INTERNATIONAL COLLABORATIVE EXERCISES (ICE) · Mr. Scott Oulton, Drug Enforcement Administration, USA Ms. Catherine Quinn, Victoria Police, Australia Prof. Franco Tagliaro, University

INTERNATIONAL COLLABORATIVE

EXERCISES (ICE)

ICE

20

19

/2

Summary Report

ICE Round 2019/2

SEIZED MATERIALS

International Collaborative Exercises (ICE)

Summary report 2019/2-Seized Materials

Copyright © 2020 UNODC

Page 1 of 116

ICE 2019/2-SM

Final summary report for ICE 2019/2 Seized Materials Test Group

Original language: English

© United Nations, July 2020. All rights reserved, worldwide.

The designations employed and the presentation of material in this publication do not imply the expression of

any opinion whatsoever on the part of the Secretariat of the United Nations concerning the legal status of any

country, territory, city or area, or of its authorities, or concerning the delimitation of its frontiers or boundaries.

This publication has not been formally edited.




Page 2 of 116

ICE 2019/2-SM

Acknowledgements

The Laboratory and Scientific Section (LSS) of the UNODC, headed by Dr. Justice Tettey, wishes to express its

appreciation and thanks to all laboratories for participating in the International Collaborative Exercises (ICE)

round 2019/2.

The valuable comments and contribution from the following members of the International Panel of Forensic

Experts are gratefully acknowledged:

Mr. Benoit Archambault, Health Canada, Canada

Mr. Elvio Dias Botelho, Brazilian Federal Police, Brazil

Prof. Heesun Chung, Sungkyunkwan University, Republic of Korea

Prof. Niamh Nic Daéid, University of Dundee, Scotland, UK

Mr. Scott Oulton, Drug Enforcement Administration, USA

Ms. Catherine Quinn, Victoria Police, Australia

Prof. Franco Tagliaro, University of Verona, Italy

Dr. Angeline Tiong Whei Yap, Health Sciences Authority, Singapore

In addition, LSS would like to acknowledge the valuable contribution of the Chemical Metrology Laboratory of

the Health Sciences Authority, Singapore, for the provision of specific software used for the quantitative

statistical calculations in the ICE programme.

The ICE is coordinated by Ms. Yen Ling Wong, Scientific Affairs Officer, a staff member of LSS. The assistance

and the contributions of the following LSS staff members are gratefully acknowledged.

Dr. Conor Crean, Scientific Affairs Officer

Mr. Joao Rodrigues, Scientific Affairs Officer

Ms. Romana Luger, Research Assistant

Dr. Gerd Krapf, Laboratory Technician

Mr. Michael Bell, Laboratory Technician

Ms. Mikaela Edwards, Individual Contractor

For additional information or comments, please contact:

Ms. Yen Ling Wong

ICE Coordinator

Scientific Affairs Officer

Laboratory and Scientific Section

UNODC, Vienna International Centre

Wagramer Strasse 5, P.O. Box 500

A-1400, Vienna, AUSTRIA

Email: [email protected]




Page 3 of 116

ICE 2019/2-SM

Contents

1. Codes and Abbreviations ..............................................................................................................................4

2. Test samples information .............................................................................................................................5

3. Introduction ..................................................................................................................................................6

4. Comments from the International Panel of Forensic Experts ......................................................................7

5. New Psychoactive Substances (NPS) reported .............................................................................................9

6. Summary of responses for Test Sample-1 ................................................................................................. 11




10. ANNEX 1: Participants’ results for Test Sample-1 ..................................................................................... 27







Page 4 of 116

ICE 2019/2-SM

1. Codes and Abbreviations

(+) “positive” Indicates that the analyte is identified; for presumptive tests (e.g. colour reactions), indicates

that a positive reaction was obtained.

(-) “negative” Indicates that the analyte is not identified.

(ANP) Analysis not performed.

Tech Code Name

140 Colorimetric reactions

141 Marquis test

142 Cobalt thiocyanate test

150 Thin layer chromatography (TLC)

160 High/ultra high performance liquid chromatography with ultraviolet-visible spectroscopy (HPLC/UPLC)

161 High/ultra high performance liquid chromatography with diode array detection (HPLC-DAD or UPLC-DAD)*

170 Gas chromatography with nitrogen-phosphorous detection (GC-NPD)

171 Gas chromatography with flame ionization detection (GC-FID)

172 Gas chromatography with electron capture detection (GC-ECD)

180 Gas chromatography with mass spectrometry (GC-MS)

190 Fourier transform infrared spectrometry (FTIR)

200 Spectrophotometry (visible, UV)

210 Others

211 Nuclear magnetic resonance spectroscopy (NMR)

220 Microcrystal test

230 Liquid chromatography with mass spectrometry (LC-MS)

231 Liquid chromatography with tandem mass spectrometry (LC-MS/MS)

250 Raman spectroscopy

*similar to 160




Page 5 of 116

ICE 2019/2-SM

2. Test samples information

The following four (4) test samples for the Seized Materials test group were prepared by the Laboratory and

Scientific Section, UNODC:

Test Sample-1 (SM-1)

SM-1 was prepared from a seizure containing 13.6% (w/w) MDMA base.


SM-2 was prepared from a sample of Caffeine and Lactose.


SM-3 was prepared from a seizure containing 38.4% (w/w) Cocaine base. The test sample also contained traces

of benzoylecgonine, methylecgonine and tropacocaine.


SM-4 was prepared from a seizure containing 21.1 % (w/w) Heroin base. The test sample also contained 6-

acetylmorphine, acetylcodeine, caffeine, narcotine, papaverine, paracetamol and trace amounts of morphine.

All test samples were prepared by preliminary grounding by mortar and pestle followed by homogenisation

using a centrifugal mill and a dry powder rotator. An aliquot (230 mg) of each test samples were weighed into

glass vials.

For each test sample, sufficient homogeneity was assured and stability studies were carried out in accordance

with methods outlined in ISO 13258:2015 “Statistical methods for use in proficiency testing by interlaboratory

comparisons” and “The international harmonized protocol for the proficiency testing of analytical chemistry

laboratories”1.

____________________________________

1 Thompson, M., Ellison, S. L. and Wood, R., The International Harmonised Protocol for the Proficiency Testing of Analytical Chemistry Laboratories,

Pure Appl. Chem., 78 (1), 145-196, 2006.




Page 6 of 116

ICE 2019/2-SM

3. Introduction

An important element of the UNODC International Quality Assurance Programme (IQAP) is the

implementation of the International Collaborative Exercises (ICE). The exercises allow laboratories, from both

developing and developed countries to continuously monitor their performance in drug testing on a truly

global scale. This report provides information on analytical results of laboratories participating in the Seized

Materials (SM) test group. In order to maintain confidentiality, the participating laboratories have been

assigned random “Round Codes”, which change every round.

The analytical results returned by laboratories participating in ICE are evaluated by UNODC and a confidential

report is provided to each laboratory on its own performance. The overall analytical results are reviewed by

the UNODC’s International Panel of Forensic Experts which oversees the implementation of these exercises,

and offers guidance and support in addressing relevant quality issues. The exercises provide an overview of

the performance and capacity of participating laboratories and enable UNODC to tailor technical support in

the laboratory sector for greatest impact.

The ICE programme is a UNODC mandated activity and is implemented through regular budget funds and

through the UNODC Global Scientific and Forensic Programme – Support Project (GLOU54), which

operationalizes the forensic aspects of the UNODC Thematic Programme on Research, Trend Analysis and

Forensics". Figure 1 shows the growth of the programme in recent years for both the Seized Materials (SM)

and the Biological Specimens (BS) test groups.

Figure 1. Growth of the ICE programme (as of 4 June 2020)

6662

77

94100 102

116

129 132 131

151

159

179173

184 185

204 204 204

195

222

213

26 2733

4237

4754

6258

62

72 74

8690

9592

96 9793

87

101104

0

50

100

150

200

250

No

. o

f la

bo

rato

rie

s

ICE round

SM BS




Page 7 of 116

ICE 2019/2-SM

4. Comments from the International Panel of Forensic Experts

4.1 Participation of Laboratories in ICE round 2019/2

In the 2019/2 round of the ICE programme, results were submitted within both the Seized Materials (SM)

and Biological Specimens (BS) test groups by 258 laboratories in 77 countries. Within the SM test group,

there were 213 participating laboratories from 67 countries and within the BS test group, results were

submitted by 104 laboratories from 48 countries.

4.2 Qualitative Analysis

Colour tests (54% of participants) were the most commonly used screening technique for test samples in

the SM test group, while GC-MS (92% of participants) was the most commonly used technique for

identification/confirmation of the components in the test samples followed by FTIR (41% of participants).

The results for the qualitative identification of the controlled substances in the SM test group, the number

of false positive/negative results and the analyses not performed are shown in the Table 1.

Table 1. Performance of participants in the 2019/2 round of ICE.

Test sample SM-1

(MDMA)

SM-2

(Caffeine)

SM-3

(Cocaine)

SM-4

(Heroin)

Correct identification

by participants 98.6% 96.2% 100.0% 98.1%

Number of false

positives 6 3 3 7

Number of false

negatives 2 1 0 2

Number of analyses

not performed 1 7 0 2

With regard to false negative results reported, there were a total of 5 (2 for SM-1, 1 for SM-2 and 2 for SM-

4). As for false positive results, there were a total of 19 false positive results (6 for SM-1, 3 for SM-2, 3 for

SM-3 and 7 for SM-4), which is a decrease in number compared to the previous round. Laboratories

reporting false positive or false negative results should investigate the reasons for this and corrective

actions should be taken as soon as possible in order to continuously improve performance. There were a

total of 10 analyses not performed, the majority of which were for SM-2. ICE participants should note that

test samples can contain any of the substances in the ICE menu and screening and identification carried

out should take this into account.




Page 8 of 116

ICE 2019/2-SM

4.3 Quantitative Analysis

The number of participants who carried out quantitative analysis, 116 (54%) for SM-1, 137 (64%) for SM-3

and 123 (58%) for SM-4 continues to be encouraging. It is also encouraging that 141 (66%) participants in

the SM test group performed quantitation and of these, 128 (91%) quantified more than one substance

and 107 (76%) quantified all three test samples. It is understood that quantitative analysis of controlled

substances is often governed by local legislation and the requirements of prosecution. With regards to the

analytical techniques used by participants performing quantitation, 57% used GC-FID, 32% used

UPLC/HPLC-DAD and 20% used mass spectrometric methods (i.e. GC-MS, LC-MS, LC-MS-MS). z-Scores

obtained by participants in quantification are shown in Table 2 below.

Table 2. Quantitative performance of participants in the 2019/2 round of ICE.

According to the recommendations in ISO 13528:2015, an unacceptable z-score is considered to give an

action signal and a questionable z-score is considered to give a warning signal. A single action signal or

warning signals in two successive rounds shall be taken that an anomaly has occurred that requires

investigation. Participants with z-scores outside acceptable limits should review their quantification

procedures as soon as possible.

The following 15 laboratories obtained a single action signal or warning signal in the two successive rounds

of 2019/1 and 2019/2 and shall take this as an anomaly, which requires further investigation: 63AEKB,

64G4V7, 8IXSA9, 8SMOGU, AK3UYT, DTIACA, ELQO7L, ICNCMG, KPSSUB, MBWNRJ, MOGXMB, P8UQDW,

PKNKQN, TKLAER and V9FHUE.

Of the 22 laboratories that obtained a single action or warning signal in ICE rounds 2018/2 and 2019/1

reported in the previous summary report, 21 performed quantitation in 2019/2 and 9 of these improved

their performance in quantitation. The following 12 laboratories also obtained an action or warning signal

in 2019/2: 63AEKB, 64G4V7, 8IXSA9, AK3UYT, DTIACA, ELQO7L, ICNCMG, KPSSUB, MBWNRJ, PKNKQN,

TKLAER and V9FHUE.

Laboratories that need to perform quantitation routinely are encouraged to participate regularly in

external proficiency testing or collaborative exercises such as the ICE programme. This will enable

laboratories to assess the quality of their quantitative methods through the z-score values obtained. In

addition to the use of z-scores as a measure of performance in quantitation, participants are encouraged

to compare their results with the assigned values provided in individual quantification reports, to assess

the accuracy of their quantitative performance. Laboratories reporting false positive or false negative

results should investigate the root causes and corrective actions taken promptly in order to continuously

improve performance. Participation in the ICE programme also helps in monitoring the effect of corrective

actions.

z-score

Test sample

SM-1

(13.6% MDMA)

SM-3

(38.4% Cocaine)

SM-4

(21.1% Heroin)

|z| ≤ 2.00, acceptable 86.2% (100) 85.4% (117) 87.8% (108)

2.00 < |z| < 3.00, questionable 6.9% (8) 5.1% (7) 6.5% (8)

|z| ≥ 3.00, unacceptable 6.9% (8) 9.5% (13) 5.7% (7)




Page 9 of 116

ICE 2019/2-SM

5. New Psychoactive Substances (NPS) reported

During the 2019/2 round of ICE, participating laboratories provided information on NPS that had been

identified in their laboratories. In total there were 336 reports of 178 substances and the most

commonly reported substances were synthetic cathinones (31%) followed by synthetic cannabinoids

(26%) as shown in Figure 2.

Figure 2. Distribution of classes of NPS reported by ICE laboratories during the 2019/2 round of ICE

In terms of the mode of action of the NPS reported by ICE participants, the predominant substances

reported were stimulants (35%), while 25% were synthetic cannabinoid receptor agonists (SCRA) and

19% were hallucinogens as shown in Figure 3.

Figure 3. Distribution of NPS reported by ICE participants in the 2019/2 round of ICE according to the

mode of action

Synthetic

cannabinoids

26%

Synthetic

cathinones

31%

Other

substances

19%

Phenethylamines

13%

Phencyclidine-type

substances

6%

Tryptamines

5%

Synthetic cannabinoid

receptor agonists

25%

Stimulants

35%

Hallucinogens

19%

Opioids

3%

Dissociatives

6%

Sedatives/Hypnotics

7%

Others

5%




Page 10 of 116

ICE 2019/2-SM

The substances most often reported by ICE participants are listed in Table 3 below in descending order.

4F-MDMB-BINACA, 5F-MDMB-PICA and Etizolam were placed under international control at the 63rd

session of the Commission on Narcotic Drugs in March 2020 and these decisions will enter into force on

3rd November 2020.

Table 3. Most commonly reported NPS by laboratories participating in ICE 2019/2

Name Convention Schedule Effective date of

international control

4F-MDMB-BINACA

methyl 2-(1-(4-fluorobutyl)-1H-

indazole-3-carboxamido)-3,3-

dimethylbutanoate

1971 II 3rd November 2020

5F-MDMB-PICA

methyl 2-(1-(5-fluoropentyl)-1H-

indole-3-carboxamido)-3,3-

dimethylbutanoate

1971 II 3rd November 2020

Ketamine 2-(2-chlorophenyl)-2-

(methylamino)cyclohexan-1-one Currently not under international control

Etizolam

4-(2-chlorophenyl)-2-ethyl-9-

methyl-6H-thieno[3,2-f][1,2,4]-

triazolo[4,3-a][1,4]diazepine

1971 IV 3rd November 2020

For further details on these substances and others reported to the UNODC Early Warning Advisory, ICE

participants can log on to the UNODC ICE portal and select the icon for the Early Warning Advisory on

New Psychoactive substances as shown below.




Page 11 of 116

ICE 2019/2-SM

6. Summary of responses for Test Sample-1

The summary of responses of all 213 participating laboratories for the identification of SM-1:

Correct identification of Test Sample-1:

False positives for Test Sample-1 (technique(s) used):

False negatives for Test Sample-1 with respect to MDMA (technique(s) used):

Round Code Tech Code

PQCCII 150 RRQFQQ 190

Analysis not performed for Test Sample-1 with respect to MDMA:

Round Code

1MA9MF ANP

Frequency of use of screening, identification and quantification techniques:

Substance Name Number of laboratories Percentage

MDMA 210 98.6%

Round Code Substance Reported Tech Code

2UVXGU Cocaine, metamfetamine 150

DTIACA 4-Ethoxy-N-(1-

methylacetonitril)amphematine,

4-piperidnol, ethylamphetamine

171, 180

KFKUP0 2,3 -

Methylenedioxymethamphetamine*

171, 180

LKHTDW Metamfetamine 190, 250

PQCCII Metamfetamine 150

UYIOY3 Noscapine 180, 190

* possible transcription error

Test Sample-1: Response Summary

No of Participants: 213 (Qualitative); 116 (Quantitative)

Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 72 87 74 18 0 2 10 63 13 1 2 0 2 2 6

(%) 33.8 40.8 34.7 8.5 0.0 0.9 4.7 29.6 6.1 0.5 0.9 0.0 0.9 0.9 2.8

Identification

(No.

19 13 10 35 6 12 29 195 87 1 7 1 5 9 3

(%) 8.9 6.1 4.7 16.4 2.8 5.6 13.6 91.5 40.8 0.5 3.3 0.5 2.3 4.2 1.4

Quantification (No.) 0 0 0 0 6 30 59 14 0 0 0 2 1 2 0

(%) 0.0 0.0 0.0 0.0 5.2 25.9 50.9 12.1 0.0 0.0 0.0 1.7 0.9 1.7 0.0




Page 12 of 116

ICE 2019/2-SM

Z-Score Report per Sample per Substance:

Round: 2019/2

Substance: SM-1; MDMA

-4.95

-4.48

-2.74

-2.72

-2.72

-2.63

-2.10

-1.97

-1.66

-1.48

-1.48

-1.48

-1.48

-1.15

-1.13

-0.95

-0.95

-0.86

-0.86

-0.77

-0.77

-0.77

-0.76

-0.74

-0.71

-0.68

-0.68

-0.68

-0.68

-0.68

-0.59

-0.59

-0.59

-0.59

-0.59

-0.59

-0.59

-0.51

-0.42

-0.42

-0.33

-0.33

-0.31

-0.28

-0.17

-0.15

-0.15

-0.15

-0.15

-0.13

-0.10

-0.08

-0.07

-0.06

-0.06

-0.06

-0.01

0.00

0.01

0.03

0.03

0.03

0.04

0.12

0.12

0.12

0.17

0.20

0.20

0.20

0.20

0.29

0.29

0.29

0.29

0.29

0.29

0.29

0.29

0.38

0.38

0.40

0.40

0.43

0.47

0.51

0.56

0.56

0.65

0.74

0.74

0.75

0.83

0.83

0.91

0.91

0.91

0.91

1.03 1.18

1.18

1.18 1.36

1.36

1.71 1.93

1.98

2.24

2.63

2.74

5.08

6.50

7.48

9.75

16.26

17.77

-4.00

-3.00

-2.00

-1.00

0.00

1.00

2.00

3.00

4.00

AK3UYT

8SMOGU

NGJDWJ

PKNKQN

SDNBD6

48PXX4

BXCKYU

AA0UJR

TPYWQP

GYEHYL

K8NOCM

64G4V7

CBISZG

999RGV

RTQ8I7

DKW45M

KPSSUB

KUD7YD

3PP2PP

OHS9XX

VOFFDF

DZZZLS

VTNITG

LG1AMG

TKLAER

MUVGFL

7KCDRK

COVWOU

KAKGTD

MTWM6W

JMYLYJ

932LRK

9ABUAU

FFFLFF

E1ZARZ

IWWWZH

BCD9DP

CD5XF1

0GRT0S

AZBAGS

OEOJOY

VK9TBJ

GC11E1

NNNNEI

75XFMQ

KJFJIJ

6OTC3V

XSNN71

H7XE2X

GQPYLA

SOWSUC

UFS8L8

CAS0HP

7RURX8

YARNPI

F0RKYD

MJDOQK

61XYO6

ACYVYR

6GM1ZU

5CPBXX

AWGGYX

PLMLOM

JJPNJY

PRZOZC

8NKZIO

ELQO7L

FJF0IF

EI96ZN

UXPP39

MMVGH6

O1HUPW

P8UQDW

RCRHBM

LDLJZA

YY3YD4

FYKJPD

FEVFVO

WRVOXF

DCOHUX

VSIQQM

LUABFV

RZDHUH

9HXOHH

H9RHNG

PCQBJD

ZNRYRN

H12HE2

HASZSM

WU22AL

77JO7Q

RH2BU2

GPV0WG

9FFVN3

PXFATB

C11111

6AX4TV

OOWPNF

JVPB7L

YL6D6J

PPNIPX

QFFJPH

224V2J

WG1S1P

DJDDMD

DTIACA

QROQON

MJYQ1I

MBWNRJ

DSEBBS

V9FHUE

ICNCMG

MOGXMB

GIGQ0G

K6G1HJ

8IXSA9

Z-scores can be interpreted by participants in line with ISO 13528:2015*, section 9.4.2 as follows: IzI ≤ 2.00 is considered to be acceptable 2.00 < IzI < 3.00 is considered to be questionable (or warning signal) IzI ≥ 3.00 is considered to be unacceptable (or action signal)

A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred that requires investigation.

Robust mean: 13.7%

Robust SD: 1.13%

Robust CV%: 8.25%

UNODC value: 13.6%

Max reported: 33.7%

Min reported: 8.09%

No of labs: 116




Page 13 of 116

ICE 2019/2-SM





Page 14 of 116

ICE 2019/2-SM

Z-Scores for Test Sample-1

Code

MDMA

Code

MDMA

Concentration

(mass%)

Deviation

from robust

average

(mass%)

z-score Concentration

(mass%)

Deviation

from robust

average

(mass%)

z-score

AK3UYT 8.1 -5.6 -4.95 GC11E1 13.3 -0.4 -0.31

8SMOGU 8.6 -5.1 -4.48 NNNNEI 13.4 -0.4 -0.28

NGJDWJ 10.6 -3.1 -2.74 75XFMQ 13.5 -0.2 -0.17

PKNKQN 10.6 -3.1 -2.72 KJFJIJ 13.5 -0.2 -0.15

SDNBD6 10.6 -3.1 -2.72 6OTC3V 13.5 -0.2 -0.15

48PXX4 10.7 -3.0 -2.63 XSNN71 13.5 -0.2 -0.15

BXCKYU 11.3 -2.4 -2.10 H7XE2X 13.5 -0.2 -0.15

AA0UJR 11.5 -2.3 -1.97 GQPYLA 13.5 -0.2 -0.13

TPYWQP 11.8 -1.9 -1.66 SOWSUC 13.6 -0.1 -0.10

GYEHYL 12.0 -1.7 -1.48 UFS8L8 13.6 -0.1 -0.08

K8NOCM 12.0 -1.7 -1.48 CAS0HP 13.6 -0.1 -0.07

64G4V7 12.0 -1.7 -1.48 7RURX8 13.6 -0.1 -0.06

CBISZG 12.0 -1.7 -1.48 YARNPI 13.6 -0.1 -0.06

999RGV 12.4 -1.3 -1.15 F0RKYD 13.6 -0.1 -0.06

RTQ8I7 12.4 -1.3 -1.13 MJDOQK 13.7 0.0 -0.01

DKW45M 12.6 -1.1 -0.95 61XYO6 13.7 0.0 0.00

KPSSUB 12.6 -1.1 -0.95 ACYVYR 13.7 0.0 0.01

KUD7YD 12.7 -1.0 -0.86 6GM1ZU 13.7 0.0 0.03

3PP2PP 12.7 -1.0 -0.86 5CPBXX 13.7 0.0 0.03

OHS9XX 12.8 -0.9 -0.77 AWGGYX 13.7 0.0 0.03

VOFFDF 12.8 -0.9 -0.77 PLMLOM 13.7 0.0 0.04

DZZZLS 12.8 -0.9 -0.77 JJPNJY 13.8 0.1 0.12

VTNITG 12.8 -0.9 -0.76 PRZOZC 13.8 0.1 0.12

LG1AMG 12.8 -0.9 -0.74 8NKZIO 13.8 0.1 0.12

TKLAER 12.9 -0.8 -0.71 ELQO7L 13.9 0.2 0.17

MUVGFL 12.9 -0.8 -0.68 FJF0IF 13.9 0.2 0.20

7KCDRK 12.9 -0.8 -0.68 EI96ZN 13.9 0.2 0.20

COVWOU 12.9 -0.8 -0.68 UXPP39 13.9 0.2 0.20

KAKGTD 12.9 -0.8 -0.68 MMVGH6 13.9 0.2 0.20

MTWM6W 12.9 -0.8 -0.68 O1HUPW 14.0 0.3 0.29

JMYLYJ 13.0 -0.7 -0.59 P8UQDW 14.0 0.3 0.29

932LRK 13.0 -0.7 -0.59 RCRHBM 14.0 0.3 0.29

9ABUAU 13.0 -0.7 -0.59 LDLJZA 14.0 0.3 0.29

FFFLFF 13.0 -0.7 -0.59 YY3YD4 14.0 0.3 0.29

E1ZARZ 13.0 -0.7 -0.59 FYKJPD 14.0 0.3 0.29

IWWWZH 13.0 -0.7 -0.59 FEVFVO 14.0 0.3 0.29

BCD9DP 13.0 -0.7 -0.59 WRVOXF 14.0 0.3 0.29

CD5XF1 13.1 -0.6 -0.51 DCOHUX 14.1 0.4 0.38

0GRT0S 13.2 -0.5 -0.42 VSIQQM 14.1 0.4 0.38

AZBAGS 13.2 -0.5 -0.42 LUABFV 14.1 0.4 0.40

OEOJOY 13.3 -0.4 -0.33 RZDHUH 14.1 0.4 0.40

VK9TBJ 13.3 -0.4 -0.33 9HXOHH 14.2 0.5 0.43




Page 15 of 116

ICE 2019/2-SM

Code

MDMA

Concentration

(mass%)

Deviation

from robust

average

(mass%)

z-score

H9RHNG 14.2 0.5 0.47

PCQBJD 14.3 0.6 0.51

ZNRYRN 14.3 0.6 0.56

H12HE2 14.3 0.6 0.56

HASZSM 14.4 0.7 0.65

WU22AL 14.5 0.8 0.74

77JO7Q 14.5 0.8 0.74

RH2BU2 14.5 0.8 0.75

GPV0WG 14.6 0.9 0.83

9FFVN3 14.6 0.9 0.83

PXFATB 14.7 1.0 0.91

C11111 14.7 1.0 0.91

6AX4TV 14.7 1.0 0.91

OOWPNF 14.7 1.0 0.91

JVPB7L 14.8 1.1 1.03

YL6D6J 15.0 1.3 1.18

PPNIPX 15.0 1.3 1.18

QFFJPH 15.0 1.3 1.18

224V2J 15.2 1.5 1.36

WG1S1P 15.2 1.5 1.36

DJDDMD 15.6 1.9 1.71

DTIACA 15.9 2.2 1.93

QROQON 15.9 2.2 1.98

MJYQ1I 16.2 2.5 2.24

MBWNRJ 16.6 2.9 2.63

DSEBBS 16.8 3.1 2.74

V9FHUE 19.4 5.7 5.08

ICNCMG 21.0 7.3 6.50

MOGXMB 22.1 8.4 7.48

GIGQ0G 24.7 11.0 9.75

K6G1HJ 32.0 18.3 16.26

8IXSA9 33.7 20.0 17.77




Page 16 of 116

ICE 2019/2-SM




False positives for Test Sample-2 (techniques(s) used):

False negatives for Test Sample-2 with respect to Caffeine (technique(s) used):


AA0UJR 140, 171

Analysis not performed for Test Sample-2 with respect to Caffeine:

Round Code

1MA9MF ANP

KQKO2K ANP

OHNQ7X ANP

Q8ZQ82 ANP

RRQFQQ ANP

S0C00Z ANP

XO00Q0 ANP



Caffeine 205 96.2%

Lactose 100 46.9%


2UVXGU Ambien, piperidine,

hydrochlorothiazide

150, 190

AA0UJR 4-Bromo-2,5-

dimethoxyphenethylamine (2C-B)

141,171

INOP4F Ketamine 230



Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 72 87 74 18 0 2 10 63 13 1 2 0 2 2 6

(%) 33.8 40.8 34.7 8.5 0.0 0.9 4.7 29.6 6.1 0.5 0.9 0.0 0.9 0.9 2.8

Identification

(No.

19 13 10 35 6 12 29 195 87 1 7 1 5 9 3

(%) 8.9 6.1 4.7 16.4 2.8 5.6 13.6 91.5 40.8 0.5 3.3 0.5 2.3 4.2 1.4


(%) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0




Page 17 of 116

ICE 2019/2-SM





False negatives for Test Sample-3 with respect to Cocaine (technique(s) used):

There were no false negative results for SM-3

Analysis not performed for Test Sample-3 with respect to Cocaine:

All participating laboratories carried out analysis for Cocaine



Cocaine 213 100%


2UVXGU Noscapine 150

KQKO2K Amfetamine 231

NE8ZAO Caffeine 150, 180



Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 72 87 74 18 0 2 10 63 13 1 2 0 2 2 6

(%) 33.8 40.8 34.7 8.5 0.0 0.9 4.7 29.6 6.1 0.5 0.9 0.0 0.9 0.9 2.8

Identification

(No.

19 13 10 35 6 12 29 195 87 1 7 1 5 9 3

(%) 8.9 6.1 4.7 16.4 2.8 5.6 13.6 91.5 40.8 0.5 3.3 0.5 2.3 4.2 1.4


(%) 0.0 0.0 0.0 0.0 5.8 19.7 54.0 16.1 0.0 0.0 0.0 0.0 0.0 1.5 0.0




Page 18 of 116

ICE 2019/2-SM


Round: 2019/2

Substance: SM-3; Cocaine

-9.17

-6.25

-5.09

-3.72

-3.54

-3.46

-3.44

-2.67

-2.09

-2.08

-1.91

-1.87

-1.80 -1.58

-1.40

-1.30

-1.22

-1.11

-0.97

-0.87

-0.86

-0.86

-0.86

-0.86

-0.86

-0.79

-0.75

-0.75

-0.73

-0.72

-0.72

-0.68

-0.67

-0.66

-0.64

-0.63

-0.59

-0.59

-0.57

-0.54

-0.54

-0.53

-0.50

-0.50

-0.50

-0.41

-0.39

-0.36

-0.34

-0.32

-0.28

-0.28

-0.26

-0.21

-0.20

-0.17

-0.14

-0.14

-0.14

-0.14

-0.14

-0.14

-0.11

-0.10

-0.10

-0.10

-0.07

-0.03

-0.03

0.01

0.04

0.04

0.10

0.11

0.15

0.16

0.19

0.19

0.19

0.22

0.22

0.22

0.22

0.24

0.26

0.26

0.29

0.29

0.29

0.33

0.33

0.37

0.40

0.40

0.40

0.44

0.45

0.48

0.48

0.50

0.51

0.53

0.58

0.58

0.61

0.62

0.66

0.69

0.76

0.78

0.80

0.91

0.91

0.95

0.95

0.95

0.95

1.02

1.06 1.23

1.31

1.34

1.42 1.56 1.70

1.78

1.81

2.36 2.52

2.75

2.75

3.29

4.27

4.50

6.43

8.21

13.60

-4.00

-3.00

-2.00

-1.00

0.00

1.00

2.00

3.00

4.00

50AP5Y

AK3UYT

64G4V7

ZAZMLT

ZNRYRN

AMYZY0

DSEBBS

KKKQP7

KPSSUB

SOWSUC

JMYLYJ

OHS9XX

MJYQ1I

BCD9DP

8NKZIO

C11111

DJDDMD

YARNPI

GPV0WG

DCOHUX

UUNUSP

RZDHUH

HHEETQ

224V2J

CBISZG

F0RKYD

KUD7YD

48PXX4

PLMLOM

GIGQ0G

XSNN71

ICNCMG

GC11E1

7KCDRK

VTNITG

3PP2PP

MBWNRJ

LG1AMG

NNNNEI

PKNKQN

DKW45M

ACYVYR

PYUYVY

PPNIPX

WRVOXF

MJDOQK

AWGGYX

UXPP39

TKLAER

MTWM6W

FJF0IF

AZBAGS

999RGV

OEOJOY

61XYO6

KAKGTD

TPYWQP

FFFLFF

RCRHBM

5CPBXX

OOWPNF

FEVFVO

LUABFV

MUVGFL

HASZSM

VSIQQM

9FFVN3

A2HMLG

H7XE2X

OZOHOD

O1HUPW

QFFJPH

X1NYNN

7RURX8

QROQON

WU22AL

6OTC3V

RG5OYA

AA0UJR

NGJDWJ

AXAVAJ

9ABUAU

P8UQDW

JVPB7L

PCQBJD

VOFFDF

WKVSHN

KJFJIJ

932LRK

PXFATB

PRZOZC

ZPRDAZ

MWX4XX

MMVGH6

77JO7Q

YY3YD4

UFS8L8

6GM1ZU

H9RHNG

RH2BU2

JJPNJY

YL6D6J

DZZZLS

75XFMQ

63AEKB

JCJJVA

COVWOU

0GRT0S

6AX4TV

CAS0HP

BQNMYR

9HXOHH

ELQO7L

JJUJHH

E1ZARZ

VK9TBJ

GYEHYL

BXCKYU

I2TTTT

GQPYLA

LDLJZA

EI96ZN

B6H3ZH

8IXSA9

C5MOP5

H12HE2

WG1S1P

8SMOGU

UYIOY3

IWWWZH

FYKJPD

6ESG22

MOGXMB

SDNBD6

DTIACA

V9FHUE

K6G1HJ



Robust mean: 37.4%

Robust SD: 2.77%

Robust CV%: 7.40%

UNODC value: 38.4%

Max reported: 75%

Min reported: 12%

No of labs: 137




Page 19 of 116

ICE 2019/2-SM





Page 20 of 116

ICE 2019/2-SM


Code

Cocaine

Code

Cocaine

Concentration

(mass%)

Deviation

from robust

average

(mass%)

z-score Concentration

(mass%)

Deviation

from robust

average

(mass%)

z-score

50AP5Y 12.0 -25.4 -9.17 AZBAGS 36.6 -0.8 -0.28

AK3UYT 20.1 -17.3 -6.25 999RGV 36.7 -0.7 -0.26

64G4V7 23.3 -14.1 -5.09 OEOJOY 36.8 -0.6 -0.21

ZAZMLT 27.1 -10.3 -3.72 61XYO6 36.8 -0.6 -0.20

ZNRYRN 27.6 -9.8 -3.54 KAKGTD 36.9 -0.5 -0.17

AMYZY0 27.8 -9.6 -3.46 TPYWQP 37.0 -0.4 -0.14

DSEBBS 27.9 -9.5 -3.44 FFFLFF 37.0 -0.4 -0.14

KKKQP7 30.0 -7.4 -2.67 RCRHBM 37.0 -0.4 -0.14

KPSSUB 31.6 -5.8 -2.09 5CPBXX 37.0 -0.4 -0.14

SOWSUC 31.6 -5.8 -2.08 OOWPNF 37.0 -0.4 -0.14

JMYLYJ 32.1 -5.3 -1.91 FEVFVO 37.0 -0.4 -0.14

OHS9XX 32.2 -5.2 -1.87 LUABFV 37.1 -0.3 -0.11

MJYQ1I 32.4 -5.0 -1.80 MUVGFL 37.1 -0.3 -0.10

BCD9DP 33.0 -4.4 -1.58 HASZSM 37.1 -0.3 -0.10

8NKZIO 33.5 -3.9 -1.40 VSIQQM 37.1 -0.3 -0.10

C11111 33.8 -3.6 -1.30 9FFVN3 37.2 -0.2 -0.07

DJDDMD 34.0 -3.4 -1.22 A2HMLG 37.3 -0.1 -0.03

YARNPI 34.3 -3.1 -1.11 H7XE2X 37.3 -0.1 -0.03

GPV0WG 34.7 -2.7 -0.97 OZOHOD 37.4 0.0 0.01

DCOHUX 35.0 -2.4 -0.87 O1HUPW 37.5 0.1 0.04

UUNUSP 35.0 -2.4 -0.86 QFFJPH 37.5 0.1 0.04

RZDHUH 35.0 -2.4 -0.86 X1NYNN 37.7 0.3 0.10

HHEETQ 35.0 -2.4 -0.86 7RURX8 37.7 0.3 0.11

224V2J 35.0 -2.4 -0.86 QROQON 37.8 0.4 0.15

CBISZG 35.0 -2.4 -0.86 WU22AL 37.8 0.4 0.16

F0RKYD 35.2 -2.2 -0.79 6OTC3V 37.9 0.5 0.19

KUD7YD 35.3 -2.1 -0.75 RG5OYA 37.9 0.5 0.19

48PXX4 35.3 -2.1 -0.75 AA0UJR 37.9 0.5 0.19

PLMLOM 35.4 -2.0 -0.73 NGJDWJ 38.0 0.6 0.22

GIGQ0G 35.4 -2.0 -0.72 AXAVAJ 38.0 0.6 0.22

XSNN71 35.4 -2.0 -0.72 9ABUAU 38.0 0.6 0.22

ICNCMG 35.5 -1.9 -0.68 P8UQDW 38.0 0.6 0.22

GC11E1 35.5 -1.9 -0.67 JVPB7L 38.1 0.6 0.24

7KCDRK 35.6 -1.8 -0.66 PCQBJD 38.1 0.7 0.26

VTNITG 35.6 -1.8 -0.64 VOFFDF 38.1 0.7 0.26

3PP2PP 35.6 -1.8 -0.63 WKVSHN 38.2 0.8 0.29

MBWNRJ 35.8 -1.7 -0.59 KJFJIJ 38.2 0.8 0.29

LG1AMG 35.8 -1.6 -0.59 932LRK 38.2 0.8 0.29

NNNNEI 35.8 -1.6 -0.57 PXFATB 38.3 0.9 0.33

PKNKQN 35.9 -1.5 -0.54 PRZOZC 38.3 0.9 0.33

DKW45M 35.9 -1.5 -0.54 ZPRDAZ 38.4 1.0 0.37

ACYVYR 35.9 -1.5 -0.53 MWX4XX 38.5 1.1 0.40

PYUYVY 36.0 -1.4 -0.50 MMVGH6 38.5 1.1 0.40

PPNIPX 36.0 -1.4 -0.50 77JO7Q 38.5 1.1 0.40

WRVOXF 36.0 -1.4 -0.50 YY3YD4 38.6 1.2 0.44

MJDOQK 36.3 -1.2 -0.41 UFS8L8 38.6 1.2 0.45

AWGGYX 36.3 -1.1 -0.39 6GM1ZU 38.7 1.3 0.48

UXPP39 36.4 -1.0 -0.36 H9RHNG 38.7 1.3 0.48

TKLAER 36.4 -1.0 -0.34 RH2BU2 38.8 1.4 0.50

MTWM6W 36.5 -0.9 -0.32 JJPNJY 38.8 1.4 0.51

FJF0IF 36.6 -0.8 -0.28 YL6D6J 38.9 1.5 0.53




Page 21 of 116

ICE 2019/2-SM

Code

Cocaine

Concentration

(mass%)

Deviation

from robust

average

(mass%)

z-score

DZZZLS 39.0 1.6 0.58

75XFMQ 39.0 1.6 0.58

63AEKB 39.1 1.7 0.61

JCJJVA 39.1 1.7 0.62

COVWOU 39.2 1.8 0.66

0GRT0S 39.3 1.9 0.69

6AX4TV 39.5 2.1 0.76

CAS0HP 39.5 2.1 0.78

BQNMYR 39.6 2.2 0.80

9HXOHH 39.9 2.5 0.91

ELQO7L 39.9 2.5 0.91

JJUJHH 40.0 2.6 0.95

E1ZARZ 40.0 2.6 0.95

VK9TBJ 40.0 2.6 0.95

GYEHYL 40.0 2.6 0.95

BXCKYU 40.2 2.8 1.02

I2TTTT 40.3 2.9 1.06

GQPYLA 40.8 3.4 1.23

LDLJZA 41.0 3.6 1.31

EI96ZN 41.1 3.7 1.34

B6H3ZH 41.3 3.9 1.42

8IXSA9 41.7 4.3 1.56

C5MOP5 42.1 4.7 1.70

H12HE2 42.3 4.9 1.78

WG1S1P 42.4 5.0 1.81

8SMOGU 43.9 6.5 2.36

UYIOY3 44.4 7.0 2.52

IWWWZH 45.0 7.6 2.75

FYKJPD 45.0 7.6 2.75

6ESG22 46.5 9.1 3.29

MOGXMB 49.2 11.8 4.27

SDNBD6 49.8 12.4 4.50

DTIACA 55.2 17.8 6.43

V9FHUE 60.1 22.7 8.21

K6G1HJ 75.0 37.6 13.60




Page 22 of 116

ICE 2019/2-SM





False negatives for Test Sample-4 with respect to Heroin (technique(s) used):


PQCCII 150

RRQFQQ 190

Analysis not performed for Test Sample-4 with respect to Heroin:

Round Code

INOP4F ANP

KQKO2K ANP



Caffeine 184 86.4%

Heroin 209 98.1%

Paracetamol 160 75.1%


2UVXGU 2,5-Dimethoxyamfetamine,

hydrocodone, MDPV

150

LHOD3U Isoquinoline 180, 190

PLMLOM Hydromorphone 230, 231

PQCCII Amfetamine 150

Q8ZQ82 Lidocaine 150

UYIOY3 Morphinan-6-ol 180, 190

YYBTFT Lidocaine 150, 190


No of Participants: 213 (Qualitative); 123(Quantitative)

Technique 140 141 142 150 160 161 171 180 190 200 210 211 230 231 250

Screening (No.) 72 87 74 18 0 2 10 63 13 1 2 0 2 2 6

(%) 33.8 40.8 34.7 8.5 0.0 0.9 4.7 29.6 6.1 0.5 0.9 0.0 0.9 0.9 2.8

Identification

(No.

19 13 10 35 6 12 29 195 87 1 7 1 5 9 3

(%) 8.9 6.1 4.7 16.4 2.8 5.6 13.6 91.5 40.8 0.5 3.3 0.5 2.3 4.2 1.4


(%) 0.0 0.0 0.0 0.0 3.3 17.9 58.5 14.6 0.0 0.0 0.0 0.8 0.8 1.6 0.0




Page 23 of 116

ICE 2019/2-SM


Round: 2019/2

Substance: SM-4; Heroin

-5.36

-3.02

-2.94

-2.38

-1.66

-1.66

-1.66

-1.60

-1.43

-1.40

-1.32 -1.10

-1.06

-1.02

-1.02

-0.93

-0.93

-0.93

-0.85

-0.80

-0.80

-0.80

-0.72

-0.72

-0.68

-0.68

-0.68

-0.63

-0.59

-0.59

-0.55

-0.55

-0.55

-0.51

-0.51

-0.51

-0.49

-0.48

-0.44

-0.42

-0.38

-0.38

-0.38

-0.38

-0.38

-0.38

-0.38

-0.34

-0.34

-0.34

-0.33

-0.29

-0.29

-0.29

-0.29

-0.27

-0.25

-0.25

-0.22

-0.21

-0.21

-0.17

-0.17

-0.17

-0.17

-0.12

-0.12

-0.12

-0.12

-0.09

-0.08

-0.08

-0.04

0.05

0.06

0.07

0.09

0.11

0.11

0.13

0.15

0.39

0.39

0.43

0.47

0.47

0.47

0.47

0.47

0.47

0.51 0.73

0.76

0.81

0.81

0.86

0.86

0.90

0.90

0.98

0.98

1.03

1.07

1.10

1.15 1.32

1.32

1.32

1.64

1.75

1.75

1.88 2.09

2.17 2.32

2.37 2.56

2.94

3.79

3.88

4.07

4.27

10.60

-4.00

-3.00

-2.00

-1.00

0.00

1.00

2.00

3.00

4.00

CD5XF1

AK3UYT

63AEKB

PKNKQN

8IXSA9

LDLJZA

50AP5Y

DCOHUX

WU22AL

H12HE2

XSNN71

OEOJOY

NGJDWJ

MMVGH6

QROQON

EI96ZN

ZNRYRN

HASZSM

JCJJVA

HHEETQ

5CPBXX

CBISZG

3PP2PP

YARNPI

KUD7YD

KJFJIJ

AZBAGS

UXPP39

AWGGYX

VSIQQM

RZDHUH

DKW45M

OOWPNF

VTNITG

LG1AMG

77JO7Q

ACYVYR

YL6D6J

NNNNEI

ZAZMLT

H9RHNG

RCRHBM

KKKQP7

QFFJPH

FEVFVO

WRVOXF

BCD9DP

PXFATB

O1HUPW

KAKGTD

AA0UJR

JJPNJY

JMYLYJ

9FFVN3

CAS0HP

GQPYLA

6AX4TV

RH2BU2

GC11E1

7RURX8

MJDOQK

VOFFDF

BXCKYU

YY3YD4

B6H3ZH

OHS9XX

0GRT0S

VK9TBJ

PPNIPX

LUABFV

MUVGFL

48PXX4

I2TTTT

PYUYVY

GPV0WG

JVPB7L

UFS8L8

TPYWQP

CDVNVK

A2HMLG

61XYO6

FJF0IF

GIGQ0G

6OTC3V

JJUJHH

9ABUAU

7KCDRK

COVWOU

IWWWZH

FYKJPD

WG1S1P

MTWM6W

9HXOHH

6GM1ZU

8NKZIO

C11111

MJYQ1I

PRZOZC

FFFLFF

64G4V7

75XFMQ

932LRK

UUNUSP

PCQBJD

DJDDMD

E1ZARZ

GYEHYL

F0RKYD

DSEBBS

AXAVAJ

DTIACA

C5MOP5

ELQO7L

P8UQDW

PLMLOM

TKLAER

SDNBD6

KPSSUB

ICNCMG

K6G1HJ

MBWNRJ

8SMOGU

V9FHUE



Robust mean: 18.9%

Robust SD: 2.35%

Robust CV%: 12.4%

UNODC value: 21.1%

Max reported: 43.8%

Min reported: 6.3%

No of labs: 123




Page 24 of 116

ICE 2019/2-SM





Page 25 of 116

ICE 2019/2-SM


Code

Heroin

Code

Heroin

Concentration (mass%)

Deviation from robust

average (mass%)

z-score Concentration (mass%)


average (mass%)

z-score

CD5XF1 6.3 -12.6 -5.36 KKKQP7 18.0 -0.9 -0.38

AK3UYT 11.8 -7.1 -3.02 QFFJPH 18.0 -0.9 -0.38

63AEKB 12.0 -6.9 -2.94 FEVFVO 18.0 -0.9 -0.38

PKNKQN 13.3 -5.6 -2.38 WRVOXF 18.0 -0.9 -0.38

8IXSA9 15.0 -3.9 -1.66 BCD9DP 18.0 -0.9 -0.38

LDLJZA 15.0 -3.9 -1.66 PXFATB 18.1 -0.8 -0.34

50AP5Y 15.0 -3.9 -1.66 O1HUPW 18.1 -0.8 -0.34

DCOHUX 15.1 -3.8 -1.60 KAKGTD 18.1 -0.8 -0.34

WU22AL 15.5 -3.4 -1.43 AA0UJR 18.1 -0.8 -0.33

H12HE2 15.6 -3.3 -1.40 JJPNJY 18.2 -0.7 -0.29

XSNN71 15.8 -3.1 -1.32 JMYLYJ 18.2 -0.7 -0.29

OEOJOY 16.3 -2.6 -1.10 9FFVN3 18.2 -0.7 -0.29

NGJDWJ 16.4 -2.5 -1.06 CAS0HP 18.2 -0.7 -0.29

MMVGH6 16.5 -2.4 -1.02 GQPYLA 18.3 -0.6 -0.27

QROQON 16.5 -2.4 -1.02 6AX4TV 18.3 -0.6 -0.25

EI96ZN 16.7 -2.2 -0.93 RH2BU2 18.3 -0.6 -0.25

ZNRYRN 16.7 -2.2 -0.93 GC11E1 18.4 -0.5 -0.22

HASZSM 16.7 -2.2 -0.93 7RURX8 18.4 -0.5 -0.21

JCJJVA 16.9 -2.0 -0.85 MJDOQK 18.4 -0.5 -0.21

HHEETQ 17.0 -1.9 -0.80 VOFFDF 18.5 -0.4 -0.17

5CPBXX 17.0 -1.9 -0.80 BXCKYU 18.5 -0.4 -0.17

CBISZG 17.0 -1.9 -0.80 YY3YD4 18.5 -0.4 -0.17

3PP2PP 17.2 -1.7 -0.72 B6H3ZH 18.5 -0.4 -0.17

YARNPI 17.2 -1.7 -0.72 OHS9XX 18.6 -0.3 -0.12

KUD7YD 17.3 -1.6 -0.68 0GRT0S 18.6 -0.3 -0.12

KJFJIJ 17.3 -1.6 -0.68 VK9TBJ 18.6 -0.3 -0.12

AZBAGS 17.3 -1.6 -0.68 PPNIPX 18.6 -0.3 -0.12

UXPP39 17.4 -1.5 -0.63 LUABFV 18.7 -0.2 -0.09

AWGGYX 17.5 -1.4 -0.59 MUVGFL 18.7 -0.2 -0.08

VSIQQM 17.5 -1.4 -0.59 48PXX4 18.7 -0.2 -0.08

RZDHUH 17.6 -1.3 -0.55 I2TTTT 18.8 -0.1 -0.04

DKW45M 17.6 -1.3 -0.55 PYUYVY 19.0 0.1 0.05

OOWPNF 17.6 -1.3 -0.55 GPV0WG 19.0 0.1 0.06

VTNITG 17.7 -1.2 -0.51 JVPB7L 19.1 0.2 0.07

LG1AMG 17.7 -1.2 -0.51 UFS8L8 19.1 0.2 0.09

77JO7Q 17.7 -1.2 -0.51 TPYWQP 19.2 0.3 0.11

ACYVYR 17.8 -1.2 -0.49 CDVNVK 19.2 0.3 0.11

YL6D6J 17.8 -1.1 -0.48 A2HMLG 19.2 0.3 0.13

NNNNEI 17.9 -1.0 -0.44 61XYO6 19.3 0.4 0.15

ZAZMLT 17.9 -1.0 -0.42 FJF0IF 19.8 0.9 0.39

H9RHNG 18.0 -0.9 -0.38 GIGQ0G 19.8 0.9 0.39

RCRHBM 18.0 -0.9 -0.38 6OTC3V 19.9 1.0 0.43




Page 26 of 116

ICE 2019/2-SM

Code

Heroin

Concentration (mass%)


average (mass%)

z-score

JJUJHH 20.0 1.1 0.47

9ABUAU 20.0 1.1 0.47

7KCDRK 20.0 1.1 0.47

COVWOU 20.0 1.1 0.47

IWWWZH 20.0 1.1 0.47

FYKJPD 20.0 1.1 0.47

WG1S1P 20.1 1.2 0.51

MTWM6W 20.6 1.7 0.73

9HXOHH 20.7 1.8 0.76

6GM1ZU 20.8 1.9 0.81

8NKZIO 20.8 1.9 0.81

C11111 20.9 2.0 0.86

MJYQ1I 20.9 2.0 0.86

PRZOZC 21.0 2.1 0.90

FFFLFF 21.0 2.1 0.90

64G4V7 21.2 2.3 0.98

75XFMQ 21.2 2.3 0.98

932LRK 21.3 2.4 1.03

UUNUSP 21.4 2.5 1.07

PCQBJD 21.5 2.6 1.10

DJDDMD 21.6 2.7 1.15

E1ZARZ 22.0 3.1 1.32

GYEHYL 22.0 3.1 1.32

F0RKYD 22.0 3.1 1.32

DSEBBS 22.8 3.9 1.64

AXAVAJ 23.0 4.1 1.75

DTIACA 23.0 4.1 1.75

C5MOP5 23.3 4.4 1.88

ELQO7L 23.8 4.9 2.09

P8UQDW 24.0 5.1 2.17

PLMLOM 24.3 5.4 2.32

TKLAER 24.5 5.6 2.37

SDNBD6 24.9 6.0 2.56

KPSSUB 25.8 6.9 2.94

ICNCMG 27.8 8.9 3.79

K6G1HJ 28.0 9.1 3.88

MBWNRJ 28.5 9.6 4.07

8SMOGU 28.9 10.0 4.27

V9FHUE 43.8 24.9 10.60




Page 27 of 116

ICE 2019/2-SM

10. ANNEX 1: Participants’ results for Test Sample-1

Identified substances for Test Sample 1

Code Identified Substances

AM777O 3,4-Methylenedioxymetamfetamine (MDMA)

AMYZY0 MDMA

AWGGYX MDMA

AXAVAJ MDMA

AZBAGS MDMA HCl

B3D1SD MDMA

B6H3ZH 3,4MDMA

BCD9DP MDMA

BD556C MDMA

BQNMYR MDMA

BXCKYU MDMA

C11111 3,4-methylenedioxymethamphetamine (MDMA)

C5MOP5 MDMA

C8CCX2 3,4-Methylenedioxymetamfetamine (MDMA)

CAS0HP MDMA

CBISZG MDMA

CD5XF1 3,4-methylenedioxymetamfetamine (MDMA)

CDVNVK 3,4-methylenedioxymethamphetamine

CILAEB MDMA

COVWOU MDMA

CXQPFE MDMA

D67Z7M MDMA

DCOHUX MDMA

DJDDMD 3,4- Methylenedioxymetamfetamine

DK6FK1 3,4-MDMA

DKW45M MDMA

DSEBBS N-Methyl-3,4-methylenedioxyamphetamine (MDMA)

DTIACA 3,4-Methylenedioxymetamfetamine (MDMA)

DZZZLS MDMA

E1ZARZ 3,4-Methylenedioxymetamfetamine (MDMA)

EI96ZN MDMA 13,9%

EIHUWT amphetamines

ELQO7L 3,4-Methylenedioxymethamfetamine (MDMA)

F0RKYD MDMA

FCGG7O 3,4-methylenedioxymetamfetamine

FEVFVO MDMA

FFFLFF MDMA




Page 28 of 116

ICE 2019/2-SM


FJF0IF 3-4-MDMA

FXP8PV 3,4-Methylenedioxymetamfetamine (MDMA)

FYKJPD MDMA

G6GBTW 3,4-Methylenedioxymetamfetamine (MDMA)

GC11E1 MDMA

GDI9LV 3,4-methylenedioxymethamphetamine (MDMA)

GGGPGE MDMA

GHKHWC MDMA

GIGQ0G MDMA

GIZGWR MDMA

GPV0WG MDMA

GQPYLA 3,4-methylenedioxymethamphetamine (MDMA)

H12HE2 MDMA

H7XE2X MDMA

H9RHNG 3,4-Methylenedioxymetamfetamine (MDMA)

HANMLJ MDMA and LACTOSE

HASZSM MDMA

HHEETQ MDMA

I2TTTT MDMA

I4IIIW 3,4-Methylenedioxymetamfetamine (MDMA)

ICNCMG MDMA

IE8EEE 3,4-Methylenedioxymetamfetamine (MDMA)

IIIDYX MDMA

INOP4F 3,4-methylenedioxyamphetamine

IRZAFP MDMA

IWWWZH 3,4-methylenedioxymethamphetamine (MDMA)

JCJJVA MDMA

JJPNJY MDMA

JJUJHH MDMA

JMYLYJ MDMA

JVPB7L MDMA HCl

K6G1HJ MDMA

K8IZ1S 3, 4-metilendioxymetamfetamine (MDMA)

K8NOCM MDMA

KAKGTD MDMA

KFKUP0 MDMA

KJFJIJ MDMA

KKKQP7 MDMA

KLCHRH MDMA

KPSSUB MDMA, GLUCOSE AND STARCH

KQKO2K MDMA

KUD7YD MDMA




Page 29 of 116

ICE 2019/2-SM


L9WDPM MDMA

LDLJZA MDMA (3,4-methylenedioxymethylamphetamine)

LG1AMG MDMA

LHOD3U 3,4-Methylenedioxymetamfetamine (MDMA)

LKHTDW 3,4-methylenedioxymethamphetamine (MDMA) and Methamphetamine

LUABFV MDMA

LVRMSV MDMA

LVUH0Z MDMA

MBWNRJ MDMA

MIIFIV 3,4-Methylenedioxymethamphetamine

MJDOQK 3,4-METHYLENEDIOXYMETHYLAMPHETAMINE HYDROCHLORIDE (MDMA)

MJYQ1I MDMA

MMVGH6 MDMA

MOGXMB MDMA

MTWM6W MDMA

MUVGFL MDMA

MWX4XX MDMA

NE8ZAO MDMA

NGJDWJ MDMA

NNNNEI MDMA

O1HUPW MDMA CLORHIDRATO

OEOJOY MDMA

OHNQ7X MDMA

OHS9XX MDMA

OOWPNF 3,4-methylenedioxymethamphetamine

OZOHOD 3,4-MDMA

P8UQDW MDMA

PCQBJD 3,4-Methylenedioxymetamfetamine hydrochloride(MDMA)

PFZFOJ MDMA (3,4-METHYLENE DIOXY METHAMPHETAMINE)

PKNKQN MDMA

PLMLOM MDMA

PPNIPX MDMA

PQCCII Methamphétamine

PXAOXX 3,4 Methylenedioxymetamfetamine (MDMA)

PXFATB MDMA

PYUYVY MDMA

Q8ZQ82 3,4-Methylenedioxy-metamphetamine (MDMA)

QBIV4X 3,4-methylenedioxymethamphetamine (MDMA)

QFFJPH MDMA HCL

QROQON 3,4-Methylenedioxymethamphetamine (MDMA)

RCRHBM MDMA

RG5OYA 3,4-Methylenedioxymetamfetamine (MDMA)




Page 30 of 116

ICE 2019/2-SM


RH2BU2 MDMA

RTQ8I7 3,4-Methylenedioxymetamfetamine (MDMA)

RZDHUH 3,4-MDMA

S0C00Z 3,4-Methylenedioxy-metamfetamine (MDMA)

SDNBD6 AMFETAMINE TYPE STIMULANTS

SFS5SX MDMA

SOWSUC MDMA

STNCC9 MDMA

SVRSSF 3,4-Methylenedioxymetamfetamine

TBUBCR MDMA

TBYTGT MDMA and Glucose

TE8ERE 3,4-Methylenedioxy-metamfetamine (MDMA)

TFF5SF 3,4-Methylenedioxymetamfetamine (MDMA)

TFKFT5 MDMA

TKLAER MDMA

TPYWQP MDMA HCl

UFS8L8 MDMA

UUNUSP MDMA

UXPP39 MDMA

UYH68O 3,4 Methilenedioxy-metamfetamine (MDMA)

UYIOY3 3,4-Methylenedioxymetamfetamine (MDMA)

V9FHUE MDMA

VJJ2BS 3,4-Methylene dioxymethamphetamine (MDMA)

VK9TBJ MDMA

VOFFDF 3,4-methylendioxymethamphetamine

VOFIVV 3,4-Methylenedioxy-metamfetamine (MDMA)

VSIQQM MDMA

VTGLIP MDMA

VTNITG MDMA HCL

WCDCCS MDMA

WG1S1P MDMA

WKVSHN MDMA

WLWWWW MDMA

WRVOXF 3,4-methylenedioxymetafetamine (MDMA)

WU22AL 3,4-MDMA

X1NYNN 3,4-Methylenedioxymetamfetamine (MDMA)

XO00Q0 3,4-Methylenedioxymetamfetamine

XSNN71 MDMA

Y5OQGB MDMA (3,4-Methylenedioxymetamphethamine)

YARNPI MDMA

YL6D6J MDMA

YY3YD4 MDMA




Page 31 of 116

ICE 2019/2-SM


YYBTFT MDMA + DEXTROSE

ZAZMLT MDMA

ZNRYRN MDMA

ZPRDAZ 3,4-Methylenedioxymetamfetamine (MDMA)




Page 32 of 116

ICE 2019/2-SM

Statement of findings for Test Sample 1

Code 3,4-Methylenedioxymetamfetamine (MDMA)

06JS66 + The sample was subjected to HPTLC using silicagelF254 as stationary phase and Ethylacetate:Methanol:Ammonia 85:10:5 as MP. A single spot was obtained after development. It was scanned and the UV Spectrum obtained was compared with the Library UV Spectrum and was found matching with MDMA and MDEA. The analysis was repeated using MDMA reference material. The RF and UV Spectra were found matching. Then the sample was subjected to GC-MS after subjecting to alkaline extraction using sodium hydroxide and ether. The ether layer is collected and ether evaporated at room temperature. The drug is dissolved in methanol and made upto 1ml. 100mg. of the sample is taken for extraction. GC-MS was performed using general method for basic drugs on HP5 column. MDMA reference material was also injected and the RT and Mass spectra compared and were found matching. It was also matched with library spectra and was found matching with MDMA. Therefore MDMA is confirmed in SM1. It is further subjected to Marquis test, Simons test and Galic acid test and gave positive results.

0GRT0S + MDMA was detected by GC-MS and quantified by GC-FID

111NTK + It was found glucose

1MA9MF ANP

224V2J +

2HSS8S + The sample contains MDMA. The concentration has not been determined.

2JJWOJ + The white powder was analysed and found to contain Methylenedioxymethylamphetmaine (MDMA).

2UVXGU + the main compounds we found in SM-1 are metamphetamine, MDMA, cocaine after TLC . Excess compounds are in the trace state.

3PP2PP + The sample is a powder containing MDMA hydrochloride at 12.7% purity

48PXX4 +

4BVR3P + The sample is in the form of white fine powder. It answers the test for the presence of MDMA

50AP5Y +

5CPBXX + MDMA is controlled by the law of 7th February 2014 and the RD of 6th September 2017

60N30D + Sample SM-1 was found to contain 3,4-methylenedioxymetamfetamine (MDMA)

61XYO6 + MDMA is sheduled as illicit drug in France

63AEKB +




Page 33 of 116

ICE 2019/2-SM


64G4V7 + The sample contains MDMA and Lactose as adulterant. MDMA is controlled substance in Poland

6AX4TV + The sample contains MDMA, glucose and saccharose. MDMA is scheduled as illicit drug in France

6ESG22 +

6GM1ZU +

6OTC3V + It has been detected the presence of 3,4-Methylenedioxymetamfetamine (MDMA) in the sample.

75XFMQ +

77JO7Q +

7KCDRK + MDMA + glucose

7RURX8 +

7WIJ9N + Detected MDMA.

8IXSA9 + SM1 was containe 33.7% MDMA

8NKZIO +

8SMOGU + a substance identified is MDMA

932LRK +

9969TL + Using the techniques CR, TLC, FT-IR, GC-FID & GC-MS, sample SM-1 was found to contain MDMA.

999RGV + List I of the Convention on Psychotropic Substances of 1971

9ABUAU +

9FFVN3 + MDMA IN DEXTROSE POWDER

9HXOHH + The sample SM-1 contains MDMA 14.16 % m/m and glucose.

9N59BB + Offwhite powder containing MDMA.

9OO999 + White powder that contains controlled substance MDMA.

9OS0B5 +




Page 34 of 116

ICE 2019/2-SM


A2HMLG + mdma

AA0UJR + negative

ACYVYR +

AK3UYT +

AM777O + Test sample 2019/2/SM-1 was found to contain 3,4-Methylenedioxymetamfetamine (MDMA), confirmed by Gas Chromatography - Mass Spectrometry.

AMYZY0 + For presumptive tests a positive Marquise reaction was obtained. GC/MS fragmentation pattern obtained with sample SM 1 are equivalent to those obtained with MDMA. The sample also contains dextrose wich was determined by FTIR.

AWGGYX + The sample was found to contain 13.7% of MDMA (as base).

AXAVAJ + MDMA is the common name for methylenedioxymethylamphetamine. It is a Class Acontrolled drug subject to the provisions of the Misuse of Drugs Act 1971 as it is structurally derived from N-alkyl- alpha-methylphenethylamine by substitution in the ring with an alkylenedioxy substituent.

AZBAGS + glucose

B3D1SD + MDMA was examined in SM-1.

B6H3ZH + CHLORHYDRATE MDMA + GLUCOSE

BCD9DP + MDMA hydrochloryde (13 % base), glucose and saccharose.

BD556C + Test Sample SM-1 found to contain MDMA

BQNMYR + The sample was analysed with colorimetric test, FTIR and GCMS in two different columns and solvents

BXCKYU +

C11111 + SM-1 sample includes 3,4-methylenedioxymethamphetamine (MDMA). there is not adulterant.

C5MOP5 + White powder containing MDMA and glucose and traces of sucrose

C8CCX2 + Test sample 2019/2/SM-1 having gross weight 05.93 gram(s) of white powder in amber glass bottle contains 3,4-Methylenedioxymetamfetamine (MDMA- A psychotropic substance) as defined in the Section 2 of the CNS Act 1997 - Pakistan.

CAS0HP + this sample is MDMA




Page 35 of 116

ICE 2019/2-SM

Code 3,4-Methylenedioxymetamfetamine(MDMA)

CBISZG + The powder was found to contain METHYLENEDIOXYMETHYLAMPHETAMINE at a concentration of (as amended) 12 per cent. MDMA is controlled under the Misuse of Drugs Act 1971 (as amended) as a Class A drug.

CD5XF1 + Sample 2019/2/SM-1 was found to contain 13.1 % of 3,4- methylenedioxymetamfetamine (MDMA)

CDVNVK + 3,4-methylenedioxymethamphetamine

CILAEB + MDMA - confirmed with GCMS, FTIR, LC Glucose - confirmed with FTIR and Wohlk reaction

COVWOU + Identified by GC-MS and GC-FID techniques and quantified by GC-FID technique.

CXQPFE +

D67Z7M + MDMA was identified in the sample 2019/2/SM1. First, colormietric test and Finally GC-MS.

DCOHUX +

DJDDMD + Presence of 3,4-Methylenedioxymetamfetamine hydrochloride and glucose was detected in the sample.

DK6FK1 + THE SAMPLE 2019/2/SM1 WAS FOUND 3,4 METYLENDIOXYMETAMFETAMINE MDMA

DKW45M + It is usually detected drug in seized drugs analyzed in our laboratory

DSEBBS + MDMA was identified with a retention time of 7.177 min by GC/MS. The concentration of sample injected in CG/MS was 202 ppm.

DTIACA + the sample contains MDMA , glucose, 4-ethoxy-N-(1-methylacetonitril)amphematine, 4-piperidnol, ethylamphetamine

DZZZLS + In the 2019/2/SM-1 was proved the presence of 3,4-Methylenedioxymetamfetamine (MDMA) with a quantification as base of 12,8%

E1ZARZ + Sample contains 13% MDMA.

EI96ZN + THE SAMPLE CONTAIN LACTOSE

EIHUWT + MDMA

ELQO7L + MDMA was identified by GC/MS and TLC; quantified by GC (FID)

F0RKYD + SM1 contient du Methylenedioxyamfetamine

FCGG7O + The sample contains the substance 3,4-methylenedioxymetamfetamine (MDMA).




Page 36 of 116

ICE 2019/2-SM


FEVFVO + 227 milligrams of white powder MDMA (14% calculated as base) - Class A Glucose (indicated) - Not Controlled

FFFLFF + 13% amount of MDMA is found with the help of quantitative methods of GC-MS.

FJF0IF + the white powder contains MDMA (13.97%ww) wich is controlled by national law

FXP8PV + in sample 2019/2/SM-1, 3,4-Methylenedioxymetamfetamine (MDMA) was found.

FYKJPD + glucose

G6GBTW + 3,4-Methylenedioxymetamfetamine (MDMA), dextrose and magnesium estearate were detected in SM1 sample.

GC11E1 +

GDI9LV + SM-1 to contain 3,4-methylenedioxymethamphetamine (MDMA) which is controlled under Malaysian Dangerous Drug Act 1952

GGGPGE + White powder analysed by GC/MS was found to contain MDMA. Mass spectra was similar to CRM

GHKHWC +

GIGQ0G + After chemical analysis was performed the sample contains MDMA /Lactose

GIZGWR + Powder contains MDMA. MDMA (also known as methylenedioxymethylamphetamine) is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016. This is because methylenedioxymethylamphetamine is structurally derived from an N-alkyl- alpha- methylphenethylamine, by substitution in the ring with an alkylenedioxy substituent. (See paragraph 1A(l) of Schedule 1 to the Misuse of Drugs (Amendment) Act, 2015).

GPV0WG +

GQPYLA + SM-1 sample includes 3,4-methylenedioxymethamphetamine (MDMA). there is not adulterant.

GYEHYL +

H12HE2 +

H7XE2X +

H9RHNG + Mass spectrometry profile correlation between sample and reference material certified

HANMLJ + MDMA and LACTOSE




Page 37 of 116

ICE 2019/2-SM


HASZSM + Mixture of MDMA and glucose (70.5 % w/w) and sucrose (1.9 % w/w)

HHEETQ + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 19. (8) N-methyl-3,4-methylenedioxyamphetamine (MDMA) (N,α-dimethyl-1,3-benzodioxole-5-ethanamine I2TTTT + Presence of MDMA in the seized sample.

I4IIIW + MDMA was confirmed at Rt of 11.82 minutes, m/z precursor ion 194.0444 with fragments 163.07487, 135.04372, 133.06448, 105.06995 and 58.06573

ICNCMG + WAS FOUND TO CONTAIN MDMA AND GLUCOSE

IE8EEE + 3,4-Methylenedioxymetamfetamine (MDMA) was detected in the sample.

IIIDYX + glucose

IIILIY +

INOP4F + We detected it using the GCMS/MS.

IRZAFP +

IWWWZH + SM-1 sample includes 3,4-methylenedioxymethamphetamine (MDMA). there is not adulterant.

JCJJVA + The sample contains MDMA which is listed as a controlled drug according to french order, appendix III of February 22nd 1990.

JJPNJY + MDMA was detected by GC-MS. Confirmed and quantified by GC-MS

JJUJHH + On chemical analysis of a representative sample of the powder MDMA was detected.

JMYLYJ + White powder containing 13.0%w/w MDMA and glucose

JVPB7L + SM-1 contains MDMA HCl. Quantitation MDMA 14.83% as base

K6G1HJ + MDMA

K8IZ1S + There is ilicit drug

K8NOCM + That I examined and analysed the said sample and found it to contain : controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 19. (8) N-methyl-3,4- methylenedioxyamphetamine (MDMA) (N,α-dimethyl-1,3-benxodioxole-5-ethanamine) calculated as the hydrochloride 14% (w/w)

KAKGTD +




Page 38 of 116

ICE 2019/2-SM


KFKUP0 + Sample 2019/2/SM-1 a white powder gave a positive result for 2,3 - Methylenedioxymethamphetamine, substance under national legislation on drugs

KJFJIJ +

KKKQP7 + Marquis reagent test gave positive indication for an ecstasy type drug. GCMS analysis confirmed presence of MDMA based on fragmentation pattern and retention time compared to a known standard. No quantitative analysis is performed for this drug type.

KLCHRH +

KPSSUB + WE FOUND A MIXTURE OF MDMA, GLUCOSE AND STARCH.

KQKO2K + MDMA positive >18.0 µg / g

KUD7YD + whitish powder containing 12.7% of MDMA

L9WDPM + Dextrose detected

LDLJZA + An off-white powder which had a neight weight of 216 milligrams and a purity of 14% (reported as base) which was found to be MDMA and glucose.

LG1AMG + Brown glass vial labelled 2019/2/SM-1 containing 0.23 grams of white powder. Analysis results; MDMA (13%) and Glucose. MDMA is a Class A controlled substance under the Misuse of Drugs Act 1971 (as amended). Glucose is not controlled under the aforementioned act.

LHOD3U + Has been detected the presence of MDMA in the sample. The sample was also found to contain dextrose.

LKHTDW + 2019/2/SM-1 contains 3,4-methylenedioxymethamphetamine (MDMA) and Methamphetamine.

LUABFV + MDMA 14,12%

LVRMSV + Also contains glucose.

LVUH0Z + Sample 2019/2/SM-1 was found to contain the controlled drug MDMA (3,4 Methylenedioxymetamfetamine) and lactose.

MBWNRJ +

MIIFIV + Sample 2019/2/SM-1 found to contain 3,4-Methylenedioxymethamphetamine.

MJDOQK + One brown glass vial which contained 223 milligrams of off-white powder. This powder contained an average of 16% 3,4-METHYLENEDIOXYMETHYLAMPHETAMINE HYDROCHLORIDE (MDMA). METHYLENEDIOXYMETHYLAMPHETAMINE HYDROCHLORIDE is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended).




Page 39 of 116

ICE 2019/2-SM


MJYQ1I + -

MMVGH6 +

MOGXMB + From Screening test using (MR) and from confirmation test by (GC-MS) the sample was found to contain the controlled drug (MDMA).

MTWM6W + SM-1 sample includes 3,4-methylenedioxymethamphetamine (MDMA) and n-methyl-3,4- methylenedioxyamphetamine. there is not adulterant.

MUVGFL +

MWX4XX + was found MDMA

NE8ZAO + Black colour with Marquis test. TLC and GCMS also gives result of MDMA

NGJDWJ +

NNNNEI + contains drug according to law

O1HUPW + DEXTROSA.

OEOJOY + Controlled drug, MDMA, present in sample. Concentration approx 13%

OHNQ7X +

OHS9XX +

OOWPNF + 1 glass bottle containing 0.20 grammes of a powder containing 0.02 grammes of 3,4- methylenedioxymethamphetamine (being a compound structurally derived from N-alkyl-α-methylphenethylamine by substitution in the ring with an alkyl-enedioxy substituent).

OZOHOD + SAMPLE WAS CONFIRMED BY GC MSD

P8UQDW + Examination revealed the presence of MDMA

PCQBJD + Also contain glucose.

PFZFOJ + The sample is in the form of white fine powder. It answers the tests for the presence of MDMA.

PKNKQN + Sample contains MDMA. HCl 12.6%. scheduled subtance according Pt law

PLMLOM + The sample contains 13.72% of MDMA.

PPNIPX + MDMA




Page 40 of 116

ICE 2019/2-SM


PQCCII -

PRZOZC +

PXAOXX + MDMA + GLUCOSE

PXFATB +

PYUYVY + Sample SM1 contains MDMA

Q8ZQ82 + The sample obtains with the positive result with Marquis reagent TLC: The Rf sample obtain with the same Rf MDMA standard

QBIV4X + SM-1 was found to contain 3,4-methylenedioxymethamphetamine (MDMA) and also contain glucose.

QFFJPH + GLUCOSE

QROQON + The white powdery substance contain 15.9% w/w of 3,4-Methylenedioxymethamphetamine (MDMA)

RCRHBM + controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 19. (8) -methyl-3,4-methylenedioxyamphetamine (MDMA) (N,a-dimethyl-1,3-benzodloxole-5-elhanamine) calculated as the hydrochloride 17 % (w/w)

RG5OYA + Sample 2019/2/SM-1 contains 3,4-Methylenedioxymetamfetamine (MDMA) and DEXTROSE

RH2BU2 + This sample was found to contain Methylenedioxymethylamphetamine, which is a Class A controlled substance under the Misuse of Drugs Act 1971.

RRQFQQ -

RTQ8I7 + 3,4-Methylenedioxymetamfetamine (MDMA) is listed in the First Schedule of Dangerous Drug Acts 1952.

RZDHUH + SM-1 contains 14,12±0,78 weight % 3,4-MDMA SM-1 contains also glucose

S0C00Z + Sample 2019/2/SM-1 consists of white powder. 3,4-Methylenedioxy-metamfetamine (MDMA), a prohibited substance included in the National Law for Narcotics, is found to be present in this sample

SDNBD6 + MDMA

SFS5SX + 2019/2/SM-1 was confirmed for MDMA which is a scheduled I controlled substance in the US.

SOWSUC + In the powder MDMA is present.




Page 41 of 116

ICE 2019/2-SM


STNCC9 + Blak colour with Marquis Test indicates the possible presence of MDMA. TLC and GCMS analysis show that SM-1 contains MDMA.

SVRSSF + The sample contains 3,4-Methylenedioxymetamfetamine.

TBUBCR + Test sample 2019/2/SM-1 found to contain MDMA

TBYTGT + The Test sample 2019/2/SM-1 was analyzed by Thin Layer Chromatography technique and was found to contain MDMA and Glucose.

TE8ERE + 3,4-Methylenedioxy-metamfetamine (MDMA) was detected in 2019/2/SM-1

TFF5SF + It was detected MDMA in the analyzed sample.

TFKFT5 + Positive for MDMA

TKLAER + Sample 2019/2/SM-1 contains MDMA and Dextrose. MDMA base concentration is 12.87%

TPYWQP + The test sample contained GLUCOSE

UFS8L8 +

UUNUSP + The analysis confirmed that SM1 contains MDMA (as controlled drug) but we are not able to give a quantitative result.

UXPP39 + In the sample SM1 was identified MDMA.

UYH68O + 3,4 Methilenedioxy-metamfetamine (MDMA) and Glucose

UYIOY3 + 3,4-Methylenedioxymetamfetamine (MDMA) and Noscapina

V9FHUE +

VJJ2BS + MDMA is not scheduled based on national law on narcotics psycotropic substances and precursors No#02/L-128

VK9TBJ + glucose-based sugar

VOFFDF + In the test sample 2019/2/SM-1 was detected 3,4-methylendioxymethamphetamine

VOFIVV + MDMA was detected in the SM-1 sample.

VSIQQM + /

VTGLIP + sample 2019/2/SM-1 was found to contain MDMA

VTNITG +

12,81 +/- 1,41 % MDMA BASE D-GLUCOSA




Page 42 of 116

ICE 2019/2-SM


WCDCCS +

WG1S1P + MDMA is on the list of drugs.

WKVSHN + The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample, indicates the MDMA presence.

WLWWWW + The sample contain MDMA, glucose

WRVOXF + One package containing 227 milligrams of an off-white powder. This powder was found to contain 3,4-methylenedioxymetamfetamine (MDMA) (class A), with a purity of 14% in base form, and glucose (not controlled).

WU22AL + 3,4-MDMA, was detected in the powder, with a W:W percentage estimated at 14.50%

X1NYNN +

XO00Q0 + It is included in Table I Schedule II, Psychotropic Substances, not used for medical purposes, approved by Government Decision 1088 of 05.10.2004

XSNN71 + MDMA 14% (as base) MDMA is classified as narcotic drug.

Y5OQGB + MDMA (3,4-Methylenedioxymetamphethamine) was found in the sample 2019/2/SM-1

YARNPI + MDMA was Identified in SM 1 and the percentage is 13.6 % in addition dextrose was identified in SM 1

YL6D6J + The simple contains MDMA

YY3YD4 + The sample contained 14.0% MDMA.

YYBTFT + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of the Dextrose anhydrous.

ZAZMLT + Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with 3,4- Methylenedioxymetamfetamine (MDMA).

ZNRYRN + sample contains 14,3 % of MDMA

ZPRDAZ +




Page 43 of 116

ICE 2019/2-SM

Identification methods for Test Sample 1

Analytical Technique Codes

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

06JS66 I SI HPTLC

0GRT0S SI

111NTK I I SI I

1MA9MF I SI

224V2J I S

2HSS8S I I S Raman

2JJWOJ S I I

2UVXGU I S

3PP2PP I I

48PXX4 S SI I

4BVR3P S S I I I caffeine

50AP5Y S S S I I

5CPBXX I SI

60N30D S I

61XYO6 SI I

63AEKB I SI

64G4V7 SI I Benedict's Reaction

6AX4TV I I

6ESG22 I I

6GM1ZU I SI I

6OTC3V SI I

75XFMQ S I I I

77JO7Q I SI

7KCDRK S I I

7RURX8 S SI SI

7WIJ9N S I

8IXSA9 S I I SI S Rapid test

8NKZIO SI

8SMOGU SI

932LRK I SI I

9969TL S S S I I

999RGV S S S I

9ABUAU SI I

Legend: S ... used for Screening I ... used for Identification SI ... used for both




Page 44 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

9FFVN3 I SI I

9HXOHH I SI

9N59BB I I SI

9OO999 S S I I I

9OS0B5 S SI

A2HMLG SI

AA0UJR SI SI SI I

ACYVYR S S I I

AK3UYT SI

AM777O S S I

AMYZY0 SI S S I I I

AWGGYX I SI

AXAVAJ S S I

AZBAGS I SI I XRD

B3D1SD SI SI SI SI I

B6H3ZH SI

BCD9DP SI

BD556C SI I

BQNMYR S S SI I

BXCKYU SI S I

C11111 SI SI SI I

C5MOP5 I I

C8CCX2 S SI

CAS0HP S I I

CBISZG S S I

CD5XF1 S S SI

CDVNVK S S I

CILAEB S I I

COVWOU SI S S I SI I

CXQPFE I

D67Z7M S S S I S Tanred

DCOHUX SI S I I

DJDDMD S I I I S

DK6FK1 S S S I

DKW45M S S S I I

DSEBBS S S S I I

DTIACA S I I I I




Page 45 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DZZZLS SI S I I SI

E1ZARZ S I I

EI96ZN S I I

EIHUWT SI

ELQO7L S S S I I

F0RKYD S I I I Hplc/RID

FCGG7O S S I SI

FEVFVO S S I I

FFFLFF SI I SI SI

FJF0IF I SI

FXP8PV SI SI

FYKJPD SI I

G6GBTW I S I

GC11E1 S I I

GDI9LV S S SI I

GGGPGE S S S I

GHKHWC S S S I I

GIGQ0G S I I

GIZGWR I

GPV0WG I SI

GQPYLA SI SI SI I

GYEHYL I I SI

H12HE2 I

H7XE2X I SI I

H9RHNG I I

HANMLJ I SI I

HASZSM I I I S

HHEETQ S I I I GC-IR

I2TTTT SI

I4IIIW SI

ICNCMG I SI

IE8EEE S S S I I

IIIDYX S I SI I

IIILIY SI I

INOP4F I I S Immuno Assay Rapid test kit

IRZAFP S I I

IWWWZH SI SI SI I




Page 46 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

JCJJVA I I

JJPNJY I SI I

JJUJHH S S I HRMS

JMYLYJ I I SI

JVPB7L S S I I I

K6G1HJ SI

K8IZ1S S SI S I I

K8NOCM S I I GC-IR

KAKGTD S S I I S DUQUENOIS LEVINE

KFKUP0 S S I I

KJFJIJ S I I I

KKKQP7 SI I

KLCHRH S S I I

KPSSUB SI SI S SI I I

KQKO2K SI

KUD7YD I SI

L9WDPM I I S

LDLJZA S S S I I

LG1AMG S S I I

LHOD3U S I I

LKHTDW S S S S I I I S FBB Test/Duquenois Levine Test

LUABFV S I

LVRMSV S I SI I

LVUH0Z S S S I SI

MBWNRJ SI SI I SI Duquenois Levine

MIIFIV S I

MJDOQK S S S I I

MJYQ1I SI

MMVGH6 S SI

MOGXMB S S I S NEGMS

MTWM6 W

SI SI SI I

MUVGFL S I

MWX4XX S I I

NE8ZAO S S S I I

NGJDWJ S I I

NNNNEI SI I SI




Page 47 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

O1HUPW S S I I

OEOJOY SI

OHNQ7X I

OHS9XX I S

OOWPNF S S I SI

OZOHOD SI I I

P8UQDW SI I SI

PCQBJD S I I I

PFZFOJ S S S I I

PKNKQN S I

PLMLOM SI I

PPNIPX SI SI SI SI I I I

PQCCII I S

PRZOZC SI I

PXAOXX S I I

PXFATB S S I

PYUYVY S S S I

Q8ZQ82 S S S I

QBIV4X S S I I

QFFJPH SI I

QROQON S S S I I I

RCRHBM S I I

RG5OYA S S I I

RH2BU2 S S I

RRQFQQ S I

RTQ8I7 S I S Janovsky test

RZDHUH I SI I

S0C00Z S S I

SDNBD6 I SI I

SFS5SX S I

SOWSUC SI I

STNCC9 S S SI I

SVRSSF SI Q-TOF LC/MS

TBUBCR S I

TBYTGT S S SI S Fast Blue B Salt test

TE8ERE S S I

TFF5SF S S S I




Page 48 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

TFKFT5 SI

TKLAER S S I I

TPYWQP S S S I

UFS8L8 S I

UUNUSP S S S I

UXPP39 I

UYH68O S S I I

UYIOY3 S S I I

V9FHUE SI

VJJ2BS S S I I S Caffeine 141/142

VK9TBJ SI I

VOFFDF I

VOFIVV SI I

VSIQQM SI SI

VTGLIP S I I

VTNITG S S S I I I DR-X

WCDCCS I SI SI

WG1S1P S S S I I

WKVSHN S S I S Dragendorff

WLWWW W

S S I I I

WRVOXF S SI SI I I

WU22AL SI

X1NYNN SI I

XO00Q0 S S S I I

XSNN71 I I

Y5OQGB S I I

YARNPI S S I I I SI Caffeine

YL6D6J S S I I

YY3YD4 I SI

YYBTFT S S I I

ZAZMLT S S I

ZNRYRN SI

ZPRDAZ S S S I I




Page 49 of 116

ICE 2019/2-SM




06JS66 Caffeine

0GRT0S --

2HSS8S none

2UVXGU caffeine, ambien, piperidine

60N30D nil

63AEKB --

64G4V7 -

6AX4TV caffeine, lactose

8IXSA9 Caffein

8SMOGU caffeine

9969TL Caffeine and Lactose

9N59BB None

9OO999 NONE

9OS0B5 caffeine

A2HMLG --

AA0UJR 2-CB

AMYZY0 none

B3D1SD Caffeine

BQNMYR Caffeine and lactose

C11111 Caffeine

C5MOP5 --

CBISZG Caffeine

CD5XF1 Caffeine

COVWOU NIL

DJDDMD Blank test sample

DK6FK1 CAFFEINE

DZZZLS CAFFEINE + LACTOSE

EIHUWT cafeine

FCGG7O Caffeine and lactose

FJF0IF --

FXP8PV NONE

G6GBTW No schedulled drugs were detected in SM2 sample.

GDI9LV Caffeine

GGGPGE Caffeine

GIZGWR Caffeine

GQPYLA Caffeine

H7XE2X Caffeine




Page 50 of 116

ICE 2019/2-SM


HANMLJ CAFFEINEand LACTOSE

HASZSM None

I4IIIW caffeine

ICNCMG CAFFEINE

INOP4F Caffeine and Ketamine

IWWWZH Caffeine

JJPNJY --

JMYLYJ --

JVPB7L none

K6G1HJ Caffeine

KAKGTD CAFFEIN

KKKQP7 Caffeine

KPSSUB CAFFEINE, LACTOSE

KUD7YD --

L9WDPM -

LHOD3U In this sample has not been identified any drug.

LKHTDW Caffeine and Lactose

MIIFIV Caffeine

MJYQ1I -

MOGXMB Caffeine

MTWM6W Caffeine

MUVGFL Caffeine

MWX4XX NONE

NE8ZAO Caffeine

OHS9XX Caffeine

OZOHOD CAFFEINE

PKNKQN Cafeine

PLMLOM Caffeine

PPNIPX -

PXAOXX CAFFEINE+ LACTOSE

PYUYVY Caffeine

RG5OYA NA

RH2BU2 Caffeine

SFS5SX Caffeine

STNCC9 Caffeine

TBYTGT Caffeine and Lactose

TE8ERE Caffeine

TFF5SF Caffeine

TFKFT5 caffeine

TPYWQP CAFFEINE

UUNUSP NONE

UXPP39 Caffeine




Page 51 of 116

ICE 2019/2-SM


UYH68O Do not

UYIOY3 Lactose and Caffeine

VOFFDF Caffeine

VTNITG NO

WKVSHN Caffeine

WLWWWW -

WU22AL NA

YYBTFT LACTOSE + CAFFEINE

ZAZMLT CAFFEINE, not controlled

ZNRYRN Caffeine




Page 52 of 116

ICE 2019/2-SM


Code Caffeine Lactose

06JS66 + ANP The sample was subjected to HPTLC using silicagelF254 as stationary phase and Ethylacetate:Methanol:Ammonia 85:10:5 as MP.A single spot was obtained after development and it was scanned. The UV Spectrum was found matching with library UV spectrum of Caffeine and the analysis repeated along with Standard Caffeine and the RF and UV Spectrum were found matching. Then the sample was subjected to GC-MS analysis using HP5 column. The RT of SM2 and Standard Caffeine compared and were found matching. The Fragmentation pattern was compared with library and was found matching with Caffeine. Therefore the presence of Caffeine was confirmed.

0GRT0S + ANP the sample contains only caffeine

111NTK + + It was found caffeine and lactose

1MA9MF ANP ANP

224V2J + ANP

2HSS8S + + The sample contains caffeïne and lactose. No drugs have been detected.

2JJWOJ + + The white powder was analysed for controlled substances with a negative result.

2UVXGU + + he main compound we found in SM-2 is caffeine after TLC . with screening we found : Ambien, Piperidine and hydrochlorothiazide

3PP2PP + ANP The sample is a caffeine based powder, It is not a drug according to our law

48PXX4 + + caféine (26%) + lactose

4BVR3P + ANP The sample is in the form of white fine powder. It answers the test for the presence of caffeine

50AP5Y + + Caffeine and Lactosa

5CPBXX + +

60N30D + ANP Sample SM-2 was found to contain caffeine

61XYO6 + +

63AEKB + - the sample contains caffeine

64G4V7 + + The sample contain caffeine and lactose.

6AX4TV + + The sample contains caffeine and lactose.




Page 53 of 116

ICE 2019/2-SM


6ESG22 + -

6GM1ZU + + Caffeine, Lactose

6OTC3V + + Any drugs has been detected in the sample

75XFMQ + + Caffeine and Lactose

77JO7Q + - CAFFEINE

7KCDRK + + Caffeine + Lactose

7RURX8 + -

7WIJ9N + ANP Caffeine is not a controlled drug, but it could be used as an adulterant. NOT DETECTED CONTROLLED DRUG.

8IXSA9 + ANP We found caffein in SM2

8NKZIO + + caffeine lactose

8SMOGU - - a substance identified is caffein

932LRK + + Caffeine and Lactose

9969TL + + Using the techniques CR, TLC, FT-IR & GC-MS, sample SM-2 was found to contain Caffeine and Lactose .

999RGV + -

9ABUAU + +

9FFVN3 + + CAFFEINE IN LACTOSE POWDER

9HXOHH + + The sample SM-2 contains caffeine and lactose.

9N59BB + ANP White powder containing caffeine.

9OO999 + ANP White powder that contains substance CAFFEINE, and none of controlled substance.

9OS0B5 + ANP

A2HMLG + ANP caffeine

AA0UJR - - negative




Page 54 of 116

ICE 2019/2-SM


ACYVYR + +

AK3UYT + ANP

AM777O + - For Test sample 2019/2/SM-2, Gas Chromatography - Mass Spectrometry indicates the presence of Caffeine, a non-controlled substance. However, this was not confirmed.

AMYZY0 + + SM 2 For presumptive tests a positive colorimetric reaction (Fehling) was obtained and Lactose was confirmated by FTIR.This finding indicates no controlled drug are present in the test sample.GC/MS Fragmentation pattern obtained with sample SM 2 is equivalent to those obtained with caffeine. SM-2 contains no controlled substance. It was found to contain caffeine and lactose.

AWGGYX + ANP The sample was analysed and no common controlled drug was detected.

AXAVAJ + ANP No controlled drugs were detected.

AZBAGS + + caffeine, lactose

B3D1SD + - Caffeine was examined in SM-2.

B6H3ZH + + CAFFEIN AND LACTOSE

BCD9DP + + Caffeine (23 %) and lactose.

BD556C + ANP Test Sample SM-2 found to contain Caffeine

BQNMYR + + The sample was analysed with FTIR and GCMS in two different columns and solvents

BXCKYU + ANP Caffeine

C11111 + ANP SM-2 sample includes Caffeine. there is not any a drugs.

C5MOP5 + + White powder containing caffeine and lactose

C8CCX2 + ANP Test sample 2019/2/SM-2 having gross weight 05.98 gram(s) of white powder in amber glass bottle contains No Narcotic and Psychotropic Substance. However, Caffeine (A non-controlled substance) is confirmed.

CAS0HP + + this sample containes caffeine and lactose

CBISZG + ANP The powder was found to contain caffeine. Caffeine is not controlled under the Misuse of Drugs Act 1971 (as amended).

CD5XF1 + ANP Sample 2019/2/SM-2 was found to contain caffeine.

CDVNVK + ANP caffeine




Page 55 of 116

ICE 2019/2-SM


CILAEB + + Caffeine - confirmed with GCMS, FTIR Lactose - confirmed with FTIR and Wohlk reaction

COVWOU + + Sample analysed /Identified by GCMS & FTIR techniques. found the presence of caffine and Lactose in the sample.

CXQPFE + ANP

D67Z7M + ANP In the sample 2019/2/SM-2 was not found controlled substance.

DCOHUX + ANP CAFEINA

DJDDMD + + Presence of caffeine and lactose was detected in the sample.

DK6FK1 + + THE SAMPLE 2019/2/SM2 WAS FOUND CAFFEINE

DKW45M + ANP Caffeine is an very usual adulterant in seized drugs analyzed in our laboratory

DSEBBS + - Caffeine was identified with a retention time of 10.616 min by GC/MS. The concentration of sample injected in GC/MS was 204 ppm. Caffeine is not controlled drug.

DTIACA + - the sample contains caffeine

DZZZLS + + In the 2019/2/SM-2 was proved the presence of caffeine and lactose.

E1ZARZ + + Sample contains Caffeine and Lactose .

EI96ZN + + THE SAMPLE CONTAIN CAFFEINE AND LACTOSE

EIHUWT + ANP cafeine

ELQO7L + + Controlled drugs were not identified

F0RKYD + + SM2 contient de la caffeine et du lactose

FCGG7O + + The analysed sample does not contain controlled drugs.

FEVFVO + + 232 milligrams of white powder Caffeine - Not Controlled Lactose (indicated) - Not Controlled

FFFLFF + + Caffeine and Lactose are found during identification step. No drug is found.

FJF0IF - ANP the white powder contains caffeine

FXP8PV + ANP in sample 2019/2/SM-2 no forensic interest substances found, caffeina was found.




Page 56 of 116

ICE 2019/2-SM


FYKJPD + + caféine lactose

G6GBTW + + Caffeine and lactose were detected in SM2 sample.

GC11E1 + - Caffeine

GDI9LV + ANP SM-2 to contain Caffeine which is controlled under Malaysian Poisons Act 1952

GGGPGE + ANP White powder analysed by GC/MS was found to contain CAFFEINE. Mass spectra was similar to CRM

GHKHWC + ANP caffein

GIGQ0G + + After chemical analysis was performed the sample contains caffeine / lactose

GIZGWR + ANP Powder contains indications of caffeine. Caffeine is not a controlled drug.

GPV0WG - ANP caffeine

GQPYLA + ANP SM-2 sample includes Caffeine which is %22,390 amount. there is not any a drugs.

GYEHYL + +

H12HE2 + ANP Caffeine

H7XE2X + +

H9RHNG + + Mass spectrometry profile correlation between sample and reference material certified

HANMLJ + + CAFFEINEand LACTOSE

HASZSM + + Mixture of lactose (72.1 % w/w) and caffeine (238.2 mg/g)

HHEETQ + ANP The sample was found to contain the following non-controlled substance(s) has (have) been detected but not certified : Caffeine. Should you need this (these) detected substance(s) to be certified, please contact us

I2TTTT + - Absence of drugs; presence of caffeine.

I4IIIW + ANP Caffeine was confirmed at Rt of 11.65 minutes with precursor ion m/z 195.0874, Fragments were 138.06599, 110.07142, 69.04532 and 83.06084

ICNCMG + + CAFFEINE AND LACTOSE

IE8EEE + + Caffeine and lactose were detected in the sample.




Page 57 of 116

ICE 2019/2-SM


IIIDYX + + coffeine, lactose

IIILIY + +

INOP4F + ANP Using GCMS/MS, we were able to detect caffeine. Using LCMS/MS, we were able to detect both caffeine and ketamine.

IRZAFP + +

IWWWZH + ANP SM-2 sample includes Caffeine which is %29 amount. there is not any a drugs.

JCJJVA + + The analysis did not reveal any controlled drug according to french order, decree of February 22nd 1990.

JJPNJY + - caffeine was detected by GC-MS

JJUJHH + ANP On chemical analysis of a representative sample of the powder caffeine was detected which is not controlled under the Misuse of Drugs Act (1971).

JMYLYJ + + White powder containing caffeine and glucose

JVPB7L + + SM-2 contains Caffeine and Lactose

K6G1HJ + - Caffeine

K8IZ1S + + There is not ilicit drugs (Caffeine and Lactose)

K8NOCM + ANP That I examined and analysed the said sample and found it to conatin : The following non- controlled substance(s)has(have) been detected but not certified: Caffeine Should you need this (these) detected substance(s) to be certified, please contact us.

KAKGTD + - THE SAMPLE NOT CONTAIN ILLICIT DRUGS

KFKUP0 + ANP Sample 2019/2/SM-2 a white powder gave a negative result for , substance under national legislation on drugs.Caffeine was detected.

KJFJIJ + ANP

KKKQP7 + ANP Marquis reagent test gave no reaction. GCMS analysis confirmed presence of caffeine based on fragmentation pattern and retention time compared to a known standard. No quantitative analysis is performed for this uncontrolled drug.

KLCHRH + + CAFFEINE - LACTOSE

KPSSUB + + WE HAVEN´T FOUND DRUGS BUT WE FOUND A MIXTURE OF CAFFEINE AND LACTOSE.

KQKO2K ANP ANP Negative for all tested compounds




Page 58 of 116

ICE 2019/2-SM


KUD7YD + ANP White powder not containing any controlled drugs

L9WDPM + + Caffeine and Lactose detected

LDLJZA + - A white powder which had a net weight of 200 milligrams, which was found to be negative for controlled substances.

LG1AMG + + Brown glass vial labelled 2019/2/SM-2 containing 0.23 grams of white powder. Analysis results; Caffeine and Lactose. Caffeine and lactose are not controlled under the Misuse of Drugs Act 1971 (as amended).

LHOD3U + + Has been detected the presence of lactose and caffeine.

LKHTDW + + 2019/2/SM-2 contains Caffeine and Lactose.

LUABFV + - CAFEINE

LVRMSV + + Sample contains coffeine, lactose.

LVUH0Z + + Sample 2019/2/SM-2 was found to contain caffeine and lactose.

MBWNRJ + ANP GC/MS told for the presence of caffeine.

MIIFIV + ANP Sample 2019/2/SM-2 found to contain caffeine.

MJDOQK + + One brown glass vial which contained 219 milligrams of white powder. No controlled drugs were detected in this powder which contained caffeine and lactose. Caffeine and lactose are not controlled under the provisions of the Misuse of Drugs Act 1971 (as amended).

MJYQ1I + ANP -

MMVGH6 + - caffeine

MOGXMB + ANP Directly from confirmation test by (GC-MS) the sample was found to contain the adulterant (Caffeine).

MTWM6W + ANP SM-2 sample includes Caffeine which is %29 amount. there is not any a drugs.

MUVGFL + ANP This sample contains caffeine, which is not a controlled substance.

MWX4XX + + WAS FOUND CAFFEIN AND LACTOSE

NE8ZAO + - Only GCMS gives Caffeine result.

NGJDWJ + - CAFFEINE




Page 59 of 116

ICE 2019/2-SM


NNNNEI + + contains no drug according to law

O1HUPW + + CAFEINA Y LACTOSA.

OEOJOY + ANP No controlled drug present Identified substance: Caffeine

OHNQ7X ANP ANP

OHS9XX + -

OOWPNF + ANP 1 glass bottle containing 0.22 grammes of a powder which did not contain any substances controlled under the Dangerous Drugs Ordinance.

OZOHOD + ANP THIS SAMPLE ONLY CONTAINS CAFFEINE CONFIRMED BY GC MSD

P8UQDW + + No controlled substances was found

PCQBJD + + Sample contain caffeine and lactose.

PFZFOJ + ANP The sample is in the form of white fine powder. it answers the tests for the presence of Caffeine.

PKNKQN + ANP Samples contains cafeine, not scheduled substance according PT law

PLMLOM + + The sample contains Caffeine and Lactose.

PPNIPX + + caffeine, lactose

PQCCII + +

PRZOZC + +

PXAOXX + + CAFFEINE +LACTOSE

PXFATB + ANP We detected CAFFEINE

PYUYVY + - Sample SM2 contains Caffeine

Q8ZQ82 ANP ANP

QBIV4X + ANP SM-2 was found to contain caffeine.

QFFJPH + + CAFFEIN LACTOSE

QROQON + + The white powdery substance contain Caffeine and Lactose.




Page 60 of 116

ICE 2019/2-SM


RCRHBM + ANP The following non-controlled substance(s) has(have) been detected but not certified: Caffeine

RG5OYA + + Sample 2019/2/SM-2 contains CAFEINE AND LACTOSE

RH2BU2 + ANP This sample was found to contain Caffeine which is not controlled under the Misuse of Drugs Act 1971.

RRQFQQ ANP ANP

RTQ8I7 + ANP Caffeine is listed in the First Schedule of Poison Act 1952.

RZDHUH + + SM-2 contains caffeine and lactose

S0C00Z ANP ANP Sample 2019/2/SM-2 consists of white powder. No prohibited substances are detected in this sample.

SDNBD6 + ANP

SFS5SX + ANP 2019/2/SM-2 was confirmed for caffeine which is a non controlled substance in the US.

SOWSUC + ANP In the powder caffeine is present.

STNCC9 + ANP GCMS analysis show that SM-2 contains caffeine.

SVRSSF + ANP The sample contains caffeine.

TBUBCR + ANP Test sample 2019/2/SM-2 found to contain caffeine

TBYTGT + + The Test sample 2019/2/SM-2 was analyzed by Thin Layer Chromatography technique and was found to contain Caffeine and Lactose.

TE8ERE + ANP Caffeine was detected in 2019/2/SM-2

TFF5SF + ANP It was detected Caffeine in the analyzed sample.

TFKFT5 + ANP Positive for caffeine

TKLAER + + Sample 2019/2/SM-2 contains Lactose and Caffeine

TPYWQP + + The test sample contained LACTOSE

UFS8L8 + - CAFFEINE

UUNUSP + - We found cafeine in SM2.

UXPP39 + - In the sample SM2 was identified caffeine, without drugs.




Page 61 of 116

ICE 2019/2-SM


UYH68O + + Caffeina and Lactose

UYIOY3 + + Lactose and Caffeine

V9FHUE + +

VJJ2BS + ANP Sample No#2 contain caffeine

VK9TBJ + + caffeine, lactose

VOFFDF + - In the test sample 2019/2/SM-2 was detected caffeine

VOFIVV + ANP No controlled drugs were found in the SM-2 sample.

VSIQQM + + /

VTGLIP + ANP sample 2019/2/SM-2 was found to contain Caffeine

VTNITG + + LACTOSA CAFEÍNA

WCDCCS + + caffeine, lactose

WG1S1P + +

WKVSHN + ANP The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample, indicates the Caffeine presence.

WLWWWW + + The sample contain caffeine, lactose

WRVOXF + + One package containing 226 milligrams of a white powder. This powder was found to contain caffeine (not controlled) and lactose (not controlled).

WU22AL + ANP Sample resulted negative, Caffeine was detected

X1NYNN + +

XO00Q0 ANP ANP

XSNN71 + + No narcotic drug has been detected in the sample.

Y5OQGB + ANP Caffeine was found in the sample 2019/2/SM-2

YARNPI + + Caffeine and Lactose were identified in SM 2

YL6D6J + + The sample contains caffeine




Page 62 of 116

ICE 2019/2-SM


YY3YD4 + + The sample contained caffeine and lactose.

YYBTFT + + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of LACTOSE and CAFFEINE in the sample.

ZAZMLT + ANP Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with caffeine.

ZNRYRN + - sample contains not contoled substance caffeine

ZPRDAZ + + Caffeine and lactose




Page 63 of 116

ICE 2019/2-SM



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

06JS66 I SI HPTLC

0GRT0S SI

111NTK I I SI I

1MA9MF I SI

224V2J I S

2HSS8S I I S Raman

2JJWOJ S I I

2UVXGU I S

3PP2PP I I

48PXX4 S SI I


50AP5Y S S S I I

5CPBXX I SI

60N30D S I

61XYO6 SI I

63AEKB I SI


6AX4TV I I

6ESG22 I I

6GM1ZU I SI I

6OTC3V SI I

75XFMQ S I I I

77JO7Q I SI

7KCDRK S I I

7RURX8 S SI SI

7WIJ9N S I


8NKZIO SI

8SMOGU SI

932LRK I SI I

9969TL S S S I I

999RGV S S S I





Page 64 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

9ABUAU SI I

9FFVN3 I SI I

9HXOHH I SI

9N59BB I I SI

9OO999 S S I I I

9OS0B5 S SI

A2HMLG SI

AA0UJR SI SI SI I

ACYVYR S S I I

AK3UYT SI

AM777O S S I

AMYZY0 SI S S I I I

AWGGYX I SI

AXAVAJ S S I

AZBAGS I SI I XRD


B6H3ZH SI

BCD9DP SI

BD556C SI I

BQNMYR S S SI I

BXCKYU SI S I

C11111 SI SI SI I

C5MOP5 I I

C8CCX2 S SI

CAS0HP S I I

CBISZG S S I

CD5XF1 S S SI

CDVNVK S S I

CILAEB S I I


CXQPFE I


DCOHUX SI S I I

DJDDMD S I I I S

DK6FK1 S S S I

DKW45M S S S I I

DSEBBS S S S I I




Page 65 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DTIACA S I I I I

DZZZLS SI S I I SI

E1ZARZ S I I

EI96ZN S I I

EIHUWT SI

ELQO7L S S S I I


FCGG7O S S I SI

FEVFVO S S I I

FFFLFF SI I SI SI

FJF0IF I SI

FXP8PV SI SI

FYKJPD SI I

G6GBTW I S I

GC11E1 S I I

GDI9LV S S SI I

GGGPGE S S S I

GHKHWC S S S I I

GIGQ0G S I I

GIZGWR I

GPV0WG I SI

GQPYLA SI SI SI I

GYEHYL I I SI

H12HE2 I

H7XE2X I SI I

H9RHNG I I

HANMLJ I SI I

HASZSM I I I S


I2TTTT SI

I4IIIW SI

ICNCMG I SI

IE8EEE S S S I I

IIIDYX S I SI I

IIILIY SI I


IRZAFP S I I




Page 66 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

IWWWZH SI SI SI I

JCJJVA I I

JJPNJY I SI I

JJUJHH S S I HRMS

JMYLYJ I I SI

JVPB7L S S I I I

K6G1HJ SI

K8IZ1S S SI S I I

K8NOCM S I I GC-IR


KFKUP0 S S I I

KJFJIJ S I I I

KKKQP7 SI I

KLCHRH S S I I


KQKO2K SI

KUD7YD I SI

L9WDPM I I S

LDLJZA S S S I I

LG1AMG S S I I

LHOD3U S I I


LUABFV S I

LVRMSV S I SI I

LVUH0Z S S S I SI


MIIFIV S I

MJDOQK S S S I I

MJYQ1I SI

MMVGH6 S SI


MTWM6 W

SI SI SI I

MUVGFL S I

MWX4XX S I I

NE8ZAO S S S I I

NGJDWJ S I I




Page 67 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

NNNNEI SI I SI

O1HUPW S S I I

OEOJOY SI

OHNQ7X I

OHS9XX I S

OOWPNF S S I SI

OZOHOD SI I I

P8UQDW SI I SI

PCQBJD S I I I

PFZFOJ S S S I I

PKNKQN S I

PLMLOM SI I


PQCCII I S

PRZOZC SI I

PXAOXX S I I

PXFATB S S I

PYUYVY S S S I

Q8ZQ82 S S S I

QBIV4X S S I I

QFFJPH SI I

QROQON S S S I I I

RCRHBM S I I

RG5OYA S S I I

RH2BU2 S S I

RRQFQQ S I


RZDHUH I SI I

S0C00Z S S I

SDNBD6 I SI I

SFS5SX S I

SOWSUC SI I

STNCC9 S S SI I


TBUBCR S I


TE8ERE S S I




Page 68 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

TFF5SF S S S I

TFKFT5 SI

TKLAER S S I I

TPYWQP S S S I

UFS8L8 S I

UUNUSP S S S I

UXPP39 I

UYH68O S S I I

UYIOY3 S S I I

V9FHUE SI


VK9TBJ SI I

VOFFDF I

VOFIVV SI I

VSIQQM SI SI

VTGLIP S I I


WCDCCS I SI SI

WG1S1P S S S I I


WLWWW W S S I I I

WRVOXF S SI SI I I

WU22AL SI

X1NYNN SI I

XO00Q0 S S S I I

XSNN71 I I

Y5OQGB S I I


YL6D6J S S I I

YY3YD4 I SI

YYBTFT S S I I

ZAZMLT S S I

ZNRYRN SI

ZPRDAZ S S S I I




Page 69 of 116

ICE 2019/2-SM




06JS66 Cocaine

0GRT0S cocaine

111NTK Cocaine

1MA9MF Cocaine

224V2J Cocaine

2HSS8S Cocaine

2JJWOJ Cocaine Hydrochloride

2UVXGU cocaine, noscapine

3PP2PP cocaine hydrochloride

48PXX4 cocaïne

4BVR3P cocaine

50AP5Y cocaine

5CPBXX cocaine

60N30D cocaine

61XYO6 Cocaïne

63AEKB cocaine

64G4V7 COCAINE

6AX4TV cocaine

6GM1ZU Cocaine

6OTC3V Cocaine

75XFMQ Cocaine

77JO7Q COCAINE

7KCDRK Cocaine

7RURX8 COCAINE 37.7%

7WIJ9N Cocaine

8IXSA9 Cocaine

8NKZIO cocaine

8SMOGU cocain

932LRK Cocaine

9969TL Cocaine, Tropacocaine and Methylecgonidine

999RGV COCAINE

9ABUAU Cocaine

9FFVN3 COCAINE

9HXOHH cocaine

9N59BB Cocaine

9OO999 COCAINE

9OS0B5 cocaine




Page 70 of 116

ICE 2019/2-SM


A2HMLG cocaine

AA0UJR Cocaine

ACYVYR cocaine

AK3UYT Cocaine

AM777O Cocaine

AMYZY0 cocaine

AWGGYX Cocaine

AXAVAJ Cocaine at 38%

AZBAGS cocaine HCl

B3D1SD Cocaine

B6H3ZH COCAIN

BCD9DP Cocaïne

BD556C Cocaine

BQNMYR Cocaine and lactose

BXCKYU cocaine

C11111 Cocaine

C5MOP5 cocaine

C8CCX2 Cocaine

CAS0HP cocaine

CBISZG COCAINE

CD5XF1 Cocaine

CDVNVK cocaine

CILAEB Cocaine

COVWOU COCAINE

CXQPFE Cocaine

D67Z7M Cocaine

DCOHUX COCAINA

DJDDMD Cocaine

DK6FK1 COCAINE

DKW45M COCAÍNE

DSEBBS Cocaine

DTIACA cocaine

DZZZLS COCAINE + LACTOSE

E1ZARZ Cocaine

EI96ZN COCAINE 41,1%

EIHUWT cocaine

ELQO7L Cocaine

F0RKYD Cocaine

FCGG7O Cocaine

FEVFVO Cocaine Hydrochloride

FFFLFF Cocaine

FJF0IF cocaine




Page 71 of 116

ICE 2019/2-SM


FXP8PV Cocaine

FYKJPD cocaine

G6GBTW Cocaine

GC11E1 Cocaine

GDI9LV Cocaine

GGGPGE COCAINE

GHKHWC COCAIN

GIGQ0G cocaine

GIZGWR Cocaine

GPV0WG cocaine

GQPYLA Cocaine

H12HE2 Cocaine

H7XE2X Cocaine

H9RHNG Cocaine

HANMLJ COCAINE

HASZSM Cocaine

HHEETQ Cocaine

I2TTTT Cocaine

I4IIIW Cocaine

ICNCMG COCAINE

IE8EEE Cocaine

IIIDYX cocaine

INOP4F Cocaine and tropacocaine

IRZAFP cocaine

IWWWZH Cocaine

JCJJVA Cocaine

JJPNJY cocaine

JJUJHH Cocaine

JMYLYJ cocaine

JVPB7L Cocaine HCl

K6G1HJ Cocaine

K8IZ1S Cocaine

K8NOCM Cocaine

KAKGTD COCAINE

KFKUP0 cocaine

KJFJIJ cocaina

KKKQP7 Cocaine

KLCHRH COCAINE

KPSSUB COCAINE, GLUCOSE, TROPOCOCAINE, PSEUDOECGONINE METHYL ESTER AND METHYL ECGONIDINE

KQKO2K Amphetamine, Cocaine

KUD7YD cocaine




Page 72 of 116

ICE 2019/2-SM


L9WDPM Cocaine

LDLJZA Cocaine Hydrochloride

LG1AMG Cocaine (Hydrochloride)

LHOD3U Allopseudococaine

LKHTDW Cocaine

LUABFV COCAINE

LVRMSV cocaine

LVUH0Z Cocaine

MBWNRJ cocain

MIIFIV Cocaine

MJDOQK COCAINE HYDROCHLORIDE

MJYQ1I Cocaine

MMVGH6 cocaine

MOGXMB Cocaine

MTWM6W Cocaine

MUVGFL Cocaine

MWX4XX COCAINE

NE8ZAO Cocaine and Caffeine

NGJDWJ COCAINE

NNNNEI Cocaine

O1HUPW CLORHIDRATO DE COCAINA

OEOJOY Cocaine

OHNQ7X COCAINE

OHS9XX Cocaine

OOWPNF Cocaine

OZOHOD COCAINE

P8UQDW cocaine

PCQBJD cocaine hydrochloride

PFZFOJ COCAINE

PKNKQN Cocaine

PLMLOM Cocaine

PPNIPX cocaine

PQCCII Cocaine

PXAOXX COCAINE

PXFATB Cocaine

PYUYVY Cocaine

Q8ZQ82 Cocaine

QBIV4X Cocaine

QFFJPH COCAINE HCL

QROQON Cocaine

RCRHBM Cocaine

RG5OYA COCAINE




Page 73 of 116

ICE 2019/2-SM


RH2BU2 Cocaine

RRQFQQ Cocaine

RTQ8I7 Cocaine

RZDHUH cocaine

S0C00Z Cocaine

SDNBD6 COCAINE and/or COCA PRODUCTS

SFS5SX Cocaine

SOWSUC cocaine

STNCC9 Cocaine

SVRSSF Cocaine

TBUBCR cocaine

TBYTGT Cocaine and Glucose

TE8ERE Cocaine

TFF5SF Cocaine

TFKFT5 cocaine

TKLAER Cocaine

TPYWQP COCAINE HCl

UFS8L8 COCAINE

UUNUSP COCAINE

UXPP39 Cocaine

UYH68O Cocaine

UYIOY3 Cocaine

V9FHUE COCAINE

VJJ2BS Cocaine

VK9TBJ cocaine

VOFFDF cocaine

VOFIVV Cocaine

VSIQQM Cocaine

VTGLIP Cocaine

VTNITG COCAÍNA HCL

WCDCCS cocaine

WG1S1P Cocaine

WKVSHN Cocaine

WLWWWW cocaine

WRVOXF Cocaine Hydrochloride

WU22AL Cocaine

X1NYNN Cocaine

XO00Q0 Cocaine

XSNN71 Cocaine

Y5OQGB Cocaine

YARNPI cocaine.HCl

YL6D6J Cocaine




Page 74 of 116

ICE 2019/2-SM


YY3YD4 Cocaine

YYBTFT COCAINE + DEXTROSE

ZAZMLT COCAINE

ZNRYRN Cocaine

ZPRDAZ Cocaine




Page 75 of 116

ICE 2019/2-SM


Code Cocaine

06JS66 + The sample was subjected to HPTLC using silicagelF254 as stationary phase and Ethylacetate:Methanol:Ammonia 85:10:5 as MP. A single spot was obtained after development. It was scanned and the UV Spectrum obtained was compared with the Library UV Spectrum and was found matching with Cocaine. The sample was re analysed along with Cocaine reference material using Methanol as the MP. The RF and UV spectra were matched and the presence of Cocaine is further confirmed by subjecting to GC-MS using general method for basic drugs on HP5 Column. The RT and Mas spectra of SM3 and reference material were compared and were found to be matching. The Mass spectrum was further compared with library spectrum and was found matching with cocaine. Scotts test was also performed and tested positive for Cocaine. 0GRT0S + cocaine was detected by GC-MS and quantified by GC-FID

111NTK + It was found glucose

1MA9MF +

224V2J +

2HSS8S + The sample contains cocaine. The concentration has not been determined.

2JJWOJ + The white powder was analysed and found to contain cocaine hydrochloride.

2UVXGU + he main compounds we found in SM-3 are cocaine and noscapine after TLC .

3PP2PP + The sample is a powder containing cocaine hydrochloride at 35.63% purity

48PXX4 +

4BVR3P + The sample is in the form of white powder. It answers the test for the presence of cocaine

50AP5Y +

5CPBXX + Cocaine is controlled by the law of 7th February 2014 and the RD of 6th September 2017

60N30D + Sample SM-3 was found to contain cocaine

61XYO6 + Cocaïne is sheduled as illicit drug in France

63AEKB + cocaine (39.06%ww) + dextrose

64G4V7 + The sample contains cocaine and small amounts of methylecgonine, tropocaine and ecgonidine methyl ester. Cocaine is controlled in Poland.

6AX4TV + The sample contains cocaine and glucose. Cocaine is scheduled as illicit drug in France




Page 76 of 116

ICE 2019/2-SM

Code Cocaine

6ESG22 +

6GM1ZU +

6OTC3V + It has been detected the presence of cocaine in the sample.

75XFMQ + Benzoylecgonine and methylecgonine

77JO7Q +

7KCDRK + Cocaine + glucose

7RURX8 +

7WIJ9N + Detected Cocaine.

8IXSA9 + SM3 was containe 41.7% COCAINE

8NKZIO +

8SMOGU + a substance identified is cocain

932LRK +

9969TL + Using the techniques CR, TLC, FT-IR, GC-FID & GC-MS, sample SM-3 was found to contain Cocaine, Tropacocaine and Methylecgonidine.

999RGV + NARCOTIC.List I Single Convention 1961

9ABUAU +

9FFVN3 + COCAINE IN DEXTROSE POWDER

9HXOHH + The sample SM-3 contains cocaine 39.89 % m/m.

9N59BB + White powder containing cocaine. Ecgonidine methylester, Tropacacaine and benzoylecgonine were also detected.

9OO999 + White powder that contains controlled substance COCAINE.

9OS0B5 +

A2HMLG + test sample 2019/2/sm3 contained 37.3%ww cocaine

AA0UJR + negative




Page 77 of 116

ICE 2019/2-SM

Code Cocaine

ACYVYR +

AK3UYT +

AM777O + Test Sample 2019/2/SM-3 was found to contain Cocaine, confirmed by Gas-Chromatography - Mass Spectrometry.

AMYZY0 + SM 3 For presumptive tests a positive cobalt thiocyanate(CT) reaction was obtained. CG/MS fragmentation pattern obtained with sample SM 3 are equivalent to those obtained with cocaine and methyl ecgonine. This finding indicates that cocaine controlled drug is present with 27.82 % percentage weight . The sample also contains dextrose wich was determined by FTIR.

AWGGYX + The sample was found to contain 36.3% of cocaine (as base).

AXAVAJ + Cocaine is a Class A controlled drug subject to the provisions of the Misuse of Drugs Act 1971.

AZBAGS + glucose

B3D1SD + Cocaine was examined in SM-3.

B6H3ZH + COCAIN 41.3 % and GLUCOSE

BCD9DP + Cocaine hydrochloryde (33 % base) and glucose.

BD556C + Test Sample SM-3 found to contain Cocaine

BQNMYR + The sample was analysed with FTIR and GCMS in two different columns and solvents. The cocaine concentration was with GCMS by areas comparitions

BXCKYU +

C11111 + SM-3 sample includes Cocaine. there are also Tropaicocaine, Methylecgonine, Benzoylecgonine by impurities in sm-3 sample.

C5MOP5 + White powder with characteristic smell, containing by weight 42.1% cocaine expressed as free base and glucose

C8CCX2 + Test sample 2019/2/SM-3 having gross weight 06.00 gram(s) of white powder in amber glass bottle contains Cocaine as defined in the Section 2 of the CNS Act 1997 - Pakistan.

CAS0HP + this sample is cocaine

CBISZG + The powder was found to contain COCAINE at a concentration of (as amended) 35 per cent. COCAINE is controlled under the Misuse of Drugs Act 1971 (as amended) as a Class A drug.




Page 78 of 116

ICE 2019/2-SM

Code Cocaine

CD5XF1 + Sample 2019/2/SM-3 was found to contain cocaine.

CDVNVK + cocaine

CILAEB + Cocaine - confirmed with GCMS, FTIR, TLC Glucose - confirmed with FTIR and Wohlk reaction

COVWOU + Identified by GCMS & GC-FID techniques and quantified by GC-FID technique.

CXQPFE +

D67Z7M + Cocaine was identified in the sample 2019/2/SM3. First, colormietric test and Finally GC-MS.

DCOHUX +

DJDDMD + Presence of cocaine hydrochloride and glucose was detected in the sample. The sample also contaned multitude of trace level alkaloid impurities:tropococaine, benzoylecgonine, methyesterlecgonine.

DK6FK1 + THE SAMPLE 2019/2/SM3 WAS FOUND COCAINE

DKW45M + Cocaine is one of the most frequent drug in seized drugs analyzed in our laboratory

DSEBBS + Cocaine was identified with a retention time of 16.430 min by GC/MS. The concentration of sample infected in GC/MS was 208 ppm.

DTIACA + the sample contains cocaine, ecgonidine and dextrose

DZZZLS + In the 2019/2/SM-3 was proved the presence of cocaine and lactose. The quantification of cocaine as base was 39,0%.

E1ZARZ + Sample contains 40%Cocaine .

EI96ZN + THE SAMPLE CONTAIN LACTOSE

EIHUWT + cocaine

ELQO7L + Cocaine was identified by GC/MS and TLC; quantified by GC (FID)

F0RKYD + SM3 contient de la cocaine , ecgonine methyl ester

FCGG7O + The sample contains the substance cocaine.

FEVFVO + 228 milligrams of white powder Cocaine HCL (37% calculated as base) - Class A Glucose (indicated) - Not Controlled




Page 79 of 116

ICE 2019/2-SM

Code Cocaine

FFFLFF + 37% amount of Cocaine is found with the help of quantitative methods of GC-MS.

FJF0IF + the white powder contains cocaine (36.6%ww) wich is controlled by national law

FXP8PV + in sample 2019/2/SM-3, Cocaine was found.

FYKJPD + Glucose

G6GBTW + Cocaine and dextrose were detected in SM3 sample.

GC11E1 +

GDI9LV + SM-3 to contain Cocaine which is controlled under Malaysian Dangerous Drug Act 1952

GGGPGE + White powder analysed by GC/MS was found to contain COCAINE. Mass spectra was similar to CRM

GHKHWC +

GIGQ0G + After chemical analysis was performed the sample contains cocaine /Methylecgonine/ lactose

GIZGWR + Powder contains cocaine. Cocaine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016. The cocaine in this case is not exempt from control under subsection (1) of Section 3 of the Misuse of Drugs Act,1977 under the terms of the Misuse of Drugs (Exemption) Order, 2017. The Exemption Order does not provide for an exemption in respect of Section 15 of the Misuse of Drugs Act, 1977.

GPV0WG +

GQPYLA + SM-3 sample includes Cocaine. there are also Tropaicocaine, Ecgonidine, Ecgonine methyl ester, Anhydroecgonine methyl ester and benzoylecgonine by impurities in sm-3 sample.

GYEHYL +

H12HE2 +

H7XE2X + sample also is contains Ecgonidine, methyl ester & Tropacocain & Benzoylecgonine

H9RHNG + Mass spectrometry profile correlation between sample and reference material certified

HANMLJ + COCAINE

HASZSM + Mixture of cocaine and glucose (52.3 % w/w) and natural accompanying substances - ecgognines, cinnamoylcocaine




Page 80 of 116

ICE 2019/2-SM

Code Cocaine

HHEETQ + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 2. (2) Cocaine (benzolymethylecgonine) calculated as the hydrochloride 39% (w/w)

I2TTTT + Presence of cocaine in the concentration of 40.31%.

I4IIIW + Cocaine drug was confirmed at Rt of 13.18 min with precursor ion m/z of 304, fragments of 182.11772, 82.06519, 105.03360, 150.09151 and 119.04928

ICNCMG + COCAINE AND GLUCOSE

IE8EEE + Cocaine was detected in the sample.

IIIDYX +

IIILIY +

INOP4F + By GCMS/MS, we defected both cocaine and tropacaine. By LCMS/MS, we detected cocaine.

IRZAFP +

IWWWZH + SM-3 sample includes Cocaine. there are also Tropaicocaine, Ecgonidine, Ecgonine methyl ester, Anhydroecgonine methyl ester by impurities in sm-3 sample.

JCJJVA + The sample contains cocaine which is listed as a controlled drug according to french order, appendix I of February 22nd 1990.

JJPNJY + Cocaine was detected by GC-MS, confirmed and quantified by GC/FID

JJUJHH + On chemical analysis of a representative sample of the powder cocaine was detected with a purity of approximately 40% calculated as base.

JMYLYJ + White powder containing 32.1%w/w cocaine and glucose

JVPB7L + SM-3 contains Cocaine HCl. Quantitation Cocaine 38.05% as base

K6G1HJ + Cocaine

K8IZ1S + There is ilicit drug

K8NOCM + That I examined and analysed the said sample and found it to contain : controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine)

KAKGTD + OTHER COMPOUNDS FOUND: ANHYDROECGONINE METHYL ESTER




Page 81 of 116

ICE 2019/2-SM

Code Cocaine

KFKUP0 + Sample 2019/2/SM-3 a white powder gave a positive result for cocaine, substance under national legislation on drugs

KJFJIJ +

KKKQP7 + Marquis reagent test gave positive indication for cocaine or an amphetamine type drug. GCMS analysis confirmed presence of cocaine based on fragmentation pattern and retention time compared to a known standard. Quantitative analysis indicated 30% purity.

KLCHRH +

KPSSUB + WE FOUND A MIXTURE OF COCAINE AND GLUCOSE AS MAJORITY COMPONENTS.

KQKO2K + Amphetamine positive >8.8 µg / g Cocaine positive >8.8µg / g

KUD7YD + white powder containing 35.3% of cocaine

L9WDPM + Ecgonine methyl ester, cinnamoyl cocaine, benzoylecgonine detected

LDLJZA + A white powder which was a net weight of 196 milligrams and a purity range of 35% - 55% (reported as salt) which was found to be cocaine hydrochloride.

LG1AMG + Brown glass vial labelled 2019/2/SM-3 containing 0.23 grams of white powder. Analysis results; Cocaine (36%) and Glucose. Cocaine is a Class A controlled substance under the Misuse of Drugs Act 1971 (as amended). Glucose is not controlled under the aforementioned act.

LHOD3U + This sample was found to contain allopseudococaine and dextrose.

LKHTDW + 2019/2/SM-3 contains Cocaine. It also contains Tropacocaine, Anhydroecgonine methyl ester, ecgonine, norcocaine and trans/cis-cinamoyl cocaine

LUABFV + COCAINE 37,09%

LVRMSV + Also contains glucose.

LVUH0Z + Sample 2019/2/SM-3 was found to contain the controlled drug cocaine.

MBWNRJ + GC/MS told for presence of tropacocaine.

MIIFIV + Sample 2019/2/SM-3 found to contain cocaine.

MJDOQK + One brown glass vial containing 226 milligrams of white powder. This powder contained an average of 41% COCAINE HYDROCHLORIDE. COCAINE HYDROCHLORIDE is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended).




Page 82 of 116

ICE 2019/2-SM

Code Cocaine

MJYQ1I + -

MMVGH6 + methylecgonine, tropacaine

MOGXMB + From Screening test using (CT) and from confirmation test by (GC-MS) the sample was found to contain the controlled drug (Cocaine).

MTWM6W + SM-3 sample includes Cocaine. there are also Tropaicocaine, Ecgonidine, Ecgonine methyl ester, Anhydroecgonine methyl ester by impurities in sm-3 sample.

MUVGFL +

MWX4XX + was found COCAINE 38.5% +/- 1.6%

NE8ZAO + Blue colour with Cobalt thiocyanate test for Cocaine.TLC and GCMS gives result of Cocaine and Caffeine

NGJDWJ +

NNNNEI + contains drug according to law

O1HUPW + DEXTROSA E IMPUREZAS ALCALOIDALES (ACIDO BENZOICO, ECGONINA METIL ESTER, ECGONIDINA METIL ESTER, COCAETILENO, TROPACOCAINA, TRANS CINNAMOILCOCAINA Y BENZOILECGONINA).

OEOJOY + Controlled drug, Cocaine, present in sample. Concentration approx 37%

OHNQ7X +

OHS9XX +

OOWPNF + 1 glass bottle containing 0.22 grammes of a powder containing 0.08 grammes of cocaine.

OZOHOD + CONFIRMED BY GC MSD, THS SAMPLE ALSO CONTAINS SOME METABOLITES SUCH AS ECGONINE METHYL ESTHER, ANHYDRO ECGONINE METHYLESTHER, AND TROPACOCAINE

P8UQDW + Examination revealed the presence of Cocaine

PCQBJD + Also contain glucose.

PFZFOJ + The sample is in the form of white powder. It answers the tests for the presence of COCAINE.

PKNKQN + Sample contains Cocaine. HCl 40,3%

PLMLOM + The sample contains 35.36% of Cocaine, it contains also Benzoylecgonine and Ecgonine methyl ester.




Page 83 of 116

ICE 2019/2-SM

Code Cocaine

PPNIPX + cocaine

PQCCII +

PRZOZC +

PXAOXX + COCAINE +GLUCOSE

PXFATB +

PYUYVY + Sample SM3 contains Cocaine 36% +/-3

Q8ZQ82 + The sample obtains with the positive result with Cobalt thiocyanate reagent TLC: The Rf sample obtain with the same Rf Cocaine standard

QBIV4X + SM-3 was found to contain cocaine.

QFFJPH + GLUCOSE

QROQON + The white powdery substance contain 37.8% w/w of cocaine

RCRHBM + controlled subslance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonlne) calculated as the hydrochlorlde 41 % (w/w)

RG5OYA + Sample 2019/2/SM-3 contains COCAINA and DEXTROSE

RH2BU2 + This sample was found to contain Cocaine, which is a Class A controlled substance under the Misuse of Drugs Act 1971.

RRQFQQ +

RTQ8I7 + Cocaine is listed in the First Schedule of Dangerous Drug Acts 1952.

RZDHUH + SM-3 contains 35,0±1,4 weight% cocaine and glucose

S0C00Z + Sample 2019/2/SM-3 consists of white powder. Cocaine, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample

SDNBD6 - COCAINE

SFS5SX + 2019/2/SM-3 was confirmed for cocaine which is a scheduled II controlled substance in the US.

SOWSUC + In the powder cocaine is present.

STNCC9 + Blue colour with Cobalt Thiocyanate Test indicates that the possible presence of Cocaine. TLC and GCMS analysis show that SM-3 contains cocaine.




Page 84 of 116

ICE 2019/2-SM

Code Cocaine

SVRSSF + The sample contains cocaine.

TBUBCR + Test sample 2019/2/SM-3 found to contain cocaine

TBYTGT + The Test sample 2019/2/SM-3 was analyzed by Thin Layer Chromatography technique and was found to contain Cocaine and Glucose.

TE8ERE + Cocaine was detected in 2019/2/SM-3

TFF5SF + It was detected Cocaine in the analyzed sample.

TFKFT5 + positive for cocaine

TKLAER + Sample 2019/2/SM-3 contains Cocaine, Dextrose and Cocaine derivates as minor components such as Anhydroecgonine methyl ester, Ecgonine methyl ester, Tropacocaine and Cynnamoilcocaine Cis/Trans Isomers. Cocaine base concentration is 36.44%

TPYWQP + The test sample contained GLUCOSE

UFS8L8 +

UUNUSP + the analysis confirmed that SM3 contains COCAINE 35.0 %W/W (as controlled drug).

UXPP39 + In the sample SM2 was identified cocaine with esters of cocaine.

UYH68O + Cocaine

UYIOY3 +

V9FHUE +

VJJ2BS + No

VK9TBJ + glucose

VOFFDF + In the test sample 2019/2/SM-2 was detected cocaine

VOFIVV + Cocaine was detected in the SM-3 sample.

VSIQQM + /

VTGLIP + sample 2019/2/SM-3 was found to contain Cocaine

VTNITG + 35,62 +/- 3,21 % COCAÍNA BASE D-GLUCOSA




Page 85 of 116

ICE 2019/2-SM

Code Cocaine

WCDCCS +

WG1S1P + Cocaine is on the list of drugs.

WKVSHN + The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample, indicates the Cocaine presence.

WLWWWW + The sample contain cocaine, glucose

WRVOXF + One package containing 226 milligrams of a partially compressed white powder. This powder was found to contain cocaine hydrochloride (class A), with a purity of 36% in base form, and glucose (not controlled).

WU22AL + Cocaine, was detected in the powder, with a W:W percentage estimated at 37.83%

X1NYNN +

XO00Q0 + It is included in Table II Schedule I, Narcotic and Psychotropic Substances, used for medical purposes, approved by Government Decision 1088 of 05.10.2004

XSNN71 + Cocaine 35% (as base). Cocaine is classified as drug.

Y5OQGB + Cocaine was found in the sample 2019/2/SM-3

YARNPI + Cocaine .Hcl was identified in SM 3. Percentage as base is 34.3 %. In addition Ecgonine methyl ester was identified

YL6D6J + The sample contains cocaine

YY3YD4 + The sample contained 38.6% cocaine. The sample also contained benzoylecgonine, anhydroecgonine methyl ester, ecgonine methyl ester, tropacocaine and cinnamoylcocaine as minor components.

YYBTFT + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of DEXTROSE in the sample

ZAZMLT + Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with cocaine.

ZNRYRN + sample contains 27,6 % of cocaine

ZPRDAZ + Also contains Tropacocaine, Methylecgonine




Page 86 of 116

ICE 2019/2-SM



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

06JS66 I SI HPTLC

0GRT0S SI

111NTK I I SI I

1MA9MF I SI

224V2J I S

2HSS8S I I S Raman

2JJWOJ S I I

2UVXGU I S

3PP2PP I I

48PXX4 S SI I


50AP5Y S S S I I

5CPBXX I SI

60N30D S I

61XYO6 SI I

63AEKB I SI


6AX4TV I I

6ESG22 I I

6GM1ZU I SI I

6OTC3V SI I

75XFMQ S I I I

77JO7Q I SI

7KCDRK S I I

7RURX8 S SI SI

7WIJ9N S I


8NKZIO SI

8SMOGU SI

932LRK I SI I

9969TL S S S I I

999RGV S S S I

9ABUAU SI I





Page 87 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

9FFVN3 I SI I

9HXOHH I SI

9N59BB I I SI

9OO999 S S I I I

9OS0B5 S SI

A2HMLG SI

AA0UJR SI SI SI I

ACYVYR S S I I

AK3UYT SI

AM777O S S I

AMYZY0 SI S S I I I

AWGGYX I SI

AXAVAJ S S I

AZBAGS I SI I XRD


B6H3ZH SI

BCD9DP SI

BD556C SI I

BQNMYR S S SI I

BXCKYU SI S I

C11111 SI SI SI I

C5MOP5 I I

C8CCX2 S SI

CAS0HP S I I

CBISZG S S I

CD5XF1 S S SI

CDVNVK S S I

CILAEB S I I


CXQPFE I


DCOHUX SI S I I

DJDDMD S I I I S

DK6FK1 S S S I

DKW45M S S S I I

DSEBBS S S S I I

DTIACA S I I I I




Page 88 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DZZZLS SI S I I SI

E1ZARZ S I I

EI96ZN S I I

EIHUWT SI

ELQO7L S S S I I


FCGG7O S S I SI

FEVFVO S S I I

FFFLFF SI I SI SI

FJF0IF I SI

FXP8PV SI SI

FYKJPD SI I

G6GBTW I S I

GC11E1 S I I

GDI9LV S S SI I

GGGPGE S S S I

GHKHWC S S S I I

GIGQ0G S I I

GIZGWR I

GPV0WG I SI

GQPYLA SI SI SI I

GYEHYL I I SI

H12HE2 I

H7XE2X I SI I

H9RHNG I I

HANMLJ I SI I

HASZSM I I I S


I2TTTT SI

I4IIIW SI

ICNCMG I SI

IE8EEE S S S I I

IIIDYX S I SI I

IIILIY SI I


IRZAFP S I I

IWWWZH SI SI SI I




Page 89 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

JCJJVA I I

JJPNJY I SI I

JJUJHH S S I HRMS

JMYLYJ I I SI

JVPB7L S S I I I

K6G1HJ SI

K8IZ1S S SI S I I

K8NOCM S I I GC-IR


KFKUP0 S S I I

KJFJIJ S I I I

KKKQP7 SI I

KLCHRH S S I I


KQKO2K SI

KUD7YD I SI

L9WDPM I I S

LDLJZA S S S I I

LG1AMG S S I I

LHOD3U S I I


LUABFV S I

LVRMSV S I SI I

LVUH0Z S S S I SI


MIIFIV S I

MJDOQK S S S I I

MJYQ1I SI

MMVGH6 S SI


MTWM6 W SI SI SI I

MUVGFL S I

MWX4XX S I I

NE8ZAO S S S I I

NGJDWJ S I I

NNNNEI SI I SI




Page 90 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

O1HUPW S S I I

OEOJOY SI

OHNQ7X I

OHS9XX I S

OOWPNF S S I SI

OZOHOD SI I I

P8UQDW SI I SI

PCQBJD S I I I

PFZFOJ S S S I I

PKNKQN S I

PLMLOM SI I


PQCCII I S

PRZOZC SI I

PXAOXX S I I

PXFATB S S I

PYUYVY S S S I

Q8ZQ82 S S S I

QBIV4X S S I I

QFFJPH SI I

QROQON S S S I I I

RCRHBM S I I

RG5OYA S S I I

RH2BU2 S S I

RRQFQQ S I


RZDHUH I SI I

S0C00Z S S I

SDNBD6 I SI I

SFS5SX S I

SOWSUC SI I

STNCC9 S S SI I


TBUBCR S I


TE8ERE S S I

TFF5SF S S S I




Page 91 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

TFKFT5 SI

TKLAER S S I I

TPYWQP S S S I

UFS8L8 S I

UUNUSP S S S I

UXPP39 I

UYH68O S S I I

UYIOY3 S S I I

V9FHUE SI


VK9TBJ SI I

VOFFDF I

VOFIVV SI I

VSIQQM SI SI

VTGLIP S I I


WCDCCS I SI SI

WG1S1P S S S I I


WLWWW W S S I I I

WRVOXF S SI SI I I

WU22AL SI

X1NYNN SI I

XO00Q0 S S S I I

XSNN71 I I

Y5OQGB S I I


YL6D6J S S I I

YY3YD4 I SI

YYBTFT S S I I

ZAZMLT S S I

ZNRYRN SI

ZPRDAZ S S S I I




Page 92 of 116

ICE 2019/2-SM




06JS66 Heroin

0GRT0S heroin

111NTK Heroin

1MA9MF Heroine

224V2J Heroine

2HSS8S Heroin

2JJWOJ Diamorphine

2UVXGU heroine, codeine, MDPV,paracetamol, caffeine

3PP2PP heroin

48PXX4 heroïne

4BVR3P Diacetyl Morphine (Heroin)

50AP5Y heroin

5CPBXX heroin, morphine, 6-MAM

60N30D heroin

61XYO6 Héroïne and morphine

63AEKB heroin + 6MAM

64G4V7 HEROINE

6AX4TV heroin, caffeine, paracetamol, morphine

6GM1ZU Heroine

6OTC3V Heroine

75XFMQ Heroin and Morphine

77JO7Q HEROIN

7KCDRK Heroine, Morphine

7RURX8 HEROINE 18.4%

7WIJ9N Heroin

8IXSA9 Heroin

8NKZIO heroin

8SMOGU diacetylmorphine, monoacetylmorphine, acetylcodeine

932LRK Heroin

9969TL Narcotine/Noscapine, Caffeine, Paracetamol, Acetylcodeine, 6-monoacetylmorphine, Diacetylmorphine and Papaverine.

999RGV HEROINE,6-MONOACETYLMORPHINE (6-MAM)

9ABUAU Heroin

9FFVN3 HEROIN

9HXOHH heroin and morphine

9N59BB Heroin

9OO999 HEROIN, MORPHINE

9OS0B5 heroin




Page 93 of 116

ICE 2019/2-SM


A2HMLG heroin

AA0UJR Heroin

ACYVYR heroin

AK3UYT Heroin

AM777O Heroin

AMYZY0 heroine

AWGGYX Diamorphine

AXAVAJ Diamorphine (Heroin)

AZBAGS heroine base

B3D1SD Heroin

B6H3ZH HEROIN

BCD9DP Heroïne and 6-MAM

BD556C Heroin, Morphine, Monoacetylmorphines

BQNMYR paracetamol, caffeine, heroin, morphine, acetylcodeine

BXCKYU opiates

C11111 Heroin

C5MOP5 heroin + 6MAM + Morphine

C8CCX2 Heroin, Acetyl Codeine, Monoacetyl Morphine, Codeine, Morphine

CAS0HP heroin

CBISZG DIAMORPHINE, Caffeine, Paracetamol

CD5XF1 Heroin, monoacetylmorphines, caffeine, noscapine and papaverine.

CDVNVK heroin and monoacetylmorphine

CILAEB Heroine

COVWOU HEROIN

CXQPFE Heroine, morphine, 6-acetylmorphine

D67Z7M Heroine and 6-monoacetylmorphine

DCOHUX HEROINA

DJDDMD Heroin, morphine

DK6FK1 HEROINE, MORPHINE, CAFFEINE AND PARACETAMOL

DKW45M HEROIN

DSEBBS Morphine, 6-Monoacetylmorphine and Heroin

DTIACA heroine

DZZZLS HEROIN + CAFFEINE + PARACETAMOL

E1ZARZ Heroin

EI96ZN HEROIN 16,7%

EIHUWT heroin

ELQO7L Heroin, 6-MAM, 6-Acetylcodeine

F0RKYD Héroïn And morphine

FCGG7O Heroin, acetylcodeine and 6-monoacetylmorphine

FEVFVO Heroin

FFFLFF Heroine, Morphine, 6-MAM

FJF0IF heroin




Page 94 of 116

ICE 2019/2-SM


FXP8PV Heroin

FYKJPD Heroine-diacetylmorphine

G6GBTW Heroin

GC11E1 Heroin

GDI9LV Heroin, Caffeine, Paracetamol

GGGPGE HEROIN

GHKHWC Heroin,morfin,acetylcodein,paracetamol

GIGQ0G Morphine / heroin

GIZGWR Heroin (Diamorphine)

GPV0WG heroin

GQPYLA Heroin

GYEHYL caffeine,paracetamol

H12HE2 Heroine

H7XE2X Heroin (Diacetylmorphine) & 6-Monoacetylmorphine

H9RHNG Heroin

HANMLJ HEROINE ,CAFFEINE , 6MAM and NASCAPINE

HASZSM Heroin

HHEETQ Heroin

I2TTTT Heroine and 6-MAM

I4IIIW Heroin

ICNCMG HEROINE

IE8EEE Heroin

IIIDYX heroine

IRZAFP heroin, morphine

IWWWZH Heroin

JCJJVA Heroin

JJPNJY eroine

JJUJHH Heroin. Morphine

JMYLYJ heroin

JVPB7L Heroin

K6G1HJ Heroine and Morphine

K8IZ1S Heroin and 6-Monoacetilmorphine

K8NOCM Heroin

KAKGTD HEROIN

KFKUP0 heroin

KJFJIJ heroina

KKKQP7 Heroin (Diamorphine)

KLCHRH O6 MONOACETYLMORPHINE-HEROINE

KPSSUB HEROIN, CAFFEINE, PARACETAMOLE, MECONIN AND 6-ACETYLMORPHINE

KQKO2K Morphine

KUD7YD heroin, morphine, 6-mam

L9WDPM Heroine, Morphine




Page 95 of 116

ICE 2019/2-SM


LDLJZA Diamorphine (Heroin)

LG1AMG Diamorphine

LHOD3U Heroin

LKHTDW Morphine and Heroin

LUABFV HEROIN AND MORPHINE

LVRMSV heroine

LVUH0Z Heroin

MBWNRJ heroin

MIIFIV Heroin, Morphine

MJDOQK DIAMORPHINE

MJYQ1I Heroin,Morphine

MMVGH6 heroin

MOGXMB Heroin, Morphine, Codeine, Acetylcodeine, Paracetamol, Meconin, Noscapine, Papaverine, 6-monoacetylmorphine, and caffeine

MTWM6W Heroin

MUVGFL Heroine

MWX4XX HEROINE, 6 MONOACETYLMORPHINE

NE8ZAO Heroin

NGJDWJ HEROINE

NNNNEI heroine, morphine, monoacetylmorphine

O1HUPW HEROINA BASE

OEOJOY Heroine

OHNQ7X HEROIN

OHS9XX Heroin

OOWPNF Heroin

OZOHOD HEROINE

P8UQDW Heroin

PCQBJD heroine, morphine

PFZFOJ DIACETYL MORPHINE (HEROIN)

PKNKQN Heroin

PLMLOM Heroine

PPNIPX heroin

PQCCII Amphétamine

PXAOXX PARACETAMOL,HEROIN,CAFFEINE

PXFATB Heroin

PYUYVY Heroin

Q8ZQ82 Heroine and Lidocaine

QBIV4X Heroin and monoacetylmorphines

QFFJPH HEROIN BASE

QROQON Heroin

RCRHBM Heroin

RG5OYA HEROIN




Page 96 of 116

ICE 2019/2-SM


RH2BU2 Heroin, Paracetamol & Caffeine

RRQFQQ Morphine

RTQ8I7 Heroin, 6-monoacetylmorphine

RZDHUH heroin

S0C00Z Heroin

SDNBD6 OPIUM/OPIATES

SFS5SX Heroin, Acetaminophen, Caffeine

SOWSUC heroin

STNCC9 Heroin,6-monoacetyl morphine,Caffeine

SVRSSF Heroine

TBUBCR heroin

TBYTGT Heroin, Morphine,Caffeine, Acetaminophen,6-Acetylmorphine, 6-Acetyl Codeine, Papaverine, Noscapine

TE8ERE Heroin, Cafffeine and Paracetamol

TFF5SF Heroin

TFKFT5 heroin

TKLAER 6-Monoacetylmorphine, Heroin, Morphine and Codeine

TPYWQP HEROIN Base

UFS8L8 HEROIN

UUNUSP HEROINE

UXPP39 Heroine

UYH68O Heroin and 6 Monoacetilmorphine

UYIOY3 Heroin

V9FHUE HEROIN

VJJ2BS Heroine

VK9TBJ heroine

VOFFDF heroine

VOFIVV Heroin

VSIQQM Heroine

VTGLIP Acetaminophen, Heroin, Morphine

VTNITG HEROÍNA HCL

WCDCCS heroin

WG1S1P Heroin

WKVSHN Heroin, Caffeine, Paracetamol, Acetylcodeine and 6-monoacetylmorphine

WLWWWW heroin

WRVOXF Heroin (Diamorphine)

WU22AL Heroin

X1NYNN Heroin

XO00Q0 Heroine

XSNN71 Heroin

Y5OQGB Heroine

YARNPI Diacetylemorphine (Heroin)




Page 97 of 116

ICE 2019/2-SM


YL6D6J Heroin

YY3YD4 Heroin

YYBTFT HEROINE + PARACETAMOL + CAFFEINE + LIDOCAINE

ZAZMLT HEROIN

ZNRYRN Heroine

ZPRDAZ Heroin




Page 98 of 116

ICE 2019/2-SM


Code Caffeine Heroin Paracetamol (Acetaminophen)

06JS66 + + + The sample was subjected to HPTLC using silicagelF254 as stationary phase and Ethylacetate:Methanol:Ammonia 85:10:5 as MP. After development the chromoplate was scanned and the UV Spectrum obtained was compared with the Library UV Spectra.They were found to match with 6-MAM, DAM,Caffeine and Noscapine. There was anothter peak in the chromatogram which could not be identified which was very close to Noscapine. Therefore HPTLC was repeated with Chloroform and Ethanol 9:1 as the MP and was found to contain Paracetamol. It was repeated again along with Paracetamol and was found to be parcetamol after both RF and UV Spwxtra were found similar. For Confirmation the SM4 was subjected to GC-MS choosing general method for basic drugs on HP 5 column and Caffeine, 6-Acetylcodeine, 6-MAM,DAM, Paracetamol and Noscapine were found based on library spectra. A small peak corresponding to PAPAverine was also noticed but ignored as it is too small to confirm. Then Standard Caffeine, DAM, Paracetamol and Noscapine reference material were injected into the system and RT and Mass spectral fragmentation compared and were found to be similar. Thus the presence of DAM, Paracetamol, Caffeine and Noscapine were confirmed. 6-MAM and 6-Acetyl Codeine were also confirmed based on library spectrum. RT could not be compared for these drugs due to non availability of reference standards. Further the sample is subjected to Marquis test and tested positive for Opiates. 0GRT0S + + + Heroin was detected by GC-MS and quantified by GC-FID

111NTK + + - It was found 6-monoacetylmorphine and caffeine

1MA9MF ANP + ANP

224V2J + + +

2HSS8S + + + The sample contains heroin. The concentration has not been determined.

2JJWOJ + + - The brown powder was analysed and found to contain heroin (diamorphine).

2UVXGU + + + he main compounds we found in SM-1 are heroine, codeine, MDPV,paracetamol, caffeine and MDPV after TLC . with screening we found 2,5-dimethoxyamfetamine and hydrocodone.

3PP2PP + + - The sample is a powder containing heroin at 17.19 % purity and also 6-monoacetylmorphine and caffeine are present

48PXX4 - + - Monoacétylmorphine 18% noscapine 18% paracétamol 18% caféine 13% acétylcodéine papavérine

4BVR3P + + + The sample is in the form of light brown powder. It answers the test for the presence of Diacetyl Morphine (Heroin), paracetamol, caffeine and mono acetyl morphine

50AP5Y + + + Caffeine and Paracetamol

5CPBXX + + + Heroin, morphine and 6-MAM are controlled by the law of 7th February 2014 and the RD of 6th September 2017




Page 99 of 116

ICE 2019/2-SM


60N30D + + + Sample SM-4 was found to contain heroin

61XYO6 + + + Héroïne and morphine are sheduled as illicit drugs in France

63AEKB + + + heroin (11.98%ww), 6MAM (14.73%ww), caffeine, paracetamol

64G4V7 + + + The sample contains heroine. Apart from heroine the sample contains caffeine, paracetamol and small amounts of noscapine, papaverine, 6-MAM, acetylcodein. Heroine is controlled in Poland. 6AX4TV + + + The sample contains heroin, noscapine, caffeine, paracetamol, morphine (trace amount). Heroin and morphine are scheduled as illicit drug in France.

6ESG22 - + -

6GM1ZU + + + Caffeine, Paracetamol

6OTC3V + + - It has been detected the presence of heroine and by-products of acetylation of morphine in the sample

75XFMQ + + + Paracetamol,Caffeine,Morphine,Acetylcodeine,06-Monoacetylmorphine,Papaverin, Narcotin

77JO7Q + + + sample also contains paracetamol and caffeine

7KCDRK + + + Heroine + Morphine+ Caffeine + Paracetamol Morphine was founded in trace

7RURX8 + + +

7WIJ9N + + ANP Detected heroin and Caffeine as adulterant.

8IXSA9 + + - SM4 was containe15% heroin

8NKZIO + + + paracetamol(acetaminophen), caffeine,

8SMOGU + + + the substance is heroin containing diacetylmorphine, monoacetylmorphine, acetylcodeine

932LRK + + + Caffeine and Paracetamol

9969TL + + + Using the techniques CR, TLC, FT-IR, GC-FID & GC-MS, sample SM-4 was found to contain Narcotine/Noscapine, Caffeine, Paracetamol, Acetylcodeine, 6-monoacetylmorphine, Diacetylmorphine and Papaverine.

999RGV + + + 1-NARCOTIC. Lists I and IV Single Convention 1961 2-List I of the Single Convention of 1961

9ABUAU + + +




Page 100 of 116

ICE 2019/2-SM


9FFVN3 + + + HEROIN AND TRACE AMOUNTS OF MORPHINE. THE SAMPLE ALSO CONTAINED CAFFEINE AND ACETAMINOPHEN.

9HXOHH - + ANP The sample SM-4 contains heroin 20.67 % m/m, morphine 0.71 % and other compounds usually present in heroin.

9N59BB + + - Brown powder containing Heroin. Caffeine, acetylcodeine, monoacetylmorphine, acetylthebaol, papaverine and noscapine were also detected.

9OO999 + + + Light brown powder that contains controlled substances heroin, morphine, 6-monoacetylmorphine and substances caffeine and paracetamol (acetaminophen)

9OS0B5 + + + Paracetamol (Acetaminophen), caffeine, 6-Monoacetylmorphine

A2HMLG + + + test sample 2019/2/sm4 contained 19.2%ww DAM, 6-MAM, acetylcodeine and meconin

AA0UJR + + + adulterants: caffeine, paracetamol, 6-MAM, morphine (remains)

ACYVYR + + +

AK3UYT + + -

AM777O + + + Test Sample 2019/2/SM-4 was found to contain Heroin, confirmed by Gas-Chromatography - Mass Spectrometry.

AMYZY0 + + ANP SM 4 For presumptive tests a positive Marquise reaction was obtained. CG/MS fragmentation pattern obtained with sample SM 4 are equivalent to those obtained with heroine, codeine, caffeine , papaverine and noscapine.This finding indicates that heroine controlled drug is present in the test sample.

AWGGYX + + + The sample was found to contain 17.5% of diamorphine (as base).

AXAVAJ + + + Diamorphine is a Class A controlled drug subject to the provisions of the Misuse of Drugs Act 1971.

AZBAGS + + + acetominophen, caffeine, acetylcodeine, O-6-monoacetylmorphine, diacetylmorphine, papaverine, noscapine

B3D1SD - + - Heroin was examined in SM-4.

B6H3ZH + + + HEROIN 18.5%, NOSCAPIN 19.7 %, ACETYLCODEINE, O6 MAM, ACETYLCODEINE, PAPAVERINE, ACETAMINOPHEN 13.9%, CAFFEIN 14.4%, MORPHIN traces

BCD9DP + + + Heroin (18 % base), 6-MAM, acetylcodeine, papaverine, noscapine (18 %), acetaminophen (15 %), caffeine (14 %).

BD556C + + + Test Sample SM-4 found to contain Heroin, Morphine, Monoacetylmorphines, Papaverine, Noscapine, Paracetamol and Caffeine.




Page 101 of 116

ICE 2019/2-SM


BQNMYR + + + The sample was analysed with colorimetric test, FTIR and GCMS in two different columns and solvents

BXCKYU + + +

C11111 + + + SM-4 sample includes Heroin,6-Monoasetylmorphine, Morphine, Meconine, Acetylcodeine, Thebaol, Papaverine and noscapine. there are also caffeine and paracetamol by adulterants in sm- 4 sample.

C5MOP5 + + + Brown powder with characteristic smell, containing by weight 23.3% heroin expressed as free base. It contains also caffeine and paracetamol

C8CCX2 + + + Test sample 2019/2/SM-4 having gross weight 05.93 gram(s) of brown powder in amber glass bottle contains Narcotic and Psychotropic substances namely Heroin, Acetyl Codeine, Monoacetyl Morphine (Opium Derivatives), Codeine, Morphine, Papaverine and Noscapine (Opium Alkaloids) as defined in the Section 2 of the CNS Act 1997 - Pakistan. Moreover, Acetaminophen and Caffeine (Non-Controlled substances) were also detected.

CAS0HP + + + this sample is heroin

CBISZG + + + The powder was found to contain DIAMORPHINE at a concentration of (as amended) 17 per cent. Caffeine and paracetamol were also present in the powder. DIAMORPHINE is controlled under the Misuse of Drugs Act 1971 (as amended) as a Class A drug. Caffeine and paracetamol are not controlled under the Misuse of Drugs Act 1971 (as amended).

CD5XF1 + + + Sample 2019/2/SM-4 found to contain 6.3 % of heroin. 6.4 % of monoacetylmorphines, caffeine, noscapine and papaverine.

CDVNVK + + + heroin and monoacetylmorphine

CILAEB + + + Heroine - confirmed with GCMS, FTIR, TLC; also heroine decomposition products were found (6- monoacetylmorphine, papaverine, noscopine) Caffeine, acetaminophene - confirmed with GCMS, FTIR

COVWOU + + + Identified by GCMS & LCMSMS techniques and quantified by GC-FID technique. Found the presence of 6-Monoacetylmorphine, Acetocodeine,caffine, Paracetamol, Papavarine, Noscapine and Morphine in traces along with the Heroin drug.

CXQPFE + + +

D67Z7M + + + Heroine and 6-monoacetylmorphine was identified in the sample 2019/2/SM4. First, colormietric test and Finally GC-MS.

DCOHUX + + -

DJDDMD + + + Presence of heroin hydrochloride, paracetamol and caffeine was detected in the sample. The sample also contained acetylcodeine, 6-MAM, papaverine, noscapine, morphine, acetylthebaol and trace amount of meconine.




Page 102 of 116

ICE 2019/2-SM


DK6FK1 + + + THE SAMPLE 2019/2/SM4 WAS FOUND HEROINE, MORPHINE, CAFFEINE AND PARACETAMOL

DKW45M + + + Heroin is one of the most frequent drug in seized drugs analyzed in our laboratory

DSEBBS + + + Morphine, 6-Monoacetylmorphine and Heroin were identified with the retention time of 19.746min, 20.933 min and 22.448 min, respectively. The concentration injected in GC/MS was 206 ppm.

DTIACA + + + the sample contains heroine, morphine, acethylcodeine, 6MAM papaverine, noscapine, paracetamol, caffeine

DZZZLS + + + In the 2019/2/SM-4 was proved the presence of heroin, caffeine and paracetamol.

E1ZARZ + + + Sample contains 22%Heroin and Paracetamol (Acetaminophen) ,Caffeine

EI96ZN + + + THE SAMPLE CONTAIN: PARACETAMOL, CAFFEINE, 6-MONO ACETYLMORPHINE, PAPAVERINE, NOSCAPINE AND ACETYLCODEINE

EIHUWT + + + heroin, acetaminophen, acetyl codeine, papaverine, 6-monoacetylmorphine

ELQO7L + + + Heroin, 6-MAM and 6-Acetylcodeine were identified by TLC & GCMS. Heroin was quantified by GC (FID).

F0RKYD + + + SM4 contient de la morphine , heroine 6-monoacethylmotphine,acethylcodeine,noscapine et papaverine , coupez a la paracetamol et a la caffeine

FCGG7O - + - The sample contains the substances heroin, acetylcodeine and 6-monoacethylmorphine.

FEVFVO + + + 222 milligrams of brown powder Diamorphine (commonly known as Heroin) (18% calculated as base) - Class A Caffeine - Not Controlled Paracetamol - Not Controlled

FFFLFF + + + 21% amount of Heroine is found with the help of quantitative methods of GC-MS. Beside, we have identified that Morphine and 6-MAM are present. Also, we have observed that Parasetamol and Caffeine are present.

FJF0IF + + + the brown powder contains diacetylmorphine (19.8%ww), monoacetylmorphine (18.7%ww), and 6- acetylcodeine (not quantified) wich are controlled by national law. the sample contains caffeine and paracetamolo to.

FXP8PV + + + in sample 2019/2/SM-4, Heroin was found

FYKJPD + + + caféine paracétamol

G6GBTW + + + Heroin, noscapine, caffeine, acetominophen, papaverine, acetylcodeine and acetylmorphine were detected in SM4 sample.




Page 103 of 116

ICE 2019/2-SM


GC11E1 + + +

GDI9LV + + + SM-4 to contain Heroin which is controlled under Malaysian Dangerous Drug Act 1952. SM-4 to contain Caffeine and Paracetamol which is controlled under Malaysian Poisons Act 1952

GGGPGE + + ANP Light brown powder analysed by GC/MS was found to contain HEROIN, 6-MAM & CAFFEINE. Every mass spectra was similar to CRM

GHKHWC - + -

GIGQ0G + + + After chemical analysis was performed the sample contains Morphine / heroin /caffeine / paracetamol / 6 MAM / 6 Acetylcodeine

GIZGWR + + + Powder contains heroin (diamorphine) and indications of paracetamol and caffeine. Diamorphine is a controlled drug under the Misuse of Drugs Acts, 1977 to 2016.

GPV0WG - + -

GQPYLA + + + SM-4 sample includes Heroin,6-Monoacetylmorphine, Morphine, Codeine, Asetylcodeine, Papaverine and noskapine. there are also caffeine and paracetamol by adulterants in sm-4 sample.

GYEHYL + + +

H12HE2 - + -

H7XE2X + + - sample also is contains Caffeine & Meconin & Acetylcodeine & Papaverine & Noscapine

H9RHNG + + + Mass spectrometry profile correlation between sample and reference material certified

HANMLJ + + - HEROINE,CAFFEINE,6MAM and NASCAPINE.

HASZSM + + + Mixture of heroin, caffeine and Paracetamol (Acetaminophen) and traces of noscapine, papaverine, acetyl morphine, acetyl codeine a morphine

HHEETQ + + + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 1. (10) Diacetylmorphine (heroin) calculated as the base 17% (w/w) The sample was found to contain the following substance(s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified : Acetaminophen. Should you need this (these) detected substance(s) to be certified, please contact us The sample was found to contain the following non-controlled substance(s) has (have) been detected but not certified : Caffeine. Should you need this (these) detected substance(s) to be certified, please contact us

I2TTTT + + - Presence of heroine in the concentration of 18.80%; with 6-monoacethyl morphine in the concentration of 19.34%. Presence also of caffeine and noscapine (less abundant).




Page 104 of 116

ICE 2019/2-SM


I4IIIW + + + Heroin drug was confirmed at Rt of 12.86 minutes with precursor ion m/z 370 with precursor ions of m/z 58.06575, 268.13239, 211.07475, 328.15329 and 193.06432

ICNCMG + + + WAS FOUND TO CONTAIN THE HEROINE, MORPHINE, CODEINE, NOSCAPINE, PAPAVERINE CAFFEINE AND PARACETAMOL

IE8EEE + + + Heroin, 6-Monoacetylmorphine, caffeine and Paracetamol (Acetaminophen), were detected in the sample.

IIIDYX + + + 6-MAM, coffeine, noscapine, acetyl-codeine, paracetamol

IIILIY + + +

INOP4F - ANP ANP The sample was not submitted. It was not received

IRZAFP + + +

IWWWZH + + + SM-4 sample includes Heroin,6-Monoasetylmorphine, Morphine, Codeine, Asetylcodeine, Papaverine and noskapine. there are also caffeine and paracetamol by adulterants in sm-4 sample.

JCJJVA + + + The sample contains heroin which is listed as a controlled drug according to french order, appendix I of February 22nd 1990.

JJPNJY + + + eroine was detected by GC/MS, confirmed and quantified by GC-FID. There are also present: acetylcodeine, caffeine, paracetamolo, 6-monoacetylmorphine

JJUJHH + + + On chemical analysis of a representative sample of the powder heroin was detected with a purity of approximately 20% calculated as base. Morphine, caffeine and paracetamol were also detected.

JMYLYJ + + + brown powder containing 18.2%w/w heroin, 23.9%w/w 6-MAM, paracetamol, caffeine, noscapine and meconin, acetylcodeine

JVPB7L + + + SM-4 contains Heroin 19.05% as base, Morphine, 6-MAM, Acetyl codeine, papaverine, Paracetamol, Caffeine

K6G1HJ + + + Found heroine, morphine, caffeine, paracetamol, 6-acetylmorphine and acetylcodein

K8IZ1S + + + There are ilicit drugs

K8NOCM + + ANP That I examined and analysed the said sample and found it to contain : controlled substance (s)witin the meaning of the Controlled Drugs and Substances Act: Schedule I 1. (10) Diacetylmorphine (heroin) The following non-controlled substance(s) has (have) been detected but not certified: Caffeine Should you need this (these) detected substance(s) to be certified, please contact us.

KAKGTD + + + OTHER COMPOUNDS FOUND: MECONING ACID, ACETYLCODEINE, O-6- MONOACETILMORPHINE




Page 105 of 116

ICE 2019/2-SM


KFKUP0 + + + Sample 2019/2/SM-4 a beige powder gave a positive result for heroin, substance under national legislation on drugs.Caffeine was also detected.

KJFJIJ - + -

KKKQP7 + + - Marquis reagent test gave positive indication for an opiate type drug. GCMS analysis confirmed presence of heroin (diamorphine) and caffeine based on their fragmentation patterns and retention times compared to known standards. Quantitative analysis of diamorphine indicated 18% purity.

KLCHRH + + + CAFFEINE - ACETAMINOPHEN - ACETYLCODEINE - PAPAVERINE - NARCOTINE

KPSSUB + + + WE FOUND A MIXTURE OF HEROIN, CAFFEINE, PARACETAMOLE AS MAJORITY COMPONENTS.

KQKO2K ANP ANP ANP Morphine positive >8.9µg / g

KUD7YD + + + brown powder containing 1.2% of morphine, 17.3% of heroin and 15.2% of 6-mam

L9WDPM + + + 6-MAM, acetaminophen, caffeine, codeine, papaverine detected

LDLJZA + + + A brown powder which had a net weight of 195 milligrams and a purity range of 5% - 25% (reported as base) which was found to be diamorphine, paracetamol and caffiene.

LG1AMG + + + Brown glass vial labelled 2019/2/SM-4 containing 0.23 grams of brown powder. Analysis results; Diamorphine (18%) and Caffeine and Paracetamol. Diamorphine is a Class A controlled substance under the Misuse of Drugs Act 1971 (as amended). Caffeine and paracetamol are not controlled under the aforementioned act.

LHOD3U + + - Presence of heroin was detected in the sample. The sample also contains caffeine, acetylcodein, 6- monoacetylmorphine, diacetylmorphine, isoquinoline and noscapine.

LKHTDW + + + 2019/2/SM-4 contains Morphine and Heroin. It also contains Paracetamol, Caffeine, Codeine, O-6- monoacetylmorphine and Papaverine.

LUABFV + + + HEROINE 18,68%, MORPHINE, CAFEINE AND PARACETAMOL

LVRMSV + + + Also contains 6-Monoacetylmorphine, coffeine, noscapine, acetyl-codeine, paracetamol

LVUH0Z + + + Sample 2019/2/SM-4 was found to contain the controlled drug heroin. The sample was also found to contain paracetamol and caffeine.

MBWNRJ + + + the GC/MS told for the presence of paracetamol, caffeine, 6MAM, Diacetilmorphine, papaverine, noscapine and the presence of morphine as trace.

MIIFIV ANP + ANP Sample 2019/2/SM-4 found to contain Heroin and Morphine.




Page 106 of 116

ICE 2019/2-SM


MJDOQK + + + One brown glass vial which contained 223 milligrams of brown powder. This powder contained an average of 18% DIAMORPHINE (COMMONLY KNOWN AS HEROIN). DIAMORPHINE is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended). MJYQ1I - + ANP -

MMVGH6 + + + 6-MAM, paracetamol, caffeine, papaverine, noscapine,acethyl codeine

MOGXMB + + + From Screening test using (MR) and from confirmation test by (GC-MS) the sample was found to contain the following drugs and adulterants (Heroin, Morphine, Codeine, Acetylcodeine, Paracetamol, Meconin, Noscapine, Papaverine, 6-mono-acetylmorphine, and caffeine).

MTWM6W + + + SM-4 sample includes Heroin,6-Monoasetylmorphine, Morphine, Codeine, Asetylcodeine, Papaverine and noskapine. there are also caffeine and paracetamol by adulterants in sm-4 sample.

MUVGFL + + + This sample was adulterated with caffeine and paracetamol.

MWX4XX + + + was found too paracetamol and caffein

NE8ZAO - + - Violet colour with Marquis test.TLC and GCMS also gives Heroin result.

NGJDWJ + + +

NNNNEI + + + contains drug according to law

O1HUPW + + + CAFEINA, ACETAMINOFEN Y OPIACEOS (MECONICA, HIDROCOTAMINA, CODEINA, MORFINA, ACETATO DE CODEINA, MONOACETILMORFINA, PAPAVERINA Y NOSCAPINA).

OEOJOY + + + Controlled drug, Heroine, present in sample. Concentration approx 16%. Caffeine and Paracetamol (no controlled drugs) was also present in sample.

OHNQ7X ANP + ANP

OHS9XX - + -

OOWPNF + + + 1 glass bottle containing 0.22 grammes of a solid containing 0.03 grammes of heroin.

OZOHOD + + + THIS SAMPLE ALSO CONTAINS ACETAMINOPHEN, CAFFEINE, ACETYL CODEINE, 6-O-MAM, PAPAVERINE AND NOSCAPINE

P8UQDW - + - Examination revealed the presence of Heroin

PCQBJD + + + Sample also contain: acetaminophen, noscapine, papaverine, caffeine, codeine, acethylcodeine, 6- monoacethylmorphine.




Page 107 of 116

ICE 2019/2-SM


PFZFOJ + + + The sample is in the form of light brown powder. It answers the tests for the presence of Diacetylmorphine (Heroin), paracetamol, Caffeine and monoacetylmorphine.

PKNKQN + + - Sample contains heroin 13.3%

PLMLOM + + + The sample contains 24.33% of Heroine. It contains also 0.76% Morphine as a minor component, Hydromorphone, Paracetamol, Caffeine, 6-monoacetylmorphine, Acetyl codeine, Papaverine and Noscapine.

PPNIPX + + - heroin, caffeine

PQCCII + - -

PRZOZC + + +

PXAOXX + + + PARACETAMOL,HEROIN,CAFFEINE,O6MONOACETYLMORPHINE, NOSCAPINE.

PXFATB + + - We detected also caffei ne, acetyl codeine and 6-monoacetyl morphine

PYUYVY - + + Sample SM4 contains Heroin 19% +/-2, and paracetamol, caffeine, acetylcodein, 6-MAM, papaverine i noscapin

Q8ZQ82 ANP + ANP The sample obtains with the positive result with Marquis reagent and Cobalt thiocyanate reagent TLC: The Rf sample obtain with the same Rf Heroine and Lidocaine standard

QBIV4X + + + SM-4 was found to contain heroin, monoacetylmorphines and also contain acetylcodeine, acetaminophen, caffeine and noscapine.

QFFJPH + + + PARACETAMOL CAFFEIN MORPHIN ACETYLCODEIN MAM PAPAVERINE NOSCAPINE ACETYLTHEBAOL

QROQON + + + The sample contain 16.5% w/w Heroin.

RCRHBM + + + controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 1. (10) Dlacetylmorphlne (heroin) calculated as the hydrochloride 20 % (w/w). The following substance(s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified: acetaminophen The following non-controlled substance(s) has(have) been detected but not certified: Caffeine

RG5OYA + + + Sample 2019/2/SM-4 contains PARACETAMOL, CAFEINE, HEROIN, PAPAVERINE, NOSCAPINE, 6-MONOACETILMORPHINE.




Page 108 of 116

ICE 2019/2-SM


RH2BU2 + + + This sample was found to contain Heroin, which is a Class A controlled substance under the Misuse of Drugs Act 1971. This sample was also found to contain Paracetamol and Caffeine which are not controlled under the Misuse of Drugs Act 1971.

RRQFQQ ANP - ANP

RTQ8I7 + + + Heroin and 6-monoacetylmorphine is listed in the First Schedule of Dangerous Drug Acts 1952. RZDHUH - + + SM-3 contains 17,6±1,0 weight% heroin SM-3 contains also paracetamol, meconine, caffeine, acetyl-codeine, O-6-monoacetyl-morphine, papaverine, noscapine

S0C00Z ANP + ANP Sample 2019/2/SM-4 consists of brown powder. Heroin, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample

SDNBD6 + - + HEROIN, ACETYLCODEINE, PAPAVERINE, NOSCAPINE

SFS5SX + + + 2019/2/SM-4 was confirmed for heroin which is a scheduled I controlled substance, acetaminophen and caffeine which are not controlled substances in the US.

SOWSUC + + + In the powder heroin is present (~36 % as base). Also paracetamol and caffeine were identified and other compounds present in heroin powders (eg. papaverine, noscapine, ..)

STNCC9 + + ANP Violet colour with Marquis Test indicates possible presence of opiates. TLC and GCMS analysis shows that SM-4 contains heroin, 6-monoacetyl morphine and caffeine.

SVRSSF - + ANP The sample contains heroine.

TBUBCR + + + Test sample 2019/2/SM-4 found to contain heroin, caffeine and paracetamol

TBYTGT + + + The Test sample 2019/2/SM-4 was analyzed by Thin Layer Chromatography technique and was found to contain Heroin, Morphine,Caffeine, Acetaminophen,6-Acetylmorphine, 6-Acetyl Codeine, Papaverine and Noscapine

TE8ERE + + + Heroin, Cafffeine and Paracetamol were detected in 2019/2/SM-4.

TFF5SF + + - It was detected heroin in the analyzed sample. It was also detected caffeine in the analyzed sample.

TFKFT5 + + + Positive for heroin

TKLAER + + + Sample 2019/2/SM-4 contains 6-monoacetylmorphine, Heroin, Morphine, Codeine, Caffeine, Acetaminophen, 6-Acetylcodeine, Papaverine, Noscapine and Tebalol. Heroin as base concentration is 24.45%

TPYWQP - + + The test sample contained PARACETAMOL (acetaminophen).The test sample also contained acetylcodeine, 6-monoacetylmorphine, and papaverine as minor components.




Page 109 of 116

ICE 2019/2-SM


UFS8L8 + + + ACETAMINOPHEN, CAFFEINE, ACETIL CODEINE, 6-MAM, ACETILTEBAOLE, PAPAVERINE, NOSCAPINE

UUNUSP + + + the analysis confirmed that SM3 contains HEROINE 21.4 %W/W (as controlled drug). We found also acetominophen, 6- monoacetylmorphine and caffeine (as non controlled)

UXPP39 + + + In the sample SM4 was identified paracetamol, caffeine, 6-monoacethylmorphine, diacethylmorphine (heroine), papaverine and noscapine.

UYH68O + + + Caffeine, Paracetamol, 6-Monoacetylmorphine and Heroin

UYIOY3 + + + 6 monoacetilMorphine, Paracetamol (Acetaminophen), morphinan-6-ol, Caffeine, papaverine

V9FHUE + + -

VJJ2BS ANP + ANP Sample No#4 except heroine contain: caffeine, 6-monoacetil morphine, noscapine and traces of acetaminophen and acetyl codeine

VK9TBJ + + + 6-MAM, acetylcodeine, caffeine, paracetamol, meconin, papaverin, noscapin

VOFFDF - + - In the test sample 2019/2/SM-2 was detected heroine, 6-monoacetylmorphine, acetylcodeine, acetaminophen, caffeine and noscapine

VOFIVV + + + Heroin was detected in the SM-4 sample.

VSIQQM + + + /

VTGLIP + + + sample 2019/2/SM-4 was found to contain Acetaminophen, Morphine, Heroin and Caffeine

VTNITG + + + 17,69 +/- 1,59 % HEROÍNA BASE PARACETAMOL CAFEÍNA

WCDCCS + + - caffeine, acetil-codein. MAM, papaverin, noscapine

WG1S1P + + + Heroin is on the list of drugs.

WKVSHN + + + The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample, indicates the Heroin, Caffein, Paracetamol, Acetylcodeine and 6-monoacetylmorphine presence.

WLWWWW + + + The sample contain heroin, morphine as minor component, caffeine and paracethamol

WRVOXF + + - One package containing 210 milligrams of a brown powder. This powder was found to contain diamorphine (commonly known as heroin; class A), with a purity of 18% in base form, and caffeine (not controlled).




Page 110 of 116

ICE 2019/2-SM


WU22AL + + + Heroin, was detected in the powder, with a W:W percentage estimated at 14.50%. Acetaminophen and Caffeine also detected in the powder.

X1NYNN + + +

XO00Q0 ANP + ANP It is included in Table I Schedule I, Narcotic Substances, not used for medical purposes, approved by Government Decision 1088 of 05.10.2004

XSNN71 + + ANP Heroin 16% (as base). Heroin is classified as narcotic drug.

Y5OQGB + + + A mix of eight (8) different substances were found in the sample 2019/2/SM-4. One of them is a controlled drug (Heroine). The others substances detected were Acetaminophen, meconin, caffeine, acetylcodeine, 6-monacetylmorphine, papaverine and noscapine.

YARNPI + + + Heroin was identified in SM 4. In addition 6-monoacetylemorphine, caffeine, acetaminophen and noscapine were identified in SM 4

YL6D6J + + + The sample contains heroin and caffeine

YY3YD4 + + + The sample contained 18.5% heroin. The sample also contained caffeine, paracetamol and acetylcodeine, 6-monoacethylmorphine with morphine, noscapine, papaverine and meconine as a minor components.

YYBTFT + + + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of PARACETAMOL, CAFFEINE and LIDOCAINE in the sample

ZAZMLT + + + Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with heroin, caffeine, acetaminophen and 6-monoacetylmorphine.

ZNRYRN - + - sample contains 16,7 % of heroine, acetylcodeine and 6-monoacetylmorphine.

ZPRDAZ + + + Also contains Caffeine, Paracetamol (Acetaminophen), Papaverine, Narcotine, 6- Monoacetylcodeine, O6-Monoacethylmorphine




Page 111 of 116

ICE 2019/2-SM



Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

06JS66 I SI HPTLC

0GRT0S SI

111NTK I I SI I

1MA9MF I SI

224V2J I S

2HSS8S I I S Raman

2JJWOJ S I I

2UVXGU I S

3PP2PP I I

48PXX4 S SI I


50AP5Y S S S I I

5CPBXX I SI

60N30D S I

61XYO6 SI I

63AEKB I SI


6AX4TV I I

6ESG22 I I

6GM1ZU I SI I

6OTC3V SI I

75XFMQ S I I I

77JO7Q I SI

7KCDRK S I I

7RURX8 S SI SI

7WIJ9N S I


8NKZIO SI

8SMOGU SI

932LRK I SI I

9969TL S S S I I

999RGV S S S I





Page 112 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

9ABUAU SI I

9FFVN3 I SI I

9HXOHH I SI

9N59BB I I SI

9OO999 S S I I I

9OS0B5 S SI

A2HMLG SI

AA0UJR SI SI SI I

ACYVYR S S I I

AK3UYT SI

AM777O S S I

AMYZY0 SI S S I I I

AWGGYX I SI

AXAVAJ S S I

AZBAGS I SI I XRD


B6H3ZH SI

BCD9DP SI

BD556C SI I

BQNMYR S S SI I

BXCKYU SI S I

C11111 SI SI SI I

C5MOP5 I I

C8CCX2 S SI

CAS0HP S I I

CBISZG S S I

CD5XF1 S S SI

CDVNVK S S I

CILAEB S I I


CXQPFE I


DCOHUX SI S I I

DJDDMD S I I I S

DK6FK1 S S S I

DKW45M S S S I I

DSEBBS S S S I I




Page 113 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

DTIACA S I I I I

DZZZLS SI S I I SI

E1ZARZ S I I

EI96ZN S I I

EIHUWT SI

ELQO7L S S S I I


FCGG7O S S I SI

FEVFVO S S I I

FFFLFF SI I SI SI

FJF0IF I SI

FXP8PV SI SI

FYKJPD SI I

G6GBTW I S I

GC11E1 S I I

GDI9LV S S SI I

GGGPGE S S S I

GHKHWC S S S I I

GIGQ0G S I I

GIZGWR I

GPV0WG I SI

GQPYLA SI SI SI I

GYEHYL I I SI

H12HE2 I

H7XE2X I SI I

H9RHNG I I

HANMLJ I SI I

HASZSM I I I S


I2TTTT SI

I4IIIW SI

ICNCMG I SI

IE8EEE S S S I I

IIIDYX S I SI I

IIILIY SI I


IRZAFP S I I




Page 114 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

IWWWZH SI SI SI I

JCJJVA I I

JJPNJY I SI I

JJUJHH S S I HRMS

JMYLYJ I I SI

JVPB7L S S I I I

K6G1HJ SI

K8IZ1S S SI S I I

K8NOCM S I I GC-IR


KFKUP0 S S I I

KJFJIJ S I I I

KKKQP7 SI I

KLCHRH S S I I


KQKO2K SI

KUD7YD I SI

L9WDPM I I S

LDLJZA S S S I I

LG1AMG S S I I

LHOD3U S I I


LUABFV S I

LVRMSV S I SI I

LVUH0Z S S S I SI


MIIFIV S I

MJDOQK S S S I I

MJYQ1I SI

MMVGH6 S SI


MTWM6 W

SI SI SI I

MUVGFL S I

MWX4XX S I I

NE8ZAO S S S I I

NGJDWJ S I I




Page 115 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

NNNNEI SI I SI

O1HUPW S S I I

OEOJOY SI

OHNQ7X I

OHS9XX I S

OOWPNF S S I SI

OZOHOD SI I I

P8UQDW SI I SI

PCQBJD S I I I

PFZFOJ S S S I I

PKNKQN S I

PLMLOM SI I


PQCCII I S

PRZOZC SI I

PXAOXX S I I

PXFATB S S I

PYUYVY S S S I

Q8ZQ82 S S S I

QBIV4X S S I I

QFFJPH SI I

QROQON S S S I I I

RCRHBM S I I

RG5OYA S S I I

RH2BU2 S S I

RRQFQQ S I


RZDHUH I SI I

S0C00Z S S I

SDNBD6 I SI I

SFS5SX S I

SOWSUC SI I

STNCC9 S S SI I


TBUBCR S I


TE8ERE S S I




Page 116 of 116

ICE 2019/2-SM

Code 140 141 142 150 160 161 171 180 190 200 211 230 231 250 210

TFF5SF S S S I

TFKFT5 SI

TKLAER S S I I

TPYWQP S S S I

UFS8L8 S I

UUNUSP S S S I

UXPP39 I

UYH68O S S I I

UYIOY3 S S I I

V9FHUE SI


VK9TBJ SI I

VOFFDF I

VOFIVV SI I

VSIQQM SI SI

VTGLIP S I I


WCDCCS I SI SI

WG1S1P S S S I I


WLWWW W S S I I I

WRVOXF S SI SI I I

WU22AL SI

X1NYNN SI I

XO00Q0 S S S I I

XSNN71 I I

Y5OQGB S I I


YL6D6J S S I I

YY3YD4 I SI

YYBTFT S S I I

ZAZMLT S S I

ZNRYRN SI

ZPRDAZ S S S I I

Vienna International Centre, P.O. Box 500, 1400 Vienna, Austria

Tel. : (+43-1) 26060-0, Fax : (+43-1) 26060-5866, www.unodc.org

Documents

INTERNATIONAL COLLABORATIVE EXERCISES (ICE) · Mr. Scott Oulton, Drug Enforcement Administration, USA Ms. Catherine Quinn, Victoria Police, Australia Prof. Franco Tagliaro, University