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Highly efficient high-power thulium-doped germanate glass fiber laser Jianfeng Wu, Zhidong Yao, Jie Zong, and Shibin Jiang NP Photonics Inc, 9030 S. Rita Road, Tucson, Arizona 85747, USA Received November 28, 2006; accepted December 12, 2006; posted January 3, 2007 (Doc. ID 77523); published February 15, 2007 A 64 W fiber laser at 1.9 m with a slope efficiency of 68% with respect to the launching pump power at 800 nm was demonstrated in a one-end pump configuration using a piece of 20 cm long newly developed thulium-doped germanate glass double-cladding single-mode fiber. A quantum efficiency of 1.8 was achieved. An output laser power of 104 W at 1.9 m was demonstrated from a piece of 40 cm long fiber with a dual- end pump configuration. © 2007 Optical Society of America OCIS codes: 140.3510, 160.5690. High-power fiber lasers have generated a significant amount of interest in recent years. Highly efficient and high-power fiber lasers at 1 m with output pow- ers greater than 1 kW were demonstrated from ytterbium-doped silica fiber. 1–3 Slope efficiency is typically around 70%. These highly efficient high- power fiber lasers are being used for many industrial applications, especially in material processing. A high-power fiber laser at 1.5 m is of great interest because of the availability of components at this wavelength and, more important, because it is a retina safe wavelength. An output power of 188 W at 1.57 m was demonstrated from an erbium and yt- terbium codoped silica glass fiber laser. 4 The typical slope efficiency of the erbium and ytterbium codoped fiber laser at 1.5 m was smaller than 45% because of the large difference between the pump wavelength and laser wavelength. A thulium-doped fiber laser near 2 m is also of great interest because of the possibility of combining high efficiency, high output power, and retina safety in addition to specific applications associated with this wavelength, such as remote sensing and bio- medical applications. Thulium exhibits a significant advantage over other rare-earth ions in that the slope efficiency can exceed the Stokes limit. 5–7 A quantum efficiency near 2 can be achieved for thu- lium ions’ 3 F 4 3 H 6 transition (near 2 m) because of the so-called cross-relaxation energy transfer be- tween thulium ions. During the cross-relaxation en- ergy transfer process, two ground-level thulium ions can be excited to the upper lasing level of the 3 F 4 3 H 6 transition by absorbing only one pump photon near 800 nm, which means one excited Tm 3+ ion at the 3 H 4 level generates two Tm 3+ ions at the 3 F 4 up- per laser level. The high doping concentration is criti- cal to realize efficient cross-relaxation energy transfer. 8 A 75W cw 2 m laser was demonstrated from a 2.5 m long ytterbium-sensitized thulium- doped silica fiber. 9 The pump laser at 975 nm was ab- sorbed by the ytterbium ion and then transferred to the 3 H 5 energy level of the thulium ion. The slope ef- ficiency of the laser with respect to the launched power is 32% owing to the lack of cross-relaxation en- ergy transfer between thulium ions in ytterbium- sensitized thulium-doped fiber. Apparently, to achieve the most efficient high-power thulium-doped fiber laser, approximately 800 nm is the best pump wavelength that can make the one-for-two cross- relaxation energy transfer occur. To date, the most ef- ficient Tm 3+ -doped fiber laser reported is from a piece of 2.2 wt. % Tm 3+ -doped silica fiber directly pumped by 800 nm laser diodes. The slope efficiency of 61% with respect to the launched power was demon- strated with an output power of 30.8 W. 6 The pub- lished highest power of a Tm-doped fiber laser is 85 W, generated from a Tm 3+ -doped fiber laser under a 793 nm pump. 10 In this Letter we present a 64 W fiber laser at 1.9 m with a slope efficiency of 68% with respect to the launching pump power at 800 nm in a one-end pump configuration using a piece of 20 cm long newly developed thulium-doped ger- manate glass double-cladding single-mode fiber, and we present a 104 W fiber laser at 1.9 m from a piece of 40 cm long dual-end pumped fiber. The core glass, 4 wt. % Tm 3+ -doped germanate glass, and cladding glasses were developed and melted in house. Tm 3+ -doped germanate glass double-cladding single-mode fibers were designed and fabricated in house as well. The low phonon en- ergy of the germanate glass host compared with silica glass helps to increase the quantum efficiency and reduce the nonradiative decay rate of the upper lasing level of 3 F 4 . The high doping concentration of thulium ions ensures cross-relaxation energy trans- fer by bringing the thulium ions closer. The emission spectrum of a bulk 4 wt. % Tm 3+ -doped germanate glass under 800 nm laser excitation is shown in Fig. 1. The emission of the 3 H 4 3 F 4 transition, which is usually used as emission source for an S-band laser and amplifier at 1.47 m, can hardly be observed. The quenching of emission at 1.47 m indicates that the transition between 3 H 4 and 3 F 4 states was domi- nated by the nonradiative decay caused by cross- relaxation energy transfer, which was used to deter- mine the optimum doping concentration of our Tm 3+ -doped germanate core glass. The same core glass composition was used to fabricate Tm 3+ -doped germanate glass single-mode fiber for the recent 638 OPTICS LETTERS / Vol. 32, No. 6 / March 15, 2007 0146-9592/07/060638-3/$15.00 © 2007 Optical Society of America

Highly efficient high-power thulium-doped germanate glass fiber laser

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638 OPTICS LETTERS / Vol. 32, No. 6 / March 15, 2007

Highly efficient high-power thulium-dopedgermanate glass fiber laser

Jianfeng Wu, Zhidong Yao, Jie Zong, and Shibin JiangNP Photonics Inc, 9030 S. Rita Road, Tucson, Arizona 85747, USA

Received November 28, 2006; accepted December 12, 2006;posted January 3, 2007 (Doc. ID 77523); published February 15, 2007

A 64 W fiber laser at 1.9 �m with a slope efficiency of 68% with respect to the launching pump power at800 nm was demonstrated in a one-end pump configuration using a piece of 20 cm long newly developedthulium-doped germanate glass double-cladding single-mode fiber. A quantum efficiency of 1.8 was achieved.An output laser power of 104 W at 1.9 �m was demonstrated from a piece of 40 cm long fiber with a dual-end pump configuration. © 2007 Optical Society of America

OCIS codes: 140.3510, 160.5690.

High-power fiber lasers have generated a significantamount of interest in recent years. Highly efficientand high-power fiber lasers at 1 �m with output pow-ers greater than 1 kW were demonstrated fromytterbium-doped silica fiber.1–3 Slope efficiency istypically around 70%. These highly efficient high-power fiber lasers are being used for many industrialapplications, especially in material processing. Ahigh-power fiber laser at 1.5 �m is of great interestbecause of the availability of components at thiswavelength and, more important, because it is aretina safe wavelength. An output power of 188 W at1.57 �m was demonstrated from an erbium and yt-terbium codoped silica glass fiber laser.4 The typicalslope efficiency of the erbium and ytterbium codopedfiber laser at 1.5 �m was smaller than 45% becauseof the large difference between the pump wavelengthand laser wavelength.

A thulium-doped fiber laser near 2 �m is also ofgreat interest because of the possibility of combininghigh efficiency, high output power, and retina safetyin addition to specific applications associated withthis wavelength, such as remote sensing and bio-medical applications. Thulium exhibits a significantadvantage over other rare-earth ions in that theslope efficiency can exceed the Stokes limit.5–7 Aquantum efficiency near 2 can be achieved for thu-lium ions’ 3F4→ 3H6 transition (near 2 �m) becauseof the so-called cross-relaxation energy transfer be-tween thulium ions. During the cross-relaxation en-ergy transfer process, two ground-level thulium ionscan be excited to the upper lasing level of the 3F4→ 3H6 transition by absorbing only one pump photonnear 800 nm, which means one excited Tm3+ ion atthe 3H4 level generates two Tm3+ ions at the 3F4 up-per laser level. The high doping concentration is criti-cal to realize efficient cross-relaxation energytransfer.8 A 75 W cw 2 �m laser was demonstratedfrom a 2.5 m long ytterbium-sensitized thulium-doped silica fiber.9 The pump laser at 975 nm was ab-sorbed by the ytterbium ion and then transferred tothe 3H5 energy level of the thulium ion. The slope ef-ficiency of the laser with respect to the launchedpower is 32% owing to the lack of cross-relaxation en-

ergy transfer between thulium ions in ytterbium-

0146-9592/07/060638-3/$15.00 ©

sensitized thulium-doped fiber. Apparently, toachieve the most efficient high-power thulium-dopedfiber laser, approximately 800 nm is the best pumpwavelength that can make the one-for-two cross-relaxation energy transfer occur. To date, the most ef-ficient Tm3+-doped fiber laser reported is from a pieceof 2.2 wt. % Tm3+-doped silica fiber directly pumpedby 800 nm laser diodes. The slope efficiency of 61%with respect to the launched power was demon-strated with an output power of 30.8 W.6 The pub-lished highest power of a Tm-doped fiber laser is85 W, generated from a Tm3+-doped fiber laser undera 793 nm pump.10 In this Letter we present a 64 Wfiber laser at 1.9 �m with a slope efficiency of 68%with respect to the launching pump power at 800 nmin a one-end pump configuration using a piece of20 cm long newly developed thulium-doped ger-manate glass double-cladding single-mode fiber, andwe present a 104 W fiber laser at 1.9 �m from a pieceof 40 cm long dual-end pumped fiber.

The core glass, 4 wt. % Tm3+-doped germanateglass, and cladding glasses were developed andmelted in house. Tm3+-doped germanate glassdouble-cladding single-mode fibers were designedand fabricated in house as well. The low phonon en-ergy of the germanate glass host compared withsilica glass helps to increase the quantum efficiencyand reduce the nonradiative decay rate of the upperlasing level of 3F4. The high doping concentration ofthulium ions ensures cross-relaxation energy trans-fer by bringing the thulium ions closer. The emissionspectrum of a bulk 4 wt. % Tm3+-doped germanateglass under 800 nm laser excitation is shown in Fig.1. The emission of the 3H4→ 3F4 transition, which isusually used as emission source for an S-band laserand amplifier at 1.47 �m, can hardly be observed.The quenching of emission at 1.47 �m indicates thatthe transition between 3H4 and 3F4 states was domi-nated by the nonradiative decay caused by cross-relaxation energy transfer, which was used to deter-mine the optimum doping concentration of ourTm3+-doped germanate core glass. The same coreglass composition was used to fabricate Tm3+-doped

germanate glass single-mode fiber for the recent

2007 Optical Society of America

March 15, 2007 / Vol. 32, No. 6 / OPTICS LETTERS 639

demonstration of an efficient single-frequency fiberlaser near 2 �m.11

Two fibers with different core diameters but thesame glasses were prepared for fiber laser demon-strations. The core diameters are 50 and 42 �m. Bothof them have a 200 �m inner cladding. The numeri-cal aperture (NA) of the core is 0.02 according to therefractive indices of bulk glasses. The V-numbers ofthese two fibers at 1.9 �m are 1.96 and 1.65, respec-tively, thus supporting only the fundamental mode atthe lasing wavelength. Instead of the commonly usedpolymer, low-index glass was used as the outsidecladding material in the high-power silica fiber. Be-cause of the large core diameter, the core and innercladding area ratio is relatively large for both fibers,which leads to a large overlap between the core andthe pump laser. Such a fiber configuration ensures ef-ficient pump absorption and shortens the length ofthe active fiber. A short fiber length can be advanta-geous to avoid optical nonlinearity.

Fig. 1. Emission spectrum of 4 wt. % doped germanateglass.

Fig. 2. (Color online) Schematic of thulium-doped german

tion. (b) Dual-end pump configuration. HR, high reflection; HT,

The experiment setup for the one-end pump con-figuration is shown in Fig. 2(a). A piece of 20 cm longTm3+-doped germanate glass double-cladding fiberwith a 50 �m core diameter was placed between twowater-cooled metal plates in a sandwich structure.Both ends of the doped fiber were polished. A multi-mode fiber with a core diameter of 200 �m and NA of0.22 was used as the pump delivery fiber. The wave-length of the pump laser (Apollo Instruments) is800 nm. One end of a commercial multimode fiber,the same as the pump delivery fiber, was coated witha dichroic thin film with high reflectivity at 1.9 �mand high transmission at 800 nm, and the other endwas fusion spliced with the pump delivery fiber. Thefusion-spliced pump delivery fiber was butt coupledto the Tm3+-doped fiber, and the dielectric coatingserved as the high-reflection (HR) mirror of the fiberlaser cavity. Fresnel reflection of approximately 5%from the other polished end of the Tm3+-doped ger-manate glass fiber functioned as the partially reflec-tive mirror of the laser cavity. The experimental re-sult for the fiber laser is shown in Fig. 3. We used thelaunching power instead of the launched power in thelaser output curve. The launching power is defined asthe power measured right after the pump laser deliv-ery fiber. The maximum output power of the fiber la-ser is 64 W, which was limited by the available pumplaser power. The slope efficiency is 68% with respectto the launching power, which is significantly higherthan the Stokes limit of 42%. The slope efficiencies ofthe fiber laser with respect to the launched powerand the absorbed power are estimated to be 71.6%and 76.4%, respectively. To the best of our knowledge,this is the most efficient fiber laser near 2 �m. Thequantum efficiency is estimated to be 1.8, which isconsistent with our previous experimental results.7,12

To achieve higher output power, another fibercoupled diode laser (Limo GmbH) was used to pumpTm3+-doped germanate glass fiber from the otherend. The second pump was launched into theTm3+-doped fiber by using free-space coupling lenses

fiber laser experiment setup. (a) One-end pump configura-

ate high transmission.

640 OPTICS LETTERS / Vol. 32, No. 6 / March 15, 2007

as illustrated in Fig. 2(b). Both pump diodes wereturned on simultaneously. A piece of 40 cm long ger-manate glass double-cladding single-mode fiber witha 42 �m core diameter is used in the dual-end pumpdemonstration. The output power curve of the fiberlaser is shown in Fig. 4. Because of the lack of anti-reflection coating on the pump coupling lenses, a fairamount of pump power and output laser power werelost as a result of the surface reflections. The trans-mission of the 1.9 �m lasers coupling lens was mea-sured as 78%. We compensated the laser power forthe transmission loss of the coupling lenses for bothpump power and output laser power in Fig. 4. Themaximum output power of the fiber laser is 104 W.To the best of out knowledge, this is the highest out-put power of a thulium-doped fiber laser pumpednear 800 nm. Because of the higher gain along the fi-

Fig. 3. (Color online) Laser output power versus launch-ing pump power. The slope efficiency is 68% with respect tothe launching power.

Fig. 4. (Color online) Dual-end pump laser result. The in-set shows the laser spectrum.

ber in the dual-end pump configuration, it has a

lower pump threshold than the one-end pump laser.The inset of Fig. 4 shows the spectrum of the fiber la-ser. The laser wavelength is 1.90 �m, which is100 nm longer than the emission peak in the bulksample. The slope efficiency of the output power ofthe fiber laser is 52.5% with respect to the launchingpump power, which can be significantly improved byoptimizing the fiber length and coupling optics. Arelative long fiber is used for the dual-end pump con-figuration to ensure that the power from one pumpcoupling into the other pump is sufficiently low toprevent laser-induced damage.

In summary, we have demonstrated a highly effi-cient 1.9 �m fiber laser by using our newly developedhighly thulium-doped germanate glass double-cladding single-mode fiber. The highest slope effi-ciency of the fiber laser reaches 68% with respect tothe launching power from a piece of 20 cm long fiberby using a one-end pump configuration. An output la-ser power of 104 W at 1.9 �m was achieved from apiece of 40 cm long dual-end pumped fiber, which isscalable with higher pump power. Our results indi-cate that a highly efficient high-power thulium fiberlaser near 2 �m is a promising laser source in theeye-safe wavelength range for a variety of applica-tions.

The authors acknowledge N. P. Barnes from NASALangley Research Center for technical discussion,and NASA and the Department of Defense for finan-cial support. J. Wu’s e-mail address [email protected]

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