JOHN.E^AYRES^^ 'JOSEPH D. GUERTIN; JR. GOLDBERG •ZOINO ... · Silresim Site Trustees -March 10, 1986 File No. A-4054.04 Page 2 and sampler blanks. It is noted that both of these

V iniraquo mmjjouTntnmdashw

gt rDONALD -TVGOLDL WILUAM S ZOINO

bullJOSEPH D GUERTIN JRpound shy JOHNEÂYRES^^ MATTHEW JBARVENIKr-

WILUAM R BELOFFNICHOLAS A CAMPAGNA JR

GOLDBERG bullZOINO amp ASSOCIATES INC MATHEW A DIPILATO LAWRENCE FELDMAN

GEOTECHNICAL-GEOHYDRDLOGICAL CONSULTANTS JOSEPH P HEHIR ROBERT A-HELLER ROSS T McGILUVRAY MICHAEL A POWERS JAMES H REYNOLDS PAUL M SANBORN RICHARD M SIMON STEVEN J TRETTEL

CONSULTANTS WALTER E JAWORSKI STANLEY M BEMBEN

March 10 1986 File No A405404-CPC

Silresim Site Trustees Post Office Box 169 Acton Massachusetts 01720

Attention Mr James Rogers

Re Analytical Data Sampling Round

- Initial

Gentlemen

Attached please find a copy of the laboratory report from the initial round of groundwater samples at the Silresim site The samples were collected on December 4 1985 from the existing monitoring wells at the site installed by Perkins Jordan Inc in 1981 and 1982 A list of samples submitted for laboratory analysis including QAQC samples is attached asTable 1

I t i s n o t e d t h a t p e s t i c i d e s P C B s a n d 2 3 7 8 Tetrachlorodibenzo-p-dioxin (TCDD) wernot detected in any samples analyzed With only a few exceptions priority pollutant metals were not found in significant concentrations in the groundwater samples Low levels (8-170 ug1) of acid extractable organic compounds were found in two of the five monitoring wells tested Base neutral extractables were found at trace levels in most samples with elevated concentrations (up to 1900 ug1) in two monitoring wells

Results of volatile organic compound (VOC) analyses are generally consistant with previous data from the site Elevated levels of VOCs were found at wells MW-102B and MW-101A locations that

previously showed high concentrations MW-105A exhibited VOC concentrations substantially higher than any previously reported levels at that location VOC concentrations at wells MW-102A and MW-105B were similar to past data from these locations

T r a c e l e v e l s o f m e t h y l e n e c h l o r i d e w e r e f o u n d i n l a b o r a t o r y f i e l d s a m p l e r a n d t r i p b l a n k s a n d a d d i t i o n a l V O C s (chloroform 111 trichloroethane acetone and 2-butanone) were f o u n d a t c o n c e n t r a t i o n s r a n g i n g f r o m 3 t o 1 3 u g 1 i n t h e f i e l d

THE GEO BUILDING 320NEEDHAM STREETbull NEWTON UPPER FALLSMASSACHUSETTS 02164 (617) 969-0050 BUFFALONYbullBRIDGEPORTCTbullVERNONCTbull MANCHESTERNHbullPROVIDENCE RlbullTAMPAFL

AN EQUAL OPPORTUNITY EMPLOYER

Silresim Site Trustees - March 10 1986 File No A-405404 Page 2

and sampler blanks It is noted that both of these blanks were generated during sampling of MW-102B a location exhibiting eleyated levels of the same VOCs observed in the blanks this is believed to represent a worst case scenario with respect to potential sample cross contaminationby VOCs The contaminants found in the laboratory and trip blanks were notated within Westons Laboratory report additional VOCs found in field and sampler blanks will be similarly qualified in data entered into GZAs Data Base Management System

As noted in Westonscover letter sample aliquots for the baseneutral extractable pesticidePCB and TCDD fractions of well MW-105B were spiked with the standard spike mixture used by EPAs Contract Laboratory program - An unspiked aliquot of the sample was not analyzed however due to miscommunication between GZA and the laboratory Well MW-105B will therefore be resampled during the next scheduled groundwater sampling round and analyzed for the appropriate parameters

S h o u l d y o u h a v e a n y q u e s t i o n s o n t h e d a t a o r r e q u i r e a n y additional information please feel free to call

Very truly yours

GOLDBERG-ZOINO amp ASSOCIATES INC

2 Lawrence Feldmen

LFevm

GZ

1 Silresim Site Trustees - March 10 1986 - File No A-405404

Page 3

TABLE 1

SAMPLE INVENTORY (DECEMBER 4 1985)

GZA Sample ID No (Weston Sample Description)

StationSampleDescription

SCC-GWS-B-105A Well MW-105A

SCC-GWS-B-105B Well MW-105B



SCC-GWS-B-001A Well MW-102A (Blind Duplicate)

SCC-QAC-SB-001 Sampler Blank (Bailer)

SCC-QAC-FB-001 Filtration SystemBlank

SCC-QACmdashTB-001 Field Blank


GZ

28 February 1986

Mr Charles Lindberg Goldberg Zoina and Assoc The GEO Building 320 Needham Street Newton Upper Falls MA 02164

Dear Mr Lindberg

Please note the following items regarding our data reports of January 27 (metals VOAs and BNAs) and January 28 (TCDD)

1 The reported target compounds for VOA and BNA analyses were priority pollutants Since HSLs are needed we searched the original data for the additional analytes and have attached revised reports (Attachment I)

2 The EPA data qualifier B for target analytes detected in the laboratory blank has been added to the report forms where appropriate It is noted that the only targets present in the laboratory blanks were methylene chloride in the VOA blank and bisshy(2-ethylhexyl)phthalate in the BNA blank The blank levels of both these analytes was below the CLP Conshy tract Required Detection Limit

3 Attachment II is a revised TCDD data report on which the surrogate recoveries have been corrected to reflect the observed inconsistency between levels in the calibration standard received from the EPA and the surrogate spiking solution made up in our laborashy tory from neat compounds Also attached is a copy of the laboratory work sheet on which relevant calcushy lations were made and the mass chromatograms

4 Attachment III is the TCDD data report form for the re-extracted samples B-101A and B-102B Re-extracshytion and analyses were performed because of the very high recoveries obtained from the original analysis of these samples More reasonable recoveries were obtained in the re-analysis

5 BNA and TCDD fractions for sample B-105B were spiked with the CLP BNA matrix spike mix and 2378 TCDD respectively Unspiked sample was not analyzed for these parameters due to a miscommunication between GZA and WESTON Laboratory

6 Zinc was found in the method blank at a concentration of 0030 mgL This concentration is consistent with previous determinations of zinc in the laboratory water Certified ultra-pure reagents are used for digestion so that the reagents should not be a source of contamination A method blank is prepared by using an aliquot of laboratory water equivalent to the quantity of sample that is used in the analyses Any contamination in the laboratory water would then be observed on analysis of the method blank However when processing samples minimal amounts of laboratory water are used and any contributions from contaminatedlaboratory water should be much less than 10 of the concentration Consequently contrishy butions from laboratory water should be less than 0003 mgL and concentrations of zinc determined in the samples should be representative of the actual concentrations in the samples

7 Both the computer data base and the original notebook entries have been reviewed for accurate transcription of data for the manganese results The notebook and data base agree Sample 8512-327mdash0030(SCCmdashGWS-B-102A) was diluted by a factor of 10 at the instrument in order for the response to fall within the calibrated range of the instrument Sample 8512-327-0050(SCCshyGWSmdashB-001A) was diluted by a factor of 100 The result obtained for sample 0050 can be verified since this sample was also replicated and spiked The results for the replicate and spike are comparable to the initial result (the spike level was significantly less than the concentration in the sample)

If you have any questions please call me at (215) 524-0180

Very Truly Yours

ROY F WESTON INC

V1

Carter P Nulton PhD Organics Section Manager WESTON Analytical Laboratories

CPNrost

A

RFWSN

8512-327-0010 -0020 -0030 -0040

- -0050 -0050 Dup-0060 -0070 -0090

-0050

Date of Report January 28 1986

GOLDBERG ZOINO AND ASSOCIATES SUMMARY REPORT

FOR SAMPLES RECEIVED DECEMBER 5 1985

Concentration (mgL)

SAMPLE DESCRIPTION A1 Be Ba Ca Sr

SCC-GWS-B-105A lt 0 0 2 SCC-GWS-B-105B lt 0 0 2 SCC-GWS-B-102A lt 0 0 2

lt 0 0 2 lt01 743 1SCC-GWS-B-102B lt05 145 SCC-GWS-B-001A lt 0 0 2 Laboratory Duplicate lt 0 0 2 SCC-QAC-SB-001 lt 0 0 2 SCC-QAC-FB-001 lt 0 0 2 SCC-GWS-B-101A lt 0 0 2 Laboratory Blank lt05 lt 0 0 2 lt01 lt0005 lt005 Blank Spike mdash 100

Rec

Blank Spike Dup mdash 100 Rec

Matrix Spike 100 Rec

Earl M Hansen PhD Manager r

WESTON Analytical Laboratories

D A T S T U n - O r A y T I T N T GO D y E R O - v P [ A O a A A A O r - T f E A D A T A A bull bull y K i P P A K P F M T A A A T L A T A U [ T ) P E - p A T A A A A T F R 0 0 P 0 P - A V

) A1E A A A R A A 0I bull A A TEDiA -bull A - A A A |v| p ( [)| f f y n p y [ iM APATJ A

0 0 i A GP GA F P h g HGL iG7 AG i G G 1 A G L

E F U S N G E 3 C R 1 P T r U N

A A i 2-3 A )0 P 0 S0 A-G A A B bull- P 0A A ( bdquo 0 P 0 bdquo 06 I P A 0 A P -A) 10 A bdquo C P 76 j02XP AIAAGUIH mdashLi POAL OOAO S C C -G3U-B -bull 102A

i A A1 Pbdquo0pO

bull UO P bdquo 0 P 0

y [M-AP bdquoOOA

y y )P p OPO lt0 bdquo 02

P A 4 0A6

00 40 () ( ) A ()

OAP

A A f AUA -B- P 0A la A A C G 11 A-B bullbullbullbull 0 0 -i A

A T IPIx Ap 11ltE

lt bdquo 0 P 0 lt bdquo 0 i 0

069

lt bdquo 0 P ( ) lt bdquo 0 P 0

0 A 4

lt 0 0 A lt 0 0 5 0 0 6

- 0 1A P bdquo 0 P 0

bdquo 2i0

P 0 bdquo 02 lt () n gt)2

bdquo P49

7 AO 067 bdquo P A R

OAK SPIKE REGQUERY PSAX A3 bdquo AX -120 P0S7 74 5 9 P bdquo 0 0 0 A IP 005 A

R IPPL IC A I IP PR IPCISIGN

lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC

bdquo 060 - P bdquo OPA

0() 4 () pC C bullbullbullbull A C-bull AB -OOP p bdquo 0 P 0 lt 0 P 0 lt 0 05 P bdquo 0 P 0 bdquo 032 bdquo 0 47 ( )070 () ( ) 9 ()

A CC- Q A CFB ()( ) - j A A A G W A B- P 0 P A

I1 IP TL ILiD B ANK

lt bdquo ( ) p ( ) lt bdquo 0 P 0 lt bdquo 0 P 0

lt 0 p 0 bdquo 0 2 4

lt 0i0

lt bdquo 0 0 A lt bdquo ( ) ( ) A lt bdquo 0 0 A

lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2

bdquo P24 Pi5bdquo 0

lt bdquo0 0 IT IP lL IOD SPIKE 063 023 bdquo 00A 304 bdquo P A3 4 4 4

Ap L K IP RIPCOOIPIPY P26 PPB 4 4 4 P027 7 6 0 P P4 NETHOP Bp TRIP

Ap IGF kFCOOFRY 066 P33

020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P

K PIN NA HI PB AlP SIP PIG7L PiGL tPGL PIG 71 PiGL PIGAL PIGL

R F W S N DIPS ORIP TIUN

P 2 -bull - bull 00 P 0 -0020 -0030 bullbullbullbull0040 - O O A O

ACC-GIJS-H- TOAA AAC-GUS-B --10AP ACC-GAl j -P- p 02A SCC--GUS-B - P 02B ACC-GUA-F-GOPA

4 bdquo A 9 bdquo 2 P9 bdquo P90 P 2 bdquo 3 P bdquo 3 P

lt bdquo P 0 lt bdquo P 0 lt bdquo PC bull P6(lt bdquo - i 0

lt bdquo 00 A P bdquo 005 lt ( oA lt bdquo00b lt bdquo 00 A

lt bdquo 060 lt 060 lt bdquo 060 lt bdquo 060 ( bdquo 0 6()

lt 00A lt 005 lt bdquo O f ) A

lt00A lt 00A

-00 AG -7) OAK

PI AIRIX ART KIP AP TKIP RECGUERY

430V7 c7

bdquo 0 P (J bdquo P P 3 P P2

bdquo 009 9 P bdquo 0

-00A Pi A TRIX AP TKE P bdquo 46 -00Al APIKIP RECGUERY AO ( ) -00AR -00AS

REPLICATE P R E C I A T O N

P bdquo 06 2 -i bdquo 4 OP

lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090

A C C -bull0 A A -PiR -00 P A G0-0 A 0bull-FB-00 P ACC--GU0-B- PC PA

NET LIOA B LANLP PIETHOD APIKiP

lt bdquo 0 P A lt 0 P A

P 0 bdquo 4 lt 0 P 5

bdquo 4 4 4

lt bdquo P 0 lt P 0 PAO lt bdquo PO bdquo 4 10

lt 005 lt bdquo 005 lt 005

lt 060 lt bdquo06()lt bdquo06()lt bdquo 060

bdquo P 07

lt 00b P bdquo 005 P bdquo 005 P 005

() (bull V ApIKE RECnUEKY P P4 P 03 P 077 9 9 o 0

PIETHOD SPIKE SPIKE REOOUERY

PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57

bdquo 0 P P P P 27 bdquo 0 P 0

SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w

- G L B p - bull i bull p bull v 0 0 i pi i-i A0-10 0 0 1 i - 1 bull i 0 0 A 010 0040 BL bull B O B - 10PR o - i 0 J 4

0SO SC C mdash0ws r -00 -1A bdquo 0 10 0 1 4 00BK mathrx P I jltL bdquo 08 B OA A

0 0 SK SPIKE REi O V E R Y bull03 00BR BlNN lt0 ATE A 0 -10 01 1 00 preoi [ON NC (4 ( i ( ) 00 bcc-oac Fi bull bull bull bull ( ) 0 -1 ( ) --i ( ) 0-14 00 O1 SOO-QAC-FB- 0(1 bdquo010 bdquo 0 1 i 004 n igt L-i- mdash ii gt0 iR 10 1 0 bdquo o -i 0 03B

lT ETHui ) BLANK S 010 bdquo030 M E T H O D S P I K E bdquo040 bdquo O A O

SPIKE RECOVERY j0 4 170 METHOD BPTKF bdquo 037

B P T K F R E C O V E R Y AS 4 A

R F U B M DEBARIPITON AY ANIDE-A CYANTOE TOTAL

-12-32 -bull0010 SCC--0UB-R - i OSA A O i NGL -0020 BCC---GUB-B 10SB A 0 4 NGL mdash 0 0 30 BCC--GBU-B--102 A A 01 NGL bull bull bull bull ( )( ) ( ) SCC mdash pjUH -bull 4Ovgt 0 10 G 020 NG mdash 0 0 S0 BCC-GWB-B--OA LA A 01 iii

OAO BCC-OAC--BR mdash 00 4 A 01 NGL 0 9 0 BC C - GUB-B-10 1A o i NG l

RFUBN D E B C R T P T I UN TOTAL ORGANIC CARBON TOTAL ORGAN10 HALOGEN

gt C j yy7 mdash 00 4() SCC--GLIBR -bull 102B 1140 HGL 1BOO I jG l - bull 0 0 4B REPLICATE 18000 UGL -004B PEEGIBION bull 3 03

NETHOG BLANK ltbdquoS NGL NETHOS BP IKE 4bdquo92 NGL

Bp IKE RFC00FRY 9 bdquo 9 NETHOD Bp IKE 4 -B2 NGL

9 bull v bullbullbull8PIKE RFC GOER Y

RFUBN DESCRIPTION 8ULFIDE

8B 12-327-0040 3C C -GLiB bullbullbullbull B- 102B 3 A 0 NG - ( )04K BCC--GUB-B- 102B B4 4 NGL - -004K SPIKE REG GOER Y 402 -004R 8C C-GUB-bullB -102B 3 bdquo A 0 NG -0048 PRECIBION 11 A

PREPARED BY S A P- R0 0 ED STEPHANIE DORRS EARL Mbdquo HANSEN PHbdquoD DATA NANACER NANAi- iER 0EBTON ANALYTICAL LABORATORIES wESTON ANALYTICAL LABORATOR IE

DATE OF REPORT December 13 1985

RFW NO 8512-337 5AMPLE DESCRIPTION DATE COLLECTED DATE EXTRACT Lb DATE ANALVZED PARAMETER vgL Alpha-BHC Beta-BHC Delta-BHC Gamma-BHC(L i ndane) Heptachlor A l d r i n Heptachlor Epoxide Endosulfan I D i e l d r i n 44-DDE Endr in Endosu1fan TT 44-DDD Endrin Aldehyde E n d o s u l f a n S u l f a t e 44-DDT Methoxychlor E n d r i n K e t o n e Chiordane ToxapheneAroclor-1016 Aroc1 or-1221 Aroc 1 or-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260

Dilut ion Factor NS = Not Spiked

ROY F WESTON ORGANIC ANALYSIS DATA SUMMARY

FOR GZA

WATER-PESTICIDEPCB SUMMARY REPORT

WO NO 0010-10-09

PET 1 TMTTS ML ffOPO 0030 0040 B105A B102A B102B 12485 12485 12485 12485 12685 12685 12685 121185 121185 121185 121185

ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0

100 100 10 100 ND = Not Detected lt detection limit

0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By

Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies


ROY F WESTON

ORGANIC ANALYSIS DATA SUMMARY

FOR GZA


WO NO 0010-10-09

NS = Not Sp iked ND = Not Detec ted lt de tec t ion l im i t


ATTACHMENT I


VOLATILE HAZARDOUS SUBSTANCE L IST COMPOUNDS

1217W002219GCMS FILE NAME CLIENT

SCC-GWS-B-IQ5A MATRIX WATER

GZA

SAMPLE DESC CLP (CIRCLE ONEMETHOD (LOU MED LEVEL8512-327-0010

DILUTION FACTOR 500 RFYI =

DATE COLLECTED DECEMBER A 1985

PH NA MOISTURE NA DATE ANALYZED DECEMBER 18 1985

WORK ORDER it

UQKQ CASCAS (Circle One)(Circle One] NumberNumber 78-87-5 1 2-Dichkgtropropane 5000 U5000 U74-87-3 Chloromelhane 10061-02- 6 Trana-1 3-Dichloropropene 5000 U5000 U 79-01-6 Trichloroethene 1700 J74-83-9 Bromomethane

75-01 Vinyl Chloride 5000 U 124-48-1 Dibromochloromethane 5000 U

75-00-3 Chloroethane 5000 U 79-00-5 11 2-Trichloroethane 5000 U

75-09-2 Methylene Chloride 18000 910071-43-2 Benzenegt50000067-6-1 Acetone

10061-01-5 Ci-1 3-Dtchloropropene 5000 U5000 U75-15-0 Carton DiauHide 110-75-8 2-Chloroethylvinylether 5000 U

75-35-4 1 1 -Oichloroethene 5000 U 75-25-2 Bromolorm 5000 U 600 J75-34-3 1 1 -Oichloroethene 591-78-6 4-Methyl-2-Pentanone 5000 U 1800 J156-60-5 Trans-1 2-Oichloroethene 106-10-1 2-Hexanone 5000 U

67-66-3 Chloroform 6000 U 127-18-4 Tetrachtoroethene 800 J

107-06-2 1 2-Dtchloroethane 7600 79-34-5 112 2-Tetrachloroethane 5000 U

78-93-3 2-Botanone 7900 5000 U 106-88-3 Toluene 1700 J 11 1-Trichloroethane

106-90-7 Chlorobenzene 920 J71-55-6 5000 UOrton TetrachiorOe 3000 U 100-41 -4 Ethylbenzene 2900 J56-23-5

106-05-4 Vinyl Acetate 5000 u 100-42-5 Styrene 5000 u75-27-4 Bromodichloromethane

Total Xylenes 5000 I

SURROGATE RECOVERY

1 1-DICH10R0ETHANE du 106

TOLUENE d8 109

p-BROMOFLUOROBENZENE 1 1 5

Data report ing quali f iers

U - NOT DETECTED COMMENT NR - NOT REQUESTED

J - PRESENT AT LESS THAN DETECTION LIMIT

B - ANALYTE PRESENT IN BLANK

2-2-^ APPROVED BY u lt mdash âr1 Hansenraquo

Manager WESTON Analy t ica l Laborator ies

ROY F WtSlOH ORGANIC ANALYSIS DATA SUMMARY

VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS

CLIENT ZA GCMS FILE NAME 1217W0Q2220

SAMPLE DESC SCC-GWS-B-l05B MATRIX Water

RFW = 8512-327-0020 METHOD flgu) MED LEVEL CLP (C i rc le Or

DATE

DATE

rOLLECTEDDecember 4 1985

ANALYZED December 11 1985

DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull

CAS f V19Ip lugKgCAS Number fCircto One)Number ^TCircto One]

74-87-3 Chloromethane 10 U 78-87-5 1 2-Dichkgtropropane 8 J

74-83-9 Bromomethane 10 u 10061-02-6 Trans-1 3-Dichloropropene 10 U

79-01-6 Trichloroethene 32 75-01shy Vinyl Chloride 8 J

124-48-1 Dibrornochloromethane 10 U 75-00-3 Chloroethane 10 U

75-09-2 Methylene Chloride 6 JB 79-00-5 11 2-Trichloroethane

67-64-1 Acetone 6 J 71-43-2 Benzene H

75-15-0 Carbon Disulfide 10 U 10061-01-5 cis-1 3-Dichloroprooene 10 U 110-75-8 2-Chloroethylyinylether 10 U

75-35-4 1 1-Qichloroethene 10 I I 75-25-2 Bromoform 10 U

75-34-3 1 1-Dichloroethane 210 591-78-6 4-Methyl-2-Pentanone 10 U

156-60-5 Trans-1 2-Dichloroethene JO 67-66-3 Chloroform 1 J 106-10-1 2-Hexanone 10 U

127-18-4 Tetrachloroethene 9 J 107-06-2 1 2-Dichkgtroethane

79-34-5 11 2 2-Tetrachloroethane 10 U78-93-3 2-Butanooe 10 u

106-88-3 Toluene 2 J71-55-6 11 1-Trichloroethane 1 5

56-23-5 Carbon TetrachloriOe in u 106-90-7 Chlorobenzene 20

106-06-4 Vinyl Acetate 10 U 100-41-4 Ethytbenzene 10 U

75-27-4 Bromodichloromethane 10 U 100-42-5 Styrene 10 U Total Xylene 17

SURROGATE RECOVERY

1 1 -DI CHLOROETHANE du HO TOLUENE dg 100 p-BROMOFLUOROBENZENE 108

Data repor t ing qua l i f ie rs

U - NOT DETECTED COMMENT

NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT


DATE February 28 1986 APPROVED BY

Ear l M Hansen PhD P- Manager

WESTON Analy t ica l Laborator ies

ROY F Wt i lUN ORGANIC ANALYSIS DATA SUMMARY


CLIENT GZA GCMS F ILE NAME 1217W00221 8

SAMPLE DESC SCC-GWS-B-102A MATRIX Water

RFV bull 8512-327-0030 METHODi bull MED LEVEL CLP (C i rc le One

DATE COLLECTED December 4 1985 DILUTION FACTOR 1

DATE ANALYZED Dprpmbpr 18 1 985 PH NA MOISTURE NA

WORK ORDER

CAS 9 Ldr wgXgCAS Number Circle One)Numbtr

7B-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 IT 10061-02-6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomethane

10 u 79-01-6 Trichloroethene 6 J 75-01bull Vinyl Chloride

124-46-1 Dibromochloromethane 10 U10 u76-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 1 J

75-09-2 Methylene Chloride 9 JB 9 J71-43-2 Benzene

67-84-1 Acetone XL 10061-01-5 ci-1 3-Dtchloropropene 10 U

75-15-0 Carbon Disulfide 10 u 110-75-8 2-Chloroethylvinylether 10 U10 u1 1 -Oichloroethene 75-25-2 Bromoform 10 U

75-35-4 75-34-3 1 1-Dichloroethane 10 u

591-78-6 4-Methyt-2-Pentanohe 10 U 156-60-5 Trans-1 2-Oichloroethene 10 u

106-10-1 2-Hexanone 10 U 67-66-3 Chloroform 10 u

127-18-4 Tetrachloroethene 3 J107-06-2 1 2-Dichloroethane 10 u

79-34-5 11 2 2-Tetrachloroethane 10 U7 J78-93-3 2-Butanone 108-88-3 Toluene 6 J

71-55-6 11 1-Trichloroethane 10 U 108-90-7 Chlorobenzene A JCarbon Tetrachloride 10 U 100-41-4 Ethylbenzene 2 J

56-23-5 10 U108-06-4 Vinyl Acetate

100-42-5 Styrene 10 U 75-27-4 Bromodichloromethane in i i

Total Xylenes 7 J

SURROGATE RECOVERY

1 1-DICHLOROETHANE du 93 TOLUENE d8 113 p-BROMOFLUOROBENZENE 120


COMMENT U NOT DETECTED

NR NOT REQUESTED J PRESENT AT LESS THAN DETECTION L IMIT

ANALYTE PRESENT IN BLANKB

APPROVED BYDATE February 28 1986 Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies

ROY F WESTON



CLIENT GZA GCMS F ILE NAME I217W002216

SAMPLE DESC SCC-GWS-B-102B MATRIX Water

RFW bull 8512-327-0040 METHODI bull MED LEVEL CLP (C i rc le One


DATE ANALYZED December 18 1985 PH NA X MOISTURE NA

WORK ORDER

ugXgfjA ugKg CASCAS (Circle One)ircle One) NumberNumber 78-87-5 1 2-Draquochkgtroprooane 27074-87-3 Chloromelhane 15 10061-02-6 Tranraquo-1 3-Dichloroprooene 10 U74-83-9 Bromomethane 2 J

79-01-6 Trraquochloroethene75-01 Vinyl Chloride 7 J 124-46-1 Dibromochloromethane 9 J75-00-3 Chloroethane 3 J 79-00-5 11 2-Trraquochloroethane k k k

75-09-2 Methylene Chloride k k k71-43-2 Benzene67-84-1 Acetone

10061-01-5 c i t r l 3-Dtchlofopropene75-15-0 Carbon DiauKide 75 LQJLL

110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Oichloroethene 920 75-25-2 Bromoform 9275-34-3 1 1-Dichloroethane 250 591-78-6 4-Methyl-2-Pentanone

156-60-5 Trans-1 2-Oichloroethene 610 k k k

k k k 106-10-1 2-Hexanone 260067-66-3 Chloroform k k kk k k 127-18-4 Tetrachloroethene

107-06-2 1 2-Dichloroethane 79-34-5 1 12 2-Tetrachloroethane k k k

78-93-3 2-Butanone k k k

106-88-3 Toluene k k k 71-55-6 11 1-Trichloroethane k k k

106-90-7 Chlorobenzene k k k 56-23-5 Carbon Tetracnlonde

100-41-4 Ethylbenzene k k k 108-06-4 Vinyl Acetate 10 u

100-42-5 Styrene 53075-27-4 Bromodichloromethane 4 J Total Xylenes

75-69-4 Trichlorofluoromethane 8 J

SURROGATE RECOVERY

1 1-DICHLOROETHANE du TOLUENE dg l i p-BROMOFLUOROBENZENE 146


COMMENT shyNOT DETECTEDU undetermined possible interference

NR NOT REQUESTED see dilution (lab dun)PRESENT AT LESS THAN DETECTION L IMITJ

B ANALYTE PRESENT IN BLANK

DATE February 28 1986 APPROVED BY_ Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies

ROY F WESTON ORGAN IC ANALYSIS DATA SUMMARY


CLIENT GZA GCMS F ILE NAME 1217W002217

SAMPLE DESC Lab

SCC-GWS -B-102Bn im MATRI X Water

RFW 8512-327-OOÔRP METHOD~^LOw) MEDLEVEL CLP (C i rc le On

DATE COLLECTED DECEMBER A 1 985 DILUTION FACTOR 1 000

DATE ANALYZED DECEMBER 18 1985 PH NA MOISTURE NA

WORK ORDER

CAS Number 74-67-3 74-83-9

Chloromethane Bromomethane

ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6

^ygI)bruqKfl ICircle One)

1 2-Dichloropropene Trans-1 3-Dichloropropene

10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1

Trichloroethene Dibromochloromethane

52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride

Acetone Carbon Disulfide 1 1-Qichloroethene 1 1-Oichloroethane

200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2

11 2-Trichloroethane

Benzene cis-1 3-Oichlofopropene 2-Chloroethy lv iny le ther Bromoform

8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3

Trans-1 2-Dichloroethene

Chloroform

10000 3300

u J

591-78-6 106-10-1

4-Methyl-2-Pentanone

2-Hexanone 29000 10000 u

107-06-2 1 2-Dichkgtroethane 66000 127-18-4 Tetrachloroethene 20000

78-93-3 2-Butanone 400000 79-34-5 112 2-Tetrachlordethane 4700 J

71-55-6 11 1-Trichloroethane 23000 106-88-3 Toluene 32000

56-23-5 Carbon Tetrachloride 2200 J 106-90-7 Chlorobenzene 15000

106-06-4 75-27-4

Vinyl Acetate Bromodichloromethane

10000 10000

U u

100-41-4

100-42-5

Ethylbenzene Styrene

12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY

1 1-DICHLOROETHANE du 1 1 1 TOLUENE ds 120 p-BROMOFLUOROBENZENE 122


COMMENTU - NOT DETECTED NR - NOT REQUESTED

J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK

APPROVED BYDATE Ear l M Hansen PhD Manager WESTON Analy t ica l Laborator ies

R0Y F WESTON ORGANIC ANALYSIS DATA SUMMARY



SAMPLE DESC SCC-GWS-B-001A MATRIX _ Water _

RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_

lgtfupKfl CAS (ugneruBllflCAS Number (Circle One)Circte One)(CircNumber 78-87-5 1 2-Dichloropropane 10 U74-87-3 Chloromethane 10 U 10061-02- 6 Trans-1 3-Dichloropropene 10 u10 u74-83-9 Bromomelhane 79-01-6 Trichloroethene 10 u76-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u76-0O-3 Chloroethane 10 u 79-00-5 11 2-Trichlorocthane 10 u76-09-2 Methylene Chloride 7 JB 71-43-2 Benzene 10 u10 U67-84-1 Acetone

10 u 10061-01-5 cis-1 3-Dichtoropropene 10 u 75-16-0 Carbon Disulfide

10 u 110-75-8 2-Chtoroelhylvinylether 10 u75-35-4 1 1-Oichloroethene 75-25-2 Bromoform 10 u75-34-3 1 1 -Dichloroethane 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 U 106-10-1 2-Heanone 10 u

67-86-3 Chloroform 10 u 127-18-4 Tetrachloroethene 10 u

107-06-2 1 2-Dlaquochkgtroethane 10 u 79-34-5 1 12 2-Tetrachloroethane 10 u78-93-3 2-Butanone 10 u 106-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u

10 u 108-90-7 Chlorobenzene 10 u56-23-5 Carbon Tetrachloride 100-41-4 Ethylbenzene108-05-4 Vinyl Acetate 10 u 10 u

10 u 100-42-5 Styrene 10 u75-27-4 Bromodichloromethane Tota l Xy lenes 10 u

SURROGATE RECOVERY

11-DICHLOROETHANE du _96_ TOLUENE dg 110 p -BROMOFLUOROBENZENE m



NR - NOT REQUESTED J - PRESENT AT LESS THAN DETECTION L IMIT B - ANALYTE PRESENT IN BLANK

T ZS B C APPROVED BY_ DATE 1 - Ear l H Hansen PhD




CLIENT GZA GCMS F ILE NAME 1217W0022 1 A

SAMPLE DESC SCC-QAC-SBOOl MATRIX V a ter

RFW 8512-327-0060 METHOD~2pound5 MED LEVEL CLP (C i rc le One

DATE COLLECTED December k 1985 DILUTION FACTOR 1

DATE ANALYZED December 18 1985 PH NA MOISTURE NA

WORK ORDER sectbull - bull

CAS (upôr ugKfl CAS ugl)raquof ugKg ^^Circte One] Number (Circle One)Number

78-87-5 1 2-Dichloropropane74-87-3 Chloromethane 10 U 10 u 10 u 10061-02-6 Trans-1 3-Dichloroproqene 10 u74-83-9 Bromomethane

79-01-6 Trichloroethene75-01-4 Vinyl Chloride 10 u 10 u 10 u 124-4S-1 Dibrombchloromathane 10 u75-0O-3 Chloroethane

79-00-5 11 2-Trichloroethane75-09-2 Methylene Chloride 5 JB 10 u 71-43-2 Benzene 10 u67-64-1 Acetone 10 U 10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 Carbon Disulfide 10 U 110-75-8 2-Chloroethylvinylether 10 u75-35-4 1 1-Dichloroethene 10 u 75-25-2 Bromoform75-34-3 1 1-Dichloroethane 10 u 10 u 591-78-6 4-Methyl-2-Pentanone 10 u156-60-5 Trans-1 2-Dichloroethene 10 u 106-10-1 2-Hexanone67-66-3 Chloroform 10 u 10 u 127-18-4 Tetrechloroethene 10 u107-06-2 1 2-Dichloroethane 10 u

11 79-34-5 112 2-Tetrachloroethane 10 u78-93-3 2-Butanone 108-88-3 Toluene 10 u71-55-6 11 1-Trichloroethane 10 u 106-90-7 Chlorobenzene56-23-5 Carbon Tetrachloride 10 u 10 u 100-41-4 Ethylbenzene 10 u106-05-4 Vinyl Acetate 10 u 100-42-5 Styrene75-27-4 Bromodichloromethane 10 u 10 u

Total Xylenes 10 u

SURROGATE RECOVERY

11-DICHLOROETHANE du 92

TOLUENE dB mi p-BROMOFLUOROBENZENE 111




DATE z z 8 r 6

APPROVED BY_ mdash u^ i^_Ear l M UHansen DL rPhD


ROY F VISION ORGAN I C AMALYSIS DATA SUMMARY


GCMS F ILE NAME 1217W002213GZACLIENT MATR I X WaterSCC-QAC-TBOO1SAMPLE DESC

METHOD LOW MED LEVEL CLP (C i rc le One8512-327-0080RFV DILUTION FACTOR 1DATE COLLECTED December k I 985

Z MOISTURE NA DATE ANALYZED December 17 1985 PH NA

WORK ORDER _

j(g7)oTiJQXQ CAS lgtr wgHflpound7JgtKCAS (Circle One) Number ircte One)jfCircNumbtr

78-87-5 1 2-Dtchloropropene 10 U74-87-3 Chloromethene 10 U 10 u 10061-02-6 Trenraquo-1 3-Dichloropropene 10 u74-83-9 Bromomethane 10 u 79-01-6 Trichloroethene 10 u75-01-4 Vinyl Chloride 10 u 124-48-1 Dibromochloromethane 10 u75-00-3 Chloroethane

79-00-5 11 2-Trichloroethane 10 u75-09-2 Methylene Chloride 13 B 10 71-43-2 Benzene 10 u67-84-1 Acetone

10061-01-5 cis-1 3-Dichloropropene 10 u75-15-0 C-artoo Disulfide 10 U 110-75-8 2 -Chloroethylvinylether

75-35-4 1 1 -Dichloroethene 10 u 10 [J

75-25-2 Brornotorm75-34-3 1 1 -Dichloroethene 10 u 10 IJ

591-78-6 4-Methyl-2-Pentanone156-60-5 Trans-1 2-Dichloroethene 10 u 1Q U

106-10-1 2-Heanone 10 U 67-66-3 Chloroform k J 127-18-4 Tetrachloroethene 10 u 107-08-2 1 2-Dichloroethene 10 u 79-34-5 1 1 2 2-Tetrechloroethane 10 u 78-93-3 2-Butenone 10 u

71-55-6 11 1-Trichloroethane 3 J 106-88-3 Toluene 10 u 106-90-7 Chlorobenzene 10 56-23-5 Carbon Tet rach lor ide 10 u u 100-41-4 Ethylbenzene 10 u 108-05-4 Vinyl Acetate 10 u

10 u 100-42-5 Styrene 10 IJ 75-27-4 Bromodichloromethane Total Xylenes 1 0 u

SURROGATE RECOVERY 98 11-DICHLOROETHANE du

TOLUENE dg 1 1 1 p-BROMOFLUOROBENZENE 1 U


U

NR j B

-

---

NOT DETECTED

NOT REQUESTED PRESENT AT LESS ANALYTE PRESENT

THAN DETECTION IN BLANK

L IMIT

C0MMENT_

-2 IH APPROVED BYDATE T Ear lEar l MM HansenHansen PhDPhD


ROY F WESTON



1217W002221 CLIENT GZA GCMS F ILE NAME

SAMPLE DESC_ SCC-GWS-B-1OlA MATRIX Water

RFW = DATE rn i 1 FCTED

8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

^ygTjlor ugICflujiVugAfl CAS (Circle One)CAS

(Circle One) NumberNumber 78-87-5 1 2-0ichkgtropropane 710 J10 000 u74-87-3 Chioromethane

10 000 u 10061-02-6 Trana-1 3-Pichloropropene 10 000 u 74-83-9 Bromomethane

10 000 u 79-01-6 Trichloroethene 6000075-01bull Vinyl Chloride

124-48-1 Oibromochloromethane 10 000 u10 000 u75-00-3 Chloroethane 79-00-5 11 2-Trichloroethane 780 J82000 B75-09-2 Methylene Chloride

10 000 u 71-43-2 Benzene 8 500 J 67-64-1 Acetone

10061-01-5 cis-1 3-0ichloropropene 0 000 u10 000 u75-15-0 Carbon PituHide 700 J 110-75-8 2-Chloroethylvinylether 10 000 u

75-35-4 1 1-Pichloroethene 75-25-2 Bromolorm 10 000 u1 8001 1 -Dichloroethane

0000 591-78-6 4-Methyl-2-Pentanone 10 000 u 156-60-5 75-34-3

Trans-1 2-Pichloroethene 106-10-1 2-Hexanone 10 000 u

67-66-3 Chloroform 3 500 127-18-4 Tetrachtoroethene 8 800 J

107-06-2 1 2-Pichtoroethane 20^000 79-34-5 1 12 2-Tetrachloroethane 0 000 u10 000 u78-93-3 2-Btrtanone 106-88-3 Toluene 19 00053000 108-90-7 Chlorobenzene 600 J71-55-6 11 1-Trichloroethane

56-23-5 Carbon Tetrachloride 10 000 u 100-41-4 Ethylberuene 7 800 J

108-05-4 Vinyl Acetate 10 000 u 10 000 u 100-42-5 Styrene 740Bromodichloromethane

Total Xylenes 3 6 0 075-27-4

75-69-4 Tr i ch1oro f1uoro- 5000 methane

SURROGATE RECOVERY

11-DICHLOROETHANE du 104 TOLUENE dg 1 00

ToFp-BROMOFLUOROBENZENE


U - NOT DETECTED COMMENT_ NR - NOT REQUESTED

J - PRESENT AT LESS THAN DETECTION LIMIT B - bull ANALYTE PRESENT IN BLANK

7- ~ ^ APPROVED BYDATE

Ear l M Hansen PhD Manager urlt TnN Ana ly t ica l Labora tor ies

ROY F wt i i UN ORGANIC ANALYSIS DATA SUMMARY


GZA GCMS F ILE NAME 1217W002212

CLIENT

SAMPLE DESC T r ip B lank M A T R I X W a t e r

RFW - 8512-327-0100 METHOD LOU MED LEVEL CLP (C i rc le One

DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H

(ZgTykrugKgupKg CASCAS (Circle One)(Circle One) Number Number 10 U78-87-5 1 2-Dichloropropene10 UChloromethane74-87-3] Tranraquo-1 3-Dichloropropene 10 u0 u 0061-02- 6

Bromomethane74 R3-9 10 u 79-01-6 Tnchloroethene 10 u 75-01- Vinyl Chloride

Dibromochloromeihane 0 u124-46-110 UChloroethane75-00-3 79-00-5 11 2-1rraquochkgtroeihane 10 u8 JB75-09-2 Methylene Chloride 10 u71-43-2 Benzene10 U67-64-1 Acetone

10061-01-5 cia-1 3-DtChloropropene 0 u Carbon DiauHide75-15-0 10 U

110-75-8 2 -Chloroethylvinylether 10 u 1 1-Dichloroethene 10 u75-35-4

75-25-2 Bromolorm 0 u10 u1 1-Dichloroethene75-34-3 591-78-6 4-Methyl- 2-Pentanone 10 u0 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexarvone 10 u10 u

67-66-3 Chloroform 127-18-4 Tetrachloroethene 10 u10 u1 2-Dchloroethane107-06-2 79-34-5 1 12 2-Tetrachloroethane 10 u0 u2-Butanone76-93-3 108-88-3 Toluene 10 u

71-55-6 1 1 1-Trraquochloroethane 10 u 108-90-7 Chlorobenzerve 0 u10 u Carbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Tota l Xylenes 10 u

SURROGATE RECOVERY 1 0 111-DICHLOROETHANE dt 1 08TOLUENE d8

p-BROMOFLUOROBENZENE 109


COMMENTNOT DETECTED

NR NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMIT

U

J ANALYTE PRESENT IN BLANKB

APPROVED BY DATE Ear l M Hansen PhD


74-87-3

ROY F WLS1QN ORGANIC ANALYSIS DATA SUMMARY


C L I E N T GZA GCMS F ILE NAME 1217W002139

SAMPLE DESC Lab B lank MATRIX Water

RFV Rq i7-R7-B lank METHOD LOU) MED LEVEL CLP (C i rc le One

DATE COLLECTED NA DILUTION FACTOR 1

DATE ANALYZED December 17 1985 PH NA MOISTURE N A

WORK ORDER

(oghor ugKflltug2jgtrugltfl CAS CAS iCircie One)(Circle One| Number Number

78-87-5 1 2-Dichloropropane 10 U Chioromethane 10 U

10061-02-6 Tranraquo-1 3-Dichloropropene 10 u10 uBromomethane74-63-9 79-01-6 Trtchloroethene 10 u10 u 75-01-4 Vinyl Chloride

124-48-1 Dibrpmochloromethane 10 u10 u75-00-3 Chloroethane 2 J 79-00-5 11 2-Trichloroethane 10 u

75-05-2 Methylene Chloride 10 U 71-43-2 Benzene 10 u

67-64-1 Acetone 10 U 10061-01-5 cia-1 3-Dichloropropene 10 u

75-15-0 Carbon DiauHide 110-75-8 2-Chloroethylvinylether 10 u10 u1 1 -Dichloroethene75 35-4 75-25-2 Bromoform 10 u10 u1 1-Dichloroethane75-34-3 591-78-6 4-Methyl-2-Pentanone 10 u10 uTrans-1 2-Dichloroethene156-60-5 106-10-1 2-Hexanone 10 u10 uChlorolorm67-66-3 127-18-4 Tetrechtoroethene 10 u10 u1 2-Dtchloroethane107-06-2 79-34-5 112 2-Tetrachloroethane 10 u10 u78-93-3 2-Butanone

10 u 106-88-3 Toluene 10 u 11 1-Tnchloroethane71-55-6 106-90-7 Chlorobenzene 10 u10 uCarbon Tetrachloride56-23-5 100-41-4 Ethylbenzene 10 u10 u

106-05-4 Vinyl Acetate 100-42-5 Styrene 10 u10 uBromodichloromethane75-27-4 Total Xylenes 10 u

SURROGATE RECOVERY

11-DICHLOROETHANE du 105 TOLUENE dg 101 p-BROMOFLUOROBENZENE 98


bdquo -PT- rTgtn COMMENTU - NOT DETLCTLD

NR - NOT REQUESTED PRESENT AT LESS THAN DETECTION L IMITJ


^2 Cgt APPROVED BY mdash Z mdash Hansen

Manager WESTON Ana ly t ica l Labora tor ies

ROY F WESTON INC ORGANIC ANALYSIS DATA SUGARY

SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS

CLIENT SAMPLE DESC _

DATE COLLECTED DATE EXTRACTED DATE ANALYZED WORK ORDER

GZA SflC-GWS-B-1Q5A 8512-327-0010 December A 1985 December 8 1985 January 6 1986

GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx

( C i r c l e O n e )

ugl or ug Kg CAS ugl or ug 7KgCA8 (Circle Qno) Number (Circle QwNumlMf

83 32 9 Acenaphthene NDPnenol 2 U

ND 1-28-5 2 4-Dinitrophenol 106-95 2 111-44-4 bis(-2-Chloroethyl)Ether

00-02-7 4-Nitrophenol95 57-8 2-Chlorophenol

32-64 9 Dibenzofuran1 3-Dichlorobenzene 21-14-2 2 4-Dinitrotoluene

541-73-1 1 4-Dichlorobenzene

606-20-2 2 6-Dinitrotoluene 06-46-7 00-51-6 Benzyl Alcohol

184-66-2 Diethylpnthalate1 2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylethei

95-50-1 95-48-7 2-Methylphenpi

86-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Eiher 00-01-6 4-Nitroaniltne

06-44-5 4-Metnylphenol 111 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7

86-30-6 N-Nttrosbdiphenylamine (1)67-72-1 Hexachlproethane 01-55-3 4-Bromophenyl-phenyletherNitrobenzene9B-95-3 18-74-1 Hexachlorobenzene78 59-1 Isopnorone 20

ND 87-86-5 Pentachlorophenpl88-75-5 2-Nitrophenol H3

85-01-8 Phenanthrene105-67-9 2 4-Dimethylphenol

120-12-7 Anthracene65-85-0 Benzoic Acid M 84-74-2 Di-n-Butylphthalate111-91-1 bisf 2-Chloroetnoxy|Methane 1206-44-0 Fluoranthene

20-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Tnchlorobenzergte B5-68-7 Butylbervrylphthalate

20-82-1

91-20-3 Napnihalene (91-94-1 3 3 -Dichlorobenzidine (3706-47-8 4-Chloroaniltne (56-55-3 Benzolta)AnthraceneHexachlorobutadiene 117-81-7 bislt2-Ethylhexyl)Phthalate 5J

87-68 3 59-50-7 4-Chloro-3-Methylphenol

218-01-9 Chrysene ND91-57-6 2-Methylnaphthalene

117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene

88-06-2 24 6-Trichlorophehol 207-08-9 BenzcHklFluoranthene

95 95-4 2 4 5-Tnchlorophenol ( 2) 50-32-8 Benzo(a)Pyrene

91-58-7 2-Chloronaphthalene 193-39-5 lndeno(1 2 3-cd)Pyrene

88-74-4 2-Nitroanilme 111 53-70-3 Dibenzla hUknthracene

131-11-3 Dimethyl Phthalate 191-24-2 Benzo(c h IjPerylene206-96-8 IAcenaphthylenc

13-Nnroenihne99-09-2 111 (-1) Cannot be separated from Diphenylamine ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s

J = PRESENT AT LESS THAN DETECTION LIMITU = NOT DETECTED B = ANALYTE FOUND IN BLANKNR = NOT REQUESTED

Approved By DATE February 28 1986 Earl M Hansen PhD

iManager WESTON Analytical Laboratories

ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY


GCMS FILE NAME 01ogBi630GZACLIENT S lC - GrU-) s -LS- IOSf lSAMPLE DESC _ MATRIX LooJlt~

8 5 1 2 - 3 2 7 - 0 0 2 0 S Di k eRFW METHOD fLoij)MED LEVEL CLP (Circle One)DATE COLLECTED DATE EXTRACTED Dec E L91pound DETECTION LIMIT_ 10 ugLDATE ANALYZED

D F UWORK ORDER

ug Kg CAS wg KgCAS ICircl One) Number (Circle OnaNumbtr

83 32-9 AcenaphthcnePhenol A8 A O

0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2

111-44-4 $(-2-ChloroethyUEthe 00-02-7 -Nitrophenol 50bull Chlprophenol 9 095 57-8 32-64 9 Dibenzoluran 10 u

5-ai-73-1 3-Dichlorobenzene 1 0 vr 21-14-2 2 4 Djnitrotoluene A2 4-Dichlorobenzene 6 0 6 - 2 0 - 2 2 6-Dinitrotoluene 10 u 106-46-7

100-51-6 Benzyl Alcohol 10 u 5 J 84-66-2 Diethylphthalate 2-Dichlotobenzene95-50-1

7005-72-3 4-Chlorophenyl-phenytethe95-48-7 bullMeihylphenoi 1 0 U

I86-73-7 Fluorene39638-32-9 s(2-Chloroisopropyl)Ether 10 u

00-01-6 4-Nnroaniline 50 u106-44-5 4-Methylphenoi ill 534-52-1 4 6-Dinitro-2-Methylphenol FT621-64-7 N-Nitroso-Di-n-Propylamine k 2 5 0 U 86-30-6 N-Nitroscx3iphenylamine (1 10 UHexachloroethane 1 0 U 101-55-3 4-Bromophenyl-phenylether

67-72-1 Nitrobenzene

118-74-1 Hexachlorobenzene 98-95-3 78-59-1 Isophorone

187-86-5 Pentachlorophenpl ( 2 j 11088-75-5 2-Nurophenol 85-01-8 Phenanthrene 10 U

105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene 10 uBenzoic Acifl 61nr

1 0 84-74-2 Di-n-Butylphthalaie 3665-85-0 111-91-1 bis- 2-Chloroethoxy)Meihane

1 0 206-44-0 Fluoranthene 10 u 120-83-2 2 4-Dichlorophenol

129-00-0 Pyrene 371 2 4-Tnchlorobenzene 37 85-68-7 Butylbenzylphthalate 10 U

120-82-1

91-20-3 Naphthalene 10 U 91-94-1 3 3 -Dichlorobenzidine (J ) 20 U r-Chloroaniline (56-55-3 Benzolta (Anthracene 10 U

106-47-8 HexachlorobutaOiene

117-81-7 bislt2-EthylhexylfPhthaiate 1987-68 3 59-50-7 l-Chloro-3-Methylphenol bull 88

218-01-9 Chrysene 10 u91-57-6 2-Methytnaphthalene 10 U 117-84-0 Di-n-Octyl Phthalate

77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)FIuoranthene

68-06-2 2 4 6-Tnchlorophenol 207-08-9 Benzo(k|Fluoranthene

95 95-4 24 b-Tnchlofophenol ( 2 ) o u 50-32-8 BenzcXapyrene

91-58-7 2-Chloronaphthalene 10 u 193-39-5 IndenoO 2 S-ctDFyrene5088-74-4 2-Nitroaniline M

1 0 53-70-3 Dibenzia hVAnthracene131-11-3 Dimethyl Phihalaie

191-24-2 Benzoic h iperylene208 96-8 Acenaphthylene 10 U

3-Nitroaniline99-09-2 111 50 u ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s


uSpiked Compounds Approved By s Earl M Hansen PhD DATE February 28 1986

Manager WESTON Analytical Laboratories

ROY F WESTON INC ORGANIC ANALYSIS DATA SUWARY


GZA GCMS FILE NAME 0 1 0 9B 1 6 2 9CLIENT SCC-GWS-B-102ASAMPLE DESC _ MATRIX Water 8512-327-0030RFW December A T9BT METHOD (Tow)MED LEVEL CLP bull (Circle One)DATE COLLECTED December 6 T9FTDATE EXTRACTED DETECTION LIMIT 10 ugLJANUARY 9 1986DATE ANALYZED

D F 1WORK ORDER

[ygjl or ug Kg CAS or wg KgCAS (Circle One) Number (Circle OneNumtor

83 32-8 Acenaphthene 10 U Phenol 10 U 1-28-5 2 4-Dinitrophenol 50 u

108-95 2 j(-2-Chloroethyl)Ether

00-02-7 4-Nitrophenol 50 u-Chlorophenol 32-64 9 Dibenzoluran 10 u3-Dichlorobenzene 21-14-2 2 4 Dmitrotoluene

541 73-1 4-Dichlorobenzene

606 20-2 2 6-Dinitrotoluene 106-46-7 100-51-6 Benzyl Alcohol

84-66-2 Djethylphthalate2-Dichlorobenzene 7005-72-3 4-Chlorophenyl-phenylether

95-50-1 95-48-7 2-Methylphenol

186-73-7 Fluorene39638-32-9 bis(2-chloroisopropyl)Ether

06-44-5 4-Methylphenol 00-01-6 4-Nitroaniline 111 50 534-52-1 4 6-Dinitro-2-Methyiphenol FTso621-64 7 N-Nitroso-Di-n-Propylamine 86-30-6 N-Nitrosodiphenylamme (1) 10 u67-72-1 Hexachloroethane 101-55-3 4-Bromophenyl-phenylether98-95-3 Niuobenzent 118-74-1 Hexachlorobenzene78-59-1 Isophorone 87-86-5 Pentachlorpphenpl 50 U88-75-5 2-Nitrophenol H 85-01-8 Phenanthrene 10 U105-67-9 2 4-Dimethylphenol 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U 64-74-2 Di-n-Butylphtnalate111-91-1 bis(-2-Chioroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene

120-82-1 1 2 4-Trichlorobenzene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene 91-94-1 3 3 -Dichlorpbenzidine (3 )106-47-8 4-Chloroaniline 20 U 56-55-3 Benzolta(Anthracene 10 U87-68 3 Hexachlorobutadiene 117-81-7 bts(2-Ethylhexyl)Phthalate A J

59-50-7 -Chloro-3-Methylphenol 218-01-9 Chrysene 10 U91-57-6 2 -Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205-99-2 Benzo(b)Fluoranthene

88-06-2 2 4 6-Trichlorophenol 207-08-9 Benzo(k)Fluoranthene95 95-4 2 4 5-Tnchlorophenol ( 2 f 30 U 50-32-8 Benzotapyrene91-58-7 2-Chloronaphthalene 10 u 193-39-5 lndenolt12 3-cd)Pyrene88 74-4 2-Nitroanlhne 111 50 u

10 u 53-70-3 Dibenzla hVAnthracene131-11-3 Dimethyl Phthalate 10 u 191-24-2 BenzcHc h iperylene206-96-8 Acenaphthyiene

99-09-2 3-Nitroanilme 111 50 u ( 3 ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( ) MDL = 5X other HSL Compounds (3) MDL = 2X other HSL Compounds

U = NOT DETECTED J = PRESENT AT LESS THAN DETECTION LIMIT NR = NOT REQUESTED B = ANALYTE FOUND IN BLANK

Approved By DATE mdashEarl M Hansen PhD


ROY F WESTON INC ORGANIC ANALYSIS DATA SUNMARY


GCMS FILE NAME 0 1 0 9 B 1 6 3 1 amp 0 1 1 1 P 1 6 6 f gt n u GZACLIENT t i o n SCC-GWS-B-IOSAMPLE DESC _ MATRIX Watgr

8512-327-0040RFW METHOD ^W)MpoundD LEVEL CLP ( C i r c l e O n e )DATE COLLECTED D e c e m b e r 4 1 9 8 5

DATE EXTRACTED D e c e m b e r 8 1 9 8 5 DETECTION LIMIT 10 ugLDATE ANALYZED J a n u a r y 9 1 9 8 6

D F l x amp 1OxWORK ORDER

ufl KB CAS UBKSCAS Circle One) Number (Circgtraquo OneNumber ____

83 32-9 Acenaphthcne 10 u 10 U106-95 2 |Pncnp[ 1-28-5 4-Dirutrophenol 50 U111-A4-4 bis-2-Chloroethyl)Eiher 00-02-7 4-Nitrophenol I2 ) I

95 57-8 12-CMorophenol 32-64 9 Dibenzoluran 10 u

541-73-1 11 3tDichlorobenzene 21-14-2 2 4 Dmitrotoluene106-46-7 11 4-Dichlorobenzene

606-20 -2 2 6-Dinitrotoluene100-51-6 j Benzyl Alcohol 8 1 84-66-2 Diethylphthalate1 2-Dichlorobenzene 10 U95-50-1 7005-72-3 4-Chlprophenyl-phenyleiher2-Meihylphenpi95-48-7 86-73 7 Eluorene39638 32-9 |bisi2 -chlor oisoprppyllEther 100-01-6 4-Nitroaniline 50 U106-44-6 4-Metnylphenol 111 534-52-1 4 6-Dinitro-2-Methylpneno TT621-64-7 ) N-Nitrosp-Pi-n-Propylamine 86-30-6 N-Nitrpsodiphenylamme (1 10 u67-72-1 Hexachlorpethane 101-55-3 4-Bromophenyl-phenyletherI Nitrobenzene 118-74-1 Hexachlorpbenzene

98-95-3 78-59-1 Isophprone 1700

87-86-5 Pentachlorpphenpi 50 U88-75-5 2-Nitrpphenpl 10 U

85-01-8 Phenanthrene 10 U105-67-9 24-Dimethylphenol 120-12-7 AnthraceneBenzoic Acid 50 U65-85-0 HE 84-74-2 Di-n-Butylphihalaie111-91-1 bis(-2-Chloroethoxy)Methane 10 U 206-44-0 Fluoranthene120-83-2 1 2 4-Dichlorophenol 129-00-0 Pyrene

120-82-1 1 2 4-Tnchlprpbenzene 85-68 7 Butylbenrylphthaiate

91-20-3 Naphthalene 3 3 -Dichlprobenzidine ( 3B1-94-1 20 U106-47-8 4-Chloroaniline

[56-55-3 Benzolta (Anthracene 10 UI Hexachlorobutadiene 117-81-7 bis(2 -Ethylhexyl)Phthalate


218-01-9 Chrysene91-57-6 2-Methylnaphthalene

117-84-0 Di-n-Octyl Phthalate77-47-4 [ Hexachlorocydopentadiene

05-99-2 Benzo(b)Fluoranthene1-24 6-Trichlorophenol88-06-2 I 2 4 5-Trichlofophenol ( 2 ) I 50 U 1-07-08-9 Benzoltk(Fluoranthene

95 95-4 E0-32-8 Benzo(a(Pyrene

91-58-7 2-Chloronaphthalene 10 U 193-39-5 lrgtdeno(1 2 3-cd)Pyrene

88-74-4 2-Nitroanilme 111 50 U 53-70-3 Dibenzia hVKnthracene131-11-3 Dimethyl Phthalate 10 U 191-24-2 Benzoltp h iperylene1206-96-8 IAcenaphthylene

99-09-2 3-Nitroamline HI 50 U l ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n = ( 2 ) M D L = 5 X o t h e r H S l C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s


Approved By Earl M Hansen PhDDATE - February 28 1986 Manager WFSTON Analyt ical Laborator ies

ROY F WESTON INC ORGANIC ANALYSIS DATA SUNWARY


CLIENT GZA GCMS FILE NAME 0111B1656

SAMPLE DESC _ RFW DATE COLLECTED

SCC-GWS-B-OOIA 8512-327-0050 December U 1985

MATRIX

METHOD

^

LOHMED

Water

LEVEL CLP (Circle One DATE DATE WORK

EXTRACTED ANALYZED ORDER

December 8 1985 January 11 1986 DETECTION LIMIT

D F l x io UgL

CAS ug l or ug Kg CAS ug l or ug Kg Number (Circle Or) Number (Circb Qna

83 32-8 Acanaphthene 10 uhoe 95 2 Pnenpl 10 U 1-28-5 2 4-Dinitrpphenol 50 U111-44-4 j(-2-Chloroethyl)Ether 00-02-7 4-Nitrophenol 50 U95-57-8 -Chlprpphenol 32-64 9 Dibenzoluran 10 U 541-73-1 3-Dichlprobenzene 21-14-2 2 4-Dimtrotoluene4-Dichlorobenrene


184-66-2 Diethylphthalate95-50-1 2-Dichlprobenzene 7005-72-3 4-Chlorophenyi-phenytethei95-48-7 2-Meinyiphenoi 86-73-7 Fluorene 10 U39638-32-9 bis(2-chloroisopropyt (Ether 100-01-6 4-Nitroaniline DO U

106-44-5 4-Methylphenol

621-64 7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinitro-2-Methylphenol (i)50 U 86-30-6 N-Nurosod ipheny lamine (11 10 U67-72-1 Hexachlorpethane 101-55-3 4-Brpmophenyl-phenylether 10 UNiuobenzentshy118-74-1 Hexachlprpbenzene 10 U

98-95-3 78-59-1 Ispphprpne

87-86-5 Pentachlorpphenol DO U88-75-5 2-Nitrpphenol m 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 U

120-12-7 AnthraceneBenzoic AciO 50 U65-85-0 III 111-91-1 bis -2-ChloroetnoxylMettiane 10 U 84-74-2 Di-n-Butylphthalate

206-44-0 Fluoranthene120-83-2 2 4-Dichlorophenol 129-00-0 Pyrene1 2 4-Trichlorobenzene120-82-1

ButylbenrylphthaiateB5-66-7 10 U91-20-3 Naphthalene 3 3-Dichlproben2iOine ( 3

106-47-B 4-Chloroanihne B1-94-1 20 U 56-55-3 Benzolta(Anthracene 10 UHexachlorobutafliene 117-81-7 bis(2 -Ethylhexyl)Phthaiate

87-68 3 59-50-7 4-Chloro-3-Methytphenol

[218-01-9 Chrysene91-57-6 2-Methylnaphthalene 117-84-0 Di-n-Octyl Phthalate77-47-4 Hexachlorocyclopentadiene 205 99-2 Benzo(b)Fluoranthene88-06-2 2 4 6-Trichiorophenol 10 U

95 954 2 4 5-Trichlorophenol ( 2 ) 50 U 207-08-9 Benzo(k)Fluoranthene 50-32-8 benzolta(Pyrehe91-58-7 2-Chlorpnaphthalene 10 U

50 U 193-39-5 IndenoO 2 3-cfl)Pyrene88-74-4 2-Nitroanilme 111 10 U 53-70-3 Dibenzta hlAnthracene131-11-3 Dimethyl Phthalate TO 191-24-2 Benzoic h iperylene 10 U206-96-8 Acenaphthylene 50 U3-Nitroahilme99-09 2 111 i 1 ) Cannot be separated from Diphenyl amine

( 2 ) M D L = 5X other HSL Compounds( 3 ) M D L = 2X other HSL Compounds

U = NR =

NOT DETECTED NOT REQUESTED

J B

= PRESENT = ANALYTE

AT LESS THAN DETECTION LIMIT FOUND IN BLANK

DATE February 28 1986 Approved By

Earl M Hansen PhD Manager WEsectTON Analytical Laboratories

ROY F WESTON INC ORGANIC ANALYSIS DATA SUMMARY lt$

SEMI-VOLATILE HAZARDOUS SUBSTANCE LIST COMPOUNDS v

G Z A GCMS FILE NAME 0 1 1 1 B 1 6 5 7CLIENT SAMPLE DESC _ S C C - O A L - S B - O O l MATRIX W a t e r RFW 8 5 1 2 - 3 2 7 - O O P O

DATE COLLECTED D e c e m b e r L 1 9 8 5 METHOD (LOOMED LEVEL CLP ( C i r c l e O n e ) DATE EXTRACTED D e c e m b e r 8 1 3 8 5

DETECTION LIMIT 1 0 u q LJ a n u a r y 1 1 1 9 8 6 shyDATE ANALYZED D F WORK ORDER

CAS (ug tor ugKg CAS Cygjôr ug Kg

Number ^Circle Or) Number (Circle On1

Phenol 1 0 U 83 32-9 Acenaphthene 0 U106-95 2 111-44-4 bis(-2-Chloroeihyl)Ether 51-28-5 2 4-Dinnrpphanoi 5 0 U

95 57-6 2-Chlprophenol 100-02-7 4-Nnrophenol I 2 ) 50 u 132-64 9 Dibenzofuran 10 u541-73-1 1 3-Dichlorobenzene

106-46-7 1 4-Dichlorobenzene 121-14-2 2 4-Dmitrotoluene

100-51-6 Benzyl Alcohol 606-20-2 2 6-Dinitrotoluene

95-50-1 1 2-Dichlprobenzene 84-66-2 Diethylphthalate

95-48-7 2-Methylphenol 7005 72-3 4-Chlorophenyl-phenylether

39638-32-9 bis(2-chloroisoprppyl)Ether 86-73-7 Fluorene

106-44-5 4-Methylphenol 100-01-6 4-Nitroaniline 50 u 111 621-64-7 N-Nitroso-Di-n-Propylamine 534-52-1 4 6-Dinnro-2-Methyiphenol

Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (11 10 u 67-72-1 Nnrobenzent- 101-55-3 4-Brpmophenyl-phenylether98 95-3

78-59-1 Isophorone 118-74-1 Hexachlprobenzene

88-75-5 2-Nitrophenol 87-86-5 Pentachlorpphenpl HT 50 u 105-67-9 2 4-Dimethylphenol 85-01-8 Phenanthrene 10 u 65-85-0 Benzoic Acid m SO u 120-12-7 Anthracene

111-91-1 bis 2-Chloroethoxy)Meth3ne 10 u 184-74-2 Di-n-Butylphthalate

120-83-2 2 4-Dichlorophenol 1206-44-0 Fluoranthene

120-62-1 1 2 4-Trichlorobenzerte 129-00-0 Pyrene

91-20-3 Naphthalene 65-66-7 Burtylbenzylphthaiate

106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlorobenzidine (3 ) 2 0 U

87-68-3 Hexachlorobutadiene 56-55-3 Benzolta)Anihracene 10 u 59-50-7 4-Chloro-3-Methylphenol 117-81-7 bislt2-Ethylhexyl)Phthalate

91-57-6 2-Methylnaphthaiene 1218-01-9 Chryaene

77-47-4 Hexachlorocyclopentadtene 117-84-0 Di-n-Octyl Phthalate

88-06-2 2 4 6-Tnchlorophenol 205-99-2 Benzo(b)Fluoranthene

95 95-4 2 4 5-Trichlorophenol ( 2 ) 207-08-9 Benzoltk)FluorantheneSO U 91-58-7 2-Chloronaphthalene 10 u 50-32-8 Benzolta)Pyrene

88-74-4 2-Niiroanilme 111 50 u 193-39-5 lndenp(1 2 3-cdtFVrene

Dimethyl Phthalate 10 u 53-70-3 Dibenzia hlAnthracene131-11-3 Acenaphihylene 10 u 191-24-2 Benzoic h iperylene206 96-8

99-09-2 3-Nitroanihne 50 u 111 ( ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n e ( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s


Approved By DATE V $pound Earl M Hansen PhD




0111B1658 G Z A GCMS FILE NAME _ 0 1 1 1 B 1 6 6 1 ( 1 1 0 P i 1 u t i o n )CLIENT S C C - G W S - B - 1 0 1 ASAMPLE DESC _ MATRIX W a t e r 8512-327-0090RFVJ

METHOD (^LOW)MED LEVEL CLP (Circle OneDATE COLLECTED December A 1985 DATE EXTRACTED December 8 1985

DETECTION LIMIT 1 0 u g LDATE ANALYZED Janua ry 11 1986 D F 1 x amp 1 OxWORK ORDER

CAS I gtr ug Kg CAS ug |^gtr ug tg

Number irele One) Number Circle One1

106-95 2 Pnenol 1 0 U 83 32-9 Acenaphthene 10 U

95-57-8

11-44-4 bif-2-ChloroethyltEther 2-Chlprophenpl

10 80

u 1-28-5 00-02-7 4-Niirpphenpl

2 4-Dinitrophenpi

V 5 0 5 0

U U

541-73-1 3-Dichlorobenzene 1 2 0 32-64 9 Dibenzoluran 0 U

06-46-7 4-Dichicrpbenzene 3 9 0 21-14-2 2 4-Dinitrotoluene

00-51-6 Benzyl Alcohol 1 L O O 606 -20 -2 2 6-Dmitroioluene

95-50-1 1 2-Dichlorobenzene 900 84-66-2 Diethylphthalate

95-48-7 2-Meihylphenoi 1 7 0 7005-72-3 4-Chlorophenyl-phenylethei

39638-32-9 bis[2-chleroitoprppyl)Elher 1 0 U 86-73-7 Fluorene

106-44-5 621-64 7

4-Methylphenol N-Niuoso-Di-n-Propylamine

100-01-6 534-52-1

4-Nitroanihne 111 4 6-Dinitrp-2-Methylphenol ( 2 )

5 0 U 5 0 U

67-72-1 Hexachloroethane 86-30-6 N-Nitrosodiphenylamine (1] 10 u 98 95-3 Nitrobenzene 101-55-3 4-Brpmophenyl-phenylethei

78-59-1 Isophprone 1 9 0 0 118-74-1 Hexachlprpbenzene

88-75-5 05-67-9

2-Nitrpphenol 2 4-Dimethylphenol

1 0

1 0

U

U

(87-86-5 85-01-8

Pentachlorpphenol Phenanthrene

5 0 10

U u

65-85-0 Benzoic Acid M 50 U 120-12-7 Anthracene

111-91-1 bis 2-Chloroethoxy)Methane 1 0 U 84-74-2 Di-n-Butylphthalate

120-83-2 2 A-Dichlorophenol bull10 U 206-44-0 Fluoranthene

120-82-1 1 2 4-Tnchlorobenzene 270 129-00-0 FVrene

91-20-3 Naphthalene 1 3 0 (35-66-7 Birtylbenrylphihaiate

106-47-8 87-68 3

4-Chlorpaniline Hexachlorobutadiene

1 0

1 0

U

U

B1-94-1 56-55-3

3 3-Dichlorobenncine I Benzolta)Anthracene

2 0 U 10 u

59-50-7 4-Chloro-3-Methylphenolshy 1 AO 117-81-7 bislt2-EthYlhexyl)Pnthaiate

91-57-6 2-Methylnaphthalene 1 0 U 218-01-9 Chrysene


88-06-2 2 4 6-Trichlorophenol 205 99-2 Benzo(b)Fluoranthene

95 95-4 2 4 5-Tfichlorophenol ( 2 ) 5 0 U 207-08-9 Benzo(k)Fluoranthene

91-58-7 2-Chloronaphthalene 1 0 U 50-32-8 Benzole)Pyrene

88 74-4 2-Nitroaniline lil 5 0 U 193-39-5 IndenoO 2 S-cdlF^yrene

131-11-3 Dimethyl Phihalate 180 53-70-3 Dibenzia hgtAnihracene

206 96-8 Acenaphthylene 1 0 U 191-24-2 Benzo(g h iperylene

99-09-2 3-Nitroaniline HI 5 0 U ( x )( 2 ) ( 3 )

C a n n o t M D L = M D L =

be separated from Diphenylamine 5X other HSL Compounds 2X other HSL Compounds



Earl M Hansen PhD Manager WFSTON Analytical labnratnripr

ROY F WESTON INC ORGANIC ANALYSIS DATA SIWARY


GZA GCMS FILE NAME 0106B1593CLIENT SAMPLE DESC _ Lab Blank Batch 308 MATRIX Water R CU sectbull 8512-327-Blank

NA METHOD LOWMED LEVEL CLP ( C i r c l e O n e )DATE COLLECTED DATE EXTRACTED December 8 1985

DATE ANALYZED January 6 1986 DETECTION LIMIT 10 ugL DF i xWORK ORDER

CAS ug gt or ug bull Kg CAS ug f or wg Kg (Circle Onlaquo] Number (Circle OneNjmbr

83 32-8 AcanaphthenePhenol 10 U 10 U

111 -AAI bis(-2-Chloroethyl)Ether 51-28-5 2 4-Dinitrophenpl TV 50 U

95 57-8

106-95-2

2-Chlorophenol 00-02-7 4-Nitrophenol TV 541-73-1 1 3-Dichlorobenzene 32-64 9 Dibenzoluran 10 U


100-51-6 Benzyl Alcohol 606-20 -2 2 6-Dinitrotoluene

1 2-Dichlorobenzene 84-66-2 Diethylphthalate

2-Methylphenol 7005-72-3 4-Chlorophenyi-phenylethei 95-50-1 95-48-7 39638-32-9 bis(2-chloroisopropyt)Ether 186-73-7 Fluorene

4-Methylphenol 100-01-6 4-Nitroanilirraquoe 50 U106-44-5 621-64-7 N-Niuoso-Di-n-Propylamine 534-52-1 4 6-Dinitrp-2-Methylphenol TV 67-72-1 Hexachloroethane 86-30-6 N-Nitrpsodiphenylamme (1) 10 U

101-55-3 4-Brpmophenyl-phenylether98-95-3 Nitrobenzene


88-75-5 2-Nitrophenol 187-86-5 Pentachlorpphenoi V) 50 U

105-67-9 2 4-Dimethylphenot 85-01-8 Phenanthrene 10 U 120-12-7 Anthracene65-85-0 Benzoic Acid in 50 U

111-91-1 bis(-2-Chlproethoxy)Methane 10 U 84-74-2 Di-n-Butylphthalate


120-82-1 1 2 4-Trichlorobenzene 129-00-0 Pyrene B5-68-7 Butylbenzylphthaiate91-20-3 Naphthalene

106-47-8 4-Chloroaniline 91-94-1 3 3 -Dichlprobenzidine I 20 U

87-68 3 Hexachlorobutadiene 56-55-3 Benzolta(Anthracene 10 U

59-50-7 4-Chloro-3-Methylphenol 117-81-7 bis2-Ethylhexyl)Pnthalate 5 J

91-57-6 2 -Methylnaphthalene 218-01-9 Chrysene 10 U

77-47-4 Hexachlorocyclopentadiene 117-84-0 Di-n-Octyl Phthalate

2 4 6-Trichlorophenol 205-99-2 Benzo(b)FIuoranthene88-06-2

95 95-4 2 4 5-Tnchlorophenol ( 2) 50 U 207-08-9 Benzo(k(Fluoranthene

91-58-7 2-Chloronaphthalene 10 U 50-32-8 BenzckaPyrene 193-39-5 lndenolt1 2 3-cd)Fyrene88-74-4 2-Nitroanilme 50 U111

131-11-3 Dimethyl Phthalate 10 U 53-70-3 Dibenzia hVAnthracene

208 96-8 Acenaphthylene 191-24-2 Benzo^p h iperylene 50 U3-Nitroanilme99-09-2 111 ( x ) C a n n o t b e s e p a r a t e d f r o m D i p h e n y l a m i n s

( 2 ) M D L = 5 X o t h e r H S L C o m p o u n d s ( 3 ) M D L = 2 X o t h e r H S L C o m p o u n d s


Approved By DATE February 28 1986 ^^-Êarl M Hansen PhD


a n I lt W A T E H S U H H O U A ib K b B i u t i a i raquo raquo a - v ^ shyltjznshy

_ Contract No

Case No G2h_ Contract Laboratory mdash

IraquoTraquottlaquoCshy

V O L A T I L E SEMI-VOLATILE yen

ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O

(gtbull- gt llaquogt

t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W

At-AMU o o J O )QltA O

6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a

out of j outside of QC limitsVolatilesbull VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS out of ( outside of OC limitsSemi-Volatiltsr ADVISORY LIMITS ONLY out of outside of QC limitsPesticides

Comments

cnou ii 7 8 6

WATER BLAIOK SPIKE Q L A V K SPIKE DUPLICATE RECOVERY

^ - c c M n - n n n t r a c t o r K(esf(nt X Client t 0 2A

FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND

1t -Dichloroethene Trichloroethene Chlorobenzene Toluene Benzene 1 2 4-Tr ich lorobenzene Acenaphthenc 24 Dinitrotoluene Di-n-Butylphthalate Pyrene

N-Nitroto-Di-fi-Propylamine 140ichlorobenzene Pentachlorophenol Phenol 2-Chlorophenol 4Chloro-3-Methylphenol 4-Nitrophenol Lindane Heptachlor Aldrin Dieldrin Endrin 44DDT

CONC SPIKE ADDED lugI

joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D

3L 4A3 ARshyAL A3 18shylS1A1

R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7

ÂSTERISKED VALUES ARE OUTSIDE QC LIMITS

RPO VOAs _ out of BN O out of mdashZ_ ACID -Q- out of J PEST ~~ out of mdashZ_

outside QC limits outside QC limits outside QC limits outside QC limits

RECOVERY VQAs ~ out oi-jL-BN A3 -out of Umdash ACID_pound2mdashout of 13 PEST _r out of


uOnvmnis

4M

ATTACHMENT II

TABLE 1 TCDD DATA REPORT FORI1 GZA

Report Date February 2 R 1986 Lab Roy F Weston

Column CP-SIL-88 Batch 8512-327

GCHS Analysis Rel Ion Relative Ion AbundanceAbundance SurroqateClient Sample Extra Aliquot TCDD Instr ur ur

Heas ID Date Time 320322 3323JT Acc 7ZT T77 Z57~ T7TID ID Cleanup ml

216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014

bullMatrix spiked with 2378 TCDD - 46 Recovery As surrogate and internal standards are both included in the same solution added to each sample before

extraction these extreme values may be due to matrix effects These samples are being re-extracted for repeat analysis

FB - Field BlankRB - Reagent Blank P - Partial ScanConfirmatory Analysis ND - Not Detected

DL - Detection LimitN - Native TCDD Spike D - DuplicateFortified Field Blank

Please Note Surroqate Recoveries have been corrected as described in the cover letter

SHEET o f

CLIENTSUBJECT yrKh SL c r wO NOshy

TASK NO_TASK DESCRIPTION

DEPT DATE APPROVED BYPREPARED BY DEPT DATE

DEPT DATE MATH CHECK BY

METHOD REV BY _v_ DEPT y DATECfY) o-lt rAA - twgt-bull fcdi-shOi-Y~rgt- 5 ~7cCo ALC-C vnmdash i poundVgtvO y S

(-u-mdashSC~t -ZZr-~mdash gtbull06 iyO v pound l0

JL J 3- e lto-joA -7 SO zb- poundamp ip Cje Ki je K ikaeftshy

3 ^ - 9 33 ^ 3 31

SJ2 pound 3 gltJ-O 5 r

Xl

laquoS raquov n r^ pound bull bull f o s - - ) amp _T32- V bull v 3 0

$3S-$ ^sO _ 0 3 ^ $r 2 0J I3) rsy3-c ^ C0AJCY~ JauCouL

C S ~ 7 amp amp s gt J azs-o

625-0^ x

0JY3 XV x y

A ~ bull ^ ^VLLcf mdash

bulloacot oa tgtue~gt CfVCpoundyylt A fr ~ stJUo yAA pound~ 2poundyiA bulllt-pound f 73

MIDRIC+MASS CHROHATOGRAM DATA 0216284 1 SCANS 300 TO 400 021686 174180 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONDS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 8 BASE U 28 3

347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME

SCANS 300 TO 409MIDRIC+MASS CHROMATOGRANS DATA 0216Z84 1 021686 174160 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1

DATA 0216Z84 1 CALI TC 3

MIDRIC+MASS CHROMATOGRAMS 021686 174100 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J

312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

MIDRIC+MASS CHROMATOGRAMS DATA 0216Z84 1 SCANS 300 TO 400 021686 174100 CALI TC 3 SAMPLE 2UL EX LAB SPIKING MIX CONOS DX RANGE G 1 407 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1

GZA (re-extractions)

Lab Roy F Weston

Batch 8512-327

GCMS Analysis Client Sample Extra Aliquot TCDD (ppb) Instr

ID ID Cleanup ml Meas D L ID Date Time

ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002

RB - Reagent Blank FB - Field Blank P - Partial ScanConfirmatory Analysis ND - Not Detected N - Native TCDD Spike OL - Detection Limit D - DuplicateFortified Field Blank

TCDD DATA REPORT FORM

Report Date February 29 1986

Column 30 meter DB-5

Rel Ion Abundance Surrogate

Acc 320 327 Relative Ion Abundance

321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628

TABLE 2 INITIAL CALIBRATION StMHAXY

TOD liOMr Resolution

Date laserXD

Sol IP

Measured RF Native Surrogate

Maan If Used Native Surrogate

Fercent Valley(Applies for FC only)

invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y

QUALITY CONTROL SUMMARY

Mean Accuracy Surrogate Measurements

Accuracy FortifiedSpike Field Blank

tel Biff (Z) Duplicate Analysis

mdash

of regftt

Saaple mdash

Saaple mdashtrademdash

Solution ID Codes

FCbullFerfotaance check solution CC1 - Concentration calibration solution 1bull 02 ugalCC2 Concentration calibration solution 2bull 10 ugalCC3 - Concentration calibration solution 3 raquo 50 uglCCA raquo Concentration calibration solution 4 - 200 ugalCCSbullConcentration calibration solution 5 raquo 00 ugal

IFB te 1B - 7 122983


MIORIC+MASS CHRONAT0GRAMS 021686 171500 SAMPLE 2UL CAL STD 1 CONDS DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME

MIDRIC+MASS CHRONATOGRAMS DATA 0216Z83 1 SCANS 300 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20

752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181

vQr mdash A A pound 5

1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500

Sbm yi Vpound^ rV =F IS

8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n

MIDRIC+MASS CHROMATOGRAMS 021686 171509 SAMPLE 2UL CAL STD 1 CONOS DX RANGE G 1 445 LABEL N -1 40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300

MIDRIC+MASS CHROMATOGRAM DATA 0216Z83 1 SCANS 380 TO 400 021686 171500 CALI TC 3 SAMPLE 2UL CAL STD 1 COW)S DX RANGE G 1 445 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680

MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 SCANS 300 TO 400 021686 165209 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20

987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy

MIDRIC+MASS CHROMATOGRAMS DATA 0216Z82 1 021686 165200 CALI TC 3 SAMPLE 2UL CAL STD 2 CONDS DX RANGE G 1 509 LABEL N -1 40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME

MIDRIC+MASS CHROMATOGRAMS 021686 165200 SAMPLE 2UL CAL STD 2 CONOS DX RANGE G 1 509 LABEL N -1

318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853

DATA 0216Z82 1 SCANS 300 TO 400 CALI TC 3

40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147

bull=r bull bull 214

377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME

MIDRIC+MASS CHROMATOGRAM DATA 0216Z82 1 021686 165280 CALI TC 3 SAMPLE 2UL CAL STD 2 COHOS DX RANGE G 1 589 LABEL N -1 40 QUAN A 1 10 J

SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1


MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c

MIDRIC+MASS CHROMATOGRAMS 021686 163200 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1 40

DATA 0216281 Ml CALI TC 3

QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME

MIDRIC+MASS CHRONATOGRAMS DATA 0216Z81 1 SCANS 390 TO 400 021686 163200 CALI TC 3 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 403 LABEL N -1 40 QUAN A 1 10 J 9 BASE U 29gt 3

963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME

MIDRIC+MASS CHROMATOGRAM 021686 163209 SAMPLE 2UL CAL STD 3 CONDS DX RANGE G 1 409 LABEL N -1

DATA 6216281 1 CALI TC 3

40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr

fllDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400

021686 161100 CALI TC 3 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378

MIDRIC+MASS CHROMATOGRAMS DATA 0216Z80 1 SCANS 300 TO 400 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N-l 48 QUAN A 1 10 J 0 BASE U 20

378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME

MIDRIC+MASS CHROMATOGRAMS DATA 0216280 1 SCANS 300 TO 408 021686 161180 CALI TC 3 SAMPLE 2UL CAL STD 4 CONOS DX RANGE G 1 408 LABEL N -1 48 QUAN A 1 10 J 0 BASE U 20

847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME

MIDRIC+MASS CHROMATOGRAM 021686 161100 SAMPLE 2UL CAL STD 4 CONDS DX RANGE G 1 408 LABEL N -1 40

DATA 0216Z80 tl CALI TC 3

QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC

360 V317 332 346 1247 983 854 720 6222 bull bull 3828 laquo 3282 145U 1

Imdash 1 rmdash r ~ I 380 400 SCAN360300 320 340

1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1


DATA 0216279 1 CALI IC 3

QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME

MIDRIC+MASS CHROMATOGRAM DATA 0216Z79 1shy SCANS 300 TO 400 021686 151400 CALI TC 3 SAMPLE 2UL CAL STD 5 CONOS DX RANGE G 1 426 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257

DATAJ 0216Z8S 1 CALI TC 3

MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1 40 QUAN A 1 10 J

310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1

MIORIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONOS DX RANGE G 1414 LABEL N -1


40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300

MIDRIC+MASS CHROMATOGRAMS 021686 183100 SAMPLE 2UL EX BLANK BATCH 373 CONDS DX RANGE G 1 414 LABEL N -1


40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j


MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1406 LABEL N -1 40 QUAN A 1 10 J

333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1

MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONDS DX RANGE G 1 406 LABEL N -1

323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1

MIDRIC+MASS CHROMATOGRAMS 021686 185800 SAMPLE 2UL 8512-327-0040102B CONOS DX RANGE G 1 406 LABEL N -1

322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033

392 9392 12688 -imdashmdashV

bull bull mdashJ

400 SCAN 1107 TIME

MIDRIC+MASS CHROMATOGRAMS DATA 8216287 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 28 3

331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1

8025b316 3613328819 85947662RIC 48691 bb4fcA 7664826466A A yv Avx r

3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME

MIORIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 300 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1 494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI

-4-poundpound -wwrv ^WxT7 T 300 328 340 360 380 400 SCAN820 853 927 1000 1033 1107 TIME

laquo raquo

MIDRIC+MASS CHROMATOGRAMS DATA 0216Z87 1 SCANS 308 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONDS DX RANGE G 1494 LABEL N -1 40 QUAN A 1 10 J 0 BASE U 20 3

377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME

MIDRIC+MASS CHROMATOGRAM DATA 8216Z87 1 SCANS 360 TO 400 021686 192000 CALI TC 3 SAMPLE 2UL 8512-327-0090101A CONOS DX RANGE G 1 494 LABEL N -1 40 QUAN A

377 1 10 J 0 BASE U 20 3

4808

Silresim Site Trustees - March 10 1986 File No A-405404 Page 2

and sampler blanks It is noted that both of these blanks were generated during sampling of MW-102B a location exhibiting eleyated levels of the same VOCs observed in the blanks this is believed to represent a worst case scenario with respect to potential sample cross contaminationby VOCs The contaminants found in the laboratory and trip blanks were notated within Westons Laboratory report additional VOCs found in field and sampler blanks will be similarly qualified in data entered into GZAs Data Base Management System

As noted in Westonscover letter sample aliquots for the baseneutral extractable pesticidePCB and TCDD fractions of well MW-105B were spiked with the standard spike mixture used by EPAs Contract Laboratory program - An unspiked aliquot of the sample was not analyzed however due to miscommunication between GZA and the laboratory Well MW-105B will therefore be resampled during the next scheduled groundwater sampling round and analyzed for the appropriate parameters

S h o u l d y o u h a v e a n y q u e s t i o n s o n t h e d a t a o r r e q u i r e a n y additional information please feel free to call

Very truly yours

GOLDBERG-ZOINO amp ASSOCIATES INC

2 Lawrence Feldmen

LFevm

GZ


Page 3

TABLE 1













GZ

28 February 1986


Dear Mr Lindberg










Very Truly Yours

ROY F WESTON INC

V1


CPNrost

A

RFWSN

8512-327-0010 -0020 -0030 -0040

- -0050 -0050 Dup-0060 -0070 -0090

-0050




Concentration (mgL)




Rec










i A A1 Pbdquo0pO


y [M-AP bdquoOOA


P A 4 0A6

00 40 () ( ) A ()

OAP


A T IPIx Ap 11ltE


069


0 A 4

lt 0 0 A lt 0 0 5 0 0 6


bdquo 2i0


bdquo P49




lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC




I1 IP TL ILiD B ANK



lt 0i0


lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2





020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P










lt00A lt 00A

-00 AG -7) OAK


430V7 c7






lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090





bdquo 4 4 4




bdquo P 07




PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57


SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


Page 3

TABLE 1













GZ

28 February 1986


Dear Mr Lindberg










Very Truly Yours

ROY F WESTON INC

V1


CPNrost

A

RFWSN

8512-327-0010 -0020 -0030 -0040

- -0050 -0050 Dup-0060 -0070 -0090

-0050




Concentration (mgL)




Rec










i A A1 Pbdquo0pO


y [M-AP bdquoOOA


P A 4 0A6

00 40 () ( ) A ()

OAP


A T IPIx Ap 11ltE


069


0 A 4

lt 0 0 A lt 0 0 5 0 0 6


bdquo 2i0


bdquo P49




lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC




I1 IP TL ILiD B ANK



lt 0i0


lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2





020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P










lt00A lt 00A

-00 AG -7) OAK


430V7 c7






lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090





bdquo 4 4 4




bdquo P 07




PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57


SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

28 February 1986


Dear Mr Lindberg










Very Truly Yours

ROY F WESTON INC

V1


CPNrost

A

RFWSN

8512-327-0010 -0020 -0030 -0040

- -0050 -0050 Dup-0060 -0070 -0090

-0050




Concentration (mgL)




Rec










i A A1 Pbdquo0pO


y [M-AP bdquoOOA


P A 4 0A6

00 40 () ( ) A ()

OAP


A T IPIx Ap 11ltE


069


0 A 4

lt 0 0 A lt 0 0 5 0 0 6


bdquo 2i0


bdquo P49




lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC




I1 IP TL ILiD B ANK



lt 0i0


lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2





020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P










lt00A lt 00A

-00 AG -7) OAK


430V7 c7






lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090





bdquo 4 4 4




bdquo P 07




PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57


SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808




Very Truly Yours

ROY F WESTON INC

V1


CPNrost

A

RFWSN

8512-327-0010 -0020 -0030 -0040

- -0050 -0050 Dup-0060 -0070 -0090

-0050




Concentration (mgL)




Rec










i A A1 Pbdquo0pO


y [M-AP bdquoOOA


P A 4 0A6

00 40 () ( ) A ()

OAP


A T IPIx Ap 11ltE


069


0 A 4

lt 0 0 A lt 0 0 5 0 0 6


bdquo 2i0


bdquo P49




lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC




I1 IP TL ILiD B ANK



lt 0i0


lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2





020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P










lt00A lt 00A

-00 AG -7) OAK


430V7 c7






lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090





bdquo 4 4 4




bdquo P 07




PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57


SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

A

RFWSN

8512-327-0010 -0020 -0030 -0040

- -0050 -0050 Dup-0060 -0070 -0090

-0050




Concentration (mgL)




Rec










i A A1 Pbdquo0pO


y [M-AP bdquoOOA


P A 4 0A6

00 40 () ( ) A ()

OAP


A T IPIx Ap 11ltE


069


0 A 4

lt 0 0 A lt 0 0 5 0 0 6


bdquo 2i0


bdquo P49




lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC




I1 IP TL ILiD B ANK



lt 0i0


lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2





020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P










lt00A lt 00A

-00 AG -7) OAK


430V7 c7






lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090





bdquo 4 4 4




bdquo P 07




PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57


SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808






i A A1 Pbdquo0pO


y [M-AP bdquoOOA


P A 4 0A6

00 40 () ( ) A ()

OAP


A T IPIx Ap 11ltE


069


0 A 4

lt 0 0 A lt 0 0 5 0 0 6


bdquo 2i0


bdquo P49




lt bdquo 0 P 0 NC

lt bdquo 0 P ( ) NC

lt bdquo 0 0 A NC

lt 0 P 0 AC

P 0 OP NC




I1 IP TL ILiD B ANK



lt 0i0


lt 0 P 0 ( ) -1 ( )

lt bdquo 0 P 0

lt 00 2 () ()

lt 0 bdquo 0 2





020 -104

00 A P P67

bdquo2P2 106

PA7 y iv v

bdquo P P P P P P










lt00A lt 00A

-00 AG -7) OAK


430V7 c7






lt bdquo P 0 NO

lt bdquo 005 NC

bdquo Jo-J NC

lt 00A NC

-bull006()-0070 -0090





bdquo 4 4 4




bdquo P 07




PIETHOD APIKIP

bdquo P22 i P2

420 P OA 2

P PS P P 57


SPIKE KEOOUFRY P 02

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

DB- G- I 0

jvj f p r n w






















FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808





FOR GZA


WO NO 0010-10-09


ugL MATRIX SP 05 05

ND ND UL ND

05

05 obsc

05 JUL

05 47

05 I D 05 To 60 1 0 ND 1 0 605 1 0 10 10 10 10 JZL 50 JUL 50 50

1 0 50 Ttr 50 50 50

TTTT 1 0


0050 B001A

12485 12685 121185

NP

1 0

0060 SB001 12485 IP685

121185

MM

iO

Approved By



ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


ROY F WESTON


FOR GZA


WO NO 0010-10-09



ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

ATTACHMENT I





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808





GZA





WORK ORDER it













SURROGATE RECOVERY


TOLUENE d8 109













DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808






DATE

DATE



DILUTION FACTOR I

PH NA Z MOISTURE NA

WORK ORDER Hbull


















SURROGATE RECOVERY
















WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808








WORK ORDER














56-23-5 10 U108-06-4 Vinyl Acetate


Total Xylenes 7 J

SURROGATE RECOVERY







ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

ROY F WESTON








WORK ORDER















SURROGATE RECOVERY










SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808




SAMPLE DESC Lab





WORK ORDER

CAS Number 74-67-3 74-83-9


ugKfl ^Circle OneI

10000 u 10000 u

CAS Number 78-67-5 10061-02-6



10000 u 10000 u

75-01-4 75-00-3

Vinyl Chloride

Chloroethine

10000 10000

u u

79-01-6 124-48-1


52000 l 0000 u

75-09-2 67-64-1 75-15-0 75-35-4 75-34-3

Methytene Chloride


200000 B 1200000

10000 u 860 J

10000 u

79-00-5 71-43-2 10061-01-5 110-75-8 75-25-2



8200 93000 10000 10000 10000

J

u u u

156-60-5 67-66-3


Chloroform

10000 3300

u J

591-78-6 106-10-1


2-Hexanone 29000 10000 u





106-06-4 75-27-4


10000 10000

U u

100-41-4

100-42-5


12000 700 J

Total Xylenes 29000

SURROGATE RECOVERY










RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808





RFV

DATE COLLECTED

8512-327-0050

DECEMBER k 1985

METHOD

DILUTION

MED

FACTOR

LEVEL

1

CLP (C i rc le 0


WORK ORDER H_








SURROGATE RECOVERY




















Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808














Total Xylenes 10 u

SURROGATE RECOVERY






DATE z z 8 r 6








WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808






WORK ORDER _














U

NR j B

-

---

NOT DETECTED



L IMIT

C0MMENT_



ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

ROY F WESTON






8 A I 7 - ^ 7 - n n q n

December k 1985

METHOD

DILUTION

LOW MED

FACTOR

LEVEL

000

CLP (C i rc le 0


WORK ORDER if

















SURROGATE RECOVERY











CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808




CLIENT



DATE

DATE

COLLECTED

ANALYZED

December

December

A 1985

17 1985

DILUTION FACTOR

PH NA

1

MOISTURE NA

WORK ORDER H












COMMENTNOT DETECTED


U




74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

74-87-3








WORK ORDER










SURROGATE RECOVERY













GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808






GCMS FILE NAME

MATRIX

METHOD

DETECTION LIMIT D F

LOWMED

0106B1603

Water

LEVEL CLP

10 ugLlx


















20-82-1


















D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808





D F UWORK ORDER



0 U 1-28-5 4-Dmitrophenol 50 U 06-95-2














120-82-1


















D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808




D F 1WORK ORDER






























98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808












98-95-3 78-59-1 Isophprone 1700





















MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808






MATRIX

METHOD

^

LOHMED

Water




D F l x io UgL







98-95-3 78-59-1 Ispphprpne











U = NR =


J B

= PRESENT = ANALYTE














































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808











































95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808









95-57-8


10 80


2 4-Dinitrophenpi

V 5 0 5 0

U U







106-44-5 621-64 7


100-01-6 534-52-1


5 0 U 5 0 U



88-75-5 05-67-9


1 0

1 0

U

U

(87-86-5 85-01-8


5 0 10

U u






106-47-8 87-68 3


1 0

1 0

U

U

B1-94-1 56-55-3


2 0 U 10 u
























95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808









95 57-8

106-95-2





























_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


_ Contract No




ttM TPAf rtc

laquoa iocuim -o

lt ltot I-iit)

IJ OICMLOHOshy

lrlaquo-IXI

NII40shyMNttNt-O


t-fLU00 bullIPHCNTL

( 4 9 shy

ItROK Ntinoi-M

3 3

I-Ill

(II-IMI

3 ~ T

(laquobullshy

AAA

Atrade

I M I W


6 6 3 0

^5 A2gt

Ay

AOshy

5 9

AbL S K

TV

3 0

AA

AAshy

oal

AL53shy

3

3LA yshy

rsb

y s

JSJL

-Al^

jIQJZJOL

06 fO 6 v b 0

9 6

VO

6 gt 6

O A

amp 0

y y

OSAA

_^Zi lt=A

o o

AlSL

6A yen

3AL S O 6 5 a-a

a o 9 a


Comments

cnou ii 7 8 6



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



FRACTION

bull VOA SMO

SAMPLE NO

BN SMO

SAMPLE NO

ACID SMO

SAMPLE NO

PEST SMO

SAMPLE NO

COMPOUND




joj

w wo

r

SAMPLE RESULT

to

CONC 0S

SJL JW 1SL 31

Ai2_ 21 AA J13 13 12 JUL

REC

33 1CL 33 13 88 ~Jo JR A332 1377 A3

CONCB S D


R E C

A3 13 12 82 81 AL A3 S3 AS 1SL 1L 3L

RPO

33 11 13

ILL

A3 12 _a_ 122Q

14 14 1 3

38 40 31 38

28 50 42 40 42 50 15 20 2 2 18 2 1 27

61145 7 1120 75 1 30

JJLX25shy76 127 39 98 46 1 18 24 96 1 1 1 1 7 2 6 1 2 7 4 1 1 1 6

36 97 9 1 0 3 12 89 2 7 1 2 3 23 97 10 90 56 123 4 0 1 3 1 40 1 20 52 1 26 5 6 1 2 1 3 8 1 2 7






uOnvmnis

4M

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

ATTACHMENT II






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808






216025 83648 110335 1000 ND 001 1786 1656 76 107Blank 220401 88792 109455

B102A 0030 1 1 55221000 HD 002 1786 1758 8 1 106 245328 891521786 1829 77 115B105A 0010 1000 ND 002 91259 116803166080 217809 75896 2291491000 46 1786 1859 76 78 106B105B 0020 002 266539 100061 133918

1000 HD 001 1886 924 75 109Blank 178124 64810 90092 B001A 0050 1000 ND 001 1086 955 72 110

227520 85379 107816 Blank 1000 ND 001 1886 1036 79 113

1 0279 124071000 ND 002 1886 1117 83 3400 582247

B102B 0040 283531 109447 1 45674106SB-001 0060 1000 ND 001 1 8 8 6 1152 75 1305 78 3700 1 563310 24031 30822

1886B-101A 0090 1000 ND 014






SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

SHEET o f








3 ^ - 9 33 ^ 3 31


Xl




625-0^ x

0JY3 XV x y




347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


347 698

1000n 827 698

323 323897 plusmn 0 580

379 14185 31027

14272

RIC

312 1962

11426 v-

T

338 560 2965

A

355 544 1060

^T y-v

mdashp_ TV- y

308 328 340 368 380 400 SCAN 828 8 53 927 1000 1033 1107 TIME


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


379 3812 10283

89li

332

379 4280 8420

1000-1

334

312 347 369336 291 188 181125 950 295 bull 382281

mdash I 379

14185 31927

3335-1

RIC 312

333 3551962 560 5441142b 2965 1060

300 320 340 360 380 820 853 927 1000 1033

3812

332099 plusmn 0500

4280

334100 plusmn 0500

14272

400 SCAN 1107 TIME

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

139-1



312 864 4568

0 BASE U 20

SCANS 300 TO 400

884

257 338 210 580

378 205 1209

257077 plusmn 0500

1000-|

379 6376 18358 6376

328 328098 plusmn 0500

311 343 361

281 255 442

743 701 2387 A =T

2238shy 14272

RIC 312 1962 338 355

11426 560 544 _---v 2965 1060 X bull bull i ^

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


310 342

1000n 1505 355

320 320096 plusmn 0500

854-i 303

322 322096 plusmn 0500

379 14185 31027

1427

R1C 312 1962 338 355

11426 560 544 2965 1060 S I I

I

300 320 349 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

ATTACHMENT III

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

TABLE 1


Lab Roy F Weston

Batch 8512-327



ND 002 4600Z 2-16-36 1831mdash Blank 1 0

ND 006 4600Z 2-16-86 185C102B 0040 1 0

4600Z 2-16-86 1920101A 0090 1 0 ND 002







321~257~ TIT 33

1 1 124 11870 5072 4651

96 69 15305 11060 11546

99 51 10356 28000 1 4628



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



Date laserXD

Sol IP




invk S ^ ~

V 7 8 mdash

J _ lt9 j f 3C

SO bullJ-J S S3

j y





mdash

of regftt

Saaple mdash


Solution ID Codes


IFB te 1B - 7 122983



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



SCANS 300 TO

BASE U 20 3

400

386-1 497

257 257077 plusmn 0500

1000-i 1286

328 328898 i 0500

378 15680 39342

15680

RIC

300 820

Q1 do lo 1026 6905

T 320 853

337 740 6319

340 927

3b0

4100

I 360

1000

I

~1 380

1033

394 622

2173

7 400 SCAN

1107 TIME


752shy 1386

320 313 331 347 365

320096 plusmn 0500

195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

322096 plusmn 0500


8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

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400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

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400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

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0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

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pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

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V vI N -vI


laquo raquo


377 5622

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332 332099

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377 3470

617-1 14628 3528

334 334100

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377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

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377 1 10 J 0 BASE U 20 3

4808


752shy 1386

320 313 331 347 365

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195 218 191 158 268 595595 t 543- 181


1000n 1844

322

305 153

247

316 229 1399

334 140 423

345 167

190

362 138 420

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8503-1 15680

RIC

318 360 1026 740 747 6905 6319 - - 4100

T 300 320 340 360 388 400 SCAN 828 853 927 1000 1033 1107 TIME

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

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332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

904n



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 5009 12945 5024

332 332093 plusmn 0500

1000n 5560

334 334100 plusmn 0500

2820mdash| 15680

RIC

400 SCAN 1107 TIME820

300


378 496

10001 1136 497

323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

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RIC

400 SCAN820 1107 TIME

300



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SCANS 300 TO

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400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

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1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

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1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


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2364

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929 634880 1476668

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RIC

306 61568

158436

316 221636 456328

r

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332 10048 42609 i

350 3136 18192

365 7616

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373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

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400

20288

332 366 4912

133461884b

379 5624 11060wo

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213-1 4320

334 334100 plusmn 0500

329 634880 1476660

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300 820

358 3136 10192

360 1000

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380 1033


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400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

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789i 4248

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377 17549

347 77420 13891 17600

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300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

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2723 7191

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377 17549

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300 820

316 8819 48691

A ft A

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377 1 10 J 0 BASE U 20 3

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378 496

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323 394 323097 172 plusmn 0500 667

378 15680 39342 15680


987-i 1768

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377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

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300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

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1000-1 6184

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377 25902 67237 25952

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300 820

317 1450 7098

1 320 853

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360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

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5016

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335 346 367

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377 25902 67237

25952

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303 1641 f

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1086

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365 71 147

I 377

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T 360 380 400 SCAN

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1000-1



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400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

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428-1 2636

328

308 224 710bull _

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377 c



QUAN A 1 10 J 0

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400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

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329 378 522

346 1374

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377 4938 11333

377 65216 146362

389 298 1041

389 280

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4768

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363

503

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360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

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400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

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378 60352

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320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

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317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

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5064

334

308 180 482

319 261 740

331 183

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347 168 527

360 216 913

390 171 846

334100 plusmn 0500

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317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

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336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

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377 400896

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SCANS 300 TO

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400

377 151552 266999 151552

320 320096

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1000-1

377 173054 332359 173056

322 322096

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2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

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400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

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376 5376 10204 5376

334

319 27 27 bull

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354 108

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377 400896 761478

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300 820

314 253 740

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359 454 1146

T 360

1000 380

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377 21440

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323 323997

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314 343 364

71 77 178

T 71 _

145 454 I

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RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

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377 2724 11870 2724

328 328898 plusmn 0500

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RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

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400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

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RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

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400

785shy 1748

332 332099 plusmn 0500

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336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

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0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

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306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


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400

2364

320 320096

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322 322096

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929 634880 1476668

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306 61568

158436

316 221636 456328

r

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332 10048 42609 i

350 3136 18192

365 7616

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373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

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300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


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400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

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789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

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332 332099

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377 3470

617-1 14628 3528

334 334100

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377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


987-i 1768

257 257077 plusmn 0500

1000n 1792

328 328098 plusmn 0500

377 25902 67237 25952

RIC

317 339 361 1450 331 303 7098 717 1641 laquo-raquo

T I i

300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1107 TIME

801shy


SCANS 300 TO

BASE U 20 3

400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

346 190 381

322096 plusmn 0500

4197-1

377 25902 67237 25952

RIC

300 820

317 1450 7098

1 320 853

339 331 7171 i

340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

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5792

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336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

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378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

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317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

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317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

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SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

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1000-1

377 173054 332359 173056

322 322096

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2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

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bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

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359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

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323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

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400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

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RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

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400

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332 332099 plusmn 0500

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334 334100 plusmn 0500

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400 SCAN820 1107 TIME

300

18-j



333 8267 16144

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0 BASE U 20 3 357

11124 18068

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257 306 3044 15960

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1000-1

323 606208 1367690

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306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

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1047-1

323 634880 1476660

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306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

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400

2364

320 320096

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1000-1 Oo6gt 3616

322 322096

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929 634880 1476668

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306 61568

158436

316 221636 456328

r

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332 10048 42609 i

350 3136 18192

365 7616

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373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

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300 820

358 3136 10192

360 1000

365 7616 27456

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380 1033


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400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

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789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

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bull n r y bull )

V vI N -vI


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377 5622

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377 3470

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334 334100

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377 17549

3077-1 347 77420 13891 17600

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300 820

316 8819 48691

A ft A

T 320 853

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80256

v v V v v

361 8594 76648

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340 927

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t t

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377 1 10 J 0 BASE U 20 3

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SCANS 300 TO

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400

378 4938

12923 4952

320

44

318 235 1131

T

346 203 501

320096 plusmn 0500

1000-1 6184

322

309 274 1222

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322096 plusmn 0500

4197-1

377 25902 67237 25952

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300 820

317 1450 7098

1 320 853

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340 927

361 303 1641

360 1000

380 1033

480 SCAN 1107 TIME


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

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40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

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335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

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pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

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332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


318 247 1418

386 317 252 157

465 shy 811 T

317 1450 7098

1 300 320 820 853


40 QUAN A 1 10 J 0 BASE U 20 3 377 5087 13833

5016

332099 plusmn 0500

335 346 367

128 176 217 247 415 573=rtrade

i 377 5792 14967

5792

334100 plusmn 0500

336 356 394 69 123 55 99 I 147


377 25902 67237

25952

333 361 331 717 I

303 1641 f

T I 7 340 360 400 SCAN 927 1000 1107 TIME


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

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332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

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789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

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bull n r y bull )

V vI N -vI


laquo raquo


377 5622

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332 332099

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377 3470

617-1 14628 3528

334 334100

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377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


SCANS 300 TO 400

BASE U 20 3

1086

323097 plusmn 0500

365 71 147

I 377

25902 67237 25952

T 360 380 400 SCAN

1000 1033 1107 TIME

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

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400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

1000-1



SCANS 300 TO

BASE U 20 3

400

378 6133 13810 6160

257 317 758 3307

3

347 290 1326

394 250 475

257077 plusmn 0500

428-1 2636

328

308 224 710bull _

328098 plusmn 0500

377 c



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 16883 40730 16928

320096 plusmn 0500

309 315

gt437

389 295 1240

377 26781 56466 26816

322096 i 0500

305 406 1188 bull

316 473

gt1-145

333 163 269

348 268 920

367 151 183

377 65216 146362

3shy

65216

316 329 346 363 2984 378 1374 508 1402 23257 522 5307 bull 954 bull 3378

T

300 320 340 360 400 SCAN 820 853 927 1000 1107 TIME


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


963-1

332

306 208 280

347 250 1167 zzz

1000-1

334

314 280 1070

329 159 159

FrE

347 212

bull 212

RIC

300 829

316 2984 23257

I 320 853

bull

329 378 522

346 1374

5307

340 927

363 184 486

377 4938 11333

377 65216 146362

389 298 1041

389 280

522

4768

332099 plusmn 0500

4952

334100 plusmn 0500

6521b

363

503

bull 954

360 1000

1

380 1033

389 1402 3378

490 SCAN 1107 TIME



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



40 QUAN A 1 10 J 8

SCANS 390 TO

BASE U 28 3

400

1000-i 4776

323 323097 plusmn 0500

377 65216 146362 65216

RIC

329 346 363 389 378 1374 508 1402

1 522

T 1 5307 954 3378

380 320 340 360 388 400 SCAN 820 853 927 1000 1033 1187 TIME

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

tr



378 22748 37045 22752

257077 plusmn 0500

317 335 346 360 370 392

500 228 161 165 151 202 3308 I

T I I 715 bull 299 323

T 504 649

1254

309 203 824A

332 210

485

345 171 494

362 300 637

390 211

1111

328098 plusmn 0500

izz

378


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


378 60352

1000-1 111640 60352

320 320096 plusmn 0500

316 332 360 234 328 217 910^ 775 1018

378 59520

986-1 134351 59520

322 322096 plusmn 0500

305 338 245 184 665 327j

378 152034

2520-1 324544

152064

RIC

317 OOi 346 360 1247 983 854 720 6222 3828 3282 - HSU

I 300 320 340 360 380 400 SCAN 820 853 927 1000 1033 1187 TIME


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


847n 4288

332

1000-1

311 342 1176

332 227 763

=F

344 213 213

366 237 378

377 5064 8861

389 191 1001

332099 plusmn 0500

5064

334

308 180 482

319 261 740

331 183

575 -mdash fw

I lt m M raquoTm

347 168 527

360 216 913

390 171 846

334100 plusmn 0500

152064

RIC

317 1247

332 983 3828

346 854 3282

360 720 145h

300 820

320 853

340 927

360 1000

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 10512 21422 10512

323037 plusmn 0500

305 171 702 bull

317 232

I335J

T

I i bull

336 270

i568 bull

346 236 710

378 152034 324544

390 195 457 J

152064

RIC



1000 1033 1107 TIME820 853 927

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

1000-1



QUAN A 1 10 J

SCANS 380 TO

BASE U 20 3

400

377 50496 90700 50496

257 257077 plusmn 0500

307 88 351

+

348 105 309

39-i 1970

328 328098 plusmn 0500

345 63 63

mdash _ I _ I laquo

377 400896

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

876-1



QUAN A 10 J 0

SCANS 300 TO

BASE U 20 3

400

377 151552 266999 151552

320 320096

plusmn 0500

1000-1

377 173054 332359 173056

322 322096

plusmn 0500

2317-n

377 409896 761478 400896

RIC

300 820

314O J

253 740

1 320 853

340 927

359 bull454 1146

360 1000

380 1033

400 SCAN 1107 TIME



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



QUAN A 1 10 J 0

SCANS 380 TO

BASE U 20 3

400

842-1 4528

332

314 63 63

346 96 184 bull

356 165

388 267 488

332999 plusmn 0500

10001

376 5376 10204 5376

334

319 27 27 bull

-3

354 108

204=

j

bull bull -c- I

377 400896 761478

388 213 1266

334100 plusmn 0500

400896

RIC

300 820

314 253 740

~7 320 853

~1 340 927

359 454 1146

T 360

1000 380

1033 400 SCAN

1107 TIME


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


377 21440

1000-1 48288

A 21440

323 323997

plusmn 0500

314 343 364

71 77 178

T 71 _

145 454 I

377 400896 761478 400896

RIC

359314 454253 1146 bull740

T ~11 400 SCAN300 320 340 360 380

1000 1033 1107 TIME820 853 927

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

403shy

257



310 1079 3102

346 490

3234

SCANS 300 TO

0 BASE U 20 3

359 565 3136

400

379 398 3155

1098

257077 plusmn 0500

1000shy

377 2724 11870 2724

328 328898 plusmn 0500

2749n 488

RIC

400 SCAN 1107 TIME820 853

300

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

672-1



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

378 603 1284

J- ( C O lt9 -5~

60 673

328 320036 plusmn 0500

1000-1 1002

322 322036 plusmn 0500

7473mdashi 488

RIC

400 SCAN820 1107 TIME

300



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808



40 QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

785shy 1748

332 332099 plusmn 0500

1000n 2228

334 334100 plusmn 0500

336 l-i 7488

RIC

400 SCAN820 1107 TIME

300

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

18-j



333 8267 16144

SCANS 300 TO

0 BASE U 20 3 357

11124 18068

400

11136

257 306 3044 15960

257077 plusmn 0500

1000-1

323 606208 1367690

606208

328

306 51072 105522

316 205824 385485

336 933 4267

351 537 924 j

379 5294 15305

392 8394 16868 bull bull

328098 plusmn 0500

1047-1

323 634880 1476660

634880

RIC

306 61568 158436

300 820

316 221696 45b38

332 10048 42600

~1 340 927

350 3136 16192

365 7616 27456

1 360

1060

bull

379 17287 72160 mdashj

380 1033

392 9392 12688

400 SCAN 1107 TIME

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

654-1


323 2364 9118

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

2364

320 320096

plusmn 0500

1000-1 Oo6gt 3616

322 322096

plusmn 0500

pound mdash

929 634880 1476668

634880

RIC

306 61568

158436

316 221636 456328

r

I V

332 10048 42609 i

350 3136 18192

365 7616

27456

373 17287 72160

392 9392 12688 bull bull

mdashT 340 360 380 400 SCAN820 927 1000 1033 1107 TIME

300

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

1000-1


322 20268 39800

40


QUAN A 1 10 J 0

SCANS 300 TO

BASE U 20 3

400

20288

332 366 4912

133461884b

379 5624 11060wo

332099 plusmn 0500

213-1 4320

334 334100 plusmn 0500

329 634880 1476660

634880

RIC

300 820

358 3136 10192

360 1000

365 7616 27456

379 17287 72160 ^

380 1033


bull bull mdashJ

400 SCAN 1107 TIME


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


331 5384

35615060 34310001 4429 53844892 8878 16564

257 257077

plusmn 0500

789i 4248

328 328098 plusmn 0500

377 17549

347 77420 13891 17600

3269-1


3 pound T

300 320 340 360 408 SCAN820 853 927 1000 1107 TIME


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


316 2304

626-1 14061 2668

320 320096 plusmn 0500

10001 4264375

2723 7191

322 322096 plusmn 0500

377 17549

347 77429 13891 17660 80256

4128shy

t316 3613328819 85947662RIC 48631 7664826466 IA

bull n r y bull )

V vI N -vI


laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808

laquo raquo


377 5622

1000H 28000 5720

332 332099

plusmn 0500

377 3470

617-1 14628 3528

334 334100

plusmn 0500

377 17549

3077-1 347 77420 13891 17600

RIC

300 820

316 8819 48691

A ft A

T 320 853

bullA 332 7662 26466 n

80256

v v V v v

361 8594 76648

V

i 1

340 927

360 1000

t t

AAA 400 SCAN

1107 TIME


377 1 10 J 0 BASE U 20 3

4808


377 1 10 J 0 BASE U 20 3

4808

Documents

JOHN.E^AYRES^^ 'JOSEPH D. GUERTIN; JR. GOLDBERG •ZOINO ... · Silresim Site Trustees -March 10, 1986 File No. A-4054.04 Page 2 and sampler blanks. It is noted that both of these