Hydrothermal Synthesis Reactor Unit Zeolites and Microporous Crystals

HIRO COMPANY

Specifications• Maximum Pressure : 3MPa • Maximum Temperature : 200℃ • Principal Material : SUS304, PTFE • Reactor Vessel Volume : 　　50ml, 100ml, 150ml, 200ml, 300ml • Number of Reaction Vessels：4 (expandable to 12)

• Mixer Variable Rotation Speed : Standard Parts 0~50rpm

Our product (Hydrothermal Synthesis Reactor Unit) was developed in 1993 for the purpose of making the synthesis reaction of Zeolites and Microporous.

Main Features1)Our stirring system of Reactor Unit is an agitating type

by rotating the reaction vessels which shall be installed in a heating device.

2)It is superior in the uniformity of the temperature inside during the synthesis reaction and in the detachment of the contents.

3)It is possible to perform multiple testing material using different of contents at one time (2 – 12 kinds of materials).

Hence, that is good for comparison experiment.

4)Easy to operate.

ReactorSetting Bolt

Stainless Steel Cap

Stainless Steel Sheet

Teflon Sheet

Teflon O-ring

Teflon Inner Vessel

Stainless Steel Vessel

Use and Operating InstructionsNo.1

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Sample materials

Stainless Steel Vessel

Teflon Inner Vessel

Sample materials

Set 「Teflon O-ring」

Set 「Teflon Sheet」

Set 「Stainless Steel Sheet」

Set 「Stainless Steel Cap」

Screw the Stainless Steel Cap securely

Stainless Steel Vessel

No.3No.2

Teflon O-ring

Teflon Sheet

Stainless Steel Sheet Stainless SteelCap

Tighten the 6 Setting Bolts evenly with a torque Wrench.

After setting up the reactor vessel, attach the set reactor vessel to the rotary drive shaft in the heater unit.

No.5No.4

Setting Bolt

Turn on the switch on the right side of the heater unit, set the temperature (Note A, Program Settings) and set it to ON to begin the heating cycle.

Turn on the rotary drive and adjust the RPM speed. Normally, the speed should be 15～20rpm.

No.7No.6

Completion of Zeolites

That’s all