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62 Annual Report 2017 Subject to alterations in specifications and other technical information. 08/2018. Fraunhofer Institute for Laser Technology ILT, www.ilt.fraunhofer.de DQS certified by DIN EN ISO 9001, Reg.-No.: DE-69572-01 1 Solid body made out of Al0.7CrCoFeNi with LMD. 2 Nanoscale microstructure of a specimen made with LMD (source: ACCESS e.V.). Task High-entropy alloys are a new alloy class that combines high heat resistance with good ductility. They are, therefore, parti- cularly suitable for components that have to withstand, both mechanically and thermally, substantial loads. For example, press hardening tools are subject to these stresses and also require the integration of complex channel structures to ef- fectively cool the tool. Within a collaborative research project, Fraunhofer ILT has developed a high-entropy alloy that can be processed using Selective Laser Melting (SLM), also known as laser-beam melting or Laser Powder Bed Fusion (LPBF). Method On the basis of the AlxCoCrFeNi alloy system, promising alloy compositions were first identified. The process used was laser material deposition (LMD), which, in contrast to SLM, enables a rapid screening of many alloy compositions with small amounts of powder mixtures. First, the aluminum content was adjusted to produce a bimodal microstructure representing the best possible compromise between high strength and sufficient ductility. Through further additives as well as adaptation of the process control, the thermal stability of the microstructure was improved by grain refining and increasing the strength. Results LMD was used with an Al0.7CoCrFeNi alloy and, through adaptation of the process control, extremely fine-grained microstructures were produced which reach a substantial hard- ness through alloying additives: up to 800 HV0.1. However, the microstructures produced still have a high crack sensitivity, which makes it necessary to use preheating in the process. Applications The process can be applied in additive manufacturing where, in particular, the highest demands are placed on design and material properties. In addition to tool making, applications can be found in turbomachinery and the aerospace sector. This project is being carried out for the state of North Rhine- Westphalia through the use of funds from the »ERDF Regional Operational Programme 2014-2020« under grant number EFRE-0800627. Contact Markus Benjamin Wilms M.Sc. Telephone +49 241 8906-567 [email protected] Dr. Andreas Weisheit Telephone +49 241 8906-403 [email protected] HIGH-ENTROPY MATERIALS FOR THE ADDITIVE MANUFACTURING OF MOLDING TOOLS 1 2

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Page 1: High-entropy materials for the additive …...MATERIALS FOR THE ADDITIVE MANUFACTURING OF MOLDING TOOLS 1 2 Title High-entropy materials for the additive manufacturing …

2

62 Annual Report 2017 Annual Report 2017 63

Sub

ject

to

alt

erat

ion

s in

sp

ecifi

cati

on

s an

d o

ther

tec

hn

ical

info

rmat

ion

. 08/

2018

.

Fraunhofer Institute for Laser Technology ILT, www.ilt.fraunhofer.de

DQS certified by DIN EN ISO 9001, Reg.-No.: DE-69572-01

Fraunhofer Institute for Laser Technology ILT, www.ilt.fraunhofer.de

DQS certified by DIN EN ISO 9001, Reg.-No.: DE-69572-01

Sub

ject

to

alt

erat

ion

s in

sp

ecifi

cati

on

s an

d o

ther

tec

hn

ical

info

rmat

ion

. 08/

2018

.

1 Solid body made out

of Al0.7CrCoFeNi with LMD.

2 Nanoscale microstructure of a specimen

made with LMD (source: ACCESS e.V.).

Task

High-entropy alloys are a new alloy class that combines high

heat resistance with good ductility. They are, therefore, parti-

cularly suitable for components that have to withstand, both

mechanically and thermally, substantial loads. For example,

press hardening tools are subject to these stresses and also

require the integration of complex channel structures to ef-

fectively cool the tool. Within a collaborative research project,

Fraunhofer ILT has developed a high-entropy alloy that can be

processed using Selective Laser Melting (SLM), also known as

laser-beam melting or Laser Powder Bed Fusion (LPBF).

Method

On the basis of the AlxCoCrFeNi alloy system, promising alloy

compositions were first identified. The process used was laser

material deposition (LMD), which, in contrast to SLM, enables

a rapid screening of many alloy compositions with small

amounts of powder mixtures. First, the aluminum content was

adjusted to produce a bimodal microstructure representing the

best possible compromise between high strength and sufficient

ductility. Through further additives as well as adaptation of the

process control, the thermal stability of the microstructure was

improved by grain refining and increasing the strength.

Results

LMD was used with an Al0.7CoCrFeNi alloy and, through

adaptation of the process control, extremely fine-grained

microstructures were produced which reach a substantial hard-

ness through alloying additives: up to 800 HV0.1. However,

the microstructures produced still have a high crack sensitivity,

which makes it necessary to use preheating in the process.

Applications

The process can be applied in additive manufacturing where,

in particular, the highest demands are placed on design and

material properties. In addition to tool making, applications

can be found in turbomachinery and the aerospace sector.

This project is being carried out for the state of North Rhine-

Westphalia through the use of funds from the »ERDF Regional

Operational Programme 2014-2020« under grant number

EFRE-0800627.

Contact

Markus Benjamin Wilms M.Sc.

Telephone +49 241 8906-567

[email protected]

Dr. Andreas Weisheit

Telephone +49 241 8906-403

[email protected]

HIGH-ENTROPY MATERIALS FOR THE ADDITIVE MANUFACTURING OF MOLDING TOOLS

1 2