14
layer 7.7 ***Spectrum does not have embedded Experimental Conditions - Values from current ly selected Conditions used*** ***Analysis Setup*** Analysis Setup Name: Normal Background Correction Enabled ---Background Settings--- Correction Mode : Modeled Background Model Name : Polynomial Background Selection : Elements Background Identification : PeakDetection Max Polynomial Order : 3 Minimum Auto-ROI Width : 100 eV Threshold Peak/BG : 6 ---Peak Fitting Settings--- Peak Fitting Mode : Standardless Vary Energy Calibration: Yes Vary Energy Resolution : Yes ---Quantification Settings--- Quantification Mode : Mixed Normalization : 100 wt% Correction Mode : NoCorrection Vary Accelerating Voltage : Yes Vary K-Factor Type : Yes Vary Reference Atomic Number: Yes ***Experimental Conditions*** Experimental Conditions Setup Name: Default ---Detector Conditions--- Energy Resolution : 134 eV Reference Energy : 5.9 keV Minimum Energy : 100 eV Detector Thickness: 3 mm Detector Distance : 11.8 mm Detector Angle : 14.6 deg Detector Azimuth : 0 deg Layer Definition : Ed ax from S/N 9577 ---Specimen Conditions--- Specimen Type : ThinFoil Specimen Thickness: 0 nm Specimen Density : 0 g/cm3 ---Microscope Conditions--- Accelerating Voltage: 200 keV Beam Current : 1 nA Speciment Tilt 1 : 0 deg Speciment Tilt 2 : 0 deg Specimen Height : 0 mm

Layer 1

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layer 7.7

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: Yes

Vary Energy Resolution : Yes

---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---

Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

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***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 9.499 40.203Co-L 0.000 100.000Pt-L 214.518 64.619

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 121.762 eV @ 5.9 keVCalibration: 4.94834 eV/ch, 2695.95 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------

Co(K) 1.17 3.80 1.00 0.99 1.495Pt(L) 98.82 96.19 6.01 0.75 5.547

layer 7.9

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetection

Max Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---

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Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoil

Specimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 4.357 40.271Co-L 0.000 100.000Pt-L 87.357 49.039

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 132.888 eV @ 5.9 keVCalibration: 5.03552 eV/ch, 3471.00 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 1.32 4.26 2.43 0.99 1.495Pt(L) 98.67 95.73 11.00 0.75 5.547

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layer 7.5

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---

Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 deg

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Speciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 120.966 72.599Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 131.668 eV @ 5.9 keVCalibration: 4.93147 eV/ch, 3340.91 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 12.17 0.75 5.547

layer 7.4

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetection

Max Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---

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Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoil

Specimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 51.636 54.171Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 129.138 eV @ 5.9 keVCalibration: 4.83420 eV/ch, 3954.68 eV at channel 0

Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------

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Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 21.70 0.75 5.547

layer 7.3

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3

Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : Yes

Vary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mm

Detector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3

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---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 133.196 76.119Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 203.033 eV @ 5.9 keVCalibration: 4.85911 eV/ch, 2945.56 eV at channel 0Accelerating voltage: 200 kV

Alpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 11.76 0.75 5.547

layer 7.2

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---

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Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 deg

Detector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 deg

Specimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 64.853 61.241

Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 181.654 eV @ 5.9 keVCalibration: 4.91345 eV/ch, 3103.83 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

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Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 19.21 0.75 5.547

layer 7

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : Polynomial

Background Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---Quantification Mode : Mixed

Normalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eV

Reference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoil

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Specimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 67.906 57.425Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keV

Measured FWHM = 156.100 eV @ 5.9 keVCalibration: 4.79664 eV/ch, 3407.93 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495

Pt(L) 100.00 100.00 17.63 0.75 5.547

layer 7.10

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: Normal

Background Correction Enabled

---Background Settings---Correction Mode : ModeledBackground Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

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---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mm

Detector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nA

Speciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000

Pt-K 0.000 100.000Pt-L 73.469 61.672Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 131.771 eV @ 5.9 keVCalibration: 4.94143 eV/ch, 2724.49 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

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***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 16.98 0.75 5.547

layer 1.5

***Spectrum does not have embedded Experimental Conditions - Values from currently selected Conditions used***

***Analysis Setup***

Analysis Setup Name: NormalBackground Correction Enabled

---Background Settings---Correction Mode : Modeled

Background Model Name : PolynomialBackground Selection : ElementsBackground Identification : PeakDetectionMax Polynomial Order : 3Minimum Auto-ROI Width : 100 eVThreshold Peak/BG : 6

---Peak Fitting Settings---Peak Fitting Mode : StandardlessVary Energy Calibration: YesVary Energy Resolution : Yes

---Quantification Settings---

Quantification Mode : MixedNormalization : 100 wt%Correction Mode : NoCorrectionVary Accelerating Voltage : YesVary K-Factor Type : YesVary Reference Atomic Number: Yes

***Experimental Conditions***

Experimental Conditions Setup Name: Default

---Detector Conditions---

Energy Resolution : 134 eVReference Energy : 5.9 keVMinimum Energy : 100 eVDetector Thickness: 3 mmDetector Distance : 11.8 mmDetector Angle : 14.6 degDetector Azimuth : 0 degLayer Definition : Edax from S/N 9577

---Specimen Conditions---

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Specimen Type : ThinFoilSpecimen Thickness: 0 nmSpecimen Density : 0 g/cm3

---Microscope Conditions---Accelerating Voltage: 200 keVBeam Current : 1 nASpeciment Tilt 1 : 0 degSpeciment Tilt 2 : 0 degSpecimen Height : 0 mm

***Peak Fitting Results***

  IntegratedPeak Intensity Uncertainty---- ---------- -----------Co-K 0.000 100.000Co-L 0.000 100.000Co-M 0.000 100.000Pt-K 0.000 100.000Pt-L 118.910 67.082Pt-M 0.000 100.000

Input FWHM = 134 eV @ 5.9 keVMeasured FWHM = 159.557 eV @ 5.9 keVCalibration: 4.93848 eV/ch, 2883.40 eV at channel 0Accelerating voltage: 200 kVAlpha tilt: 0 degrees 

***Quantification Results***

Correction method: None  DetectorElement Weight % Atomic % Uncert. % Correction k-Factor------- -------- -------- --------- ---------- --------

Co(K) 0.00 0.00 100.00 0.99 1.495Pt(L) 100.00 100.00 11.42 0.75 5.547