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Instrumentation
Frank Ruiz, Ruiz & AssociatesSteve Doe, Parker Hannifin Corporation
IFPAC SM - 2001Fifteenth International ForumProcess Analytical ChemistrySM
January 21-24, 2001,Amelia Island, Florida, U.S.A
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
AgendaAgendaPart I: Mechanics, Steve DoePart I: Mechanics, Steve Doe
��Surface Mount History in the Semiconductor IndustrySurface Mount History in the Semiconductor Industry��Substrate Design: SP76 Parallels & EnhancementsSubstrate Design: SP76 Parallels & Enhancements��Elastomer or Metallic Device Interface Seals?Elastomer or Metallic Device Interface Seals?
Part II: System Design, Frank RuizPart II: System Design, Frank Ruiz��Device Design for System FlexibilityDevice Design for System Flexibility��Designing a Sample Conditioning SystemDesigning a Sample Conditioning System��Future DevelopmentsFuture Developments
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Surface Mount HistorySurface Mount History�� Parker: surface mount supplier to semiconductor Parker: surface mount supplier to semiconductor
market for several yearsmarket for several years
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Surface Mount HistorySurface Mount History�� SP76 based on Semiconductor Industry 1½” footprintSP76 based on Semiconductor Industry 1½” footprint�� SEMI organization forum for industry standardsSEMI organization forum for industry standards�� Initial SEMI surface mount effort in early 1990’sInitial SEMI surface mount effort in early 1990’s�� Motivations similar to those of today’s Petrochemical Motivations similar to those of today’s Petrochemical
IndustryIndustry�� Market penetration most significant in AsiaMarket penetration most significant in Asia�� Global Standard for interface seal?Global Standard for interface seal?�� 1111//88” footprint being introduced (and embraced)” footprint being introduced (and embraced)�� Semiconductor Industry Use: Gas DeliverySemiconductor Industry Use: Gas Delivery
Analytical Industry Use: Sample ConditioningAnalytical Industry Use: Sample Conditioning
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design�� Meets SP76 designMeets SP76 design
specification for specification for elastomeric seal elastomeric seal option, however...option, however...
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design�� Achieves addedAchieves added
system flexibilitysystem flexibilitywith 5 streams, with 5 streams, and…and…
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design�� Provides ability Provides ability
to mount largerto mount largerdevices such asdevices such ascurrent designs current designs for flow controllers,for flow controllers,regulators and otherregulators and otherdevices. devices.
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate Block to Block SealingSubstrate Block to Block Sealing�� Incorporates standard OIncorporates standard O--RingRing
seal (size 2seal (size 2--007)007)�� 11//88” through hole w/ ” through hole w/ counterbore counterbore to to
capture ocapture o--ringring
�� Blocking flow passagesBlocking flow passagesprovides system flexibilityprovides system flexibility
�� Developing “plug” from either a Developing “plug” from either a solid elastomer or metallic disksolid elastomer or metallic diskmolded into Omolded into O--RingRing
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Substrate DesignSubstrate Design
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Elastomeric or Metallic Device Seals?Elastomeric or Metallic Device Seals?Pro’sPro’s Con’sCon’s
�� Elastomeric:Elastomeric: Used in numerous Used in numerous 1x101x10--44 cc He/seccc He/secsample systemssample systems leak integrity leak integrity devices; entrenched,devices; entrenched,successful technologysuccessful technology
�� Metallic: Metallic: 1x101x10--1010 cc He/seccc He/sec Seal & mating surfaces Seal & mating surfaces leak integrityleak integrity subject to handlingsubject to handling
damage resulting in damage resulting in leaksleaks
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Elastomeric or Metallic Device Seals?Elastomeric or Metallic Device Seals?
Conclusion:Conclusion:Recommend Elastomeric for majority of sampling systems Recommend Elastomeric for majority of sampling systems
and Metallic for PPB detection level applicationsand Metallic for PPB detection level applications
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Designing a Sample Conditioning SystemDesigning a Sample Conditioning System
(1.5 CR) (1.5 CL)(1.5 CL) (1.5 C)
A A B C CB
A A- B-B C-C
(1.5 CR5)
D D
-DD
1.5" BASE BLOCKS
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Designing a Sample Conditioning SystemDesigning a Sample Conditioning System
1.5" BASE 2.375" BASE
TWO STANDARD BASE SIZES
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
COMPONENTS
TEMP.SENSOR
PRESS.XTR PRESSURE TRANSDUCER
TEMPERATURE SENSOR
FILTER
NEEDLE VALVE
3-WAY VALVE
BALL VALVE
PRESSURE REDUCING REGULATOR
BACK PRESSURE REGULATOR
RELIEF VALVE
FLOW CONTROLLER
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Designing a Sample Conditioning SystemDesigning a Sample Conditioning System
IR-4000
(2.5 CL)
PRESSURE REGULATOR
12
3L
345
D
D
Three Inlet ports tiedtogether inside the body of the component.
All three Outlet portsare common to thediaphragm cavity.
D-D
1 2 3 4 5
1 2 3 4 5
SpringHole
CHANNEL #
IR-4000 BODY
E E
E-E
PRESSURE REDUCING REGULATOR IR-4000 EXAMPLE
ComponentINLETComponent
OUTLET BLANK
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
IN INBLOCKED
OUT OUTBLOCKED
BLANKIR-4000
(2.5 C)
PRESSURE REGULATOR
12
3L
345
A A
INOUT
BLOCKED
BLANK
CHANNELNUMBERS
A A-
(2.5 C)
1
2345
PRIMARY FLOW DIRECTION
These inlet channels are connectedtogether inside the component.
These outlet ports are connectedtogether inside the component.
The number in the circle is the channelto which this port is connected."3L" Is Channel 3, Left Center Port.
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
IR-4000
IR-4000 CONNECTIONS TO SUBSTRATE(TOP VIEW OF SUBSTRATE)
IR-4000
(2.5 CL) (2.5 CR)
IR-4000
(2.5 C)
PRESSURE REGULATOR
12
3L
345
IR-4000
(2.5 C)
PRESSURE REGULATOR
12
345
PRESSURE REGULATOR
12
3R3
45
PRESSURE REGULATOR
123
45
3L 3R
OUTLETOF COMPONENT
INLETOF COMPONENT
BLANK OUTLETOF COMPONENT
PLUGGED
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
H2OTemp
AIR
AIR
ZEROPARKER
STREAM SWITCH
FLOWCONTROLLER
O2
Temp
FLOWCONTROLLER
ZEROPUMP
R-max
PARKERSTREAM SWITCH
R-max N2
RETURN HDR.
NeSSI SYSTEM 3
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
H2OTemp
AIR
C
AIR
ZEROPARKER
STREAM SWITCH
C
FLOWCONTROLLER
O2
Temp
FLOWCONTROLLER
ZEROPUMP
R-max
PARKERSTREAM SWITCH
R-maxN2
RETURN HDR.
CIRCUIT 1
CIRCUIT 2
4
6
7
9
2
3
1
NeSSI SYSTEM 3(Modified)
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
H2OTemp
AIR
FLOWCONTROLLER
ZEROPUMPPARKER
STREAM SWITCH
R-max
N2
RETURN HDR.
4
6
2
9
2
3
1
O2
NeSSI SYSTEM 3(Modified)
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
IR-4000
IR-4000 CONNECTIONS TO SUBSTRATE(TOP VIEW OF SUBSTRATE)
IR-4000
(2.5 CL) (2.5 CR)
IR-4000
(2.5 C)
PRESSURE REGULATOR
12
3L
345
IR-4000
(2.5 C)
PRESSURE REGULATOR
12
345
PRESSURE REGULATOR
12
3R3
45
PRESSURE REGULATOR
123
45
3L 3R
OUTLETOF COMPONENT
INLETOF COMPONENT
BLANK OUTLETOF COMPONENT
PLUGGED
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
COMMON
NORMALLY CLOSED
NORMALLY OPEN
AIR
3-WAY R-max
FILTER
(1.5 CR)
H2O CELL
(1.5 CR)
FLOW CONTROLLERWITH EXTERNAL NEEDLE VALVE
UPSTREAM REFERENCE
(2.5 CL)
DOME
DOME
BPR-4000
(2.5 CL)
BACK PRESSURE REGULATOR
123
3L45
IR-4000
(2.5 CR)
PRESSURE REGULATOR
3R45
123
4 3R
33R4
a123
ANALYZERCELL
METERING VALVE1.5" SUBSTRATE
123
3R45 FLOW
CONTROLLER
23
3L4
15
1
4
2
3
(2.5 C)
2
1
3
12
(2.5 CR)
4
(1.5 CL)
TEMP. SENSOR1.5" SUBSTRATE
12
3L
345
TEMP
a
NeSSI SYSTEMNo. 3
H20 ANALYZER
ACTUATING AIR
ASPIRATOR
ACTUATING AIR
VENT RECOVERY
ASPIRATOR
SAMPLE IN
RTN.
RETURN HDR.
IN
9
6
BY-PASS
4
TO R-max
FROM R-max
FROM R-max
3TO R-max
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
H2O
Temp
AIR
FLOWCONTROLLER
ZEROPUMPPARKER
STREAM SWITCH
R-max
N2
RETURN HDR.
NeSSI SYSTEM 3(Modified)
4
6
7
9
2
3
1
O2
5 10
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
COMMON
NORMALLY CLOSED
NORMALLY OPEN
AIR
3-WAY R-max
FILTER
(1.5 CR)
(1.5 C)
FLOW CONTROLLERWITH EXTERNAL NEEDLE VALVE
UPSTREAM REFERENCE
(2.5 CL)
DOME
DOME
BPR-4000
(2.5 CL)
BACK PRESSURE REGULATOR
123
3L45
IR-4000
(2.5 CR)
PRESSURE REGULATOR
3R45
123
4 3R
3
METERING VALVE1.5" SUBSTRATE
123
3R45 FLOW
CONTROLLER
23
3L4
15
1
4
2
3
(2.5 C)
2
1
3
12
4
(1.5 C)
TEMP. SENSOR1.5" SUBSTRATE
123
345
TEMP
NeSSI SYSTEMNo. 3
EXTERNAL H20 ANALYZER
ACTUATING AIR
VENT RECOVERY
ASPIRATOR
ACTUATING AIR
RETURN
ASPIRATOR
SAMPLE IN
RTN.
RETURN HDR.
IN
9
67
BY-PASS
4
TO R-max
FROM R-max
FROM R-max
3TO R-max
5TO ANALYZER
5
10 FROM ANALYZER
10FROMANALYZER
69
7
Surf
ace
Mou
nt T
echn
olog
y fo
r Su
rfac
e M
ount
Tec
hnol
ogy
for
Sam
ple
Cond
ition
ing
Syst
ems
Sam
ple
Cond
ition
ing
Syst
ems
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Future Developments (Steve & Frank)Future Developments (Steve & Frank)�� Solicit input from other suppliers to include analyzer & sensor Solicit input from other suppliers to include analyzer & sensor
devices on stickdevices on stick�� Develop automation software for system designDevelop automation software for system design�� Develop pricing for total offeringDevelop pricing for total offering�� ReRe--present system with updates at PITTCONpresent system with updates at PITTCON--20012001�� Build betaBuild beta--site system for field testing?site system for field testing?
Surface Mount Technology for Surface Mount Technology for Sample Conditioning SystemsSample Conditioning Systems
Thank you!Thank you!
Questions?Questions?