Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 11375 (1985): Groundnut Oil for Cosmetic Industry [PCD19: Cosmetics]

IS:11375 -1985

Indian Standard SPECIFICATION FOR

GROUNDNUT OIL FOR COSMETIC INDUSTRY

Cosmetics Sectional Committee, PCDC 19

Chairman

Dn S. S. GOTHOSKAR

Members

SARI C. D. ANAND

Representing

Directorate General of Health Services, New Delhi

Directorate General of Technical Development, New Delhi

SHRI N.K. AG~ARWAL ( Mternate) ASSISTANT DIRECTOR Food & Drug Administration, Maharashtra State,

Bombay DR P. D. PILANKAR ( Alternate )

SHRI B. S. BARVE Lakme Ltd, Bombay SHRI S. M. SHANBHAG ( Alternate )

DR S. G. BEAT The Tata Oil Mills Co Ltd, Bombay SHRI F. E. DARUWALLA ( Allernate )

DR D. CHHIB~A Hindustan Lever Ltd, Bombay SHRI R. GOVEBNOR ( Alternate)

SHRI V. G. DESEPANDF. Hindustan Ciba-Geigy Ltd, Bombay DR S. S. KARMARKAR ( Alternate )

DR A. S. DIVATIA Consumer Education and Research Centre, Ahmadabad

KUMARI RANI ADVANI ( Alternate ) SHRI S. M. MODY Johnson &Johnson Ltd, Bombay SHRIMATI T. JACOB Lady Irwin College, New Delhi SFIRI P. MAZUMDAR National Test House, Calcutta

SHRI P. K. CHAKRABORTY ( Alternate ) SHRI R. C. MEHTA Drugs Control Administration, Government of

Gujarat, Ahmadabad SHRI J. P. GANATRA ( Alternate )

SHRI A. MINHAZUDDIN Millet Rochas Pvt Ltd, Madras KUYARI NASRIN BEGAM ( Alternate)

DR S. S. NISHAT Hygienic Research Institute, Bombay SHRI KAILASH S. CHHABRA ( Alternate )

DR S. G. PATNEKAR Perfumes & Flavours Association of India, Bombay SRRI SGDHIR J AIN ( Alternate )

SHRI K. S. RAO Swastik Household and Industrial Products Pvt Ltd, Bombay

SIIRI C. R. KRISHNAMOORTHY ( Alternate)

( Continued on page 2 )

@ CopVright 1986

INDIAN STANDARDS INSTITUTION

This publication is protected under the Indian Copyright Act ( XIV of 1957 ) and reproduction in whole or in part by any means except with written permission of the publisher shall be deemed to be an infringement of copyright under the said Act.

IS:11375 - 1985

( Continued from page 1

Members

SHRI A. c. ROY

1

Rc/wasenting

Indian Soap and Toiletries Makers Association, Bombay

DR S.K. ROY Central Drugs Laboratory, Calcutta DR A.C. DAS GUPTA ( Alternate )

SHRI P. ROY Bengal Chemical & Pharmaceutical Works Ltd, Calcutta

DR A. N. BASU ( Alternate) SRRI V. SITARAM Basic Chemicals, Pharmaceuticals & Cosmetics

Export Promotion Council, Bombay SHRI I. SUNDARESH ( Alternate)

SHRIMATI USHA SUKTHANKAR Consuuier’s Guidance Society, Bombay SHRIMATI USRA KAMERKAR ( Alternate )

SRRI M.S. TRAKuR Godrej Soaps Ltd, Bombay SHRI N. G. IYER ( Alternate )

SRRIM.S.SAXENA, Director General, IS1 ( L%-o#cio Member ) Director ( P & C )

Secretary

( DR ) SHRIEJATI VIJAY MALIK Assistant Director ( P & C ), IS1

Raw Materials and GRAS List Subcommittee, PCDC 19 : 1

DR G. L. MADAN

Members

SIIRI D. CI~I~IBBA

Shaw Wallace & Co Ltd, Calcutta

SHRI R. GOVERNOR ( Alternate ) Hindustan Lever Ltd, Bombay

ASSISTANTGOMMISSIONER Food & Drug Administration, Maharashtra State, ( COSMETICS )

SENIOR SCIENTIFIC OFFICER Bombay

CLASS I ( CHEM ) ( Alternate ) SERI B. S. BARVE Lakme Ltd, Bombay

SHRI S. M. SHANBHAU ( Alternate ) DR S. G. BHAT The Tata Oil Mills Co Ltd, Bombay

SHRI F. E. DARUWALLA ( Alternate ) SHRI V. G. DESHPANUE SHRI J. P. GANATRA

Hindustan Ciba-Geigy Ltd, Bombay Drugs Control Administration, Gujarat State,

Ahmadabad SHRI R. D. DEODRAR ( Alternate )

SHRI S. M. MODY Johnson & Johnson Ltd, Bombay Srmr S. D. PARANJAPE ( Alternate )

SHRI K.S. RAO Swastik Household & Industrial Products Pvt Ltd, Bombay

SARI C. R. KRISHNAMOORTHY ( Alternate ) SHRI V. R. RATHI Sudershan Chemical Industries Ltd, Pune

SHRI U. N. LIMAYE ( Alternate )

( Continued on page 7 )

2

IS: 11375 -1985

Indian Standard SPECIFICATION FOR

GROUNDNUT OIL

0. F

FOR COSMETIC INDUSTRY

OREWORD

was adopted by the Indian Standards 0.1 This Indian Standard Institution on 15 October 1985, after the draft finalized by the Cosmetics Sectional Committee had been approved by the Petroleum, Coal and Related Products Division Council.

0.2 IS : 544-1968* covers number of grades used in a variety of industries. The present standard has been drawn up specifically to cater to the needs of the cosmetic industry.

0.3 Both the types of oil expressed and solvent extracted, are covered in the present standard. All other changes considered necessary to align the standard with others in the series for raw materials and finished cosmetics have been included.

0.4 For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, expressing the result of a test or analysis, shall be rounded off in accor- dance with IS : 2-19607. The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.

1. SCOPE

1.1 This standard prescribes the requjrements and the methods of sampling and test for groundnut oil for cosmetic industry.

2. TYPES

2.1 The material shall be of two types, namely:

Ty@e I - Refined oil, and

?YPe 2 - Raw expeller oil. -

*Specification for groundnut oil ( second revision ). +Rules for rounding off numerical values ( revised ).

3

IS:11375 - 1985

3. REQUIREMENTS

3.1 Description

3.1.1 TyFe 1 - The material shall be groundnut oil obtained from clean and sound groundnut ( Arachis hypogea Linn, fam. Leguminosae ) or good quality groundnut cake by a process of expression or solvent extraction using solvent hexane conforming to IS : 3470-1966*.

The oil shall be refined by neutralisation with alkali, bleached with bleaching earth or activated carbon or both, and deodorised with steam. The oil shall be practically odourless or have a very mild odour characteristic of groundnut oil.

3.1.2 Type 2 - The material shall be groundnut oil obtained from clean and sound groundnut ( rlrachis hypogea Linn, fam., Leguminosae ) by a process of expression. The oil shall have the characteristic odour of groundnut oil.

3.2 The material shall be clear and free from rancidity, adulterants, sediment, suspended and other foreign matter, separated water and added colouring and flavouring substances.

3.3 Admixture with Other Oils - The material shall be free from admixture with other oils when tested according to the methods prescribed in IS : 548 ( Part 2 )-19761.

3.4 The material shall also comply with the requirements given in Table’ 1.

4. PACKING

4.1 The TateriaI shall be supplied in suitable well-closed containers, which do not deteriorate the product, in quantities, as agreed to between the purchaser and the supplier.

5. MARKING

5.1 The containers shall be marked with the following:

a) Name and type of the material;

b) Manufactur’s name and/or his recognised trade-mark, if any;

c) Net mass of the material in the container;

d) Month and year of manufacture; and

e) Code number to enable the lot of manufacture to be traced back from records.

*Specification for hexane, food grade. tMethods of sampling and test for oils and fats: Part 2 Purity tests ( third revision ).

4

IS : 11375 - 1985

TABLE 1 REQUIREMENTS FOR GROUNDNUT OIL FOR COSMETIC INDUSTRY

( Clauses 3.4 and 7.1 )

SL CHARACTERISTIC REQUIREMENT FOR METHOD OF TEST NO. ~---__*__--~ CL REF TO

(1)

i)

ii)

Moisture and insoluble impurities, percent by mass, Max

Colour in a 1” cell on the Lovi- bond scale, expressed as

R (f&;iv~~~d~;ta;e$; than

Rtlative density at 30”/3O”C Saponification value Iodine value ( Wij’s ) Acid value, Max Unsaponifiable matter, percent

by mass, Max

Type 1 Type 2

(3) (4)

0.10 0.20

(5)

5 and 6 1

3 15

iii) iv) v)

vi) vii)

viii)

13 i of Is: 1 548 ( Part 1 l)- 1964’

10 > 11 I 15 I 14 I

ix) Bellier test ( Turbidity tem- perature )

I.4 620 to 1.4 640 0.909 to 0.913

188 to 196 G5 to 2.0 99

1.0 1.0

38°C to 38°C to 41°C 41°C

250 -

13 of IS : 548 (Part 2 )- 1976t

x)

xi)

Flash point, Pensky-Martens ( closed ) , “C, Min

Test for rancidity shall be free from rancidity

P: 21 of IS : 1448$

Appendix A

*Methods of sampling and test for oils and fats: Part 1 Sampling, physical and chemical tests ( revised ).

TMethods of sampling and tests for oils and fats: Part 2 Purity test ( third revision ). $Mehhods of test for petroleum and its products: Part 21 Flash point ( closed ) by

Pensky- Martens apparatus (first revision ).

5.2 In addition, words ‘NOT FOR DIRECT EDIBLE CONSUMPTION’ ( either printed on the label affixed to the container or lithographed or stencilled thereon with indelible ink ) in a type size of not less than 50 mm shall be marked.

5.2.1 The container may also be marked with the IS1 Certification Mark.

NOTE - The use of the IS1 Certification Mark is governed by the provisions of the Indian Standards Institution ( Certification Marks ) Act and the Rules and Regu- lations made thereunder. The IS1 Mark on products covered by an Indian Standard conveys the assurance that they have been produced to comply with the require- ments of that standard under a well-defined system of inspection, testing and quality control which is devised and supervised by IS1 and operated by the producer. IS1 marked products are also continuously checked by ISI for conformity to that standard as a further safeguard. Details of conditions under which a licence for the use of the IS1 Certification Mark may be granted to manufacturers or processors, may be obtained from the Indian Standards Institution.

5

IS : 11375 - 1985

6. SAMPLING

6.1 Representative samples of the material shall be drawn as prescribed under 3 of IS : 548 ( Part 1 )-1964*.

7. TEST

7.1 Tests shall be carried out as prescribed in IS : 548 ( Part 1 )-1964*, IS : 548 ( Part 2 ) 1976t and Part 21 of IS : 1448-1970: reference to which is given in co1 5 of Table 1.

7.2 Quality of Reagents - Unless specified otherwise, pure chemicals and distilled water (see IS : 1070-19775 ) shall be used in tests.

NOTE - ‘Pure chemicals’ shall mean chemicals that do not contain impurities which affect the results of analysis.

APPENDIX A [ Tuble 1, Item (I xi )]

A-l. TEST FOR RANCIDITY

A-l.1 Reagents

A-1.1.1 Phloroglucinol Solution - Dissolve 0-l g of phloroglucinol in 100 ml of diethyl ether.

A-l.2 Procedure - Shake 10 ml of the material, melt if necessary, with 10 ml of concentrated hydrochloric acid and 10 ml of phloroglucinol solution. Shake for 1 minute.

A-1.2.1 The material shall be taken to have passed the test if no pink colour develops.

- *Method of sampling and test for oils and fats: Part 1 Sampling, physical and

chemical tests ( revised ). $Method of sampling and test for oils and fats: Part 2 Purity test ( third revision ). $Methods of test for petroleum and its products: Part 21 Flask point ( closed ) by

Pensky-Martens apparatus (Jirst revision ). @pecification for water for general laboratory use ( second revision ).

6

IS:11375-1985

,( Continued from page 2 )

Members Representing

DR S. K. ROY Central Drugs Laboratory, Calcutta DR A. C. DAS GUPTA ( Alternate )

DR M. P. SAHAKARI Italab Pvt Ltd, Bombay SHRI M. R. PAREKH ( Aftcrnafc I ) SHRI K.S. SANTHANAM ( AfternateII)

DR N. D. SHAH Geoffrey Manners & Co Ltd, Bombay DR M. M. DOSEI ( Ahrnutc )

SERI NAVINOHANDRA R. SHAH Devarsons Pvt Ltd, Ahmadabad

SHRI VINODCHANDRA K. MEHTA ( Alternate ) SERI M. S. THAKUR Godrej Soaps Ltd, Bombay

SKRI N. G. DYER ( ADZ&)

INTERNATIONAL SYSTEM OF UNITS ( SI UNITS)

Base Units

QUANTITY

Length

Mass

Time

Electric current

Thermodynamic temperature

Luminous intensity

Amount of substance

Supplementary Units

QUANTITY

Plane angle

Solid angle

Derived Units

QUANTITY

Force

Energy

Power

Flux

Flux density

Frequency

Electric conductance

Electromotive force

Pressure, stress

UNIT

metre

kilogram

second

ampere

kelvin

cande!a

mole

UNIT

radian

steradian

UZIT

newton

joule

watt

weber

tesla

hertz

siemens

volt

Pascal

SYMROL

m

k

S

A

K

cd

mol

SYMBOL

rad

sr

SYMBOL

7

W

Wb

T

HZ

S

V

Pa

DEFINITION

1 N = 1 kg.m/s*

1 J = 1 N.m

1 W = 1 J/s

1 Wb = 1 V.s

1 T = 1 Wb/m’

1 Hz = 1 c/s (s-l)

I S = 1 A/V

1 V = 1 W/A

1 Pa = 1 N/m2

AMENDMENT NO. 1 JULY 2004TO

IS 11375:1985 SPECIFICATION FOR GROUNDNUTOIL FOR COSMETIC INDUSTRY

[ Page 5, Table 1 ] — Insert the following at the end of the table

(1) (2) (3) (4) (5)

xii) Peroxide value, meq/kg, Max 5.0 10.0 Annex B

( Page 6, Appendix A ) — Insert the following new Annex Bat the end:

ANNEX B[Table 1, S1 No. (xii)]

DETERMINATION OF PEROXIDE VALUE

B-1 REAGENTS

B-1.l Glacial Acetic Acid

B-1.2 Chloroform

B-L3 Saturated Potassium Idlde Solution

B-1.4 Sodium Thiosulphate — 0.01 N.

B-2 PROCEDURE

Weigh 5.0 + 0.5 g of the sample in a 250-ml glass-stoppered conical flask. Add30 ml of a mixture of 3 volumes glacial acetic acid and 2 volumes of chloroform.Swirl until dissolved, and add 0.5 ml of saturated potassium iodide solution.Allow to stand for exactly 1 rein, with occasional shaking, add 30 ml of water.Titrate gradually, with continuous and vigorous shaking, with 0.01 N sodiumthiosulphate solution until the yellow colour almost disappears. Add 0.5 ml ofstarch solution, continue the titration, shaking vigorously until the blue colourjust disappears (A). Carry out a blank determination under the same condh.ionwithout adding any sample (B). The volume of 0.01 N sodium thlosulphate inthe blank determination must not exceed 0.1 ml.

1

Amend No. 1 to IS 11375:1985

B-3 CALHJLATION

Calculate the peroxide value from the expression:

(A-B) ~ loPeroxide value = —

M

where

A = volume, in ml, of 0.01 N sodium thiosulphate required for titration;

B = volume, in ml, of 0.01 Nsodium thiosulphate required for blanktitration; and

M = mass in g of the sample.

.

[ PCD 19)

Reprography UniL BIS, New Delhi, India

2