraction: refractionated to yield superolein and
PMF
Fractionation principle
Slurry
Molten
fat
Olein Stearin
solid/liquid separation
crystallisation
8
Membrane filter press Courtesy of
Some Value-added Down Stream Products of A
Refinery
• Palm Mid-Fraction for Cocoa Butter Equivalent
(CBE)
• Cocoa Butter Substitute (from Palm Kernel Oil)
• Cocoa Butter Extender (from hydrogenated
superolein)
• Fully hydrogenated products
• Interesterified products
PORAM Specifications of Palm
Olein and Stearin
RBD/NBD RBD/NBD
Palm Olein Palm Stearin
FFA (as palmitic) 0.1% max 0.1% max
M&I 0.1% max 0.1% max
IV 56 min 48 max
MP 24 max 44 min
Colour 3 or 6 Red 3 Red
Thank you