ICP Test Report Certification Packet · ICP Test Report Certification Packet Company name: ... ICP-0178 11-0894 ... may release from substrate during acid etching process as well

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc.

Product Series: Omni-Blok Fuse Holder

Product #: 154DR

Issue Date: July 10, 2014

It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,

2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

[Global EHS Engineer]

(1) Parts, sub-materials and unit parts

This document covers the Omni-Blok Fuse Holder RoHS-Compliant series products

manufactured by Littelfuse, Inc.

＜ Raw Materials Used

Please see Table 1

(2) The ICP data on all measurable substances

Please see appropriate pages as identifed in Table 1

Remarks：

Pb (lead) contained in the high temperature melting solder > 85% and is categorized as exempt under section 7a of the RoHS Annex.

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

ICP ID Raw Material Part Number Raw Material Description Page(s) Part Number

ICP-0169 910-238 Cap (Base & Plating) 3-8 0154003.DR

ICP-0170 909-434 Body-Ceramic 9-42 0154003.DR

ICP-0171 082xxx Element - 2% by weight Ag Clad

Cu 43-48

ICP-0172 082xxx Element - 5% by weight Ag Clad

Cu 49-54 0154003.DR

ICP-0178 11-0894 (497xxx)

Element - Ag Plated 36 Alloy

55-59

(Ni36Fe64MAg7%)

ICP-0173 11-0803 (497xxx)

Element - Ag Plated Dumet

60-64

(Ni42Fe58MCuMAg5%)

ICP-0174 692321 Solder 65-70 ICP-0137 087266 Anaerobic Adhesive 71-85

ICP-0176 425809 Ink 86-97 0154003.DR

ICP-0177 155900-4 Omni Body – Natural Color 98-108 0154003.DR

ICP-0179 883-059 Omni Clip 109-114 0154003.DR

ICP-0182 692323 Solder wire-92.5Pb5Sn2.5Ag 115-120 0154003.DR

Test Report Number : TWNC00362137

Authorized by: On Behalf of Intertek Testing Services Taiwan Limited K. Y. Liang Director

*THJ0362137* Page 1 of 6 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C. 全國公證檢驗股份有限公司

11492 台北市內湖區瑞光路 423 號 8 樓 Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Mar 25, 2014 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Silver Plated Brass Cap Part Number : 910-238 Date Sample Received : Mar 18, 2014 Date Test Started : Mar 20, 2014

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Tested Components

(1) Grey metal substrate (2) Silvery plating layer

Test Report

Number: TWNC00362137 Test Conducted




Test Result Summary: Result

Test Item Unit Test Method (1) (2)

RL

Heavy Metal

Cadmium (Cd) content ppm

With reference to IEC 62321-5: 2013, by microwave or acid digestion and determined by ICP-OES.

ND ND 2

Lead (Pb) content ppm


85(#) 753(#) 2

Mercury (Hg) content ppm


ND ND 2

Chromium VI (Cr6+) content mg/kg with

50 cm2

With reference to IEC 62321: 2008, by boiling water extraction and determined by UV-Vis Spectrophotometer.

Negative Negative 0.02

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample mg/kg with 50cm2 = Milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. # = The result of lead was only for reference if the base material contained lead, because the lead

may release from substrate during acid etching process as well as from electroplating layer. Responsibility of Chemist: Ryan Lin/ Pelny Hsiao Date Sample Received : Mar 18, 2014 Test Period : Mar 20, 2014 to Mar 25, 2014 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm)

The above limits were quoted from Annex II of 2011/65/EU for homogeneous material.

Test Report





Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI) Reference Standard：Cd/Pb: IEC 62321-5:2013; Hg: IEC 62321-4:2013; Chromium (VI): IEC 62321:2008 Remarks: *1: List of Appropriate Acid：

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

For different material, digest the sample with

appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Confirm the tested samples are totally

dissolved

Sample preparation

Take sample and immerse into Aqua Regia, start to etch plating layer

Stop the etching procedure upon color change completely

Take the Aqua solution as plating component and etched body as substrate component

Cr6+

Make up with deionized water and add diphenyl-carbazide solution

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

By boiling water extraction

Negative *2

Substrate Plating

Test Report





End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for anyparticular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and onlyaccepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes nowarranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conductthe Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Number: TWNC00362137








:::::

============================================================================================

:

2014/01/14

CERAMIC

The following sample(s) was/were submitted and identified by/on behalf of the applicant as :

Sample Submitted By

Testing Period

Test Result(s)

No. : CE/2014/13109 Date : 2014/01/21 Page : 1 of 27Test Report*CE/2014/13109*CERAMTEC GMBH

CERAMTEC GMBH

GESCHAFTSBEREICH MULTIFUNKTIONSKERAMIK,LUITPOLDSTRABE 15, 91207 LAUF

FREQUENTA C221Sample Receiving Date

Sample DescriptionStyle/Item No.

2014/01/14 TO 2014/01/21

Please refer to next page(s).

33, Wu Chuan Rd., New Taipei Industrial Park, New Taipei City, Taiwan / 新北市新北產業園區五權路33號t+886 (02)2299 3279 f+886 (02)2299 3237 www.sgs.tw

Member of the SGS Group

SGS Taiwan Ltd.

This document is issued by the Company subject to its General Conditions of Service printed overleaf, available on request or accessible at http://www.sgs.com/en/Terms-and-Conditions.aspx and, for electronic format documents, subject to Terms and Conditions for Electronic Documents at http://www.sgs.com/en/Terms-and-Conditions/Termse-Document.aspx. Attention is drawn to the limitation of liability, indemnification and jurisdiction issues defined therein. Any holder of this document is advised that information contained hereon reflects the Company’s findings at the time of its intervention only and within the limits of client’s instruction, if any. The Company’s sole responsibility is to its Client and this document does not exonerate parties to a transaction from exercising all their rights and obligations under the transaction documents. This document cannot be reproduced, except in full, without prior written approval of the Company. Any unauthorized alteration, forgery or falsification of the content or appearance of this document is unlawful and offenders may be prosecuted to the fullest extent of the law. Unless otherwise stated the results shown in this test report refer only to the sample(s) tested.

For Question,Please Contact with SGSwww.tw.sgs.com

Signature Not Verified

2014.026 CS

LITTELFUSE PHILIPPINES INC.LIMA TECHNOLOGY CENTER, LIPA CITY,MALVAR, BATANGAS

LITTELFUSE PHILIPPINES INC. LIMA TECHNOLOGY CENTER, LIPA CITY, MALVAR, BATANGAS

Test Result(s)

ResultNo.1

mg/kg With reference to IEC 62321-5: 2013 andperformed by ICP-AES.

2 n.d.


2 n.d.


2 n.d.

mg/kg With reference to IEC 62321: 2008 andperformed by UV-VIS.

2 n.d.

% With reference to EN 14372. Analysis wasperformed by GC/MS.

0.003 n.d.


0.003 n.d.


0.01 n.d.


0.01 n.d.


0.003 n.d.


0.003 n.d.

mg/kg With reference to US EPA 3550C: 2007.Analysis was performed by LC/MS.

10 n.d.

mg/kg With reference to US EPA 3550C: 2007.Analysis was performed by LC/MS.

10 n.d.

mg/kg With reference to US EPA 3540C method.Analysis was performed by GC/MS.

0.5 n.d.


0.5 n.d.


5 n.d.

MDLMethod

PFOA (CAS No.: 335-67-1)

Polychlorinated Biphenyls (PCBs)(CAS No.: 1336-36-3)Polychlorinated Terphenyls(PCTs)

Test Item(s)

Mercury (Hg)

Hexavalent Chromium Cr(VI)

Cadmium (Cd)

Lead (Pb)

Unit

BBP (Benzyl butyl phthalate)(CAS No.: 85-68-7)DEHP (Di- (2-ethylhexyl)phthalate) (CAS No.: 117-81-7)DIDP (Di-isodecyl phthalate) (CASNo.: 26761-40-0; 68515-49-1)

Polychlorinated Naphthalene(PCNs)

DINP (Di-isononyl phthalate) (CASNo.: 28553-12-0; 68515-48-0)DNOP (Di-n-octyl phthalate) (CASNo.: 117-84-0)DBP (Dibutyl phthalate) (CAS No.:84-74-2)Perfluorooctane sulfonates(PFOS-Acid, Metal Salt, Amide)

PART NAME No.1 CREAM CERAMIC

Test Report No. : CE/2014/13109 Date : 2014/01/21 Page : 2 of 27

CERAMTEC GMBH *CE/2014/13109*




SGS Taiwan Ltd.




ResultNo.1


100 n.d.

** Analysis was performed by FTIR andFLAME Test.

- Negative

mg/kg With reference to ISO 17226-1(2008).Analysis was performed by HPLC/DAD.

3 n.d.

mg/kg With reference to US EPA 8270D method.Analysis was performed by GC/MS.

0.5 n.d.


0.5 n.d.


0.5 n.d.

- n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.- n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.5 n.d.Decabromodiphenyl ether

Hexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl ether

Hexabromobiphenyl

Sum of PBBs

Pentabromobiphenyl

MonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenyl

Alkanes, C10-13, chloro (ShortChain Chlorinated Paraffins) (CASNo.: 85535-84-8)

Monobromodiphenyl etherDibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl ether

Formaldehyde (CAS No.: 50-00-0)

Pentabromodiphenyl ether

DecabromobiphenylSum of PBDEs

PVC

HeptabromobiphenylOctabromobiphenylNonabromobiphenyl

Monomethyl dibromodiphenylmethane (DBBT)Monomethyl dichlorodiphenylmethane (Ugilec121)Monomethyl tetrachlorodiphenylmethane (Ugilec141)

mg/kg With reference to IEC 62321: 2008 andperformed by GC/MS.




Test Item(s) Unit Method MDL



SGS Taiwan Ltd.




ResultNo.1

0.03 n.d.0.03 n.d.

- Negative- Negative- Negative

- Negative- Negative- Negative

mg/kg With reference to LFGB 82.02-2. Analysiswas performed by GC/MS.

3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.

Tremolite (CAS No.: 77536-68-6)AZO

9): 4,4'-DIAMINODIPHENYLMETHANE(CAS No.: 101-77-9)10): 3,3'-DICHLOROBENZIDINE(CAS No.: 91-94-1)11): 3,3'-DIMETHOXYBENZIDINE(CAS No.: 119-90-4)

5): O-AMINOAZOTOLUENE (CASNo.: 97-56-3)6): 2-AMINO-4-NITROTOLUENE(CAS No.: 99-55-8)7): P-CHLOROANILINE (CAS No.:106-47-8)8): 2,4-DIAMINOANISOLE (CASNo.: 615-05-4)

2): BENZIDINE (CAS No.: 92-87-5)3): 4-CHLORO-O-TOLUIDINE(CAS No.: 95-69-2)4): 2-NAPHTHYLAMINE (CASNo.: 91-59-8)

AsbestosActinolite (CAS No.: 77536-66-4)Amosite (CAS No.: 12172-73-5)Anthophyllite (CAS No.: 77536-67-5)

Organic-tin compoundsTributyl Tin (TBT)Triphenyl Tin (TphT)

1): 4-AMINODIPHENYL (CAS No.:92-67-1)

Chrysotile (CAS No.: 12001-29-5)Crocidolite (CAS No.: 12001-28-4)

mg/kg With reference to ISO 17353. Analysis wasperformed by GC/FPD.

%

With reference to EPA 600/R-93/116method. Analysis was performed by StereoMicroscope (SM), Dispersion StainingPolarized Light Microscope (DS-PLM) andX-ray Diffraction Spectrometer (XRD).







SGS Taiwan Ltd.




ResultNo.1


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.


3 n.d.

12): 3,3'-DIMETHYLBENZIDINE(CAS No.: 119-93-7)


21): O-ANISIDINE (CAS No.: 90-04-0)22): 4-AMINOAZOBENZENE(CAS No.: 60-09-3)23): 2,4-XYLIDINE (CAS No.: 95-68-1)24): 2,6-XYLIDINE (CAS No.: 87-62-7)

17): 4,4'-THIODIANILINE (CASNo.: 139-65-1)18): O-TOLUIDINE (CAS No.: 95-53-4)19): 2,4-TOLUYLENEDIAMINE(CAS No.: 95-80-7)20): 2,4,5-TRIMETHYLANILINE(CAS No.: 137-17-7)

13): 3,3'-DIMETHYL-4,4'-DIAMINODIPHENYLMETHANE(CAS No.: 838-88-0)14): P-CRESIDINE (2-METHOXY-5-METHYLANILINE) (CAS No.:120-71-8)15): 4,4'-METHYLENE-BIS- (2-CHLOROANILINE) (CAS No.:101-14-4)16): 4,4'-OXYDIANILINE (CASNo.: 101-80-4)






SGS Taiwan Ltd.




ResultNo.1

50 n.d.

50 n.d.

50 n.d.

50 n.d.

mg/kg With reference to US EPA 5021 method.Analysis was performed by GC/MS.

1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.

Chlorofluorocarbon-115 (CAS No.:76-15-3)Group IIIChlorofluorocarbon-13 (CAS No.:75-72-9)

MDL

HalogenHalogen-Fluorine (F) (CAS No.:14762-94-8)

Chlorofluorocarbon-112 (CAS No.:76-12-0)Chlorofluorocarbon-211 (CAS No.:422-78-6)Chlorofluorocarbon-212 (CAS No.:3182-26-1)Chlorofluorocarbon-213 (CAS No.:2354-06-5)

Test Report

CFC's (Chlorofluorocarbons)Group I

Halogen-Chlorine (Cl) (CAS No.:22537-15-1)Halogen-Bromine (Br) (CAS No.:10097-32-2)Halogen-Iodine (I) (CAS No.:14362-44-8)

mg/kg With reference to BS EN 14582:2007.Analysis was performed by IC.

No. : CE/2014/13109 Date : 2014/01/21 Page : 6 of 27



Chlorofluorocarbon-111 (CAS No.:354-56-3)


Test Item(s) Unit Method



SGS Taiwan Ltd.




ResultNo.1


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


HCFC-121 (CAS No.: 354-14-3)

HCFC-122 (CAS No.: 354-21-2)

HCFC-123 (CAS No.: 306-83-2)

HCFC-124 (CAS No.: 2837-89-0)

HCFCs(Hydrochlorofluorocarbons)HCFC-21 (CAS No.: 75-43-4)

HCFC-22 (CAS No.: 75-45-6)

HCFC-31 (CAS No.: 593-70-4)

HCFC-142b (CAS No.: 75-68-3)

HCFC-131 (CAS No.: 359-28-4)

HCFC-132b (CAS No.: 1649-08-7)

HCFC-133a (CAS No.: 75-88-7)

HCFC-141b (CAS No.: 1717-00-6)







SGS Taiwan Ltd.




ResultNo.1


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.

HCFC-221 (CAS No.: 422-26-4)

HCFC-222 (CAS No.: 422-49-1)

HCFC-223 (CAS No.: 422-52-6)

HCFC-231 (CAS No.: 421-94-3)

HCFC-232 (CAS No.: 460-89-9)

HCFC-233 (CAS No.: 7125-84-0)

HCFC-234 (CAS No.: 425-94-5)

HCFC-224 (CAS No.: 422-54-8)

HCFC-225ca (CAS No.: 422-56-0)

HCFC-225cb (CAS No.: 507-55-1)

HCFC-226 (CAS No.: 431-87-8)

HCFC-244

HCFC-251 (CAS No.: 421-41-0)

HCFC-243 (CAS No.: 460-69-5)





HCFC-235 (CAS No.: 460-92-4)

HCFC-241 (CAS No.: 666-27-3)

HCFC-242 (CAS No.: 460-63-9)



SGS Taiwan Ltd.




ResultNo.1


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.

HCFC-252 (CAS No.: 819-00-1)

Halon-1211 (CAS No.: 353-59-3)

Halon-1301 (CAS No.: 75-63-8)

Halon-2402 (CAS No.: 124-73-2)

CHCs (Chlorinate hydrocarbon)

HCFC-261 (CAS No.: 420-97-3)

HCFC-262 (CAS No.: 421-02-03)

HCFC-271 (CAS No.: 430-55-7)

Halons

1,1-Dichloroethane (CAS No.: 75-34-3)1,1-Dichloroethene (CAS No.: 75-35-4)1,1-Dichloropropene (CAS No.:563-58-6)1,2,3-Trichloropropane (CAS No.:96-18-4)

1,1,1,2-Tetrachloroethane (CASNo.: 630-20-6)1,1,1-Trichloroethane (CAS No.:71-55-6)1,1,2,2-Tetrachloroethane (CASNo.: 79-34-5)1,1,2-Trichloroethane (CAS No.:79-00-5)





HCFC-253 (CAS No.: 460-35-5)



SGS Taiwan Ltd.




ResultNo.1


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.


1 n.d.

Tetrachloroethene (CAS No.: 127-18-4)trans-1,2-Dichloroethene (CASNo.: 156-60-5)

Carbon tetrachloride (CAS No.:56-23-5)

Test Item(s)

trans-1,3-Dichloropropene (CASNo.: 10061-02-6)Trichloroethylene (CAS No.: 79-01-6)

cis-1,2-Dichloroethene (CAS No.:156-59-2)cis-1,3-Dichloropropene (CAS No.:10061-01-5)Hexachlorobutadiene (CAS No.:87-68-3)Methylene Chloride (CAS No.: 75-09-2)

Chloroethane (CAS No.: 75-00-3)

Chloroform (CAS No.: 67-66-3)

Chloromethane (CAS No.: 74-87-3)

1,2-Dichloroethane (CAS No.:107-06-2)1,2-Dichloropropane (CAS No.:78-87-5)1,3-Dichloropropane (CAS No.:142-28-9)2,2-Dichloropropane (CAS No.:594-20-7)

Unit Method MDL






SGS Taiwan Ltd.




1.2.3.4.5.6.7.

mg/kg = ppm 0.1wt% = 1000ppm

MDL = Method Detection Limit

Testing range of asbestos qualitative analysis is from less than 0.1% to 100%. The judgment criterion: asbestosfibers being found is shown as "Positive"; asbestos fibers not being found is shown as "Negative".

** = Qualitative analysis (No Unit)

Note

n.d. = Not Detected

" - " = Not Regulated

Negative = Undetectable / Positive = Detectable

PFOS Reference Information : POPs - (EU) 757/2010Outlawing PFOS as substances or preparations in concentrations above 0.001% (10ppm), in semi-finished productsor articles or parts at a level above 0.1%(1000ppm), in textiles or other coated materials above 1μg/m².






SGS Taiwan Ltd.







Note** (For IEC 62321)(1) For non-metallic material, add alkaline digestion reagent and heat to 90~95 .(2) For metallic material, add pure water and heat to boiling.

1) These samples were dissolved totally by pre-conditioning method according to below flow chart.Cr6+ test method excluded

2) Name of the person who made measurement: Climbgreat Yang3) Name of the person in charge of measurement: Troy Chang

Cutting / Preparation

Sample Measurement

Pb Cd

Acid digestion by suitable aciddepended on different samplematerial (as below table)

Microwave digestion withHNO3/HCl/HF

Filtration

Add appropriate amountof digestion reagent

Heat to appropriatetemperature to extract

Cool, filter digestatethrough filter

Add diphenyl-carbazidefor color development

measure the absorbanceat 540 nm by UV-VIS

Hg

SolutionResidue

1) Alkali Fusion2) HCl to dissolve

ICP-AES

Sample Material Digestion AcidSteel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, H2O2

Glass HNO3/HFGold, platinum, palladium, ceramic Aqua regiaSilver HNO3

Plastic H2SO4, H2O2, HNO3, HClOthers Added appropriate reagent to total

digestion

Cr6(Note**)



SGS Taiwan Ltd.







Analytical flow chart of volatile organic compounds (VOCs)

� Name of the person who made measurement�Chun Wu� Name of the person in charge of measurement�Shinjyh Chen

Reference method�US EPA 5021

Emitted gas was performed by GC/MS

Sample pretreatment

Bake the sample in the oven

Data

Take sample and put it into headspace glasswareand seal.



SGS Taiwan Ltd.







DBBT analytical flow chart

� Name of the person who made measurement: Roman Wong� Name of the person in charge of measurement: Troy Chang

Sample pretreatment/separation

Sample extraction by soxhlet method

Concentrate/Dilute Extracted solution

Analysis was performed by GC/MS

Data



SGS Taiwan Ltd.







Analytical flow chart of halogen content

� Name of the person who made measurement: Rita Chen� Name of the person in charge of measurement: Troy Chang

Sample pretreatment / Separation

Weighting and putting sample in cell

Oxygen Bomb Combustion / Absorption

Analysis was performed by IC

Dilution to fixed volume



SGS Taiwan Ltd.







Formaldehyde analytical flow chart

� Name of the person who made measurement: Yaling Tu� Name of the person in charge of measurement: Troy Chang

� Test Method�US EPA 8315A�ISO 17226-1�

Sample pretreatment

Sample extraction

Derived by DNPH Concentrate/Dilute Extractedsolution

Analysis was performed by HPLC/DAD

Data



SGS Taiwan Ltd.







Analysis flow chart for determination of PVC in material

� Name of the person who made measurement: Ginny Chen� Name of the person in charge of measurement: Troy Chang

Sample pre-treatment

Flame test

Sample analyzed by FTIR

Check wave-number of C-Cl bonding

Data



SGS Taiwan Ltd.







Analysis flow chart for determination of Asbestos

� Name of the person who made measurement: Victor Kao� Name of the person in charge of measurement: Wendy Wei

��Reference method: EPA 600/R-93/116�

Sampling

Transportation and Storage

Preparation of primary analytical sample

Containing Asbestos/Positive

Asbestos identification by dispersion stainingpolarized light microscope (DS-PLM)

Asbestos fiber is present Asbestos fiber is absent

Not containing Asbestos/Negative

Examination by stereomicroscope (SM)

Asbestos identification by dispersion stainingpolarized light microscope (DS-PLM)

Continue when problems are encountered withDS-PLM and/or for quality assurance purposes

Interference matrix removal

Asbestos identification by X-raydiffraction spectrometer (XRD)



SGS Taiwan Ltd.







Analytical flow chart of Organic-Tin content

Sample pretreatment

Sample extraction by organic solvent

Derived by Sodium tetraethylborate


Data

� Name of the person who made measurement: Ginny Chen� Name of the person in charge of measurement: Troy Chang

Analysis was performed by GC/FPD



SGS Taiwan Ltd.







Chlorinated Paraffins analytical flow chart

� Name of the person who made measurement: Barry Tseng� Name of the person in charge of measurement: Troy Chang

Sample pretreatment


Concentrate/Dilute the extracted solution


Data



SGS Taiwan Ltd.







PCNs analytical flow chart


Sample pretreatment




Data



SGS Taiwan Ltd.







PCTs analytical flow chart


Sample pretreatment




Data



SGS Taiwan Ltd.







PCBs analytical flow chart


Sample pretreatment




Data



SGS Taiwan Ltd.







PFOA/PFOS analytical flow chart of Ultrasonic extraction (LC/MS) procedure� Name of the person who made measurement: Roman Wong� Name of the person in charge of measurement: Troy Chang

Sample pretreatment

Sample extraction by Ultrasonic extraction(Reference method: US EPA 3550C)


Analysis was performed by LC/MS

Data



SGS Taiwan Ltd.







Analytical flow chart of phthalate content


Sample pretreatment/separation

Sample extraction by soxhlet method



Data



SGS Taiwan Ltd.







PBB/PBDE analytical FLOW CHART

First testing process

Optional screen process

Confirmation process

Sample

Screen analysis

Issue Report

Sample pretreatment

Sample extraction/Soxhlet method

Concentrate/DiluteExtracted solution

Analysis by GC/MS

Filter




SGS Taiwan Ltd.




* The tested sample / part is marked by an arrow if it's shown on the photo. *

** End of Report **






SGS Taiwan Ltd.









Applicant: Littelfuse Philippines Inc. Date : Jun 25, 2014 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Ceramic Body Part Number : 909-434 Date Sample Received : Jun 24, 2014 Date Test Started : Jun 24, 2014

Test Conducted :


Test Report

Number : TWNC00379383 Test Conducted




Test Result Summary:

Result Test Item Unit Test Method

Off white ceramic RL

Heavy Metal

Antimony (Sb) Content ppm With reference to USEPA 3052, by microwave digestion and determined by ICP-OES.

ND 2

Phthalates

Diisobutyl Phthalate (DIBP) ppm

With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

ND 10

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample Responsibility of Chemist: Pelny Hsiao/ Vico Lin Date Sample Received : Jun 24, 2014 Test Period : Jun 24, 2014 to Jun 25, 2014

Test Report





Measurement Flowchart: Test for Heavy Metal (Sb) Contents Reference Method：USEPA 3052

Sampling

Weigh sample and digest in microwave digestion oven with suitable acid

Transfer the digested solution and make up with deionized water

Analyzed by ICP-OES

Confirm the tested samples are totally dissolved

Test Report





Measurement Flowchart: Test for Phthalates Contents Reference Method: EN 14372: 2004

Sampling

Weigh sample and add organic solvent

By solvent extraction

Concentrate the extract and make up with organic solvent

Analyzed by GC-MS

Test Report





End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.

Number : TWNC00379383

*THJ0379383* Page 6 of 7

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.

全國公證檢驗股份有限公司 11492 台北市內湖區瑞光路 423 號 8 樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Number : TWNC00379383

*THJ0379383* Page 7 of 7

Intertek Testing Services Taiwan Ltd. 8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.


Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410







Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : 2% by weight Ag Clad Cu(082xxx) Part Number : 082685 Date Sample Received : Mar 18, 2014 Date Test Started : Mar 18, 2014

Test Conducted :


Test Report







Silvery metal RL

Heavy Metal



ND 2



ND 2



ND 2


50 cm2


Negative(#) 0.02

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample mg/kg with 50cm2 = Milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. # = Due to the insufficient sample area, reduced total sample surface of 10 cm2 was used and the

dilution factor was adjusted accordingly. Responsibility of Chemist: Ryan Lin/ Pelny Hsiao Date Sample Received : Mar 18, 2014 Test Period : Mar 18, 2014 to Mar 20, 2014 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm)


Test Report








Sampling

For different material, digest the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction


Cool and filter the extract

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample

Boiling water extraction

MetalPolymers / Electronics

Negative*2 Confirm the tested samples are totally

dissolved

Test Report





End of Report
















Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : 5% By weight Ag Clad Cu(082xxx) Part Number : 082686 Date Sample Received : Mar 18, 2014 Date Test Started : Mar 18, 2014

Test Conducted :


Test Report







Silvery metal RL

Heavy Metal



ND 2



ND 2



ND 2


50 cm2


Negative 0.02

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample mg/kg with 50cm2 = Milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. Responsibility of Chemist: Ryan Lin/ Pelny Hsiao Date Sample Received : Mar 18, 2014 Test Period : Mar 18, 2014 to Mar 20, 2014 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm)


Test Report








Sampling



Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample




dissolved

Test Report





End of Report










Polyfil AGGina GregorioOberallmendstrasse 20A

6300 Zug / SwitzerlandF0rth,2013-06-31

Test report No. FUHLl236935E

Atrival in hb: 2012{12-04i P€.iod of XRF amltcis ind. s€mpl6 p€pa.alion and pholo documerlôn: 2012- 12-07 - 2012-12- 10Podod of analysis ior u|€ €od€l; 2013{6-08 - 2013-06-29Head ol Ino.ganic Lab: Claudia Lisi

Copyino ihis ret epon is pemitted only in agemenl Rilh lhe conl€ct€d lab. Ths l€61 r€sulls r€fsr only lo lhe tested ilem.lhis €port consi6ls ot 6 pag€(s).The lest meihotts signed wnh 'ae noi lbl6d in lhe atlachmont oflhs acc€dihlion c€rllfrcate.

Testing of a material sample according to the RoHS directive 201 l/65/EC

Samole descrioiioni Ni36Fe64MAg wire; part no. 962464; batch 497255Rev,8

Conclusion based on tested item

Test ordet Slatug

t*ting accordlng to th€ RoHS dirEctive 201'l /65/EC pa33

Please see overview of test results

- Tosl resu/fs see ,ext pages -

lnlenek Consumer Goods GmbHw0rzburger St|aoe 152

re l . :+49 911 74075 0Fax:+4991I 74075 [email protected]

Amtsgercht Fudh, FIRB 5756USt- ldNr DE169317871

Geschritsi0hrof l;l',iii,lXii:,i::[lli:.:]il'.fli:KavCrbnhardtla;"li,rq Mii letsserer

tlTk*"

PaBe 2 of 5 page(s)ofourrest epon No. FUHr!236935E daled 20134631

Samole deacriotion: Ni36Fe64MAg wire; part no. 962464;

nlt = non MatalM = Metalcm = composit. Material

List of component oarts:

batch 497255Rev,8

Samplo No. Part No. Matarlal De6crlptlon

236935 1 Ni36Fe64MAo wirel Dart no. 962464i batch 497255Rev.B

EE!!E

Comment

LOD =

lnlenek consumer Goods GmbFl

Limit of Detection

Below LimitOver LimitInconclusive, further test necessaryStandard deviation

Composite sample

Remaft:

Results were obtained by EDXRF for primary screening. Additional chemicaltesting using ICP (for Cd, Pb),AAS (for Hg), lC-UCA/IS (for CrVl) and GC/MS (for PBBS/PBDES) are recommended, ifthe concentrationexceeds the belowwaming value according to IEC 62321.

Element Unit non - matal mola:cd m q / K q BL < (70_30) <X < (130+30) sOL BL< 170-30) <X< (130+30)< OL

BL s (700-30) < x < (1300+30) < oL BL s (700-30) < X < (1300+30) < OLHO m q / k q BL < (700-3o) < X < (1300+30) < OL BL < t70G.30) < X < {1300+30) < OLBr BLs l30G3o)<XCr m q / k q B L < ( 7 0 G 3 o ) < X BL<f700-3o)<X

Element Unit compoaite materialcd m q / K q L O D < X < ( 1 s 0 + 3 0 ) < O LPb m o / K o BL I {500-30) < X < (1500+30) < OLHq m o / k o BL s (500-30) < X < (1500+30) < OL

m q / k q B L 3 ( 2 5 0 - 3 0 ) < XCr m o / K o B L < f 5 0 0 - 3 o ) < X

tel.:+49 911 74075 0Fax: +49 911 1447 5 30cg.gemaf y@ nteJtek.com

Amtsgerichl Fijnlr, HRB 5756

Page 3 of 5 pageG) ol our t€st repolt No. FU H L1 235935E dated 201 34631

Sample description: Ni36Fe64MAg wire; pan no. 95246,4;batch 497255Rev.8

1, xRF screening

I\rethod: XRF according to IEC 62321:2008'

Analysis of reorder

2. Analysis of metals by ICP-MS, results in mg/kg

Method:

Staius

Status

pass

Pb. Cd. Cr: DIN EN ISO 17294-2'"Digsstion:with conc. HNO3 + HCI'*

Detection limit: Pb 0.5 mg/kg, Cd 0.2 mg/kg, Cr 1 mg/kg. Hg: 0.'1 mgrkg

Sample No. Pari No. Pb Hg cd

236935 I < 0.2 < 0.5 330

Comment:

lrbYId. Con||lni.. Good Gr bll

/*z''z?'-Prr|.dri / r.6 M.r.iF ,

d ^ r 4 4 o r t 3 d o 6 r L * . x ! e D r b

- Ftow chatts sea ne* pase(s) -

lnrenek Conslmer Good5 GmbH

[email protected] cht Fildh, HRB 5756

Samola No. P.rt l{o. Pb H€ cd Br236935 BL BL BL BL

El€mont3 Rotls.limit valueLoad {Pbl 1000 mo/koMorcury{Hq) 1000 mo/koCrdmlum (Cd) 100 mq/lqCh.omiu|n Vl (CrVl) '1000 mo/koPolyb.omlnated Blphenyle (PgB8) 1000 mq/kqpolvbrominatod DiDh€nyl lthor {PBDE3l 1000 mq/kq

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Polyfil AGGina GregorioOberallmendstrasse 20A

6300 zug / SwitzerlandFilrth,2013-06-31

Test report No. FUHL't236937E

Testing of a material sample according to the RoHS directive 2011/65/EC

Sampl€ d€scriotion: Ni42FeSSMCulttAg wire; part no. HL25351

Advalin f6b: 2012{12-04; P€dod of XRF snalysis incl. sample prepaEiion and pholo d@ume alion-,2412-1247 - 2012-12-10Penod ol analysis ior the @Et€r: 2013-0fi8 - 2013{G29H@d of Inooenic Lab: Claudia Lbt

Copying lhls lest Eporl is pemilted dly in ag@menl with th€ @ntact€d lab. Tho test csulls eier only lo the !6s1€d iin.This repoft @nsists of 6 page{s).The test melhods signed with ' aE not ljsl€d in lh€ attschm€nt ol lhe aeedibnon @nin@le.

Conclusion based on tested item

Tost ordel Statust$ting according to lhe RoHS directlve 2011/6tEC pass

Please see overview of test results

- Iest aesulls see ngxl pages

lntertek Conslmer Goods Gmbli fe l . : +49911 74075 0

cg [email protected]

s r / , r n a e r . a r L L n q n ' ! \ " _ i

.nhqe.r. J r . cB / \b Ka? o do, . , : . : ' : . : i . . . , t .PH*r ls i ,diNf.DFl69:17871 la;-JorqMil leFsei ler ' ' "^

Pa8E 2 oi 5 paSEls) ot our tes epon No. FUHL1235937E dat€d 2013-0631

Sample description: Niil2FesSMCuMAg wire; part no. HL26351

nM = non MeialM = metalcM = composite Material

Llst of comoonent oarts:

Photo:

Comment

B L =

Limit of Detection

Below LimitOver LimitInconclusive, furlher test necessaryStandard deviation

Composite samplecs

Remark:

Results were obtained by EDXRF for primary screening. Additionalchemicaltesting using ICP (for Cd, Pb),AAS (for Hg), IC-UC /lS (for CrVl) and GC/MS (for PBBS/PBDEs) are recommended, if the concentrationexceeds lhe below waming value according to IEC 62321.

Element Unlt non - ne|al metalcd BL< (70-3s) <X< {130+30)< OL BL< (70-3ol < X < (130+30)< OLPb mo/Ko BL < (700-30) < x < (1300+30) < oL BL s {700-30) < X < (1300+30) < OLHq m q / K q BL < (700-30) < x < (1300+30) < oL BL 3 {700_30) < X < (1300+30) 3 OL

B L < ( 3 0 0 - 3 0 ) < XCr m q / K q BL<(700-30 )<X BLs(700-30 )<X

Element Unit connoalle mai0rialcd m o / K o L O o < X < ( 1 5 0 + 3 0 ) < O LPb m q / k a BL 3 {500-30) < X < ('1500+30) < OLHq m q / K q BL < 1500-30) < X < (1500+30) s OL

m q / K q BL<f250-3o)<XCr m q / k q B L < ( 5 0 0 - 3 0 ) < X

nrenek consuder Goods GmbH Tel. +49 91i 74075 0Fax +49911 74075 l0c9.!eREn'@hlertek.com

Aml5ger chl Fijrth, NRB 5756U5t - ldNr . D1r69317871

Sample No, Part No. Mderial Dqscriplion

236937 1 Ni42Fe5SMCuMAq wire; part no. H126351

P.8e 3 oi 5 page(s) ot ou/ rest repo't No. FU H Lr 2369371 dated 20r 3-0&3r

Sample descriotion: Ni42FeSSMCuMAg wire; part no. HL26351

1. XRF scr€ening

Method: XRF according to IEC 62321:2008'

Analysis of reorder

2. Analysis of metals by ICP.MS, results in mg/kg

Method: Pb, Cd, Cr: DIN EN ISO 17234-2.'Digestion: with conc. HNO3 + HCr

Detection limit Pb 0.5 mg/kg, Cd 0.2 mg/kg, Cr 1 mg/kg, Hg: 0.1 mg/kg

Samplo No. Pa.t o. Pb Hg cd

236937 I < 1 < 0.2 < 0.5 360

Commont:

lntcrtd( Conruner Good GmbH

/-*o.-F-hiiileitung I Ltb Manater- ,

o a td'! o ( cdhldr o Dr, K r..*6du&r, x. rd. d D. r.'oL niolfl. oM, r.|.!di*, oor, R.l&., oItliE oi{ rudl

Statu€

Status

pass

- Flow charb see next page(s)

lnterlek co.siner Good5 GmbH

cq,qe ndiy@ nrerLek..otrrAmtsgercht Firrth, HRB 5756

Samllol{o Part l{o. Pb Hg cd Br236937 BL BL BL BL

Elsm.nts RoHs{lmli wlueLead (Pbl 1000 mo/koMsrcurv (Ho) 1000 mo/koC.dmlum (Cd) '100 ma/kqChromium Vl (Cr Vl) 1000 mq/kqPolvbromlnated BlDhente (PBB3) 1000 mo/kqPolvbrominatsd Diohonyl oth.r {PAOE's) 1000 mo/kq

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Applicant: Littelfuse Philippines Inc. Date : Nov 07, 2013 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Solder Part Number : 692321 Date Sample Received : Oct 30, 2013 Date Test Started : Oct 31, 2013

Test Conducted :


Test Report







Silvery metal RL

Heavy Metal



ND 2



880880 2



ND 2


50 cm2


Negative 0.02

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, quantitation limit of analyte in sample mg/kg with 50cm2 = Milligram per kilogram with 50 square centimeter Negative = A negative test result indicated positive observation was not found at the time of test. Responsibility of Chemist: Kevin Liu/ Irene Chiou Date Sample Received : Oct 30, 2013 Test Period : Oct 31, 2013 to Nov 07, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm)


Test Report





Test For Cd/Pb/Hg/Chromium (VI) Reference Standard：Cd/Pb: IEC 62321-5:2013; Hg: IEC 62321-4:2013; Chromium (VI): IEC 62321:2008

Sampling



Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample




dissolved

Test Report





End of Report










Test Report Number: 140101201SHA-001

Intertek Testing Services Ltd., Shanghai Page 1 of 10 Block B, Jinling Business Square, No.801 YiShan Road, Shanghai, China. 200233

上海天祥質量技術服務有限公司

上海市宜山路801 號金陵商務廣場B 座 200233 Telephone: +86 21 6120 6060 Facsimile: +86 21 6127 9740

www.intertek.com www.intertek.com.cn

Applicant: LITTELFUSE, INC. Date: Jan. 29, 2014 800 E. NORTHWEST HWY

DES PLAINES, IL 60016 ATTN: J. CABILAN / A. CESISTA JR

Sample Description: One (1) submitted sample said to be: Blue liquid Part Description : Sealant Part Number : 087266

***************************************************************************************************************************************************** Tests conducted:

As requested by the applicant, for details refer to attached page(s). ***************************************************************************************************************************************************** Conclusion:

Tested sample Standard Result Submitted sample Restriction of the use of certain hazardous substance in electrical

and electronic equipment (RoHS Directive 2011/65/EU) Pass

**************************************************************************************************************************************************** To be continued

Prepared and check by: For Intertek Testing Services Ltd., Shanghai

Authorized by: For Intertek testing services Ltd., Shanghai

Joy Zhou Jonny Jing Manager






Tests Conducted 1. RoHS testing and Halogen content (I) Test Result Summary：

Testing Item Result (ppm) Heavy Metal Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks：ppm = parts per million = mg/kg

ND = not detected Responsibility of Chemist：John Zeng / Leaf Liu

***************************************************************************************************************************************************** To be continued






Tests Conducted (II) RoHS Requirement：

Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)

The above limits were quoted from RoHS Directive 2011/65/EU for homogeneous material.

(III) Test Method：

Testing Item Testing Method Reporting Limit

Cadmium (Cd) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 ppm

Lead (Pb) content With reference to IEC 62321-5 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 ppm

Mercury (Hg) content With reference to IEC 62321-4 Edition 1.0: 2013, by acid digestion until the tested sample was totally dissolved, and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-VIS Spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)

With reference to IEC 62321 edition 1.0:2008 in Annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by Ion Chromatography

50 ppm

Remark：Reporting limit = Quantitation Limit of Analyze in Sample

***************************************************************************************************************************************************** To be continued






Tests Conducted (IV) Measurement Flowchart：

Test for Cd/ Pb/ Hg/Cr (VI)/ PBBs/PBDEs Contents Reference Standard: IEC 62321 Edition 1.0：2008 & 2013

Remarks：

*1: List of appropriate acid：

MATERIAL ACID ADDED FOR DIGESTION Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCL,HF Electronics HNO3,HCL,H2O2,HBF4

*2: If the result of spot test is positive, Chromium (VI) would be determined as detected.

*****************************************************************************************************************************************************

To be continued

No

Yes

Sampling/grinding or cutting

Weigh sample and for different material, digest

the sample with appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline

solution

Definite temp. Extraction

Make up with deionized water and add diphenyl-carbazide

solution

Cr6+

Weigh sample and add organic

solvent

Soxhlet extraction or

Solvent extraction

Concentrate the extract and make up with organic

solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

Spot test

Get 50cm2 samples


Metal Polymers / electronics

Positive*2


dissolved Cool and filter the extract






Tests Conducted (V) Measurement flowchart：

Test or Halogen content Reference standard： EN 14582

*****************************************************************************************************************************************************

To be continued

Add absorbent in a combustion

flask & place weighted sample

in equipment

Fill the combustion flask with Oxygen

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask


Sampling/grinding or cutting

Analyzed by Ion Chromatography






Tests Conducted 2. Phthalate content test

With reference to EN 14372 by Gas Chromatography-Mass Spectrometry (GC-MS) analysis.

Tested Compound Result (%,w/w) Client’ requirement (%, w/w) Di-butyl phthalate (DBP) ND - Di(2-ethyl hexyl) phthalate(DEHP) ND - Benzyl butyl phthalate (BBP) ND - Sum of three phthalates ND 0.1

Remark：Detection Limit = 0.01%(w/w)

ND = Not Detected *****************************************************************************************************************************************************

To be continued






Tests Conducted

Measurement flowchart： Test for phthalate content

****************************************************************************************************************************************************

To be continued

Weigh sample and place in a

thimble

Extracted by soxhlet extraction

with organic solvent

Concentrate the extract

Make up with organic solvent

Transfer the extract into a

volumetric flask

Analyze by GC-MS






Tests Conducted 3. HBCDD content

(Ⅰ)Test result summary：

Testing item Result (ppm)

HBCDD (hexabromocyclododecane) ND

Remarks：ppm = parts per million = mg/kg

ND = Not detected

(Ⅱ) Test method：

Testing item Testing method Reporting limit

HBCDD (hexabromocyclododecane) With reference to US EPA 3540C, by solvent extraction and determined by GC-MS

10 ppm

Date sample received: Jan. 24, 2014 Testing period: Jan. 24, 2014 To Jan. 28, 2014

****************************************************************************************************************************************************

To be continued






Tests Conducted

Measurement flowchart： Test for HBCDD (hexabromocyclododecane) content

****************************************************************************************************************************************************

To be continued

Weigh sample and place into a thimble

Soxhlet extraction with organic solvent

Concentrate the extract

Analyze by GC-MS

Make up with organic solvent

Transfer the extract into a volumetric flask






Tests Conducted

****************************************************************************************************************************************************

End of report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to

the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of

our gross negligence or wilful misconduct.


Authorized by: On Behalf of Intertek Testing Services Taiwan Limited

K. Y. Liang Director


8F., No. 423, Ruiguang Rd., Neihu District, Taipei 11492, Taiwan, R.O.C.


Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

Applicant: Littelfuse Philippines Inc. Date : Jun 19, 2013 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description: One (1) group of submitted sample(s) said to be : Part Description : Anaerobic Adhesive Part Number : 087266 Date Sample Received : Jun 11, 2013 Date Test Started : Jun 13, 2013

Test Conducted :


Test Report





Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410



Green liquid RL

Heavy Metal


ND 2

Phthalates

Diisobutyl Phthalate (DIBP) ppm With reference to EN 14372: 2004, by solvent extraction and determined by GC-MS.

ND 10

Remarks: ppm = parts per million based on wet weight of tested sample = mg/kg ND = Not detected RL = Reporting Limit, Quantitation limit of analyte in sample Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Jun 11,2013 Test Period : Jun 13,2013 To Jun 17,2013

Test Report





Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Sampling



Analyzed by ICP-OES


Test Report





Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410


Sampling




Analyzed by GC-MS

Test Report





Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2410

End of Report

This report is made solely on the basis of your instructions and/or information and materials supplied by you. It is not intended to be a recommendation for any particular course of action. Intertek does not accept a duty of care or any other responsibility to any person other than the Client in respect of this report and only accepts liability to the Client insofar as is expressly contained in the terms and conditions governing Intertek's provision of services to you. Intertek makes no warranties or representations either express or implied with respect to this report save as provided for in those terms and conditions. We have aimed to conduct the Review on a diligent and careful basis and we do not accept any liability to you for any loss arising out of or in connection with this report, in contract, tort, by statute or otherwise, except in the event of our gross negligence or wilful misconduct.







Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Black Ink 425809 Part Number : 425809 Date Sample Received : Mar 18, 2014 Date Test Started : Mar 18, 2014

Test Conducted :


Test Report







Submitted sample RL

Heavy Metal



ND 2



ND 2



ND 2


ND 2

Chromium VI (Cr6+) content ppm

With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.

ND 1

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ppm ND 5

Dibrominated Biphenyls (DiBB) ppm ND 5

Tribrominated Biphenyls (TriBB) ppm ND 5

Tetrabrominated Biphenyls (TetraBB) ppm ND 5

Pentabrominated Biphenyls (PentaBB) ppm ND 5

Hexabrominated Biphenyls (HexaBB) ppm ND 5

Heptabrominated Biphenyls (HeptaBB) ppm ND 5

Octabrominated Biphenyls (OctaBB) ppm ND 5

Nonabrominated Biphenyls (NonaBB) ppm ND 5

Decabrominated Biphenyl (DecaBB) ppm

With reference to IEC 62321: 2008, by solvent extraction and determined by GC-MS and further HPLC-DAD confirmation when necessary.

ND 5

Test Report





Result

Test Item Unit Test Method Submitted sample

RL

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ppm ND 5

Dibrominated Diphenyl Ethers (DiBDE) ppm ND 5

Tribrominated Diphenyl Ethers (TriBDE) ppm ND 5

Tetrabrominated Diphenyl Ethers (TetraBDE) ppm ND 5

Pentabrominated Diphenyl Ethers (PentaBDE) ppm ND 5

Hexabrominated Diphenyl Ethers (HexaBDE) ppm ND 5

Heptabrominated Diphenyl Ethers (HeptaBDE) ppm ND 5

Octabrominated Diphenyl Ethers (OctaBDE) ppm ND 5

Nonabrominated Diphenyl Ethers (NonaBDE) ppm ND 5

Decabrominated Diphenyl Ether (DecaBDE) ppm


ND 5

Halogen Content Fluorine (F) ppm ND 50 Chlorine (Cl) ppm ND 50 Bromine (Br) ppm ND 50 Iodine (I) ppm

With reference to EN 14582:2007 by combustion bomb with oxygen and determined by Ion Chromatography. ND 50

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ppm ND 10

Dibutyl Phthalate (DBP) ppm ND 10

Benzyl Butyl Phthalate (BBP) ppm ND 10

Diisodecyl Phthalate (DIBP) ppm


ND 10

Test Report





Result

Test Item Unit Test Method Submitted sample

RL

Others

Hexabromocyclododecane (HBCDD) ppm

With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.

ND 10

Remarks: ppm = Parts per million based on wet weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample Responsibility of Chemist: Ryan Lin/ Pelny Hsiao/ Vico Lin Date Sample Received : Mar 18, 2014 Test Period : Mar 18, 2014 to Mar 21, 2014 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)


Test Report





Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard：Cd/Pb: IEC 62321-5:2013; Hg: IEC 62321-4:2013; Chromium (VI)/PBBs/PBDEs: IEC 62321:2008 Remarks: *1: List of Appropriate Acid：






solvent

PBBs/PBDEs

Analyzed by GC-MS

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized waterand add diphenyl-carbazide

solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample


Negative *2

Substrate Plating




Cr6+


appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES


dissolved

Test Report






Sampling



Analyzed by ICP-OES


Test Report





Measurement Flowchart: Test for Halogen Contents Reference Method：EN 14582

Add absorbent in a combustion bomb & place weighed sample into sample cup

Fill oxygen into the combustion bomb

Ignite then leave the bomb at room temperature



Sampling


Test Report






Sampling




Analyzed by GC-MS

Test Report





Measurement Flowchart: Test for Hexabromocyclododecane (HBCDD) Content Reference Method：USEPA 3540C

Sampling




Analyzed by GC-MS

Test Report





End of Report
















Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Omni Body Part Number : 155900-4 Date Sample Received : Oct 30, 2013 Date Test Started : Oct 31, 2013

Test Conducted :


Test Report







Beige plastic RL

Heavy Metal



ND 2



ND 2



ND 2

Chromium VI (Cr6+) content ppm

With reference to IEC 62321: 2008, by alkaline digestion and determined by UV-Vis Spectrophotometer.

ND 1

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ppm ND 5

Dibrominated Biphenyls (DiBB) ppm ND 5

Tribrominated Biphenyls (TriBB) ppm ND 5

Tetrabrominated Biphenyls (TetraBB) ppm ND 5

Pentabrominated Biphenyls (PentaBB) ppm ND 5

Hexabrominated Biphenyls (HexaBB) ppm ND 5

Heptabrominated Biphenyls (HeptaBB) ppm ND 5

Octabrominated Biphenyls (OctaBB) ppm ND 5

Nonabrominated Biphenyls (NonaBB) ppm ND 5

Decabrominated Biphenyl (DecaBB) ppm


ND 5

Test Report





Result

Test Item Unit Test Method Beige plastic

RL

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ppm ND 5

Dibrominated Diphenyl Ethers (DiBDE) ppm ND 5

Tribrominated Diphenyl Ethers (TriBDE) ppm ND 5

Tetrabrominated Diphenyl Ethers (TetraBDE) ppm ND 5

Pentabrominated Diphenyl Ethers (PentaBDE) ppm ND 5

Hexabrominated Diphenyl Ethers (HexaBDE) ppm ND 5

Heptabrominated Diphenyl Ethers (HeptaBDE) ppm ND 5

Octabrominated Diphenyl Ethers (OctaBDE) ppm ND 5

Nonabrominated Diphenyl Ethers (NonaBDE) ppm ND 5

Decabrominated Diphenyl Ether (DecaBDE) ppm


ND 5

Halogen Content Fluorine (F) ppm 111 50 Chlorine (Cl) ppm ND 50 Bromine (Br) ppm ND 50 Iodine (I) ppm

With reference to EN 14582:2007 by combustion bomb with oxygen and determined by Ion Chromatography. ND 50

Phthalates Di(2-ethylhexyl) Phthalate (DEHP) ppm ND 10

Dibutyl Phthalate (DBP) ppm ND 10

Benzyl Butyl Phthalate (BBP) ppm


ND 10

Others

Hexabromocyclododecane (HBCDD) ppm

With reference to USEPA 3540C, by solvent extraction and determined by GC-MS.

ND 10

Test Report





Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected RL = Reporting limit, quantitation limit of analyte in sample Responsibility of Chemist: Kevin Liu/ Irene Chiou/ Vico Lin Date Sample Received : Oct 30, 2013 Test Period : Oct 31, 2013 to Nov 07, 2013 RoHS Limit Restricted Substances Limits Cadmium (Cd) content 0.01% (100ppm) Lead (Pb) content 0.1% (1000ppm) Mercury (Hg) content 0.1% (1000ppm) Chromium VI (Cr6+) content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ethers (PBDEs) 0.1% (1000ppm)


Test Report





Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard：Cd/Pb: IEC 62321-5:2013; Hg: IEC 62321-4:2013; Chromium (VI)/PBBs/PBDEs: IEC 62321:2008 Remarks: *1: List of Appropriate Acid：






solvent

PBBs/PBDEs

Analyzed by GC-MS

Sample preparation

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part

Make up with deionized waterand add diphenyl-carbazide

solution

Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample


Negative *2

Substrate Plating




Cr6+


appropriate acid*1


Cd/Pb/Hg

Analyzed by ICP-OES


dissolved

Test Report





Measurement Flowchart: Test for Halogen Contents Reference Method：EN 14582

Add absorbent in a combustion bomb & place weighed sample into sample cup

Fill oxygen into the combustion bomb

Ignite then leave the bomb at room temperature



Sampling


Test Report






Sampling




Analyzed by GC-MS

Test Report





Measurement Flowchart: Test for Hexabromocyclododecane (HBCDD) Content Reference Method：USEPA 3540C

Sampling




Analyzed by GC-MS

Test Report





End of Report
















Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Omni Clip Part Number : 883-059 Date Sample Received : Oct 30, 2013 Date Test Started : Oct 31, 2013

Test Conducted :


Test Report







Silvery metal RL

Heavy Metal



ND 2



43 2



ND 2


50 cm2


Negative 0.02



Test Report






Sampling



Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample




dissolved

Test Report





End of Report
















Malvar, Batangas

Sample Description: One (1) group of submitted samples said to be : Part Description : Solder- 92.5Pb5Sn2.5Ag Part Number : 692323 Date Sample Received : Oct 30, 2013 Date Test Started : Oct 31, 2013

Test Conducted :


Test Report







Silvery metal RL

Heavy Metal



ND 2



913043 2



ND 2


50 cm2


Negative 0.02



Test Report






Sampling



Cd/Pb/Hg

Analyzed by ICP-OES





Cr6+

Analyzed by UV-VIS

By spot test

Get 50cm2 sample




dissolved

Test Report





End of Report








