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ANALYTICAL REPORT
Job Number: 720-13220-1
Job Description: Hitachi GST
For:ENVIRON International Corp.
6001 Shellmound StreetSuite 700
Emeryville, CA 94608
Attention: Ms. Anne Gates
_____________________________________________
Dimple SharmaProject Manager I
[email protected]/28/2008
cc: Mr. Chris Ritchie
TestAmerica Laboratories, Inc.
TestAmerica San Francisco 1220 Quarry Lane, Pleasanton, CA
94566
Tel (925) 484-1919 Fax (925) 484-1096 www.testamericainc.com
Page 1 of 40
mailto:[email protected]://www.testamericainc.comMODocharText
Box//original signed by//
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Job Narrative720-J13220-1
CommentsNo additional comments.
Receipt TAT changed to 48 HR as per Chris Ritchie.
All other samples were received in good condition within
temperature requirements.
GC/MS VOA No analytical or quality issues were noted.
Page 2 of 40
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EXECUTIVE SUMMARY - Detections
Client: ENVIRON International Corp. Job Number: 720-13220-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
720-13220-2 EW-6
1.0 ug/L 8260B57Chloroform0.50 ug/L
8260B1.11,1-Dichloroethene0.50 ug/L
8260B1.21,1,1-Trichloroethane
720-13220-3 EW-4
0.50 ug/L 8260B0.53Carbon tetrachloride1.0 ug/L
8260B62Chloroform0.50 ug/L 8260B1.41,1-Dichloroethene0.50 ug/L
8260B5.21,1,1-Trichloroethane
720-13220-4 EW-13
2.0 ug/L 8260B100Chloroform1.0 ug/L
8260B1.41,1,1-Trichloroethane
720-13220-5FD EW-13 FD
2.0 ug/L 8260B100Chloroform1.0 ug/L
8260B1.51,1,1-Trichloroethane
720-13220-6 EW-10
10 ug/L 8260B300Chloroform
720-13220-7 EW-5
4.0 ug/L 8260B240Chloroform2.0 ug/L
8260B3.41,1,1-Trichloroethane
720-13220-9 EW-12
1.0 ug/L 8260B8.4Chloroform0.50 ug/L
8260B0.841,1,1-Trichloroethane
720-13220-10 EW-11
1.0 ug/L 8260B21Chloroform0.50 ug/L
8260B1.11,1,1-Trichloroethane
TestAmerica San Francisco
Page 3 of 40
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EXECUTIVE SUMMARY - Detections
Client: ENVIRON International Corp. Job Number: 720-13220-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
720-13220-11 EW-14
1.0 ug/L 8260B57Chloroform0.50 ug/L
8260B1.21,1,1-Trichloroethane
TestAmerica San Francisco
Page 4 of 40
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METHOD SUMMARY
Job Number: 720-13220-1Client: ENVIRON International Corp.
Preparation MethodMethodLab LocationDescription
Matrix: Water
SW846 8260BVolatile Organic Compounds by GC/MS (Low Level) TAL
SF
SW846 5030BTAL SFPurge-and-Trap
Lab References:
TAL SF = TestAmerica San Francisco
Method References:
SW846 = "Test Methods For Evaluating Solid Waste,
Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica San Francisco
Page 5 of 40
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SAMPLE SUMMARY
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
02/27/2008 0800 02/27/2008 1510EW-6-TB720-13220-1TB Water
02/27/2008 0905 02/27/2008 1510EW-6720-13220-2 Water
02/27/2008 0941 02/27/2008 1510EW-4720-13220-3 Water
02/27/2008 1015 02/27/2008 1510EW-13720-13220-4 Water
02/27/2008 1020 02/27/2008 1510EW-13 FD720-13220-5FD Water
02/27/2008 1105 02/27/2008 1510EW-10720-13220-6 Water
02/27/2008 1208 02/27/2008 1510EW-5720-13220-7 Water
02/27/2008 1230 02/27/2008 1510EW-12-EB720-13220-8EB Water
02/27/2008 1247 02/27/2008 1510EW-12720-13220-9 Water
02/27/2008 1311 02/27/2008 1510EW-11720-13220-10 Water
02/27/2008 1342 02/27/2008 1510EW-14720-13220-11 Water
TestAmerica San Francisco
Page 6 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-6-TB
02/27/2008 0800
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-1TB
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 1800
02/27/2008 1800
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 7 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-6-TB
02/27/2008 0800
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-1TB
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 1800
02/27/2008 1800
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
96 71 - 1394-Bromofluorobenzene98 62 - 1181,2-Dichloroethane-d4
(Surr)92 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 8 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-6
02/27/2008 0905
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1126
02/28/2008 1126
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane57
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-Dichloroethane1.1 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 9 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-6
02/27/2008 0905
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1126
02/28/2008 1126
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene1.2 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
116 71 - 1394-Bromofluorobenzene102 62 -
1181,2-Dichloroethane-d4 (Surr)111 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 10 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-4
02/27/2008 0941
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1159
02/28/2008 1159
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfide0.53 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane62
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-Dichloroethane1.4 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 11 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-4
02/27/2008 0941
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1159
02/28/2008 1159
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene5.2 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
108 71 - 1394-Bromofluorobenzene96 62 - 1181,2-Dichloroethane-d4
(Surr)108 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 12 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-13
02/27/2008 1015
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2046
02/27/2008 2046
2.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 10Methyl tert-butyl etherND 100AcetoneND 1.0BenzeneND
1.0DichlorobromomethaneND 2.0BromobenzeneND 2.0ChlorobromomethaneND
2.0BromoformND 2.0BromomethaneND 1002-Butanone (MEK)ND
2.0n-ButylbenzeneND 2.0sec-ButylbenzeneND 2.0tert-ButylbenzeneND
10Carbon disulfideND 1.0Carbon tetrachlorideND 1.0ChlorobenzeneND
2.0Chloroethane100 2.0ChloroformND 2.0ChloromethaneND
1.02-ChlorotolueneND 1.04-ChlorotolueneND 1.0ChlorodibromomethaneND
1.01,2-DichlorobenzeneND 1.01,3-DichlorobenzeneND
1.01,4-DichlorobenzeneND 2.01,3-DichloropropaneND
1.01,1-DichloropropeneND 2.01,2-Dibromo-3-ChloropropaneND
1.0Ethylene DibromideND 1.0DibromomethaneND
1.0DichlorodifluoromethaneND 1.01,1-DichloroethaneND
1.01,2-DichloroethaneND 1.01,1-DichloroetheneND
1.0cis-1,2-DichloroetheneND 1.0trans-1,2-DichloroetheneND
1.01,2-DichloropropaneND 1.0cis-1,3-DichloropropeneND
1.0trans-1,3-DichloropropeneND 1.0EthylbenzeneND
2.0HexachlorobutadieneND 1002-HexanoneND 1.0IsopropylbenzeneND
2.04-IsopropyltolueneND 10Methylene Chloride
TestAmerica San Francisco Page 13 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-13
02/27/2008 1015
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2046
02/27/2008 2046
2.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 1004-Methyl-2-pentanone (MIBK)ND 2.0NaphthaleneND
2.0N-PropylbenzeneND 1.0StyreneND 1.01,1,1,2-TetrachloroethaneND
1.01,1,2,2-TetrachloroethaneND 1.0TetrachloroetheneND 1.0TolueneND
2.01,2,3-TrichlorobenzeneND 2.01,2,4-Trichlorobenzene1.4
1.01,1,1-TrichloroethaneND 1.01,1,2-TrichloroethaneND
1.0TrichloroetheneND 2.0TrichlorofluoromethaneND
1.01,2,3-TrichloropropaneND
1.01,1,2-Trichloro-1,2,2-trifluoroethaneND
1.01,2,4-TrimethylbenzeneND 1.01,3,5-TrimethylbenzeneND 100Vinyl
acetateND 1.0Vinyl chlorideND 2.0Xylenes, TotalND
1.02,2-Dichloropropane
Surrogate %Rec Acceptance Limits
107 71 - 1394-Bromofluorobenzene107 62 -
1181,2-Dichloroethane-d4 (Surr)108 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 14 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-13 FD
02/27/2008 1020
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-5FD
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1233
02/28/2008 1233
2.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 10Methyl tert-butyl etherND 100AcetoneND 1.0BenzeneND
1.0DichlorobromomethaneND 2.0BromobenzeneND 2.0ChlorobromomethaneND
2.0BromoformND 2.0BromomethaneND 1002-Butanone (MEK)ND
2.0n-ButylbenzeneND 2.0sec-ButylbenzeneND 2.0tert-ButylbenzeneND
10Carbon disulfideND 1.0Carbon tetrachlorideND 1.0ChlorobenzeneND
2.0Chloroethane100 2.0ChloroformND 2.0ChloromethaneND
1.02-ChlorotolueneND 1.04-ChlorotolueneND 1.0ChlorodibromomethaneND
1.01,2-DichlorobenzeneND 1.01,3-DichlorobenzeneND
1.01,4-DichlorobenzeneND 2.01,3-DichloropropaneND
1.01,1-DichloropropeneND 2.01,2-Dibromo-3-ChloropropaneND
1.0Ethylene DibromideND 1.0DibromomethaneND
1.0DichlorodifluoromethaneND 1.01,1-DichloroethaneND
1.01,2-DichloroethaneND 1.01,1-DichloroetheneND
1.0cis-1,2-DichloroetheneND 1.0trans-1,2-DichloroetheneND
1.01,2-DichloropropaneND 1.0cis-1,3-DichloropropeneND
1.0trans-1,3-DichloropropeneND 1.0EthylbenzeneND
2.0HexachlorobutadieneND 1002-HexanoneND 1.0IsopropylbenzeneND
2.04-IsopropyltolueneND 10Methylene Chloride
TestAmerica San Francisco Page 15 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-13 FD
02/27/2008 1020
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-5FD
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1233
02/28/2008 1233
2.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 1004-Methyl-2-pentanone (MIBK)ND 2.0NaphthaleneND
2.0N-PropylbenzeneND 1.0StyreneND 1.01,1,1,2-TetrachloroethaneND
1.01,1,2,2-TetrachloroethaneND 1.0TetrachloroetheneND 1.0TolueneND
2.01,2,3-TrichlorobenzeneND 2.01,2,4-Trichlorobenzene1.5
1.01,1,1-TrichloroethaneND 1.01,1,2-TrichloroethaneND
1.0TrichloroetheneND 2.0TrichlorofluoromethaneND
1.01,2,3-TrichloropropaneND
1.01,1,2-Trichloro-1,2,2-trifluoroethaneND
1.01,2,4-TrimethylbenzeneND 1.01,3,5-TrimethylbenzeneND 100Vinyl
acetateND 1.0Vinyl chlorideND 2.0Xylenes, TotalND
1.02,2-Dichloropropane
Surrogate %Rec Acceptance Limits
112 71 - 1394-Bromofluorobenzene103 62 -
1181,2-Dichloroethane-d4 (Surr)110 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 16 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-10
02/27/2008 1105
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2120
02/27/2008 2120
10
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 50Methyl tert-butyl etherND 500AcetoneND 5.0BenzeneND
5.0DichlorobromomethaneND 10BromobenzeneND 10ChlorobromomethaneND
10BromoformND 10BromomethaneND 5002-Butanone (MEK)ND
10n-ButylbenzeneND 10sec-ButylbenzeneND 10tert-ButylbenzeneND
50Carbon disulfideND 5.0Carbon tetrachlorideND 5.0ChlorobenzeneND
10Chloroethane300 10ChloroformND 10ChloromethaneND
5.02-ChlorotolueneND 5.04-ChlorotolueneND 5.0ChlorodibromomethaneND
5.01,2-DichlorobenzeneND 5.01,3-DichlorobenzeneND
5.01,4-DichlorobenzeneND 101,3-DichloropropaneND
5.01,1-DichloropropeneND 101,2-Dibromo-3-ChloropropaneND
5.0Ethylene DibromideND 5.0DibromomethaneND
5.0DichlorodifluoromethaneND 5.01,1-DichloroethaneND
5.01,2-DichloroethaneND 5.01,1-DichloroetheneND
5.0cis-1,2-DichloroetheneND 5.0trans-1,2-DichloroetheneND
5.01,2-DichloropropaneND 5.0cis-1,3-DichloropropeneND
5.0trans-1,3-DichloropropeneND 5.0EthylbenzeneND
10HexachlorobutadieneND 5002-HexanoneND 5.0IsopropylbenzeneND
104-IsopropyltolueneND 50Methylene Chloride
TestAmerica San Francisco Page 17 of 40
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-10
02/27/2008 1105
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2120
02/27/2008 2120
10
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5004-Methyl-2-pentanone (MIBK)ND 10NaphthaleneND
10N-PropylbenzeneND 5.0StyreneND 5.01,1,1,2-TetrachloroethaneND
5.01,1,2,2-TetrachloroethaneND 5.0TetrachloroetheneND 5.0TolueneND
101,2,3-TrichlorobenzeneND 101,2,4-TrichlorobenzeneND
5.01,1,1-TrichloroethaneND 5.01,1,2-TrichloroethaneND
5.0TrichloroetheneND 10TrichlorofluoromethaneND
5.01,2,3-TrichloropropaneND
5.01,1,2-Trichloro-1,2,2-trifluoroethaneND
5.01,2,4-TrimethylbenzeneND 5.01,3,5-TrimethylbenzeneND 500Vinyl
acetateND 5.0Vinyl chlorideND 10Xylenes, TotalND
5.02,2-Dichloropropane
Surrogate %Rec Acceptance Limits
107 71 - 1394-Bromofluorobenzene109 62 -
1181,2-Dichloroethane-d4 (Surr)106 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 18 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-5
02/27/2008 1208
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2153
02/27/2008 2153
4.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 20Methyl tert-butyl etherND 200AcetoneND 2.0BenzeneND
2.0DichlorobromomethaneND 4.0BromobenzeneND 4.0ChlorobromomethaneND
4.0BromoformND 4.0BromomethaneND 2002-Butanone (MEK)ND
4.0n-ButylbenzeneND 4.0sec-ButylbenzeneND 4.0tert-ButylbenzeneND
20Carbon disulfideND 2.0Carbon tetrachlorideND 2.0ChlorobenzeneND
4.0Chloroethane240 4.0ChloroformND 4.0ChloromethaneND
2.02-ChlorotolueneND 2.04-ChlorotolueneND 2.0ChlorodibromomethaneND
2.01,2-DichlorobenzeneND 2.01,3-DichlorobenzeneND
2.01,4-DichlorobenzeneND 4.01,3-DichloropropaneND
2.01,1-DichloropropeneND 4.01,2-Dibromo-3-ChloropropaneND
2.0Ethylene DibromideND 2.0DibromomethaneND
2.0DichlorodifluoromethaneND 2.01,1-DichloroethaneND
2.01,2-DichloroethaneND 2.01,1-DichloroetheneND
2.0cis-1,2-DichloroetheneND 2.0trans-1,2-DichloroetheneND
2.01,2-DichloropropaneND 2.0cis-1,3-DichloropropeneND
2.0trans-1,3-DichloropropeneND 2.0EthylbenzeneND
4.0HexachlorobutadieneND 2002-HexanoneND 2.0IsopropylbenzeneND
4.04-IsopropyltolueneND 20Methylene Chloride
TestAmerica San Francisco Page 19 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-5
02/27/2008 1208
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2153
02/27/2008 2153
4.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 2004-Methyl-2-pentanone (MIBK)ND 4.0NaphthaleneND
4.0N-PropylbenzeneND 2.0StyreneND 2.01,1,1,2-TetrachloroethaneND
2.01,1,2,2-TetrachloroethaneND 2.0TetrachloroetheneND 2.0TolueneND
4.01,2,3-TrichlorobenzeneND 4.01,2,4-Trichlorobenzene3.4
2.01,1,1-TrichloroethaneND 2.01,1,2-TrichloroethaneND
2.0TrichloroetheneND 4.0TrichlorofluoromethaneND
2.01,2,3-TrichloropropaneND
2.01,1,2-Trichloro-1,2,2-trifluoroethaneND
2.01,2,4-TrimethylbenzeneND 2.01,3,5-TrimethylbenzeneND 200Vinyl
acetateND 2.0Vinyl chlorideND 4.0Xylenes, TotalND
2.02,2-Dichloropropane
Surrogate %Rec Acceptance Limits
109 71 - 1394-Bromofluorobenzene106 62 -
1181,2-Dichloroethane-d4 (Surr)105 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 20 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-12-EB
02/27/2008 1230
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-8EB
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 0218
02/28/2008 0218
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 21 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-12-EB
02/27/2008 1230
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-8EB
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 0218
02/28/2008 0218
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
110 71 - 1394-Bromofluorobenzene107 62 -
1181,2-Dichloroethane-d4 (Surr)107 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 22 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-12
02/27/2008 1247
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-9
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2226
02/27/2008 2226
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane8.4
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 23 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-12
02/27/2008 1247
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-9
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2226
02/27/2008 2226
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene0.84 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
106 71 - 1394-Bromofluorobenzene109 62 -
1181,2-Dichloroethane-d4 (Surr)106 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 24 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-11
02/27/2008 1311
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-10
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2259
02/27/2008 2259
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane21
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 25 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-11
02/27/2008 1311
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-10
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2259
02/27/2008 2259
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene1.1 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
108 71 - 1394-Bromofluorobenzene108 62 -
1181,2-Dichloroethane-d4 (Surr)108 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 26 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-14
02/27/2008 1342
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-11
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2332
02/27/2008 2332
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane57
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 27 of 40
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13220-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-14
02/27/2008 1342
02/27/2008 1510Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13220-11
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/27/2008 2332
02/27/2008 2332
1.0
8260B Analysis Batch: 720-32409
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900F
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene1.2 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
110 71 - 1394-Bromofluorobenzene109 62 -
1181,2-Dichloroethane-d4 (Surr)105 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 28 of 40
-
DATA REPORTING QUALIFIERS
Lab Section Qualifier Description
Page 29 of 40
-
Quality Control Results
Client: ENVIRON International Corp. Job Number: 720-13220-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep
Batch
ReportBasis
GC/MS VOA
Analysis Batch:720-32409Lab Control Spike Water 8260BLCS
720-32409/2 TLab Control Spike Duplicate Water 8260BLCSD
720-32409/1 TMethod Blank Water 8260BMB 720-32409/3 T
WaterEW-6-TB 8260B720-13220-1TB TMatrix Spike Water
8260B720-13220-A-3 MS TMatrix Spike Duplicate Water
8260B720-13220-A-3 MSD T
WaterEW-13 8260B720-13220-4 TWaterEW-10 8260B720-13220-6
TWaterEW-5 8260B720-13220-7 TWaterEW-12-EB 8260B720-13220-8EB
TWaterEW-12 8260B720-13220-9 TWaterEW-11 8260B720-13220-10
TWaterEW-14 8260B720-13220-11 T
Analysis Batch:720-32438Lab Control Spike Water 8260BLCS
720-32438/2 TLab Control Spike Duplicate Water 8260BLCSD
720-32438/1 TMethod Blank Water 8260BMB 720-32438/3 T
WaterEW-6 8260B720-13220-2 TWaterEW-4 8260B720-13220-3
TWaterEW-13 FD 8260B720-13220-5FD T
Report Basis
T = Total
TestAmerica San Francisco
Page 30 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
02/27/2008 1726
Method Blank - Batch: 720-32409
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 720-32409
Prep Batch: N/A
02/27/2008 1726
c:\saturnws\data\200802\0227
40 mL
40 mL
Units: ug/L
Method: 8260BPreparation: 5030B
Varian 3900FMB 720-32409/3
Analyte Result Qual RL
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-Hexanone
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 31 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
02/27/2008 1726
Method Blank - Batch: 720-32409
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 720-32409
Prep Batch: N/A
02/27/2008 1726
c:\saturnws\data\200802\0227
40 mL
40 mL
Units: ug/L
Method: 8260BPreparation: 5030B
Varian 3900FMB 720-32409/3
Analyte Result Qual RL
ND 0.50IsopropylbenzeneND 1.04-IsopropyltolueneND 5.0Methylene
ChlorideND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 102 71 - 1391,2-Dichloroethane-d4 (Surr)
104 62 - 118Toluene-d8 (Surr) 106 73 - 117
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 32 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
02/27/2008 1620
02/27/2008 1653
Lab Control Spike/Lab Control Spike Duplicate Recovery Report -
Batch: 720-32409
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
02/27/2008 1620
Prep Batch: N/A
Analysis Batch: 720-32409
c:\saturnws\data\200802\022708
40 mL
40 mL
c:\saturnws\data\200802\022708\
40 mL
40 mL
ug/L
02/27/2008 1653
Analysis Batch: 720-32409
Prep Batch: N/A
Method: 8260BPreparation: 5030B
Varian 3900F
Varian 3900F
LCS 720-32409/2
LCSD 720-32409/1
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9697 69 - 129 2 20Benzene
104105 61 - 121 1 20Chlorobenzene
9797 65 - 125 0 201,1-Dichloroethene
9699 70 - 130 3 20Toluene
9198 74 - 134 7 20Trichloroethene
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 105 99 71 - 1391,2-Dichloroethane-d4 (Surr)
97 96 62 - 118Toluene-d8 (Surr) 105 99 73 - 117
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 33 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
02/27/2008 1906
02/27/2008 1940
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch:
720-32409
4.0
4.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 720-32409
Analysis Batch: 720-32409
02/27/2008 1906
02/27/2008 1940
Prep Batch: N/A
Prep Batch: N/A
c:\saturnws\data\200802\022
40 mL
40 mL
c:\saturnws\data\200802\0227
40 mL
40 mL
Method: 8260BPreparation: 5030B
Varian 3900F
Varian 3900F
720-13220-A-3 MS
720-13220-A-3 MSD
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
89 92 69 - 129 3 20Benzene
96 101 61 - 121 5 20Chlorobenzene
87 95 65 - 125 9 201,1-Dichloroethene
88 91 70 - 130 3 20Toluene
85 90 74 - 134 6 20Trichloroethene
Surrogate MS % Rec MSD % Rec Acceptance Limits
4-Bromofluorobenzene 97 96 71 - 1391,2-Dichloroethane-d4 (Surr)
97 95 62 - 118Toluene-d8 (Surr) 100 93 73 - 117
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 34 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
02/28/2008 1052
Method Blank - Batch: 720-32438
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 720-32438
Prep Batch: N/A
02/28/2008 1052
c:\saturnws\data\200802\0228
40 mL
40 mL
Units: ug/L
Method: 8260BPreparation: 5030B
Varian 3900GMB 720-32438/3
Analyte Result Qual RL
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-Hexanone
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 35 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
02/28/2008 1052
Method Blank - Batch: 720-32438
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 720-32438
Prep Batch: N/A
02/28/2008 1052
c:\saturnws\data\200802\0228
40 mL
40 mL
Units: ug/L
Method: 8260BPreparation: 5030B
Varian 3900GMB 720-32438/3
Analyte Result Qual RL
ND 0.50IsopropylbenzeneND 1.04-IsopropyltolueneND 5.0Methylene
ChlorideND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 115 71 - 1391,2-Dichloroethane-d4 (Surr)
107 62 - 118Toluene-d8 (Surr) 109 73 - 117
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 36 of 40
-
Quality Control Results
Job Number: 720-13220-1Client: ENVIRON International Corp.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
02/28/2008 0945
02/28/2008 1018
Lab Control Spike/Lab Control Spike Duplicate Recovery Report -
Batch: 720-32438
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
02/28/2008 0945
Prep Batch: N/A
Analysis Batch: 720-32438
c:\saturnws\data\200802\022808
40 mL
40 mL
c:\saturnws\data\200802\022808\
40 mL
40 mL
ug/L
02/28/2008 1018
Analysis Batch: 720-32438
Prep Batch: N/A
Method: 8260BPreparation: 5030B
Varian 3900G
Varian 3900G
LCS 720-32438/2
LCSD 720-32438/1
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9696 69 - 129 1 20Benzene
107102 61 - 121 5 20Chlorobenzene
10198 65 - 125 3 201,1-Dichloroethene
9894 70 - 130 3 20Toluene
9188 74 - 134 4 20Trichloroethene
Surrogate LCS % Rec LCSD % Rec Acceptance Limits
4-Bromofluorobenzene 97 105 71 - 1391,2-Dichloroethane-d4 (Surr)
93 99 62 - 118Toluene-d8 (Surr) 88 96 73 - 117
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 37 of 40
-
Page 38 of 40
MODocharText Box
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MODocharText Box
-
Page 39 of 40
MODocharText Box
MODocharText Box
MODocharText Box
-
Login Sample Receipt Check List
Client: ENVIRON International Corp. Job Number: 720-13220-1
Login Number: 13220
Question T / F/ NA Comment
Creator: Bullock, Tracy
List Source: TestAmerica San Francisco
List Number: 1
Radioactivity either was not measured or, if measured, is at or
below background
N/A
The cooler's custody seal, if present, is intact. N/A
The cooler or samples do not appear to have been compromised or
tampered with.
True
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. False
There are no discrepancies between the sample IDs on the
containers and the COC.
True
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses, incl. any
requested MS/MSDs
True
VOA sample vials do not have headspace or bubble is
-
ANALYTICAL REPORT
Job Number: 720-13236-1
Job Description: Hitachi GST
For:ENVIRON International Corp.
6001 Shellmound StreetSuite 700
Emeryville, CA 94608
Attention: Ms. Anne Gates
_____________________________________________
Dimple SharmaProject Manager I
[email protected]/29/2008
cc: Mr. Chris Ritchie
TestAmerica Laboratories, Inc.
TestAmerica San Francisco 1220 Quarry Lane, Pleasanton, CA
94566
Tel (925) 484-1919 Fax (925) 484-1096 www.testamericainc.com
Page 1 of 29
mailto:[email protected]://www.testamericainc.comMODocharText
Box//original signed by//
-
Job Narrative720-J13236-1
CommentsNo additional comments.
Receipt All samples were received in good condition within
temperature requirements.
GC/MS VOA No analytical or quality issues were noted.
Page 2 of 29
-
EXECUTIVE SUMMARY - Detections
Client: ENVIRON International Corp. Job Number: 720-13236-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
720-13236-2 EW-2
1.0 ug/L 8260B19Chloroform0.50 ug/L
8260B0.931,1-Dichloroethene0.50 ug/L
8260B1.21,1,1-Trichloroethane
720-13236-3 EW-3
1.0 ug/L 8260B1.1Chloroform
720-13236-4 EW-7
1.0 ug/L 8260B3.1Chloroform0.50 ug/L
8260B0.801,1-Dichloroethene
720-13236-6 EW-15
1.0 ug/L 8260B2.3Chloroform0.50 ug/L
8260B1.11,1,1-Trichloroethane
720-13236-7 EW-8
1.0 ug/L 8260B1.9Chloroform
720-13236-8 EW-1
1.0 ug/L 8260B17Chloroform0.50 ug/L
8260B1.71,1-Dichloroethene0.50 ug/L
8260B3.61,1,1-Trichloroethane
TestAmerica San Francisco
Page 3 of 29
-
METHOD SUMMARY
Job Number: 720-13236-1Client: ENVIRON International Corp.
Preparation MethodMethodLab LocationDescription
Matrix: Water
SW846 8260BVolatile Organic Compounds by GC/MS (Low Level) TAL
SF
SW846 5030BTAL SFPurge-and-Trap
Lab References:
TAL SF = TestAmerica San Francisco
Method References:
SW846 = "Test Methods For Evaluating Solid Waste,
Physical/Chemical Methods", Third Edition, November 1986 And Its
Updates.
TestAmerica San Francisco
Page 4 of 29
-
SAMPLE SUMMARY
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
02/28/2008 0800 02/28/2008 1325EW-2-TB720-13236-1TB Water
02/28/2008 0915 02/28/2008 1325EW-2720-13236-2 Water
02/28/2008 0945 02/28/2008 1325EW-3720-13236-3 Water
02/28/2008 1015 02/28/2008 1325EW-7720-13236-4 Water
02/28/2008 1030 02/28/2008 1325EW-15-CB720-13236-5 Water
02/28/2008 1045 02/28/2008 1325EW-15720-13236-6 Water
02/28/2008 1110 02/28/2008 1325EW-8720-13236-7 Water
02/28/2008 1145 02/28/2008 1325EW-1720-13236-8 Water
TestAmerica San Francisco
Page 5 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-2-TB
02/28/2008 0800
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-1TB
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1447
02/28/2008 1447
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 6 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-2-TB
02/28/2008 0800
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-1TB
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1447
02/28/2008 1447
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
120 71 - 1394-Bromofluorobenzene107 62 -
1181,2-Dichloroethane-d4 (Surr)113 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 7 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-2
02/28/2008 0915
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1521
02/28/2008 1521
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane19
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-Dichloroethane0.93 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 8 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-2
02/28/2008 0915
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1521
02/28/2008 1521
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene1.2 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
118 71 - 1394-Bromofluorobenzene107 62 -
1181,2-Dichloroethane-d4 (Surr)114 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 9 of 29
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-3
02/28/2008 0945
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1702
02/28/2008 1702
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane1.1
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 10 of 29
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-3
02/28/2008 0945
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1702
02/28/2008 1702
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
114 71 - 1394-Bromofluorobenzene106 62 -
1181,2-Dichloroethane-d4 (Surr)107 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 11 of 29
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Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-7
02/28/2008 1015
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1736
02/28/2008 1736
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane3.1
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-Dichloroethane0.80 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 12 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-7
02/28/2008 1015
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1736
02/28/2008 1736
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
112 71 - 1394-Bromofluorobenzene105 62 -
1181,2-Dichloroethane-d4 (Surr)108 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 13 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-15-CB
02/28/2008 1030
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-5
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1809
02/28/2008 1809
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 14 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-15-CB
02/28/2008 1030
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-5
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1809
02/28/2008 1809
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
118 71 - 1394-Bromofluorobenzene105 62 -
1181,2-Dichloroethane-d4 (Surr)110 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 15 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-15
02/28/2008 1045
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1843
02/28/2008 1843
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane2.3
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 16 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-15
02/28/2008 1045
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1843
02/28/2008 1843
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene1.1 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
114 71 - 1394-Bromofluorobenzene102 62 -
1181,2-Dichloroethane-d4 (Surr)108 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 17 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-8
02/28/2008 1110
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1916
02/28/2008 1916
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane1.9
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 18 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-8
02/28/2008 1110
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1916
02/28/2008 1916
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
112 71 - 1394-Bromofluorobenzene102 62 -
1181,2-Dichloroethane-d4 (Surr)106 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 19 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-1
02/28/2008 1145
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-8
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1950
02/28/2008 1950
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0Chloroethane17
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-Dichloroethane1.7 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-HexanoneND 0.50IsopropylbenzeneND
1.04-IsopropyltolueneND 5.0Methylene Chloride
TestAmerica San Francisco Page 20 of 29
-
Analytical Data
Client: ENVIRON International Corp. Job Number: 720-13236-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
EW-1
02/28/2008 1145
02/28/2008 1325Client Matrix:
8260B Volatile Organic Compounds by GC/MS (Low Level)
720-13236-8
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
02/28/2008 1950
02/28/2008 1950
1.0
8260B Analysis Batch: 720-32438
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: Varian 3900G
c:\saturnws\data\200802\02
40 mL
40 mL
5030B
Analyte Result (ug/L) RLQualifier
ND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-Trichlorobenzene3.6 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate %Rec Acceptance Limits
123 71 - 1394-Bromofluorobenzene108 62 -
1181,2-Dichloroethane-d4 (Surr)115 73 - 117Toluene-d8 (Surr)
TestAmerica San Francisco Page 21 of 29
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DATA REPORTING QUALIFIERS
Lab Section Qualifier Description
Page 22 of 29
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Quality Control Results
Client: ENVIRON International Corp. Job Number: 720-13236-1
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep
Batch
ReportBasis
GC/MS VOA
Analysis Batch:720-32438Lab Control Spike Water 8260BLCS
720-32438/2 TLab Control Spike Duplicate Water 8260BLCSD
720-32438/1 TMethod Blank Water 8260BMB 720-32438/3 TMatrix Spike
Water 8260B720-13081-B-2 MS TMatrix Spike Duplicate Water
8260B720-13081-C-2 MSD T
WaterEW-2-TB 8260B720-13236-1TB TWaterEW-2 8260B720-13236-2
TWaterEW-3 8260B720-13236-3 TWaterEW-7 8260B720-13236-4
TWaterEW-15-CB 8260B720-13236-5 TWaterEW-15 8260B720-13236-6
TWaterEW-8 8260B720-13236-7 TWaterEW-1 8260B720-13236-8 T
Report Basis
T = Total
TestAmerica San Francisco
Page 23 of 29
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Quality Control Results
Job Number: 720-13236-1Client: ENVIRON International Corp.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
02/28/2008 1052
Method Blank - Batch: 720-32438
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 720-32438
Prep Batch: N/A
02/28/2008 1052
c:\saturnws\data\200802\0228
40 mL
40 mL
Units: ug/L
Method: 8260BPreparation: 5030B
Varian 3900GMB 720-32438/3
Analyte Result Qual RL
ND 5.0Methyl tert-butyl etherND 50AcetoneND 0.50BenzeneND
0.50DichlorobromomethaneND 1.0BromobenzeneND
1.0ChlorobromomethaneND 1.0BromoformND 1.0BromomethaneND
502-Butanone (MEK)ND 1.0n-ButylbenzeneND 1.0sec-ButylbenzeneND
1.0tert-ButylbenzeneND 5.0Carbon disulfideND 0.50Carbon
tetrachlorideND 0.50ChlorobenzeneND 1.0ChloroethaneND
1.0ChloroformND 1.0ChloromethaneND 0.502-ChlorotolueneND
0.504-ChlorotolueneND 0.50ChlorodibromomethaneND
0.501,2-DichlorobenzeneND 0.501,3-DichlorobenzeneND
0.501,4-DichlorobenzeneND 1.01,3-DichloropropaneND
0.501,1-DichloropropeneND 1.01,2-Dibromo-3-ChloropropaneND
0.50Ethylene DibromideND 0.50DibromomethaneND
0.50DichlorodifluoromethaneND 0.501,1-DichloroethaneND
0.501,2-DichloroethaneND 0.501,1-DichloroetheneND
0.50cis-1,2-DichloroetheneND 0.50trans-1,2-DichloroetheneND
0.501,2-DichloropropaneND 0.50cis-1,3-DichloropropeneND
0.50trans-1,3-DichloropropeneND 0.50EthylbenzeneND
1.0HexachlorobutadieneND 502-Hexanone
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 24 of 29
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Quality Control Results
Job Number: 720-13236-1Client: ENVIRON International Corp.
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
02/28/2008 1052
Method Blank - Batch: 720-32438
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 720-32438
Prep Batch: N/A
02/28/2008 1052
c:\saturnws\data\200802\0228
40 mL
40 mL
Units: ug/L
Method: 8260BPreparation: 5030B
Varian 3900GMB 720-32438/3
Analyte Result Qual RL
ND 0.50IsopropylbenzeneND 1.04-IsopropyltolueneND 5.0Methylene
ChlorideND 504-Methyl-2-pentanone (MIBK)ND 1.0NaphthaleneND
1.0N-PropylbenzeneND 0.50StyreneND 0.501,1,1,2-TetrachloroethaneND
0.501,1,2,2-TetrachloroethaneND 0.50TetrachloroetheneND
0.50TolueneND 1.01,2,3-TrichlorobenzeneND
1.01,2,4-TrichlorobenzeneND 0.501,1,1-TrichloroethaneND
0.501,1,2-TrichloroethaneND 0.50TrichloroetheneND
1.0TrichlorofluoromethaneND 0.501,2,3-TrichloropropaneND
0.501,1,2-Trichloro-1,2,2-trifluoroethaneND
0.501,2,4-TrimethylbenzeneND 0.501,3,5-TrimethylbenzeneND 50Vinyl
acetateND 0.50Vinyl chlorideND 1.0Xylenes, TotalND
0.502,2-Dichloropropane
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 115 71 - 1391,2-Dichloroethane-d4 (Surr)
107 62 - 118Toluene-d8 (Surr) 109 73 - 117
TestAmerica San Francisco
Calculations are performed before rounding to avoid round-off
errors in calculated results.
Page 25 of 29
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Quality Control Results
Job Number: 720-13236-1Client: ENVIRON International Corp.
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
02/28/2008 0945
02/28/2008 1018
Lab Contro
