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Inventory
tag-out
Biodiesel Process Overview
Reactor
Glycerin
IsolatedShipment
Lot
Shippingsample/test
PurchasingInventory Production
SalesShipping
CustomerSupport
Purchase Order
Receiving
Receiving Inspection
per material spec
Method Cut Tank “I” Reactor
SourceReactor or Holding Tank
MWTMonomer
Weigh Tank
MethanolGlycerin Recovery
MethanolBulk Methanol
Biodiesel Recovery
Glyce
rin
Me
tha
no
l
Me
tha
no
l
Me
tha
no
l
Acid Wash
Ca
taly
st
Fe
ed
sto
ck
Mu
ltip
leB
atc
he
s
D6751
Reactor-F or I
Multiple BulkStorage Tanks
INSPECTION POINTS
ReceivingList
Checklistmaterial
dependent
Glycerin Demethylation
Glycerinsales or scrap
Biodiesel
CatalystSodium Methylate
Water
Step-01
Step-02
Demethylationof Biodiesel
Step-03
Water Wash
recovery
Step-04a
Step-04b
01-15-0002-03Page 1 of 5
3/27/07
Shipment Lot Inspect
Step-05
BatchFinal
DryStep-04c
FeedstockSoybean Oil
COA
References
1. Purchase Order
01-12-0005 Listing of Quality Records 19-02-0001 Receiving & Unloading Tanker Trucks
06-09-0001 Purchase Order Procedure 19-02-0009 Receiving & Unloading Railcars
06-12-0002 Purchase Order Form 19-02-0010 Shipping Product by Tanker or Railcar
2. Receiving
06-09-0001 Purchase Order Procedure 19-12-0004 Bulk Receiving Checklist
19-02-0001 Receiving & Unloading Tanker Trucks 19-12-0005 Inventory Checklist for Bulk Receiving
19-02-0009 Receiving & Unloading Railcars 19-12-0007 Daily Receiving Report Log
19-12-0003 Railcar Checklist (Ship & Receive)
3. Receiving Inspection
11-02-0002 QA Lab Specification Transmittal Sheet (except shipment samples) 11-11-0002 Lab Spec Methanol
11-02-0013 Work Instruction for Providing Samples to QA 11-11-0003 Lab Spec Sodium Methoxide
11-11-0001 Lab Spec Soybean Oil
4. Step 01 - Reactor
23-12-0001 “I” Reactor Log Sheet 11-11-0006 Lab Spec-”I” Reactor Demethylation of Glycerin
23-12-0002 “I” Reactor Demethylation Log Sheet 11-11-0010 Lab Spec-”I” Reactor (In-Process)
23-12-0003 “H” Reactor Log Sheet 11-13-0001 Batch Step 1-Biodiesel “I” Reactor
11-02-0006 Glycerin Determination in Reactor Sample 11-13-0011 Batch Step 1-Biodiesel “H” Reactor
11-02-0008 Test Method Oil in Glycerin 23-13-0002 Biodiesel, “I” Reactor SOP
11-11-0004 Lab Spec Reactor (In-Process) 23-13-0005 Biodiesel, “H” Reactor SOP
5. Step 02 - Glycerin
11-02-0009 K-F Water Determination Method 11-11-0011 Lab Spec-”F” Reactor Demethylation of Biodiesel
11-11-0006 Lab Spec-”I” Reactor Demethylation of Glycerin 11-13-0002 Batch Step 2-Biodiesel Glycerin
01-15-0002-03Page 2 of 5
References
6. Step 03 – Demethylation of Biodiesel
11-11-0006 Lab Spec-”I” Reactor Demethylation of Glycerin 23-12-0002 “I” Reactor Demethylation Log Sheet
11-11-0009 Lab Spec Demethylation of Biodiesel 24-12-0001 Cut Tank Log Sheet
11-13-0004 Batch Step 3-Biodiesel Demethylation by Cut Tank 24-13-0001 Cut Tank Demethylation Procedure
7. Step 04 – Blend Tank
11-11-0005 Lab Spec Blend (In-Process) 23-12-0006 Isolation of Bulk Tanks Ready for Shipment
11-13-0007 Batch Step 4-Biodiesel Wash by Blend Tank 23-13-0003 Recovery of Biodiesel from Water Wash
11-13-0012 Batch Card Citric Acid Solution 23-13-0004 Biodiesel Single or Double Water Wash SOP
11-13-0013 Batch Card Biodiesel from Water Wash
8. Step 05 – Shipment Lot
11-02-0002 QA Lab Specification Transmittal Sheet (except shipment samples) 11-02-0014 WI for Relative Density Determination
11-02-0011 Determining Significant Process Change 11-02-0015 WI for COA for Shipment of Biodiesel (D6751)
11-02-0012 Shipment Lot Tank Homogeneity 11-13-0006 Batch Step 5-Biodiesel Lot D6751 COA
11-02-0013 Work Instruction for Providing Samples to QA 23-13-0006 Isolation of Bulk Tanks Ready for Shipment
9. Shipment D6751
03-02-0001 Shipment & Billing of Finished Goods Procedure 11-11-0008 Lab-Ship Sample Test
03-12-0003 Open Sales Orders Form 19-02-0010 Shipping Product by Tanker or Railcar
11-02-0003 QA STS Definitions (for D6751 Shipment) 19-12-0006 Daily Shipping Report Log
11-02-0015 WI for COA for Shipment of Biodiesel (D6751) 19-02-0004 Pulling Samples from Tankers Loaded for
11-02-0016 WI for QA STS for Ship or Past 30 Days Sample Shipment
01-15-0002-03Page 3 of 5
Document Approvals
Role/Position
(Normative)
Owner:
(informational)
Approval Date
COO Bill McIlwain
CTO Terry Boone
Role/Position Reviewed By:
QA Ravi Doshi
HSE John Roberts
Purchasing Peggy Davis
Approved By:
Document Control Jan Rector
Instructions for filling out Document Approval Form1. Identify the owner of the document who has technical authority for content.2. Identify the authority required to review and approve (authority role).3. Identify who acts within required authority for this release.4. Approval date signifies that Document Control has received acceptance of approval.5. Document Control has structural control as defined in 01-01-0001 Preparation & Release of Controlled Documents.
01-15-0002-03Page 4 of 5
Revision HistoryDate Revision No. Modification Reason
10/31/06 00 Original issue
12/7/06 01 Multiple clerical updates.
1/12/07 02 Deleted tanks under Feedstock, added Tank 81; deleted tanks under Methanol
Glycerin Recovery and Biodiesel Recovery; updated doc. number for H Reactor BC;
Deleted inspection checkpoint under Glycerin.
3/27/07 03 Add References; deleted tank numbers & document numbers in flow chart.
01-15-0002-03Page 5 of 5