Upload
piurajak7775
View
220
Download
0
Embed Size (px)
Citation preview
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 1/14
layer 7.7
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: Yes
Vary Energy Resolution : Yes
---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---
Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 2/14
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 9.499 40.203Co-L 0.000 100.000Pt-L 214.518 64.619
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 121.762 eV @ 5.9 keVCalibration: 4.94834 eV/ch, 2695.95 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------
Co(K) 1.17 3.80 1.00 0.99 1.495Pt(L) 98.82 96.19 6.01 0.75 5.547
layer 7.9
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetection
Max Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 3/14
Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoil
Specimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 4.357 40.271Co-L 0.000 100.000Pt-L 87.357 49.039
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 132.888 eV @ 5.9 keVCalibration: 5.03552 eV/ch, 3471.00 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 1.32 4.26 2.43 0.99 1.495Pt(L) 98.67 95.73 11.00 0.75 5.547
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 4/14
layer 7.5
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---
Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 deg
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 5/14
Speciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 120.966 72.599Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 131.668 eV @ 5.9 keVCalibration: 4.93147 eV/ch, 3340.91 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 12.17 0.75 5.547
layer 7.4
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetection
Max Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 6/14
Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoil
Specimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 51.636 54.171Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 129.138 eV @ 5.9 keVCalibration: 4.83420 eV/ch, 3954.68 eV at channel 0
Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 7/14
Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 21.70 0.75 5.547
layer 7.3
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3
Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : Yes
Vary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mm
Detector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 8/14
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 133.196 76.119Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 203.033 eV @ 5.9 keVCalibration: 4.85911 eV/ch, 2945.56 eV at channel 0Accelerating voltage: 200 kV
Alpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 11.76 0.75 5.547
layer 7.2
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 9/14
Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 deg
Detector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 deg
Specimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 64.853 61.241
Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 181.654 eV @ 5.9 keVCalibration: 4.91345 eV/ch, 3103.83 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 10/14
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 19.21 0.75 5.547
layer 7
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : Polynomial
Background Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---Quantification Mode : Mixed
Normalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eV
Reference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoil
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 11/14
Specimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 67.906 57.425Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keV
Measured FWHM = 156.100 eV @ 5.9 keVCalibration: 4.79664 eV/ch, 3407.93 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495
Pt(L) 100.00 100.00 17.63 0.75 5.547
layer 7.10
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: Normal
Background Correction Enabled
---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 12/14
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mm
Detector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nA
Speciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000
Pt-K 0.000 100.000Pt-L 73.469 61.672Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 131.771 eV @ 5.9 keVCalibration: 4.94143 eV/ch, 2724.49 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 13/14
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 16.98 0.75 5.547
layer 1.5
***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***
***Analysis Setup***
Analysis Setup Name: NormalBackground Correction Enabled
---Background Settings---Correction Mode : Modeled
Background Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6
---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes
---Quantification Settings---
Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes
***Experimental Conditions***
Experimental Conditions Setup Name: Default
---Detector Conditions---
Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577
---Specimen Conditions---
8/13/2019 Layer 1
http://slidepdf.com/reader/full/layer-1 14/14
Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3
---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm
***Peak Fitting Results***
IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 118.910 67.082Pt-M 0.000 100.000
Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 159.557 eV @ 5.9 keVCalibration: 4.93848 eV/ch, 2883.40 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees
***Quantification Results***
Correction method: None DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------
Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 11.42 0.75 5.547