24
3735 3049 2843 1661 1497 1434 1360 1283 1245 1216 1161 1119 1047 1018 962 865 803 748 709 642 600 539 600 800 1000 1200 1400 1600 1800 2000 2200 2400 2600 2800 3000 3200 3400 3600 3800 W avenum bercm -1 85 90 95 100 Transm ittance [% ] N N O O O trum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a).

IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

  • Upload
    leon

  • View
    37

  • Download
    5

Embed Size (px)

DESCRIPTION

IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a). 1 H NMR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a). Formula Weight = 374.432. - PowerPoint PPT Presentation

Citation preview

Page 1: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

3735

3049

2843

1661

1497

1434

1360

1283

1245

1216

1161

1119

1047

1018

962

865

803

748

709

642

600 53

9

600800100012001400160018002000220024002600280030003200340036003800Wavenumber cm-1

85

90

95

100

Tran

smitt

ance

[%]

Analytical Spectroscopy Laboratory EAC/SSH/VIT Univ. 4/5/2010 11:14:13 AM

N N

O

O

O

IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a).

Page 2: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

O

1H NMR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a).

Page 3: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

O

Formula Weight = 374.432

Mass spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a).

Page 4: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

Formula Weight = 374.4324

N N

O

O

O

HRMS spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a).

Page 5: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

3732

3645

3524

3462

3007

2387

2168

2115

1836

1664

1490

1413

1362

1303

1268

1228

1172

1088

1046

1007

967

901

852

791

746

687

635

592

553

522

600800100012001400160018002000220024002600280030003200340036003800Wavenumber cm-1

94

95

96

97

98

99

100

Tran

smitt

ance

[%]

Analytical Spectroscopy Laboratory EAC/SSH/VIT Univ. 4/5/2010 11:36:14 AM

N N

O

OO

O

IR spectrum of 1-acetyl-5-(2, 3, 4-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5b)

Page 6: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

OO

O

1HNMR spectrum of 1-acetyl-5-(2, 3, 4-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5b)

Page 7: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

Formula Weight = 404.458

N N

O

OO

O

Mass spectrum of 1-acetyl-5-(2, 3, 4-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5b)

Page 8: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

Formula Weight = 404.4584

N N

O

OO

O

HRMS spectrum of 1-acetyl-5-(2, 3, 4-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5b)

Page 9: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

Dr. techn. Murthy CHAVALI CNP 16

3791

3043 2990

2172

2118

1825

1655

1591

1508

1465

1413

1353

1320

1237

1179

1125

1070

1016

964

918

864

825

763

696

628

528

600800100012001400160018002000220024002600280030003200340036003800Wavenumber cm-1

92

93

94

95

96

97

98

99

100

Tran

smitt

ance

[%]

Analytical Spectroscopy Laboratory EAC/SSH/VIT Univ. 4/5/2010 11:57:49 AM

N N

O

OO

O

IR Spectrum of 1-acetyl-5-(2-naphthyl)-3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-pyrazole, (5c)

Page 10: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

OO

O

1H NMR Spectrum of 1-acetyl-5-(2-naphthyl)-3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-pyrazole, (5c)

Page 11: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

Formula Weight = 404.458

N N

O

OO

O

Mass Spectrum of 1-acetyl-5-(2-naphthyl)-3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-pyrazole, (5c)

Page 12: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

OO

O

Formula Weight = 404.4584

HRMS Spectrum of 1-acetyl-5-(2-naphthyl)-3-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-pyrazole, (5c)

Page 13: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

3440

3052

2173

1797

1663

1620

1508

1476

1416

1361

1307

1261

1209

1157

1126

1072

1034

959

913

856

821

746 63

259

055

5

600800100012001400160018002000220024002600280030003200340036003800Wavenumber cm-1

92

93

94

95

96

97

98

99

100

Tran

smitt

ance

[%]

Analytical Spectroscopy Laboratory EAC/SSH/VIT Univ. 4/5/2010 11:47:26 AM

N N

O

O

O

IR spectrum of 1-acetyl-5-(2,4-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5d).

Page 14: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

O

1H NMR spectrum of 1-acetyl-5-(2,4-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5d).

Page 15: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

O

Formula Weight = 374.432

Mass spectrum of 1-acetyl-5-(2,4-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5d).

Page 16: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

O

Formula Weight = 374.4324

HRMS spectrum of 1-acetyl-5-(2,4-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4d).

Page 17: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

Dr. techn. Murthy CHAVALI CNP 15

3792

3361

2996

2935 28

37

2313

1660

1512

1407

1359

1317

1279

1205

1151

1028

955

871

819

743

617

550

600800100012001400160018002000220024002600280030003200340036003800Wavenumber cm-1

70

75

80

85

90

95

100

105

Tran

smitt

ance

[%]

Analytical Spectroscopy Laboratory EAC/SSH/VIT Univ. 4/5/2010 12:14:15 PM

N N

O

O

OO

IR spectrum of 1-acetyl-5-(2, 4, 5-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4e).

Page 18: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

OO

1H NMR spectrum of 1-acetyl-5-(2, 4, 5-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4e).

Page 19: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

OO

Formula Weight = 404.458

MASS Spectrum of CNP 5

Mass spectrum of 1-acetyl-5-(2, 4, 5-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4e).

Page 20: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

OO

Formula Weight = 404.4584

HRMS spectrum of 1-acetyl-5-(2, 4, 5-trimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4e).

Page 21: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

3769

3006

1777

1664

1600

1517

1476

1424

1353

1295

1235

1210

1183

1155

1061

1017

990

964

926

899

844

821

759

694

647

603

545

600800100012001400160018002000220024002600280030003200340036003800Wavenumber cm-1

86

88

90

92

94

96

98

100

Tran

smitt

ance

[%]

Analytical Spectroscopy Laboratory EAC/SSH/VIT Univ. 4/5/2010 12:06:45 PM

N N

O

O

O

IR Spectrum of 1-acetyl-5-(3, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4f).

Page 22: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

N N

O

O

O

HNMR Spectrum of 1-acetyl-5-(3, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4f).

Page 23: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

MASS Spectrum of CNP 6

N N

O

O

O

Formula Weight = 374.432

Mass Spectrum of 1-acetyl-5-(3, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (4f).

Page 24: IR spectrum of 1-acetyl-5-(2, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5a)

HRMS Spectrum of 1-acetyl-5-(3, 5-dimethoxyphenyl)-3-(2-naphthyl)-4,5-dihydro-1H-pyrazole, (5f).

N N

O

O

O

Formula Weight = 374.4324