GROUND WATER EVALUATION HASTINGS GROUNDWATER …

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GROUND WATER EVALUATION

HASTINGS GROUNDWATER CONTAMINATION SITE

HASTINGS, NEBRASKA

MAY 7, 1987

WORK ASSIGNMENT NO. 90-7LS2

DOCUMENT NO. 190-Ril-RT-CWVX-l

WOODWARD-CLYDE CONSULTANTS 5055 Antioch Road

Overland Park, Kansas 66203

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TABLE OF CONTENTS

Section

1.0 INTRODUCTION

1.1 PURPOSE OF INVESTIGATION

1.2 HISTORICAL INVESTIGATIONS

1.3 REVIEW OF SITE HISTORY

2.0 HYDROGEOLOGY

2 .1 GEOLOGY

2.1.1 Pleistocene Deposits 2.1.2 Cretaceous Deposits

2.2 HYDROGEOLOGY

2.2.1 Ground Water Flow 2.2.2 Recharge Sources 2.2.3 Ground Water Use

2.3 GROUND WATER QUALITY INVESTIGATIONS

2.3.1 Ground Water Monitoring Locations 2.3.2 Analytical Results

3.0 GROUND WATER CONTAMINATION

3.1 BACKGROUND WATER QUALITY

3.2 HASTINGS AREA

3.2.1 Contamination Problem Definition 3.2.2 Mechanisms of Transport 3.2.3 Suspected Source Areas

Page

1-1

1-1

1-1

1-2

2-1

2-1

2-1 2-2

2-2

2-2 2-4 2-5

2-6

2-7 2-7

3-1

3-3

3-4

3-4 3-8 3-9

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TABLE OF CONTENTS (continued)

Section

4. 0 CONCLUSIONS

4.1 SITE CHARACTERIZATION

4.2 EXTENT OF CONTAMINATION

4.1.2 Vo1ati1e Organic Compounds 4.2.2 Metals 4.2.3 Pesticides

5.0 RECOMMENDATIONS

5.1 GENERAL RECOMMENDATIONS

5.2 SPECIFIC RECOMMENDATIONS

6.0 REFERENCES

APPENDIX A

APPENDIX B

APPENDIX C

WELL LOGS FROM STATE OF NEBRASKA MONITORING WELLS

REM II GROUND WATER DATA

DECEMBER 1986 GROUND WATER DATA

4-1

4-1

4-1

4-2 4-2 4-3

5-1

5-1

5-2

6-1

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LIST OF FIGURES

Figure Number Tit1e

1-1 SITE LOCATION MAP

1-2 HASTINGS AREA EXISTING WELLS

2-1 GENERALIZED GEOLOGIC CROSS SECTION

2-2 POTENTIOMETRIC SURFACE

3-1 STIFF DIAGRAM NO. 1






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LIST OF TABLES

Table Number Title Page

2-1 GROUND WATER MEASUREMENTS - OBSERVATION WELLS 2-9

2-2 AQUIFER TRANSMISSIVITY OF SELECTED WELLS 2-10

2-3 MUNICIPAL WATER WITHDRAWALS FROM SELECTED WELLS (1982 to 1986) 2-lla

2-4 SUMMARY OF wee SAMPLING AT HASTINGS SITE 2-12

2-5 SUMMARY OF WELLS SAMPLED BY wee IN MAY 1985 2-13

2-6 SUMMARY OF WELLS SAMPLED BY wee IN SEPTEMBER 1985 2-14

2-7 SUMMARY OF WELLS SAMPLED BY wee IN DECEMBER 1985 2-15

2-8 SUMMARY OF WELLS SAMPLED BY wee IN MARCH 1986 2-16

2-9 SUMMARY OF WELLS SAMPLED BY wee IN JUNE 1986 2-17

2-10 SUMMARY OF WELLS SAMPLED BY wee IN SEPTEMBER 1986 2-18

2-11 WELLS LOCATED IN HASTINGS AREA 2-19

2~12 DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - MAY 1985 2-20a

2-13 DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - SEPTEMBER 1985 2-21

2-14 DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - DECEMBER 1985 2-22a

2-15 DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - MARCH 1986 2-23a

2-16 DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - JUNE 1986 2-24

2-17 DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - SEPTEMBER 1986 2-25

2-18 DETECTED PESTICIDES IN GROUND WATER SAMPLES - SEPTEMBER 1985 2-26

2-19 DETECTED DISSOLVED METALS IN GROUND WATER SAMPLES - MARCH 1986 2-27a

2-20 DETECTED TOTAL METALS IN GROUND WATER SAMPLES - MARCH 1986 2-28a

PROJ3094 L

LIST OF TABLES (continued)

Table Number Title Page

2-21 DETECTED SPECIAL PARAMETERS IN GROUND WATER SAMPLES - SEPTEMBER 1986 2-29a

2-22 DETECTED SPECIAL PARAMETERS IN GROUND WATER SAMPLES - DECEMBER 1985 2-30

2-23 DETECTED SPECIAL PARAMETERS IN GROUND WATER SAMPLES - MARCH 1986 2-31

2-24 DETECTED EDB IN GROUND WATER SAMPLES - MARCH 1986 2-32

2-25 DETECTED EOB IN GROUND WATER SAMPLES - JUNE 1986 2-33

2-26 DETECTED EDS IN GROUND WATER SAMPLES - SEPTEMBER 1986 2-34

2-27 TOTAL DISSOLVED SOLIDS IN GROUND WATER SAMPLES 2-35

2-28 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - OBSERVATION WELL OW-Is 2-36

2-29 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - OBSERVATION WELL OW-ld 2-37

2-30 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - OBSERVATION WELL OW-2S 2-38

2-31 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - OBSERVATION WELL OW-2d 2-39







PROJ3095

LIST OF TABLES (continued)

Tab1e Number Title Page

2-38 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - MUNICIPAL WELL M-3 2-46





2-43 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - MUNICIPAL WELL CMS-24 2-51

2-44 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - DOMESTIC WELL 0-8 2-52

2-45 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - IRRIGATION WELL I-46- 2-53

2-46 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS - IRRIGATION WELL I-49 2-54

3-1 CHEMICAL PROPERTIES OF CONTAMINANTS IDENTIFIED IN WELLS 3-12

3-2 PHYSICAL CHARACTERISTICS OF WELLS 3-13a

PROJ3096

1.0 INTRODUCTION

Section: 1.0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 1-1

This report presents an interpretation of ground water quality data and related information obtained from an investigation of wells in the vicinity of Hastings, Nebraska. The Hastings Ground Water Contamination Site encompasses an area within and east of the City of Hastings, Adams County, Nebraska. The City is located south of Interstate Highway I-80 in south central Nebraska. Principal access routes to the City of Hastings are U.S. Highways 6 and 281 (Figure 1-1), and two principal railroad lines.

Work was performed by Woodward-Clyde Consultants (WCC) as the lead team member under the REM II contract, which is part of the remedial program established by the United States Environmental Protection Agency (USEPA) under the Comprehensive Environmental Response, Compensation and Liability Act (CERCLA). Work was administered through the USEPA Region VII office in Kansas City, Kansas.

1.1 PURPOSE OF INVESTIGATION

Investigations in the Hastings area were initiated in early 1985 as a result of the detection of volatile organic contaminants in 1983 by the State of Nebraska in the potable water obtained from four Hastings municipal water supply wells and in private municipal water supply wells at Community Municipal Services, Inc. (CMS). The purpose of the investigation was to attempt to identify contaminant sources and quantify levels of contamination in the Hastings area. This report summarizes the results of this investigation.

1.2 HISTORICAL INVESTIGATIONS

The initial site evaluation studies performed to date include: quarterly sampling of existing municipal, industrial, domestic, irrigation, and State of Nebraska monitoring wells; and soil-gas contaminant analyses and soil

PROJ3097

Section: 1.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 1-2

sampling in the City. The evaluation presented herein is based on the ground water surveys, historical information of the area, and published results of investigations of the geology and ground water resources of the region. Soil gas contaminant analyses and soil sampling results are not discussed here.

1.3 REVIEW OF SITE HISTORY

The City of Hastings has a central industrial area (Figure 1-2) that has been in use since the late 1800's. A number of businesses operated in the area at various times since the early 1900's. These included a coal gas manufacturing plant, grain elevator, railroad yard, manufacturing facilities, and junkyards. The extent to which these businesses utilized volatile organic compounds (VOCs) in their activities is not known. Two firms are known to have used TCE and TCA in their vapor degreasing processes.

The City operated two landfills that are now closed. The North landfill, located near the eastern Hastings' city limits, is on the site of an old clay pit which was used as a source for a brickyard. Most of the fine grained sediments were removed during the brickyard's operating life forming a deep pit. The depth of the fill at the site was estimated by an electrical resistivity survey to be between 40 and 50 feet. Companies have reported sending industrial wastes to the North Landfill during the 1950's and 1960's.

The South Landfill, also located near the eastern Hastings' city limits and south of U.S. Highway 6, also is on the site of an old clay pit that was previously used as a commercial source for clay. It.was operated as a landfill subsequent to the use of the North _Landfill. Companies have also reported sending industrial wastes to the South Landfill(l970's).

Data collected by the State of Nebraska in 1983 included CMS well 20 and CMS well 24 located at the Hastings East Industrial Park. This area, the

PROJ3098


former U.S. Naval Ammunitions Depot (NAO), is located approximately two miles east of the City of Hastings. Data obtained from sampling of CMS wells and Hastings public water supply wells were utilized for the purpose of scoring the site according to the Hazard Ranking System (HRS). As a result of the HRS scoring, the Hastings Groundwater Contamination Site was proposed for the National Priorities List (NPL) in October 1984. The site went final in May 1986.

Areas serviced by the CMS system are included within the boundaries of the Hastings Site; however, areas previously used for production by the former NAO are not within the scope of this report.

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2.0 HYDROGEOLOGY


Several previous hydrogeologic and geologic investigations have been perfonned in the Hastings study area. Surficial and subsurface geologic and hydrologic investigations in the vicinity of the Hastings Ground Water Contamination Site have been conducted and reported by the State of Nebraska Conservation and Survey Division (1953), USGS (1959), Keech and Dreeszen (1968), and Ragon (1974). Information presented in this report is based on the previous investigations and on-site studies.

2.1 GEOLOGY

Domestic, private, public, and irrigation wells on-site for which data exist are shown in Figure 1-2. Boring logs of the municipal wells and observation wells (Fischer and Spalding, 1985) are illustrated graphically in generalized geologic cross Section A-A' (see Figure 2-1) depicting unconsolidated deposits across the site area in an east-west direction. The location of Section A-A' is shown on Figure 1-2. The Pleistocene and Cretaceous deposits are the primary deposits of interest in the site area and are discussed in the following sections.

2. 1.1 PLEISTOCENE DEPOSITS

Deposits of the Pleistocene Epoch make up the majority of the unconsolidated deposits in the area. Peorian and younger loesses and loessial soils mantle the upland surface to a depth of approximately 50 feet throughout much of Adams and Clay Counties except on the steepest slopes and along major stream valleys. The loess consists of fine- to coarse-textured silt and clayey silt with the upper portion being light brown to light brownish-gray in color while the middle to lower portion is light gray to light yellowish-gray (Keech and Dreeszen, 1959).

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The loess is underlain by the medium-grained deposits of the Sappa Formation considered by Condra, Reed, and Gordon (1950) to be of the Yarmouth Interglacial Age or of the late Kansan Glacial Age. The Sappa Formation consists of an upper sandy clay unit and a lower sand unit with a combined thickness of up to 50 feet.

The Sappa Formation is underlain by a Pleistocene sand and gravel, which is a relatively thick (up to 100 feet) unit of coarse-textured sand and gravel with continuous and discontinuous layers or lenses of fine grained silts and clays deposited during the retreat and waning of the Kansan ice sheet up through early Yarmouthian time.

2. 1.2 CRETACEOUS DEPOSITS

The Niobrara Formation of the Cretaceous Period is a gray to black marine shale which frequently contains chalky zones and underlies the unconsolidated deposits in the site area as the uppermost bedrock unit. The upper Niobrara consists of weathered shale and gray silty clay.

2.2 HYDROGEOLOGY

The sand and gravel deposits form a prolific aquifer beneath the Hastings area. The sands and gravels have a saturated thickness of approximately 70 feet, so large quantities of ground water are readily available. The following sections describe the ground water flow and pertinent hydrogeologic features of the saturated zones as well as the ground water recharge sources within the investigated area.

2.2.1 GROUND WATER FLOW

A potentiometric surface map for the Hastings area is presented in Figure 2-2. The potentiometric surface slopes toward the east-southeast (see

PROJ3103


Figure 2-2) with a gradient of approximately 12 feet per mile

(0.002 ft/ft).

The well logs in Appendix A and Figure 2-1 indicate that the aquifer consists primarily of coarse-grained deposits; however, some zones of fine-grained materials including clay, silty clay, silt, and sandy silt are also present. The fine grained materials range in thickness from thin lenses to layers up to ten feet thick. Ground water is typically encountered at a depth of approximately 120 feet below the surface.

Five observation well clusters, designated OW-1 through OW-5, were installed by the State of Nebraska to evaluate the lateral and vertical distribution of contamination in the aquifer. Each well cluster consists of one well above and one well below one or more layers of the fine-grained materials. Water level records for the "OW" observation wells are presented in Table 2-1. The water levels in the shallow wells, designated "s", are indicative of the potentiometric head at the unsaturated/saturated interface (i.e., water table). The water levels in the deep wells, designated "d", reflect the potentiometric head beneath a fine-grained soil layer. The water level measurements presented in Table 2-1 indicate that the aquifer within the vicinity of cluster wells OW-1, OW-2, OW-3, and OW-5 possess a higher hydrostatic head at the deep monitored portion than the shallow monitored portion of the aquifer. On the other hand, water level measurements recorded in OW-4 indicate a higher head in the shallow portion compared to the deeper portion of the aquifer. These observed trends are continuous through the year though the magnitude in the head differences within the well clusters fluctuates. The presence of the fine grained materials between the shallow and deep screened levels in the cluster wells OW-1, OW-2, OW-3, and OW-5 may cause the observed upward water level gradients. These fine grained materials possess low permeability and may effectively create a semi-confined aquifer condition between the monitored levels. This hypothesis is further strengthened since a slight downward flow gradient exists at the vicinity of well OW-4 where the fine grained

PROJ3104


materials do not exist between the shallow and deep screened level. It is likely that the fine grained materials are areally discontinuous since they were not present in the OW-4 well cluster vicinity.

The water from both the shallow and the deep levels is characterized as calcium bicarbonate facies, but the samples from the shallow 'OW' wells have usually shown higher levels of dissolved solids than the deeper 'OW' wells. However, dissolved solids data does not indicate the presence of two separate aquifers.

The potentiometric surface map (see Figure 2-2) depicts flow to be from the west to the east-southeast. The municipal wells extraction lower the ground water surface in the vicinity of the wells while the pumps are operating. The cones of depression in the potentiometric surface map due to municipal well pumpage are shown in Figure 2-2. Within the radial influence of the well, which is dependent upon pumping and aquifer parameters, the direction of ground water movement can be changed drama ti ca lly.

The State of Nebraska maintains records of aquifer tests performed within the state. Aquifer test data from selected wells within the area of interest are presented in Table 2-2. The transmissivity of the aquifer ranges from 90,000 gallons per day per foot (gpd/ft) to 225,000 gpd/ft for wells M-17 and M-13, respectively. The hydraulic conductivity for the aquifer ranged from 989 gallons per day per square foot (gpd/ft2) to 2184 gpd/ft2 for wells M-17 and M-13, respectively. These values are typical of sand and gravel aquifers.

2.2.2 RECHARGE SOURCES

Recharge of ground water occurs from infiltration of precipitation, seepage from streams, and inflow from irrigation. The fine-grained loessial sediments that comprise the surficial 50 feet of subsurface deposits impede the

PROJ3105


downward flow of precipitation and irrigation runoff to the aquifer. The U.S. Weather Service at Hastings records an annual precipitation of 25 inches although precipitation varies considerably from year to year.

Recharge of ground water from precipitation was estimated for an area of

western Clay County by Keech and Dreeszen (1959) from analysis of the potentiometric head in the aquifer. They estimated an average annual

recharge over the area of 1.6 inches.

Recharge of the aquifer from streams and lakes occurs in the Hastings area. The West Fork of the Big Blue River, Pawnee Creek, and Lake Hastings are the principal sources of recharge. No estimate of the quantity of recharge

has been made.

Irrigation in the Hastings area utilizes pumpage from the aquifer. Some irrigation water returns to the aquifer as seepage. Keech and Dreeszen (1959) reported a maximum return of 10% of the pumped water. Improved methods of irrigation have resulted in substantially less recharge from seepage.

2.2.3 GROUND WATER USE

During a study of ground water use between 1950 and 1982, it was concluded that the use of ground water exceeded replenishment by recharge in the Hastings area during that period. Water levels had declined more than 20 feet since water levels were first recorded in the 1930 1 s (Keech and Dreeszen, 1968).

Ground water withdrawals from selected Hastings municipal wells, as furnished by the City of Hastings, are presented in Table 2-3. This high quality water (low dissolved solids) is pumped directly into the Hastings municipal water system without treatment. Total water use by industries and irrigators in the area has not been determined. Significant withdrawals are made in the Hastings area for industrial and irrigation purposes.

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2.3 GROUND WATER QUALITY INVESTIGATIONS

Section: 2.0 Site: Hastings Revision: O Date: 05/07/87 Page: 2-6

The wells in the Hastings area were sampled in March and April of 1983 by the Nebraska Department of Health and in June and August of 1983 by the Nebraska Department of Environmental Control. The Community Municipal Services (CMS) water supply well 24 and several irrigation wells were sampled during this initial monitoring. Limited data are also available from state sampling in 1984 and 1985. Area municipal and private wells were also sampled in April 1985 by the Field Investigation Team (FIT) contracted to the USEPA.

The REM II Team has sampled wells in the Hastings area on a quarterly schedule during 1985 and 1986. The first sampling event by REM II in May 1985 was limited to the 10 observation wells installed by the State of Nebraska. A total of 42 and 29 wells were sampled in September 1985 and December 1985, respectively. The fourth sampling event included 25 wells that were sampled in March 1986. The quarterly sampling continued with the June/July 1986 sampling of 22 wells and the September 1986 sampling at 25 locations.

In addition to the above, ground water sampling was conducted by USEPA and NOOH in June 1985. Samples were collected at a total of 7 sampling points. Selected results of interest for VOC compounds observed in these samples include:

PROJ3107

JUNE 1985 ( ug/1)

- D-8 M-12

TCE 330 0.7 TCA O.f 0.4 CC1 4 1.6 NO

PCE 6.3 NO EDB 0.04 NO

All data reported above was obtained by USEPA.

2.3.l GROUND WATER MONITORING LOCATIONS


CMS-24

6.0 0.5 22 ND

0.32

The ground water monitoring locations included in this report include 10 municipal wells, 1 Community Municipal Services (CMS) well, 8 irrigation wells, 10 State of Nebraska observation wells, 5 industrial supply wells, and 4 domestic supply wells. Various existing wells were used as sampling points during each sampling event. Other than the state observation wells, these existing wells have limitations to their use as monitoring wells due to their construction (depth, screened interval, etc.). Table 2-4 indicates which wells were sampled during each REM II sampling event. Tables 2-5 through 2-10 summarize wells samples by REM II and the analyses requested for each sampling event. Table 2-11 summarizes the types of wells located within the study area. Data obtained from additional wells installed by REM II in 1986 are not included in these tables.

2.3.2 ANALYTICAL RESULTS

Summaries of the detected volatile organic compounds by sampling event are presented in Tables 2-12 through 2-17. Table 2-18 presents the results of the pesticide analyses performed during the September 1985 sampling event. Summaries of the March 1986 detected metals analyses are shown in Tables

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2-19 (disso1ved) and 2-20 (total). Tab1es 2-21, 2-22 and 2-23 present the results of the selected genera1 water quality parameters for September 1985, December 1985, and March 1986, respectively.

Certain ground water samples were analyzed for EDB in September 1985 and in March, June, and September 1986. Tables 2-24, 2-25, and 2-26 show the results of the 1,2 Oibromoethane (EDS) scans for March, June, and September 1986, respectively. The concentration of total dissolved solids (TDS) for selected wells is shown in Table 2-27.

Tables 2-28 through 2-46 present summaries of detected volatile organic compounds for the wells sampled at the Hastings Groundwater Contamination Site.

Analytical results from the REM II (June/July, September and December 1986) sampling of the USEPA monitoring wells have been included in the reports prepared for the three subsites of the Hastings Groundwater Contamination Site.

Chemical analytical results for the REM II water sampling events are presented in Appendix B.

Data generated by the December 1986 REM II sampling event is included in Appendix C, however, it is not tabulated or discussed in this report.

PROJ3109

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3.0 GROUND WATER CONTAMINATION

Section: 3.0 Site: Hastings Revis ion: 0 Date: 05/07/87 Page: 3-1

Contaminants have been identified in the ground water which occurs in the aquifer beneath the Hastings area. Volatile organic compounds (VOCs) are the predominant contaminants of concern; however, some heavy metals have been detected in concentrations which exceed water quality criteria. Many of these volatile organic compounds may present a significant health risk

if not removed prior to consumption of the ground water. Twelve different V0Cs of concern have been identified. The analytical data showing concentrations of all chemicals analyzed are included in Appendix B.

Evaluation of ground water chemical concentration data is dependent upon a clear understanding of:

o The hydrogeology of the site (i.e., hydraulic conductivity, storativity, effective porosity, and aquifer thickness);

o The chemical properties of the constituent (i.e., solubility, density, vapor pressure);

o The physical characteristics of the well from which the sample was obtained (i.e., casing material, screened interval, and casing diameter); and

o The manner in which the sample was collected (i.e., sampling protocol, method of preservation, quality control, and quality assurance).

The site hydrogeology can be effectively used to understand the chemical concentration data. Hydrogeologic properties (hydraulic conductivity, storativity, and effective porosity) together with natural flow gradients or induced flow gradients (pumping wells) may result in contaminant pathway identification, travel time estimates, and source location identification.

The chemical properties of importance to the migration of V0Cs are presented in Table 3-1. The chemical properties included are solubility, density, vapor pressure, and octanol/water partition coefficient.

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The physical characteristics of the wells are presented in Table 3-2. The physical characteristics included are well casing materials, screen lengths, and casing diameters. The well construction (i.e., depth, screened interval) and use (i.e., observation, domestic, industrial, and municipal) impacts the representativeness of the samples since the wells may not be screened at the specific depth that contaminants are present and the volume of water pumped from other levels may be diluting the contaminated interval.

The State of Nebraska observation wells have a 4-inch diameter and screen lengths of 10 (deep) and 20 (shallow) feet. These characteristics make the samples collected discrete (i.e., the vertical locations from which the samples were taken are fairly well defined). Domestic wells generally have a 5- or 6-inch casing diameter and are typically screened to a depth of 150 feet. The uncertainty of the length and depth of the well screen lessens

the value of water samples collected because water quality data cannot be attributed to a certain vertical position in the aquifer.

Irrigation, industrial, and municipal wells are constructed with similar designs in that they are generally screened across long intervals (up to 70 feet or more) in order to achieve high flow rates. Thus, they do not give a discrete interval sample as is the case with monitoring wells. These wells also generally have large diameters (12 to 36 inches). These large wells obtain water from a large vertical section of the aquifer and, therefore, the detected contamination could occur within any portion of the screened length. As a result, the actual concentrations and ,locations of the contaminants are very difficult to discern due to the dilution effect relating to the long screened interval.

The extent of use of a well has an effect on the consistency of the quality of water obtained from it. This is an important distinction that is made between wells that are used for different purposes, i.e., wells that are used regularly versus those that are used periodically. For example,

PROJ3113


irrigation wells only operate during the spring and summer, whereas, municipal and industrial wells normally operate year around. The result is that irrigation wells have a large area from which they capture water during the summer because of heavy use. The difference in area is reflected in the discreteness and representatives of the sample collected. Thus, the potential for significant variations in data may occur.

3.1 BACKGROUND WATER QUALITY

Ground water quality is influenced by the quality of precipitation and surface water that recharges the aquifer. Precipitation generally has a low total dissolved solids content (less than 20 mg/1). Surface water quality of base flow and overland flow in the Little Blue River Basin was reported by Mundorff and Waddell (1966) as being good with low concentrations of dissolved solids (273 mg/1, baseflow; and 73 mg/1, overland fl ow).

Ground water in the Hastings area is classified as a calcium bicarbonatetype water having moderately low concentrations of dissolved solids (215 to 462 mg/1). Ground and surface waters found elsewhere in the Great Plains may have concentrations of total dissolved solids exceeding 1,000 mg/1.

Mundorff and Waddell (1966) reported that water from the Cretaceous bedrock is probably calcium sulfate type and has a total dissolved solid content greater than 700 mg/1. This value is considerably higher than the mean total dissolved solid content of 308 mg/1 that was calculated from Table 2-27. The relatively high total dissolved solid content in ground water found in the bedrock and the apparent difference in ground water type between bedrock and alluvial aquifer indicate that ground water in the aquifer of concern probably does not originate from the Cretaceous bedrock. The observed value, however, was for ground water near the surface that has probably been buffered by recharge sources (i.e., precipitation, surface water) to lower the dissolved solids content.

l PROJ3114

3.2 HASTINGS AREA


The area covered by this report (Hastings Ground Water Contamination Site) includes contamination identified in the City of Hastings and contamination identified on property lying to the east of Hastings extending to the vicinity of the Central Community College campus. Contaminants have been detected in Hastings municipal wells, irrigation and domestic wells, private municipal wells (operated by Community and Municipal Services), and State of Nebraska observation wells. Volatile organic contaminants were detected in 1983 in wells M-3, M-10, M-12, M-18, and CMS-24. Municipal well M-18 showed the highest concentration of VOCs (greater than 2000 ug/1 of trichloroethene) and was thus completely decommissioned. In December 1985 municipal well M-3 was removed from service due to continued detection of carbon tetrachloride. In addition, other wells taken out of service and placed on emergency standby include M-10, M-12, CMS-20 and CMS-24.

3.2.1 CONTAMINATION PROBLEM DEFINITION

The ground water that has been sampled to date in the Hastings area has exhibited evidence of voe contamination. Isolated cases of detection of pesticides, semi-volatile organic compounds, heavy metals, and nitrates have also occurred. A discussion of the extent of contamination by each of these parameters follows.

Volatile Organic Compounds

Several volatile organic compounds (VOCs) have been detected at varying concentrations in the ground water samples obtained from the Hastings area. Of these detected VOCs, the following compounds are of concern due to their observed levels of concentration and their hazardous nature: Trichloroethene (TCE); Carbon Tetrachloride (CC1 4); 1,1-Dichloroethene; Tetrachloroethene (PCE); Benzene; Toluene; and 1,2-Dibromoethane (EDB), Trans-1,2 Dichloroethene; 1,1,1-Trichloroethane (TCA); 1,1,2-Trichloroethane;

PROJ3115 - - .......... -· fl.


1,1,2,2-Tetrachloroethene; and Chloroform. Tables 2-28 through 2-46 present a summary of the detected voes at the site. A brief discussion of the primary contaminants of concern follows.

Trichloroethene (TCE) has been detected at the greatest concentrations over a large areal extent and is considered the primary contaminant of concern. TCE has been detected in observation well OW-4s at concentrations up to 3500 ug/1, which is 1250 times the 10-6 Health Risk Criteria of 2.8 ug/1. The proposed maximum contaminant limit (MCL) for TCE is 5 ug/1. MCLs are defined as enforceable standards and are set as close to the maximum contaminant level goal (MCLG) as is feasible. MCLGs for potential carcinogens are set at zero. The term "feasible" applies to the use of the best technology available to reduce contaminant levels taking cost into consideration. Six wells (OW-4s, OW-4d, OW-5s, D-8, I-46, M-18) have shown detected TCE concentrations of over 100 ug/1.

The observation wells show a vertical variation in the TCE concentrations. A vertical distribution is expected because the density of TCE is greater than water. The measured concentration of TCE from water samples is below the reported solubility of llOO mg/1 (see Table 3-1), however, the potential exists for nonaqueous phase TCE to be present at points in the aquifer. The source concentration of TCE is likely to be very high to produce concentrations in ground water samples of 1000 ug/1. Therefore, the TCE may migrate through the ground water to the bottom of the aquifer due to the density differential.

The concentration of TCE has varied in most of the wells from samples acquired on different dates. For example, TCE was detected in well OW-4s at a concentration of 110.0 ug/1 in December 1985, at 3500 ug/1 in March 1986, and at a concentration of 8.0 ug/1 in June 1986. It is possible that variations in the concentration of TCE reflect the potential migration of contaminants in response to changes in the magnitude and direction of ve1ocity of the ground water. It is also theorized that the source of TCE

PROJ3116

) .,


provides s1ugs of highly concentrated TCE in water as it enters the aquifer at the interface of the unsaturated and saturated zones.

Carbon tetrachloride (CC1 4) was detected in eight wells (OW-3d, OW-4s, M-18, CMS-24, I-46, I-49, 0-8, and M-3) in the Hastings area. Of these eight wells, M-3 has the highest reported concentration of 46.4 ug/1, which is over 110 times the 10-6 Health Risk Criteria of 0.42 ug/1 and which is above the proposed MCL for cc1 4 of 5 ug/1. cc1 4 was detected in well M-3 from all samples obtained. CC1 4 was also detected once in well M-18 in May 1983. The presence of CC1 4 in OW-3d may be the result of the density differential between cc1 4 and water.

Tetrachloroethene was detected in eight wells (OW-ls, OW-ld, OW-4s, OW-4d, OW-Ss, 0-8, I-46, I-49) but at relatively low concentrations. Tetrachloroethene was detected at concentrations from 1.8 ug/1 to 42.0 ug/1. The 42.0 ug/1 concentration is 45 times the 10-6 Health Risk Criteria of 0.88 ug/1. Tetrachloroethene was also detected in well M-18 in April and May 1983 at concentrations of 60.4 ug/1 and 53.0 ug/1, respectively. As with TCE and CCT 4 , the presence of the PCE in the deep wells (OW-ld, OW-4d) may be due to the density differential.

Samples obtained from eight wells were analyzed for 1,2-Dibromoethane (EDB). EDB was d~tected in samples obtained from three of the wells including CMS-24, 0-8, and I-49. The highest concentration observed was 6.8 ug/1 (well I-49).

1,1,-Dichloroethene was detected once in well I-49 at a concentration of 5.00 ug/1. Benzene was detected twice in well OW-4d at a maximum concentration of 48.0 ug/1 in May 1985, and lower concentrations of 6.0 ug/1 in

September 1985, and 6.0 ug/1 in December 1985. Benzene was not detected in the March 1986 sampling. The presence of benzene in a deep well even though its density is less than water may be the result of vertical gradients induced by heavy pumping.

PR013117

Semi-Volatile Organic Compounds


The only detected semi-volatile organic compound was Bis(2-ethy1hexy1) phthalate at wells OW-4d, OW-5s, and OW-5d during the September 1985 sampling at concentrations of 12.0, 8.0, and 9.0 ug/1, respectively. These results have not been duplicated by subsequent sampling and may be due to the low concentrations detected. Therefore, it is possible that these results are not representative of the true ground water quality in the area.

Pesticides

The only pesticide detected at the Hastings site was Aldrin. In September 1985 Aldrin was detected in a sample obtained from OW-3s at a concentration of 0.17 ug/1. A duplicate sample from well OW-5s exhibited an Aldrin concentration of 0.13 ug/1, however, the initial sample obtained from this well was nondetectable for Aldrin at a detection limit of 0.05 ug/1.

Pesticide analyses were also performed on these wells in May 1985 and June 1986. Aldrin was not detected in either of these wells during these sampling events.

Although the concentrations of Aldrin reported in September 1985 exceeds the Ambient Water Quality Criteria for a 10-6 cancer risk level of 0.074 ug/1, because the presence of Aldrin was not confirmed by subsequent sampling events Aldrin is not considered a contaminant of concern for the Hastings Ground Water Contamination Site.

Metals

Several of the wells in the Hastings area showed the presence of metals. Metals found in concentrations above National Interim Primary Drinking Water Regulation (NIPDWR) and Secondary Drinking Water Regulations included lead, cadmium, and iron. Detected metals (total and dissolved) for the March 1986 sampling event are presented in tables 2-19 and 2-20.

PROJ3118


Total iron was detected in wells OW-ls, OW-Id, OW-2d, OW-4s, and OW-5s at concentrations of 600, 320, 410, 1200, and 1600 ug/1, respectively, which are all above the secondary criteria of 300 ug/1 1.

Concentrations of total lead and total cadmium were detected in industrial well IN-10 at concentrations of 360 and 53 ug/1, which were above the NIPOWR criteria of 50 and IO ug/1, respectively. However, concentrations of lead and cadmium observed in well IN-IO may be a result of the degradation of well materials. No records detailing well construction are available, therefore, metals data generated from this well is inconclusive.

Special Parameters

Selected general ground water quality parameters (special parameters) analyzed for during the sampling events included total alkalinity, chloride sulfate, and nitrate. Elevated levels of ground water quality parameters {sulfate and nitrate) were observed. State of Nebraska observation well OW-5s showed a concentration of sulfate of 290 mg/1 which was slightly higher than the secondary criteria of 250 mg/1. Elevated levels of nitrate (above the drinking water standard of 10 mg/1 as nitrogen) were reported in OW-2s, OW-5s, I-3, I-23, and 0-7. A maximum concentration of 22.0 mg/1 was observed in well I-23. Total alkalinity ranged from 148 to 457 ug/1.

Infonnation on selected general ground water quality parameters in the vicinity of Hastings is summarized in Tables 2-21 through 2-23. Figures 3-1 through 3-6 are Stiff diagrams that graphically show the balance of

1 These regulations (secondary) control contaminants in drinking water that primarily affect the aesthetic qualities relating to the public acceptance of drinking water. At considerably higher concentrations of these contaminants, health implications may also exist as well as aesthetic degradation. The regulations are not federally enforceable but are intended as guidelines for the states (40 CFR Part 143).

PROJ3119

Section: 3.0 Site: Hastings Revision: O Date: 05/07/87 Page: 3-9

ionic constituents. The Stiff diagrams show that calcium (Ca+2) and

bicarbonate (Hco3- 1) are the major ions occurring in the ground water in the Hastings area. Concentrations of sodium (Na-1), magnesium (Mg+2),

chloride (Cl-1), and sulfate (so-2) ions are found in lesser amounts and are relatively consistent in concentration throughout the area.

Total Dissolved Solids

Table 2-27 presents concentration data of total dissolved solids from samp1es taken in the Hastings area in 1985 and 1986. These data show that the shallow ground water has a higher dissolved solids content than the deeper water. Leaching of soluble salts in the unsaturated zone appears to have resulted in the transport of dissolved solids to the saturated zone.

3.2.2 MECHANISMS OF TRANSPORT

Generally, the VOCs identified at Hastings have moderately low solubilities (within the range of 150 to 1800 mg/1 which is less than 1%). Thus, the organic liquids released to the subsurface may migrate as nonaqueous phases. Some components may dissolve into the ground water as the organic liquid migrates. Some of the VOCs identified have densities greater than water (from 1.2 to 2.6 gm/cm3) and some have densities lower than water

(from 0.86 to 0.88 gm/cm3). Because a density difference of one percent or greater usually results in stratification, the identified compounds will either float or sink in the aquifer.

Transport by advection (i.e., movement with the bulk velocity of ground water) occurs from west to east based on the potentiometric surface map for June 1985; however, insufficient information is available to accurately describe the path traced by contaminants to define the localized areas of contamination. Difficulty arises in accurate determination of solute transport because of the variability in the potentiometric surface, distances traveled, variations in aquifer transmissivity and the lack of

PROJ3120


monitoring wells in the study area. As previously noted, the variability in the potentiometric surface may be attributed to ground water withdrawals by wells for various purposes within the study area.

Dispersion is the molecular diffusion and mechanical mixing of dissolved contaminants which cause them to spread as they move with the ground water. Dispersion is characterized in both the longitudinal and transverse directions. The extent of dispersion of VOCs in ground water in the Hastings area is not known.

3.2.3 SUSPECTED SOURCE AREAS

A number of potential sources for the detected volatile contaminants is suspected from a review of historical activities and analysis of aerial photography. Insufficient information is available to locate the exact sources, however, enough information is available to show that multiple source areas exists and, in certain cases, identify their relative locations.

Trichloroethene (TCE) has been detected at several locations with a range in concentration from trace levels to moderately high amounts. Major concentrations and trends are identified; however, no attempt is made to explain the presence of TCE in all of the wells in which it was observed. A minimum of two major sources of TCE can be inferred from chemical concentration data.

Detection of TCE in observations wells OW-5 and OW-4 indicative of at least one source of TCE contamination. TCE was detected in observation well OW-5s (shallow) at a maximum concentration of 1900 ug/1 in May 1985. Subsequent measurements of 1400 ug/1, 740 ug/1, 1100 ug/1, and 1100 ug/1 occurred in September and December, 1985, and March and June 1986, respectively. The maximum concentration found in OW-5d (deep) was 51 ug/1 in May 1985. The well logs for the deep wells in the area and the measured water

} pROJ312l


levels in OW-5 indicate that the deeper portion of the aquifer in this area is separated from the upper screened portion via low permeability fine grained materials. This fact is supported from the contaminant concentration gradients within the aquifer. TCE identified at OW-4d indicates that contaminants have migrated to the deeper portion of the aquifer. Water level measurements at OW-4 indicate that there is a slight downward flow gradient between the shallow and deep screened areas. Measured TCE

concentrations support this fact because concentrations steadily increased from 106 ug/1 in October 1984 to 1800 ug/1 in March 1986. A detected concentration of 20 ug/1 was measured in June 1986.

These results indicate that a major source area for TCE may be in the vicinity of OW-5. Concentrations of TCE decrease with distance both upgradient (west), as documented by ground water samples from M-10, and downgradient (east) of the source (indicate which wells show lower concen

trations), OW-4s and OW-4d.

Contamination at municipal well M-18 was observed in samples taken in April and May 1983. Since that time, the well has been decorrmissioned and contamination by TCE has been substantially reduced; CC1 4 , benzene, 1,1-DCA, 1,1-0CE, Trans-1,2-0CE, 1,1,1-TCA, 1,1,2-TCA, and PCE have not been detected. This suggests that contamination by TCE at well M-18 is caused from pumpage either by withdrawing contaminated water that is horizontally proximate to the well, or by withdrawing contaminated water that is vertically proximate to the well and occurs in the aquifer below the screened portion.

The contaminants in M-18 appear to be corning from the source in the vicinity of OW-5. M-18 lies along the ground water flow path of water migrating from the OW-5 area.

Wells CMS-24, I-49, and 0-8 have also shown contamination by trichloroethene (TCE) at various times since April 1985. levels in 0-8 ranged from 182 ug/1 to 1200 ug/1 in September 1986 and March 1986, respectively.

PROJ3122


In September 1986, two (2) CMS System samples were obtained. CMS System sample No. 1 was obtained on September 2, 1986 and contained 4.5 ug/1 of TCE and 17 ug/1 of CC1 4. CMS system sample No. 2 was obtained on September 10, 1986 and was nondetectable for both CC1 4 and TCE at detection limits of

1.2 and 0.8 ug/1, respectively. These samples were also analyzed for EDS and both showed nondetectable levels.

The history of detection of contaminants at these three wells indicates the presence of an upgradient source. Well D-8 is located approximately 3000 feet downgradient from the old North Landfill which was reported as

having received industrial wastes during the 1950's and 1960's. Therefore, the North Landfill may be the second major source of TCE contamination.

Community well CMS-24 and irrigation well I-49 have also shown contamination by CC1 4 and EDB (1,2-Dibromoethane). These wells lie on approximately

the same flow path according to the June 1985 potentiometric surface (Figure 2-2) and are downgradient from the Far-Mar-Co grain storage facility. Both EDS and CC1 4 were used in the past as grain· fumigants which suggests that the Far-Mar-Co facility may be a potential source area.

A source of CC1 4 contamination is suspected to be in the upgradient proximity of municipal well M-3 due to the persistent carbon tetrachloride (CC1 4) concentrations detected in the well. It is possible that the source

for contamination at well M-3 is also the source for CC1 4 contamination at we 11 OW-3.

Concentrations of metals including cadmium, lead, and iron were detected in industrial well IN-10. The source area is probably in close proximity to

the well given the general mobility and retardation of heavy metals.

PROJ3123 [l

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4. 0 CONCLUSIONS

Section: 4.0 Site: Hastings Revision: 0 Date: 05/07/87 Page 4-1

The conclusions of this report are presented according to the two topics of investigation: site characterization and extent of contamination. The site is characterized by the review of previous investigations and by the acquisition of new information as part of this study. The extent of contamination is evaluated through the compilation of water quality analyses obtained through this and previous studies.

4.1 SITE CHARACTERIZATION

Borehole logs indicate a saturated multi layered system of sand, gravel, and silty/clayey deposits, although the areal continuity of these fine-grained layers is not well established. These logs indicate that the fine grained (silt/clay) layer of deposits, although in existence over a wide area, may not be continuous. This observation becomes very important in the evaluation of contaminant transport in the ground water system.

4.2 EXTENT OF CONTAMINATION

Contamination is likely to be more widespread than can be characterized by the available sampling locations. At any location, the screened interval and depth of an existing well may not be ideal for the specific sampling objectives due to the physical properties of the contaminants. A precise definition of on-site and off-site plumes will require the installation of additional monitoring wells in the Hastings area.

There appears to be more than one source of contamination. Differences in ground water chemistry appear to verify the multi-source concept.

PROJ3130

4.2.1 VOLATILE ORGANIC COMPOUNDS

Section: 4.0 Site: Hastings Revision: 0 Date: 05/07/87 Page 4-2

At least two separate sources of TCE are indicated. One appears to be located near OW-5. A second source is indicated by the presence of TCE in well D-8 at higher levels than in observation wells which are located upgradient of D-8, yet downgradient of OW-5 area. TCE has been detected at concentrations 1250 times the 10-6 Health Risk Criteria of 2.8 ug/1.

Two separate sources of CC1 4 are also indicated by evaluation of analytical data. One is located upgradient of or in the pumping radius of influence of municipal well M-3. Another is located upgradient (west) of irrigation well I-49. Although other sources may exist, there is not enough data available to identify them. cc1 4 has been detected at concentrations over 110 times the 10-6 Health Risk Criteria of 0.42 ug/1.

A single source of EDB is indicated by the levels detected and locations of detection. The source appears to be located upgradient (west) of irrigation well I-49 and CMS-24 and downgradient (east) of the state observation we 11 s ( OW-2) .

4.2.2 METALS

A single source of metal contamination may exist in the proximity of IN-10. However, well construction details for this well are not available and the well itself may be serving as the source of metals contamination.

4.2.3 PESTICIDES

Currently existing data is not sufficient to identify Aldrin (the only pesticide detected) as a contaminant of concern in the Hastings study area. Additional data regarding pesticides is required to confirm their absence in the area.

PROJ3131

5.0 RECOMMENDATIONS


This report is the result of work performed to date and represents progress made as part of the Site Work Plan. Adjustments can be made to the plan to address the results of work performed thus far. Recommendations that detail additional data needs are an important part of the conclusions to this report because they identify areas that may require inclusion in revisions to the Site Work Plan.

General recommendations pertain to the overall program established by the REM II project. Specific recommendations pertain to particular needs or situations that can be addressed in future work.

5.1 GENERAL RECOMMENDATIONS

1) Continue monitoring water levels and water quality.

The cost of remedial actions mandates a sufficient understanding of the site and the contaminants present such that the best remedial action can be prescribed. Substantial information about the nature of the contamination is gained with each sampling period.

2) Intensify investigative efforts to identify contaminant sources.

The sources of contamination must be identified. This requires a plan including the installation of additional monitoring wells. Other investigative methods, such as soil/gas contaminant surveys, have shown that they can provide a cost-effective way to screen areas for assistance in the location of the additional monitoring wells and soil sampling.

PROJ3132

5.2 SPECIFIC RECOMMENDATIONS

1) Establish a ground water level monitoring network.


Determination of the source(s) of contamination can be generally made by back-calculating the travel time for contaminants from their observed location to an upgradient potential source location. The successful use of this procedure is dependent on the accuracy of the potentiometric surface map drawn from water level data. Presently, only one sampling period was made that obtained the accuracy and coverage needed to create an adequate potentiometric surface map. Est~blishment of a ground water level monitoring network of wells in and around the Hastings area will provide better information as to the shape of the potentiometric surface. Quarterly monitoring should show seasonal variations.

2) Correlate water use over time to potentiometric surface and to contaminant transport.

Historical information can provide a basis for numerical simulation of contaminant transport. A three-dimensional model of the layered aquifer will allow consideration of various contaminant sources and evaluation of various remedial measures. A contaminant transport model, however, cannot be considered without sufficient background information including available information on water use.

PROJ3133

6. 0 REFERENCES


Condra, G.E., and E.C. Reed, 1943. The geologic section of Nebraska: Nebraska Geological Survey Bulletin 14, 82 p.

Condra, G.E., Reed, E.C., and E.D. Gordon, 1950. Correlation of the pleistocene deposits of Nebraska: Nebraska Geological Survey Bulletin 15A, 74 p.

Fischer, A.J. and R.F. Spalding, May 1985. Hasting's groundwater VOC investigation, Cooperative Agreement Report with the Department of Environmental Control and the Conservation and Survey Division, Institute of Agriculture and Natural Resources, University of Nebraska-Lincoln, Lincoln, Nebraska.

Groundwater management in the little Blue Basin, Nebraska Geological Survey Information Series II, 1985, approx. 30 p.

Keech, C.F., and V. H. Dreeszen, 1968. Availability of groundwater Adams County, Nebraska. Atlas HA-287, United States Geologic Survey.

Keech, C.F., and V. H. Dreeszen, 1959. Geology and groundwater resources of Adams County, Nebraska. United States Geologic Survey Water Supply Paper 1468, 157 p.

Mundorff, J.C. and K.M. Waddell, 1966. Fluvial Sediment and Chemical Quality of Water in the Little Blue River Basin, Nebraska and Kansas. United States Geological Survey, Water Supply Paper 1819-H, 45 p.

Nebraska Conservation and Survey Division, 1953. Logs of test holes Adams County, Nebraska, Conservation and Survey Division, the University of Nebraska in cooperation with the Geological Survey, United States Department of the Interior.

PROJ3134


Ragon, L.G., 1974. Soil survey of Adams County, Nebraska. United States

Department of Agriculture, Soil Conservation Service, 78 p.

Shultz, C.8., Reed, E.C., and A.L. Lugn, 1951. The Red Cloud sand and gravel, a new Pleistocene formation in Nebraska. Science, V. 114, no. 2969, p. 547-549.

Superfund Public Health Evaluation Manual, 1986. EPA 540/1-86/060.

University of Nebraska-Lincoln, Institute of Agriculture and Natural Resources (IANR) records. (Open file irrigation well information)

40 CFR Part 141, National Primary Drinking Water Regulations.

40 CFR Part 143, National Secondary Drinking Water Regulations.

PROB 135

Ground1

TABLE 2-1

GROUND WATER MEASUREMENTS OBSERVATION WELLS



Observation 2 Surface Elevation Groundwater Elevations ft, msl)

We 11 No. (ft.) Jan. 1985 ay 1985 Sept. 1985 Dec. 1985

OW-ls 1911.6 1791.4 1794.5 1791.4 1792.1 1793.0 1792.8 1791.3 OW-ld 1911.4 1791.8 1794.3 1791.6 1792 .1 1793 .1 1793 .2 1791.4 OW-2s 1910.4 1790.6 1792.6 1790. 5 1791.4 1792.2 1792.4 1790.4 OW-2d 1910.5 1790.5 1792. 7 1790.4 1791.3 1792.3 1792.7 1790.1 OW-3s 1911.2 1795.2 1796.7 1795 .1 1795. 7 1796.5 1796.5 1795.4 OW-3d 1912.5 1795.3 1797 .3 1795.7 1797.9 1797 .0 1796.7 1795.5 OW-4s 1916.6 1796.0 1797.9 1795.9 1796.7 1797 .6 1796.9 1796.3 OW-4d 1916.6 1795.B 1800.6 1795. 6 1796 .6 1797 .5 1796.8 1796.1 OW-5s 1921. 2 1799.4 1799.6 1798.2 1799.2 1800.3 1799.8 1798.8 OW-5d 1921.4 1922.3 1798.6 1798.6 1799. 3 1800.4 1800.0 1799.0

Notes 1

2

Ground surface elevation (datum) is from EPA Survey Revision 1, dated November 11, 1986. Ground water measurements presented for October 1984 and January 1985 are from Fisher and Spalding (1985). The May 1985, September 1985, December 1985, and March, June, and September 1986 measurements were obtained by Woodward-Clyde Consultants.

s - indicates shallow screen and d - indicates deep screen

Notes

Well

M-13 M-16 M-17 1-4 I-21 CMS~19

TABLE 2-2

AQUIFER TRANSMISSIVITY OF SELECTED WELLS1 HASTINGS GROUNDWATER CONTAMINATION SITE

Discharge Thickness Transrnissivity {gem) (ft) (ged/ft)

2,000 103 225,000 1,000 84 150,000 1,000 91 90,000 1,200 70 96,400 1,000 78 97,800

800 82 90,000


Hydraulic Conductiv~ty

(ged/ft)

2,184 1,786

989 1,377 1,254 1,098

1 Taken from State of Nebraska Well Registration Records for Adams County.

PROJ3137

CITY WELL NUMBER:

January February March April May June

July August September October November December

TABLE 2-3

Section: 2.0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-lla

MUNICIPAL WATER WITHDRAWALS FROM SELECTED WELLS (1982 TO 1986)


GALLONS PUMPED IN 1982

3 7 10

383,800

5,785,500 9,085,900 6,913,300 3,697,900 1,822,600 1,990,700

20,484,900 9,400 5,139,300 25,232,500 877,400 4,209,100 2,132,800 6,591,900

2,110,700

12

33,260,000 32,011,000 37,333,000 27,461,000 36,216,000 31,216,000 34,699,000 29,932,000 33,652,000 18,659,000 34,898,000 31,854,000

PROJ3138

CITY WELL NUMBER:

January February March April May June July August September October November December

Section: 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-llb

TABLE 2-3 (continued)



3

6,396,200 4,648,600

495,900


7

13,769,200 19,585,200 7,522,600

10

17,354,700 22,508,400 2,488,000

185,400

12

27,906,000 27,176,000. 23,046,000 21,445,000 21,445,000

3,811,000 1,245,000

pROJ3139

CITY WELL NUMBER:

January February March April May June July August

September October

November December

Section: 2. 0 Site: Hastings Revision: a Date: 05/07 /87 Page: 2-llc




3

7,719,313 22,813,560

990,500


7

145,000

273,083 2,327,220

9,322,500

20,858,000 18,381,150

10

7,910,667

7,910,667

12

PROJ3140

Section: 2.0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-lld





CITY WELL NUMBER: 3 7 10 12

January 19,086,900 February 18,081,500 March 21,576,000 April 94,500 1,643,140 May June 1,538,900 1,014,500 1,271,400 July 6,323,000 13,970,200 9,023,500 August 2,187,000 September 41,800 7,213,300 31,100 October 27,761,600 November 34,448,500 December 9,500 17,935,400 40,100

PROJ3141

CITY WELL NUMBER:

January February


MUNICIPAL WATER WITHDRAWALS

Section: 2.0 Site: Hastings Revision: O Date: 05/07 /87 Page: 2-lle

FROM SELECTED WELLS (1982 TO 1986) HASTINGS GROUNDWATER CONTAMINATION SITE

3


7

33,914,200 21,530,900

10

PROJ3142 ....... ,,,, ''

12

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-12

TABLE 2-4

SUMMARY OF REM II SAMPLING AT HASTINGS SITE

Well Number Ma.z 1985 Seet, 1985 Dec. 1985 March 1986 June 1986 Seet. 1986

OW-ls X X X X X X OW-ld X X X X X X OW-2s X X X X X OW-2d X X X X X X OW-3s X X X X X X OW-3d X X X X X X OW-4s X X X X X X OW-4d X X X X X X OW-5s X X X X X X OW-5d X X X X X X M-3 X X M-6 X X X M-7 X X X X X M-9 X M-10 X X X M-11 X X X M-12 X X X M-15 X X M-16 X M-18 X X CMS-24 X X X X D-1 X X D-2 X 0-7 X D-8 X X X X X IN-I X IN-3 X IN-4 X IN-9 X X IN-10 X X I-1 X I-2 X I-3 X I-7 X I-8 X I-46 X X X I-47 X I-49 X X X X CMS System Sample X

] PROJ3143

TABLE 2-5

SUMMARY OF WELLS SAMPLED BY REM II IN MAY 1985

CHEMICAL ANALYSES PERFORMED Well EPA Sample Volatile Semi-Volatiles Dissolved/

Number Number Organics (BNA) Pesticides Total Metals

OW-ls ACL57012 X

OW-ld ACL57013 X

OW-2s ACL5700i X X X X

Ow-2d ACL57002 X X X X

OW-3s ACL57008 X

OW-3d ACL57009 X

OW-4s ACL57010 X

OW-4d ACL57011 X

OW-5s ACL57003 X X X X

OW-5d ACL57004 X X X X

NOTES 1 Special parameters included pitrate, sulfate, and chloride.

Section 2.0 Site: Hastings Revision: 2.0 Date: 05/07/87 Page: 2-13

Special 1 Parameters EDB

X

X

X X

X X

X

X

X

X

X

X

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-14

TABLE 2-6 SUMMARY OF WELLS SAMPLED BY REM II IN SEPTEMBER, 1985

CHEMICAL ANALYSES PERFORMED Well EPA Sample Volatile Semi-Vol a tiles Dissolved/ Special

Number Number Organics (BNA) Pesticides Total Metals Parameters 1 EDB

OW-ls CKCS2201 X X X OW-ld CKCS2202 X X X OW-2s CKCS2203 X X X OW-2d CKCS2204 X X X OW-3s CKCS2228 X X X X X OW-3d CKCS2229 X X X X X OW-4s CKCS2230 X X X X X OW-4d CKCS2231 X X X X X OW-5s CKCS2226 X X X X X OW-5d CKCS2227 X X X X X M-3 CKCS2221 X X X M-6 CKCS2217 X X X M-7 CKCS2222 X X X M-9 CKCS2219 X X X M-10 CKCS2220 X X X M-11 CKCS2218 X X X M-12 CKCS2224 X X X M-16 CKCS2216 X X X M-18 CKCS2234 X X X CMS-24 CKCS2210 X X X X D-1 CKCS2207 X X X D-2 CKCS2306 X X X D-7 CKCS2211 X X X X D-8 CKCS2212 X X X X IN-3 CKCS2208 X X X

'"d IN-4 CKCS2302 X X X X ~ 0 1-3 CKCS2206 X X X '--,

I-7 CKCS2209 X X X (.;_) ......

I-23 CKCS2213 X ~ X X X v-, 1-46 CKCS2309 X X X

NOTES 1 Special parameters included nitrate, sulfate, chloride, and total alkalinity.

Well Number

OW-ls OW-ld OW-2s OW-2d OW-3s OW-3d OW-4s OW-4d OW-5s OW-5d M-3 M-7 M-10 M-12 M-18 CMS-24 D-8 IN-1 IN-9 IN-10 I-2 I-8

'"d 1-46 ~ I-47 0 ...... 1-49 \.;.) _. +"- NOTES 0\

1 Special

TABLE 2-7

SUMMARY OF WELLS SAMPLED BY REM II IN DECEMBER 1985

CHEMICAL ANALYSES PERFORMED EPA Sample Volatile Dissolved/

Number Organics Total Metals

DKJS2201 X DKJS2202 X DKJS2208 X DKJS2209 X DKJS2010 X DKJS2011 X DKJS2016 X DKJS2017 X DKJS2027 X X DKJS2028 X DKJS2018 X DKJS2019 X DKJS2020 X DKJS2021 X DKJS2032 X X DKJS2006 X X DKJS2003 X X DKJS2024 X X DKJS2004 X X DKJS2025 X X DKJS2014 X X DKJS2030 X X DKJS2031 X X DKJS2013 X X DKJS2007 X X

parameters included chloride, sulfate, and total alkalinity.

Section: 2 .... Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-15

Special 1 Parameters

X

X X X X X X X X X X X

Well Number

OW-ls OW-ld OW-2s OW-2d OW-3s OW-3d OW-4s OW-4d OW-5s OW-5d M-7 M-10 M-12 CMS-24 D-1 0-8 IN-9 IN-10 1-46 1-49

NOTES '"t:) ;:,j 1 Special 0 ._. w -~ ---.l

TABLE 2-8

SUMMARY OF WELLS SAMPLED BY REM II IN MARCH 1986

CHEMICAL ANALYSES PERFORMED EPA Sample Volatile Dissolved/ Special 1 Number Organics Total Metals Parameters

FKJS2201 X X X FKJS2202 X X X FKJS2203 X X X FKJS2019 X X X FKJS2010 X X X FKJS2011 X X X FKJS2012 X X X FKJS2020 X X X FKJS2021 X X X FKJS2022 X X X FKJS2013 X FKJS2014 X FKJS2015 X FKJS2006 X FKJS2027 X FKJS2028 X FKJS2029 X FKJS2025 X X X FKJS2017 X FKJS2018 X X X

parameters included chloride, sulfate, and total alkalinity.


EDB

X

X X

X X

Well Number

OW-ls OW-ld OW-2s OW-2d OW-3s OW-3d OW-4s OW-4d OW-5s OW-5d M-6 M-7 M-11 M-15 CMS-24 D-8 I-49

NOTES

EPA Sample Number

JKLS2002 JKLS2001 JKLS2003 JKLS2005 JKLS2006 JKLS2007 JKLS2008 JKLS2009 JKLS2010 JKLS2011 JKLS2217 JKLS2023 JKLS2025 JKLS2026 JKLS2030 JKLS2032 JKLS2031

Volatile Organics

X X X X X X X X X X X X X X X X X

TABLE 2-9

SUMMARY OF WELLS SAMPLED BY REM II IN JUNE 1986

CHEMICAL ANALYSES PERFORMED Semi-Volatiles Dissolved/

(BNA) Pesticides Total Metals

X X X X X

X X X X X

X X X X X

1 Special parameters included chloride, sulfate, and total alkalinity.

Section: 2.0 Revision: 0 Site: Hastings Date: 05/07/87 Page: 2-17

Special Pararneters1

X X X X X X X X X X

X X X

EDB

X X

Well Number

OW-ls OW-ld OW-2s OW-2d OW-3s OW-3d OW-4s OW-4d OW-5s OW-5d M-6 M-7 M-11 M-15 D-8 I-49 CMS System

NOTES 1 Special

'"d ~ 0 ....... \.>.) ...... +'" \0

TABLE 2-10

SUMMARY OF WELLS SAMPLED BY REM II IN SEPTEMBER 1986

CHEMICAL ANALYSES PERFORMED EPA Sample Volatile Semi-Volatiles Dissolved/

Number Organics (BNA) Pesticides Total Metals

QKLS2007 X QKLS2008 X QKLS2011 X QKLS2012 X QKLS2009 X QKLS2010 X QKLS2013 X X X QKLS2014 X X X QKLS2005 X X X QKLS2006 X X X QKLS2002 X QKLS2001 X QKLS2003 X QKLS2004 X QKLS2018 X X X QKLS2021 X X X X QKLS2005 X

parameters included sulfate,_ chloride, and total alkalinity.

Section: 2.0 Revision: 0 Site: Hastings Date: 05/07/87 Page: 2-18

Special 1 Parameters

X X X X X X X X X X

X X

EDB

X X

X X X

State of Nebraska Observation Wells

OW-ls OW-Id OW-2s OW-2d OW-3s OW-3d OW-4s OW-4d OW-5s OW-5d

Municipal Wells

M-3 M-6 M-7 M-9

M-10 M-11 M-12 M-15 M-16 M-18

TABLE 2-11

TYPES OF WELLS LOCATED IN THE STUDY AREA


HASTINGS AREA

Community and Municipal Services

Wells

CMS-24

Irrigation Wells

1-2 1-3 1-7 1-8

1-23 I-46 1-47 I-49


Industrial Wells

IN-1 IN-3 IN-4 IN-9 IN-10

Domestic Wells

0-1 D-2 0-7 0-8

Parameters

Acetone Benzene Carbon Tetrachloride

Ch 1 oroform Methylene Chloride Tetrachloroethene

Toluene Trichloroethene 1,1,1-Trichloroethane

4-Methyl-1,2-Pentanone Ethyl benzene Xylenes

Notes 1Tlfri"ly detected compounds listed.

TABLE 2-12 DETECTED VOLATILE ORGANIC COMPOUNDS

IN GROUNDWATER SAMPLES - MAY 1985 HASTINGS GROUNDWATER CONTAMINATION SITE

(Concentrations in ug/1)

Observation Well Number OW-ls OW-Id OW-2s

ACL57012 ACL57013 ACL57001

18.0 22.0 3.00 2.00 1.00 ND(5)

ND(5) ND(5) ND(5)

ND(5) ND(5} ND(5} I I 15.0

ND(5) ND(5) ND(5)

2.00 3.00 ND(5) 18.0 24.0 1.00

ND(5) ND(5) ND(5)

2.00 ND( 10) ND( 10) 2.00 ND(5) ND(5} 4.00 3.00 ND(5}

2) See Appendix B for complete chemical analyses. 3) I - Analyses attempted but no result could be reported. 4) ND(5) - Not detected at detection limit indicated.

OW-2d

ACL57002

N0(5) N0(5) ND(5)

ND(5) 19.0

ND(5)

ND(5) 5.00

ND(5)

ND( 10) ND(5) ND(5)

Section: 2.0 Site: Hastings Revision: O Date: 05/07 /87 Page: 2-20a

Parameters


Chloroform Methylene Chloride Tetrachloroethene



Notes ITOnly detected compounds listed.

TABLE 2-12 {continued) DETECTED VOLATILE ORGANIC COMPOUNDS

IN GROUNDWATER SAMPLES - MAY 1985 HASTINGS GROUNDWATER CONTAMINATION SITE


Observation Well Number OW-3s OW-3d OW-4s

ACL57008 ACL57009 ACL57010

1.00 3.00 ND(lO) 2.00 14.0 1.00

ND(5) 13.0 ND(5)

ND(5) 1.00 ND(5) 23.0 14.0 19.0

ND{5) ND{5) ND{5)

6.00 72.0 2.00 5.00 1.00 ND(5)

ND(5) ND{5) ND(5)

ND( 10) ND( 10) ND(IO) 1.00 13.0 ND(5) 4.00 55,0 2.00

2) See Appendix B for complete chemical analyses. 3} I - Analyses attempted but no result could be reported.

'i:::) 4) ND(5) - Not detected at detection limit indicated. ~ '-< w -Vt N

OW-4d

ACL5711

15.0 2.00

ND(5)

ND(5) I 4.00

4.00 180

2.00

ND{lO) 1.00 4.00

Section: 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-20b

Parameters


Chloroform Methylene Chloride Tetrachloroethene



Notes

TABLE 2-12 (continued) DETECTED VOLATILE ORGANIC COMPOUNDS

IN GROUNDWATER SAMPLES HASTINGS GROUNDWATER CONTAMINATION SITE


Observation We 11 Number OW-5d

OW-5s OW-5d Du~licate

ACL57003 ACL57004 ACL57005

110 3.00 2.00 24.0 5.00 6.00

ND( 100) ND(5) ND{5)

ND(lOO) ND(5) ND(5) 860 28.0 26.0 55.0 2.00 2.00

32.0 30.0 33.0 1900. 51.0 52.0 350 6.00 5.00

ND{200) ND(IO) ND( 10) ND( 100) 6.00 8.00 ND(IOO) 24.0 30.0

TTOnly detected compounds listed. 2) See Appendix B for complete chemical analyses. 3) I - Analyses attempted but no result could be reported. 4) ND(5) - Not detected at detection limit indicated.

Section: 2.0 Site: Hastings Revision: O Date: 05/07/87 Page: 2-20c

Well Number

OW-ls . OW-2s

OW-4d OW-5s OW-5d M-3 M-18 D-8 1-46

Notes

1) 2) 3)

TABLE 2-13

DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER SAMPLES - SEPTEMBER 1985 HASTINGS GROUNDWATER CONTAMINATION SITE


HASTINGS AREA

EPA Tri- Carbon 1,1,1-Tri- Trans-1,2-Sample chloro- Tetra- Methylene chloro- Oichloro-Number ethene chloride chloride ethane Benzene ethene

CKCS2201 3.2M ND(5) 32.0 ND(5) ND(5) ND(5) CKCS2203 13.0 ND(5) ND(5) ND(5) ND(5) ND(5) CKCS2231 250 ND(5) ND(5) ND(5) 48.0 ND(5) CKCS2226 1400. ND(50) ND(52) 19.0M ND(50) ND(50) CKCS2227 4.00M ND(5) ND(7) ND(5) ND(5) ND(5) CKCS2221 ND(5) 26.0 ND(5) ND(5) ND(5) ND(5) CKCS2216 ND(5) CKCS2212 690

ND(5~ N0(5~ ND(5) ND(5) ND(5) ND(5 ND(5 N0(5) ND(5) 23.0M

CKCS2309 42.0 ND(5) ND(5) ND(5) N0(5) ND(5)

Only wells with detected compounds are listed and only detected compounds are listed. NO( ) - compound not detected at the level indicated.


1,1- Tetra-Oich 1 oro- chloro-ethene ethene

ND(5) ND(5) ND(5) ND(5) ND(5) 3.0M ND(50) 36.0M ND(5) ND(5) ND(5) ND(5) N0(5) ND(5) ND(5) ND(5) ND(5) ND(5}

M - the value indicated is below the quantification limit but above the detection limit.

" '

Section 2.0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-22a

TABLE 2-14

DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - DECEMBER 1985

HASTINGS GROUND WATER CONTAMINATION SITE (Concentrations in ug/1)

HASTINGS AREA

EPA Tri- Carbon 1,1,1-Tri- Tetra Trans-1,2- 1,1-Well Sample chloro- Tetra- chloro- chloro- Dichloro- Dichloro-

Number Number ethene chloride Chloroform ethene ethene Benzene ethene ethene

OW-ls DKJS2001 45.0J ND( 1) ND(l) ND( 1) ND(l) ND(5) ND(l) ND( 1) OW-ld OKJS2002 49.0J NO(l) ND(l) ND(l~ ND(l~ ND(5l ND(ll ND(li OW-2s OKJS2008 ND(l) ND(l) ND( 1) ND(l ND(l ND(5 . ND(l ND(l OW-2d DKJS2009 33.0J ND(l} ND(l) ND(l) ND(l) ND(5) ND(l) ND(l) OW-3s OKJS2010 6.00J ND(l) ND(l) ND(l~ ND(l) ND(5) ND(l) ND(l) OW-3d DKJS2011 18.0J 34.0J ND(l) ND(l ND(l) ND(5) ND(l) ND(l) OW-4s OKJS2016 llOJ ND(l) ND(l) ND(l) ND(l) ND(5) ND(l) ND(l) OW-4d OKJS2017 680J ND(l) ND(l) 8.00J 9.00J 6.00J ND(l) ND(l) OW-5s DKJS2027 740J ND(l) ND( 1) 18.0J 23.0J ND(5) ND(l) ND(l) OW-5d OKJS2028 13.0J ND(l) ND(l) ND(l) ND(l) ND(5) ND(l) ND(l)

M-3 DKJS2018 ND(l) 32.0J ND~ll NDPl ND~l~ ND(5l ND~ll NDPl M-7 DKJS2019 3.00J ND(l) ND 1 ND 1 ND 1 ND(5 ND 1 ND 1 M-10 DKJS2020 5.00J ND(l) ND(l) ND(l) ND(l) ND(5) ND(l) ND( 1) M-12 OKJS2021 3.00J ND(l~ ND(l~ NDP~ ND(l) ND(5~ NO(l ~ NO(l~ M-18 DKJS2032 (shallow) 190J ND(l ND(l ND 1 ND(l) ND(5 ND(l ND(l

DKJS2033 (deep) 120J ND(l) ND(l) ND(l) ND(l) ND(5) ND(5) ND(l)

Notes

1) Only wells with detected compounds are listed and only detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore,

is only an estimated value.

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87

TABLE 2-14 (continued) Page: 2-22b

DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - DECEMBER 1985


HASTING AREA

EPA Tri- Carbon 1,1,1-Tri- Tetra Trans-1,2- 1,1-Well Sample chloro- Tetra- chloro- chloro- Dichloro- Dich 1 oro-

Number Number ethene chloride Chloroform ethene ethene

CMS-24 DKJS2006 ND(l) 7.00J ND(l) ND(l) ND(l) 0-8 DKJS2003 1100.J ND(l) ND(l) ND(l) 6.00J

1-46 DKJS2031 180J ND(l) ND(l) 2.00J 2.00J I-49 DKJS2007 52.0J 32.0J ND(l) 7.00J ND(l)

IN-1 DKJS2024 2.00J ND(l) ND(l) ND(l) ND(l) IN-9 DKJS2004 7 .OOJ ND(l~ ND(l) Nop~ ND(l) IN-lOb DKJS2026 2.00J ND(l 4.00J NO 1 NO(l)

Notes Tflmly wells with detected compounds are listed and only detected compounds are listed. 2) NO( ) - compound not detected at the level indicated •

Benzene ethene

ND(5) ND(l) ND( 5) . 90.0J

ND(5) NDil~ ND(5) ND 1

ND(5) ND(l) ND(5) ND(ll ND(5) NO(l

• 1.\ J - compound was qualitatively identifiedi however, compound failed to meet all criteria and, therefore, is only an estimated value.

ethene

ND(l) ND( 1)

ND(l) 5.00J

ND(l) ND(l) ND(l)

Section: 2.0 Site: Hastings Revision: O Date: 05/07/87 Page: 2-23a

TABLE 2-15

DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER SAMPLES - MARCH 1986



HASTINGS AREA

EPA Tri- Carbon 1,1,1-Tri Tetra Trans-1,2- 1, 1-Sample Chloro- Tetra- Chloro- chloro- Dichloro- Dichloro-

Well Number Number ethene chloride Chloroform ethane ethene ethene ethene

OW-ls FKJS2001 90.0 NOP} ND~ll ND(l} 0. 7M ND(ll ND(ll OW-ld FKJS2002 lOOJ ND 1) ND 1 ND( 1) 0.7M ND(l ND(l OW-2s FKJS2003 2.40 ND( 1) ND( 1) ND(l) ND(l) ND(l) ND(l) OW-2d FKJS2019 3.50 NO(l) ND(l) ND(l) ND( 1) ND(l) ND( 1) OW-3s FKJS2010 22.0 0.7M ND(ll ND(l} ND(l) ND(l) ND(ll OW-3d FKJS201 l 21.0 24.0 ND(l ND(l) ND(l) ND(l) ND(l OW-4s FKJS2012 3500. ND(25) ND(25) 40.0 42.0 34.0/33.0 ND(25) OW-4d FKJS2020 1800. ND(50~ ND(50! ND(50) 21.0M ND(50) ND(50) OW-5s FKJS2021 1100. NO(SO ND(50 ND(50) ND(50) ND(50) ND(50) OW-5d FKJS2022 25.0 ND(l) ND(l) ND(l) 0.6M ND(l) ND(l)

M-7 FKJS2013 1. 70 ND(l) ND(ll ND(ll NO(l} ND(l) NO(l ~ · M-10 FKJS2014 1.30 ND(l) ND(l ND(l ND(l) ND(l) ND(l M-12 FKJS2015 1.70 ND(l) ND(l) ND(l) ND(l) ND(l) ND(l)

CMS-24 FKJS2006 1. lOJ 7.60J ND(l} ND( 1} ND(l} ND(l} ND(l)

Notes

1) Only wells with detected compounds are listed and only detected compounds are listed. 2) ND ( ) - compound not detected at the level indicated. 3) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore is only

an estimated value. 1) M - the value indicated is below the quantification limit but above the detection limit.

Well Number

D-8

I-46 I-49

IN-9 IN-lOa IN-lOb

Notes

EPA Sample Number

FKJS2028

FKJS2017 FKJS2018

FKJS2029 FKJS2025 FKJS2026

Tri-Chloro-ethene

1200.

54.0 48.0/39.0

6.90 0.9M 0.5M


DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER SAMPLES - MARCH 1986

HASTINGS GROUNDWATER CONTAMINATION SITE (concentrations in ug/1)

HASTINGS AREA

Carbon 1,1,1-Tri- Tetra-Tetra- Chloro- chloro-

chloride Chloroform ethane ethene

ND(5) ND(5) ND(5) ND(5)

4.40 ND(l~ ND( 1) ND(l) 25.0/21.0 ND(l 5.00/4.20 1.80/1. 50

NDP~ ND(l) ND(l~ NO(l) ND 1 4.10 ND(l ND(l) ND(l) 4.10 NO(l) ND(l)

1) Only wells with detected compounds are listed and only detected compounds are listed. 2) NO ( ) - compound not detected at the level indicated.

Section: 2.0 Site: Hast 1 ngs Revision: 0 Date: 05/07/87 Page: 2-23b

Trans-1,2- 1,1-Dichloro- Dichloro-

ethene ethene

41.0 ND(5)

ND(l) ND(l) ND(l) 1.70/1.30

ND(l~ ND(l

ND(l! ND(l

ND(l) ND(l)

3) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore is only an estimated value.

4) M - the value indicated is below the quantification limit but above the detection limit.

Well Number

OW-ls OW-Id OW-2s OW-3d OW-4s OW-4d OW-5s OW-5d D-8 CMS-24 1-49

Notes

EPA Sample Number

JKLS2002 JKLS2001 JKLS2003 JKLS2007 JKLS2008 JKLS2009 JKLS2010 JKLS2011 JKLS2032 JKLS2030 JKLS203l

TABLE 2-16

DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUNDWATER SAMPLES - JUNE 1986



HASTINGS AREA

Tri- Carbon Chloro- Tetra- Tetra-ethene chloride Chloroethene

16.0 ND(l) ND(l) 45.0 ND(l) ND(l) 2.0 ND(l) ND(l)

38.0 18.0 ND( 1) 8.0 ND(l) ND(l)

NO(l) ND(l) 20.0 ND(l) ND(l) ND(l) 19.0 ND(l) ND(l) 690.0 ND(l) 4.0 7.0 18.0 ND(l~

58.0J 37.0J ND(l


1,1,1-Tri Trans-1,2-Chloro- Dichloro-ethane ethene

ND(l) ND(l) ND(l) ND(l} ND(l) ND(l) ND(l) ND(l) ND(l) ND(l) 14.0 NO(l) 18.0 ND(l) ND(l) ND(l) ND(l) 28.0 ND(l) ND(l) 2.00J ND(l)

1) Only wells with detected compounds are listed and only detected compounds are listed. 2) ND ( ) - compound not detected at the level indicated. 1) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore is only

an estimated value. 1) M - the value indicated is below the quantification limit but above the detection limit.

TABLE 2-17

DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER SAMPLES - SEPTEMBER 1986 HASTINGS GROUND WATER CONTAMINATION SITE


HASTINGS AREA

Tri- Tetra- 1,1-Di-Well USEPA chloro- chloroe- 1,1,1-Tri- chloroe- Chloro-Number SAMPLE NO. ethene thene chloroethane thene form

OWls QKLS2007 30.0 N0(5.0} ND(0.7} ND(5.0} ND(5.0) OWld QKLS2008 44.0 ND( 1.3) ND(5.0) ND(5.0) ND(5.0) OW2s QKLS2011 ND(3.0) ND(0.7) ND(5.0) ND(5.0) ND(5.0) OW2d QKLS2012 9.0 N0(0.6) ND(5.0) ND(5.0) ND(5,0) OW3s QKLS2009 ND(3.0) ND(0.5) ND(5.0) ND(5.0) ND(5,0) OW3d QKLS2010 68.0 ND(5.0) ND(5.0) ND(5.0) ND(5.0) OW4s QKLS2013 5.0 ND(0.4~ ND(5.0~ ND(5.0~ ND(5,0) OW4d QKLS2014 74.0 ND( 1. 0 ND(5.0 ND(5.0 ND(5.0) OW5s QKLS2015 1100. 0 29.0 35,0 3.5 N0(5.0) OW5d QKLS2016 34.0 NO( 1. 7) 3.5 N0(5.0) ND(5.0) 0-8 QKLS2018 182.0 ND( 1.5~ 8.0 1. 5 1.0 1-49 QKLS2021 68.6 NO(l.4 6.0 1.1 ND(5.0) CMS Sys tern #1 QKLS2005 4.5 ND(5.0) ND(5.0) ND(5.0) ND(5.0) CMS System #2 QKLS2006 ND(0.8) ND(S.O) ND(5.0) ND(5.0) ND(5.0) M-15 QKLS2004 ND(0.8) ND(5.0) ND(5.0) ND(5.0) ND(5.0)

Notes

1 1) Only wells with detected compounds are listed and only detected compounds are listed. , 2) ND() - compound not detected at the level indicated.


1,1-0i-Carbon chloro-

Tetrachloride thane

ND(5.0) ND{5.0) ND(5.0) ND(5,0) ND(5,0) ND(5,0) ND(5,0) ND(5,0) ND(5.0) N0(5.0) ND(0.6) ND(S.O) ND(5.0) ND(5.0) ND(5.0) ND(5,0) ND(5.0) ND(5.0) ND(5.0) N0(5.0)

4.4 ND(5.0) 45.0 1.0 16.8 ND(5.0) 1.2 ND(5.0)

ND(5.0) 0.5

, 3) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore is only an estimated value.

' _., 4) M - the value indicated is below.the quantification limit but above the detection limit.

TABLE 2-18

DETECTED PESTICIDES

Section: 2. 0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-26

IN GROUND WATER SAMPLES - SEPTEMBER 1985 HASTINGS GROUND WATER CONTAMINATION SITE

Well Number

OW-5s1

OW-3s


CITY OF HASTINGS

EPA Sample Number

CKCS2226D

CKCS2228

A1drin

0.13

0.17

Note 1 - Sample number CKCS2226 was non-detectable for Aldrin at a detection limit of 0.05 ug/1.

PROJ3161

"'d ~ 0 '--< vJ ...... 0,.. N

Well Number: OW-ls

EP{ Sample Number: FKJS2001

Parameter

Barium 120.0 Cadmium N0(5) Ca lei um 100,000 Chromium . NO( 10) Iron N0(50) Magnesium 16,000 Manganese 7.6 Sodium 58,000 Vanadium 12.0 Zinc 38.0

NOTES:

TABLE 2-19

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-27a

DETECTED DISSOLVED METALS IN GROUND WATER SAMPLES MARCH 1986


OW-ld

FKJS2002

190.0 ND(5)

68,000 ND( 10) ND(50) 11,000

2.0 31,000 ND( 10)

90.0


HASTINGS AREA

OW-2s OW-2d OW-3s


170.0 180.0 230.0 ND(5) N0(5) ND(5)

110.000 57,000 81,000 ND( 10) ND( 10) NO(lO) ND(50) ND(5) ND(50) 16,000 8,700 13,000

ND(2) N0(2) 2.6 62,000 31,000 32,000 ND( 10) ND{ 10) NO( 10)

31.0 130.0 180.0

OW-3d OW-4s

FKJS2011 FKJS2012

250.0 140.0 N0(5) N0(5)

80,000 120.000 NO(lO) NO( 10) ND(50) N0(50) 13,000 17,000

2.4 2.8 29,000 61,000 ND ( 10) NO( 10}

98.0 99.0

ND - Not Detected; Detection limit shown in parentheses. M - Value indicated is below the quantification limit but above the detection limit. I - Incomplete Analysis J - Associated value is an estimate because QC criteria were not met.

OW-4d

FKJS2020

310.0 N0(5)

110,000 NO( 10)

51.0 18,000

4.6 37,000 ND( 10) 160.0

'"O ;,;:J

Well Number:

EPA Sample Number:-

Parameter

Barium Cadmium Calcium Chromium Iron Magnesium Manganese Sodium Vanadium Zinc

OW-5s

FKJS2021

67.0 ND(5)

200,000 ND( 10)

77 .o 27,000

70.0 120,000

11.0 150.0

TABLE 2-19 (continued) DETECTED DISSOLVED METALS IN GROUND WATER SAMPLES

MARCH 1986



HASTINGS AREA

OW-5d I-49 IN-10


120.0 250.0 190.0 ND(5) ND(5) 21.0

47,000 94,000 56,000 ND( 10) ND( IO~ ND(lO)

67.0 ND(50 ND(50) 7,900 14,000 11,000

4.7 ND(2) 180.0 23,000 35,000 26,000 ND( 10) ND( 10) ND( 10)

52.0 ND(20) 2,500

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-27b

5 NOTES:

ND - Not Detected; Detection limit shown in parentheses. M - Value indicated is below the quantification limit but above the detection limit. I - Incomplete Analysis J - Associated value is an estimate because QC criteria were not met.

Section: 2.0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-28a

TABLE 2-20 DETECTED TOTAL METALS IN GROUND WATER SAMPLES

MARCH 1986 HASTINGS GROUND WATER CONTAMINATION SITE

(Concentrations ·in ugl/)

HASTINGS AREA

We 11 Number : OW-ls OW-ld OW-2s OW-2d OW-3s OW-3d OW-4s OW-4d

EPA Sample Number: FKJS2001 FKJS2002 FKJS2003 FKJS2019 FKJS2010 FKJS2011 FKJS2012 FKJS2020

Parameter

Aluminum 730.0 110.0 230.0 330.0 71.0 ND(50) 1.300 ND(50) Barium 140.0 160.0 150.0 160.0 230.0 . 230.0 180.0 290.0 Cadmium ND(5) ND(5) ND(5) ND( 10) ND(5) ND(5) ND(5) ND(5) Calcium 100,000 64,000 100,000 55,000 79,000 75,000 120,000 100,000 Chromium ND( 10) ND( 10) ND(lO} ND( 10} ND( 10) ND( 10) ND( 10) ND( 10) Copper ND( 10) 13.0 ND( 10) 10.0 ND( 10) ND(lO) ND( 10) 13.0 Iron 600.0 320.0 220.0 410.0 150.0 73.0 1,200 230,0 l..ead ND(50) ND(50) ND(50) ND(50) ND(50) ND(50) ND(50) ND(50) Magnesium 16,000 11.000 16,000 8,700 13,000 13,000 17,000 17,000 Manganese 50.0 6.1 4.0 7.0 2.2 ND{2) 24.0 5.3 Potassium 9.400 7,600 8,800 7,900 7,600 7,600 10,000 8,100 Sodium 62,000 29,000 58,000 28,000 32,000 28,000 58,000 36,000 Vanadium ND( 10) ND( 10) ND( 10) ND(lO) ND( 10) ND( 10) ND( 10) ND{ 10) Zinc 30.0 150.0 ND(20) 130.0 170.0 87.0 130.0 240.0

"'1::1 Molybdenum ~

ND( 10) ND( 10) · ND( 10) ND( 10) ND(lO) ND( 10) ND( 10) ND( 10) 0

NOTES: '--' w _.

°' ..j::,. ND - Not Detected; Detection limit shown in parentheses • M - Value indicated is below the quantification limit but above the detection limit. I - Incomplete Analysis J - Associated value is an .estimate because QC criteria were not met.

~ ~ 0 '-; w -O'\ v-,

We 11 Number : OW-5s

EPA Sample Number: FKJS2021

Parameter

Aluminum 1,700 Barium 83.0 Cadmium ND(5} Calcium 190,000 Chromium ND( 10) Copper ND(lO) Iron 1600 lead ND(50) Magnesium 26,000 Manganese 90.0 Potassium 14,000 Sodium 110,000 Vanadium NO( 10) Zinc 150.0 Molybdenum ND( 10)

NOTES:

TABLE 2-20 (continued) DETECTED TOTAL METALS IN GROUND WATER SAMPLES

MARCH 1986 HASTINGS GROUND WATER CONTAMINATION SITE


HASTINGS AREA

OW-5d 1-49 IN-10


83.0 ND(50} ND(50} 120.0 250.0 250.0 ND{5) ND(5) 53.0

47,000 88,000 64,000 ND( 10) ND( 10) ND( 10)

20.0 NO(lO) 96.0 240.0 230.0 17,000

ND(50) ND(50} 360.0 7,800 14,000 11,000

6.0 4.4 190.0 I 8,100 I

23,000 33,000 26,000 ND{ 10) ND{ 10) NO(lO) 260.0 ND{20) 5,700

ND(lO) NO(lO) NO( 10)

ND - Not Detected; Detection limit shown in parentheses.

Section: 2.0 Site: Hastings Revision: O Date: 05/07/87 Page: 2-28b

M - Value indicated is below the quantification limit but above the detection limit. I - Incomplete Analysis J - Associated value is an estimate because QC criteria were not met.

I

Well Number

OW - ls OW - ld OW - 2s OW - 2d OW - 3s OW - 3d OW - 4s OW - 4d OW - 5s OW - Sd

M - 3 M - 6 M - 7 M - 9 M - 10 M - 11 M - 12 M - 16 M - 18

CMS - 24

I - 3 I - 7 I - 23 I - 46

TABLE 2-21

SELECTED GENERAL WATER QUALITY PARAMETERS IN GROUND WATER SAMPLES

SEPTEMBER 1985

HASTINGS GROUND WATER CONTAMINATION SITE (Concentrations in mg/1)

HAST! NGS AREA

Parameter EPA Sample

Number Nitrate Chloride Sulfate

CKCS2201 6.9 24.0 52.0 CKCS2202 2.3 16.0 35.0 CKCS2203 12.0 43.0 80.0 CKCS2204 3.6 24.0 61.0 CKCS2228 4.0 34.0 35.0 CKCS2229 4.3 25.0 61.0 CKCS2230 1.4 112.0 32.0 CKCS2231 4.9 39.0 67.0 CKCS2226 11.0 53.0 290.0 CKCS2227 2.6 9.3 23.0

CKCS2221 6.9 25.0 90.0 CKCS2217 4.4 10.0 29.0 CKCS2222 4.1 17.0 44.0 CKCS2219 3.9 12.0 24.0 CKCS2220 3.7 16.0 44.0 CKCS2218 4.5 11.0 30.0 CKCS2224 3.9 19.0 57.0 CKCS2216 6.1 10.0 31.0 CKCS2234 8.6 45.0 86.0

CKCS2210 6.1 22.0 32.0

CKCS2206 12.0 28.0 30.0 CKCS2209 8.4 24.0 30.0 CKCS2213 22.0 64.0 52.0 CKCS2209 4.9 25.0 36.0

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-29a

ota Alkali n i t.z:

334.0 205.0 159.0 240.0 287.0 188.0 299.0 224.0 457.0 148.0

218.0 159.0 181.0 154.0 179.0 160.0 192.0 160.0 356.0

203.0

264.0 245.0 267.0 267.0

PROJ3166

Well Number

IN - 3 IN - 4

D - 1 D - 2 D - 7 D - 8



SEPTEMBER 1985


HASTINGS AREA

Section 2.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-29b

Parameter EPA Sample ota

Number Nitrate Chloride Sulfate Alkalinit:z:

CKCS2208 5.9 9.2 24.0 192.0 CKCS2302 7.8 22.0 23.0 268.0

CKCS2207 8.7 41.0 30.0 191.0 CKCS2306 6.8 23.0 61.0 220.0 CKCS2211 11.0 22.0 61.0 197.0 CKCS2212 9.1 23.0 37.0 267.0

PROJ3167 3


TABLE 2-22


DECEMBER 1985

HASTINGS GROUND WATER CONTAMINATION SITE (Concentrations in mg/l)

HASTINGS AREA

Parameter

Well EPA Sample Total Number Number Chloride Sulfate Alkalinitt

OW - 5s DKJS2027 69.5 170.0 191.0J

M - 18 DKJS2032 46.1 53.0 365.0J

CMS - 24 DKJS2006 23.9 33.0 211.0J

I - 2 DKJS2014 28.4 25.0 200.0J I - 8 DKJS2030 16.7 20.0 195.0J I - 46 DKJS2031 26.9 30.0 274.0J I - 47 DKJS2013 20.0 32.0 197.0J I - 49 DKJS2007 20.6 48.0 259.0J

IN - 9 DKJS2004 14.8 33.0 189.0J IN - 10 DKJS2025 16.7 19.0 139.0J

D - 8 DKJS2003 22.5 30.0 262.0J

NOTES:

NA - Not Analyzed J - Indicated value is an estimate because QC criteria were not met.

NOTE:

TABLE 2-23


MARCH 1986


HASTINGS AREA

Section 2.0 Site: Hastings Revision: O Date: 05/07/87 Page: 2-31

Parameter

Parameter

OW - ls OW - ld OW - 2s OW - 2d OW - 3s OW - 3d OW - 4s OW - 4d OW - 5s OW - Sd

I - 49

IN - 10

EPA Sample Number

FKJS2001 FKJS2002 FKJS2003 FKJS2019 FKJS2010 FKJS2011 FKJS2012 FKJS2020 FKJS2021

. FKJS2022

FKJS2018

FKJS2025

NA - Not Analyzed

Nitrate Chloride

NA 25.5 NA 18.1 NA 39.4 NA 14.1 NA 29.6 NA 38.3 NA 77. 5 NA 30.1 NA 60.5 NA 9.36

NA 20.8

NA 20.9

ota Sulfate Alkali nit:z:

53.0 349.0 36.0 214.0 53.0 300.0 38.0 402.0 36.0 NA 52.0 182.0 70.0 298.0 91.0 249.0

242.0 435.0 23.8 166.0

51.0 261.0

27.0 178.0

PR013169 -- -I ..

NOTES:

TABLE 2-24

EDS IN GROUND WATER SAMPLES

MARCH 1986

Section 2.0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-32


HASTINGS AREA

EPA Sample Well Number Number 1,2 - Oibromoethane

CMS - 24 FKJS2006 0.13

I - 46 FKJS2017 N0(0.02)

I - 49 FKJS2018 6.8

IN - 9 FKJS2029 ND(0.02)

D - 8 FKJS2028 ND(0.02)

ND - Not detected; detection limit shown in parentheses.

PROJ3170

NOTES:

TABLE 2-25

EDB IN GROUND WATER SAMPLES JUNE 1986



Well Number

OW-2s

OW-2d

CMS-24

D-8

I-49


HASTINGS AREA

EPA Sample Number 1,2 - Dibromoethane

JKLS2003 ND(0.4)

JKLS2005 ND(0.4)

JKLS2030 ND(0.4)

JKLS2032 ND(0.4)

JKLS2031 3.70

ND - Not detected; detection limit shown in parentheses.

PROJ3171

NOTES:

TABLE 2-26

EDB IN GROUND WATER SAMPLES SEPTEMBER 1986



Well Number

OW-2s

OW-2d

0-8

I-49

CMS System

CMS System


HASTINGS AREA

EPA Sample Number 1,2 - Dibromoethane

QKLS2011 ND(0.1)

QKLS2012 ND(0.1)

QKLS2018 0.5

QKLS2021 3.2

(9/2/86) QKLS2005 ND(O.l)

(9/10/86) QKLS2006 ND(O.l)

NO - Not detected; detection limit shown in parentheses.

PROJ3172

NOTE:

TABLE 2-27

Section: 2. 0 Site: Hastings Revision: 0 Date: 05/07 /87 Page: 2-35

TOTAL DISSOLVED SOLIDS! IN GROUND WATER SAMPLES

HASTINGS AREA (mg/1)

WELL May September December March NUMBER 1985 1985 1985 1986

OW - ls 397 390 396 449 OW - ld 233 195 240 276 OW - 2s 384 390 390 455 OW - 2d 234 325 276 215 OW - 3s 475 390 286 280 OW - 3d 281 319 273 302 OW - 4s 520 488 455 475 OW - 4d 221 358 234 335 OW - Ss 845 845 683 634 OW - Sd 185 195 195 172

M - 7 260 230 215 M - 10 254 228 182 M - 12 286 237 163

CMS - 24 293 260 263

IN - 9 NS 2 260 241 IN - 10 NS 2 185/273 257 /267 .

I - 46 306 319 325 I - 49 NS 2 325 163

D - 1 325 NS 2 397 D - 8 338 325 299

1 Total dissolved solids content was approximated by multiplying .the measured specific conductance by 0.65.

2 NS= Not Sampled

June 1986

439 280 532 262 216 369 425 347 850 227

272

305

425

390

I. PROJ3173

""O ~ 0 ._ w ...... ---.l ~

TABLE 2-28


SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS HASTINGS GROUNDWATER CONTAMINATION SITE


OBSERVATION WELL OW-ls

Parameters 5/85 9/85 12/85 3/86 6/86

Acetone 18.0 ND(lO) ND(2) ND(lO) Benzene 2.00 ND{5) ND(5) ND(l) ND(5) Carbon Tetrachloride ND(5) ND(5) ND(l) ND(l) ND(l)

Chloroform ND(5) ND(5) ND(l) ND(l) ND(l) Dibromochloromethane ND(5) ND(5) ND(l) ND(l) ND(l)

1,2-Dichloroethane ND(5) ND(5) ND(3) ND(l) ND(l) 1,1-Dichloroethene ND(5) ND(5) ND(l~ ND(l~ ND(l) Trans-1,2-Dichloroethene ND(5) ND(5) ND(l ND(l ND(l)

Methylene Chloride I 32.0 ND( 10) ND(l) ND( 10) Tetrachloroethene ND(5) ND(5~ ND(l) 0.7M NO( 1) Toluene 2.00 ND(5 ND(5) ND(l) ND(5)

Trichloroethene 18.0 3.2M 45.0J 90.0 16.0 1,1,1-Trichloroethane ND(5) ND(5) NO(l) ND(l) ND(l)

4-Methyl-2-Pentanone 2.00 ND( 10) ND(2) Ethyl Benzene 2.00 ND(5~ ND(5) ND(l) ND(5~ Xylenes 4.00 ND(5 ND(l) ND(5

Notes Tronly detected compounds are listed. 2) ND ( ) 1 compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5) M - the value indicated is below the quantification limit but above the detection limit. 6) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,

therefore, is only an estimated value.

9/86

ND(IO) N0(0.2)

ND(5)

ND(5) ND(5)

N0(5) ND(5) ND(5)

ND(0.5) ND(5)

ND(0.2)

30.0 ND(0.7)

ND(0.5)


TABLE 2-29 SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS

HASTINGS GROUNDWATER CONTAMINATION SITE (Concentrations in ug/1)

OBSERVATION WELL OW-ld

Parameters 5/85 9/85 12/85 3/86 6/86 9/86

Acetone 22.0 ND(lO) ND(2) ND(lO) Benzene 1.00 ND(5) ND(5) ND(l) ND(5) ND(0.2) Carbon Tetrachloride ND{5) ND{5) ND(l) ND(l) ND{l) ND{5)

Chloroform ND(5) ND(5) ND(l) ND(l) ND(l) ND(5) Dibromochloromethane ND(5) ND(5) ND(l) ND(l) ND(l) ND(5)

1,2-Dichloroethane N0(5) ND(5) ND(l) ND(l) ND(l) ND(5) 1,1-Dichloroethene ND(5) ND(5) ND(l) ND(l) ND(l) ND(5) Trans-1,2-Dichloroethene ND(5) ND(5) ND(l) ND(l) ND( 1) ND(5)

__ Methylene Chloride I N0(5~ ND(lO) NO(l) NO( 10) N0(0.6) ·~ Tetrachloroethene N0(5) ND(5 ND(l) 0.7M ND(l) ND( 1.3)

Toluene 3.00 N0(5) ND(5) ND(l) ND(5) N0(0,2)

Trichloroethene 24.0 30 49.0 lOOJ 45,0 44.0 1,1,1-Trichloroethane N0(5) ND(5) NO(l) NO(l) ND(l) ND(5)

4-Methyl-2-Pentanone ND(lO) NO( 10) N0(2) ND(l) Ethyl Benzene ND(5) N0(5) ND(5) NO(lj ND(5~ N0(0.5) Xylenes 3.00 ND(5) ND(l ND(5

Notes Jr-only detected compounds are listed. 2) NO ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5) M - the value indicated is below the quantification limit but above the detection limit. 6) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,


1-,j

5 '-' I.>) --.J

°'




OBSERVATION WELL OW-2s

Parameters 5/85 9/85 12/85 3/86

Acetone 3.00 ND(lO} ND(7) Benzene N0(5~ N0(5) N0(5) NO(l) Carbon Tetrachloride ND(5 ND{5) ND(l) ND(l)

Chloroform ND(5} ND(5} ND(l~ ND~l) Dibromochloromethane ND(5) ND(5) ND(l ND 1)

1,2-Dichloroethane ND{5) ND(5} ND(l) ND(l} 1,1-Dichloroethene ND(5i ND(5) ND(l) ND(l) Trans-1,2-Dichloroethene ND(5 ND(5) ND(l) ND(l)

Methylene Chloride 15.0 ND(5~ ND(lO~ ND{l~ Tetrachloroethene ND(5} ND(5 ND(l ND(l Toluene ND(5) ND(5) ND(5) ND(l)

Trichloroethene 1.00 13.0 4.00J 2.40 1,1,1-Trichloroethane ND(5) ND(5) ND(l) ND(l)

4-Methyl-2-Pentanone ND( 10) ND( 10) NDF} Ethyl Benzene ND(5) ND(5) ND(5} ND 1) Xylenes ND(5) ND(5) ND(l}

Notes ~nly detected compounds are listed. 2) ND ( }, compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed.


6/86 9/86

ND( 10) N0(5) ND(0.2) ND(l) ND(5)

ND( 1} ND(5) ND(l} ND(5}

ND(l} ND{5} ND(l) ND(5) ND(l) N0(5)

ND( 10) ND{0.5} ND(l} ND(0.7) ND(5) ND(0.2)

2.00 N0(3) ND(l} ND(5)

ND(5) ND(0.5) ND(5)

5) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore, is only an estimated value.

'"ti :,;; 0 '-< l,.) ...... -...J -...J




OBSERVATION WELL OW-2d

Parameters 5/85 9/85 12/85 3/86

Acetone ND(5l ND(lol ND(2) Benzene ND(5 ND(5 ND(5) ND(l) Carbon Tetrachloride ND(5) ND(5) ND(l) ND(l)

Ch 1 oroform ND(5) ND(5) ND(l~ Nop~ Dibromochloromethane ND(S) ND(S) ND(l ND 1

1,2-Dichloroethane ND(5) ND(5~ ND~l! NOP~ 1,1-Dichloroethene ND(5) ND(5 ND 2 ND 1 Trans-1,2-Dichloroethene ND(5) ND(5) ND( 1) ND(l)

Methylene Chloride 19.0 ND(5) ND( 10) ND(l) Tetrachloroethene ND(5) ND(5) ND( 1) ND( 1) Toluene ND(5) ND(S) ND(5) ND(l)

Trichloroethene 5.00 92 33.0J 3.50 1,1,1-Trichloroethane ND(5) ND(5) ND(l} ND(l)

4-Methyl-2-Pentanone ND( 10) ND( 10) ND(2) Ethyl Benzene ND(5) ND(5) ND(5) ND(l) Xylenes ND(5) ND(5) ND(l)

Notes n--Tinly detected compounds are listed . 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported.


6/86 9/86

ND( 10) ND(5) ND(0.2) ND(l) ND(S)

ND(l) ND(5~ ND(l) ND(5

ND(l) NDi5! ND( 1) ND 5 ND(l) ND(5)

ND( 10) ND(0.6) ND(l) ND(0.6) ND(5) ND(0.2)

ND(l) 9.0 ND(l) ND(5)

N0(5) ND(0.5) ND(5)

4) -, Not analyzed for compound listed. 5) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,

therefore, is only an estimated value. I

"'t) ::;o 0 '-< l,,.) ----i 00

TABLE 2-32

Section: 2.0 Site: Hastings Revision. O Date: 05/07/87 Page: 2-40

SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS HASTINGS GROUND WATER CONTAMINATION SITE



Parameters 5/85 9/85 12/85 3/86 6/86

Acetone 1.00 ND(IO) ND(2! ND(lO! Benzene 2.00 ND(5) ND(5} ND(l N0(5 Carbon Tetrachloride ND(5) ND(5) ND(l) 0.7M ND(l)

Chloroform ND~5) N0(5) ND(l~ ND(l~ ND(li Dibromochloromethane ND 5) ND(5) ND(l NO(l ND(l

1,2-Dichloroethane ND(5) NO?) ND(l! NO(l~ NO(ll 1,1-Dichloroethene ND(5) ND 5) ND(l ND(l NO(l Trans-1,2-Dichloroethene ND(5) ND(5) NO( 1) ND(l) ND(l)

Methylene Chloride 23.0 N0(7) ND( 10) ND(l) ND( 10) Tetrachloroethene ND(5) ND(5) ND(l) ND(l) ND(l) Toluene 6.00 ND(5) ND(5) ND(l) ND(5)

Trichloroethene 5.00 3M 6.00J 22.0 ND(l) 1,1,1-Trichloroethane ND(5) IM ND(l) ND(l) ND(l)

4-Methyl-2-Pentanone ND(lO) NO( 10) ND(2) Ethyl Benzene 1.00 N0(5) ND(5) ND(l) ND(5) Xylenes 4.00 ND(5) ND(l) ND(5)

Notes TTonly detected compo~nds are listed. 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5) M - The value indicated is below the quantification limit but above the detection limit. 6) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,


9/86

ND(0.2) ND(5)

ND(5) ND(5)

N0(5! ND(5 ND(5)

ND(0.7) ND(0.5) ND(0.2)

44.0 ND(5)

ND(0.5)

'"O ~ 0 '--w ..... -.....J \0

TABLE 2-33





Parameters 5/85 9/85 12/85 3/86 6/86

Acetone 3.00 NO{lO) N0(2) NO( 10! Benzene 14.0 N0(5) N0(5) NO(l) ND(5 Carbon Tetrachloride 13.0 23.0 34.0J 24.0 18.0

Chloroform 1.00 ND(5} ND(l) ND(l) ND(l) Dibromochloromethane ND(5) N0(5) ND(l) ND(l) ND(l)

1,2-Dichloroethane ND(5) ND(5) ND(l) ND(l) ND(l) 1,1-Dichloroethene ND(5) ND(5) ND(l) ND(l) ND(l) Trans-1,2-Dichloroethene ND(5) ND(5) ND(l) ND(l) ND(l)

Methylene Chloride 14.0 ND(5) ND(lO) ND(l) ND( 10) Tetrachloroethene ND(5) ND(5) ND( 1) ND(l) ND( 1) Toluene 72.0 ND(5) ND(5) ND(l) ND(5)

Trichloroethene 1.00 3M 18.0J 21.0 38.0 1,1,1-Trichloroethane ND(5) ND(5) ND(l) ND(l) ND(l)

4-Methyl-2-Pentanone ND( 10) ND( 10) ND(2) Ethyl Benzene 13.0 ND(5) ND(5) ND(ll N0(5l Xylenes 55.0 ND(5) ND(l ND(5

Notes "i"}Only detected compounds are listed. 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5) M - the value indicated is below the quantification limit but above the detection limit. 6) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,


9/86

ND(0.2) ND(5)

ND(5) ND(5)

N0(5) ND(5) ND(5)

ND(5) ND(5)

ND(0.2)

68.0 ND(5)

ND(0.5)

"t:I ::,;; 0 c...; vJ -00 0

TABLE 2-34





Parameters 5/85 9/85 12/85 3/86 6/86

Acetone ND( 10) NO( 101 ND(50l NO( 101 Benzene 1.00 ND(5 ND(5) ND(25 ND(5 Carbon Tetrachloride ND(5) ND(5) ND(l) ND(25) ND(l)

Chloroform ND~5) N0(5) ND(l~ ND(25) ND(l~ Dibromochloromethane ND 5) ND(5) ND(l ND(25) ND(l

1,2-Dichloroethane ND(5) ND(5) ND(l) ND(25) ND(l) 1,1-Dichloroethene ND(5) ND(5) ND(l) ND(25) ND(l) Trans-1,2-Dichloroethene ND(5) ND(5) ND(l) 34.0 ND( 1)

Methylene Chloride 19.0 ND(5) ND( 10) ND(25) ND(IO) Tetrachloroethene ND(5) ND(5) ND(l) 42.0 ND(l) Toluene 2.00 ND(5) ND(5) ND(42) ND(5)

Trichloroethene ND(5) ND(5) llOJ 3500. 8.00 1,1,1-Trichloroethane ND(5) ND(5) ND(l) 40.0 ND(l)

4-Methyl-2-Pentanone ND( 10) ND( 10) ND(50) Ethyl Benzene ND(5) ND(5) ND(5) ND(25) N0(5) Xylenes 2.00 N0(5) ND(25) ND(5)

Notes TTonly detected compounds are listed. 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,


9/86

ND(0.2) ND(5)

ND{5) ND(5)

ND(5) ND(5) ND(5)

ND(0.5) ND(0.4) ND(0.2)

5.0 ND(5)

N0(0,5)

'"c ~ 0 '--< w _. 00 _.



{Concentrations in ug/1)


Parameters 10/84 5/85 9/85 12/85

Acetone 15.0 ND(IO) ND(IOO) Benzene 2.00 48.0 6.00J ND(50) Carbon Tetrachloride ND(5) ND{5) ND{l) N0(50)

Ch 1 oroform ND(5) ND(5) ND(l) ND(50) Oibromochloromethane N0(5) ND(5) ND{l) ND(50)

1,2-Dichloroethane ND(5) ND(5) ND(l) ND(50) 1,1-0ichloroethene ND(5) ND(5) ND(l) ND(50) Trans-1,2-Dichloroethene ND(5) ND(5) ND(l) ND(50)

Methylene Chloride ND(5) ND(5) ND(IO) ND(50) Tetrachloroethene 4.00 3.00M 9.00J 21.0M Toluene 4.00 ND(5} ND(5) ND(71}

Trichloroethene 180 250 680J 1800. 1,1,1-Trichloroethane 2.00 ND(5} 8.00J ND(50)

4-Methyl-2-Pentanone ND(IO) ND{lO) ND(lOO) Ethyl Benzene 1.00 ND(5) ND(5} ND(50) Xylenes 4.00 ND(5) ND(50)

Notes n-7Jnly detected compounds are listed. 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed.


3/86 6/86

ND(lO) ND(5) ND(0.2) ND(l) ND(5)

ND(l) ND{5) NO(l) N0(5)

ND(l) N0(5) ND(l) ND(5) ND(l) ND(5)

ND( 10) ND(0.5) ND(l) ND(2.5) ND(5} N0(5)

20.0 61.0 14.0 ND(5)

ND(5) ND(0.5) ND(5)

5) J - compound was qualitatively identified; however, compound failed to meet all therefore, is only an estimated value.'

QA criteria and,

9/86

ND(0.2) ND{O.l)

ND(O.l) ND(O.l)

NO(O.l) N0(0.1) N0(0.1)

NO{O.l) ND(l)

ND(0.2}

74.0 ND(0.1}

ND(0.5)



(Concentrations in ug/1} OBSERVATION WELL OW-5s

Parameters 5/85 9/85 12/85 3/86 6/86

Acetone 110 ND{71} ND(lOO} ND( 10} Benzene 24.0 ND{50) ND(5) ND(50~ ND(5) Carbon Tetrachloride ND( 100) ND(50) ND{l) ND(50 ND(l)

Chloroform ND~ lOOl ND(50~ ND(ll ND(50~ ND(l! Dibromochloromethane ND 100 ND{50 ND{l ND(50 ND{l

1,2-Dichloroethane ND( 100~ ND(50~ ND~l~ ND~50~ ND(Jl 1,1-Dichloroethene ND( 100 ND(50 ND 1 ND 50 ND{l Trans-1,2-Dichloroethene ND( 100) ND{50) ND(l) ND(50) ND(l

Methylene Chloride 860 ND(52) ND(lO) ND~50! ND{ 10} Tetrachloroethene 55.0 36.0M 23.0J ND 50 29.0 Toluene 32.0 ND(50) ND(5) ND(52) ND(5)

1,1,2-Trichloroethane I ND{50) ND(l) ND(50) ND(l) Trichloroethene 1900 1400. 740J 1100. 1100. 1,1,1-Trichloroethane 350 19.0M 18.0J ND{50) 18.0

4-Methyl-2-Pentanone ND(200) ND( 100) ND(lOO) Ethyl Benzene ND(lOO) ND(50) ND(5) ND(50) ND(5) Xylenes ND( 100) ND(50) ND(50) ND(5)

Notes n-only detected compounds are listed. 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5) M - The value indicated is below the quantification limit but above the detection limit. 6) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,


9/86

ND(0.2l ND(5

N0(5~ ND(5

ND(5) 3.5

ND(5)

ND(0,3) 29.0

ND(0.2)

ND(5) 1100 35.0

ND(0.5)

t:r'!

'"d ~ 0 <-< v-> _. 00 v->

TABLE 2-37

Section: 2. 0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 2-45




Parameters 5/85 9/85 12/85 3/86 6/86

Acetone 3.00 ND( lOl ND(2~ ND(lO~ Benzene 5.00 ND(5 ND(5) ND(l ND(5 Carbon Tetrachloride ND(5) ND(5) ND(l) ND(l) ND(l)

Chloroform ND~5~ ND~5l NDPl NDP~ NDP~ Dibromochloromethane ND 5 ND 5 ND 1 ND 1 ND 1

1,2-Dichloroethane N0~5} ND(5) ND(li ND(ll ND(l) 1,1-Dichloroethene ND 5) ND(5) ND(l ND(l ND(l) Trans-1,2-Dichloroethene N0(5) N0(5) NO(l) NO(l) ND(l)

Methylene Chloride 28.0 ND(7) NO(lO) NO(l} NO( 10} Tetrachloroethene 2.00 ND(5) ND(l} 0.6M ND(l) Toluene 30.0 ND(5) ND(5) ND(l) ND(5)

Trichloroethene 51.0 4.00M 13.0J 25.0 19.0 1,1,1-Trichloroethane 6.00 ND(5) ND(l) ND{l) ND(l}

4-Methyl-1,2-Pentanone ND( 10) ND( 10) ND(2~ Ethyl Benzene 6,00 ND(5) ND(5) ND(l ND(5} Xylenes 24.0 ND(5) ND( 1) ND(5)

Notes TTonly detected compounds are listed. 2) ND ( ), compound not detected at the level indicated. 3) I - Analysis attempted but no result could be reported. 4) -, Not analyzed for compound listed. 5~ M - the value indicated is below the quantification limit but above the detection limit. 5 J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,


9/86

ND(0.2) ND(5)

ND~5i ND 5

ND(5) ND(5) ND(5}

ND(5} ND( 1. 7) ND(0.2)

34.0 3.5

ND(0.5)




MUNICIPAL WELL M-3 (CITY OF HASTINGS)

Parameters 4/83 5/11/83 5/24/83 4/85 9/85 12/85

Carbon Tetrachloride 27.1 46.4* 31.3 22.0 26.0 32.0J

Chloroform ND ND ND ND(l) ND(5) ND(l)

Trichloroethene ND ND ND ND(l} ND(5} ND(l}

Notes 117Jnly detected compounds are listed. 2) NO( ) - compound not detected at the level indicated.


3/86 6/86

NS NS

NS NS

NS NS

3) "*"- Multiple samples collected during this month; concentration reported is the highest concentration detected during the month.

4) -. Not analyzed for compound listed. 5) Data reported as less than ( ) reported as received from Nebraska State Laboratories. 6) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore,

is only an estimated value. · 7) NS - not sampled.

9/86

NS

NS

NS

TABLE 2-39



MUNICIPAL WELL M-7 (CITY OF HASTINGS}

Parameters 5/24/83 4/85 9/85 12/85 3/86

Trichloroethene 6.81 ND(l) ND(5) 3.00J 1. 70

Toluene . • 966 ND(5) ND(5) ND(5) ND(l)

Methylene Chloride 1.15 ND( 10) ND(5) ND( 10) ND(l)

Benzene .382 ND(5) ND(5) ND(5) ND(l)

Notes

1) Only detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) M - the value indicated is below the quantification limit but above the detection limit. 4) Data reported as less than ( ) reported as received from Nebraska State Laboratories. 5) J - compound was qualitatively identified; however, compound failed to meet all QA criteria

and, therefore, is only an estimated value. ?) - Samples were collected; parameter not analyzed.

Section: ,.o Site: Hastings Revision: O Date: 05/07/87 Page: 2-47

6/86 9/86

ND( 1) ND(2.5)

ND(5) ND(0.6)

ND( 10) ND(l)

ND(5) ND(0.2)

Parameters

Trichloroethene

Notes

4/83

19.6





5/11/83

19.8

5/24/83

46.5

4/85

ND(l)

9/85

2M

TIOnly detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) -, not analyzed for compound listed. 4) NS - Not samples.


12/85

5.00J

3/86 · 6/86

1.30 NS

5) M - the value indicated is below the quantification limit but above the detection limit. 6) Data reported as less than ( ) reported as received from Nebraska State Laboratories. 7) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore,

._. is only an estimated value.

9/86

NS

--·

Parameters 4/83

1,1-Dichloroethane NO

Trichloroethene 352.0

1,1,1-Trichloroethane 10.4

Notes





5/11/83 5/24/83 4/85 6/85 9/85

ND 3.47 ND(l) 0.9 ND(5)

249.2 ND ND(l) 0.7 ND(5)

3.8 ND ND(l) 0.4 ND(5)

Tionly detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) -, not analyzed for compound listed. 4) NS - Not sampled.


12/85 3/86

ND(l) ND(l)

3.00J 1.70

ND(l) ND(l)

6/86

NS

NS

NS


9/86

NS

NS

NS

"tl ~ 0 '-< uJ -00 00



MUNICIPAL WELL M-18 (CITY OF HASTINGS}

Section: 2.0 Site: Hastings Revision~ 0 Date: 05/07/87 Page: 2-50

12/85 Parameters 3/83 4/83 5/83 4/85 9/85 _ltl_ JJiL 3/86

Benzene 4.22* ND(5) ND(5) ND(5) ND(5) NS Carbon Tetrachloride ND 3.18* ND(l) ND(5) ND(l) ND(l) NS

1,1-Dichloroethane 13.5 13.3* ND(l) ND(5) ND(l) ND(l) NS

1,1-Dichloroethene 24.6 16.0* ND(l) ND(5) ND(l) ND(l) NS Trans-1,2-Dichloroethene 74.2 75.7* ND(l) ND(5) ND(l) ND(l) NS

Methylene Chloride 4.45* ND(lO) ND(5~ ND(lO) ND( 10) NS Tetrachloroethene 60.4 53.0* ND(l) ND(5 NO(l) ND(l) NS Toluene ND(5} ND(5) ND(5) ND(5) NS

Trichloroethene 500 2,000 1,620* 34.0 ND(5) 190J 120J NS 1,1,1-Trichloroethane 120 133* ND(l) ND(5) ND(l) ND(l) NS 1,1,2-Trichloroethane 4.42 ND(l) ND(5) ND(l) ND( 1) NS

Notes T)7Jnly detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) "*" - Multiple samples collected during this month; concentration reported is the highest

concentration detected during the month. 4) Samples M-18a and M-18b, collected in December 1985, were obtained at depths of approximately

150 feet and 200 feet, respectively. 5) -, not analyzed for compound listed. 6) Data reported as less than ( ) reported as received from Nebraska State Laboratories. 7) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and,

is only an estimated value. 8) NS - Not sampled.

6/86 9/86

NS NS NS NS

NS NS

NS NS NS NS

NS NS NS NS NS NS

NS NS NS NS NS NS

therefore,

TABLE 2-43




MUNICIPAL WELL CMS-24 (COMMUNITY AND MUNICIPAL SERVICES)

Parameters 6/85 9/85 12/85 3/86 6/86

Carbon Tetrachloride 22 ND(5) 7.00J 7.60J 18.0

Chloroform 0.2 ND(5) ND(l) ND( 1) ND(l)

1,1-Dichloroethene 0.1 ND(5) ND(l) ND(l) ND(l)

Trichloroethene 6.0 ND(5) ND(l) 1. lOJ 7.00

1,1,1-Trichloroethane 0.5 ND(5) ND(l) ND(l) ND(l)

1,2-Dibromoethane .32 ND(.02) NS 0.13 ND(0.4)

Notes 1Jlmly detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) -, not analyzed for compound listed. 4) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore, 5} NS - Not sampled.

is only an estimated value.

9/86

NS

NS

NS

NS

NS

NS





DOMESTIC WELL D-8 (MORRISON-QUIRK)

Parameters 6/853 6/853 9/85 12/85 3/86 6/86

Benzene 2.8 2.3 ND(5) N0(5) N0(5) ND( 10) Carbon Tetrachloride ND 1.6 ND(5l ND(ll ND(5l ND{5) Chloroform ND 0.6 ND(5 ND{l ND{5 ND(l)

1,1-Dichloroethene ND 0.2 ND(5) ND(l) ND(5) ND{l) -Trans-1,2-Dichloroethene 25.6 5.0/0.14 23.0M 90.0J 41.0 28.0 Tetrachloroethene 4.6 6.3 ND(5) 6.00J 5.00 4.00

Toluene 3.3 3 .1 ND(5) ND(5) N0(5) NO(S) Trichloroethene 545.4 330 690 1100.J 1200. 690 1,1,1-Trichloroethane ND 0.4 N0(5) ND{l) N0(5) ND(l)

1,2-Dibromoethane ND 0.042 ND(.02) N0(0.02) Acetone ND{ 100) ND( 10) ND( 10)

Notes Tfl)nly detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) Split samples were taken and analyzed by the State of Nebraska Department of Health Laboratories

(left column) and United States Environmental Protection Agency, Cincinnati, Ohio (right column). 4} The results presented are for Cis/Trans-1,2-Dichloroethene. 5) -, not analyzed for compound listed. 6) M - The value indicated is below the quantification limit but above the detection limit.

9/86

ND(0.2) 4.4 1.0

1. 5 ND(5)

ND(l.5)

ND(0.2) 182 8.0

ND(0.5)


Parameters

Carbon Tetrachloride

Tetrachloroethene

Trichloroethene

l,l,l-Tr1chloroethane

Notes



IRRIGATION WELL 1-46

9/85 12/85 3/86

ND(5} ND(l) 4.40

ND(5} 2,00J ND(l}

42.0 180J 54.0

ND(5) 2.00J ND(l}

ITTnly detected compounds are listed. 2) ND( ) - compound not detected at the level indicated. 3) -. not analyzed for compound listed. 4) NS - Not sampled.


6/86

NS

NS

NS

NS

TABLE 2-46

SUMMARY OF DETECTED VOLATILE ORGANIC COMPOUNDS IN GROUND WATER HASTINGS GROUND WATER CONTAMINATION SITE

Parameter

1,1,1-Trichloroethane


Tetrachloroethene

Ethylene Dibromide

Notes


HASTINGS AREA

Irrigation Well 1-49

12/85 3/86

7J ND(l)

32J 25.0

ND(l) 1.8

6.8

T}Only detected compounds are listed. 2) ND() - compound not detected at the level indicated.

6/86

2{J)

37(J}

ND(l)

3.7

3) Data reported as less than ( ) reported as received from Nebraska State Laboratories.


9/86

6.0

45.0

ND(l.4}

3.2

I) J - compound was qualitatively identified; however, compound failed to meet all QA criteria and, therefore, is only an estimated value

i) -, not analyzed for compound listed.

Contaminant


Trichloroethene

Tetrachloroethene

1,1-Dichloroethene

Toluene

Benzene

1,2-0ibromoethane

Notes

TABLE 3-1

CHEMICAL PROPERTIES OF CONTAMINANTS IDENTIFIED IN WELLS HASTINGS GROUND WATER CONTAMINATION SITE

So lubil ity1 Vapor1 Density1 in water at Pressure

20°c (mg/1} (gm/cm 3 ) ( tor rs}

785 1.5940 46.10

1100 1.4642 57.90

150 - 200 2.6227 7.79

400 1.218 591.0

535 0.8669 12.42

820 - 1780 0.87865 35.01

4300 2 .17 - 2 .18 6.449


log 2 Octanol/Water Partition

Coefficient

2.64

2.29

2.88

1.48

2.69

1.95 - 2.13

1. 76

~ Water Related Environme·ntal Fate of 129 Priority Pollutants, Volume I, NTIS No. PBB0-204373. Condensed Chemical Dictionary, 10th Edition, Revised by Gessner G. Hawley. 1982, Van Nostrand Reinhold Publishing Company, 1135 p.

Well No. Well Location

OW-ls T7NR9W8, NW, SE, SW OW-Id T7NR9W8, NW, SE, SW OW-2s T7NR9W8, NE, SE, SW OW-2d T7NR9W8, NE, SE, SW OW-3s T7NR9Wl8, NW, NE, NE OW-3d T7NR9Wl8, NW, NE, NE OW-4s T7NR9W7, SW, SE, SE OW-4d T7NR9W7, SW, SE, SE OW-5s T7NR10Wl2, SW, SE, SE OW-5d T7NR10W12, SW, SE, SE

M-3 T7NR10Wl3, NW, SW, NE M-7 T7NR9W8, SW, SW, NW M-10 T7NR10W12, SW, SE, SE M-11 T7NR10Wl2, SW, NW, SW M-12 T7NR9W8, NE, SE, SW M-15 T7NR9W7, NW, SE, NE M-18 T7NR9W7, SE, SE, SE

:MS-24 T7NR9Wl6, NW, NE, NE

'"CJ IN-9 T7NR9W8, NW, SE, SE ~ IN-10 T7NR10W12, NW, SW, SW 0 '-< !..;.} ....... fote '° 4'>- ~R--=- Not recorded

TABLE 3-2

PHYSICAL CHARACTERISTICS OF WELLS

Section: 3.0 Site: Hastings Revision: 0 Date: 05/07/87 Page: 3-13a

Ground Screen Elevation Well Casings Elevation Top Bottom Diameter

feet {NVGD} feet {NVGD} feet (NVGO} inches

1914 1790 1770 4 1914 1755 1745 4 1914 1790 1770 4 1915 1752 1742 4 1914 1800 1780 4 1914 1730 1720 4 1917 1800 1780 4 1917 1745 1735 4 1920 1800 1780 4 1920 1750 1740 4

NR 1800 1748 24 NR 1780 1725 24

1924 1801 1741 24 1934 1790 1738 24 1912 1751 1691 24 1905 1785 1713 24 1918 1796 1725 24

1906 1778 1708 17

1894 NR NR NR 1912 NR NR NR


Section: 3.0 Site: Hastings Revision: O Date: 05/07/87 Page: 3-13b

PHYSICAL CHARACTERISTICS OF WELLS SAMPLED IN DECEMBER 1985

Ground Screen Elevation Well Casings Elevation Top Bottom

Well No. Well Location feet (MSL) feet (NGVD) feet (NGVD)

1-49 T7NR9W9, SW, SE, SW 1910 1754 1689

D-8 T7NR9W16, NE, NW, NW Information Not Found

Note

NR - Not recorded

Log Information Obtained From:

'OW' wells - Fischer, A.J. and R.F. Spalding, 1985, Hastings Groundwater voe Investigation. 'I' wells - State of Nebraska, Irrigation Well Registration. 'IN' wells - Driller's logs, State of Nebrask Files. 'M,CMS' wells - State of Nebraska, Municipal Well Registration.

Diameter (inches)

NR

Appendix A

State Of Nebraska

rt>nitoring We11 Logs

PROJ3196

APPENDIX A

Logs of Monitoring Wells, Hastings, Nebraska . :

Field descriptions of drill samples and electric-log characteristics are the basis for these logs. Logs are arranged by monitoring well number followed by the field number. Color descriptions are for wet samples. Legal location is given followed by well identification number and field log number. · ·

SE~ Sh'~, Sec. 8, T. 7N:, R. 9W. (1, 2-8-84)

Location: 3rd Avenue, 100 feet north of railroad tracks. Ground altit~de: 1912 ft .. {Hastings East 7.5-minute quadrangle). Depth to water: 122 feet, Oct. 21, 1984

Depth, in feet i From To

Quaternary deposits Road fill • • • • • • • • • • • • • . ••. Clay, silty, dark-brown. • • . • • • • ••.•••• Clay, silty, dark-brown; sand is medium to coarse. Sand, gravelly; coarse sand to fine gravel .•.• Clay, pale-yellow; coarse sand .••.•••••• Clay, silty, pale-yellow; sand is medium to coarse Clay, silty, dark-brown; sand is very fine to medium Silt, yellow-brown; sand is very fine to coarse Sand, medium to coarse, yellow-brown .•..• Sand, fine to medium, ye 1 lo,,.,-brown; some s i 1 t • Sand, medium to coarse, some fine, yellow-brown .•.• Sand, medium, yellow-brown •.•••.•..•.•••••• Sand, fine to medium, yellow-brown; clay iron stained ••.• Gravel, sand, coarse sand to fine gravel, yellow .• Si l t, c 1 ayey . . . . . . . . . . . . . . . . . . . . Gravel, fine to medium, silt from 103-105 ••...• Sand, medium to coarse; fine gravel •••••••.•••.• Sand, fine to coarse; light-brown color; very fine gravel Sand, medium sand, light-brown; very fine gravel ..•. Si 1 t . . . . . . . . . . . . . . . . . . . . . . Sand, medium to coarse; very fine to fine gravel .... Silt, slightly clayey . • • . . . . • . • . . ••• Sand,. medium to coarse; very fine gravel ..•.•• Silt, slightly clayey ...........••.. Gravel, very fine to fine, with some medium to coarse sand Gravel, very fine to fine, with some medium to coarse sand;

iron stain silt from 211-215 ..•.

NE¼ SE¼ SW¼ Sec. 8, T. 7N., R. 9W. (2, 3-8-84)

. o· .. l

5 10 15 18 35 42 50 55 60 65 75 91 96

102 105 110 118 130 137 151 154 199 201

211

1 . 5

10 15 18

~ 35 42 50 55 60 65 75 91 96

102 - 105 - 110 - 118 - 130 - 137 - 151 - 154 - 199 - 201 - 211

235

Location: 28 feet SDuth of the intersection of East 2nd Street and 6th Avenue Ground altitude: 1911 ft. (Hastings East 7.5-minute quadrangle). Depth to water: 121 feet, Oct. 21, 1984

28 I PROJ3197

:.

(2, 3-8-84 continued)

Quaternary deposits Road fill ••••.••••...••• Clay, dark-brown • •••••.•.•.•.•. Clay, pale-brown •••••••.•• Clay, slightly sandy, yellowish-brown .•.••..•••.• Clay, dark-gray to dark-brown •••• Clay, slightly sandy, yellowish-brown .••••• Clay, slightly sandy, pale-brown; more sandy than above. Sand, very fine with some coarse, pale-brown to brown .• Sand, medium, yellowish-brown .••••••.•••••••• Sand, slightly silty; sand is very fine to fine, yellowish-

brown to -olive-brown ••••...•......... Sand, medium to coarse; gravel. fine to medium, some iron

staining . . . . . . . . . . . . . . . . . . . . Silt, light yellow-brown •••..••.•••.. Sand, fine to coarse; very fine to fine gravel .•••••. Silt, slightly clayey •••••••••••••••.•••• Sand, fine to medium; very fine to fine gravel, olive-brown Sand, very fine to coarse with fine to medium gravel with

shale fragments •..••..••..••.••••• Shale, light yellow-brown .••..•.••.•••••• Sand, very fine to coarse, with fine gravel, olive-brown

SE¼ N\,P. NE'. Sec. 18, T. 7N~, R. 9W. (3, l-B-84)

Oeeth, in From

0 1 3 5

23 30 37 45 55

65

86 -130 -136 -151 -153 -180 -195 -197 -

Location: Northeast corner of South Cedar Avenue and East "B" Street in Hanns Park. 59 ft. east of center of Cedar Avenue, 96 ft north of center of 11 811 Street.

Ground altitude: 1918 ft. (Hastings West 7 .5-minute quadrangle). Depth to water: 119 feet, Oct. 21, 1984

Quaternary deposits Clay, some sand; dark-brown •••••• Clay, silty, light-brown •••.•. Clay. silty, some sand; yellow .••..... Clay, silty; iron stained silt, pale-yellow Clay, silty; clay, dark-brown ••••••• Clay, silty, light yellowjsh-brown . . . . . • Clay, slightly sandy silt stringers, yellowish-brown •••• Sand, coarse sand with some silt, yellowish-brown .. Silt, slightly sandy, yellowish-brown ..••..•.. Sand, slightly silty; sand is fine to coarse, yellowish-

brown . . . . . . . . . . . . . . . . . . . . . . . . Sand, coarse to very coarse, with fine to medium gravel Cl ay, wh i te . . • . . . . • • • . • • • . . . Sand, gravel; medium to coarse sand with some fine, gravel

is fine to medium . . . . . . •.•. Silt, pale-brown • . . • • • . • • • . . . ••• Gravel, very fine to fine, some sand; clay from 140 ft to

142 ft. • • • • • • • • . • • ••••..

29

Deeth, in From

0 -3.5

5 10 19 22 30 37 57

60 78 89

94 -119 -126 -

feet To

1 3= 5

23 30 37 45 55 65

86

130 136 151 153 180

195 197 200

feet To

3.5 5

10 19 22 30 37 57 60

78 89 94

119 126

142

l pROJ3198

(3, 1-8-84 continued)

in feet Deeth, From To

Gravel, sand; very.fine gravel to fine gravel, sand is medium to coarse. • • • • • • • • • • .•••

Silt, slightly sandy • • • • . •••• Sand, medium to coarse •...•. Silt, slightly sandy • • • . . .•... Sand, gravel; medium to coarse sand with some very coarse,

very fine gravel, some silt •. • . • • . . ••• Silt, some clay, yellowish-brown .....••.••••.. Sand, some gravel; sand is medium to coarse. . . •.•

SW~ sw1 .. SP .. Sec. 7, T. 7N., R. 9W. (4, 5-8-84)

142 167 173 176

180 200 206

- 167 - 173 - 176

180

- 200 . - 206

- 220

Location: From South California Avenue, 389 feet east down railroad right of way and 100 feet south of Burlington Northern Railroad.

Ground altitude: 1916 feet (Hastings West 7.5 minute quadrangle). Depth to water: 122 feet, Oct. 21, 1984

Depth. in feet

Quaternary deposits Clay, some silt; clay dark-brown to black, from 2.3 feet to

5 feet light-brown to tan.clay ......•. ; C1ay, some si1t; clay is 1ight-brown to tan, iron stained

s i l t . . . . . . . . . . . . . . . . . · . . · · C1ay, some silt; clay is light-brown, some sand .•.•.•• C1ay, some silt; clay is light-brown with some sand stringers

very fine . . . . . . . . . . . . . . . . . . . . . Sand, some silt; sand is very fine to fine, light-brown to

tan s i l t . . . . . . . . . . . . . . . . . . . . . . Sand, fine to coarse, light yellowish-brown ••••••.•• Sand, gravel; sand is medium to coarse, gravel is fine to

very coarse . . . . . . . . . . . . . . . . . . . . . . . Si 1 t, iron stained • • ·• . • • . • • . . . . • • • • . • • • Sand, gravel; sand is medium to very coarse, reddish-brown,

· with very fine to very coarse gravel •••.••.• Silt, some sand; silt is brown to tan ......••. Sand, with gravel; sand is medium to coarse, yellowish-

brown . . . . . . . . . . . . . . . . . . . . . . . Silt, with some clay ................•. Sand, with gravel; sand is coarse to very coarse with some

medium, gravel very fine to coarse, yellowish-red Silt, with some clay ...•..........•...• Sand, with gravel; sand is coarse to very coarse; gravel

very fine to coarse, yellowish-red ..••..•... Silt, with some c1ay; yellowish-red •...••..... Sand, with grave1; sand is medjum to very coarse, yellow-

brown, with gravel being medium to very coarse Clay, some sand and s~ale; light yellowish-brown ..••

Cretaceous deposits Shale, pinkish-white . . . . . . . .

30

From To

0 5

5 20 20 35

35 50

50 i:-.,:,

55 80

80 - 101 101 105

105 - 130 130 - 135

135 - 151 151 - 153

153 - 182 182 - 185

185 - 197 197 - 199

199 - 214 214 - 230

71r,

pROJ3199

=

.

NE~ SE¼ SE~ Sec. 12, T. 7N., R. lOW. (5, 4-8-84)

Location: Across from Police station on Minnesota street, 111 feet west of·main rail of Burlington Northern railroad tracks.

Ground altitude: 1920 feet (Hastings !·Jest 7.5-minute quadrangle). Depth to water: 124 feet, Oct. 21, 1984 ·

Quaternary deposits Road fill • • . • • . ....••.•..• Clay, dark-yellow to dark-brown •..•.... Clay, yellowish-brown ..........•... Clay, with some sand and silt; yellowish-brown Clay, with some sand and silt. pale-brown .••. Silt, with fine sand, yellowish-brown ..•...•.•••• Sand, some silt; sand is fine to coarse, yellowish-brown Sand, gravel; sand is fine to coarse, with coarse gravel,

some iron stain ••••••••..•••••••••• Silt, some sand; silt is olive-yellow ..••••.•.... Sand, with gravel; sand is fine, yellow to yellowish-brown,

gravel is medium to coarse ...••...•••••.•• Si l t , some c 1 ay . • . . . . . • . . . . . . • • • • . • . . • Sand, with gravel; sand is very fine to coarse, gravel is

medium with some co3rse, yellowish-brown .•.••

31

Depth, From

0 I

15 20 35 65 70

86 98

110 157

165

in feet To

1 10 20 35 65 70 86

98 - 110

- 157 - 165

- 200

PROJ3200

:

Appendix B-1

Ground Water Analyses

May 1985

PROJ3201

ANALYSIS TYPE: ~OLATILE: ANALYSES .... . ..

TITLE: HASTINGS SHPT 2,3,4' MATRIX: WATER UNITS: UG/L LAB: ROC HETHOD: f~2~ CASE: 4'3•1 SAMPLE PREP: _______ ANALYST/ENTRY: ElB REVIEWER •.1 - .,. __ G:f5_ DATE: 06/10/SS

SAMPLE NUl'\BERS

ACL57001 ACL57002 ACL~7003 ACLS7004 CONPOUND t.:i • ,~ J.:· ts·'s- ! ~--(

..... . .

CHLOROMETHANE 10.0 u 10.0 u 200 u 10.0 u 1'kON01'1ETHANE 10.0 u 10.0 u 200 u 10.0 u VINYL CHLORIDE 10.0 u 10.0 u 200 u 10.0 u CHLOROETHANE 10.0 u 10.0 u 200 u 10.0 u METHYLENE CHLORIDE •t5.0 ,,.o .,o ~s.o ACETONE ..3.oo ti 10.0 u 110· '.fol ~.oo H CARBON Ill SULFit1E 5,00 u 5,00 u 100 u s.oo u 1 • 1 [1 I CHL OF:OETHENE 5.00 u 5,00. u 100 u s.oo u 1,1 [lICHLOF.:OETHANE s.oo u s.oo u 100 u s.oo u T~ANS-1,2,-DICHLOROETHENE 5,00 u 5,00 u 100 u s.oo u CHLOROFORM s.oo u :5,00 u 100 u s.oo u 1,2,DICHLOROETHANE s.oo u :s.oo u 100 u s.oo u ~-:E!UTANONE I I I 1,1,1 lRlCHLOROETHANE :i.oo u s.oo u sso ,g e.oo ~

CARBON TETRACHLORIDE ~.oo u s.oo u 100 u :i.oo u VlNYL ACETATE I 1 I :E!ROMODICHLOROMETHANE ~.oo u s.oo u 100 u :;.oo u 1,1,2,2,-TEiRACHLOROETHANE :;.oo u 5,00 u 100 u :;.oo u 1,2-DICHLOROfROPANE I I I TRANS-1,3-DICHLOROPROPENE s.oo u 5,00 u 100 u s.oo u TJ;.ICHLOROETHENE ~-1, 00 ti s.oo 4 ,,oo.· ,a 51 .o •J DIIROHOCHLOROMETHANE s.oo u s.oo u 100 u 5,00 u 1,1,:-TRICHLOROETHANE I I I

{l:ENZENE :;.oo u s.oo u ,2• .o H -~.oo CIS-1,3-DlCHLOROPROPENE :;.oo u !i. 00 u 100 u :;.oo u ~-'CHLOF.:OEiHYL VINYL ETHEf.: I I I ~F;OMOrOF;M 5.00 u 5,00 u 100 u 5.00 l 2 - HE>'. A tl DI~ E 10.0 u 10.0 u 200 u 10.0 l 4-MCTHYL-2-PENiANONE 10.0 u 10.0 u :?00 u 10.0 l JtTRA:H~O~OETHENE. 5,00 u :i.OO u ..!i:i. 0 M .:?. 00 I'

·iD!..UEN~ :;.oo u ~.oo u .3:?. 0: M '30. 0 CHLOR::if:ENZENE :;.oo u :i,00 u 100 u :;.oo l

·ETH'l'L U:NZENC :;.00 u 5.00 u 100 u .,.oo ST YRE::H: 5,00 u :i. 00 u 100 u 5.00 l TOTAL XYLENES :i,00 u ~.oo u 100 u 24.0

PROJ3202

ANALYSIS TYPE: ~OLATIL£:ANALYSES

TITLE: HASTINGS SHPT 2,3,4 t'lATRIX: WATER UNITS: UG/L LAB: ROC METHOI•: 952~0 ~ CASE: -43~1

~FLE P~EP: _______ ANALYST/ENT~Y: EJB REVIEWER:-~ --- _J,_ DATE: 06/10/85

SAMF'LE NUHBEF<S

ACLS700S ACLS7008 ACLfJ;09 ACL:i7010 COMPOUNI• ti5;,f{,J.,,j) ~ ~-; r~ • . ~ ,· ...... -

CHLOROHETHANE 10,0 u 10.0 u 10,0 u 10.0 u B"OHONETHANE 10,0 u 10.0 u 10,0 u 10.0 u VINYL CHLORII•E 10.0 u 10.0 u 10.0 u 10.0 u CHLOROETHANE 10,0 u I I I

,ttETHYLENE CHLORIDE 26,0 :23 .o .t• .o · 19.0 .ACETOtJE i..2 • 00 M r:'1 • 00 H .3. 00 H 10.0 u CARBO I~ I• I SLlL F IItE S,00 u :i,00 u S,00 u s.oo u 1,1 DICHLOROElHENE s.oo u :i,00 u :i,00 u 5,00 u 1,1 DlCHLOROETHANE S,00 u :i,00 u S,00 u 5,00 u TR At i S- 1 , 2 , - Ir I CH L Or: CE THEN E :;.oo u S,00 u S,00 u s.oo u

.CHLOti:OrOii:tf s.oo u s.oo u 1,00 l'I ~.oo u l,~,~ICHLOROETHANC s.oo u :i,00 u S,00 u 5,00 u

- :?-Bt.rTANONE 1 I I 1 ~1,1,1 ltlCHLOROETHANE :'5, 00 J 5,00 u S,00 u 5,00 u

CA~~ON TtTRACHLOF-:lDE s.oo u s.oo u ·aJ,O s.oo u 1.'IWl'L ACCTATE I I I J E~O~~~ICHLOROMETHANE s.oo u s.oo u S,00 u s.oo. u 1,1,:,~,-TETRACHLOROETHANE S,00 u s.oo u S,00 u !i,00 u 1,:-t!CHLOROf·ROrANE I I I l ~\.:, US - l , 2 - I: I CH L O 1' 0 F· RO F· ENE: S,00 u S,00 u s.oo u s.oo u •;;,: :1-n.Oi.OCTHE~:E :i:?. 0 J ,5. 00 1.00 t1 s.oo u LII~~MOCHLO~~METHANE s.co u s.oo u s.00 u s.oo u :,!,:-T~ICHlO~JClHANE I I I

~t-tt::r::r ,6. 00 .!? , 00 H 1.4,0- 1 ~ 00· H CIS-1,!-llCH~01'DP~CFEN£ s.oo u s.oo u S,00 u S. 00 u :-:~:.O~~ClHY~ VINYL ETHER l I I I- r~ :, ~~ :, ~ : : . !". S,00 u s.oo u s.oo u S,00 u :-;..::x:.~~~:;E 10.0 u I I ~ ~:T!-:i':..-~-rt~;iA~lOHE 10.0 u 10.0 u 10,0 u 10,0 u

~=1r .. ;:.:H:.. O~_O!THE:m: a.oo M S. 00 u S,00 u s.oo u :~:.. Jr~::: t'.33,0 :'t..00 ~2.0 f:! •· 00 M c::. :,~::I r:~:ztt~E s.oo u s.oo u S,00 u s.oo u c T ~Y:. f.~:::rm: ra. 00 ;1.00 M •.13 .. 0· s.oo u S1Yr.::::~:: '5.00 u s.oo u s.oo u !i. 00 t .. ,.. ~ .. XY;..tN::S '30. 0 ,:.. • 00 I'\ 45S,O ;? • c, 0 to: •. •...., . r • ._

PR.013203

ANALYSIS TYPE: ~O~A~iLf ANALYSES

1"1TLE: HASTINGS SHPT 2,J,4 NATRIX: WATER UNITS: UG/L LAB: ROC NETHOD: 952~£:(S CASE! 4341

~PLE PREP! _______ ANALYST/ENTRY: EJB RE~IEWER! --- -- -- DATE: 06/10/85

SAMPLE NUNBEl\:S

ACL:5'7011 ACLS?Ol:? ACLSJ01J f.iJ ~ r6: fil~

COHF'OUND

CHLOJ\OHETHANE 10.0 u 10.0 u 10.0 u l!ROMOMETHANE 10.0 u 10.0 u 10.0 u VINYL CHLORIDE 10.0 u 10.0 u 10.0 u CHLOF:DETHANE 10.0 u 10.0 u 10.0 u METHYLENE CHLORIDE I I I "CETONE t5.0 ,s.o .--22.0 CARBON DISULFII1E 5.00 u s.oo u s.oo u 1, 1 t1 I CHL OROETHENE s.oo u s.oo u s.oo u 1, 1 t1l CHLO~OETHANE s.oo u s.oo u 5,00 u TRANS-1,2,-DICHLOROETHEHE 5,00 u s.oo u s.oo u CHLOROFORM s.oo u s.oo u s.oo u

-- 1,2,DICHLOROETHANE :;.oo u 5.00 u s.oo u ~-t<UTANONE I I 1 ~,1,1 TRICHLOROETHANE .2.00 " s.oo u s.oo u CARIION TETRACHLORIDE 5,00 u s.oo u s.oo u Vlt~YL ACETATE I I l ~ROMO~ICHLOROMETHANE s.oo u s.oo u s.oo u 1,1,2,2,-TETRACHLOROETHANE s.oo u s.oo u 5,00 u , ,2-DlCHLOROFROPANE I I l

~ANS-1,3-DICHLOROPROPENE 5.00 u s.oo u s.oo u ,F.ICHLOROETHENE ·•.180 · ,e.o· 1•.0-~I~ROMOCHLOROMETHANE s.oo u :;.oo u S,00 u 1,1,2-TRICHLOROETHAHE I I I ,1-.CNZENE 2.00 H ,2·. 00 H 1-~oo 11 CIS-1,3-~ICHLOROPROPENE 5,00 u s.oo u 5,00 u 2-CHLOI\OETHYL VINYL ETHER l l I f;f\OMOrORM s.oo u s.oo u s.oo u 2-HEXt.iNONE I I I ~~METHYL~2-P£NTANONE 10,0 u a.oo. t'{ 10.0 u TETfi:ACHLOROETHEME .a.oo H s.oo u s.oo u -10LUENE ,t • 00 H ;2.06 H \3.00 H CHL01':0BENZENE s.oo u s.oo u S,00 u

-£THY!. ItENZENE ;I.. 00 H •. 2 • 00 M s.oo u STYF;ENE s.oo u s.oo u s.oo u

,1DTH!.. XYLENES ~.oo. H !4.00 M ~.oo;: H

PROJ3204 )

ANALYSIS TYPE: PESTICIDES

ilTLE: HASTINGS SHF'T 2,3,-4 PIATRIX: WATER UNITS: UG/L \I<: ROC KETHOD: 95~6c~ CASE: •341

.AMPLE PREF·: _______ ANALYST/ENTRY: E-41 REVIEWER: __ DATE: 06/10/8~

SAMPLE NUl'1.BERS ·z.::::. -z.D

AC~OOJ 'S'D

ACL57001 ACL:57002 ACL57O0"'1 CONPOUNI•

: :

ALPHA-BHC o.os u o.os u 0.05 u o.os l!ETA-BHC o.os u o.os u o.os u 0. OS IlELTA-BHC o.os u o.os u o.os u o.os GAMMA-E<HC o.os u o.os u o.os u o.os HEF'TACHLOR o.os u o.os u o.os u o.os ALIIRIN o.os u o.os u o.os u o.os HEF'TACHLOR Ef•OXIIJE o.os u o.os u o.os u o.os ENI10SULFAN l o.os u o.os u o.os u o.os I1IELI1R IN 0.1 u 0.1 u 0. 1 u 0.1 • ,~'-IlDE 0.1 u 0.1 u 0,1 u 0.1 £NI1R IN 0.1 u 0.1 u 0.1 u 0.1 ENI10SULFAN II 0.1 u 0.1 u 0.1 u 0.1 4', -1 • -r,rir, Ool u 0.1 u 0. 1 u 0.1 ENil!UN ALI1EHYI1E 0.1 u 0.1 u 0.1 u 0.1 ENI10SULFAN SULFATE 0.1 u 0.1 u 0.1 u 0.1 ~, • '-I1I1T 0.1 u 0.1 u 0.1 u 0.1 ENI1RI N KETONE 0.1 u 0. 1 u 0.1 u 0.1 t'IETHOXYCHLOR o.s u o.s u o.s u o.s C: H L OR It AN E o.s u o.s u o.s u o.s .' DXAF·HENE 1.00 u 1.00 u 1.00 u 1.00 u ARDCLOR-1016 o.s u o.s u o.s u o.s AROCLOR-1=21 o.s u o.s u o.s u o.s ;iF;OCLOR-1=3::? o.s u o.s u o.s u o.s ~f.DCLOR-1=4= o.s u o.s u 0. !:i u o.s A E O CLO F; - 1 ~ 4 8 o.s u o.s u o.s u o.s H ~- D CL OF; - 1 ::? ~ 4 1.00 u 1.00 u 1.00 u 1.00 u t. F; 0 CL O F: - 1 :? 6 0 1.00 u 1.00 u 1.00 u 1.00 L

PROJ3205

ANALYSIS TYPE: PESTICIDES

ilTLE: HASTINGS SHPT 2,3,. t\ATRIX: WATER AB: fi:OC

.AMPLE PREP: _______ ANALYST/ENTRY: E• l t1ETHOI1: 'i'S2.ll'IP~ S ~EVIEWER: -~M-

SAMF'LE NUHIIEF:S • ,

ACLS700S <=:::>D-~~

,

COl'iF'OUN[l

ALF'HA-BHC o.os u !IETA-BHC o.os u I1EL TA-I<HC o.os u GAMHA-I<HC o.os u HEF'i ACHLOR 0.05 u ALNUN o.os u HE F· TA CHLO R £F·OXII•E o.o:; u ENI10SULFAN I o.os u ItIELI•RIN 0.1 u <4,,_,_DI1E 0.1 u ENI1RI N 0.1 u ENI10SULFAN II 0.1 u 4, 4 '-I1I1ri 0,1 u £ N r, i:.: I N AL r, EH yr, E 0.1 u ENI10S ULF M~ SULFATE 0.1 u 4, 4 '-I1I1T 0.1 u EN It F: I N KET ONE 0.1 u HETHOXYCHLOR o.s u 'HLORI1ANC o.s u

TOXAF·HENE 1.00 u Ar. 0 CL OR - 1 0 1 6 o.s u Ar: 0 CLO R - 1 :? :? 1 0.:; u M:OCLOF-1.:!3:? o.s u M. u :L or:-1 :?4: o.s u I-, i: u: L O F' - l :? 4 S 0. :i u ?.i OCLC1R-1:~4 1.00 u AROCLOR-1:?60 1,00 u

T,..

UNITS: UG/L CASE: 4341 DATE: 06/10/8S

-- ANALYSIS TYF'E: 1'1ETALS (CONTRACTOR> • •

TITLE: HASTINGS NATRIX: WATER UNITS: UG/L LAB: RNA NETHOt1: 9001_1't~ (d..J. CASE: -4341 SAMPLE PREP: _______ ANALYST/ENTRY: E-42 ~EVlE~ER: ~- _ IIATE: 06/11/85

SAHPLE NUMBERS

ACLS7001 ACLS7002 ACL.S7003 ACLS700-4 COMPOUND z. s Zd ~ '::) s 'Sb

ALUl'tIHUN 200 u 200 u 37.0 H 200 u ANTll"IONY 60.0 u 60.0 u 60.0 u 60.0 u ARSENIC 10.0 u 10.0 u 10.0 u 10.0 u BARIUH • 1:iO H 170 H 120 H 140 M BERYLLIUM :;.oo u 5.00 u 5.00 u s.oo u CA!•t-UUM s.oo u s.oo u s.oo u S,60 CALCIUH 81000. 61000. 220000. :soooo. CHROMIUM 10.0 u 4.30 H 10.0 u 10.0 u COBALT so.o u so.o u so.o u so.o u COF·PER 6.90 H 8.60 H 6 • 10 t1 7.40 H IRON 38.0 M 53.0 H 230 :;1. 0 I'\ LEA!I s.oo u s.oo u s.oo u 2.60 H MAGNESIUM 13000. 10000. 32000. 8900. MANGANESE 15.0 u 7.40 H 130 7.60 H t'IEF.CURY 0.2 u 0.2 u 0.2 u 0.2 NICKEL 40.0 u •O.O u 9.40 t1 40.0 u f·OTASSIUM 9600. 8800. 15000. 7000. SELENIUH :;.oo u s.oo u s.oo u s.oo u SILVER 10.0 u 10.0 u 4.90 t1 10.0 ~

S0!1IUM 73000. 31000. 1soooo. 2•000. iHALLIUH 10.0 u 10.0 u 10.0 u 10,0 t.: i'IN 40,0 u 40.0 u 40.0 u -4 0. 0 L VANM!1IUH 8,90 M 6.90 M 9.90 M 6,00 ,. ZINC Jl.O 1:?0 soo 130 C '{ ANII•E 10.0 u 10.0 u 10.0 u 10.0 l

PROJ3207

TITLE: HASTINGS L.Afj: RMA

ANALYSIS TYPE: HETALS <CONTRACTOR>

SAMPLE P~EP: _______ ANALYST/ENTRY: E~:?

HATRIX: WATER 1'1ETHOtt: 9OO1t1~/ jr ~£VIEWER: _cz_f:-==-~

SAHF·LE NUMBERS • ,.

ACLS700S .,

COHPOUHD '":::> o-dv.p

ALUHINUH :?3.0 H ANTIHONY • 60.0 u ARSENIC 10.0 u :E'ARIUH 15(1 t1 :E'CRYLLIUH :i.00 u CA!tH I UI'\ 5.60 CALCIUM S:?000, CHROMIUM 10,0 u COE-ALT so.o u COF'f•ER ~:;.o IRON 88,0 H LEAII 62,0 HAGNESIUl'I 9;?00. MANGANESE 9,50 K HEF<CURY 0.:? u NICKEL 6,00 H f·OTASSIUH 6800. SELENIUM 2,10 H SILVER 10.0 u SODIUM :?4000. THALLIUM 10.0 u TIN ~o.o u VANADIUM 6,50 t1 ZINC l!jO CYANIDE 10,0 u

UNITS: UG/L CASE: '4341 DATE: 06/11/85

PROJ3208

ANALYSIS TYPE: SEl'!IVOLATILES < f·AGE 1)

iITLE: HASTINGS SHPT 2,J,<111 t!ATRIX: WATER UNITS: UG/L 1 AB: ROC METHOD: 9S2 U'I~ _k,!.$. CASE: .\341

H1F'LE PREP: _______ ANALYST/ENTRY: E39 REVlEWE~: ~- - - DATE: 06/10/8~

SAHPLE NUNBERS

• ACL5?001 ACLS700:? ACL=t?OOJ ACLS7004 COMPOUND 'Z.,.':, -z...D sS "SD -

N-NITROSODIHETHYLAMINE 10.0 u 10.0 u 10.0 u 10.0 u f·HENOL 10.0 u 10.0 u 10.0 u 10.0 u ANILINE 10.0 u 10.0 u 10.0 u . 10. 0 u ~IS<~-CHLOROETHYL> ETHER 10.0 u 10.0 u 10.0 u 10.0 u :?-CHL OROF'HENOL 10.0 u 10.0 u 10.0 u 10.0 u 1,3 I1 I CH L ORO E< E NZ ENE 10.0 u 10.0 u 10.0 u 10.0 u 1,4 I• l CHLOROBENZENE 10.0 u 10.0 u 10.0 u 10,0 u l<CNZYL ALCOHOL 10.0 u 10.0 u 10.0 u 10,0 u 1,: t1 I CHLO R OE< ENZ ENE 10.0 u 10.0 u 10,0 u 10.0 u ::!-l'IETHYLF'HENOL 10.0 u 10.0 u 10.0 u 10.0 u ~15(2-CH~OROISOPROPYL>ETHER 10.0 u 10.0 u 10.0 u 10.0 u 4-MCTHYLF'HENOL 10.0 u 10.0 u 10.0 u 10.0 u N-NlTROSO-DIPRDPYLAMINE 10.0 u 10.0 u 10.0 u 10.0 u HCXACHLOROETHANE 10.0 u 10.0 u 10.0 u 10.0 u NITRO!-ENZENE 10.0 u 10.0 u 10.0 u 10.0 LI l SDF·HORONE 10.0 u 10.0 u 10.0 u 10.0 L! :-NITROPHENOL 10.0 u 10.0 u 10.0 u 10,0 L! :,4-DIMETHYLPHENOL 10.0 u 10.0 u 10.0 u 10.c u r:t:,.•:oz r AC Ir, ~o.o u so.o u ~o.o u 6.00 r. fIS!:-CHLORDETHOXY) HETHANE 10.0 u 10.0 u 10.0 u 10.c u .: ' 4 I•! CHL.ORQF·HENOL 10.0 u 10.0 u 10.0 u 10.0 L! 1,=,4-TRlCH~OROtENZENE 10.0 u 10.0 u 10.0 u 10.0 l t•M HTHA~ENC 10.0 u 10.0 u 10.0 u lC•. 0 L 4 - C H !.. 0 f:: J A'., ! L I NE 10.0 u 10.0 u 10.0 u H•. 0 l HCXA:HLOR~B~TADIENE 10.0 u 10.0 u 10.0 L1 lO.O l ~-CHLOR0-3-~ETHYL~HENOL 10.0 u 10.0 u 10,0 LI 10.0 L :-M!:THYLNArHTHALENE 10,C'• u 10.0 u 10.0 u g·,,o L ~: !: ~; ;1: H L D f: 0 C Y Cl D F· ENT A !1 I ENE 10.0 u l 0. C• u 10.0 u 1 C·, Cl l :,~,t-T~!:H:..OROPHENOL 10.0 u 10.0 u 10.,::, u ! C, • 0 L ::~,~-T~lCHL.D~OPH[NOL :iO. 0 u ~o.o u ~-:-,. 0 11 ~C·. 0 L ... :-.CH~ or::iti,;~ HTHALE~lE 10.0 u 10.0 u 10.0 u l O, 0 l : - : ~ : i F. :, ,-, ! l l :.. 1 ~J ::: ~o.o u ~o.o u ~o.o Lt 5(·. 0 L l-:: ~ i:.: :~ Y L. f' HT H,;:.. HTC 10.0 u 10,0 u 10.0 LI l '::•, 0 t ,· I C r r l ,; : H T H t' L. ::: !l ~ 10.0 u 10.0 u 10.0 LI 1 C·. C L 3 - f~ ! ; :'~ 0 t1 ~~: - ! tJ;: :iO. 0 L! ~o.c u ~-,. 0 LI ~~.o l ,·.:r11.:., HTtil:rJ: 1':). 0 u 10.0 u 1 0. ,:) LI l O. 0 l :,4-DlNliR~f·H~NDL 10.0 u l ·:), 0 u 10.0 u :~.o t ·.-tJI H:OF'H[!.J_ ~--j. 0 u ~•:).0 LJ ~.,.,:, L' ~-=·. 0 1: I:CtJZOnm,:,:~ l C. ,:; u 10.0 u 10.0 LI lC·,O l :,4-~INIT~010U~CNC 10.0 u 10.0 u 10.0 LI 1 ~- • 0 l

PROJ3209

ANALYSIS TYPE: SEMIV0LATILES <PAGE 1>

TITLE: HASTINGS SHPT 2,3,~ ~B: f;:OC

NATRIX: WATER UNITS: UG/L

AHF'LE P~EP: _______ ANALYST/ENTRY: E39 t1£THO[i: 9:i2!"1Q.9 > CASE: 4'341 REVIEWER:-~-~~-- nATE: 06/10/85

COl"IF'OUNI•

N-NIT~OSODil"IETHYLAl"IINE F'J-:CNOL ANILINE ~15<2-CHLOROETHYL> ETHER :!- CHL OROF·HENOL 1•3 DICHLOROPENZENE l•4 DICHLOROE<ENZENE ICN:YL ALCOHOL ;,~ DICH~ORO~ENZENE :::--~CTHYLF'HENOL l!S<~-CHLOROISOP~OPYL>ETHER 4-ME THYLF'HCNCI:.. t · - ~ I T c. 0 5 0- t1 I F ;:; 0 F' Y L AH I NE HCXACHLOROETH~NE Nl Tf:U<[NZENC 1 S or-1-;or;ONE :!- t; l T f, D f· H C NOL 2•4-DI~ETHYLPHEN0L

ENZC•IC AC!I1 ~IS<~-CHLOROETHOXY) HETHANE :,4 DICHL0R0FHEN0L l,~,4-TRICHLORO~ENZENE NA F· HT HALE NE 4-CHLOROANILINE HEXACHLDROBUTADIENE 4-CHL0R0-J-METHYLPHEN0L 2-~ETHYLNAFHTHALENE HCXACHL0R0CYCLOPENTA0IENE ~,4,6-TRICHLOROPHENOL 2,4,S-TRICHLOR0fHEHOL 2-CHLORONAPHTHALENE :!-NlTROANILINE DIMCTHYLPHTHA~AlE ACE NAF·HT HYLENC 3-NITROANILlNE ACE NAF'HT HCNE 2,4-DINITROPHEHOL • -NlH:OPHEHDL L1 I r. t NZ OF UR AN ~,4-DINITR0T0ULENE

10.0 10,0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 50.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 ~o.o 10.0 50.0 10.0 10.0 50.0 10.0 10.0 50.0 10.0 10.0

SAMPLE NUMBERS

u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

PROJ3210

ANALYSIS TYPE: SENIVOLATILES <F~GE 2>

iITLE: HASTINGS SHPT 2,3,~ I AI<: ROC

AMPLE FREP: _______ ANALYST/ENTRY: E~O

COl'\POUNI•

~,6-DINIT~OTOLUENE DIETHYLFHTHALATE • -CHLOROPHENYL PHENYL ETHER 'F'LUOI\ENE • -NITROANILINE ~,6-DINITR0-2-METHYLPHENOL N-NITROSODIPHENYLAMINE ~-iROHOPHENYL PHENYL ETHER HCXACHLOROBENZENE PENTACHLOROPHENOL f· HE NA NT HRE NE ANTHRACENE DI-N-BUTYLPHTHALATE FLU01':ANTHENE l C: t,:: 1!1 I NC F YRE IJE ~UTYL JENZYL FHTHALATE 3,3' DlCHLOROBENZIDINE ! C tJ Z O C A ) ANT HR ACE NE

1sc:-ETHYLHEXYL)PHTHALATE -HF:Y:.l:i~C ~I-N~o:TYL PHTHALATE 1-- C 1 l Z D •: f. :, F" !.. U ~ R ANT HEN E 1: [ : ; : :1 •'. I; i i LU J RAH T HE NE !- r. 1:: :i ·: ,; ) F· Y F. t: ~l E IN~E~D~1,=,J-CD>PYRENE ~I~C:~Z~CA,H>ANTH~ACENE :. Ci;::. ·: G , H , ! > n:: F-: Y LENE

ACLS7001 -z.. '::>

10.0 10.0 10.0 10.0 so.o

.so.o 10.0 10.0 10.0 so.o 10.0 10.0 ~.oo

10.0 100

10.0 10.0 :?0. 0 10.0

9,00 10.0 10.0 10.0 10.0 10.0 10.c 10.0 10.0

u u u u u u u u u u u u M u u u u u u M u u u u u u u L!

NATRIX: WATER l1ETH0t1: 9521 N09,.- (S REVIEWE~: -~-f::::. __

SAl'IF'LE NUNBERS

UNITS: UG/L CASE: •3-41 DATE: 06/10/BS

ACL57002 ,z..D

ACL5'00J ACL:i7004

10.0 10.0 10.0 10.0 so.o so.o 10.0 10.0 10.0 so.o 10.0 10.0 10.0 10.0

100 10.0 10.0 ~o.o 10.0 lJ.O 10.0 10.0 10.0 10.0 10.0 10.0 10.0 10.0

u u u u u u u u u u u u u u u u u u u

u u u u u u u u

s:s 10.0 10.0 10.0 10.0 ~o.o so.o 10.0 10.0 10.0 :iO.O 10.0 10.0 J.oo

10.0 100

10.0 10.0 :?O. 0 10.0 10.0 10.0 10.0 10.0 10.0 10.0 1 C • c, 10. C: 10. C:

u u u u u u u u u u u u M u u u u u u

u u u u u u u u

SD

10.0 10.0 10.0 10.0 :;o.o :i0. 0 10.0 10.0 10.0 :i O • 0 10.0 10.0 10.0 10.0

100 10.0 10.0 ~o.o 10.0 19,0 10.0 10.0 10.0 10.c 10.0 1':).0 10.0 10.0

PROJ3211

u u u u u u u u u u u u LI u u u u u u

u u u u LI u LI u

ANALYSIS TYPE: SEKIVOLATILES <PAGE 2>

TITLE: HASTINGS SHFT ~,3,4 • r,l:: ROC

HPLE fREr: _______ ANALYST/ENTRY: E•O

:,6-DINITROTOLUENE ~IETHYLPHTHALATE 4-CHLOR• rHENYL PHENYL ETHER FL UOf,ENE 4- NI Tr, 0 ANILINE 4,6-DINITR0-2-METHYLPHENOL H-NITRCSODIFHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE FENTACHLOROPHENOL FHENANTHRENE ANTHRACENE I- I - N - ~ UT Y L F' HT H AL ATE F'l UOF:MJTHE~lC BENZlI• I NE F )'RENE ~UTYL ~CNZYL FHTHALATE 3,3' DICHLOROBENZIDINE -~N:O<A>ANTHRACENE

!Et2-ETHYLHCXYL)PHTH~LATE :HF. YSE NE I ; - 1, - 0 CT Y L F· HT HALAT E f:N:O<B>rLUOR~NTHENE l!~:D<K>FLUOR~NTHENE !- t t:: ti ( A) F Y F: E ~, E !NIENOCl,:,~-CD>PYRENE DIIr~:rr~,H:ANTHRA~E~C r i: l. Z (I •: ~ • H , I ) F· ER Y LENE

SAHF·LE

ACLS?00S -st:,- C>..i'

10.0 u 10.0 u 10.0 u 10.0 u so.o u so.o u 10.0 u 10,0 u 10.0 u ~o.o u 10.0 u 10.0 u 10,0 u 10,0 u

100 u 10.0 u 10.0 u 20.0 u 10.0 u 9,00 t1

10.0 u 10.0 u 10,0 u 10,0 u 10,0 u 10.0 u 10.0 u 10.0 u

NATF.:IX: WATER P'IETH• r,: 95211"100 REVIEWER: ~../:riJ_

HUHBERS I •

UNITS: UG/L CASE: •341 I•ATE: Oe/10/85

PROJ3212

Appendix B-2


September 1985

PROJ3213

ANALYSIS TYPE: VOt.ATJL.E ANALYSES

TITLE: HASTINGS HATRIY.: W"TER UNJTS: UG/L AB: ROC HETHOD: 9~2o..-~~ CASE: 4987

SAMPLE PREP: _______ ANALYST/ENTRY: E46 REVIEWER: - ---- Dl".TE: 04/08/86

SAHPLE NUHBERS

CKCS:?310 CKCS2312 CKCS2313 CKCS2314 COHPOUND

CHLOROHETHANE 20.0 u 20.0 u 20.0 u 20.0 ll BROHOHETHANE 10.0 u 10.0 u 10.0 u 10.0 lJ VINYL CHLORIDE 20.0 u 20.0 u 20.0 u 20.0 u CHLOROETHANE 10.0 u 10.0 u 10.0 u 10.0 u METHYLENE CHLORIDE .s.oo u s.oo u 6.00 u s.oo u ACETONE 10.0 u 10.0 u 10.0 u 10.0 u CARBON DISULFIDE s.oo u s.oo u s.oo u s.oo u 1, 1 I1ICHLOROETHENE s.oo u s.oo u s.oo LI s.oo u 1,1 DICHLOROETHANE s.oo u s.oo u s.oo u s.oo u TRANS-1,2,-DICHLOROETHENE s.oo u s.oo lJ s.oo u s.oo u CHLOROFORl1 s.oo u s.oo u s.oo u s.oo u 1,2,DICHLOROETHANE s.oo u s.oo u s.oo u s.oo u 2-BUTANONE l I I 1,1,1 TRICHLOROETHANE s.oo u s.oo u s.oo LI s.oo u CARBON TETRACHLORIDE s.oo u s.oo u s.oo u s.oo u VINYL ACETATE I I I BROMOD!CHLOROMETHANE s.oo u s.oo LI s.oo u s.oo u 1,1,2,2,-TETRACHLOROETHANE s.oo u s.oo u s.oo LI s.oo u 1,2-DICHLOROPRDPANE s.oo u s.oo u s.oo u s.oo u fRANS-1,3-DICHLOROPROPENE s.oo u s.oo u s.oo u s.oo u TRICHLOROETHENE s.oo u s.oo s.oo u s.oo u DIBROHOCHLOROHETHANE s.oo LI s.oo lJ s.oo u s.oo u 1,1,2-TRICHLOROETHANE s.oo u s.oo u s.oo ti s.oo u BENZENE s.oo u s.oo u s.oo u s.oo u CIS-1,3-D!CHLOROPROPFNE s.oo u s.oo u s.oo u s.oo u 2-CHLOROETHYL VINYL ETHER I I I BROHOFORM s.oo u s.oo u s.oo u s.oo u 2-HEXANONE 10.0 u 10.0 u 10.0 LI 10.0 u

.. 4-METHYL-2-PENTANONE 10.0 u 10.0 u 10.0 ll 10.0 u TETRACHLOROETHENE s.oo lJ s.oo u s.oo lJ s.oo u TOLUENE s.oo u s.oo u s.oo u s.oo u

1' CHLDROBENZENE s.oo u s.oo u s.oo lJ s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u STYRENE s.oo u s.oo u s.oo lJ s.oo lJ TOTAL XYLENES s.oo LI s.oo u s.oo u s.oo u

PROJ3214

ANALYSIS TYF'E: VOLATILE ANALYSES

LE: HASTINGS HATRIY.: WI\TER UNlTS: UG/L L..• .d: ROC HETHOD: 9~2~L.c'~ CASE': 4987 SAMPLE PREP: _______ ANALYST/ENTRY: E-16 RF.VIE~ER: - ------ D~TF.: 01\/08/86

SAMPLE NUHBERS

CKCS2302 CK.CS2303 CKCS2307 CKCS2309 COMPOUND

CHLOROHETH~NE 20.0 u 20.0 u 20.0 ll 20.0 u BROMOHETHANE 10.0 u 10.0 u 10.0 u 10.0 u VI_NYL CHLORIDE 20.0 u 20.0 u 20.0 u 20.0 u CHLOfi:OETHANE 10.0 u 10.0 u 10.0 u 10.0 u METHYLENE CHLORIDE s.oo u s.oo u 9,00 u s.oo u ACETONE 10.0 LI 10.0 u 10.0 LI 30.0 u CARBON DISULFIDE s.oo u 5,00 u s.oo u s.oo u 1,1 DICHLOROETHENE s.oo u s.oo u s.oo u s.oo u

i 1,1 DICHLOROETHANE s.oo u s.oo u s.oo u s.oo u

Ii TRANS-1,2,-DICHLOROETHENE 5,00 u s.oo u s.oo u s.oo u CHLOROFORM 5.00 u s.oo u s.oo u s.oo u

:j 1,2,DICHLOROETHANE 5.00 lJ s.00 u s.oo u s.oo u I 2-BUTANONE I I I

11 1,1,1 TRICHLOROETHANE s.oo u s.oo u s.oo u s.oo u

I' CARBON TETRACHLORIDE s.oo u s.oo u s.oo u s.oo u VINYL ACETATE I I I

r BROMODICHLOROHETHANE s.oo u s.oo u s.00 u s.oo u )1 ·,1,2,2,-TETRACHLOROETHANE s.oo ll s.oo u s.oo ll s.oo u

,2-DICHLOROPROPANE s.oo ll s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE s.oo u s.oo u s.oo ll s.oo u TRICHLOROETHENE' s.oo u s.oo u 60.0 42.0 DIBROMOCHLOROMETHANE s.oo u 5.00 u s.oo u s.oo u

II 1,1,2-TRICHLOROETHANE s.oo u s.oo u s.oo u s.oo u h BENZENE s.oo u s.oo u s.oo u s.oo u /, CIS-1,3-DICHLOROPROPENE s.oo u 5.00 u s.oo u s.oo u

II 2-CHLOROETHYL VINYL ETHE~ I I I BROMOFORH s.oo u 5,00 u s.oo \J s.oo u

·I. 2-HEXANONE 10.0 u 10.0 u 10.0 lJ 10.0 u 4-METHYL-2-PENTANONE 10.0 u 10.0 u 10.0 ll 10.0 u

111 TETRACHLOROETHENE s.oo u s.oo u s.oo \I s.oo u '\I TOLUENE s.oo u s.oo u s.oo u s.oo u ! ' /II CHLOROE<ENZENE s.oo u s.oo LI s.oo u s.oo u

ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u STYRENE s.oo lJ s.oo u s.oo u s.oo u TOTAL XYLENES s.oo u s.oo u s.oo u s.oo u

l PROJ3215

-------------.. - -·,--- -~- ..... -.·-.·-··· ....... .. . ,..

ANALYSIS TYF·E:

·.-~LE: HASTINGS -AB! ROC SAMPLE PREP: _______ ANALYST/ENTRY! E'°'S

CKC52223F -: COMPOUND

CHLOROHETHANE 20.0 u BROHOHETHANE 10.0 u VINYL CHLORIDE 20.0 u CHLOROETHANE' 10.0 u METHYLENE CHLORIDE 10. 0-ACETONE 9.00 M CARBON DISULFIDE s.oo tJ 1,1 DICHLOROETHE'NE s.oo u 1,1 t1 I CHLO RO ETHANE s.oo ll TRANS-1,2,-DICHLOROETHENE s.oo u CHLOROFORM s.oo u 1,2,DICHLOROETHANE s.oo u 2-BUTANON.E I 1,1,1 TRICHLOROETHANE s.oo u CARBON TETRACHLORIDE s.oo u VINYL ACETATE' I BROMODICHLOROMETHANE s.oo ll ·,1,2,2,-TETRACHLOROETHANE s.oo u

,2-DlCHLOROPROPANE s.oo ll TRANS-1,3-DICHLOROPROPENE' s.oo lJ

TRICHLOROETHENE s.oo u DIBROMOCHLOROHETHANE s.oo u 1,1,2-TRICHLOROETHANE s.oo u BENZENE s.oo u CIS-1,3-DICHLOROPROPENE s.oo u 2-CHLOROETHYL VINYL ETHER I 'BROMOFORli s.oo u 2-HEXANONE 10.0 u 4-METHYL-2-F'ENTANONE 10.0 u TETRACHLOROETHENE s.oo u TOLUENE s.oo u CHLOROBENZENE' s.oo u ETHYL I!ENZENE s.oo u STYRENE s.oo LI TOTAL XYLENES s.oo u

VOLAT1LE ANALYSES

HATRIY.! WA~ UN1TS: METHOD: 95 .l i(:.1.'l CASE! REV!F.~ER! _ -- Dl'\TE:

SAMF'LE NUMBERS

CKCS2224 CKCS2228

20.0 u 20.0 u lO.O u 10.0 u 20.0 u 20.0 u 10.0 u l O, 0 u s.oo LI ,.oo u

10.0 u 10.0 tJ 5.00 u s.oo u 5.00 u 5,00 u s.oo u s.oo lJ s.oo u S,00 ll s.oo LI S,00 u s.oo u s.oo u

I I S,00 u 1.00 H s.oo u s.oo u

I I s.oo LI 5,00 u s.oo u 5.00 u s.oo u s.oo ll s.oo ll 5,00 lJ s.oo u 3.00 K s.oo u s.oo LI s.oo u s.oo u s.oo u s.oo l1 s.oo u S,00 u

I I s.oo u s.oo u

10.0 u lO.O u 10.0 u 10,0 ll s.oo u s.oo u s.oo u s.oo ll s.oo LI 5,00 u s.oo ll s.oo lJ s.oo u ~LOO, u s.oo u s.oo u

PROJ32l6

UG/L 4987 04/08/86

CKCS2229

20.0 10.0 20.0 10.0 s.oo

10.0 s.oo s.oo s.oo s.oo 5,00 s.oo

s.oo 23.0

s.oo s.oo s.oo s.oo 3.00 5.00 5,00 s.oo s.oo

s.oo 10.0 10.0 s.oo s.oo s.oo s.oo s.oo s.oo

') :..,

u u u u u u u u u u u u

u

u u u u H u u u u

u u u u u u u u u

·ANALYSIS TYF·E: VOLATILE ANALYSES

... TTLE: HASTINGS HATRIX: Wh~ UNITS: UG/L 3: ROC METHOD: 95~ :'( CASE: 4987

SAMPLE PREP: _______ ANALYST/E'NTRY: E-\S REVIE.JE'R: __ 5?M. Itt:TE! Ot\/O8/86

SAHPLE NUMBERS

CKCS223'3F CKCS22'3'1 CKCS223'1D CKCS2:?34F ~ COMPOUND

CHLOROHETHANE 20.0 u 20.0 u ~o.o u 20.0 u BROHOHETHANE 10.0 u 10.0 u 10.0 u l. 0 • 0 u VINYL CHLORIDE 20.0 ll 20.0 u 20.0 u 20.0 u CHLOROETHANE 10.0 u 10.0 u 10.0 u 10.0 u METHYLENE CHLORIDE 10.0 s.oo u s.oo u 5.00 ACETONE 9.00 H 10.0 u 10.0 u 4.00 H CARBON DISULFIDE s.oo u s.oo u s.oo u s.oo u 1,1 DICHLOROETHENE s.oo u s.oo u s.oo u s.oo u 1, 1 DICHLOROETHANE s.oo u 5 • 00 u s.oo u s.oo u TRANS-1,2,-DICHLOROETHENE' s.oo u s.oo u s.oo u s.oo u CHLOROFORM s.oo u s.oo u 5.00 u s.oo u 1,2,DICHLOROETHANE s.oo u s.oo lJ s.oo u s.oo u 2-BUTANONE 2.00 H I I 1,1,1 TRICHLOROETHANE s.oo u s.oo u s.oo u s.oo u CARBON TETRACHLORIDE s.oo u s.oo u s.oo u s.oo u VINYL ACETATE I I I BROMODICHLOROMETHANE s.oo u s.oo u s.oo u s.oo u 1,1,2,2,-TETRACHLOROETHANE s.oo ll s.oo u s.oo ti s.oo u

2-DICHLOROPROPANE s.oo u s.oo u s.oo u 5,00 u . ,,ANS-1, 3-I:iI CHLOROF'ROPENE s.oo u s.oo u s.oo lJ s.oo u

TRICHLOROETHENE s.oo u s.oo u s.oo u s.oo u DIBROMOCHLOROMETHANE s.oo u s.oo u s.oo lJ s.oo u 1,1,2-TRICHLOROETHANE s.oo u s.oo u s.oo u s.oo u BENZENE s.oo u s.oo u s.oo ll s.oo u CIS-1,3-DICHLOROPROPENf s.oo u s.oo u s.oo u s.oo u 2-CHLOROETHYL VINYL ETHER I I I BROHOFORH s.oo u s.oo u s.oo u s.oo u 2-HEXANONE 10.0 u 10.0 u 10.0 u 10.0 u 4-METHYL-2-PENTANONE 10.0 u 10.0 ti 10.0 u 10.0 u TETRACHLOROETHENE s.oo u s.oo u s.oo LI s.oo u TOLUENE 2.00 H s.oo u s.oo u s.oo u CHLOROBENZENE s.oo u s.oo u s.oo lJ s.oo u ETHYL BENZENE s.oo u s.oo ll s.oo lJ s.oo u STYRENE s.oo u ,5,00 u s.oo u s.oo u TOTAL XYLENES s.oo ll s.oo u S,00 u s.oo u

I PROJ3217

ANALYSIS TYPE: VOLATILC ANALYSES

TITLE: HASTINGS MATRIX: ~ UNITS: UG/L LAB: ROC METHOD: 91."." _ ~ CASE: 4907 ~AMPLE PREP: _______ ANALYST/ENTRY: E4S RCVIEWER: ____ J_ DATE: 04/08/86

SAMPLE NUMBERS

CKCS2301 Cl<CS2308 CKCS2316 Cl{CS2317 COMPOUND

':'

CHLOROMETHANE 20, 0 u 20,0 u 20,0 u 20.0 u BROMOHETHANE 10.0 u 10,0 u 10.0 u 10.0 u VINYL CHLORIDE 20,0 -u 20,0 u 20.0 u 20.0 u CHLOROETHANE 10,0 u 10.0 u 10,0 u 10.0 u METHYLENE CHLORIDE 5, 00 u 7, 00 u S, 0 0 u 5.00 u ACETONE 10.0 u 10 I 0 u 10.0 u 1 0 , 0 u CARBON DISULFIDE S, 00 u s.oo u S. 0 0 u S. 0 0 u 1,1 DICHLOROCTHENE S, 00 u 4.00 M S. 00 u S, 00 u 111 DICHLOROCTHANE s I 00 u s.oo u S. 0 0 u S. 0 0 u TRANS-1,2,-DICHLOROCTHENC s I 00 u S. 00 u S. 00 u ~, 0 0 u CHLOROFORM s.oo u s. 00 u S. 00 u S. 00 u L, 2, DI Cl ILOR OETHANE s.oo u s.oo u s. 00 u s.oo u

- 2-BUT~,NONE I I I I 1,1,1 TRICHLOROETHANE S, 00 u 22,0 S. 00 u s.oo u CARBON TETRACHLORIDE s.oo u s.oo u S, 00 u S. 00 u VINYL ACETATE I I I I BROMODICHLOROMETHANE S, 00 u s.oo u S, 00 u S. 00 u 1,1,2,2,-TETRACHLOROETHANE S,00 u S. 00 u s.oo u S, 00 u I. ,2-DICHLOROPROPANE s.oo u s.oo u s.oo u s.oo u TRANS-1,3-DICHLDROPROPENE s.oo u S, 00 u S. 00 u s.oo u

"'lCHLOROETHENE S, 00 u iS0 s. 00 u s.oo u ~!BROMOCHLOROMETHANE S, 00 u S, 00 u S,00 u s.oo u L,1,2-TRICHLOR0ETHANE 5. 00 u s.oo u S, 00 u S, 00 u JiENZENE s.oo u s.oo u s.oo u s.oo u CIS-1,3-DICHLOROPROPENE 5, 00 u S,00 u S, 00 u s.oo u 2-CHLOROETHYL VINYL ETHER I I I I !<ROMOrORM s.oo u s. 0 0 u S, 0 0 u S. 00 u 2-HEXANONE 10.0 u 10,0 u 10,0 u 10.0 u 4-METHYL-2-PENTANONE 10.0 u 10,0 u 10.0 u 10,0 u TETRACHLOROETHENE S, 00 u 2, 00 M S. 00 u s.oo u TOLUENE s. 00 u s.oo u S, 00 u S. 0 0 u CHLOROI'.IE:NZENE s. 00 u s.oo u s.oo u S. 00 u ETHYL BENZENE 5.00 u s.oo u s.oo u s. a o u STYRENE S. 00 u S, 00 u S. 0 0 u S, 0 0 u TOTAL XYLENES s.oo u s.oo u s.oo u S. 0 0 u

H _ PROJ3218

··---·- .... _ - -- ------ ·----~----•·•--- -.. -c•----. --~ ... _. -~ .. -.,. ..... -.. , ...... - - -....... -~

AHAL·YSIS TYPE: VOL.AT ILE' AHAL YSES

TITLE: HASTINGS MATRIY.: WhTtit . UNITS! UG/L HETHOfl ! 95 l CASE! 4987 :..AB! ROC RF.VIEWER: _ rt+~ /

ANALYST/ENTRY! DflTE: SAMPLE PREP: _______ E-16 01/08/86

SAMPLE NUMBERS

CKCS2210 CKCS2211 CKCS2212 CKCS2213 -COMPOUND

CHLO ROH ETHANE 20.0 u 20.0 u 200 u 20.0 u BRDMOMETHAHE 10.0 ll 10.0 lJ 100 u 10.0 u VINYL CHLORIDE 20.0 u 20.0 u 200 u 20.0 u CHLOROETHANE 10.0 u 10.0 u 100 u 10.0 u METHYLENE CHLORIDE s.oo u s.oo u ~o.o u s.oo u ACETONE 10.0 u 10.0 u 100 u 10.0 u CARBON DISULFIDE s.oo u s.oo u so.o u s.oo u 1, 1 DICHLOROETHENE s.oo u s.oo u so.o u s.oo u 1,1 DICHLOROETHAHE s.oo u s.oo u so.o u s.oo u TRANS-1,2,-DICHLOROETHENE s.oo u s.oo u 23.o M s.oo u CHLOROFORM s.oo LI s.oo u so.o u s.oo u 1,2,DICHLOROETHAN~ s.oo LI s.oo u so.o u s.oo u 2-BUTANONE I I I I 1 , 1 , 1 TRICHLOROETHANE s.oo LI 5,00 u so.o u s.oo u CARBON TETRACHLORIDE 1.00 H s.oo u so.o u s.oo u VINYL ACETATE I I I I BROHODICHLOROMETHANE 5,00 u s.oo LI so.o u S,00 u 1,1,2,2,-TETRACHLOROETHANE s.oo lJ s.oo u so.o u s.oo. u 1,2-DICHLOROPROPANE s.oo u s.oo u so.o u S,00 u TRANS-1,3-DICHLOROPROPENE s.oo u s.oo u so.o lJ s.oo u TRICHLOROETHENE s.oo ll s.oo II 690 ~.oo u DIBROMOCHLDROHETHANE s.oo LI s.oo u 50.0 u s.oo u 1,1,2-TRICHLOROETHANE s.oo u s.oo u so.o u s.oo u BENZENE s.oo u s.oo u so.o u s.oo u

'.. CIS-1,3-DICHLOROPROPENE s.oo u s.oo lJ so.o LI s.oo u 2-CHLOROETHYL VINYL ETHER I I I I BROM OF ORM s.oo u s.oo u !jO.O u s.oo u 2-HEXAHONE 10.0 LI lO.O lJ 100 LI 10.0 u 4-NETHYL-2-PENTAHONf 10.0 u 10.0 u 100 u 10.0 u

-~ETRACHLOROETHENE s.oo ll s.oo u 50,0 u s.oo u TOLUENE s.oo u s.oo u so.o u s.oo u CHLOROBENZENE s.oo u 5,00 u so.o u s.oo u ETHYL BENZENE s.oo u s.oo lJ so.o u s.oo u STYRENE s.oo lJ s.oo u so.o u 5,00 u TOTAL X'fLENES s.oo u s.oo u so .o LI s.oo u

-PROJ3219 l

ANALYSIS TYPE: VOLATILE ANALYSES

TITLE: HASTINGS HATRIX: ~ UN!TS: UG/L LAB: ROC HETHOn: 9" 2 ,~c__i.:[_ CASE: 4987 SAHPLE PREP: _______ ANALYST/ENTRY! E-15 RF.VIEWER• - - I'lt'\TE ! 01/08/8~

SAMPLE NUMBERS

: _, CKCS221SF CKCS2218 Ct<CS2219 CKCS222C - COMPOUHD

CHLOROHETHANE' 20.0 u 20.0 u 20.0 u 20.0 BROHOHETHANE 10.0 u 10.0 LI 10.0 lJ 10.0 VINYL CHLORIDE 20.0 u 20.0 u 20.0 lJ 20.0 CHLOROETHANE 10.0 u 10.0 u 10.0 u 10.0 METHYLENE CHLORIDE s.oo u s.oo u s.oo u s.oo ACETONE 6.00 H 10.0 u 10.0 u 10.0 CARBON DISULFIDE s.oo u s.oo LI s.oo lJ s.oo 1,1 DICHLOROETHENE s.oo u 5.00 u s.oo u s.oo I

1,1 DICHLOROETHANE s.oo u s.oo u s.oo u s.oo I

TRANS-1,2,-DICHLOROETHENE s.oo u s.oo u s.oo u s.oo I CHLOROFORM s.oo u 5.00 u s.oo LI s.oo l 1,2,DICHLOROETHANE s.oo u s.oo u s.oo u s.oo l 2-BUTANONE I . I I 1,1,1 TRICHLOROETHANE s.oo u s.oo LI s.oo LI s.oo l CARBON TETRACHLORIDE s.oo u· s.oo u s.oo u s.oo L VINYL ACETATE I I I BROHODICHLOROHETHANE s.oo u s.oo LI s.oo lJ s.oo lJ 1,1,2,2,~TETRACHLOROETHANE s.oo u s.oo u s.oo u s.oo u 1,2-DICHLOROPROPANE s.oo u s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE s.oo u s.oo u s.oo LI s.oo u TRICHLOROETHENE s.oo LI s.oo u s.oo ll 2.00 H DIBROHOCHLOROHETHANE s.oo u s.oo u s.oo u s.oo u 1,1,2-TRICHLOROETHANE s.oo u s.oo ll s.oo u s.oo u BENZENE s.oo u s.oo LI s.oo u s.oo u CIS-1,3-DICHLOROFROPENE s.oo u s.oo u s.oo u s.oo u 2-CHLOROETHYL VINYL ETHER I I I BROHOFORH s.oo u s.oo u s.oo u s.oo u 2-HEXAHONE 10.0 u 10.0 u 10.0 u 10.0 u 4-HETHYL-2-PENTANONE 10.0 u 10.0 u 10.0 u 10.0 u TETRACHLOROETHtNE ~.oo LI s.oo u s.oo u s.oo u TOLUENE s.oo u s.oo u s.oo u s.oo u CHLOROBENZENE s.oo u s.oo LI s.oo u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo lJ 5,00 u STYRENE s.oo u s.oo u s.oo u s.oo u TDTAL.XYLENES s.oo u. s.oo LI s.oo ll s.oo u

PROJ3220 ··------ '----------~------.. --------_,,......., ... ,.~-~~. ~ ---·--:-- ..... --:-•.-":-~. - J .....

ANALYSIS TYPE: VOLATilc ANALYSES

TITLE: HASTINGS HATRIY.: W~ UNITS: UG/L LAB: UHL METHOD: 9 ,'2 CASE': 4987 SAMPLE PREP: _______ ANALYST/ENTRY: E-12 RE'v·r El>IE'R: C?.__1.::1 DATE: 0'1/08/86

SAMPLE NUMBERS

CKCS2201 CKCS2202 CKCS2203 r.~;cs2204 COMPOUND

CHLOROMETHANE 10.0 ll 10.0 lJ 10.0 u 10.0 u BROMOHETHANE 10.0 .u 10.0 u io.o ll 10.0 u VINYL CHLORIDE 10.0 u 10.0 u 10.0 ll l O. 0 u CHLOROETHANE 10.0 u 10.0 u 10.0 u 10.0 u METHYLENE CHLORIDE 32.0 s.oo ll s.oo u s.oo u ACETONE 10.0 u 10.0 u 10.0 u 10.0 u CARBON DISULFIDE s.oo u s.oo u s.oo u s.oo u 1, 1 DICHLOROETHEHE s.oo u s.oo ll s.oo u s.oo u 1,1 DICHLOROETHANE s.oo u s.oo u s.oo LI s.oo u TRANS-1,2,-DICHLOROETHENE s.oo u 5,00 u s.oo ll s.oo u CHLOROFORM s.oo u s;oo u s.oo u 5,00 u ~,2,0ICHLOROETHANE s.oo u s.oo u s.oo u s.oo u 2-BUTANONE I I I I 1 ,1, 1 TRICHLOROETHANE s.oo u s.oo LI s.oo u s.oo u CARBON TETRACHLORIDE s.oo u s.oo u s.oo u s.oo u VINYL ACETATE 10.0 ll 10.0 u lO,O u 10.0 u BROHODICHLOROHETHANE s.oo u s.oo LI s.oo LI s.oo u 1,1,2,2,-TETRACHLOROETHANE s.oo u s.oo u s.oo LI s.oo u 1,2-IIICHLOROPROPANE s.oo ll s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE s.oo ll s.oo u s.oo u s.oo u TRICHLOROETHENE 3.20 H 30.0 13.0 92.0 DIBROMOCHLOROMETHANE s.oo LI s.oo u s.oo lJ s.oo u 1,1,2-TRICHLOROETHANE s.oo u s.oo u s.oo u s.oo u BENZENE s.oo u s.oo u s.oo tJ s.oo u CIS-1,3-DICHLOROPROPENE s.oo u s.oo lJ s.oo ll s.oo u 2-CHLOROETHYL VINYL ETHER 10.0 u 10.0 u 10.0 u 10.0 u BROMOFORli s.oo LI s.oo u s.oo ll s.oo u 2-HEXANONE 10.0 u 10.0 lJ 10.0 LI l O, 0 u 4-METHYL-2-PENTANONE 10.0 u 10.0 u 10.0 lJ 10.0 u TETRACHLOROETHENE s.oo ll s.oo u s.oo u s.oo u TOLUENE s.oo u s.oo ll s.oo u s.oo u CHLOROBENZENE s.oo u s.oo u s.oo u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u STYRENE s.oo u s.oo Lt s.oo u s.oo u TOTAL XYLENES s.oo u s.oo u s.oo ll s.oo u

PROJ3221 ______ .,._..,... _______ . ....,..----·~~•·•·•~•-,••·• ... -. - ··•·. - ... ':'._ r;~-•."

ANALYSIS TYf'E: VOLATILE ANALYSES

fITLE: HASTINGS MATRIX: Wf\TER UNITS! UG/L _AB: ROC METHon: 95~~L{ CASE: 4987 Sf '.E f'REF·: ------- ANALYST/ENTRY: E-16 REVIEWER: .... _ --~ It ATE: 04/08/86

SAMf'LE NUMBERS

CKCS2227 CKCS2230 CKCS2231 CKCS2301D COMPOUND

CHLOROMETHANE 20.0 LI 20.0 LI 20.0 u 20.0 u BROMOHETHANE 10.0 LI l0.0 ti 10.0 lJ lO.O u VINYL CHLORIDE 20.0 LI 20.0 LI 20.0 LI 20.0 u CHLOROETHANE 10.0 u l0.0 u 10.0 LI 10.0 u METHYLENE CHLORIDE 7.00 LI s.oo u s.oo LI s.oo u ACETONE 10.0 u 10.0 lJ 10.0 u 10.0 u CARBON ItISULFIItE s.oo u s.oo u s.oo lJ s.oo u 1, 1 DICHLOROETHF.NE 5.00 u s.oo u s.oo u s.oo u 1, 1 DICHLOROETHANE s.oo LI s.oo u s.oo LI s.oo u TRANS-1,2,-DICHLOROETHENE 5.00 lJ 5.00 LI s.oo u s.oo u CHLOROFORM s.oo u s.oo u s.oo u s.oo u 1,2,DICHLOROETHANE s.oo LI s.oo u s.oo lJ s.oo u 2-BUTANONE I I I I 1 , 1 , 1 TRICHLOROETHANE s.oo LI s.oo u 5.00 u s.oo u CARBON TETRACHLORIDE s.oo lJ s.oo LI s.oo u s.oo u VINYL ACETATE I I I I BROMDDICHLOROMETHANE s.oo LI s.oo u s.oo lJ 5.00 u 1,1,2,2,-TETRACHLDROETHANE s.oo u 5.00 LI s.oo u s.oo u 1 1-DICHLOROf'ROPANE s.oo lJ s.oo u s.oo u 5.00 u

'S-1,3-DICHLORDPRDF'ENF. s.oo u s.oo LI s.oo u s.oo u TR.1.CHLORDETHENE 4.00 M s.oo LI 2;i0 s.oo u DIBRDHOCHLORDMETHANE 5.00 lJ 5.00 u s.oo LI s.oo u 1,1,2-TRICHLOROETHANE s.oo LI s.oo u s.oo u 5.00 u E:ENZENE s.oo LI s.oo u 48.0 s.oo u CIS-1,3-ItICHLOROf'ROf'ENE s.oo u s.oo u s.oo u s.oo u 2-CHLOROETHYL VINYL ETHER I I I I BROMOFORM s.oo LI s.oo u s.oo LI s.oo u 2-HEXANONE 10.0 lJ 10.0 LI l0.0 u 10.0 u 4-METHYL-2-PENTANONE 10.0 LI 10.0 LI 10.0 LI 10.0 u TETRACHLDRDETHENF. s.oo LI s.oo lJ 3.00 M s.oo u TOLUENE s.oo u s.oo LI s.oo lJ 5.00 u CHLOROBENZENE s.oo LI s.oo u 5.00 LI s.oo u ETHYL BENZENE s.oo LI s.oo LI s.oo u s.oo u STYRENE s.oo u s.oo u s.oo lJ s.oo u TOTAL XYLENES s.oo LI s.oo LI s.oo lJ s.oo u

PROJ3222

ANALYSIS TYPE: VOLATILE flNf'lLYSES

"ITLE: HASTINGS MATRIX: WI•~ UNITS: UG/L .AB: ROC METHOfl: 9!'" ,, MOO~ CASF:: 4987 3A . PREF': _______ ANALYST/ENTRY: E46 RF.VIEWER: _ ~- _____ I:1(\TE: 04/08/86

SAMPLE NUMBERS

CKCS2216 CKCS2217 CKCS2226 CKCS2226D COMF·OUND

CHLOROMETHANE 20.0 u 20.0 lJ 2()0 u 200 u BROMOMETHANE 10.0 u 10.0 u l00 u 100 u VINYL CHLORIDE 20.0 u 20.0 u 200 u 200 u CHLOROETHANE 10.0 u 10.0 lJ 100 u 100 u METHYLENE CHLORIDE 5.00 LI s.oo LI 52.0 u 32.0 u ACETONE 10.0 u 10.0 LI 71.0 u 13.0 u CARBON DISULFIDE 5.00 LI s.oo u 50.0 u ~o.o u 1 , 1 DICHLOROETHENE 5.00 u s.oo u so.o u 50.0 u 1 , 1 t1 I CHLOROETHANE s.oo l1 s.oo u 50.0 u ~;o. o u TRANS-1,2,-DICHLOROETHENE s.oo u s.oo LI 50.0 u 50.0 u CHLOROFORM s.oo LI 5.00 LI 50.0 u 50.0 u 1,2,DICHLOROETHANE s.oo LI s.oo u 50.0 u ~,o. o u 2-BUTANONE I I I I 1 , 1 , 1 TRICHLOROETHANE s.oo u 5,00 LI 19.0 H 1 B. 0 M CARBON TETRACHLORIDE 5,00 l.l 5,00 lJ so.o ll 5'0. 0 u VINYL ACETATE I I I I BROMODICHLOROMETHANE s.oo u 5,00 u 50.0 u 50.0 u 1,1,2,2,-TETRACHLOROETHANE 5.00 u s.oo u 50.0 u 50.0 u l DI CHLOROF'ROPANE s.oo u s.oo lJ so.o u 50.0 u 1. 3-1,3-DICHLOROPROPENE 5,00 u s.oo u 50.0 LI 50.0 u TF: I CHLDROE TH ENE 5,00 u s.oo LI 1-100. 1400. DIBRDMOCHLOROMETHANE 5,00 lJ s.oo u 50.0 u 50.0 u 1,1,2-TRICHLOROETHANE 5,00 LI s.oo u 50.0 u 50.0 u BENZENE s.oo LI 5.00 u so.o LI 50.0 u CIS-1,3-DICHLOROPROPENE 5.00 u s.oo LI 50.0 u so.o u 2-CHLOROETHYL VINYL ETHER I I I I BROMDFORM s.oo u 5,00 u 50.0 u so.o u 2-HEXANONE 10.0 ll l0.0 LI 100 u l 00 u 4-METHYL-2-PENTANDNE 10.0 u 10.0 u 100 u 100 u TETRACHLOROETHENE 5.00 lJ 5.00 u 3t.. 0 H :.:z:~.o M TOLUENE 5.00 u 5.00 LI 50.0 u 50.0 u CHLOROBENZENE 5,00 LI 5.00 LI 50.0 lJ 50.0 u ETHYL BENZENE 5.00 u 5.00 LI 50.0 u 50.0 u STYRENE 5.00 LI 5.00 u so.o LI 50.0 u TOTAL XYLENES 5.00 u 5,00 u ·so, o LI 50.0 u

PROJ3223

ANALYSIS TYF·E: VOLATILE ANALYSES

TITLE! HASTINGS HA1RIX: ~ UNITS: UG/L LAB: UHL METHOI1: 9.~i2 . l,: CASE: 4987 -~lo\PLE f'Fi:EP: _______ ANALYST/E'NTRY: E'12 REVIEWER . __ ft}_ __ :"'[ TttiTE': 0-1/08/86

SAMF·LE NUMBERS

CKCS2209 CKCS2304 CKCS2305 CKCS2306 COMPOUND

CHLOROMETHANE 10.0 LI 10.0 u 10.0 l I lO.O u BROMOMETHANE 10.0 LI l0.0 u 10.0 LI 10.0 u VINYL CHLOFi:IttE 10.0 u 10.0 lJ 10.0 LI 10.0 u CHLOROETHANE 10.0 u 10.0 LI 10.0 lJ l.O. 0 u METHYLENE CHLORIDE 5.00 LI 6.90 LI s.oo u s.oo u ACETONE 10.0 LI 10.0 u 10.0 LI 10.0 u CARBON DISULFIDE s.oo LI s.oo lJ s.oo u 5.00 u 1 , 1 DICHLOROETHENE 5.00 u s.oo \j s.oo ll s.oo u 1, 1 r, I CH L DR OE THANE s.oo LI s.oo u s.oo lJ 5.00 u TRANS-1,2,-DICHLORDETHENE s.oo LI s.oo u s.oo u s.oo u CHLOROFORM s.oo LI s·.oo LI s.oo u s.oo u 1,2,DICHLORDETHANE s.oo u s.oo u s.oo u s.oo u 2-BUTANONE 1 1 I l 1 , 1 , 1 TRICHLOROETHANE' s.oo ll s.oo lJ s.oo u s.oo u CARBON TETRACHLORIDE s.oo u s.oo u 5.00 u s.oo u VINYL ACETATE 10.0 lJ 10.0 \) 10.0 u 10.0 u BROMODICHLOROMETHANE s.oo u s.oo u s.oo LI s.oo u 1,1,2,2,-TETRACHLOROETHANE s.oo LI s.oo u s.oo u s.oo u 1,2-DICHLOROPROPANE 5.00 u s.oo lJ s.oo lJ s.oo u

ANS-1,3-DICHLOROPROPENE 5.00 u :i.oo lJ s.oo lJ s.oo u I ,,;ICHLOFWETHENE 5.00 LI 5.00 u s.oo LI s.oo u DIBROHOCHLOROMETHANE s.oo u s.oo u s.oo LI s.oo u 1,1,2-TRICHLOROETHANE' s.oo u s.oo Ll s.oo LI s.oo u BENZENE 5.00 lJ s.oo u s.oo lJ 5.00 u CIS-1,3-DICHLOROPROPENE s.oo u s.oo u s.oo u s.oo u 2-CHLDRDETHYL VINYL ETHER 10.0 u 10.0 u l0.O LI l0.0 u I-:ROMOFORM 5,00 u s.oo lJ s.oo u s.oo u 2-HEXANONE 10.0 u l0.0 u 10.0 u 10.0 u 4-METHYL-2-PENTANONE 10.0 ll 10.0 u 10.0 u 10.0 u TETRACHLDRDETHFNE s.oo u s.oo LI s.oo u s.oo u TOLUENE s.oo u s.oo u s.oo lJ s.oo u CHLOROf:ENZENE s.oo u s.oo u s.oo u s.oo u ETHYL BENZENE 5.00 u s.oo u s.oo LI s.oo u STYRENE 5.00 u s.oo lJ s.oo u s.oo u TOTAL XYLENES 5.00 u s.oo LI, 5.00 u s.oo u

PROJ3224

ANALYSIS TYFE: VOLATILE ~NALYSES

TITLE: HASTINGS HATRIX: W. E'R UNITS! UG/L LAB! UHL HETHOD! CASE':. 4 987 SAMPLE PREP: _______ ANALYST/ENTRY: E"l2 REVIElilE • Dt"lTE! 01/08/8~ •

SAHF'LE NUHBERS

CKCS2206 CKCS:2207 CKCS2207D CKCS220E COHPOUHD

CHLOROHETHANE 10.0 u 10.0 u 10.0 u l (). 0

BROHOHETHANE 10.0 u 10.0 u 10.0 u 10.0 VINYL CHLORIDE 10.0 u 10.0 LI 10.0 u 10.0 CHLOROETHANE 10.0 u 10.0 u l O. 0 lJ 10.0 HETHYLENE CHLORIDE s.oo u s.oo u s.oo u s.oo ACETONE 10.0 u 10.0 u 10.0 LI 10.0 CARBON DISULFIDE s.oo u s.oo u 5.00 u s.oo 1,1 DICHLOROETHENE s.oo u s.oo u s.oo u s.oo 1,1 DICHLOROETHANE s.oo ll s.oo u s.oo u s.oo TRANS-1,2,-DICHLOROETHENE s.oo u s.oo u s.oo lJ s.oo CHLOROFORH s.oo u s·.oo ll s.oo u s.oo 1,2,DICHLOROETHANE s.oo u s.oo u s.oo u s.oo 2-BUTANONE I I I 1,1,1 TRICHLOROETHANE s.oo u 5.00 u s.oo Lt s.oo I

CARBON TETRACHLORIDE s.oo u s.oo u s.oo u s.'oo I

VINYL ACETATE 10.0 u 10.0 u 10.0 u 10.0 I

BROMOOICHLOROHETHANE s.oo u s.oo u s.oo u s.oo I

1,1,2,2,-TETRACHLOROETHANE' s.oo u s.oo u s.oo u s.oo l

1,2-DICHLOROPROPAHE s.oo u s.oo u s.oo u s.oo l TRANS-1,3-DICHLOROF'ROPEHE s.oo LI s.oo LI s.oo u s.oo l TR 1 CHLOROE_THENE s.oo u s.oo u s.oo u s.oo l

DIBROHOCHLOROHETHANE s.oo u s.oo u s.oo u s.oo t 1,1,2-TRICHLOROETHANE s.oo u s.oo u s.oo u s.oo l

BENZENE s.oo u s.oo u s.oo u s.oo l

CIS-1,3-DICHLOROPROPENE 5.00 u 5.00 LI s.oo u 5.00 L

2-CHLOROETHYL VINYL ETHER 10.0 u 10.0 u ·10 .o lJ 10.0 L

BROMOFORH s.oo LI s.oo u s.oo u s.oo L:

2-HEXANONE 10.0 u 10.0 LI 10.0 lJ 10.0 u 4-METHYL-2-PENTANONE 10.0 u 10.0 lJ 10.0 lJ 10.0 u TETRACHLOROETHFNE s.oo u s.oo u s.oo u s.oo u TOLUENE s.oo LI s.oo LI s.oo u 5.00 u CHLOROBENZENE 5.00 u s.oo u s.oo u s.oo u ETHYL BENZENE 5.00 u s.oo u s.oo u s.oo u STYRENE s.oo u s.oo LI s.oo lJ s.oo u TOTAL XYLENES s.oo u s.oo u s.oo u s.oo u

PROJ3225

. . .. ~·- ~-;--•-.......... •-"\ ... ..,._.,..-~_ ..... ,.....__.,,,... ___ ....,_ __ -:-,,--,---..-:s:-:-•---...... ---- .-~-. ····-·- - ~ ..

ANALYSIS TYF'E! I'IISSOL.VED HF.Tf\LS (CONTRACTOR)

TITLE: HASTINGS LAB: RHA SAHPLE PREP: _______ ANALYST/ENTRY: E~3

CKCS222B ~

COMPOUND .. .. ALUMINUM 30.0 ANTIMONY 60.0 ARSENIC s.10 BARIUM 230 BERYLLIUM s.oo CADHIUH 8.30 CALCIUM 91000. CHROMIUM 10.0 COBALT so.o COPPER 6.40

. IRON 3S.O LEAD s.oo MAGNESIUM 1s000. MANGANESE 1s.o MERCURY 0.2 NICKEL 40.0 F'OTASSIUH 7600. SELENIUM s.oo SILVER 10.0 SODIUM 26000. THALLIUM 10.0 TIN 40.0 VANADIUM a.so ZINC 26.0 CYANIDE

H u M

u

u u H H u

u u

u

LI u

u u H

I

MATRIX: U~T R HETH OD: 9 l H06LL1"' RE'VIHIER: ~ _ -----

SAMPLE NUMBERS

CKCS2229

200 u 60.0 u

'1. 8 0 M 210

s.oo u 19.0

79000. 10.0 u so.o u

5.30 H s:i.o H

s.oo u 14000.

15.0 U. 0.2 u

"10. 0 u 7600.

5.00 u 10.0 u

27000. 10.0 u '10. 0 u s.so M

72.0 I

UNITS: UG/L Cl'ISE': 4987 I'tt:TE: 0'1/08/86

PROJ3226

ANALYSIS TYF·E: DJSSDLVE'D HE'TflLS <CONTRACTOR>

TITLE: HASTINGS MATRIX: UATER UNITS: UG/L LAB! RHA METHOD: 90r)Mc__c CASE: 4987 SAMF'LE PREP: _______ ANALYST/ENTRY! E-14 REVIEWER: ____ J_ D~TE: 0-\/08/86

: .. SAMPLE NUMBERS

CKCS2307D CKCS.2308 CKCS2309 CKCS.2310 COMPOIJHD

ALUM1NUl1 200 u 200 u 25.0 M 200 u ANTIMONY 60.0 u 60.0 u 60.0 lJ 60.0 u ARSENIC 10.0 u 10.0 u 10.0 u lO.O u BARIUM 150 H 130 ti 300 250 BERYLLIUH s.oo u s .. oo u s.oo u s.oo u

.CADHIUH s.oo u s.oo u s.oo u s.oo u CALCIUl1 59000. 46000. 94000. 72000. CHROMIUM 10.0 u 1-1.0 10.0 u 10.0 u COBALT so.o u 50~0 LI so.o u so.o u COPPER 25.0 LI 25,0 u 3.20 H 5,30 H IRON 100 u 100 u 100 u 100 u LEAD s.oo u s.oo ll s.oo u s.oo u MAGNESIUM 8300. 6800. 14000, 11000. MANGANESE 1s.o lJ 15.0 u 15,0 u 15.0 u MERCURY 0.2 u 0.2 u 0.2 u 0.2 u NICKEL 40.0 ll 40, 0 u -10.0 lJ 40.0 u f'OTASSIUM ssoo. sooo. 7500. 7300. SELENIUM s.oo u s.oo u s.oo u 9.30 J SILVER 10.0 u 10.0 u l O, 0 u 10.0 u SODIUM 21000. 18000. 35000. 19000. THALLIUM 10.0 u 10.0 LI lO.O u 10.0 u TIN 40.0 u -40. 0 lJ 4 0. 0 u 40.0 u VANADIUM 6.10 H 6.80 H a.oo M 4.80 M ZINC 20.0 ll 20.0 LI 91.0 91.0 CYANIDE I I I I

PROJ3227

ANALYSIS TYPE: DISSOLVE'D HF.TALS (CONTRACTOR>

TITLE: HASTINGS HATRix: w•~ UNITS: UG/L LAB: RHA METHOD= 90 Go CASF.: 4987 SAMPLE PREP: _______ ANALYST/ENTRY: F.-11\ RF.VIF.WE'R: . ----- D~TE: 01\/08/86

, .. .. SAHF'LE NUMBERS

CKCS2312 CKCS:2313 CKCS2314 CKCS2316 COMPOUND

ALUMINUM 200 u 200 u 200 u 200 u ANTIMONY 60,0 u 60,0 u 60.0 u 60.0 u ARSENIC 10.0 u 10.0 u 10.0 u 10.0 u BARIUH 3-10 170 H 180 H 210 BERYLLIUM s.oo u s .• oo u s.oo u s.oo u

.CADHIUH s.oo lJ s.oo LI s.oo u s.oo u CALCIUH 110000. s1000. s0000. 67000. CHROHIUH 10.0 u 10.0 LI 10.0 u 10.0 u COBALT so.o u so.o u 50.0 u !'.iO • 0 u COF'F'ER 2s.o u 2s.o u- 2s.o u 12.0 t1 IRON 100 u 100 u 100 u 100 u LEAD s.oo u s.oo u s.oo u s.oo u MAGNESIUM 1s000. 7500. 7600. 10000. MANGANESE 15.0 u lS.O u 15,0 u l:J. 0 u MERCURY 0.2 u 0.2 u 0.2 u 0.2 l.;

NICKEL 40,0 u 40,0 u -10. 0 u ,t O • 0 u POTASSIUM· 8000. 6100. 6300. 6300, SELENIUM s.oo LI 3,40 H s.oo u s.oo u SILVER 10.0 u 10.0 ll 10.0 u 10.0 u SODIUH 29000. 18000. 18000. 19000. THALLIUH 10.0 u 10.0 ll 10.0 LI 10.0 u TIN -40. 0 ll 40.0 u 1\0,0 u -10.0 u VANADIUM 7,60 H 6,60 H 5.50 H 5,10 H ZINC 20.0 u 68.0 20.0 LI 130 CYANIDE I l I l

] PROJ3228

----------- • - --··-·-·-··- ----· --- -·-----····· ·-- ·----•-· ··•-···· -· ... -

TITLE: HASTINGS LAB: RHA

ANALYSIS TYPE: DJSSOLVFD HETALS (CONTRACTOR>

SAMPLE PREP: _______ ANALYST/ENTRY: E~4

MATRIX: WAB2 METHOD! 90 1 J; ~ RF.VIEWER: Jj ___ _1

UNITS! UG/L Cf\SE: -4987 !lf.iTE'! 0'1/08/86

COMPOUND

ALUMINUM ANTIMONY ARSENIC BARIUM BERYLLIUM CADMIUM CALCIUM CHROMIUM COBALT COF'F'ER IRON LEAD MAGNESIUM MANGANESE MERCURY NICKEL POTASSIUM SELENIUM SILVER SODIUM THALLIUM TIN VANADIUM ZINC CYANIDE

SAMPLE NUMBERS

CKCS2317

200 u 60.0 u 10.0 u

390 s.oo u s.oo u

120000. 10.0 u so.o u 2s.o u

100 u s.oo u

18000. 1s.o u

0.2 u 40.0 u

8700. s.oo u

10.0 u 35000.

10.0 u 40.0 u ?.70 H

20.0 u I

PROJ3229

ANAL YS JS TYF·E: DISSOLVED HETALS CCONTRf"ICTOR)

TITLE: HASTINGS HATRIY.: ~ UNITS: UG/L LAB! Rt1A HETHOD: 9 0 CASE: 49_87

REVIE~~R Q_j,J_ SAMPLE PREF: _______ f\NALYST/ENTRY: E'43 DtiTE: 04/08/86

SAHF'LE NUMBERS

CKCS:?216 CKCS:?217 CKCS2218 CKCS2219 COMPOUND

ALUHINUH ' 200 u 200 ~

u 200 u 200 u ANTIMONY 60.0 lJ 60.0 LI 60.0 lJ 60.0 u ARSENIC s.10 H 4.70 H . 4. 40 Ii -1.so H BARIUM 140 H 150 H 11>0 H 1i'O H BERYLLIUH s.oo u s.oo u s.oo u s.oo u CA!1MIUH 5.00 u 5.00 u 5.00 u 5,00 u CALCIUM 52000. S4000. 56000. 54000. CHROMIUM 10.0 u 10.0 lJ 10.0 u 10.0 u

I COBALT so.o u 50.0 u so.o u so.o u COF'PER 16.0 M l l • 0 H 10.0 Ii ,.so H IRON 27,0 M JI\. 0 H 1\2 • 0 Ii :.H. 0 H LEAD s.oo u s.00 u 5,00 u s.oo l MAGNESIUM 9100. 9200, 9300. 8600. MANGANESE 1s.o u 1s.o lJ 15,0 u 15,0 l MERCURY 0.2 u 0.2 u 0,2 u 0.2 NICKEL 40.0 u -10.0 ll 40.0 u -10.0 l F'OTASSIUH 5400. 5400. 5600. ssoo. SELENIUM 7,00 6,80 5,80 s.oo l SILVER 10.0 u 10.0 lJ 10.0 lJ 10.0 l S0!1IUl1 2:?000. 23000. 23000. 21000. THALLIUM 10,0 u 10.0 u 10,0 lJ 10,0 TIN 40.0 u '10.0 lJ 40.0 u -10.0 VANADIUM 5.50 H 6,30 11 6.50 H 5.80 ZINC 16.0 H 17.0 M 26.0 13.0 CYANIDE I I I

PROJ3230

___________________ ,___ ___ .---.~-----·~~•~.-r--,:-·:-:~ -• ... ·•:.,:--•-··" ~--·.-·

Appendix B-3


December 1985

PROJ3231

' . . .'-! ANALYSIS TYPE: VOLATILES

TITLE: HASTINGS MATRIX: WATER UNITS: UG/L LAB: EPA7 t}_-:f METHOD: 6041WOO CASE: SAMPLE PREP: __ "5_ __ ANALYST/ENTRY! VJS REVIEWER: ~------- DATE: 01/09/86

SAMPLE NUMBERS

DKJS2001 J)KJS2002 DKJS2003 DKJS2004 COMPOUND

ACROLEIN 12.0 u 12.0 u 18.0 u 12,0 u ACRYLONITRILE 22.0 u 22.0 u 22.0 u 22.0 u CHLOROHETHANE 57.0 u 12.0 u 12.0 u 12.0 u BROMOMETHANE 24.0 u 22,0 u 22.0 u 22.0 u VINYL CHLORIDE 14,0 u 14,0 u 14.0 u 14.0 u CHLOROETHANE 14.0 u 14.0 u 14.0 u 14.0 u METHYLENE CHLORIDE· 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1.00 u 1,1-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,2-DICHLOROETHYLENE 1.00 u 1.00 u 90.0 J 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 3,00 u 1.00 u 1.00 u 1.00 u 1,1,1-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CARBON TETRACHLORIDE 1.00 u 1.00 u 1.00 u 1.00 u BROMODICHLOROMETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE s.oo u s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u TRICHLOROETHYLENE 45,0 J 49,0 J 1100. J 7.00 J CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u DIBROMOCHLOROMETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 2-CHLOROETHYLVINYL ETHER 18.0 u 18,0 u 18.0 u 18,0 u BROMOFORH 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2,2-TETRACHLOROETHENE 1.00 u 1.00 u 6,00 J 1,00 u TOLUENE s.oo u S,00 u s.oo u 5.oo u 1,1,2,2-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROBENZENE s.oo u s.oo u 5,00 u 5.00 u ETHYL BENZENE s.oo u s.oo u 5,00 u 5,00 u

} PROJ3232

ANALYSIS TYPE: VOLATILES

TITLE: HASTINGS MATRIX: WATER UNITS: UG/L LAB: EPA7 ~°JS' METHOD! 6041W00 CASE: SAMPLE PREP:_----- ANALYST/ENTRY: VJS REVIEWER: fc-iJ _______ DATE: 01/09/86

SAMPLE NUMBERS

DKJS2005 DKJS2006 DKJS2007 DKJS2008 COMPOUND

ACROLEIN 12.0 u 12.0 u 12.0 u 12.0 u ACRYLOHITRILE 22.0 u 22.0 u 22.0 u 22.0 u CHLOROMETHANE 12.0 u 12.0 u 12.0 u 12.0 u .BROMOHETHANE 22.0 u 22.0 u 22.0 u 22.0 u VINYL CHLORIDE 14.0 u 14.0 u 14.0 u 14.0 u CHLOROETHANE 14.0 u 14.0 u 14.0 u 14.0 u METHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u s.oo J 1.00 u 1,1-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,2-DICHLOROETHYLENE 2.00 u 1.00 u 1.00 u 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,1-TRICHLOROETHANE 1.00 u 1.00 u 7,00 J 1.00 u CARBON TETRACHLORIDE 1.00 u 1.00 J 32.0 J 1.00 u BROMODICHLOROHETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE ::;.oo u s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROfEHE 1.00 u 1.00 u 1.00 u 1.00 u TRICHLOROETHYLENE 130 J 1.00 u ~2.0 J 4.00 J CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u DIBROHOCHLOROMETHANE 1.00 u 1,00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1,00 u 1.00 u 2-CHLOROETH'l'LVINYL ETHER .18.0 u 18.0 u 18,0 u 1s.o u BROMOFORM 1.00 u 1.00 u 1,00 u 1.00 u 1,1,2,2-TETRACHLOROETHENE 1.00 u 1.00 u 1.00 u 1.00 u TOLUENE s.oo u s.00 u 5,00 u s.oo u 1,1,2,2-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROBENZENE s.oo u 5.00 u s.oo u s.oo u ETHYL BENZENE s.oo u s.00 u s.00 u s.oo u

PROJ3233

• ., • t •


TITLE: HASTINGS LAB: EPA7 V :rr; SAMPLE PREP: _______ ANALYST/ENTRY: VJS

COMPOUND

ACROLEIN ACRYLONITRILE CHLOROMETHANE BROHOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE 1,1-DICHLOROETHYLENE 1,1-DICHLOROETHANE TRANS-1,2-DICHLOROETHYLENE CHLOROFORM 1,2-DICHLOROETHANE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROHODICHLOROHETHANE 1,2-DICHLOROPROPANE BENZENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE CIS-1,3-DICHLOROPROPENE DIBROHOCHLORDHETHANE 1,1,2-TRICHLORDETHANE 2-CHLOROETHYLVINYL ETHER BROHOF'ORH 1,1,2,2-TETRACHLORDETHENE TOLUENE 1,1,2,2-TETRACHLDROETHANE CHLOROBENZENE ETHYL BENZENE

...

DKJS20080

12.0 22.0 12.0 22.0 14.0 14.0 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00

18.0 1.00 1.00 5.00 1.00 5.00 s.oo

u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

MATRIX! WATER METHOD: 6041\J00 REVIEWER: ff:fJ ______ _

SAMPLE NUMBERS

UNITS: UG/L CASE: DATE: 01/09/Bo

DKJS2009 DKJS2010 DKJS2011

16.0 22.0 51.0 22.0 14.0 14.0 10.0 2.00 1.00 1.00 1.00 1.00 1.00 1.00 1.0Q 1.00 5. 00 1.00

33.0 1.00 1.00 1.00

18.0 1.00 1.00 5.00 1.00 s.oo s.oo

u u u u u u u u u u u u u u u u u u J u u u u u u u u u u

12.0 22.0 12.0 22.0 14.0 14,0 10.0

1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1,00 s.oo 1.00 6.00 1.00 1.00 1.00

18.0 1.00 1.00 5.00 1.00 s.oo s.oo

u u u u u u u u u u u u u u u u u u J u u u u u u u u u u

PROJ3234

12.0 U 22.0 U 12.0 U 22.0 U 14.0 U 14.0 U 10.0 U

1.00 U 1.00 U 1.00 U 1.00 U 1.00 U 1.00 U

34.0 J 1.00 U 1.00 U 5.00 U 1. 00 U

18.0 J 1.00 U 1.00 U 1.00 U

18.0 U 1.00 U 1.00 U s.oo u 1.00 U s.oo u s.oo u


TITLE: HASTINGS HATRlX: .!ATER UNITS: UG/L LAB: EPA7 J.}:SJ METHOD: 6041WOO CASE: SAMPLE PREP: ----- ANALYST/ENTRY: VJS REVIEWER: kf~------ DATE: 01/09/86

SAMPLE NUMBERS


ACROLEIN 12.0 u 12.0 u 12.0 u 12.0 u ACRYLONITRILE 22.0 u 22.0 u 22.0 u 22.0 u CHLOROHETHANE 12.0 u 12.0 u 12.0 u 12.0 u BROMOMETHANE 22.0 u 22.0 u 22.0 u 22.0 u VINYL CHLORIDE 1 -4. 0 u 14.0 u 14.0 u 14.0 u CHLOROETHANE 14.0 u 14.0 u 14.0 u 14.0 u METHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 ·u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1.00 u 1,1-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u TRAHS-1,2-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,1-TRICHLOROETHAHE 1.00 u 1.00 u 1.00 u 1.00 u CARBON TETRACHLORIDE 1.00 u 1.00 u 1.00 u 1.00 u BROMODICHLOROHETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROPROPAHE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE 5,00 u s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE 1.00 u 1,00 u 1.00 u 1.00 u TRICHLOROETHYLENE 150 J 1.00 u 1.00 u 1.00 u CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u DIBROMOCHLOROMETHAHE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 2-CHLOROETHYLVINYL ETHER 1a.o u 1B.O u 1a.o u 18.0 u BROM OF ORM 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2,2-TETRACHLORDETHENE 1.00 u 1.00 u 1.00 u 1.00 u TOLUENE s.oo u s.oo u s.oo u 5.00 u 1,1,2,2-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROBENZEHE 5.00 u s.oo u s.oo u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u

} PROJ3235

. .. . . ~ .. . . , · ..... ~


TITLE: HASTINGS HATRIX: WATER UNITS: UG/L LAB: Ef'A7 J.S HETHOD: 6041WOO CASE: SAMPLE PREP:li-- - ANALYST/ENTRY: VJS REVIEWER! _(:d-z ______ DATE: 01/09/86

SAHPLE NUMBERS

DKJS2016 DKJS2017 DKJS2017D DKJS201B COHPOUND

ACROLEIN 12.0 u 12.0 u 12.0 u 12.0 u ACRYLOHITRILE 22.0 u 22.0 u 22.0 u 22.0 u CHLOROHETHANE 12.0 u 12.0 u 12.0 u 12.0 u BROMDHETHANE 22,0 u 22.0 u 22,0 u 22.0 u VINYL CHLORIDE 14,0 u 14.0 u 14,0 u 14.0 u CHLOROETHANE 14.0 u 14.0 u 14,0 u 14.0 u HETHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u J.oo u 1.00 u 1,1-DICHLOROETHAHE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,2-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1,00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,1-TRICHLORDETHANE 1.00 u s.oo J 9.00 J 1.00 u CARBON TETRACHLORIDE 1.00 u 1.00 u 1.00 u 32,0 J BROMODICHLOROHETHAHE 1. 00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE s.oo u 6.00 J s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u TRICHLDROETHYLENE 110 J 680 J 620 J 1.00 u CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 .u DIBROMOCHLOROMETHAHE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2-TR!CHLOROETHANE 1.00 u 1.00 u 1,00 u 1.00 u 2-CHLOROETHYLVINYL ETHER 18.0 u 18.0 u 18.0 u 18.0 u BROHOFORH 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2,2-TETRACHLOROETHENE 1.00 u 9.00 J 10.0 J 1.00 u TOLUENE S, 00 u s.oo u s.oo u s.oo u 1,1,2,2-TETRACHLOROETHANE 1 .oo u 1.00 u 1.00 u 1.00 u CHLOROBEHZEHE s.oo u s.oo u s.oo u 5.00 u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u

PROJ3236

.... ,I • • •


TITLE: HASTINGS HATRIX: WATER UNITS: UG/L LAB: EPA7 METHOD: 6041WOO . CASE: SAMPLE PREP:_'-.,.L14. ANALYST/ENTRY: VJS REVIEWER:~---- DATE: 01/09/86

SAMPLE NUMBERS


ACROLEIM 12.0 u 12.0 u 12,0 u 12.0 u ACRYLONITRILE 22.0 u 22.0 u 22,0 u 22,0 u CHLOROMETHANE 12.0 u 12.0 u 12,0 u 12,0 u BROMOHETHANE 22.0 u 22.0 u 22,0 u 22.0 u VINYL CHLORIDE 14,0 u 14,0 u 14,0 u 14,0 u CHLOROETHANE 14,0 u 14,0 u 14,0 u 14,0 u METHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10,0 u 1,1-DICHLOROETHYLENE 1,00 u 1.00 u 1.00 u 1.00 u 1,1-DICHLOROETHANE 1,00 u 1,00 u 1.00 u 1.00 u TRANS-1,2-DICHLOROETHYLENE 1,00 u 1,00 u 1.00 u 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 1,00 u 1,00 u 1.00 u 1.00 u 1,1,1-TRICHLOROETHANE 1.00 u 1,00 u 1.00 u 1.00 u CARBON TETRACHLORIDE 1,00 u 1.00 u 1,00 u 1.00 u BROMODICHLOROMETHANE 1,00 u 1,00 u 1,00 u 1,00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1,00 u 1.00 u BENZENE S,00 u s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE 1,00 u 1.00 u 1.00 u 1,00 u TRICHLOROETHYLENE 3.00 J s.oo J 3,00 J 2.00 J CIS-1,3-DICHLOROPROPENE 1,00 u 1,00 u 1.00 u 1.00 u DIBROHOCHLOROMETHANE 1,00 u 1.00 u 1.00 u 1.00 u 1,1,2-TRICHLORDETHANE 1.00 u 1.00 u 1.00 u 1.00 u 2-CHLDROETHYLVINYL ETHER 18,0 u 18.0 u 18,0 u 18.0 u BROMDFDRM 1,00 u 1.00 u 1,00 u 1.00 u 1,1,2,2-TETRACHLOROETHENE 1,00 u 1.00 u 1,00 u 1.00 u TOLUENE s.oo u s.oo u s.oo u s.oo u 1,1,2,2-TETRACHLOROETHANE 1.00 u 1,00 u 1.00 u 1.00 u CHLOROBENZENE s.oo u s.oo u s.oo u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u 5.00 u

pROJ3237

.._ , . ._ .. ,


TITLE: HASTINGS MATRIX: WATER UNITS! UG/L LAB! EPA7 METHOD! 6041WOO CASE! SAMPLE PREP! _______ ANALYST/ENTRY: E09 REVIEWER: (r.J.$ ___ ~ DATE: 01/24/86

SAHPLE NUMBERS

DKJS2024D DKJS202~ DKJS2026 DKJ52027 COMPOUND

ACROLEIN 12.0 u 12.0 u 12.0 u 12.0 u ACRYLOHITRILE 22.0 u 22.0 u 22.0 u 22.0 u CHLOROHETHANE 12.0 u 12.0 u 12.0 u 12.0 u BROMOMETHANE 22.0 u 22.0 u 22,0 u 22.0 u VINYL CHLORIDE 14,0 u 14,0 u 14.0 u 14,0 u CHLOROETHANE 14,0 u 14.0 u 14.0 u 14.0 u METHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u LOO u 1.00 u 1,1-DICHLOROETHANE 1.00 u 1.00 u LOO u 1.00 u iRANS-1,2-DICHLOROETHYLENE 1.00 u 1.00 u LOO u LOO u CHLOROFORM 1,00 u 1,00 u 4,00 J 1.00 u 1,2-DICHLOROETHANE 1.00 u 1.00 u LOO u 1.00 u 1,1,1-TR!CHLOROETHAHE 1.00 u 1,00 u LOO u 18,0 J CARBON TETRACHLORIDE 1.00 u 1.00 u 1.00 u 1.00 u BROMODICHLOROMETHANE 1,00 u 1.00 u LOO u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u LOO u 1.00 u BENZENE 5.00 u s.oo u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1,00 u 1.00 u iR!CHLOROETHYLEHE 3.00 J 1.00 u 2,00 J 740 J CIS-1,3-DICHLOROPROPENE 1,00 u 1.00 u LOO u 1.00 u DIBROMOCHLORDMETHANE 1.00 u 1,00 u 1.00 u 1,00 u 1,1,2-TRICHLOROETHANE 1.00 u 1,00 u 1,00 u 1,00 u 2-CHLOROETHYLVINYL ETHER 18.0 u 18,0 u 18.0 u 18,0 u BROMOF'ORM 1.00 u 1.00 u 1.00 u 1,00 u 1,1,2,2-TETRACHLORDETHENE 1.00 u 1.00 u 1.00 u 23,0 J TOLUENE 5.00 u s.oo u s.oo u s.oo u 1,1,2,2-TETRACHLOROETHANE 1.00 u 1.00 ·u LOO u 1.00 u CHLOROBENZENE s.oo u s.oo u S,00 u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u

H pROJ3238


TITLE: HASTINGS HATRIX: WATER UNITS: UG/L LAB: EPA7 METHOD: 6041WOO ~ CASE: SAMPLE PREP: _______ ANALYST/ENTRY: E09 REVIEWER: .fni, _____ DATE: 01/24/86

SAMPLE NUMBERS


ACROLEIN 12.0 u 12.0 u 12.0 u 12.0 u ACRYLONITRILE 22.0 u 22.0 u 22.0 u 22.0 u CHLOROl'IETHANE 12.0 u 12.0 u 12.0 u 12.0 u BROMDHETHANE 22.0 u 22.0 u 22.0 u 22,0 u VINYL CHLORIDE 14,0 u 14.0 u 14.0 u 14,0 u CHLOROETHANE 14.0 u 14.0 u 14.0 u 14,0 u METHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1.00 u 1,1-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,2-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,1-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 2.00 J CARBON TETRACHLORIDE 1.00 u 1.00 u 1.00 u 1.00 u BROHODICHLOROMETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE s.oo u s.oo u s.oo u 5.00 u TRANS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u TRICHLOROETHYLENE 13.0 J 1.00 u 1.00 u 180 J CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u DIBRDHOCHLOROHETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1,00 u 2-CHLOROETHYLVINYL ETHER 18.0 u 18.0 u 18.0 u 18,0 u BROHOFORH 1.00 u 1.00 u 1.00 u 1,00 u 1,1,2,2-TETRACHLOROETHENE 1.00 u 1.00 u 1.00 u 2.00· J TOLUENE s.oo u s.oo u s.oo u s.oo u 1,1,2,2-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROBENZENE s.oo u s.oo u s.oo u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u

PROJ3239


TITLE: HASTINGS HATRIX: WATER UNITS: UG/L l.AB: EPA7 HETHOD: 60.UWOO CASE: SAMPLE PREP: _______ ANALYST/ENTRY! E09 REVIEWER: -Erl->---~ DATE: 01/24/86

SAHPLE NUMBERS

DKJS2032 DKJS2033 DKJS2035F Dl<JS2036F COHPOUND

ACROLEIN 12.0 u 12,0 u 12.0 u 12,0 u ACRYLONITRILE 22.0 u 22,0 u 22,0 u 22.0 u CHLOROHETHANE 12.0 u 12.0 u 12.0 u 12.0 u BROHOHETHANE 22.0 u 22.0 u 22.0 u 22.0 u VINYL CHLORIDE 14,0 u 14,0 u 14,0 u 14.0 u CHLOROEiHANE 14.0 u 14,0 u 14,0 u 14,0 u HETHYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u 1.00 u 1.00 u 1.00 u 1,1-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,2-DICHLOROEiHYLENE 1.00 u 1.00 u 1,00 u 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,1-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CARBON TETRACHLORIDE 1.00 u 1.00 u 1.00 u 1.00 u BROMODICHLOROHETHANE 1.00 u 1. 00 u 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE s.oo u 5,00 u 5,00 u 5,00 u TRANS-1,3-DICHLOROPROPENE 1.00 u 1. 00 u 1.00 u 1.00 u TRICHLOROETHYLENE 190 J 120 J 1.00 u 1.00 u CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u DIBROHOCHLOROHETHANE 1.00 u 1.00 u 1.00 u 1,00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 2-CHLOROETHYLVINYL ETHER 18.0 u 18,0 u 10.0 u 18,0 u .BROHOFORH 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2,2-TETRACHLOROETHENE 1.00 u 1.00 u 1.00 u 1.00 u TOLUENE s.oo u s.oo u s.oo u s.oo u 1,1,2,2-TETRACHLOROETHANE 1,00 u 1.00 u 1.00 u 1.00 u CHLOROBENZENE S,00 u s.oo u s.oo u s.oo u ETHYL BENZENE s.oo u s.oo u s.oo u s.oo u

PROJ3240

- ,, • ! • • .. ,, ....


TITLE: HASTINGS LAB: EPA7

HATRIX: WATER UNITS: UG/L HETHOD: 6041WOO CASE:

SAMPLE PREP: _______ ANALYST/ENTRY: E09 REVIEWER: (;;;::CJ __ ~ DATE: 01/24/86

COHPOUND

ACROLEIN ACRYLONITRILE CHLOROMETHANE BROHOHETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE 1,1-DICHLOROETHYLENE 1,1-DICHLOROETHANE TRANS-1,2-DICHLOROETHYLENE CHLOROFORH 1,2-DICHLOROETHANE 1,1,1-TRICHLOROETHANE CARBON TETRACHLORIDE BROHODICHLOROHETHANE 1,2-DICHLOROPROPANE BENZENE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE CIS-1,3-DICHLOROPRDPENE DIBROHOCHLOROMETHANE 1,1,2-TRICHLOROETHAHE 2-CHLOROETHYLVINYL ETHER BROMOFORM 1,1,2,2-TETRACHLOROETHENE TOLUENE 1,1,2,2-TETRACHLOROETHANE CHLOROBENZENE ETHYL BENZENE

SAHPLE NUMBERS

DKJS2037F

12.0 u 22.0 u 12.0 u 22.0 u 14.0 u 14,0 u 10.0 u

1.00 u 1.00 u 1.00 u 1.00 u 1.00 u 1.00 u 1.00 u 1.00 u 1.00 u s.oo u 1.00 u 1.00 u 1.00 u 1.00 u 1.00 u

18,0 u 1.00 u 1.00 u s.oo u 1.00 u 5,00 u s.oo u

J PROJ3241

DATA SHEET

ACTIVITY TITLE: l+a ~rt'nss I N~. . PROJECT LEADER: Becn1 cJ - W\tJC COLLECTION DATE: __ / 2 ___ -o ___ 5 __

Analytical Lab: E::f 11- :J1]; Sample Matrix: _ ___,W,._~ _____ r __

SAMPLE NUMBERS J)K:JS2 Df<Js2 .DKJ.S2 DK.TS;2. ])f<JS2 .D<J'S_z

003 D04 ooro 007 012 C/.3

ANALYSIS UNITS

A I~ /;,,;tt, rng It :2 ~ ;,2 :r /gq j ~,1 ~ ~5? j ;21,t3 J /97 J (),l'-'";J€.J c'hJ[£ ':)1.~ /~,t ;;. 3, 1 "10, (i, .35,2. -:2P.O

S(A l+:..:t{. fr'JJ 1. '2/),0 g3_0 33.o 4-g, 0 30.D 3~.o (, ~ ·M.ft/ ci.JfTl,urn :ssclv, ~ I U I ti I U I u I I,,{ IU

I

·0-Jh Ltc,.tl Oicscl<Jc-. SIA .5 LA 5 tA ~ u. 5' u 5U ,

I

.. -

.

I PROJ3242

DATA SHEET

ACTIVITY TITLE: :t±:tA.sfino S1

}J e.. _

PROJECT LEADER: brrn1- r-J - rJw'C. COLLECTION DATE: _ __,_l __ :l-_---r_s __ :.

Ana lyt i cal Lab: _~ ___ P __ t1-_1[If~·..___ __ Sample Matrix: ------

SAMPLE NUMBERS PKJ""S;2... .Pl<T52 l>KJS;;.. :t;J<:IS:;i.. 1)1<:TS:2..

or o o~1- D:J'l.1) o:i.s o:>ei,

ANALYSIS UNITS

Al ktf;n,·~~, 01c1Le Joo :r 3 ;,;2. J /14 J' 111- S /31 J :2.15 J

CA le r;di rndlx 2g, 'I ~3./ I ~-1 !G. 0 J(c, 7 I g', g

Si.f f;.1-e. °'3/i ?..5.o ?i),O ~3,0 33,0 ;q,o ;lS, 0

(a.Arn i'um Di ~siJ . .IJJ If. I U I U I u I U t, g> 9,J' J I j,(,81 Lec..cl D·<:.,,lv·, · J SH SU 5 t{ 5 t{ 5U SU

,

·--·-·

.

PROJ3243

DATA SHEET

ACTIVITY TlTLE: bttAst-,·°os /Ve. J .

PROJECT LEADER: {3 ernt-i r,/- WW C:. COLLECTION DATE: l .:2-? 5

, ,lb r.:=p,~ Ana yt i ca a : _c.-____ """"~__,;::JL.LJ-=a __ Sample Matrix: wd-.er -~-'-----

SAAPLE NUMBERS })K:rs;i... l>K J"S:2.. J)f<JS ;i.. l>K .:T.S.,-;i... .Pk JS 1 .DI< J"S

02 D 03 03A 0,3..3

ANALYSIS UNITS

,4( kll Ln;+... ft\J,}) lC/1 1 ;)07 :f l'15 J ;271./- .J .~&SJ 3515

Ch lc,~dt r-,BU ,9.S } CJ, 5 /~.7 2 {;,, '1 1/-t. I L/S. ! S\A_ l¾te.. «t}fi /10. S-5. 0 JO.O ~o.o 5'3.0 S/,O

r{).1 nHU m o~("ofv'<?. µ_1/e I.,'? ;r I lA I IA I t1 I ;;2. I U.

Lud )

D i'c.<;c /v< JJ.J Lf Su .t;' t{ ~ 11 ~ t1 s t{ 5 l1 ,I

•·· -· -

.

PROJ3244

DATA SHEET

ACTIVITY TITLE: H:r,. g,·hj ,1

)/e. PROJECT LEADER: Berac.r:) - wwc_ COLLECTION DATE: / 1· o 5

Analytical Lab: tZ""P± li Sample Matrix: W&..,,,j-er

ANALYSIS UNITS

A-I ~f ;n;-1.. lnd'/.£

C1i lt)";Jt:- ffl}/ 1.

~i../-½,,fe. rnJ,/j

(\.d ll1 ,'-4 rn D;~, Iv. µ.~ {J

La;d O :ssc lv1J. J-lj!) /

.

SAMPLE NUMBERS

IJ)K.TS2 I J)KJS~ DKJ5J._ I 036 F 037 - /03 P

Nfi-r,,:thcftJ 35.4 :f

) '!D. 2

J '67.D

I l-i I li I U

5u '{'{A 5 l~

PROJ3245

ANALYSIS TYF'E: IHSSOLVED METALS

TITLE: HASTINGS GROUNDWATER MATRIX: WATER LAB: EF·A REGION VII METHOD: 20011J77 GlA SAMPLE F'REF': _ _,vi..A __ ANALYST/ENTRY: ;~ REVIEWER: ---------- DATE: 01/06/E:6

SAMF'LE NUMBERS

DKJS2003 DKJS2004 DKJS2006 DKJS2006t1 ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u 10. u ALUMINUM UGIL ·50 u 50 u 50 u 50 u AF:SENI C UG/L 50 u 50 u 50 u 50 u BARIUM UG/L 250 ~ 150 ~ 190 :r 190 .:r BERYLLIUM UGIL "') u 2. u 2. u 2. u ... c.;Dr-iI UM UG/L NIA I NIA I NIA I N/A I COBALT UG/L 10. u 10. u 10. u 10. u Cl-iROMIUM UGIL 10. u 10. u 10. u 10. u COF"F'ER UG/L 10. u 10. u 10. u 10. u IRON UG/L 50 u 50 u 50 u 50 u MAt~GANESE UG/L 2. u 2. u 2. u 2. u MOLYBDENUM UG/L 10. u 10. u 10. u 10. u NICKEL UGIL 20 u 20 u 20 u 20 u LEAD UG/L NIA I N/A I NIA I N/A I ANTIMONY UG/L 50 u 50 u 50 u 50 u SELENIUM UG/L 50 u 50 u 50 u 50 u TIT,!;NIUM UG/L 50 u 50 u 50 u 50 u THALLIUM UG/L N/A I NIA I N/A I N/A I 1.)t1N.;r, r UM UG/L 10. u 10. u 10. u 10. ll

ZINC UG/L 52 1100 20 u 20 u CALCIUM MG/L 88 63 74 74 Mt!!GNESIUM MG/L 14 9.2 11 11 SODIUM MG/L 30 26 26 26 F'OT?.SSIUM MG/L 5.7 5.7 5.7 I:' I:'

..J • ..J

PROJ3246

ANALYSIS TYF'E! DISSOLl.'ED METALS

TITLE! HASTINGS GROUNDWATER MATF-.:IX: WATER LAB: EF'A F:EGI ON ~II ~ETHOD: -~001 W77 6:.~-1) SAMF'LE F'F:EF': __ &_L __ ANALYST /ENTRY: GS1 REVIEWER. __________ DATE: 01/06/86

))J'J SAMF'LE NUMBERS

DKJS2007 DKJS2012 Dl<JS2013 I:it,J32014 ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u 10. u ALUMINUM UG/L 50 u 50 u 50 u 50 u ARSENIC UGIL 50 u 50 u 50 u 50 u BARIUM UGIL 250 ~ ·340 j 230 .:r 280 :r f:ERYLL IUM UG/l 2. u .., u 2 • u .., u .... .:. .. CADi-iIUM UG/L N/A I N/A I N/i:i I NIA I cm:;.L T UG/L 10. u 10. u 10. u 10. u CHROMIUM UGIL 10. u 10. u 10. u 10. u COF'F'ER UG/L 10. u 10. u 10. u 10. u IRON UG/L 50 u 50 u 50 u 50 u MANGANESE UG/L 3.6 2.6 2.3 2.s MOLYBDENUM UG/L 10. u 10. u 10. u 10. u NICKEL UG/L 20 u 20 u 20· u 20 u LEAD UG/L NIA I N/A I NIA I N/A I ANTIMONY UGIL 50 u 50 u 50 u 50 u SELENIUM UG/L 50 u 50 u 50 u 50 u TITANIUM UGIL 50 u 50 u 50 u 50 u THALLIUM UG/L NIA I NIA I NIA I N/A I v,;N~1I.1 I UM UG/L 10. u 10. u 10. u 10. u ZI!~C UG/L 20 u 20 u 20 u 20 u U1LCIUM MG/L 92 100 70 73 MAGNESIUM MG/L 14 14 9,8 10. SG'OIUM .MG/L -.., .:,..., 24 23 32 FGTH'.:iSI UM MG/L 6,3 5.7 6. 6,

PROJ3247

... . .. .. .. ..

ANALYSIS TYPE: IHSSDLVED METALS

TITLE! HASTINGS GROUNI)WATER MATRIX: WATER LAB: EF·A REGION \..1 I I METHOD: 2001LJ77 ~L SAMPLE F·REF': _.../.Y.,M __ ANALYST/ENTRY! GSl F'.:E\.JI EWER: --------..!~ DATE: 01/06/86

Jtf!.J SAMPLE NUMBERS

DKJS2015 1:tKJS2024 DKJS2024D ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u ALUMINUM UG/L 50 u 50 u 50 u ARSENIC UG/L 50 u 50 u 50 u BAF:IUM UG/L 390 :r 130 J 140 J BERYLLIUM UG/L 2. u 2. u 2. u CADMIUM UG/L N/A I N/A I NIA I COBALT UG/L 10. u 10. u 10. u CHROMIUM UG/L 10. u 10. u 10. u COF'F'EF: UG/L 10. u 10. u 10. u IRON UG/L 50 u 50 u 50 u MANGANESE UG/L 2. u 2. u 2. u MOLYBDENUM UG/L 10. u 10. u 10. u NICKEL UG/L 20 u 20 u 20 u LEAD UG/L NIA I NIA I NIA I ANTIMONY UG/L 50 u 50 u 50 u SELENIUM UG/L 50 u 50 u 50 u TITi!iN!UM UG/L 50 u 50 u 50 u THAi...LIUM UG/L NIA I N/A I NIA I v.;NADIUM UG/L 10. u · 10. u 10. u ZINC UG/L 20 u 71 J 41 J CALCIUM MG/L 120 57 J 58 J M,;GNESIUM MG/L 16 9 ., .... J 9.4 J sor,IUM HG/L 34 25 j 25 j

F·OTASSIUM MG/L 7.7 4 ,.., • 7 J 4.9 J

PROJ3248

ANALYSIS TYPE! DISSOLVED METALS

TITLE: HASTINGS GROUNDWATER LAB: EPA REGION VII

MATRIX: WATER

sr-1MPLE PREP: _ _,&/.i __ ANALYST /ENTRY: GS2 )'Ii.()

METHOD: 2001W77 G-l.;r\ REVIEWER!------ DATE! 01/06/66

ELEMENT

SILVER ALUMINUM ARSENIC BARIUM BERYLLIUM CADMIUM COE:AL T CHROMIUM COPPER IRON MANGANESE MOLYBDENUM NICKEL LEAD ANTIMONY SELENIUM TITANIUM THALLIUM VANi!1DIUM ZINC CALCIUM MAGNESIUM 2,DDIUM POTASSIUM

UNITS

UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UG/L UG/L UGIL UG/L UG/L UGIL UG/L UG/L MG/L MG/L MG/l MG/L

I)l<JS2025

10. U 50 U 50 U

120 T 2. U

N/A I 10. U 10. U 10. U

500 190

10 • U 20 U

NIA I 50 U 50 U 50 U

NIA I 10. U

490 40 9.

20 3.7

DKJS2026

10. 50 50

170

N/A 10. 10. 19 50

140 10. 20

NIA 50 50 50

N/A 10.

560 57 10. 22

u u u J u I u u J u J u u I u u u I u J J J J

3.9 J

SAMPLE NUMBERS

DKJS2027

10. U 50 U 50 U 63 J

N/A

,., .... 10. 10. 10. 50 84 10. 20

NIA 50 50 50

NIA 10.

130 170

24 93

u I u u u u J u u I u u u I u J J J J

9.2 J

DKJS2029

10. U 50 U 50 U

260 :r 2. U

N/A I 10. U 10. U 10. U 50 U

2. U 10. U 20 U

N/A I 50 U 50 U 50 U

N/A I 10. U 20 U 77 11 30

5.3

PROJ3249

ANALYSIS TYPE: DISSOLVED METALS

TITLE! HASTINGS GROUNDWATER LAB! EPA REGION VII SAMF'LE F'REP:_..A/JA __ ANALYST/ENTRY: GS2

..b,tJ

ELEMENT

SILVER ALUMINUM ARSENIC BARIUM BERYLLIUM CADMIUM COBALT CHROMIUM C• F·PER IRON MANGANESE MOLYBDENUM NICKEL LEAD ANTIMONY SELENIUM TITANIUM THt1LLIUM VANADIUM ZINC Ci!1LCIUM MAGNESIUM SODIUM F·OTASSI UM

UNITS

UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UGIL UG/L UGIL UG/L UGIL UGIL UG/L UG/L MG/L MG/L

'MG/L MG/L

DKJS2030

10. 50 50

180 2.

N/A 10. 10. 10. 50 2.

10. 20

N/A 50 50 50

N/A 10. 20 67 10. 24

u u u :r u I u u u u

u u I u u u I u u

MATRIX! WATER METHOD: 2001W77 G-l-/1\ REVIEWER:------ DATE! 01/06/86

DKJS2031

10. 50 50

310 2.

N/A 10. 10. 10. 50

10. 20

NIA 50 50 50

NIA 11

190 93 13 33

u u u j u I u u u u u u u I u u u I

SAMPLE NUMBERS'

DKJS2032

10. 50 50

190

NIA 10. 10. 10. 50 2.

10. 20

NIA 50 50 50

N/A 10. 82

110 17 66 6,7

u u u ::r u I u u u u u u u I u u u I u

!1KJS2033

10. 50 50

180

N/A 10. 10. 10. 50

10. 20

NIA 50 50 50

NIA 10. 20

110 17 65 7.

u u u :r u I u u u u u u u I u u u I u u

PROJ3250


TITLE: HASTINGS GROUNDWATER LAB: EPA REGIO~ .VII

MATRIX: WATER

SAMPLE F'REP: _.../.Yj.11__ ANALYST /ENTRY: ~ll METHOD: 2001W77 b-~ REVIEWER!---------- DATE: 01/06/86

SAMPLE NUMBERS

DKJS2036F DKJS2037F

ELEMENT UNITS

SILVER UG/L 10, u 10, u ALUMINUM UG/L 50 u 50 u ARSENIC UG/L 50 u 50 u BAF,IUM UG/L 2. u 2. u BERYLLIUM UG/L 2. u .., u .... CADMIUM UG/L N/A I N/A I COBALT UG/L 10, u 10, u CHROMIUM UG/L 10, u 10, u COPPER UG/L 10, u 10, u IRON UG/L 50 u 50 u MANGANESE UG/L 2. u 2, u MOLYBDENUM UG/L 10. u 10, u NICKEL UG/L 20 u 20 u LEAD UG/L N/A I N/A I ANTIMONY UG/L 50 u 50 u SELENIUM UG/L 50 u 50 u TITANIUM UG/L 50 u 50 u THALLIUM UG/L N/A I N/A I VANADIUM UG/L 10. u 10. u ZINC UG/L 20 u 20 u CALCIUM MG/L 2. u 2. u Mi!tGNESIUM MG/L 2. u 2. u SODIUM MG/L 2. u 2. u F·•TASS IUM MG/L 2. u 2. u

J PROJ3251

ANALYSIS TYPE: TOTAL HETALS

TITLE: HASTINGS, NEBR. MATRIX: WATER LAB: EPA REGION VII METHOD: 2001W77 l SAMPLE PREP: __ G,-.1/.Ji. ANALYST /ENTRY: ;~ REVIEWER: ______ G~:..t!'i .DATE: 01/14/86

SAMPLE NUMBERS

DKJS2024 DKJS202•D DKJS2026 DKJS2027 ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u 10. u ALUHINUH UG/L so u so u 210 10000 ARSENIC UG/L :so u so u so u 50 u BARIUM UG/L 1.-0 1 "0 520 200 BERYLLIUM UG/L 2. u 2. u 2, u 2. u CADHIUH UG/L s. u s. u 140 s. u COBALT UG/L 10. u 10. u 10. u 13 CHROMIUM UG/L 10. u 10. u 15 11 COPPER UG/L 10. u 10. u 2700 23 IRON UG/L so u so u 98000 9200 MANGANESE UG/L 2. u 2. u "80 390 MOLYBDENUM UG/L 10. u 10. u 12 10. u NICKEL UG/L 20 u 20 u 25 20 u LEAD UG/L so u so u 1200 so u ANTIMONY UG/L so u so u 50 u so u SELENIUH UG/L so u so u 50 u so u TITANIUM UG/L so u 50 u so u 260 THALLIUM UG/L NIA I NIA I NIA I N/A I VANADIUM UG/L 10. u 10. u 41 23 ZINC UG/L 79 48 14000 230 CALCIUM 116/L S9 59 61 180 MAGNESIUM HG/L 9.2 9.3 11 26 SODIUM MG/L 25 26 2S 98 POTASSIUM HG/L 3.4 3,4 4.3 11

I PR013252

- , .. . . ... ......

Appendix 8-4

Ground iater Analyses

March 1986

H PROJ3253

. . . ....... • .. ··----•4·• -~ .• -··· _ .. --~ --··:· ·--· - -· ..... ··------------.....--.!--•,.,_.__ J•----------~~--------'•

ANALYSIS TYP~; ~l§SOLVEP ~ET~LS

TITLE: HASTINGS MATRIX: IJATER LAB: EPA REGION VII METHOD: 2001W77 (;.l./7\ SAHPLE PREP:_..A/JJ __ ANALYST/ENTRY: ;,U REVIEWER:---------- DATE: 03/26/86

ELEMENT UNITS

SILVER UG/L ALUMINUM UG/L ARSENIC UG/L BARIUM UG/L BERYLLIUM UG/L CADHlUH UG/L COBALT UG/L CHROMIUM UG/L COPPER UG/L IRON UG/L MANGANESE UG/L MOLYBDENUM UG/L NICKEL UG/L LEAD UG/L ANTIMONY UG/L SELENIUM UG/L ;"ITANIUM UG/L THALLIUM UG/L VANADIUM UG/L ZINC UG/L CALCIUM HG/L MAGNESIUM MG/L SODIUM HG/L POTASSIUM HG/L

FKJS2021

10. so so 67 2. 5.

10. 10. 10. 77 70 10. 20 so so so so

N/A 11

1SO 200

27 120

NIA

u u u

u u u u u

u u u u u u I

I

SAMPLE NUMBERS

-~-·

PROJ3254

.. ,• .. . -••'· .... · ....... -- _ .. ___ _ - . . -·· •-1. :.,._._. ·-·- .••• -· ··-.:-.. ---.---~···---•··-""-----·,--·-:- .... __________ .J" •


TITLE: HASTINGS . LAB: EPA REGIO~ V!I SAMPLE PREP: _~L/r-__ 1".NAL YST /ENTRY: JU

ELEMENT

SILVER ALUHINUH ARSENIC BARIUM BERYLLIUM CADMIUM COBALT CHROMIUM COPPER IRON HANGANESE HOLYBDENUH NICKEL LEAD ANTIMONY SELENIUM TITANIUH THALLIUM VANADIUM ZINC CALCIUM MAGNESIUM SODIUM POTASSIUM

UNITS

UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L HG/L HG/L MG/L MG/L

FKJS2010

10. U so u 50 lJ

230 2. U s. ll

10. U 10. U 10. U so u

2.6 10 • U 20 U :SO LI so u 50 LI so u

N/A I 10 • U

180 81 13 32

N/A I

MATRIX! WATER METHOD: 2001W77 G-<-1'\ REVIEWER:---------- DATE: 03/26/86

FKJS2011

10. :so 50

250

s. 10. 10. 10. so 2.4

10. 20 so :so so so

N/A 10. 98 80 13 29

N/A

u lJ u

u u u u u u

u u u lJ u lJ I u

I

SAMPLE NUMBERS

FKJS2012

10. U :SO ll 50 U

140 2. LI s. u

10. U 10. lJ 10 • LI so u 2.a

10. lJ 20 U 50 U so u so lJ so u

NIA I 10. U 99

120 17 · 61

N/A I

I

FKJS2012D

10. U so u so u

170 2. U s. u

10. U 10. U 10. U 50 U

2.3 10. U 20 U so u so u so u so u

H/A I 10. U

100 120

18 62

NIA I

PROJ3255

·• .... . - . - . -· · ...... -. .. · .. ·- -•-.·--·· ····-·· ·=-······-·····-·-----•.'·-·•-~· .. ~. ·• .. , - -·-. -· ---- ----· ·-.~ - - . -

ANALYSIS TYPE: TOTAL METALS

TITLE: HASTINGS,NEB. MATRIX: IJATER LAB: EPA REGION VII METHOD: 2001W77 ,1J SAMPLE PREP: __ ~1L"-- ANALYST/ENTRY: GMS REVIEWER: 11,J--Y-----:- DATE: 03/17/86

''r,'} SAMPLE NUM!<ERS

FKJS2010 FKJS2011 FKJ'.32012 FK JS2012D ELEMENT UNITS

SILVER UG/L 10, u 10, u 10. u 10, u ALUMINUM UG/L 71 so u 1300 1400 ARSCNIC UG/L so u so u so u so u BARIUM UG/L 230 230 100 170 BERYLLIUM UG/L 2. u ,, ... . u 2. u ,,

~ . u CADMIUM UG/L s. u s. u s. u s. u COBALT UG/L 10. u 10, u 10, u 10. u CHROMIUM UG/L 1 0 . u 1 0 . u iO. u 10, u COPPCR UG/L 10 I u 10. u 1 0 . u 10, u IRON UG/L 150 73 1200 1200 MANGANESE UG/L 2.2 2, u 24 19-MOLYDDENUM UG/L 10, u 10, u 10, u 1 0 . u NICl<I:::L UG/L 20 u 20 u 20 u 20 u LEAD UG/L so u so u so u so u ANTIMONY UG/L so u so u so u so u SELENIUM UG/L so u so u so u so u TITANIUM UG/L so u so u so u so u THALLIUM UG/L 300 u 300 u 300 u 300 u VANADIUM UG/L 10, u 10. u 10. u 10, u ZINC UG/L 170 87 130 110 CALCIUM MG/L 79 7S 120 110 MAGNESIUM MG/L 13 13 17 17 SODIUM MG/L 32 2!3 SB SB POTASSIUM MG/L 7,6 7,6 10. 10.

PROJ3256

·~ - ..... -... - ... ; ....... - ........ '. ·- -···- -- ---·--- -•-···-: ... ·--··-- ··•------•-·-. ·-~-

ANALYSIS TYPE: DISSOLVcD METALS t ~ I ., .... I I r ~ ~ . ~ \.- : :·. ~. : . 1. •·'

TITLE: HASTINGS HATRIX: WATER LAB: EPA REGION VII METHOD: 2001 U77 G LJ!> SAHPLE PREP:_f-A __ ANALYST/ENTRY! GS4 R~VIEWER! -------- _ D~TE! 03/26/86

..b~ SAHPLE NUHBERS

FKJS2001 FKJS:2002 FKJS:?003 FKJS:?004 ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u 10. u ALUMINUM UG/L so u so ll so u so u ARSENIC UG/L so u so u so u so u BARIUH UG/L 120 190 170 150 BERYLLIUM UG/L 2. LI 2 • u 2. u 2 • u CADH IUH UG/L s. u s. u s. u s. u COBALT UG/L 10. u 10. u 10. u 10. u CHROMIUM UG/L 10. u 10. u 10. u 10. u COPPER UG/L 10. u 10. LI 10. u 10. u IRON UG/L so u so u so lJ so u MANGANESE UG/L 7.6 2. 2. u 2. u MOLYBDENUM UG/L 10. u 10. u 10. u 10. u NICKEL UG/L 20 u 20 u 20 u 20 u LEAD UG/L so u 50 u so u so u ANTIMONY UG/L so u so u so u so u SELENIUM UG/L so u 50 u so u so u TITANIUM UG/L so u so u so u so u THALLIUM UG/L N/A I N/A I NIA I H/A I VANADIUM UG/L 12 10. u 10. u 11 ZINC UG/L 3·9 90 31 20 u CALCIUM HG/L 100 68 110 57 MAGNESIUM .HG/L 16 11 16 8.7 SODIUH HG/L SB 31 62 25 POTASSIUM MG/L N/A I H/A 1 H/A I NIA 1

.:

B PR013257

\ . :>' ...,

-·· ... .•. -·- -·--·-~· -~-' .... __ . ._.-.!... ~.,: ............ .--.:.,:.. C. ,-. ........ ~----•: • .,,:,_~·:.-:.,,,....,,, •• ~-~-~----·--·-- :...... ..... _ .... .,,1, ._ _ __,._ •

ANALYSIS TYPE! TOT~L HETALS.

TITLE! HASTINGS LAB: EPA REGION VII SAMPLE PREP: _ _vM_ ~NALYSTIENTRY: GRS

lJ~

MATRIX: WATER METHOfl: 200 l lJ77 / 2.1'\ REVIEWER! ~---\J'"___ DATE: 0~/08/86

ELEMENT

SILVER ALUMINUM ARSENIC BARIUM BERYLLIUM CADMIUM COBALT CHROMIUM COPF'ER IRON MANGANESE HOL YB!tENUH NICKEL LEAD ANTIMOHY SELENIUM TITANIUM THALLIUM VANA!1 I UH ZINC CALCIUM MAGNESIUM SODIUM POTASSIUM

UHITS

UG/L UG/L UG/L UG/L UGIL UG/L UG/L UGIL UG/L UG/L UGIL UG/L UG/L UG/L UG/L UG/L UGIL UG/L UGIL UG/L HG/L MGIL MGIL MG/L

FKJS2022

10. 83 so

120 2. s.

10. 10. 20

2-,0 6.

10. 20 so so so so

NIA 10.

260 47 7.8

23 NIA

u

u

u u u u

u u u u u u I u

I

FKJS20::?5

10. so so

2~0 2.

53 10. 10. 96

17000 190

10. 20

360 so so so

H/A 10.

5700 64 11 26

H/A

u u LI

u

u u

ti LI

lJ ll u I u

I

SAMPLE NUMBERS

FKJS2026

10. 150 so

400

110 10. 10.

720 : 84000

470 15 20

1800 so so so

N/A 42

24000 69 12 26

NIA

u

u

u

u u

u

u u u I

I

PROJ3258

.. - . . . . . . ~-.. . ... . ··~ ·. . .., .• _.._.~., ,_. .-. ~ .•,:;.. .• •:-•·•--••4~ •• ·•-i-.·- ~.,·-~----•-••·..-....'·b..,.....::a... ... •,..:.,,1o.•,.,••-.:-.-.:-. .-1--• _ _:,. ______ .• •·• _

ANALYSIS TYPE: DISSOLVED HETAL9

TITLE! HASTINGS HATRIX: WATER LAB: EPA REGIO~ VII METHOD: 2001 W77 G-'-1'\ SAMPLE PREP:_F-"~-- ANALYST/ENTRY: ;U REVIEWER:---------- !Jf'ITE: 03/26/86

SAMPLE NUMBERS

FKJS2016 FKJS:?019 FKJS:?019 FKJS2020 ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u 10. u ALUMINUM UG/L so u so u so u so u ARSENIC UG/L so u so u so u so u BARIUM UG/L 360 250 180 310 BERYLLIUM UG/L 2 . u 2. u 2. u 2. u CADHIUl1 UG/L s. u s. u s. u s. u COBALT UG/L 10. u 10. lJ 10. u 10. u CHROMIUM UG/L 18 10. u 10. u 10. u COPPER UG/L 10. u 10. u 10. u 10. u IRON UG/L so u so ll so ll 51 MANGANESE UG/L 2. u 2. u 2. u 4.6 MOLYBDENUM UG/L 10. u 10. u 10. u 10. u NICKEL UG/L 20 u 20 u 20 u 20 u LEAD UG/L so u so u so lJ 50 u ANTIMONY UG/L so u so u so u 50 u SELENIUM UG/L so u so u so u 50 u TITANIUM UG/L 50 u 50 u so u so u THALLIUM UG/L N/A I H/A I H/A I N/A I VANADIUM UG/L 14 10. u 10. u 10. u ZINC UG/L 20 u 20 u 130 160 CALCIUM HG/L 100 94 S7 110 MAGNESIUM HG/L 14 1-4 9.7 18 SOI1IUH MG/L 27 3S 31 37 POTASSIUM HG/L H/A I H/A I NIA I N/A I

PROJ3259

..... ... . . ..,..,. • • .. :..:_ •• _,:. . .,:_ ••• .: . .:-•-'--- ._:,_ - •-•n=•-----...-_ ..... ______ .. ,_. •-·•••.,,,,..,·-•-••-••-._

: :~'-~:. • :-•. 1 ~- i j r r ' .... :'· • •. :- 1t •~ i: I I • ~ ~

ANALYSIS TYPE: DISSOLVED t1ETALS . I· •·· . . .. ..,

TITLE: HASTINGS MATRIX: LJATER LAB: EPA REGION VII METHOD: 2001W77 GL.f>'\ SAMPLE PREP:_ft-Ld' __ ~NALYST/ENTRY: i~ REVIEWER:---------- DATE: 03/26/86

SAHPLE NUHBERS

FKJS2005 FKJS2007 FKJS2008 FKJS2009F ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. lJ 10. u ALUMINUM UG/L so u so u so u so u ARSENIC UG/L so u so u so u so u BARIUM UG/L 190 180 180 2. u BERYLLIUM UG/L 2. LI 2. u 2. u "'I .... u CADMIUM UG/L s. u s. u s. u s. u COBALT UG/L 10. u 10. LI 10. u 10. u CHROMIUM UG/L 10. u 10. ll 10. u 10. u COPPER UG/L 10. u 10. u 10. u 10. u IRON UG/L so u so u so u so u HANGANESE UG/L 2. u 2. 2. u 2. u MOLYBDENUM UG/L 10. u 10. u 10. u 10. u NICKEL UG/L 20 ll 20 ll 20 ll 20 u LEAD UG/L so u so u so u 50 u ANTIMONY UG/L so u so u so u so u SELENIUM UG/L 50 u 50 lJ 50 lJ so u TITANIUM UG/L so LI so lJ 50 u so u THALLIUM UG/L N/A I N/A I N/A I N/A I VANADIUM UG/L 10. u 10. 10. u 10. u ZINC UG/L 20 u 20 u 49 20 u CALCIUM HG/L 66 52 54 2. u MAGNESIUM l1G/L 9.3 ,.s a.1 2. u SODIUM HG/L 25 18 19 2. u POTASSIUM HG/L NIA I N/A I N/A I N/A I

PROJ3260 \

>

. • - .. --·. :•·\, • • • :. '1.1!: - - • .. ·•· _ _:_: :., : .... - • - .•. - ~--•-·:-• ......... L.. ~4, • .. -~ •-""t.-. .. :...~:----.t -·!-.&..!·-:-.-i....:.t......:a..-. _ __, __ :. .. : • . --:·._.I,·-•·-·_ ... "

ANALYSIS TYPE: TOTAL ME1A.LS

TITLE: HASTINGS,NEB. LAB: EPA REGION VII SAMPLE PREP: __ ~0-- ANALYST/CNTRY: GMS

~ Lf'\

MATRIX: I.JATER METHOD: 200iW77 J Q REVIEWER: tfh--~M-

SAMPLE NUMBERS

Fl<JS2016 FKJS2018 FKJS2019 ELEMENT

SILVER ALUMINUM ARSENIC BARIUM BERYLLIUM CADMIUM COBALT CHROMIUM COPPER IRON MANGANESE MOL 'rnDENUM NI Cl<EL LEAD ANTIMONY SELENIUM TITANIUM THALLIUM VANADIUM ZINC CALCIUM MAGNESIUM SODIUM POTASSIUM

UNITS

UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L HG/L

- MG/L MG/L MG/L

10, so so

330 ,:, .... s.

10. 13 10. so

,:, .... 10. 20 so so so so

300 ii 20 93 13 25 8.

u u u

u u u

u u u u u u u u u u

u

10, so so

2SO 2, s.

10. 10, 1 0 .

230 4.4

10. 20 so so so so

300 10. 20 88 14 33 8,1

u u u

u u u u u

u u u u u u u u u

10. U 330 so u

160 2. · U

u u u

s. 10, 10.

10, 410

7. 10. 20 so so so so

300 10.

130

8,7 20 7.9

u u u u u u u u

DATE: 03/17/06

FK JS2020

10, so so

290

s. 10. 10. 13

230 5,3

10, 20 so so so so

300 10,

240 100

17 36

8,1

u u u

u u u u

u u u u u u u u

J PROJ3261

... • .,. .L. .. :. --·· . -...... ... .;.. ..... ..,. ·•----·-· ..... ·--·---··-··----·-·-' .... ·---·---···-·- .. ·-··•

ANALYSIS TYPE: TOTAL METALS . ·- ..

; •: I . ... , I .·,

TITLE: HASTINGS,NEB, MATRIX: tJATER LAB: EPA RCGION VII METHOD: 2001.W77 ~ SriMPLE PREP: __ f_L~- ANALYST/ENTRY: GMS RCVICWER:~-~- ___ DATE:: 03/17/06

~I.ft\ SAMPLE NUMf.<ERS

FKJS2001 Fl(JS20 02 FKJS2003 FJ<JS2004 ELEMENT UNITS

SILVER UG/L 10, u 10. u 10. u 10, u ALUMINUM UG/L 730 110 230 so u ARSENIC UG/L so u so u so u so u BARIUM UG/L 140 160 1SO 140 BERYLLIUM UG/L ,:, ... ' u 2, u ,:, .... u 2. u CADMIUM UG/L s. u s. u s. u s. u COBALT UG/L 10, u 10. u 10, u 10, u CHROMIUM UG/L 10. u 10, u 10, u 10. u COPPER UG/L 10, u 13 10, u 10, u IRON UG/L 600 320 220 so u HANGANCSE UG/L so 6.1 4, ,:, .... u MOL Yr{DENUM UG/L 10, u 10. u 1 0 , u 10, u NICl<EL UG/L 20 u 20 u 20 u 20 u LEAD UG/L so u so u so u so u ANTIMONY UG/L so u so u so u so u SELENIUM UG/L so u so u so u so u TITANIUM UG/L so u so u so u so u THALLIUM UG/L 300 u 300 u 300 u 300 u VANADIUM UG/L 10, u 10, u 10, u 10, u ZINC UG/L 30 1S0 20 u 20 u CALCIUM MG/L 100 64 i 00 S4 MAGNESIUM MG/L 16 11 16 8,6 SODIUM ~- MG/L 62 29 sa 24 POTASSIUM HG/L 9,4 7,6 8,B 7,6

.., '

PROJ3262

. . . . .. . .•. - .... f• ·--··· - ·----·- ··- .. ~-··· ·---· .. , ~---- . .._·-·----·-·----·--··-----·-··- - .:.. ... -- _ .... ! •

ANALYSIS TYPE: TOTAL METALS

TITLE: IIASTINGS,NEB. MATRIX: WATER LAB: EPA RCGION VII HCTHOD: 2001W77 ~ SAMPLE PREP: __ ~<1- ANALYST/ENTRY: GMS REVIEWER: {jiJ-_p ______ DATE: 03/17/0b

G-i..l'\ SAMPLE NUMBERS

FKJS200S FKJS20 07 FKJS2008 Fl<JS200?F ELEMENT UNITS

SILVER UG/L 10. u 10. u 10. u 10. u ALUMINUM UG/L so u so u so u so u ARSENIC UG/L so u so u ~o u so u BARIUM UG/L 180 170 160 ,:,

'- . u BERYLLIUM UG/L ':) u 2. u ,:, u ,:, u .... ,_. ,_ . CADMIUM UG/L s. u s. u s. u ,... u ..) . COBALT UG/L 10, u 10. u 10. u 10. u CHROMIUM UG/L 10, u 10. u 10, u 10. u COPPER UG/L 10. u 10. u 10, u 10. u IRON UG/L so u 190 so u so u MANGANESE UG/L "'J ... . u 2. u "'J .... u "'J

'- . u HOLYE:DENUM UG/L 10. u 10. u 10. u 10. u NICl<EL UG/L 20 u 20 u 20 u 20 u LEAD UG/L so u so u so u so u ANTIMONY UG/L so u so u so u so u SELENIUM UG/L so u so u so u so u TITANIUM UG/L so u so u so u so u THALLIUM UG/L 300 u 30 0 u 300 u 300 u VANADIUM UG/L 11 10. u 10. u 10, u ZINC UG/L 20 u -33 3!j 20 u CALCIUM MG/L 63 40 so 2. u MAGNESIUM MG/L 9.2 7,S 7.8 ., ... u SODIUM MG/L 24 18 18 ,., u ,_ . POTASSIUM HG/L 7,6 7.6 S.3 ':) .... u

PROJ3263

. __ .,: __ . - · •.. --··· -···. ·-·-· • .,. ·,. ___ _. __ ~- ........ -:-.- .:,.; _________ _.... ..... ,_-,....,,J,,,,;...._,~-1 • ._.....,_ .. ~ .• ·---:.·-· --- ·- -·-

iITLE: IIAGTHIGS,NEB, LAB: EPA RCGION VII

. ANALY~IG TYP.E: TqTAL ~ETAL~

SAMPLE PREP: __ ~=0..- ANALYST/ENTRY: GHS G-'-f'l

MATRIX: WATER METHOD: 2O01W77 ... , RCVICWCR: .fc!J__Jtl~-

SAMPLI::: NUMBERS

FKJS202i

ELEMENT UNITS

SILVER UG/L 10, u ALUMINUM UG/L 1700 ARSENIC UG/L so u BARIUM UG/L 83 BERYLLIUM UG/L 2. u CADMIUM UG/L s. u COBALT UG/L i0, u CHROMIUM UG/L 10. u COPPER UG/L 10. u IRON UG/L 1600 MANGANESE UG/L 90 MOLYBDENUM UG/L i0, u NICKEL UG/L 20 u LEAD UG/L so u ANTIMONY UG/L so u SELENIUM UG/L so u TITANIUM UG/L so u THALLIUM UG/L 300 u VANADIUM UG/L 10. u ZINC UG/L 1S0 CALCIUM MG/L 190 HAGNESIUM MG/L 26 SODIUM MG/L 110 POTASSIUM MG/L 14

DATE: 03/17/06

PROJ3264

- - ........... - .. ... ··-· -----~• ... _. __ •·- -=- :-.-..... - --·-. ---·--=-------------_..._ •·----- __ ..... ___ ..,,,. _____ .


TITLE: HASTINGS LAB: EPA REGION VII SAMPLE PREP:-P-A-- ANALYST/ENTRY: GSS

.Z,11\J

ELEMENT

SILVER ALUMINUM ARSENIC BARIUM BERYLLIUH CADMIUM COBALT CHROHIUH COPPER IRON MANGANESE HOLYBDEHUH NICKEL LEAD ANTIMONY SELENIUM TITANIUM THALLIUM VANADIUM ZINC CALCIUM MAGNESIUM SODIUM POTASSIUM

UNITS

UGIL UG/L UG/L UG/L UG/L UG/L UG/L UGIL UGIL UG/L UG/L UGIL UGIL UG/L UG/L UG/L UG/L UG/L UG/L UG/L HGIL HGIL HG/L HG/L

FKJS2022

10. so so

120

s. 10. 10. 10. 67 4.7

10. 20 so so so so

N/A 10. 52 47 7.9

23 NIA

u LI u

u u u LI u

u u u u u u I u

I

HATRIX: WATER HETHOD: 2<>01W77 GJ_r) REVIEWER: .i,r<.J._______ D~TE: 03/26/86

F'KJS202S

10, .so so

190 2.

21 10. 10. 10. so

180 10. 20 so so so so

N/A 10.

2500 56 11 26

N/A

LI u LI

u

u LI u u

u u LI u u Lt I u

I

SAMPLE NUMBERS

F'KJS2026

10. .so so

230 2.

15 10. 10. 11 so 88 10. 20 so so so so

NIA 10.

2100 70 12 26

NIA

u u u

u

u u

u

u u u u u u I u

I

PROJ3265


TITLE: HASTINGS--MARCH SAMPLING MATRIX: WATER UNITS: UG/L LAB: AQT HETH DD: 9302M6:t @__ CASE: 5673 SAMF'LE F·REF': ------- ANALYST/ENTRY: Al'\1 REVIEWER :(14-,.JLI!} ____ t1ATE: 0'1/24/8~

SAMPLE NUMBERS

FKJ52001 F1'JS2002 FKJS2003 FKJS:?004 COMPOUND

CHLOROMETHANE 2.00 u 2.00 u 2.00 u 2.00 I BROMOMETHANE 2. 00 u :;.oo u 2.00 u 2.00 l IJ!NYL CHLORIDE 2.00 u 2.00 u 2.00 u 2.00 l CHLOROETHANE 2.00 u 2.00 u :2-00 u 2.00 t METHYLENE CHLORIDE 1.00 u 1. 00 u 1.00 u 1.00 L ACETONE 2.00 u 2.00 u 7.00 u 2.00 L CARBON DISULFH1E 1.00 u 1.00 u 1.00 u 1.00 u 1 , 1 t1 I CHLOROETHENE 1.00 u 1. 00 u 1.00 u 1.00 u 1, l DICHLOROETHANE 1.00 u 1. 00 u 1.00 u 1.00 u TRANS-1,2,-DICHLOROETHENE 1.00 u 1.00 u 1.00 u 1.00 u CHLOROFORM 1.00 u 1.00 u 1.00 u 1.00 u 1,2,DICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 2-BUTANONE 2. 00 u 2.00 u 2.00 u 2.00 u 1,1,1 TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u CARBON TETRACHLORIDE LOO u 1.00 u 1.00 u 1.00 u VINYL ACETATE 2.00 u 2.00 u 2.00 u 2.00 u BROMODICHLOROMETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2,2,-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROF'ROPANE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,3-DICHLOROPROF'ENE 1.00 u 1.00 u 1.00 u 1.00 u TRICHLOROETHENE 90.0 100 J 2.40 1.00 u DIBROMOCHLOROMETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE 1.00 u 1.00 u 1.00 u 1.00 u CIS-1,3-DICHLOROF'ROPENE LOO u LOO u 1.00 u 1.00 u :-CHLOROETH'fL VINYL ETHEF: I I I I BF:OMOFORM 1.00 u 1.00 u 1.00 u 1.00 u 2-HEXANONE :2.00 u :2.00 u 2. 00 u 2,00 u 4-METHYL-2-PENTANONE 2,00 u 2,00 u 2.00 u 2.00 u TETRACHLOROETHENE o.7 Ii o.7 M 1.00 u 1.00 u TOLUENE 1.00 u 1.00 u 1. 00 u 1.00 u CHLOROBENZENE 1.00 u 1.00 u 1.00 u 1,00 u ETHYL BENZENE 1.00 u LOO u 1.00 u 1.00 u STYRENE 1.00 u 1.00 u 1.00 u 1,00 u TOTAL XYLEMES 1.00 u LOO u 1.00 u 1.00 u

PROJ3266 ....... '\./1 p'


TITLE: HAST INGS--MARCH SAMPLING MATRIX: WATER murs: UG/L LAB: AGT METHOD: 9302~ CASE: 5673 SAMPLE PREP: _______ ANALYST/ENTRY! AM1 RE IJ IE lJ ER : ~~ - - - _ DATE: 04/24/86

SAMPLE NUMBEF:S

FKJS2009F FKJ52010 FKJS2011 FKJ52012 COMPOUND

CHLO ROME THANE 2.00 u 2.00 u 2.00 u 50.0 u BROHOMETHANE 2.00 u 2.00 u .2, 00 u 50.0 u IJINYL CHLORIDE 2. 00 u 2.00 u 2,00 u 50,0 u CHLOROETHANE 2,00 u :::! , 00 u 2,00 u 50.0 u METHYLENE CHLORIDE 200 1.00 u 1,00 u 25. 0 u ACETONE 26.0 2.00 u :::! • 00 u 50.0 u CARBON t1ISULFIDE 1.00 u 1.00 u 1.00 u 25.0 u l , 1 t1 I CHL OROETHENE 1.00 u 1.00 u 1.00 u 25.0 u 1, 1 DICHLOROETHANE 1.00 u 1.00 u 1. 00 u 25. 0 u TRANS-1,2,-DICHLOROETHENE LOO u 1.00 u 1.00 u 34.0 CHLOROFORM 1.00 u 1.00 u 1.00 u 25.0 u 1,2,DICHLOROETHANE 1.00 u 1.00 u 1.00 u 2s.o u 2-BUTANONE 2.00 u 2.00 u 2.00 u 50.0 u 1, 1, 1 TRICHLOROETHANE LOO u 1.00 u 1.00 u 40.0 CARBON TETRACHLORIDE 1.00 u 0.7 M 2-i .o 25,0 u '-..1INYL ACETATE 2,00 u 2.00 u 2,00 u 50.0 u BROHODICHLOROMETHANE 1.00 u 1.00 u 1.00 u 25.0 u 1,1,2,2,-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 25.0 u 1,2-DICHLOROPROPANE 1.00 u LOO u 1.00 u 25.0 u TRANS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1,00 u 25,0 u TRICHLOROETHENE 1.00 u 22.0 21,0 3500. DIBROMOCHLOROMETHANE 1.00 u 1.00 u 1.00 u 25.0 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 25,0 u BENZENE 1,00 u 1.00 u 1.00 u 25.0 u CIS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 25·, 0 u 2-CHLOROETHYL VINYL ETHER I I I I BROMOFORM LOO u 1, 00 u 1.00 u 25.0 u 2-HEXANONE 2,00 u 2,00 u 2,00 u 50.0 u 4-METHYL-2-PENTANONE 2,00 u 2,00 u 2.00 u 50.0 u TETRACHLOROETHENE 1.00 u 1.00 u 1.00 u 42.0 TOLUENE 1.00 u 1,00 u 1.00 u 42,0 u CHLOROBENZENE 1.00 u 1.00 u 1.00 u 25,0 u ETHYL BENZENE 1,00 u 1,00 u 1.00 u 25.0 u STYRENE 1.00 u 1.00 u 1,00 u 25,0 u TOTAL XYLDlES 1.00 u 1.00 u 1.00 u 25,0 u

PROJ3267


TITLE! HASTINGS--MARCH SAMPLHlG MATRIX! tJATER UNITS! UG/L LAB! AQT HETHOD: 9302H~1Q__ CASE: 5673 SAMPLE PREP: _______ ANALYST/ENTRY! AM! REVIEWER!~ ___ DATE! 0~/24/86

SAMPLE NUMBERS

FKJS2012D FKJS2013 FKJS.2014 FKJS201:S COMPOUND

CHLOROMETHANE 50,0 u 2.00 u 2.00 u 2.00 u BROMOMETHANE 50.0 u 2.00 u 2.00 u 2.00 u \JI NYL CHLORIDE so.o u 2.00 u 2.00 u 2.00 u CHLORDETHANE 50,0 u 2.00 u 2,00 u 2,00 u METHYLENE CHLORIDE 25,0 u 1.00 u 1.00 u 1,00 u ~-:icETONE 50,0 u 2,00 u 2,00 u 2,00 u CARBON DISULFIDE 25,0 u 1.00 u 1.00 u 1,00 u 1, 1 DICHLOROETHENE 25,0 u 1.00 u 1,00 u 1.00 u 1 , 1 DICHLOROETHANE 25,0 u 1.00 u 1.00 u 1,00 u TRANS-1,2,-DICHLOROETHENE 33,0 1.00 u 1.00 u 1.00 u CHLOROFORM 25,0 u 1,00 u 1.00 u 1.00 u 1,2,DICHLOROETHANE 25,0 u 1,00 u 1.00 u 1.00 u 2-BUTANONE so.a u 2.00 u 2.00 u 2.00 u 1, 1 , 1 TRICHLOROETHANE 38.0 1.00 u 1.00 u 1,00 u CARBON TETRACHLORHIE 25,0 u 1.00 u 1.00 u 1.00 u VINYL ACETATE 50.0 u 2.00 u 2 • 00 u 2.00 u BROMODICHLOROHETHANE 25,0 u 1.00 u 1.00 u 1,00 u 1,1,2,2,-TETRACHLOROETHANE 25,0 u 1.00 u 1.00 u 1,00 u 1,2-DICHLOROPROPANE 25,0 u 1.00 u LOO u 1.00 u TRANS-1,3-DICHLOROPROPENE 25.0 u 1.00 u 1.00 u 1,00 u TRICHLOROETHENE 3500. 1.70 1.30 1.70 DIBROMOCHLOROMETHANE 25,0 u 1,00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 25,0 u 1 .• 00 u 1.00 u 1.00 u BENZENE 25.0 u LOO u 1.00 u 1.00 u CIS-1,3-DICHLOROPROPENE 25,0 u 1.00 u 1.00 u 1.00 u 2-CHLOROETHYL VINYL ETHER I I I I BROMOFORH 25,0 u 1.00 u 1.00 u 1,00 u 2-HEXANONE 50,0 u 2,00 u 2,00 u 2,00 u 4-METHYL-2-PEHTANONE 50.0 u 2,00 u 2,00 u 2.00 u TETRACHLOROETHENE 42,0 1.00 u 1.00 u 1,00 u TOLUENE 38,0 u 1,00 u 1.00 u 1.00 u CHLOROBENZENE 25,0 u 1.00 u 1.00 u 1.00 u ETHYL BENZENE 25.0 u 1.00 u 1.00 u 1,00 u STYRENE 25.0 u 1.00 u 1.00 u 1,00 u TOTAL XYLENES 25,0 u 1.00 u 1.00 u 1.00 u

PROJ3268


TITLE: HASTINGS--MARCH SAMF'LING MATRIX: WATER UNITS: UG/L LAB: AQT METHOD: 93~ CASE: 5673 SAMF'LE F'F:EF': _______ ANALYST/ENTRY: AMl REVIEWER: _____ tlfHE: 01/:?4/86

SAMF'LE NUMBERS

FKJS:?005 FKJS2006 FKJS2007 FKJS2008 COMPOUND

CHLOROMETHANE 2.00 u ::?.OO u 2.00 u 2-. 00 u BROMOHETHANE 2.00 u 2.00 u 2.00 u 2. 0 0 u l,,'!NYL CHLORIDE 2,00 u 2. 0 0 u 2,00 u 2,00 u CHLOROETHANE 2.00 u 2.00 u 2.00 u 2.00 u METHYLENE CHLOR IC1E LOO u 1.00 u 1.00 u 1.00 u ACETONE 2.00 u 2,00 u 2,00 u 2,00 u CtiRBON DISULFIDE 1.00 u 1,00 u 1.00 u 1,00 u 1 , 1 DICHLOROETHENE 1.00 u 1.00 u 1.00 u 1.00 u 1 , l DICHLOROETHANE 1.00 u 1,00 u 1.00 u 1.00 u TRANS-1,2,-DICHLDROETHENE 1,80 1,00 u 1.00 u 1,00 u CHLOROFORM 1,00 u 1.00 u 1,00 u 1,00 . u 1,2,DICHLORDETHANE 1,00 u 1.00 u 1,00 u 1.00 u 2-BUTANONE 2.00 u 2,00 u 2.00 u 2,00 u 1, 1 , 1 TRICHLOROETHANE 1.00 u 1,00 u 1,00 u 1.00 u CARBON TETRACHLORir1E 1.00 u 7,60 J 1,00 u 1.00 u VINYL ACETATE 2.00 u 2,00 u 2.00 u 2, 00 u BROMODICHLOROMETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2,2,-TETRACHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 u 1.00 u TRANS-1,3-DICHLOROPROPENE 1.00 u 1.00 u 1.00 u 1.00 u TRICHLOROETHENE 350 1. 10 J 1.00 u 1.00 u DIBROMOCHLOROMETHANE 1.00 u 1.00 u 1,00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u BENZENE 1.00 u 1,00 u 1.00 u 1,00 u CIS-1,3-DICHLOROPROPENE 1.00 u 1,00 u 1.00 u 1.00 u 2-CHLOROETHYL VINYL ETHER I I I I BR0!'10FORM 1.00 u 1.00 u 1.00 u 1.00 u 2-HEXANONE 2.00 u 2.00 u 2,00 u 2.00 u 4-METHYL-2-PENTANONE 2.00 u 2.00 u 2.00 u 2.00 u TETRACHLOROETHENE 1.00 u 1.00 u 1.00 u 1.00 u TOLUENE 1.00 u 1,00 u 1,00 u 1, 00 u CHLDROBENZENE 1.00 u 1.00 u 1.00 u 1, 00 u ETHYL BENZENE 1.00 u 1.00 u 1.00 u 1.00 u STYRENE 1.00 u 1.00 u 1.00 u 1.00 u TOTAL XYLENES 1.00 u 1.00 u 1.00 u 1.00 u

PROJ3269


TITLE: HASTINGS--MARCH SAMPLING LAB: AQT SAMPLE PREP: _______ ANALYST/ENTRY: AM2

COMPOUND

CHLOROMETHANE BROMOMETHANE VINYL CHLOR IrtE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1 DICHLOROETHENE 1,1 DICHLOROETHANE TRANS-1,2,-DICHLOROETHENE CHLOROFORM 1,2,DICHLOROETHANE 2-BUTANONE 1,1,1 TRICHLOROETHANE CARBON TETRACHLORIDE t)!NYL ACETATE BROMODICHLOROMETHANE 1,1,2,2,-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYL VINYL ETHER BROMOFOF:M 2-HEXANONE 4-METHYL-2-PENTANONE TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES

FKJS2028

10.0 10.0 10.0 10.0

5.00 10.0 s.oo 5.00 s.oo

41.0 s.oo s.oo

10.0 s.oo 5,00

10,0 S,00 s.oo 5,00 s.oo

1200. 5,00 5,00 5,00 5,00

s.oo 10.0 10,0 s.oo 5.oo s.oo 5.00 5.00 5,00

u u u u u u u u u

u u u u u u u u u u

u u u u

I u u u

u u u u u

MATRIX! WATER METHOD! 930~M?J..,,,t-REVIEWER:6-i~'"'l7'~L---

SAMPLE NUMBERS

FKJS2029

2.00 2,00 2,00 2,00 1.00 2,00 1.00 1.00 1.00 1.00 1,00 1.00 2 • 0 0 1.00 1.00 2.00 1,00 1.00 1, 00 1,00 6.90 1.00 1,00 1.00 1,00

1,00 2.00 2,00 1,00 1, 00 1,00 1,00 1.00 1.00

u u u u u u u u u u u u u u u u \1

u u u

u u u u

I u u u u u u u u u

UNITS: UG/L CASE: 5673 DATE: 04/24/8,

PROJ3270

ANALYSIS TYF·E ! VOLATILE ANALYSES

TITLE: HASTINGS--MARCH SAMPLING MATRIX: IJATER UNITS: UG/L LAB: AOT METHOt1: 930::?~ ~ CASE: 5673 SAHF'LE F'F:EF': ------- ANALYST/ENTRY! AM:? REVIEWER:6r(; '.!L ___ DATE! 0'\/24/E

SAHF'LE NUMBERS

FKJS::?019 FKJS:?020 FKJS2021 FKJS:?02 COMPOUND

CHLOROMETHANE 2. 00 u 100 u 10,0 u 2. 00 BROMOMETHANE 2. 00 u 100 u 100 u 2.00 VINYL CHLORIDE 2. 00 u 100 - u 100 u 2.00 CHLOROETHANE 2. 00 u 100 u 100 u 2.00 METHYLENE CHLORIDE 1.00 u 50.0 u so.o u 1.00 ACETONE 2. 00 u 100 u 100 u 2,00 CARBON t1ISULFIDE 1.00 u so.a u so.o u 1.00 1,1 DICHLOROETHENE 1.00 u so.a u 50,0 u 1.00 1, 1 DICHLOROETHANE 1.00 u 50.0 u so.o u 1,00 TRANS-1,2,-DICHLOROETHENE 1.00 u so.o u 50.0 u 1,00 CHLOROFORM 1.00 u 50,0 u so.o u 1.00 1,2,DICHLOROETHANE 1.00 u so.o u 50.0 u 1.00 2-BUTANONE 2.00 u 100 u 100 u 2.00 1, 1 , 1 TRICHLOROETHANE 1.00 u 50,0 u 50.0 u 1.00 CARBON TETRACHLORIDE 1.00 u 50.0 u 50.0 u 1.00 VINYL ACETATE 2.00 u 100 u 100 u 2 • 00 BROHODICHLOROMETHANE 1.00 u 50.0 u 50,0 u 1,00 I

1,1,2,2,-TETRACHLOROETHANE 1.00 u 50,0 u 50.0 u 1,00 I 1,2-DICHLOROPROPANE 1.00 u so.o u 50.0 u 1.00 l TRANS-1,3-DICHLOROF'ROPENE 1.00 u 50.0 u 50,0 u 1.00 l TRICHLOROETHENE 3.50 1800. 1100, 25.0 DIBROHOCHLOROMETHANE 1.00 u 50.0 u 50,0 u 1.00 l 1,1,2-TRICHLOROETHANE 1,00 u 50,0 u 50.0 u 1,00 L BENZENE 1.00 u so.o u 50.0 u 1.00 L CIS-1,3-DICHLOROPROF'ENE 1.00 u 50,0 u so.o u 1,00 L 2-CHLOF:OETHYL VINYL ETHER I I I E<ROMOFORM 1.00 u SO,O u 50.0 u 1,00 L 2-HEXANONE 2.00 u roo u 100 u 2.00 L 4-METHYL-2-PENTANONE 2,00 u 100 u 100 u 2,00 L TETRACHLOROETHENE 1.00 u 21.0 M 50.0 u 0,6 TOLUENE 1.00 u 71.0 u s2.o u 1.00 L CHLOROBENZENE 1.00 u 50,0 u 50.0 u 1.00 L ETHYL BENZENE 1.00 u 50,0 u 50.0 u 1.00 L STYRENE 1.00 u 50,0 u 50,0 u 1, 00 L TOTAL XYLENES 1, o.o u 50.0 u 50,0 u 1, 00 L

PROJ3271

ANALYSIS TYF'E! VOLATILE ANALYSES

TITLE! HASTINGS--HARCH SAMPLING MATRIX: WATER UNITS: UG/L LAB! A(H METHOD: 9302VM@__ CASE! 5673 SAMF'LE PREF': _______ ANALYST/ENTRY: AM:? REVIEWER: µJ, ·· ____ Dt'\TE: 0"/24/B

SAMPLE NUMBERS

FKJS202S FKJS2026 FKJS202'. COHPOUND

CHLOROHETHANE 2.00 u 2.00 u 2,00 BROMOHETHANE 2,00 u 2,00 u 2.00 VINYL CHLORIDE 2,00 u 2,00 u 2.00 CHLOROETHAl'IE 2,00 u 2,00 u 2,00 METHYLENE CHLORIDE LOO u LOO u 1,00 ACETONE 2.00 u 2.00 u 2.00 CARBON I)ISULFIDE 1,00 u 1.00 u 1.00 1, 1 DICHLOROETHENE 1.00 u 1,00 u 1, 00 1 , 1 DICHLDROETHANE 1,00 u 1.00 u LOO TRANS-1,2,-DICHLOROETHENE 1.00 u 1.00 u . 1. 00 CHLOROFORM 4.10 4, 10 1.00 1,2,DICHLOROETHANE LOO u 1.00 u 1.00 2-BUTANONE. 2.00 u 2,00 u 2.00 l, 1, 1 TRICHLOROETHANE LOO u 1.00 u LOO CARBON TETRACHLORIDE 1,00 u 1,00 u 1.00 VINYL ACETATE 2.00 u 2,00 u 2,00 I BROMODICHLOROHETHANE 1.00 u 1.00 u 1,00 I 1,1,2,2,-TETRACHLOROETHANE 1.00 u 1.00 u 1,00 l 1,2-DICHLOROPROPANE 1.00 u 1.00 u 1.00 l TRANS-1,3-DICHLOROFROPEHE 1.00 u 1.00 u 1,00 l TRICHLOROETHENE 0.9 11 o.s M 1.00 l DIBROHOCHLDROHETHANE 1.00 u 1.00 u 1.00 l 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 l BENZENE 1.00 u 1.00 u 1.00 l CIS-1,3-DICHLOROPROPENE 1,00 u 1.00 u 1.00 l 2-CHLOROETHYL VINYL ETHER I I BROMOFORH 1, 00 u 1.00 u 1 .• 00 2-HEXANONE 2,00 u 2.00 u 2,00 4-HETHYL-2-PENTANONE 2.00 u 2,00 u 2.00 TETRACHLOROETHENE 1,00 u 1,00 u 1.00 TOLUENE 1.00 u 1.00 u 1,00 CHLOROBENZENE 1.00 u 1,00 u 1.00 ETHYL BENZENE 1. 00 u 1.00 u 1.00 STYRENE 1,00 u 1.00 u 1.00 TOTAL XYLEHES 1.00 u 1.00 u 1.00

PROJ3272


TITLE: HASTINGS--MARCH SAMPLING LAB: AQT SAMPLE PREP: _______ ANALYST/ENTRY: AM2

COMPOUND

CHLOROHETHANE BROMOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1 DICHLOROETHENE 1,1 DICHLOROETHANE TRANS-1,2,-DICHLOROETHENE CHLOROFORM 1,2,DICHLOROETHANE 2-BUTANONE 1,1,1 TRICHLOROETHANE CARBON TETRACHLORIDE t)! NY L ACETATE BROMODICHLOROMETHANE 1,1,2,2,-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYL VINYL ETHER BROMOFORM 2-HEXANONE 4-HETHYL-2-PENTANONE TETRACHLOROETHEHE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES

____ _,, __ ----------

FKJS2016

2,00 2.00 2.00 2.00 1.00 2,00 1.00 1,00 1.00 1.00 1,00 1.00 2,00 1.00 1.00 2.00 1.00 1.00 1,00 LOO

180 1.00 1,00 1.00 1.00

1.00 2,00 2.00 1.00 1.00 1.00 1.00 1.00 1.00

u u u u u u u u u u u u u u u u u u u u

u u u u

I u u u u u u u u u

MATRIX: t.JATER METHOD: 9302H9°J.I!~ REVIEWER: fl,~-f./J.~----

SAMF'LE NUMBERS

UNI TS! UG/l CASE: 5673 DATE: 04/24/B,

FKJS2017 FKJS2018

2,00 2.00 2,00 2,00 1.00 2,00 1,00 1.00 1.00 1.00 1,00 1,00 2,00 1.00 4,40 2,00 1.00 1.00 1.00 1.00

54,0 1.00 1,00 1.00 1.00

1.00 2.00 2,00 1.00 1,00 1.00 1.00 1.00 1.00

u u u u u u u u u u u u u u

u u u u u

u u u u

I u u u u u u u u u

2,00 2,00 2.00 2,00 1,00 2,00 1.00 1.70 1,00 1.00 1,00 1.00 2.00 s.oo

25,0 2, 00 1,00 1.00 1,00 1, 00

48.0 1.00 1,00 1.00 1, 00

1,00 2.00 2.00 1,80 1.00 1.00 1,00 1.00 1,00

u u u u u u u

u u u u u

u u u u u

u u u u

I u u u

u u u u u

J PROJ3273


TITLE: HASTINGS--MARCH SAMPLING LAB: AOT SAMPLE PREP: _______ ANALYST/ENTRY: AM2

MATRIX: WATE~ METHOD! 93_02 0 c__--REVIEWER: &i~ ___ _

COMPOUND

CHLOROHETHANE BROMOHETHANE VINYL CHLORit1E CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1 DICHLOROETHENE 1,1 DICHLOROETHANE TRANS-1,2,-DICHLOROETHEHE CHLOROFORH 1,2,DICHLOROETHANE 2-BUTANONE 1,1,l TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLDROMETHANE 1,1,2,2,-TETRACHLOROETHANE 1,2-DICHLOROPROPANE TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROHOCHLOROHETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYL VINYL ETHER· BROHOFORM 2-HEXANONE 4-HETHYL-2-PENTANONE TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES

SAMPLE NUMBERS

FKJS2023P

I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I I

UNITS! UG/L CASE: 5673 Dl'lTE: 04/24/E

PROJ3274

TITLr: HASTINGS LAB: ENV

ANALYSIS TYPE:

SAMrLE PREP: _______ ANALYST/CNTRY: E04

I:K JS20 08 COMPOUND

HMX 0,06S RDX 0.095 1,3,5 TR INITROI:iENZENE 0. O(, 1,3 DINITRON:NZENE 0.11 NITROE<CNZCNC 0.18 TETRYL 0,0?1 2,4,6 TRINITROTOLUENC 0.12 2,6 DINITROTOLUCNC 0.19 2,4 DIN!TROTOLUENE 0 • ;: 1 1, S D!NITRDDENZI:NC PICRIC ACID 1. 90 u

u u u u u u u u u I

EXPLOSIVCS BY HPLC-UV

MATRIX: t.JATf:~UNITS: UG/L METHOD: ENV-EX L CASE: ~160G REVIEWER: _,f(. _ t:f DATC~ 04/17/C

SAMPLE:

l, >./

NUMBERS

FICJ'S2016

0.065 u 0. 09S u 0, 06 u 0.11 u 0.10 u 0. 091 u 0.12 u 0.19 u 0.21 u

I 1.90 u

PROJ3275

... - ... • • • ••-•-e----•••-:.-••r<r•••--•-•-4'- -- • -------•-----""'--•-••-

TITLE: HASTINGS LAB: ENV

ANALYSIS TYPE:

SAMPLC PREP: _______ ANALYST/ENTRY: E04

FKJS2004 COMPOUND

W1X 0. 06S RDX 0.09S 1,3,S TRINITRODENZCNC 0.06 1,3 DINITRODCNZENE O.ii NITR OE<ENZENE 0.18 TETRYL 0.091 2,4,6 TRIN!TROTOLUENC 0, 12 2,6 DINITROTDLUCNE 0,1? ~,4 DINITROTOLUENE 0,21 1,S DINITRODENZENE PICRIC ACID 1. 90 u

u u u u u u u u u I

EXrL•SIVES BY HPLC-UV

MATRIX: WATER . /UNITS: UG/L METHOD: ENV-E~~ CASE: 2160G RCVIEWER: ~~ DATE:: 04/17/0!

SAMPLE NUMBERS

Fl(JS20 OS Fl(JS2 0 07

0,065 u 0,065 u 0.38 0,44 0.06 u 1.40 0 .11 u O,ii u 0.10 u 2.90 0.091 u 0,0?i u 0.12 u 6,30 0.37 0,53 0.21 u 0,21 u

I I 1.90 u 1. 90 u

' I '1 PROJ3276

TITLE~ HASTINGS--HARCH SAMPLING HriTRIX: WATER

ANALYSIS: GC/HS SCANS UNITS! UG/L

LAB: AOT

REVIEWED BY: GCS ((l-? DATE: 04Mr/86 CASE NO: 5673 METHOD NO: 93011"'

, t.__,, TENTATIVELY IDENTI IED COMPOUNDS

SAMPLE NO. COHF·OUND NAME ** FRACTION .EST. CONC. *

FKJS2001 NOTHING SIGNIFICANT FOUND FKJS2002 NOTHING SIGNIFICANT FOUND FKJS2003 PROPENE VOA o.9

FKJS2005 NOTHING SIGNIFICANT FOUND FKJS2006 NOTHING SIGNIFICANT FOUND FKJS2007 NOTHING SIGNIFICANT FOUND FKJS2008 NuT/.lHlG SIGNIFICANT FOUND FKJS2009F NO- !ING SIGN IF I CANT FOUND FKJS2010 NOTHING SIGNIFICANT FOUND FKJS2011 NOTHING SIGNIFICANT FOUND FKJS2012 NOTHING SIGNIFICANT FOUND -·· . - - ~

* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TU AN INTERNAL STANDARD, AN AUTHENTIC STANDARD HAS NOT BEEN RUN,

** THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ~OUTINE, AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY :• HPOUND MASS SPECTRA AND RETENTION TIMES.

J

PROJ3277

·. .. . . -· ·-- ......... ·. ___ _. ·--~-- • .s.-· · . ...:,._ __ ~..;-.•.-• • .:. •• _;.-~ .. ..:--J.~~------·-..___ __ ._~...:....;...:.,....:...;_;;_ ........ , ,, .. __ . __ ~ ... :.....:..:. _ .....

DATA SHEET

ACTIVITY TITLE: --,.r\--i.::::::9 .... S.J..T.1.--:u.:½:.l.-1~4-<...;;:i. ____________ _

PROJECT LEADER: t:sz _q:''c-C COLLECTION DATE: 5 -~ l,

Analytical Lab: ---'E=..i.P~A.__ __ _ Sample Matrix: Wo._±9,,1

SAMPLE NUMBERS

IF~~~ 00« I C03 I 00'--f I oos I 0C6DI ANALYSIS UNITS

PROJ3278

- -· ........ ·--. ,._ ........ :· .. : ____ . ..._ .. :.,_; ____ "--·•-··-·-·-·-.:,_----··-----------·--.:.-, ... ___ _

DATA SHEET

ACTIVITY TITLE: __ \:\_...a_,_5..._± ..... 1' ...... \/\,""'"'~~$__._ __________ _

PROJECT LEADER: (&,,-, '5: COLLECTION DATE: 3 -~ 6

Ana lyt 1 ca 1 Lab: __ E_P____._A _____ _ Sample Matrix: l ,L;o.7: R,.C

SAMPLE NUMBERS

ANALYSIS UNIJS

f-\-\"'c\:¼:+v h,,- \<:) ,:)C,~ * ;'.;2 L.\ :) ;;2 l,' 4D~ a49 J

I I \-b C'~.,\,., .... ; .. \ J;, • , .... '77,r; * '3:72,. \ ;,o,i 14, \ ~., ' \J .

c;., \~~~0 ~\\_.A \o 10.D '7 ;:J I ('\ ?-,L. f'i -5 l.c :')<x. 0 9Lo I ~ _,,_,- ~ ___,,.- --- _.,.,.

I"- I ' ~ 1;1r, ...,, ,1.-, -- ---- ---- --- -----E+h vl.::itq,\,,;birt.u ·Jo JJA \ 0 o. {)::) u I~. 9..

I 'U *f\JuO~

.

.

PROJ3279

DATA SHEET

ACTIVITY TITLE: __ }-\......:;Q..__-, ....... ±.,__;11..,11.' w.-(S+' ..._.5..._ ________ _

PROJECT LEADER: Ce..-ff.e, COLLECTION DATE: 3 -~ '2

Analytical Lab: E;.P A: Sample Matrix: UJ9.---\- :e.:e

SAMPLE NUMBERS

IFOK~S1;i_l I 7 I I I _ ~ _ _ 0;2;:;2_ c;:uJB o.;25 0=2 b o¥y E ANALYSIS UNITS

4 I to.\:~ :+ ~, , , . . '°\ \ Q Y~t; l b t,., "' / 11i ~9Y * I • j rt \,.w >1 ~ , ~ Q. (,.,(). -r; q,3b y d-0,9 l i ,5 \ l l

~11\~+" ,i~-\ Q 24:J ;:,3,~ / ' ~,.o :½. I o.~ / J

* Y\)C', (\~ ..

PROJ3280

. . .. . . .,,. ·- . --- . "•"' ........ -- ~- -'-- . - ............. - __ ,.__ ____ ·-·-- ,.,,,,.,. ~----···•-- ·--·•·. ·--

DATA SHEET

ACTIVITY TITLE: __.\:\._..o...----=5 ___ -\-..... , ...... ½-.._~..,....$---_________ _

PROJECT LEADER: J;:'e,.Q;;g,_:s:: \..J COLLECTION DATE: _3 __ -_i_b __

Ana lyt i ca 1 Lab: _E____._P __ A _____ _ Sample Matrix: l .th-\e,r:

SAMPLE NUMBERS

IFOKO~~~, I I I I _ ~ _ OoJD 00?, 009F 010 0\ \ ANALYSIS UNITS

_____,,, .. * A\ {"o.\:,.,._:-\-v 1,.,u"1 \ Q iz;i ,s-s I 11 \~~

C ,"'' X I (, \ 0 V ~ .~ \.u.l" }~ \~.D ~ \ 3. ,:) \ LA ·~°' ,_ 5<;? I '2,

~11\~~+() ,~.~~O I '7, 1 ~ ,,,L..\ /).~ 3l..o 5J,o I lJ ~

____.,,.. - I ' r--../ f , I D ~, l \.JI:"' --. ~ ~

\ 3,1t; ~ ~ 0,DL//J ------~ \..... \ :-tr~"t" -\... \:+'" ~

r~ v\ e.•rH .. \'); b n, ..... :Jo IJ,. \ C ~ ~ ~ "' ~ ~ D. l'l ';J \1 J cj -

* (\, C-1 ()-A "rt_\.._

.

-I

PROJ3281

• - ...... - -·--· ··•··- -• ...: •• • .. ---.. ·----··• .. e- .. ,,.;,...-.. -·---'-... ~ .. ---.1--.---..,---,_._..__..._.,.__...., ______ _

DATA SHEET

ACTIVITY TITLE: ____ H ___ Q.: ____ 5 __ ;-\-....,_~-~~2),....."&a¼------------PROJECT LEADER: te-f<':R. f' COLLECTION DATE: °3 -~ l,

Analytical Lab: F PA: Sample Matrix: t~.Ja±e f':

SAMPLE NUMBERS

ANALYSIS UNITS

'lb~\)~ b \'"t,u~ -v-\ ~li O. l~ o.o~u l-.. '7 o .o~ u 0' c,;:;. l1 I

-·

PROJ3282

• .. - .· . . . • .. • • . . ·. • • . . .,., . .. - .. , • .... • ,:,-·. r . ' .. -... • • •• . .. • - .•.

Appendix B-5


June 1986

PROJ3283

., ~NALYSJS TYPE: ~OLATILES

TITLE: HASTINGS LAB: Ef'A 7 St,MPLE PREP: J..l.~--- t1HAL YST /ENTRY: 1

•1JS

.. COMPOUND

CHLORONETHANE BROMOMETHANE l,.'IHYL CHLORIDE CHLOROEiHAHE HETHYLEHE CHLORIDE l,l-DICHLOROETHYLENE 1,1-DICHLOROETHANE TRANS-1,2-DICHLOROETHYLENE CHLOROFORM l,2-DICHLOROETHANE 1,1,1-TRICHLOROETHANE CARP.ON TETRACHLORIDE BROMODICHLOROMETHANE 1~2-DICHLOROPROPAHE BENZENE ! ! ·. I TRANS-1,3-DICHLOROPROPENE TRI CHLOF:OETHYLEHE : . CIS-1,J-DICHLOROPROPEHE DIBROMOCHLOROHETHANE 1,1,2-TRICHLOROETHANE 2-CHLOROETHYLVlNYL. ETHER BROMOFORH : . 1 1,1,2,2-TETRACHLOROETHENE TOLUENE 1,1,2,2-TETRACHLOROETHAHE CHLOROl3ENZENE

J ETHYL BENZENE ' XYLENES, TOTAL 1- · ACETONE , 2-BUTAN0HE I . ' ETHYLENE DIBROMIDEi

' I: ·1

JKLS2001

12.0 22.0 14.0 1 c\. 0 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 s.oo .J.·. 00

45.0 1.00 1.00 1.00

1s.o 1.00 1,00 s.oo 1.00 s.oo 5,00 s. 0·)

10.0 10.0 10.0

MATRIX: WATER UNITS: UG/L METHOD: 6241UOO,...,/f__J? CASE: REVI E IJER: ~e...-~ I•ATE: 06/:?S/3:)

u u u u u u u u u u u u u u ·'. u u ~

u u u u u u u u u u u u u u )

I

SAMPLE NUMBERS

JKLS:?002

12.0 :?:? • 0 14.0 14,0 10.0 1.00 1.00

'1. 00 1.00 1, 00 . 1 .oo ' 1.00 1.00 1.00 s.oo 1 .oo ·

16.0 1 .qo· 1.00 1.00

18.0 1.00 , 1,00 s.oo 1.00 5,60 s.oo s.oo

10.0 10.0 10.0 ' I

I I I

i I

u u. U· u u u u u u ; u ,, u !j

I

u f u J .. U I.

u u

ii . u u u ·t u i

u ' u u u u u u

l,f '• ~- .=•.: J . i' j,'

i1 I°;

I ; : '

I i I ! I . ~ !q . I

'' I

JKLS2003

1:?, 0 22.0 14.0 14.0 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 5,00 1.00 2.00 1,00 1.00 1.00

1a.o 1 • 00 :, 1,00 s.oo 1.00 s.oo S,00 s.oo

10.0 10.0 10,0

i. I

u u

·u u u u u u u u u u

. u ~ I~:, u ,.

,u ·u u u

I

u ~ u u u u u u u

;u .u : .. :; .

. l' ... i·· ~: ·' :'j ,i .•' . ..... , .

,:':

12.0· U :?:?. 0 · U 14.0l u 14.0 U 10.0 U 1.00 U 1.00 U 1.00 U 1.00 i I u 1 .oo I u 1.00 U 1.c,o u 1. oo I u 1.00 •1u 5. 00 _., U 1 • 00 I u 1,00 U 1.00 U 1.00 U 1,00 U

1a.o u 1.00 U 1.00 U s.oo ; I u 1.00·-u s. 00 1 u s.oo u s.oo . u

10.c !u 10.0 . . ·.u l 0. Q i t-,U 1,. i

I • ,, ! .. , .

· I i : i l ! ! . t

,I

• I I

I I I .l

. PROJ3284 ~~~~-.:;;;:~~-==·7:;;:,:- .. 1 ... • :;t .. ~-r-C'::~~-:~7"".~,--- ... --...-~~------,...... ... --- ....

! ·, ! i

i r, il , ~ ... . .

ANALYSIS TYPE: VOLATILES . . i

.. ,TLE! HASTINGS

iAB: EF·A 7 .SJ\MPLE PREP:-U7..::t_ ANALYST /ENTRY: VJS

COMPOUND

t:HLOROHETHANE r BROHOHETHANE

IJINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE 1,1-DICHLOROETHYLENE 1,1-DICHLOROETHANE TRANS-1,2-DICHLOROETHYLENE CHLOROFORH : !

11,2-DICHLOROETHAHi I 1, 1, 1-TRI CHLOROETHANE t ~CARBON TETRACHLORIDE ; jBROHODICHLOROHETHANE · 11,2-DICHLOROPROPANE : BENZENE . · .• i:

TRANS-1,3-DICHLOROPROPEHE TRICHLOROETHYLENE 1. c1s-1,l-DICHLOROPROPENE DIBROHOCHLOROHETHANE 1,1,2-TRICHLOROETHAHE 2-CHLOROETHYLVIHYL!.ETHER BROHOFORH j l . 1,1,2,2-TETRACHLOROETHEHE • TOLUENE !· 1,1,2,2-TETRACHLOROETHANE CHLOROBENZEHE i~. ETHYL BENZENE XYLENES,TOTAL t"lCETONE .::!-BUTANONE · ETHYLENE DIBROHIDE'

: '

i . ,

I ! . i.

!

JKLS2030

12.0 22.0 1 -4. 0 1-4. 0 10.0 1.00

'I' 1.00 1.00 1.00 1.00 1.00

18.0 1.00 1.00 s.oo 1.00 1.00 1.00 1.00 1.00

18.0 1.00 1.00 s.oo 1.00 s.oo s.oo s.oo

10.0 10.0 10.0

i HATRIX: ,WATER: HETHOD: '624lU~lq__fZ REVlEIJER: tJJ.L~

! . Si\HPLE NUMBERS

L~ITS: tASE: DATE:

• I ~: . . .. ;., .JKLS:!032 '. JKLS2034F •

I • • I I I I/ ' : , 1·1 \.

u 12.0 , I u 12.0 ; u uu 22. o '. uu _ :?:? • o ,·;: uu· _

1-4.0·; l 14.0 U 14 • 0 J U . : 1 4 • 0 ': U U 10.0, U t 10.0 U U . 1 • 00 U : 1. 00 · U

f

I

UG/L

061:.e1s6

JKLS2O!S l :

1:?.o < I u 22,0 I 1, U 14.oi u 14.0 . U 10.0 U 1.00 U

U. 1,00 U. · 1.00 ·U 1.00 U u .:?B.o: . ~ 1.00 ·u . 1.00 u ui 1.00·. u 1

1i 1.00 ·.u -:1.00··,u uj 1.00• .. u.,t·;. 1.00:···u_;~,1.00. U ~ n 1 • oo . i u . ,-•: _ 1 • o o ~ lr \J ,~ ~ · i 1. o o I u

.,, 1_ • o o 1. . u . . r 1 ~ o o 1 1:J. :, ~ : 1 1 • o o . u

U ::l ·.· 1.00_,, U, }·-· 1.00 .. U li; f,11.00 U u :'.' 1 • 9 0 i 4 . _, 1 • 0 0 1 . u ~ t .. 1 • 0 0 u U. 5.00 ·: U ,: : s.oo =, U s.oo.: U .u ~ 1 • o ~ l ~ :~ · 1 • o o ·· 1; u 1 • o o ;_ . u

. · 690 l l ~ i: .J '. :, 1 :• 1. 00 i. y :,: , 1. 00 I, U

u 1.00 ,. u :·:: 1.00 ·. u 1.od u U 1,¢0 U ·t: 1.00 !' Ii . 1.00 U U 1.00 U ~:i 1.0~; ij,U i. j . 1.00 U u 1 a_. o u ~ . 1 a • o ·· • -

1. u ,,ii , 1 a • o u

u :' . 1 • o o U V : 1 • o o . IJ 1;!: · i 1 • o o u u • .-.oo '! r· 1.00 '.: ·: u ,_,. ; 1.00 u u s.oo u· ._; s.oo itl s.oo - u U 1.00 U 1

..: lo00 \j 1o00i U U , 5. 00 U i ~ s. 00 :r tJ' :S. 00 U u ~r.oo· 1 uj 1 ~ s.oo r u· s.oo u U 5o00 I U:.: S,00 . U S.00 L' U 10 • 0 I U' ;! . 10 • 0 . U, • 10 • 0 1 U U 10. 0 I I . u••

1 \i· 1 0 , 0 .

1 U - _10. 0 i ~ . U '

u 1 o. o ,, . 1 u .. 1 1 o. o · 1 ul' -_- : 1 o o = • (I u : !I : . ; !·;. ·• \ Ii Ii~: ·11·:, / I;! :! ;,, .. '_11. : __ · ! .

)

,

. · ! 11 , ! · ,1 ; t! . , . : I ,! ·'

' I • ; I . ·I. . .'.I :

1~ ! ;_~.

I rt"' ; 1) I I . •1 I 1._:.

., ;

- •. i :j • · ; . F . • I I .• II

; - I ll· ; , L .. . I I .. :.: i r , , . . t

: ·: ·1 if~, .. ; · ~ .·· i,i; ~ ! .

•• 1;, I

I : i

---..___,_l,,.---·-·-~:!!"~-----PROJ3285

~NnLY5IS TYPE: ETHYLENE DIBROMIDE

TITLE! HASTINGS ~B: EPA 7

-AMPLE PREP: _______ ~NALYST/EHTRY: IRR

COMPOUND

ETHYLENE DIBROHIDE

Jr.LS::?003

0.4.

. - . ·--- -----·--··-. . . - .

u

HATRIX: IJATEP. HETHOD: 618 RE'HEIJER: -4-{.f __ -.,_-l_

SAHPLE HUHBERS

UNITS: UG/L

DATE: 07 /1 O/S6

JKLS::?005 JKLS20.:!8 JKLS2o;;o

u u

ANALYSIS TYPE: ETHYLENE DIBROMIDE

ITLE: HASTINGS t"IB: EPA 7 AMPLE PREP! _______ ANALYST/ENTRY! IRR

COMPOUND

ETHYLENE DIBROMIDE. 3.;o

MATRIX: WATER METHOD! '618 RE 1,.1IEIJER ! ./;;:JJ __ 1.1_..U1.,.._

St'\MF'LE NUMBERS

UNITS! UG/l.. CASE! !tATE: Oi /10/86

JKLS::?031D JKLS::?032 JKL520'.;-1E°

0 ... u 0,4

PROJ3286

u

u

:- •

. ANALYSIS TYF·E: t.10L,HILES

lTLE: Ht'\STINGS HATRIX: WATER UNITS: UG/L .:tB: EPA 7 . r:rs METHOD: o241W00"]Jk6 CASE: t'1~PLE PREP:~----- ANALYST/ENTRY: VJS F:EVIEUER! _____ DATE: C6/H·/S6

SAMPLE NUMBERS

'jKLS:?008 Jt,LS2009 jKLS2010 jKLS:?011 COMPOUND

CHLOROHETHANE 12.0 u 12.0 u l:?.O u 12.0 u f'.ROMOHETHAN:: 22.0 u :?2.0 u 22.0 u :?2.0 u IJINYL CHLORII•E 1 -4 • 0 u 14.0 u 14.0 u 14.0 u CHLOROETHANE 14.0 u 14.0 u 14.0 u 14.0 u M::THYLENE CHLORIDE 10.0 u 10.0 u 10.0 u 10.0 u 1,1-DICHLOROETHYLENE 1.00 u . 1.00 u 1.00 u 1.00 u 1,1-DICHLOROETHANE 1.00 u .. 1.00 u 1.00 u 1.00 u TRANS-1,2-DICHLORDETHYLENE 1.00 u . 1.00 u 1.00 u 1.00 u CHLOROFORM 1.00 u 1.00 u l.00 u 1.00 L!

' .1,2-DICHLOROETHANE 1.00 u .. 1.00 ~ u l.00 u 1.00 u l l,1,l-TRICHLOROETHANE 1.00 u l-4.0 ~18.0 " 1.00 u ' . CARBON TETRACHLORIDE 1.00 u 1,00 u 1,00 u 1.00 u \ BROHODICHLOROHETHANE .... 1 .oo u ---· 1,00 u 1,00 u 1.00 u f 1,2-DICHLOROPROPANE 1.00 u 1,00 u l.00 u 1.00 u ~

BENZENE s.oo u s:oo u s.oo u s.oo u . TRANS-1,3-DICHLOROPROPENE 1,00 u 1.00 u 1.00 u 1.00 u TRICHLOROETHYLENE . s.oo 1.00 u

., 1100. > 19 •. , i

ClS-1,3-DICHLOROPROPENE 1.00 u 1 .oo u 1.00 u 1.00 u DlP.ROMOCHLOROHETHANE 1.00 u 1.00 u 1.00 u 1.00 u 1,1,2-TRICHLOROETHANE 1.00 u 1.00 u 1.00 u 1.00 u 2-CHLOROETHYLVINYL ETHER 18.0 u 18.0 u ·1e.o u 18.0 u BROMOFORK 1.00 u 1.00 u 1.00 t .u 1.00 u 1,1,2,2-TETRACHLOROETHEHE 1.00 u 20.0 ·. 29,0 1.00 u TOLUENE s.oo [J s.oo u s.oo .. u s.oo u

~ 1,112,2-TETRACHLOROETHANE 1,00 u 1.00 u 2.00 { 1.00 u j CHLOROBENZENE s.oo u S,00 u s.oo u s.oo u "' ETHYL BENZENE s.oo u 'S • 00 u s.oo u s.oo u • > XYLENES,TOTAL . 5,00 u s.oo u s.oo s.oo u ' u ; t'•CETONE 10.0 u 10.0 u 10.0 u 10.0 u • 2-BUTANONE 10.0 u 10.0 u 10.0 u 10.0 u 1·

ETHYLENE DIBROMIDE 10.0 u 10.0 u 10.0 u 10.0 u

PROJ3287

i I • : ,·• ~ . _ ANALYSlS TYF·E: VOLATIL.~, ~ l!!1;i l:ii' i•~: i ! I I· .. __ ._.,,;_HASTINGS i • HATRix:· \ilATER; UNITS: UGil. LAI:: c.F'A 7 1 HETHO[I! .62411,,J.00--, fa O °CASE! SMIF'LE PF:EP:_LJ._TJ_· ltNALYST/ENTF:Y: 'JJS REVIEWER: ".;J.Ci..,_.f'~ DATE! O6/:!E-;/S~

COMPOUND :

CHLOROHETHMlE BROHOliETHANE VINYL CHLORIDE CHLOROETHANE

,· ,

METHYLENE CHLORIDE 1,1-DICHLOROETHYLENE 1,1-DICHLOROETHANE TRANS-1,2-DICHLOROETHYLENE CHLOROFORH l,2-DICHLOROETHANE-1,1,1-TRICHLOROETH~N~ tARBON TETRACHLORIDE BRONODICHLOROHETHAHE ·. 1,2-DICHLOROPROPANE BENZENE . ,· TRANS-1,3-DICHLOROPROPENE TRICHLOROETHYLENE ClS-1,3-DICHLOROPROPENE DIBROHOCHLOROHETHANE 1,1,2-TRICHLOROETHAHE 2-CHLOROETHYLVINYW.ETHER BROHOFORH . : . '. :' 1, 1, 2, 2-TETRACHLOROETHENE .. TOLUENE 1,1,2,2-TETRACHLOROETHANE CHLOROBENZENE ETHYL BENZENE XYLENES,TOTAL ACETONE :?-BUTANONE ETHYLENE DIBROHIDE

-.•-~ .. -. ---------

1:?. 0 :?:? • 0 14.0 1-1.0 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 :s.oo 1.00 1.00 1.00 1.00 1.00

18.0 1.00 1.00 s.oo 1.00 s.oo s.oo s.~o

10.0 10.0 10.0

u u u u u u u u

; S~MPLE iNUHI-ERS ~,~' : ,;b~ ,t Sc>; I ; ~ ~! I;· .. CA.t~-tfl

·• JKLS:?007;1 '. . ~KLS2ofo if:·. JKLSZ0:!9 , . I j'j j ·· 1 : i 1111 ~''j_ ' , 'r. i • ' ~ f ! I • l<i ! I I

,., I 'I : 12.0 i l u 12.0 '.' : 12.0 u :?2. 0 U 2:?. 0 i U 2~. 0 U 1 • • 0 l U r 1 4 • 0 :.: U 14 • C· , U 1 ... ~: U 1-4.0 ,:ti 14.C U

1 o • o : u4 1 o • 01 Iii. u1: 1 o • o i : 1 u

1.00. 4.00 1.00'; U 1 • 0 0 U ! ' 1 • 0 0 l1 U · 1 • CO U

_i;oo,.~ ~ 1.00 ·ru 1.00: U U i · 1.00 · U 1.00 ' i.J •. 1.0~ U ul 1.00: U, ·1.00 ;·u 1.00:, U u · ~ ... oo.~! u • 11.0 ~--J t' '.. ·1,00. u ~1

1

• ~.a._o l~.'-.:i: ';: .. 1· 1.00\ J!t:·!_ 1.00\!l.u

U .. . 1. oo. t • 9 i

1 ~ ,; 1. oo 1 J·. ·:.,-· 1. oi i. u

1. ~o t -Y. i1 : 1. oo .•• ··i • 1. o I . u u !1• s. o o · · r1 · · s. o o · ·, u, ' · I · s. o _. u u 1 • o o!, I u f; . 1 • o o. u · : 1 • o ., u U 38.0 1 . ,: 1100 •• , ·, . 1S0. U 1 • 0 Q l U :, 1 • 0 0 . ,1 U 1 • 0 0 LJ

u 1.00 : u .r 1.00 ·1·· u 1.00 . u u 1.00

1·i 1 ~,:t,; 1~00 :u:~,:·1~00:j,u

u • _1a.o; 1.i_uy,.:._1e~o ·:. _llt:~ .,1a.of 1;_.u u . 1.~o).:u,. 1._ 1.00 -.~tfri __ 1.oq: u u 1.00

1.- u

1 ~ 2s.o · • 11 ,"11;·" ! · 1.0~, _u

u· s.oo;' u- ''. s.oo 1.u s.c,o_·, u u 1.00', u ;! 1.00 ;:;u 1 •. 00 ; u U S. 00 • ,. U . S. 00 • '.U 5. 00' U u s.001 · ti i

1 ·s.oo

11·!u s.oo .1 u I . • • .

u s.001.1 u, .,;. s.oo . u,; s.oo_,;' u u I 10.~ ·: ~ !/'' 10.0 j_U,:.- _1_0.0 ;jl 1' ,!J u -! 10.0· ·.: •.!! 10 o ·u:·· 10.0·· ·u. U

·, . I-~. ., A • • ~. l ·: I ••

10.0 :i: 1- Ui ·.' 10.0 u !'·: 10.0 r· • u

I • ·I ;.; ' I I t I . : =·! • t · ! I l . . · ,. ·= i, \ '.:· I :

1[l ·r11.: ~ : I I! I '; l

i j ! \, ,. : l ·I· t j

II:'. '.I :; /~ i \.< . ·- r,· i ...

;_•: ~I 1, ; :'1·· I- . H· . "~·-. . r

r .; .

t . I : ~J

l ;,·1· d. t . . . ~-

:1 l .

·11: I : : ~• ~ ~ d

: • .. ' i.

I \. \ I •

• .. ! ; . :: ,;; ~

• . f ; '.-' • ; :. :..:··1·J!i.i'~ . • • • )l •••• ' . . • I . I

PROJ3288

j : I

~-

6N~LYSIS TYPE! VOLATILES

.-<f:-r-HASTINGS .,·,p.~ EF"A 7 ,.;MPLE PREP: _.LJ.~->-- ANALYST /EHTRY: '-'JS

c""' f- ,.,

JKLS:20:?1 COMPOUND

CHLOROHETHANE 1:?.0 F.:F.:OHOHETHANE ::?:? • 0 '.'INYL CHLORII•E 14.0 CHL OF:OETHANE 14. 0 HETHYLEHE CHLORIDE 10.0 l,l-DICHLOROETHYLENE 1.00 1,1-DICHLOfi:OETHANE 1.00 TRANS-1,:?-DICHLOROETHYLENE 1.00 CHLOROFOfi:H 1.00 1,2-DICHLOROETHANE 1.00 1,1,1-TR!CHLOROETHANE 1.00 CARBON TETRACHLORIDE 1.00 BROHOD!CHLOROHETHANE

. 1.00

l,2-DICHLOROPROPANE 1.00 riENZENE s.oo TRANS-1,3-DICHLORDPROPENE 1.00 TRICHLOROETHYLENE 2.00 :IS-1,3-DICHLOROPROPENE 1.00 DIBROHOCHLOROHETHANE 1.00 1,1,2-TRICHLOROETHANE 1.00 2-CHLOROETHYLVINYL ETHER 1 a·. o . BROHOFORH 1.00 1,1,2,2-TETRACHLOROETHENE 1.00 TOLUENE s.09 l,l,2,2-TETRACHLOROETHANE 1.00 .:HLOROBENZENE s.oo ·1HYL BENZENE s.oo <YLENES,TOTAL s.oo ·1CETONE 10.0 ~-BUT AN ONE 10.0

THYLENE DIBROHIDE 10.0

u u u u u u u u u u u u u u u u

u u u u u ll u u u u u u u u

MATRIX: WATER UNITS: UG/L METHOD: 6:?41uoo..-,1tO cnsE: REVIEWER!-----~ DATE: 06/1~/36

. SAMPLE NUHBERS ·I· . . I ' AiJo;,- I M-"1 ··: • "'4- (.

JKLS2022F JKLS:?0:23 ·. JKLS20:?4

,, I

u u ti u

12.0 22.0 1 •• ·:> 14,0 10.0 I• u• !

u 1,00 .1. 00

. i.oo 1.00 1.00

' u

1 .oo f '' 1.001·!

1,00 1 .oo i s.'00 1 .

1.00: : 1. 00 ~ ; 1.00; : 1.00 1. 00: j

18,0 . j 1,00 i 1.00 s.oo 1. 00, s.oo' 5,00 ,.! 5,00i

10.0 10.0 10.0 I.

I

u u .. u. ,: U: .': I j ~ . . i ~r •. , U. u u u .. u Li •; u u• u' u. u· u U•i :: u,· u·j u u U. U.

r,

' I I • j'.

l I j !.

I I ! • I

; I

12.0 22.0 1• .0 14.0 10.0

1.00 1.00 1.00 1.00 1.00 1.00 1,00 1.00 1.00 s.oo 1,00 1.00 1.00 1.00 1.00

18.0 1.00 1.00 s.oo 1.00 s.oo s.oo s.oo

10.0 10.0 10.0

d •I •

!u u

.u

l· ~ ·u

u u

f, -~·, ;1'.u'·. i~I I. . ! .. U. lf;U. .,I ;u 'U u

.:U

\;~

.u u u

lu ' l··u u'(

:·ui· : u· . I

-:U I _.µ,

. U .. I I •'

! . I > l' ' • I

I!,.: I;· ;· .. . ' . I

:!: I ,• I

:t .,

i I.• •:. ~;.

'2 )-~ L: /. I

12. 0 , U :?:?. " ti 14.0 I u 14,0 · U 10.0 U

1.00 U 1.00 U 1. 0 ,; U 1. 00 . U 1. oo; ·. u 1. 00; U 1 • 00 ,! U 1, 00: ! U 1. oo,· u s.oo u 1.00 U 1. oo· u 1. oo, U 1.00 U 1.00 U

1 s. o ·u 1.00, U 1.00,. U :i,OO: .U 1,00j · ·u 5,00! ·U s.o~: t u s.o·:>:; u

10.0 i U ' 10.0· ·:: U 1 I u 10 .o ! ,

I

l' -: ; I

I! 1•

i :1 I .

1.·

. I j: r. . . Ii I ~- i . . . l : ... : ·. · l • r:i

- ~--·------·-«--~•··--· . ... . -- ------------- -PROJ3289

. AHAL YSI S TYF·E: VOLATILES

ITLE: HASTINGS MATRIX: WATER UNITS: U,. 'l :.:, .. r,f:: EF'A 7 _ METHOD: 6241Wv~~ C?.SE!

s;.HFLE F'REP: _u;>:-:2_ ANALYST /ENTF;Y: '.'JS RE\.'IEWER: _____ I1ATE: O~J:.9:'26 I

I SAHF'LE NUHBE.RS ,-A.- I\ ~-15

JKLS2C>:?5 JKLS:?026

COl'IPOUHD

~HLOROMETHAHE 1:?. 0 u 12.0 u BF:OMOHETHflNE 2:?.0 u 22.0 u VINYL CHLORIDE 1• .0 u 14.0 u CHLOROETHANE 14.0 u 14.0 u METHYLENE CHLORIDE 10.0 u 10.0 u lrl-DICHLOROETHYLENE 1.00 u · 1.no u 1,1-DICHLOROETHANE 1.00 u 1.00. u

;. TRANS-1,2-DICHLOROETHYLENE 1.00 u 1.00 u i CHLOROFORM 1.00 u 1.00 u

1,2-DICHLOROETHANE 1.00 u 1.00 u 1,1,1-TRICHLOROETHANE 1.00 u 1.00 u CARBON TETRACHLORID~-- 1.00 u 1.p.o u BROMODICHLDROHETHANE 1.00 u 1.00 u 1,2-DICHLOROPROPANE 1. 00 u 1.00 u IiEHZENE 5.00 u s.oo u TRAHS-1,3-DICHLOROPROPEHE 1.00 u 1.00 u TRICHLOROETHYLENE 1.00 u 1.00 u CIS-1,3-DICHLOROF'ROPENE 1.00 u 1.00 u DIBROHOCHLOROMETHANE 1.00 u 1 .09 u 1,1,2-TRICHLOROETHANE 1. 00 u 1.00 u 2-CHLOROETHYLVINYL ETHER 1B.O u 18.0 u BF.:OHOFORH 1.00 -U 1.00 u 1,1,2,2-TETRACHLOROETHEHE 1.00 u 1.00 u

•. i. .. TOLUENE s.oo u s.oo u i, . 1,1,2,2-TETRACHLOROETHAHE 1.00 u _1.00 u ! .· . . CHLOROBENZENE :i.00 u s.oo u i ETHYL BENZENE !i.oo u 5.00 u :- XYLENES,TOTAL s.oo u s.oo u , .. t'\CETOHE 10.0 u 10.0 u

2-BUTAHOHE 10.0 u 10.0 u ETHYLENE DIBROMIDE 10.0 u 10.0 u

H_ PROJ3290

. .. I

-. . .

AHALYSlS TYPE~ VOLhTILES

!TITLE: HASTINGS 1..t1?-! EPA 7

l'IATR!X: WATER METHOD! 6241\J~~i/3 REVIEWER: -.U.L/2/j2 :St,HPLE f'F:EP: _.J_;t'.'~- AHAL YST /ENTRY: VJS

I

COMPOUND

CHLORDMETHAHE BROMOMETHAHE VINYL CHLORIDE .. CHLOROETHANE METHYLENE CHLORIDE l,l-DICHLOROETHYLENE l,1-DICHLOROETHAHE TRANS-l,2-DICHLORDETHYLENE CHLOROFORM 1,2-DICHLOROETHAHE 1,1,l-TRICHLOROETHANE CARBON TETRACHLORIDE BROMODICHLOROHETHANE 1,2-DICHLORDPROPANE BENZENE . TRANS-1,3-DICHLORDPROPENE TRICHLOROETHYLEHE ; CIS-1,3-DICHLOROPROPEHE DIBROMOCHLOROMETHAHE 1,1,2-TRICHLOROETHANE 2-CHLDROETHYLVINYLi ETHER BROHOFORM : 1,1,2,2-TETRACHLOROETHENE TOLUENE . 1,1,2,2-TETRACHLOROETHANE CHLOROBENZENE ETHYL BENZENE XYLENES,TOTAL ACETONE ' 2-BUTANONE ETHYLENE DIBROHIDE

1 SAMPLE NUHP.ERS . g U.,JK..

JKLS:?100

12.0 22.0 14.0 14.0 10.0 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00

u u u u u u u u u u u u u u u u u u· u u .. u ., 1a.o

1.00 1.00 s.oo 1.00 5.00 s.oo '5.00

..u ;

10.0 10.0 10.0

u u ,! u: u· UU i

~ ·1 u

I•

.;

! I

,I 11

~ • i ~ ! I

I

. L~---.

! I

l·

~ ~ J ..

J

J

UNITS: UG/L CASE: ItATE: N,/:!5/S6

. . ·;

.

t . ~---

i:.

~; .·, . : I

..

I ii . ~-r . f •' • • I• • I · .. p ..

-~ :

i . i • -

PROJ3291

! ' I

,. •. ANALYSIS TYPE: TOTAL HETALS

~: HASTINGS B! EPA REG)1l~b'II HPLE PREP:~~- ANALYST/ENTRY! GH4

(;l.~

HATRIX: WATER METHOD: -~00 l lJ77 11 0 REVIEW.ER: ----k~- DATE! 07/0i/96

ENENT

ILVER LUMINUH RSENIC ARIUt1 ERYLLIUH ADMlUH OBALT HROMIUH OPPER RON ANGANESE OLYBDENUN ICKEL EAD NTIMONY ELENIUH ITANIUH HALLIUH ANADIUH INC ALCIUH AGNESIUH ODIUN OTASSIUN

UNITS

UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L HG/L HG/L 116/L HG/L

"w-'S :s JKLS2010D

10. U 6200

so u 130

2. U s. u

16 10. U 10 •. U r :s6oo ·,

t

540 10. U 20 u so u so u so u

lSO 300 U

14 79

190 27 98 s.s

GtJ-:i.::l JKLS2011

10. U 73 so u

130 2. U -s. u.

10. U · •. 10 • u. 10. _ U

120 ~

2. U 10. U-20 u·· so u so u so u so u

300 U-10. U 53 47

a~ 21-2.9

SAMPLE NUHEIERS eu+Nk.

I . : ; .::r=-~ JKLS2034F JKLS2035

. !

,10. :so so . 2. 2. s.

10. .10 •

• I 10. I • SQ. I·. .. 2. · ,. !10 •

.. ,.:.'20· . i. • - ·:so··.

so ,so

. 'SO, . 300

10. I :?O, ., : -· 2~

2~~ 2. I I I I

I

! :

.•qt-,- 1

U . , i 10. U I SO u . so U 240

u u u

u :z. u u s. u U 10. U u I '10. u u I: .10.. u U 1: so '· U u. .1•! I 2 •.. u. Ii

U .. Iii,• :10,.'. U ' · U . -· -:J . .'20 :·;·: U ~ u .- .. j \sor;-; u· u r •so· u u 'i lso u u .. i so u U i'300 U u ··- 1·10. u u ._ -F ,- 20 . . u : U · . i i.6 4 ! _ ... ;. U . ·-· -~j -·· 9 • .... u · ,II 127 · •: .. U .. :: lt 3.6,

! ! }l f: · .. ~ ··1 ii' 1 ' I l

.iJJi!~-;~;1 ·.{ l· '. f-j~ .. ;.;. ~ -~; l . ·,... -

!·•

PROJ3292

\ I . ;l r; ,·, I .= •

=• • I ,· • I

i • ,:

'

··--·-··-·-···-----··-------------

r .. . ..

: ' . ;·• .. ,. ·t • '; •· 1.·

f

ITLE: HASTINGS

~NAL,~lS TYPE: TOTAL HETALS

MATRIX! lilATER. AB: EPA REGY,f~ ~II AMPLE PREP:_14-~L- ANALYST/ENTRY! GM4

6-t..,.\

METHOD: 2001W77~JtS REVIE~ER! ____ _L ___ _ DATE: 07/07/St.

LEMENT UNITS

SILVER UG/L ALUMINUM UG/L ARSENIC UG/L BARIUM UG/L · :&ERYLLIUM UG/L CADMIUM UG/l: COBALT UG/L CHROMIUM UG/L COPPER UG/L IRON UG/L MANGANESE UG/L HOLYBrtENUH UG/L HICKEL UG/L LEAD UG/L ANTIMOMY UG/L SELENIUM UG/L TITANIUM UG/L THALLIUM UG/L ',.'ANADIUl'i UG/L ZINC UG/L CALCIUM HG/L MAGNESIUM HG/L SODIUM HG/L POTASSIUM HG/L

. -~--~ ~

.JKLS:?007

10. u 50 u so u

240 2. u

. s. u 10. u 10. u 10. u

100 :z.1·

10. u 20 u 50 u so u so u so u

300 u 10. u 69 79 13 29

5 • 7

~-'1~ JKLS:?008

10. 190

so 160

u

u

2 • U s. u

10. U 10. · .u 10 • U

::360 · r

0•0 10. U 20 U so u so u so u so u

JOO U 10. u:

140 100

15 ss s.7

SAMPLE NUMBERS ' t::c,>-'fei

! (~LS2009

I •

: . 10. U i 110 I so

JOO u

2 • U s. u

10. U 10. U 16

:=&.w-5-r JKLS:?010

' .: . : •. I

10. u 12000

:so u 240 ,, 2. u

s. u _: 21

13 .:?l

310 -. 11000 I 7.2

. 10. · ~ 20 ii so j I 50

so 1 I so

300 . 10.

= I .

200 110

1~. 38

.: 3 • 8 l ., ' ·i ;i:

I .

u u u u u u u u

570 ,10.

.·, i20 \ ·so

so 50

'350 300 ··:n , 140 210 :JO 110

l·. e.s

i I•:

l

I .. . ·;

Ii p

\

l_ pROJ3293

u u u u u

u

i.

• i

.:. . nNALYSIS TYPE: nISSOLVED HETALS -· -,&..f:':

0

Hf1ST!t;GS ~r:: EF·A F:EGHll-1 'JI!

HATFi:I>:: 1,JATER METHOD:· :?0011.Ji;:., 1 LO

"M:?LE F"F:E.P: ___ "!_/,A_ .:i!'ll'IL YST /ENTF:i': rit'~ REVIE~E.R! -----~ ~ATE! 06/:?7/~6

LEHEHT

S!LVER 1"llUHINUH :'IRSEHl C P.MUUH Bt:F:"t'LL!UH CAI1HIUH rOl:1/\LT CHROHIUH COPPER !ROH Hi\NGAHESE HOLYBtrENUH NICKEL

'LEAD ,"lNTIHO!~Y SELEH!UH )ITAHIUH THt"ILLIUH '.'r.f'-iADIU:i ZINC CALCIUM MAGHESIUH SODIUH r• TASS!UH

UNITS

UG/L UG/L UG/L UG/L UG/L UG/L IJG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L UG/L -HG/L

. HG/L HG/L HG/L

o-.>-ss -P Jl-:LS:?01 OI1

10. 50 :::iO 43 ., -· :s. 10, 10. lO, 50 BS 10. 20 so so 50 50

300 10.

110 :?10

110 14

u u u

u u u u u u

u u u u u u

·u. u

10. so so ., -· ., -· s. 10. 10-. 10. so

10. 20 50 so so

300 10. 20

. ., -· --, -·

Si"1HPLE NUHBEF;S : "I-'-f O

JKLS:?03~

U 10. U 50 U :iO u ::::;o u ~-u s. U ,10. u· · ; 1 o. U ! I • •• 10 • U I 50 u l :? •

U 1· I 110_. u . ,.,0 ·,, I - L

u : r: ; ,s9; U P ~ I ' ro' u ! ··: ~ i :~o· u · I · so·

' . . U .! 300 U · , ! 0~ f

I U · I. ;20

I i 4 •• U ·-:1 t 166· U . 11·. i' · 1 . d1··:, i ~ n. U ·. · ~ ~ 27' U 1,'. ; • S. 7

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PROJ3294

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.:.1ML YSIS TYPE: r, I S E O L 1•1 E D MEH1LS

ITLE: HASTHIGS MATRIX: IJ ,'\TE R

AB: EPA REGI.RJ' AII METHOD! 200!1.J71M.B c~HPLE PREP! ____ i _ AN~LYST/ENTRY! GM2 RE 1.'IEWER: _____ !•ATE: 06/27/86

G-J..tr\ SM·iF'LE NUMBE:RS

Dw-'3c::i 6,..,.)- 1.h, ~-L/~ D(..o)-!p-S JKL52C-07 J~:LS:?OC•S JKLS200 JKLS2010

LE!iENT UNITS

SILIJER UG/L 10. u 10. u 10. u 10. u. ALUMHIUH UG/L so u so u so u :;o u ,"IRSnl!C UG/L so u so u so u :;o u P.l'iRIUM UG/L :?30 1:?0 300 43 BERYLLIUM UG/L :? • u 2. u ., u ., u ... -· Ct1DMIUH UG/L s. u s. u s. u ~. u COBALT UG/L 10. u 10. u 10. u 10. u CHROMIU!i UG/L 10. u 1 O •. ·U 10. u 10. u COPPER UG/L 10. u 10. u 10. u 10. u

• IP.ON UG/L so u so u so u so u ! MANGANESE UG/L J. .:?. u J.2 100

MOLYBDENUM UG/L 10. u 10. u 10. u 10. u ~

NICKEL UG/L 20 u 20 u 20 u 20 u LEAD UG/L so u 50 u so u so u

I· !. r'\NTIHONY UG/L so u 50 u 50 u so u

SELENIUM UG/L so u so u 50 u so u TITANIUM UG/L :so u so u so u so u THALLIUM UG/L ?00 u 300 u 300 u 300 u VANA!I I UH UG/L 10. u 10. u 10. u 10. u ZINC UG/L 75 94 1:?0 S2 CALCIUH HG/L 81 97 · 120 210 MAGNESIUM HG/L 14 1S 20 30 SODIUM HG/L Jl S4 40 110· POTASSIUM HG/L s.-1 a.a s.4 14

t•. r r

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PROJ3295 1

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EPA REGION VII INORGANIC DATA

TITL~: .1KLS2 DATE: 06/25/96 MATRIX: WATE~ .: . . ·:

• •I

STD, CURVE ~ 1 READING

i STD 100 114 2 STD so 47 3 STD 30 21 4 STD 20 .l: ii s STD 10 . ·, ,7,9 l., STD s ··. ·t 2,S 7 STD 1 .; · .. : D,3

'8 BLK 0 . :0, 0 ·, , .

SAMPLE NO, . !RESULT

JKLS2034F .11<LS2901C J'KLS2901A Jl<L5203S . JKLS2002

· ,·: '.~ ,:tG/L

0,1 6.80 .. ~.

' 26,0 52,0

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u .·

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0 6.8

26 52

I ,

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PARAMETER: SULFATE AG SO4 HCTH0D: 37SiU0~ -:J/p~ ANALYST: KLC ¥_~~

MULTI PLICATION' QC FACTOR REr-'

1 1 !

7,2 1 1

%REC

94,4

PROJ3296

'

CHL• r-:IDC FPA REGION VII

TITLE: JKL~2 CHLORIDE DATE:. 06/23/Bb MATRIX: WATER ;

. BLANK MLS TITRANT BLAN!{ 1 0

INORGANIC DATA

PARAMETER: CHLORID~

METHOD: 32S1~ ~ AHAL YST: 'J!H /

I!. •· I -

j l . ; i I . ! [~ . , 1· i 1

STANDARD

STANDARD 1

MLn TITRANT HLS STANDARD NORMALITY

.STANDARD 2 ~STANDARD 3

24.73 24.? 24,73

SAMPLE NO, RESULTS l'fG/L

l'l<LS2.001 o~ld J'KLS20 02 o,.,-J~ 1KLS200Jo,.a-Z• 1KL52004P JKLS200S• ... -2-I .1KLS2006 • ..-. ~j .JK LS2 0 07 .,u>--~

J'K LS2 0 0 8 0vr 11,~ J'KLS20 09 PelJ ~ J'KLS2010 19111-,;, J'KLS2900C l'KLS2900A JKLS2900M J'K LS2011 t?z,4...J JKLS2034F J'KLS203S ':r-'I° JKLS203SS JKLS203SR

17.4 21.4 34.2 11. 0 14,6 23,6 40,S ~.-~. 36,4' ·l.;i."1 17-.-9 17.8

i 8,9S . 1

17.7 139 12S

25 2S 2S

MLS TITRANT

3, 4!j • .23 6,77 2, 17 2.09

.: 4,67 · a. 01

13 7.2 12,87 3, 55····- ·

0

-

U 0 ·1,77

U 0 3,5 27.42

1, 42S3?E-02 .. 1. -42713E-02 i 1,42539E-02 .

' '

HLS SAMPLE

fOO 100 , 100 :: 100' 100 100 100 10 0: 100· 100

· 100

100 100 100 100 100

i I I j I·

i QC X REC

100 .8

100 .3

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PROJ3297

. . . . ·-

NUTRIENTS I

'I.

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EPA RCGION VII INORGAN C DATA

TITLE: JKLS2 DATE: 06/10/06 MATRIX: WATER

STD, CU~VE READING

i 2 3 • 5 6

STD 20 0 STD 150 STD 100 STD SO STD S BLK 0

; SAMPLE NO.

J'KLS2003 JKLS20 07 J'KLS2009 J'KLS2010 JKLS2931C J'KLS2931A 1KLS2001 J'KLS20 04P JKLS20 OS .1KLS2006 JKLS2008 J'KLS2011 JKLS2930H JKLS2011S J'KLS2011R

20!3 197 109 38 3,S 0,9

RESULT I NG/L i

ss.o ss.o ,120 "280 91. 0

41.0 7. 00 43.8 26.S 31.S 26.0

0.6 30 ,4

READING

ss ss 120 140 91

41

'· '43.8 2£>.S 31.S 26 ,·6 30 .4

. i PARAMETER: SULFATE AS SO4 METHOD: 3751W~o~~ ~ ANALYST1 .KC2 t:.-f'

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MULTIPLICATION FACTOR

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94 96,S

6,1 72.1 I I .. i.

PROJ3298

,.

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1

ALKALI~ITY , EPA RCGION VII INORGANIC PATA

I

TITLE: JKLS2 ALK DATE: 06/23/86 MATRIX: WATER

STANDARD

STANDARD STANDARD

1 2

HG NA2C03

21.8 21.9

HLS H2S04

20, 1S 20 ,4

SAMPLE NO, RESULTS NC/L

HLG TITIMNT

J'KLS2900C 22,4 2.2 JKLS2900A 21.7

'1 .: ' • I j I. f

PARAMETER:~ ALKALINITY:~·. HE:THOD: :31 D 1W)?h_a ·. 1 ·l ANtLY~T: I R,f p -,:..?L_I f ti)

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JKLS2001 ow-Id 198 JKLS2002°..a- 1

" 332 Jl<LS20 O3 t>&..>•'1.S 304 -.1KLS2004P--~ 17.3 JKLS200So.--'Z-=l 172 J'l<LS2006.,..,,.-5_, 171 JKLS20Q7cu-3d 192 JKLS2 0 QQ.::,11....f,s 302 J'KLS20 09!Jw-'1:/ 277 JKLS2010Pt.cl-~-' ,f44

19.S 32,6? 29,9 1.? 16,9 16.8 10,87 29,7 27,2~ 43,? 1S,6

10·0 !_ ·.' _.

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JKLS201i ~ iS9 JKLS2034F 1 JKLS203S ::C-i.fO 1 fi'O JKLS203SL 189 JKLS203SS 40S JKLS203SR 223 J'KLS2901C 22,4

-J'KL.S2901A 21, 7

I~ j ··ir -- -~--- &.-,,,--.....

U • OS 18. 7 ·9,3 19,92

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- === •=·-*=··· .. -<::wnr===-2> 0 . X:.:..~. C ··-• - -·

APPENDIX B-6

GROUND WATER ANALYSES

SEPTEMBER 1986

IITLE: ANALYSIS TYF'E: VCLATlLE ANALYSES.

HASTINGS MATRIX! WATER UNITS: UG/L AB: EMS! METHOD: 9302M01/)d- CASE: 2463G

SAHF'LE F'REF·: ------- ANALYST/ENTRY! El9 REV! ElJER: 4'£4__ --1+ DATE! 10/:!2/86

M--1 SAMF'LE NUMBERS

~-'7 M-tl M-1~ QKLS2001 QKLS2002 GKLS2003 cn:Ls2004

COMPOUND

CHLOF:OMETHANE 0.2 u 0.2 u 0.2 u 0.2 u BROMOMETHANE o.5 u 0 • 5 u 0.5 u o.~ u VINYL CHLORIDE 0.2 u 0,2 u 0,2 u 0,2 u CHLOROETHANE 0~2 u 0.2 u 0,2 u 0.2 u METHYLENE CHLORIDE 1.00 u 1.30 u 0.9 u 1. 10 u ACETONE N/A I NIA I NIA I N/A I CAF:BON It! SULFIDE N/A I N/A I N/A I NIA I 1, 1 DICHLOROETHENE 0.1 ·u 0.1 u 0.1 u o.i u 1, 1 DICHLOROETHANE 0.1 u 0.1 u 0,1 u 0,5 TRANS-1,2,-DICHLOROETHENE 0.1 u 0,1 u 0.1 u 0,1 u CHL OF:OFORM 0.1 u 0.1 u 0.1 u 0.1 u 1,2,DICHLOROETHANE 0. 1 u 0.1 u 0.1 u 0,1 u 2-BUTANONE NIA I N/A I NIA I ~UA I 1 , 1 , 1 TRICHLOROETHANE 0.1 u 0,1 u 0.1 u 0.1 u CARBON TETRACHLORIDE 0,1 u 0, 1 u 0.1 u 0,1 u VINYL ACETATE NIA I NIA I N/A I NIA I BROMODICHLOROMETHANE 0,1 u 0, 1 u 0. 1 u 0,1 u 1,1,2,2,-TETRACHLOROETHANE 0,1 u 0,1 u 0,1 u 0.1 u

,2-DICHLOROPROPANE 0,1 u 0.1 u 0, 1 u 0, 1 u 1RANS-1,3-DICHLOROPROPENE 0,1 u 0.1 u 0,1 u 0,1 u TRICHLOROETHENE 2,50 u 0.1 u L10 u 0,8 u DIBROMOCHLOROMETHANE 0.1 u 0.1 u 0,1 u 0,1 u 1,1,2-TRICHLOROETHANE 0.1 u 0,1 u 0,1 u 0.1 u BENZENE 0.2 u 0.2 u 0,2 u 0.2 u CIS-1,3-DICHLOROPROPENE 0.1 u 0,1 u 0.1 u 0,1 u 2-CHLOROETHYL VINYL ETHER 0,4 u 0,4 u 0,4 u 0.4 u :E-:ROMOFORM 0.1 u 0.1 u 0.1 u 0.1 u 2-HEXANONE NIA I NIA l NIA I N/A I 4-METHYL-2-PENTANONE NIA I NIA I N/A I NIA I TETRACHLOROETHENE 0.3 u 0.1 u 0,1 u 0.1 u TOLUENE 0,6 u 0,2 u 0,2 u 0.6 u CHLOROBENZENE 0.1 u 0, 1 u 0. 1 u 0,1 u ETHYL BENZENE 0,5 u 0,5 u 0.5 u 0.5 u STYRENE NIA I NIA I ~UA I H/A I TOTAL XYLENES N/A I NIA I N/A I N/A I

PROJ3301

AUALYSIS TYF·E: VOLATILE ANALYSES

·rLE: HASTING~ MATRIX: WATER UNITS: UG/L .B: EMSI HETHor•: 9302HOV./ CASE! 2463G

SAMF'LE F'REF': ------- ANALYST/ENTRY: E19 REVIEWER! p/./! - - DATE! 10/22186

CW1S~.s~ (AS SAMPLE NUMBERS , J~W,-,, c,w-1..s ti- I

QKLS2005 QKLS2006 OKLS2007 COMPOUND

CHLOROMETHANE 0.2 u 0.2 u 0 • 2 u BROMOMETHANE 0.5 u 0.5 u o.s u VINYL CHLORI!1E 0.2 u 0.2 u 0.2 u CHLOROETHANE 0.2 u 0.2 u 0.2 u METHYLENE CHLORIDE 0.6 u .o.s u o.s u ACETONE NIA I N/A I NIA I CAR:E:ON DI SULF II1E NIA I NIA I NIA I 1, 1 DICHLOROETHENE 0, 1 u 0.1 u 0,1 u 1 , 1 DICHLOROETHANE 0.1 u 0.1 u 0,1 u TRANS-1,2,-DICHLOROETHENE 0.1 u 0.1 u 0.1 u CHLOROFORM 0.1 u 0.1 u 0. 1 u 1,2,DICHLOROETHANE 0. 1 u 0.1 u 0, 1 u 2-BUTANONE NIA I NIA I NIA 1 1, 1 , 1 TRICHLOROETHANE 0. 1 u 0.1 u o.7 u CARBON TETRACHLORIDE 17.0 1.20 u 0, 1 u 'JINYL ACETATE NIA I NIA I NIA I BROMODICHLOROMETHANE 0.1 u 0,1 u 0.1 u t,1,2,2,-TETRACHLOROETHANE 0,1 u 0,1 u 0,1 u

2-DICHLOROPROPANE 0,1 u 0,1 u 0,1 u ,~ANS-1,3-DICHLDRDPRDPENE 0.1 u 0.1 u 0, l u TRICHLOF:OETHENE 4,50 0,8 u 30.0 D!BROMOCHLOROMETHANE 0.1 u 0.1 u 0.1 u 1,1,2-TRICHLOROETHANE 0,1 u 0,1 u 0.1 u BENZENE 0,2 u 0.2 u 0.2 u CIS-1,3-DICHLOROPROPENE 0.1 u 0.1 u 0.1 u 2-CHLOROETHYL VINYL ETHER 0,4 u 0,4 u 0.4 u BRO MO FORM 0.1 u 0.1 u 0.1 u 2-HEXANONE NIA I NIA I N/A I 4-METHYL-2-PENTANONE N/A I NIA I NIA I TETRACHLOROETHENE 0.1 u 0.1 u 0. 1 u TOLUENE 0,5 u 0.2 u 0 • 2 u CHLOROf:ENZENE 0. 1 u 0.1 u 0, 1 u ETHYL BENZENE 0,5 u 0,5 u 0,5 u STYRENE NIA I NIA I NIA I TOTAL XYLENES N/A I N/A I NIA I

] PROJ3302


r TITLE: HASTINGS MATRIX: WOTER ~ UNITS: UG/L LAB! EMSI METHOD: 9~0:?MO CASE! 2463G SAMf'LE F'REF' ! ------- ANALYST/ENTRY: E20 REVIEWER! /.ff/{__ -!;:. Df':TE: 10/22186

owk/ SAMF'LE NUMBERS 4 OW].:, ow~ Oi.03

OKLS2008 OKLS2009 OKLS2010 cn:Ls2011 COMPOUND

CHLOROMETHANE 0. 2 u 0.2 u 0,2 u 0. 2 l BROMDMETHANE o.5 u 0.5 u 0.5 u 0,5 l VINYL CHLORH1E 0. 2 u 0.2 u 0.2 u 0.2 t CHLORDETHANE 0,2 u 0,2 u 0,2 u 0,2 l METHYLENE CHLORIDE 0.6 u 0,7 u 0.1 u 0,5 l ACETONE NIA I NIA I N/A I N/A J CARBON DISULFIDE NIA I NIA I NIA I tUA J 1,1 :Ct I CHLOROETHENE 0.1 u 0,1 u 0,1 u 0.1 L 1,1 t1I CHLOROETHANE 0.1 u 0.1 u 0.1 u 0.1 L TRANS-1,2,-DICHLOROETHENE 0.1 u 0.1 u 0,1 u 0.1 L CHLOROFORM 0,1 u 0.1 u 0.1 u 0.1 u 1,2,DICHL•RDETHANE 0.1 u 0,1 u 0,1 u 0.1 u 2-BUTANONE NIA I NIA I N/A I rUA I 1 , 1 , 1 TRICHLOROETHANE 0.1 u 0.1 u 0.1 u 0.1 u CARBON TETRACHLORir1E 0,1 u 0.1 u 0.6 u 0.1 u 'H~YL ACETATE NIA I NIA I NIA l N/A I

dROMODICHL• ROMETHANE 0.1 u 0.1 u 0,1 u 0.1 u 1,1,2,2,-TETRACHLOROETHANE 0,1 u 0.1 u 0,1 u 0.1 u 1,2-DICHLOROPROPANE 0,1 u 0,1 u 0,1 u 0.1 u TRANS-1,3-DICHLOROF'ROPENE 0,1 u 0.1 u 0,1 u 0,1 u TRICHLOROETHENE 44,0 3.-oo u 68,0 3.00 u DIBROMOCHLOROMETHANE 0.1 u 0.1 u 0,1 u 0.1 u 1,1,2-TRICHLOROETHANE 0.1 u 0.1 u 0.1 u 0.1 u BENZENE 0.2 u 0 • .2 u 0. 2 u 0.2 u CIS-1,3-DICHLOROPROPENE 0,1 u 0.1 u 0.1 u 0.1 u 2-CHL OF:OETHYL VINYL ETHER 0.4 u 0,4 u 0,5 u 0,4 u BR OMO FORM 0. 1 u 0.1 u 0.1 u 0, 1 u 2-HEXANONE NIA I NIA l NIA I NIA I 4-METHYL-2-PENTANONE NIA ! NIA I NIA I N/A I TETRACHLOROETHENE 1.30 u 0,5 u 0. 1 u 0,7 u TOLUENE 0.2 u 0.2 u 0.2 u 0,2 u CHLOROBENZENE 0.1 u 0.1 u 0. 1 u 0, 1 u ETHYL BENZENE 0,5 u 0,5 u 0.5 u 0,5 u STYRENE N/A I NIA I N/A I N/A I TOTAL XYLENES NIA I NIA I NIA I ~i / A I

l PROJ3303

~ltKITl C sz -,


!TLE: HASTINGS MATRIX: WtHER UNITS: UG/L

u:: EMSI METHOD: 9302MO½ CASE: :::?463G

SAMPLE PREF'!------- ANALYST/ENTRY! E20 REVIEWER! 4'..{4 --i DATE: 10/22/86

ow-~ SAMF'LE NUMBERS Ow4-S ovJ4-d u 1,,,J Ll-d ( ")

OKLS2012 QKLS2013 QKLS2014 m::LS2014D COMPOUND

CHLOROMETHANE 0.2 u 0.2 u 0.2 u 0,2 u BROMOMETHANE o.s u o.s u o.s u 0,5 u VINYL CHLORI!IE 0.2 u 0.2 u 0. 2 u 0,2 u CHLOF:OETHANE 0.2 u 0.2 u 0.2 u 0.2 u METHYLENE CHLORIDE o.6 u 0.5 u 0.1 u 0.5 u ACETONE NIA I NIA I NIA I N/A I CARBON rt I SULFIDE NIA I NIA I ~UA I N/A I 1,1 DICHLOROETHENE 0.1 u 0.1 u 0, 1 u 0.1 u 1,1 IlICHLOROETHANE 0.1 u 0,1 u 0,1 u 0,1 u TRANS-1,2,-rtICHLOROETHENE 0.1 u 0.1 u 0.1 u 0.1 u CHLOROFORM 0.1 u 0.1 u 0,1 u 0.1 u 1,2,DICHLOROETHANE 0,1 u 0.1 u 0,1 u 0.1 u 2-E:UTANONE NIA I NIA I NIA I N/A I 1, 1, 1 TF:I CHLDROETHANE 0 • 1 u 0,1 u 0.1 u 0,1 u CARBON TETRACHLORIDE 0 • 1 u 0,1 u 0,1 u 0,1 u VINYL ACETATE NIA I NIA I NIA I H/A I BRDMODICHLDROMETHANE 0,1 u 0.1 u 0,1 u 0.1 u 1,1,2,2,-TETRACHLOROETHANE 0.1 u 0.1 u 0,1 u 0,1 u

·2-DICHLOROPROPANE 0.1 u 0.1 u 0.1 u 0,1 u ~ANS-1,3-DICHLOROPROPENE 0.1 u 0,1 u 0,1 u 0, 1 u

TRICHLOROETHENE 9.00 s.oo 74,0 61. 0 DIBROMOCHLOROMETHANE 0,1 u 0,1 u 0.1 u 0,1 u 1,1,2-TRICHLDROETHANE 0.1 u 0,1 u 0,1 u 0.1 u BENZENE 0, 2 u 0.2 u 0,2 u 0,2 u ClS-1,3-DICHLOROPROPENE 0.1 u · 0. 1 u 0,1 u 0, l u 2-CHLOROETHYL VINYL ETHER 0.4 u 0,4 u 0,4 u 0,4 u BROMOFORM 0,1 u 0.1 u 0.1 u 0, 1 u 2-HEXANDNE NIA I NIA I NIA I ~J/A I 4-METHYL-2-PENTANONE NIA I NIA I NIA I ~UA I TETRACHLOROETHENE 0,6 u 0,4 u 1.00 u 2, 5 0 u TOLUENE 0.2 u 0,2 u 0,2 u 0.2 u CHLOF:OBENZENE 0.1 u 0.1 u 0, 1 tJ 0, 1 u ETHYL BENZENE o.5 u 0.5 u 0.5 u 0,5 u STYRENE NIA I NIA r· NIA I NIA I TOTAL XYLENES NIA I NIA I NIA I ~!/ A I

I. PROJ3304

ANALYSIS TYF·E: VOLATILE AHALYSES

•TLE: HASTINGS MATRIX: Wt.TER UNITS: UG/L .. -1B: EMSI METHOD! 9302MO~ CASE: 2463G

SAMF'LE F·REF': ------- ANALYST/ENTRY: E20 REVIEWER! p.?4 --f r1ATE: 10122186

ow5.s SA,r·LE NUMBERS O&" ()WSi· Field g~k-

OKLS201S OKLS2016 OKLS2017F OKLS2018 CQ_MF'OUND

CHLOROMETHANE 0.2 u 0.2 u 0. 2 u 0.2 u BROMOMETHANE o.s u o.s u o.s u 0,5 u VINYL CHLORIDE 0.2 u 0.2 u 0.2 u 0.2 u CHLOF:OETHANE 0.2 u 0.2 u 0.2 u 0.2 u METHYLENE CHLORIDE 0.3 u 0.1 u 6.60 1.50 u ACETONE N/A I N/A I NIA I N/A I CARBON !II SULFIDE NIA I NIA I NIA I N/A I 1,1 DICHLOROETHENE 3.50 0. 1 u 0.1 u 1.50

; 1,1 !1 I CHLOROETHANE 0.1 u 0 • 1 u 0.1 u 0,1 u ., TRANS-1,2,-DICHLOROETHENE 0.1 u 0,1 u 0.1 u 0, 1 u +- CHLOROFORM 0.1 u 0.1 u 0.1 u 1.00 ' 1,2,DICHLOROETHANE 0.1 u 0.1 u 0.1 u 0.1 u 2-BUTANONE NIA I N/A I NIA I NIA I 1, 1 , 1 TRI CHLOROETHM,E 35.0 3,50 0, 1 u 8,00 CARBON TETRACHLORIDE 0.1 u 0. 1 u 0.1 u 4,40 VINYL ACETATE N/A I N/A I ~UA I i-UA I BRDMODICHLOROMETHANE 0.1 u 0, 1 u 0,1 u 0,1 u \,1,2,2,-TETRACHLOROETHANE 0.1 u 0.1 u 0,1 u 0.1 u

,2-DICHLOROPROPANE 0.1 u 0.1 u 0.1 u 0 .1 u fRANS-1,3-DICHLOROPROF'ENE 0.1 u 0.1 u 0.1 u 0.1 u TRICHLORDETHENE 1100. 34,0 0, 1 u 180 DIBROMOCHLORDMETHANE 0,1 u 0.1 u 0,1 u 0,1 u 1,1,2-TRICHLDROETHANE 0.1 u 0, l u 0.1 u 0,1 u BENZENE 0,2 u 0,2 u 0,2 u 0,2 u CIS-1,3-DICHLOROPROPENE 0.1 u 0.1 u 0,1 u 0, 1 u 2 - CHLO F: 0 ETHYL VINYL ETHER 0.4 u 0.4 u 0.4 u 0,4 u BF:OMOFORM 0.1 u 0.1 u 0.1 u 0.1 u 2-HEXANONE N/A I N/A I NIA I NIA I 4-HETHYL-2-PENTA~ONE NIA I N/A I ~UA I ~UA I TETRACHLORDETHENE 29.0 1,70 u 0,1 u 1.50 u TOLUENE 0,2 u 0.2 u 0.2 u 0,2 u CHLORDBENZENE 0. 1 u 0 • 1 u 0, 1 u 0.1 u ETHYL BENZENE 0.5 u 0,5 u 0,5 u 0,5 u STYRENE NIA I NIA I ~UA I NIA I TOTAL XYLENES NIA 1 N/A I NIA I rUA I

PROJ3305

/ **CORRECTED DATA**


£TLE! HASTINGS ·AB! EMSI

AMPLE PREP! ______ _ ANALYST/ENTRY! E20

MATRIX: WATER METHOD: 9302MO(f\;.._{_ REV I EWER: .:A.:Jf..-~-f-

COMPOUND

CHLOROME:THANE BF:OMOMETHANE l.!INYL CHLOF:IDE CHLOROETHANE METHYLENE CHLOF:IDE ACETONE CARBON DISULFIDE 1,1 !1 ! CHLOROETHENE 1, 1 DICHLOROETHANE TRANS-1,2,-DICHLOROETHENE C:iLOROFORM 1,2,DICHLOROETHANE 2-BUTANDNE l , 1 , 1 TRICHLOROETHANE CARBON TETRACHLORIDE VINYL (1CEH1TE BF:OMODICHLOROMETHANE 1,1,2,2,-TETRACHLOROETHANE

,2-DICHLOROPROPANE fRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DlBROMOCHLOROMETHANE 1,1,2-TRICHLOROETHANE BENZENE CIS-1,3-DICHLOROPROPENE 2-CHLOROETHYL VINYL ETHER BROMOFORM 2-HEXANONE 4-METHYL-2-PENTANONE TETRACHLOROETHENE TOLUENE CHLO ROBE1~ZENE ETHYL BENZENE STYREHE TOTAL XYLENES

r-~ Gkv-,t... QKLS2019F~

0.2 u 0.5 u 0.2 u 0.2 u 0.1 u NIA I NIA I 0.1 u 0.1 u 0 • 1 u 0.1 u 0.1 u NIA I 0.1 u 0.1 u NIA I 0. 1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.2 u 0.1 u 0.4 u 0. 1 u N/A I NIA I 0,4 0.2 u 0.1 u 0,5 u N/A I N/A I

SAMPLE NUMBERS -r~

QKLS2021

0.2 u 0.5 u 0.2 u 0.1 u 2.00 u NIA I NIA I 1.10 1.00 0.1 u 0.1 u 1.00 NIA I 6.00

45.0 NIA I 0.1 u 0.1 u 0.1 u 0. l u

69.0 0.1 u 0.1 u 0.2 u 0.1 u 0.4 u 0.1 u NIA 1 NIA I 1. 40 u 0.2 u 0.1 u 0,5 u NIA I NIA I

UNITS! UGIL CASE! 2463G !1 ATE : 1 0 12 2 / 8 6

PROJ3306

TITLE: HASTINGS LAB: Er1SI ANALYST/ENTRY: LT

COMF·OUND NAME

DICHLORODIFLUOROMElHANE TRICHLORDFLUORDMETHANE 1~2 DICHLOROBENZENE 1,4 D!CHLOROBENZENE 1~3 DICHLOROBENZENE ETHYLENE DIBROM!DE

1

• 1 • 1 .,. . ·-' .3 ..,.. . _, • 1

. :

u u u u

i . u u

UNITS: UG/L CASE:

• 1 • 1 • 3 .3 .3 • 1

SA32463G 10-22-8,~

u u u u u LI

PROJ3307

TITLE: HASTlNGS LAB: EMSI ANALYST/ENTRY: LT

CDMF'DUND NAME

D!CHLORODIFLUOROMETHANE TRICHLOROFLUDROHETHANE 1~2 DICHLOROBENZENE 1,4 DICHLOPDBEN?ENE 1,3 DICHLOROBENZENE ETHYLENE DIBROM!DE

MATF:IX: l•J.::,TER UNITS: UG/L METHOD: 93(•2vM)1 Ci!'1SE: SAS2463G. REVIEWER: BG~ DATE: 10-=2-86 ~/'7

SAl'IF'LE NUMBEF:S

•· - .... . , .. ·--: .. ' . ~ .- . - ....

1

i

i'

~ . . ••.

~~ I

1:·,. :·: l_:, · •. ,.

. . I

• 1 • 1

. ..::, "'!' . -·

• l

, .

PROJ3308

u u u u u u

TlTLE: HASTINGS LAB: EMS! PttlAL YST /ENTRY: LT

COMPOUND t·JAl"IE

DICHLORODIFLUOROMETHANE TF: I CHLOF:OFLUOF:or-1:::THANE 1,2 D!CHLOROBENZENE 1, 4 DICHLOF:08El'!ZEr~E 1~3 DICHL• ROSEN!ENE ETl-!YLEME DI B;::;or--; l DE

t-1;.TF:IX: l.JATE~: UNITS; UG/L METHOD: 9302M01 CASE: SAS2463G REVIEWER: 82~ DATE: 10-22-86 (; '/{

O W~cf SAMPLE NUMBER·3

C1!:::LS20l 2

• 1 u • 1 ll .3 u .,. ...... u . -~ u • 1 LI

.. - .. -- ... __ . . . .

--;:-.· __

..

pROJ3309 -)

-------------------•----------.~••~.-...-- 1....,._.. • •· M.a...P.,.-:...&__,..,_,~-CU:--0..-,, =---p

I 'I

TITLE: HP:ST I NGS LAB: EMSI ANALYST/ENTRY: LT

C01'1F'OUND NAME

DICHLORODIFLUOROME~HANE TRICHLOROFLUOROMETHANE 1,2 DICHLOROBENZENE 1,4 DICHLOROBENZENE 1,3 DICHLOROBENZENE ETHYLENE DIBROMIDE

MATRIX: W0TER UNITS: UG/L METHOD: 9302vM•)l CA·:iE: SA'32463G REVIEWER: BGM DATE: 10-22-86 ~t /'I

SAMPLE NUMBERS \o i

1

- -- .. I(,~, LS'?') 1 c. .· , ... ·-· -. I

•·-. I .. ', :: .. i•-1 U .' ·. · .. ·· .. - _. 1 U , . ·' -., I •

.. ;_, u ...,.. .. _-,,

c.. ._;

u ·u

. - . ~ ~. -: ... ·• . · .

.. ~~ ·-

. ~ ._ ·i

...... - ...:.\ . :

- .. ·.:.-:;· ..

·. j.

PROJ3310

, , 1·l1LI:: H~ST!i•·JGS :...;.;r,~ Ei·lS J {.:,1.;C,L.YST/ENTR·/: LT

CDMF"OUt-lD NAME.

D!CHLOROD!FLUOROMETHANE TF: I C:i-!LOF:OFLUOF:OMETH.'~NE 1~? DlCHLOROBENZENE !~4 D!CHLOROEENZENE 1 ~ 3 I:•!CHLC1F:OBENZ:EIJE ETHYLENE D!BRCM!DE

:

Mt"·, T~-: I:, : l•JA T ER i·1F1 HDC•:

.-1' U . .. ..

. ; 1 ;· s·

.3 • 3 . ::s

3.:2

-~-::- ·-::- ....

u u u u

·:•~·· .: }·=:\~-.::._:"·• ·- _.::.. •,. . .. _ .

. ·· ./iili ;1;,:tii~ : -/ < ~ ,_,; ·"'.":"_ ·':..:·.· .. .- ..

·-. ·r-•;. •. ). -.:·:_.: _. -· •··

·· .. ·. ~~-. -. i /,_;_;_,. _-; ... . •

. - ,.:.. . . ·:--: · . .-·. __ _._

·-: . .... --. -..

-··: .. :: ~- .;··_ : ....

PROJ3311

.......... --- ... ••' ·- -

-·-·· :. -:- . ~.

ANi!iLYSIS TYF·E: i

SEMIVOLATILES (F'AGE 1 ) I

TITLE: BLAYNEY @ H~0iSTINGS tiATRIX: WATER U!UTS!. UG/L LAB: IT METHOD: ~01 CASE! 6385" 3" ·•t:·LE F·REF': ------- ANALYST/ENTRY! E8S F:E:IEWiR: ~--~f, :!rf:TE: 10/14/86

ow~ ; o:cJ~E NUMBERS·

--:I.'¥1 QKLS2013 •QKLS2014 OKLS2021

COMF'OUNI:r ! 'I

PHENOL 20.0 u :20.0 u 20.0 I u BIS(2-CHLOROETHYL> ETHER 20.0 u ·1

u 20.0 u i I 20 .0 I

2 - CH l ORO F· HEN O l 20.0 u 20.q u 20.0 ·1 u '! 1,3 DICHLOROBENZENE 20.0 u 20.0 u 20,0 u

I

l • 4 ItI CHLOROE:ENZENE 20,0 u 20.q u 20.0 u BENZYL ALCOHOL 20.0 u 20.0 u 20,0 u 1,2 DI CHLOROP,ENZENE 20.0 u 120.0 : I u 20.0 .u 2-l-iETHYLF·HDlOL 20.0 u !20.0 I : u 20.0 u

I ! I I BISC2-CHLOROISOPROPYL>ETHER 20.c, ll 20.q u 20.0 I

u 4 - METHYL F' HEN O L 20.0 u 20.0 : I u 20.0 u

I ' I N-NITROSO-DIPROPYLAMINE 20.0 u 2,::,. q u 20.0 ; . u HEXACHLOROETHANE 20.0 u : 20. 0 .. u ' 20,0 u NIT'ROBENZENE 20,0 u I 20. d : u 20.0 u , I ' 1 SOF'HOROt~E 20.0 u i 20. tj u ·, 20.0 ! u ., 2 - ti I T F: 0 r· HEN O L 20.0 u :20.0 u 20.0 u 2,4-DIMETHYLPHENOL 20.0 u 20.0 u 20.0 u HEl'l: 0 IC ACID 10') u 100 : u 100 u BlS(2-CHLOROETHOXY) liETHAME 20,0 u 20.0 u 20.0 u 2~4 !1 I CP.LOROF·HE~IOL 20.0 u 20.0 u 20.0 u 1,~,4-TRICHLOROBENZENE 20. 0 u 20.0 u 20.0 u l· THALENE 20.0 u :o.o u 20.0 u 4-1...r!LOROANILINE 20.0 u 20,0 u 20.0 u HEXACHLOROBUTADIENE 20.0 u 20.0 u 20.0 u 4-CHLORD-3-METHYLF'HENOL 20.0 u 20.0 u 20.0 .u 2-METHYLNAPHTHALENE 20.0 u 20.0 u 20.0 u HEXACHLDROCYCLOPENTADIENE 20.0 u 20.0 u 20.0 u 2,4,6-TRICHLOROPHENOL 20.0 u 20,0 u 20.0 u 2,4,5-TRICHLOROPHENOL 100 u 100 ' u 100 u 2-CHLDRONAPHTHALENE 20.0 . u 20.0 u 20.0 u

-:-NITROANILINE 100 u 100 I u 100 u I

DIMETHYLPHTHALATE 20.0 u :20.0 u 20.0 u ,; C Er,A PHT HYL EHE 20. 0 u : 20. 0 u :o.o u I. ~-~HT F,OMH LI i',E 100 u 100 u 100 u I

,·1 CE r, ,:1 F· HT HEN E 2•:).0 u 20.0 ' u 20.0 u ~, 4-(IIIJITF:OPHENOL 1 •JO u 100 I u 1 ·JO u 1-NI T F:OF'HENDL 1 O·J u 100 i u 100 u I

;-, I Ii !:: NZ O :=- U F: A N 20.0 u 20.0 u ::o. 0 u 2,4-DINITROTOLUENE 20.0 u 20. 0 u 20.0 u

I

I

I_ PROJ3312

• I ' "!

ii I I . i :, ; r I

AN ALYS ! S T YF' E :

.E! BLAYNEY e HASTINGS

SEMIVOLATILES (PAGE I I.

I I . ,· MATRIX; WATER UNITS! UG/L

LAB: IT SAMPLE PREP! _______ ANALYST/ENTRY! EB9

COMF'OUN!1

2,6-DINITROTOLUENE DIETHYLPHTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 4,6-DINITR0-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLORDBENZENE PENTACHLOROPHENOL F'HENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE PYF:ENE BUTYL BENZYL PHTHALATE ,.3, DICHLOROBENZIDINE

ZO(A)ANTHRACENE Bi~C2-ETHYLHEXYLJPHTHALATE CHRYSENE DI-N-OCTYL PHTHALATE BENZO<B)FLUORANTHENE BENZO<K>FLUORANTHENE B ENZ O < A ) F' YR ENE INDENO<l,2,3-CD)PYRENE DIBENZO(A,H>ANTHRACENE BENZOCG,H,I>PERYLENE

ow4s QKLS2013

20,0 20,0 20.0 20.0

100 100 20.0 20.0 20.0

100 20.0 20.0 20.0 20.0 20.0 20.0 40.0 20.0

9,00 20.0 20.0 20.0 20.0 20.0 20.0 20.0 ~o.o

METHOD: 9 3~~9,: . • 1 CA SE: 6385 REV~E\JE'R: ~-8,-~f-T'. I !IATE: 70/ ~4f F6

I : lsAMF'LE'. NUMBE_~~ 1 . .:: j ! : OW1Yci ...1...-~· t l ,

. i OKL~20~4 QKLS2/.21 • ,· 1

I i . 1 20.ci U i'.20,0 . u

1·!20.9. I; U .J 1 20.0"ll' U i ioo f, · · u · 1 oo I . u ; 20.q : U

u u u u u u u u u u u u

j 20.qi!i U .•120.0 :.·.f; u ' l O O I .1 : \ '1 u ·1

: ! ;g: ~ '! [ ~ I

U 20.0 u ! 20. 0 U 20.0 U :20.0 u 140.9

I I u u u u u u LJ

1j20,~,:-

H · .,i29.0 ·tjt U ,:!20.0' U U '20. 0 I U u 20.9 u U 20.0 U u u u u

20.0 I 20. o I ' u u : 20. 0, 20.d u u

,,

.20.0 U 20. o 1, U .20.0: l u 20, 0 :if U

100 I u 100 :, U

I

20.0 U 20,0f .)U

f!. 2 0 • 0 ·; : ' U .100 ·.·1./U

20 .o , .r u 'I

20.0 ·1 u 20.0: U 20. o 1

20.0 20.0 40,0 20.0 20,0 20.0 20.0 20.0 20.0 20,0 20.0 20,0 20.0

u u u u :;\ u

1! u :1 u ! ~ u

I

u JU

lJ .u u IJ

. I

PROJ3313

I I ,,

Ii !

A N ALYS I S T Y F· E :

TITLE! BLAYNEY AT HASTINGS LAB! IT : ' C• LE F' F: E F' : ___ - - - - AN ALY S T / on R Y : E 8 2

COMPOm!D

F'HENOL BISC2-CHLOROETHYL) ETHER 2-CHLOROF'HENOL 1,3 DICHLORDBENZENE 1,4 DICHLOROBENZENE BENZYL ALCOHOL 1,2 DICHLOROBENZEHE 2-METHY LF'HENOL B1S<2-CHLOROISOPROPYL)ETHER 4 - MET HY L F· HEN O L N-NITROSO-DIPROPYLAHINE HEXACHLOROETHANE NITRO BENZENE I SOF'HORONE 2-NITROF'HENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BISC2-CHLOROETHOXY> METHANE ~.4 DICHLOROPHENOL

,4-TRICHLOROBENZENE NHF'HTHALENE 4-CHLOROANILINE .HEXACHLORDBUTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCLOPENTADIENE 2,4,6-TRICHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2-CHLORONAPHTHALENE 2-NITRO(lNILINE DIMETHYLPHTHALATE ACENAPHTHYLENE 3-NITROANILINE A CE NA F'HTHENE 2,4-DINITROPHENOL 4 - N I T F: D F· HEN O L It I B E NZ D FU F: AN 2,4-DINITROTDLUENE

owS's •KLS201S

20.0 20.0 20. 0 20.0 :,,). 0

20.0 20.0 20.0 20.0 20.0 20. o· 20.0 20.0 20.0 20.0 :io.o

100 20.0 20.0 20.0 20.0 20.0 20.0 ;>O. 0 2•). 0 20.0

· 20. 0 1 OC• 20.0

100 ::?O. 0 :?.O. 0

100 2,.-,. 0

100 1-:)0

::?O. 0 ::o. 0

u u u u u u u u u u u u u u u u ll u u u u u u u u u u u u u u u u u LI LI u u

i i SEMIVOLATILES CF'hGE l> '1

I I I MATRIX! WATER I

ME"T HOt1: 9 3C<!M O 1. Gi)~: F; E 'JI E lJ s R ! _ Q--J] Q-" .J...C

I 7 - . ·SAMF·,E NUMBERS

. DWoc7 QKLS2016

I '

I I

i i . '

,100! 1 oo ;_ ,

1 100 1

I

100 I 100: · 100. I·

100 100 100 ,: I

u u u u u u u u u

I • I

''

I. 100 · . j i 100 . t I ·, u : ! I j

u I j •

I 100 I i · I· 100 i; :

u' : i u· 100 i. · 100 100 I 500; I 100 . 100 I

100 100 100

u· u u u u u u u u

100 ' U 100 U 100 U 1 oo l , : . u

l 100. ~ ! I U 500 : ~ · U 100:' U 500 1

100 I 100 : 500 : 100 50() 500 1 o,:-, l OC·

u u u u u u u u u

I

1

LIMITS: UG/L CASE: 6385. !tATE: 10/10/86

: 1

., '' ! ,·

PROJ3314

ti NA LY S I S T)' F' E :

TITLE: BLAYNEY AT HASTINGS L. ;:. I' : IT SAMPLE PREP: _______ ANALYST/ENTRY: E83

COMPOUND

2,6-DINITROTOLUENE DI ETHYLF'HTHALATE 4-CHLOROPHENYL PHENYL ETHER FLUORENE 4-NITROANILINE 4,6-DINITR0-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE PENT~CHLOROPHENOL PHENANTHRENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE PYREtlE BUTYL BENZYL PHTHALATE 3,3' D!CHLOROBENZIDINE BENZOCA)ANTHRACENE BISC2-ETHYLHEXYL)PHTHALATE r•i;:;YSENE

i-OCTYL PHTHALATE B~~ZOCB>FLU•RANTHENE BENZO<K>FLUORANTHENE BEt~ZO CA) PYF:ENE INDENOCl,2,3-CD)PYRENE DIBENZOCA,H>ANTHRACENE BENZOCG,H,I)PERYLENE

cn0S5 Ol<LS2O15

20.0 20.0 20.0 20.0

100 100 20.0 20.0 20.0

100 20.0 20.0 20.0 20.0 2 ,, • 'J 20,0 40,0 20.0 20.0 .'.;O, 0 20.0 20.0 20.0 20.0 20.0 20.0 20.0

u u u u u u u u u u u U. u· u u u u u u u u u u u u u u

SEMIVO~ATILES <PAGE 2)·; 1. 1: ! ,

METHODi 9302M01 · CASE: 6385 MATRIX: WATER ~ UNITS: UG/L

F:E 1JIE~~R:; -$ _Jr:- I1ATE: 10/10/86

i i SM\PLE NUMBERS CN~~, . . I aTT6 i\'1 !,

:100 U :100 I , u

j ! 1 0 0 I '.::i ; U

1100 I ', ii U 1 500 U 500, U

• 100 I U 100 U

,:100 ! U 500 l: 1 U i :·'

• I

I ! I ·:· ' I I I

!

i:

·1 ' .

, '.10 0 : ,!· U i i j I I ' j l ., ' ; 10 0 , I U ; 1( • !

: 100 ! : I; u : i, 100 ! : i u

I' ! 100 U

:•-

,, ·1f I -

1 r :1

;_ : ·

., ·, I I

· 100 · U 200 i U

,:100 : ' I . U , , I I ; ; . 1 1 oo I' 1 • u I 100 ·I i U 1300 ~- . '100 ' 100 100 100 100 100

u u u

! u I, ~

' i .. I ' ,. ' !: I :

' t

: : ! I • ; . .

I I

!

I .

!

I !

:

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.I l

I I . ! I . ;i I

.,

I: i I

I

, l

I I' ;

I \ I

!. I, I

I:

I

! 'j' .,

PROJ3315

,.

I! I

ANALYSIS TYPE: SEMIVOLATILES CF'AGE 1)

TITLE: H(1STINGS LAB! IT/WCT S~~PLE PREP: _______ ANALYST/ENTRY: ES9

COMF·QUND

F'HENDL BIS<2-CHLOROETHYL) ETHER 2 - CH L OR OF' HE NOL 1~3 DICHLOROBENZENE 1,4 DICHLOROBENZENE BENZYL ALCOHOL 1,2 DICHLOROBENZENE 2-METHYLF'HENOL BIS<2-CHLOROISOPROPYL>ETHER 4-MET HY LF'HENOL N-NITROSO-DIPROPYLAMINE HEXACHLOROETHANE NITROP.ENZENE ISOPHORONE 2-NITROPHENOL 2,4-DIMETHYLPHENOL BENZOIC ACID BISC2-CHLOROETHOXY) METHANE 2,4 DICHLOROPHENOL

~,4-TRICHLOROP.ENZENE " HTHALENE 4-CHLORDANILINE

-HEXACHLOROP.UTADIENE 4-CHLOR0-3-METHYLPHENOL 2-METHYLNAPHTHALENE HEXACHLOROCYCCOF'ENT At1 I ENE 2,4,6-TRICHLOROPHENOL 2,4,S-TRICHLOROPHENOL 2-CHLOR • NAPHTHALENE 2-NITROANILINE DIMETHYLPHTHALATE /'\ CE N AF· HT HYLE NE 3-NITROr1NILINE ACE NA F· HT HEN E ~ , 4 - D I N I T R O F· H E N O L 4 - N I T F: 0 F· HEN O L DI BENZOFUF:AI-~ 2,4-DINITROTOLUENE

Ml,TRIX: WATER~ METHOD: 9302H F:EVIEUER: 6f{,, - . -.tr

SAMPLE NUMBERS D~

I OKLS2018

i 20,0 u I 20.0 u

I 20,0 u 20.0 u 20,0 u

! 20.0 u 2 (). 0 u 20.0 u 20.0 u 20.0 u 20.0 u 20.0 u 20.0 u 20.0 u 20.0 u 2•J. 0 u

100 u 20.0 u 20.0 u 20.0 u 20.0 u 20.0 u 20.0 u 20,0 u 20.0 u 20,0 u 20.0 u

100 u 20.0 u

100 u 20.0 u 20.0 u

100 u 20.0 u

100 u 100 u :o.o u 20. 0 u

UNITS: UG/L CASE: 6385. t1 ATE : 1 0 I O 3 / 8 6

f PROJ3316

ANALYSIS TYPE: SEMIVOLATILES (PAGE 2)

- 1 l" LE : H A ST Hi G S .riB: IT/WCT A~PLE PREP: _______ ANALYST/ENTRY: E60

COMF·OUND

2,6-DINITROTOLUENE DI ETHYLF·HTH AL ATE 4-CHLOROPHENYL PHENYL ETHER FLUOF:ENE 4-NITROANILI!JE 4,6-DINITR0-2-METHYLPHENOL N-NITROSODIPHENYLAMINE 4-BROMOPHENYL PHENYL ETHER HEXACHLOROBENZENE PENTACHLOROPHENOL F·HENANTHF;ENE ANTHRACENE DI-N-BUTYLPHTHALATE FLUORANTHENE PYF:ENE BUTYL BENZYL PHTHALATE 3,3' DICHLDRDBENZIDINE BENZO<A>ANTHRACENE BIS<2-ETHYLHEXYL)PHTHALATE c:•t:•YSENE I -OCTYL PHTHALATE BENLOCB>FLUORANTHENE BENZOCK)FLUORANTHENE E( ENZ O < A ) PY F: E NE INDENOCl,2,3-CD)PYRENE DIBENZO<A,HlANTHRACENE BENZOCG,H,I>PERYLENE

MATRIX: WATER / METHOD: 9302M°b~ RE 1JIEWER ! t:f"i-.,_,,-'(·-1:r I SAMPLE NUMBERS I OS

- - ·•·- -- Q KL S 2 0 18

I

20.0 20.0 20.0 20.0

' l 00 I 1 oo t 20. 0

I

20.0 20.0

100 20. 0 20.0 20.0 20. 0 20.0 20.0 40.0 20.0 20,0 20.0 I 20 .o

i. 20.0 20.0 20,0 20,0 20.0 20.0

u u u u u u u u u u u u u u u u u u u ·u u u u u u u u

UNITS: UG/L CASE: 6385 . t1ATE ! 10/03/86

pROJ3317

ANr-iL YS IS TYF·E:

TITLE! HASTIMGS LAB: CSMRI s;1MF'LE F" REF' : _______ ANALYST /DIH:Y: E17

<Dtv4-..S Ot-:LS2013

COMF'OUND

ALUMINUM 200 u MIT IMONY 60.0 u AF:SENIC 10.0 u BAF:IUM 130 M BEF:YLL I UH s.oo u CAI1MI UH S. C•O u CALCIUM 100000. CHF:OM I UM 10, 0 u COBALT 50.0 u C OF'F'E R 2s.o u IRON 140 J LEAD s.oo u MAGNESIUM 15000. MANGANESE 15.0 u MERCURY 0.2 u NICKEL 40.0 u F· •TASSIUM 7900. SELENIUM s.oo u SILVER 10.0 u SODIUM 50000. THALLIUM 10.0 u

N/A l .AD!UM so.o u

.ZINC 20.0 u CYANIDE N/A I

TOTAL METALS <CONTRACTOR)

MATF:IX: WATER ~.·UH ITS: UG/l METHOD: 9001MO CASE: 6385 REVIEIJER: k(f_ --7' DATE! l 0/22/86

CW~tE NUMBERS

(9lu>5 QUJ5'~ QKLS2014

l :oo ; u I

60.0 u 10.0 u

1 '10 M s.oo u s.oo u

55000. 10,0 u 50.0 u 25.0 u 97.0 Ii 3.50 Ii

8800~ i .• !

15.0 '!' u I 0.2 u ' 40. 0 u 5500~

s.oo u 10.0 u

23000. 10.0 u

N/A l so.o u 35,0

NIA 1

ClKLS2015 '

: !

4000. 60.0 10.0

110 i s.oo s.oo

190000. 10.0 50.0 25.0

3400. I 6.50 29000 •

220 I

0 • 2 40.0

11000. s.oo

10.0 100000.

10.0 NIA

15,0 19.0

N/A

' ' . ' .. :

Ol<LS201t,

200 u 6·). 0 u 10.0 H 120 u 5.00 u s.oo

46000. u 10.0 u 50.0 u 25,0 J 120

5,60 I

7400. 15.0

u 0.2 u 40.0

4900. u s.oo u 10.0

20•:)00. u 10,0

I N/A H 11.0 H 15.0

l ~UA

PROJ3318

L' l! u M LI LI

u u u

I ,.,

u

u M u u

u

M M

u

I

I

ANALYSIS TYPE: TOTAL METALS (CONTRACTOR)

:-rTLE: H?1STINGS . r-1 B : CS MF: I ,AMPLE PREP: _______ ANALYST/ENTRY! E22

ALUMINUM ANTIMONY ARSENIC Br"iF:IUH 'EERYLLlUM C AI1M I UH CALCIUM CHROMIUM COBALT COF'F'ER IRON LEAD MAGNESIUM Mt1NGANESE MERCURY NICKEL POTASSIUM SELENIUM SI L'JEF: .-:--riruM

_LIUM Tlr'-1 1.,'ANADIUM ZINC CYANl!JE

COMPOUND

MAT F: IX : WAT E F: _/ U ~l ITS : UGI L METHOD! 9001M;~7/-\ft,.. CA:.E: 63f:5 · F: Et..' IE t.JE R: -&--(•\:.:kf-7- C!A TE! 10 /2 3 /8 6

I I

SAHF'LE NUM!,EF:S

__ J D<? QKLS2O18

I

j: 200 u I 6·:>. 0 u I

10.0 u .I 260

' ! 5. 00 u . l

5.00 u 990,:)0.

1 •:). 0 u

·I 50.0 u 25.0 u ,,

:I 100 ! • u -5. 00 :, · u

'1 15000. :I ,!

15.0 u ., '! 0. 2 u

\

40.0 u ': 7600.

5.70 u 10.0 u

.! 28000 • ! 10.0 u

N/A I ~.o. o u 17.0 M

N/A I

. ;

PROJ3319

nNALYSIS TYPE: TOTAL METALS (CONTRACTOR)

TITLE: HASTINGS LAB: CSMF:I SAMPLE PREP: _______ ANALYST/ENTRY: E17

MATRIX: WATER~ METHOD: 9001MO ~

REV I EWEFj: -4"..C. -+ U~HTS: UG/L CASE! 6385· Irr:TE! 10/22/86

E-AMF'LE NUMBERS r4r4

Ol<LS2021

I ,

I

COrffOUNit I •

ALUMINUM 200 u r1NT I t1CNY 60.0 u s!\F:SEN IC 10.0 u E:ARIUM 240 BEF<YLLIUH 5,00 u CAitM IUM 5.00 u CP1LCIUM 89000. CHROMIUM 10.0 u COBALT 50.0 u ' ...

COPPER 25.0 u ; I ! j I

J! i:, ,, •;1 • IRON 190 J r:: I .I

111 l l LEAD 1.00 M j" ( ! I

• I - : ,:· :!!

MAGNESIUM 13000. I ! i MANGANESE 7.00 H MERCURY 0,2 u i· NI Ct(EL 40,0 u POTASSIUM 71 0•:>, SELENIUM 5,00 u SILVER 10,0 u SODIUM 30000. .,. LIUM 10,0 u T J. I< M/A I 'Jr!\NAI:rIUM 50.0 u ZINC 20.0 u C'fANit1E NIA I

' I I l I; I .

fl

PROJ3320

TITLE! HASTINGS !...AB: CSMF;I

AN t'• L Y S I S TY F· E :

3AMPLE PREP: _______ ANALYST/ENTRY: E18

ALUMINUM ANTIMONY ARSENIC P.AF:IUM BERYLLIUM CADMIUM c;1LCIUM CHF:OM I UM COBALT COF'F'ER IRON LEAD MAGNESIUM MANGANESE MERCURY ~l l CKEL F'OTASSIUM SELENIUM SILVER SODIUM . ''\LLIUM

VANADIUM ZINC CYANIDE

COMF'OUND

ouxf.s QKLS2013

200 60.0

120 5,00 5,00

100000. 1 0 , 0 50.0 25.0

100 5.00

15000. 15,0 0.2

40,0 8600.

5,00 10,0

5000-0. 10.0

N/A 13,0 20,0

NIA

u u M M u u

u u u u u

u u

u

u u

u I

M u

I

I

It! SSOLl..1ED META;;:S C CONT ·ACTOF:)

MATRIX: WATER . UNITS: UG/L METHOD: 9001MO I CASE: 6385. REVIEWER: _G(.£$.---lf. DATE: 1':)/22/86

200 U 60, 0 · · U 10,0 I U

11 ~0 M 5,00 U 5,00 U

54000, 10,0 U 50.0 U 25. o I ; u

100 '"U

200 60.0 10.0

' 60.0 5.00 5,00

200000. .10.0 50. O • 25.0

u u u

! H u u

u u

·u

DvJYd OKLS2016

200 60,0 lC•,O

120 5,00 5. 0·)

45000. 10.0 50,0 25.0

u u u M u u

u u u L1

5,00 1: u 1 " 0

1.20 I J

M 100

2,90 ;M 8900. j. ·,

15.0 1 ·u ~ : u 0.... '

40. 0 i U 4900, . M

5.00 ., U I

, 10,0 I· U 22000,

10.0 U N/A I

50,0 U 20.0

N/A I

i I I!

28000 • . 170

0.2 U 40.0 U

11000. I

s.oo u 10.0 U

98000. 10.0 U

H/A I 50,0 U

9,00 M N/A I

PROJ3321

7400. 15,0 .0,2 40,0

4700, 5,00

10,0

10.0 N/A

50.0 20,0

N/A

u u

u M u u

u I

u u

I

ANALYSIS TYPE: DISSOLVED METALS (CONTRACTOR)

"ITLE: H,~1STINGS _A~: CSMRI :::; M~ F· LE F' RE P : _ _ _ _ _ _ _ A N AL Y S T /ENT F: Y : E 2 3

COMPOUND

ALUMHlUM ANTIMONY ARSENIC BAF:IUM :E:EF:YLL I UM CADMIUM CALCIUM CHROMIUM COBALT COF"F'ER IRON LEAD MAGNESIUM MANGANESE MERCURY ~II Cr~EL F'OTASSlUM SELENIUM SILVER SODIUM

'.LIUM

VANADIUM ZINC CYANIDE

MATF:rx: WATER ~ METHOD: 9001M F:E V 1 E IJE R : #1 - -i

I

j SAf'LE MUMBEF:S

_ QKLt601s

200 u 60.0 u 10.0 u

270 5.00 u 5.00 u

100000. 10.0 u

l 50. 0 ; ! 1 u 25.0 I• u

100 I u ii i i

i I . i

5.00 u : I

15000. 15.0 u [

, .. 0,2 u i

40.0 u 7700.

6,10 u 10.0 u

2SOOQ. 10.0 u

N/A l 50,0 u 20,0

I H/A I

'ii ..

'

UNITS: UG/L CASE: 6385 . D,;TE: 10/23/86

fl PROJ3322

TITLF.: HASTINGS '..Al): CSMF:I

Ml AL Y S I S TY F· E :

;~MPLE PREP: _______ ANALYST/ENTRY: E18

SAM!=·LE

QKcfft;{ COMPOUNt1

(~LUM I HUM 200 u AiHIMONY 60.0 u AF:SEHI C 10.0 u B1~RIUM 240 BERYLLIUM 5.00 u CADMIUM 5. c,,::, u CALCIUM 90000. CHROMIUM 10.0 u COBALT 50.0 u COF·F·ER 25.0 u IRON 100 u LEAD 5.00 u MAGNESIUM 13000. MANGANESE 15.0 u MERCURY 0.2 u NICKEL 40.0 u POTASSIUM 7300. SELENIUM 5.00 u SILVER 10.0 u

-. I UM 30000 • . ~LIUM 10.0 u

iIN NIA I VANADIUM 50.0 u ZINC 20.0 u CYANIDE N/A I

DISSOLVED METALS (CONTRACTOR>

MATRIX! IJATER ~-. UNITS: UG/L METHOD: 900 MC1 CASE: 6385. RE'v'l EWER: ~- ---7:.. I !tAT E ! 10 /22/ 86

NUMBERS

I -I· !

'. I I

; I

PROJ3323

,_;;.;::;E N1_J: 24631~ CONTRACT NO: s~s ~MO t!': 2463G-5, -7, -~, -11 TQ ~'.() SITE: BLAYNEY AT H,c:.:.:,fIHG'.:J

EPA SAMPLE

wls Qf:LS2007

-.>l4 m:Ls:::,:i,:,2

...,.; 3.s C!f: L5:20r)·~ L..>3d m<LS2010

))~ Ql<L.S2011

)W:l-ol m-:L.S2012

.J> 4S QKLS2013

w..>4d QKL.S2014

_,v S-...$ m::LS2015 ,~ ~- \ QKLS2016

P'6 Ql<LS'.2018

't.¥1. m<LS2021

NO.

At·H'tl. YT I Cr-";L

CHLOF:IDE MG/LAS Cl-

22. 4,J

17.7J

26.7J 47,J

3(>. 3,J

t 7. 1J

94.2J

15.6J

77.6J

9.4J

28,J

30.3J

LABLlRATOFV: ACCULA~S M!::'.THOD MU::;~ ~.:-1 '). 1 , 3'..25. :2, 7.7'.:,. 4 Er~·A #: C!l<LS2 ~ 1'1;:. ff~! X: ~•!.~ TEF; - tJ'

~~' RCSULTS i

SULFATE Ml:/L AS SIJ4=

34 60

\ 58'

38

41

,. 213

26

38

! AU~ALINIT'r'

MG/LAS Ca.CO3 I

~17 I

!19::

19:2

281

437

151

26(•

26(i

I I I '

' I

PROJ3324

APPENDIX C

DECEMBER 1986 GROUND WATER DATA

PROJ3325


'LE: HASTINGS HATRIX! WATER ~ UNITS! UG/L • AOUATECH METHOD: 9302MO 1 :r._ CASE: 6696 L-. ~.

SAMPLE PREP: _______ ANALYST/ENTRY: E73 REVIEWER: ~2-- _ D~TE: 01/27/87

SAMF"LE NUMBERS · I.49 D8 cm5 S35-kn-i cwls

J09S2009 J09S2010 J09S2011 J09S2012 COMPOUND

CHLOROMETHANE 1.00 H 20.0 u 10.0 u 10.0 u BROMOMETHANE 10.0 u 20.0 u 10.0 u 10.0 u VINYL CHLORIDE 10.0 u 20.0 u 10.0 u 10.0 u CHLOROETHANE 10.0 u 20.0 u 10.0 u 10.0 u METHYLENE CHLORIDE s.00 u 10.0 u s.oo u s.oo u ACETONE 10.0 u 20.0 u 10.0 u 10.0 u CARBON DISULFIDE s.oo u 10.0 u s.oo u s.oo u 1, 1 ItICHLOROETHENE 1.00 H 10.0 u s.oo u s.oo u 1, 1 DICHLOROETHANE s.oo u 10.0 u s.oo u s.oo u TRANS-1,2,-DICHLOROETHENE. s.oo u 18.0 s.oo u 1.00 H CHLOROFORM 1.00 H 10.0 u s.oo u s.oo u 1,2,DICHLOROETHANE s.oo u 10.0 u s.oo u 4,00 11 2-BUTANONE 10.0 u 20.0 u I 10.0 u 1,1,1 TRICHLOROETHANE 4.00 H 10.0 u s.oo u s.oo u CARBON TETRACHLORIDE 41.0 10.0 u s.oo u s.oo u VINYL ACETATE 10.0 u 20.0 u 10.0 u 10.0 u BROMODICHLOROMETHANE s.oo u 10.0 u s.oo u s.oo u 1 ,1,2,2,-TETRACHLOROETHANE s.oo u 10.0 u s.oo u s.oo u

2-DICHLOROPROPANE s.oo u 10.0 u s.oo u s.oo u TRANS-1,3-DICHLOROPROPENE s.oo u 10.0 u s.oo u s.oo u TRICHLOROETHENE 45.0 330 s.oo u 71.0 DIBROMOCHLOROMETHANE s.oo u 10.0 u s.oo u s.oo u 1,1,2-TRICHLOROETHANE s.oo u 10.0 u s.oo u s.oo u BENZENE s.oo u 10.0 u s.oo u. s.oo u CIS-1,3-DICHLOROPROPENE s.oo u 10.0 u s.oo u s.oo u 2-CHLOROETHYL VINYL ETHER 10.0 u 20.0 u 10.0 u 10.0 u BROMOFORH s.oo u 10.0 u s.oo u s.oo u 2-HEXANONE 10.0 u 20.0 u 10.0 u 10.0 u 4-METHYL-2-PENTANONE 10.0 u 20.0 u 10.0 u 10.0 u TETRACHLOROETHENE 2.00 t1 2.00 H s.oo u s.oo u TOLUENE s.oo u 10.0 u s.oo u s.oo u CHLOROBENZENE s.oo u 10.0 u s.oo u s.oo u ETHYL BENZENE s.oo u 10.0 u· s.oo u s.oo u STYRENE s.oo u 10.0 u s.oo u s.oo u TOTAL XYLENES s.oo u lO.O u s.oo u s.oo u

~

PROJ3326


-r-"Tt.E: HASTINGS HATRIXl W~TER i_ UNITS: UG/L AQUATECH METHOD: 9302HO CASE: 6696

SAMPLE PREP: _______ ANALYST/ENTRY: E73 REVIEWER: W-- __ !:,:_ D~TE: 01/27/87

SAMPLE NUMBERS CWld OW$d cv,J4 S C .-~d

J09S2013 J0952017 J0952018 J0952019 COMPOUND

CHLOROMETHANE 10.0 u 10.0 u 200 u 10.0 u BROHOHETHANE 10.0 u 10.0 u 200 u 10.0 u VINYL CHLORIDE 10.0 u 10.0 u 200 u 10.0 u CHLOROETHANE 10,0 u 10.0 u 200 u 10.0 u METHYLENE CHLORIDE s.oo u s.oo u 100 u s.oo u ACETONE 10.0 u 10,0 u 200 u 10,0 u CARBON DISULFIDE S,00 u s.oo u 100 u s.oo u 1,1 DICHLOROETHENE S,00 u S,00 u 100 u s.oo u 1,1 DICHLOROETHANE s.oo u 5,00 u 100 u s.oo u TRANS-1,2,-DICHLOROETHENE 5,00 u s.oo u 40.0 H s.oo u CHLOROFORM S,00 u s.oo u 100 u s.oo u 1,2,DICHLOROETHANE s.oo u s.oo u 100 u s.oo u 2-BUTANONE 10.0 u I 200 u I 1,1,1 TRICHLOROETHANE s.oo u s.oo u 66.0 H s.oo u CARBON TETRACHLORIDE 5.00 u 9.00 100 u s. 00 u VlNYL ACETATE 10.0 u 10.0 u 200 u 10.0 u BROHODICHLOROMETHANE S,00 u 5,00 u 100 u 5,00 u 1,1,2,2,-TETRACHLOROETHANE s.oo u 5,00 u 100 u ·s.oo u

,_DICHLOROPROPANE s.oo u s.oo u 100 u 5,00 u , .. ANS-1, 3-DI CHLOROF'ROPENE s.oo u 5.00 u 100 u s.oo u TRICHLOROETHENE 17,0 66,0 2600, 190 DIBROHOCHLOROHETHANE s.oo u s.oo u 100 u s.oo u 1,1,2-TRICHLOROETHANE 5,00 u s.oo u 100 u s.oo u BENZENE 5,00 u 5,00 u 100 u s.oo u CIS-1,3-DICHLOROPROPENE s.oo u 5.00 u 100 u s.oo u 2-CHLOROETHYL VINYL ETHER 10,0 u 10.0 u 200 u 10.0 u 'BROMOFORH S,00 u s.oo u 100 u s.oo u 2-HEXANONE 10.0 u 10.0 u 200 u 10.0 u 4-HETHYL-2-PENTANONE 10.0 u 10.0 u 200 u 10,0 u TETRACHLOROETHENE S,00 u s.oo u 36.0 H 2.00 H TOLUENE s.oo u s.oo u 100 u S,00 u CHLOROBENZENE s.oo u s.oo u 100 u s.oo u ETHYL BENZENE s.oo u s.oo u 100 u s.oo u STYRENE 5.00 u s.oo u 100 u s.oo u TOTAL XYLENES s.oo u s.oo u 100 u 5,00 u

PROJ3327


_E: HASTINGS LAo: AQUATECH SAMPLE PREP: _______ ANALYST/ENTRY: E74

COMPOUND

CHLOROMETHANE BROHOMETHANE VINYL CHLORIDE CHLOROETHANE METHYLENE CHLORIDE ACETONE CARBON DISULFIDE 1,1 DICHLOROETHENE 1,1 DICHLOROETHANE TRANS-1,2,-DICHLOROETHENE CHLOROFORM 1,2,DICHLOROETHANE 2-BUTANONE 1,1,1 TRICHLOROETHANE CARBON TETRACHLORIDE VINYL ACETATE BROMODICHLOROMETHANE

1 ,2,2,-TETRACHLOROETHANE ~-DICHLDROPROPANE

TRANS-1,3-DICHLOROPROPENE TRICHLOROETHENE DIBROMOCHLOROMETHANE 1,1,2-TRICHLDROETHANE BENZENE CIS-1,J-DICHLOROPROF'ENE 2-CHLOROETHYL VINYL ETHER BROMOFORM 2-HEXANONE 4-METHYL-2-PENTANONE TETRACHLOROETHENE TOLUENE CHLOROBENZENE ETHYL BENZENE STYRENE TOTAL XYLENES

CwS~ J09S2020

10.0 10.0 10.0 10.0 s.oo

10.0 s.oo 2.00 s.oo s.oo s.oo s.oo

10.0 17.0 s.oo

10.0 s.oo s.oo s.oo s.oo

770 s.oo s.oo s.oo s.oo

10.0 s.oo

10.0 10.0 19.0 s.oo s.oo s.oo s.oo s.oo

u u u u u u u H u u u u u

u u u u u u

u u u u u u u u

u u u u u

MATRIX! WATER METHOD: 9302M01J L REVIEWER: _/;fS_'§;;! __ ~~

SAMPLE NUMBERS .

UNITS: UG/L CASE: 6696 D~TE: 01/27/87

ow Sc.\ f'."1~1<".\ l3 \c, ,•, I< J09S2021 J09S2028F

10.0 10.0 10.0 10.0 s.oo

10.0 s.oo s.oo s.oo s.oo s.oo s.oo

10.0 s.oo s.oo



10.0 s.oo

10.0 10.0 s.oo s.oo s.oo s.oo s.oo s.oo

u u u u u u u u u u u u u u u u u u u u


10.0 l.O.O 10.0 10.0

1.00 92.0 s.oo s.oo s.oo s.oo 5.00 s.oo

s.oo s.oo

10.0 s.oo s.oo s.oo s.oo s.oo s.oo s.oo s.oo s.oo

10.0 s.oo

10.0 10.0 s.oo s.oo s.oo s.oo s.oo s.oo

u u u u M

u u u u u u

I u u u u u u u u u u u u u u u u u u u u u u

PROJ3328

ANALYSIS TYPE: VOLATILES BY 601 l 602

1 ..i., LE: HASTINGS LAB: AOUATECH SAMPLE PREP: _______ ANALYST/ENTRY: E72

COMPOUND

BtNZENE BROHODICHLOROMETHANE BROHOFORH BROMOMETHANE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYL VINYL ETHER CHLOROFORM CHLOROMETHANE DIROHOCHLOROMETHANE 1,2-DICHLOROBENZENE 1,3-DICHLOROBENZENE 1,4-DICHLOROBENZENE 1,1-DICHLOROETHANE 1,2-DICHLOROETHANE

1-DICHLORDETHENE 3-1,2-DICHLOROETHENE

TRANS-1,2-DICHLOROETHENE 1,2-DICHLOROPROPANE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE ETHYLBENZENE METHYLENE CHLORIDE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,1,1-TRICHLOROETHANE 1,1,2-TRICHLOROETHANE TRlCHLOF:OETHENE TRICHLOROFLUOROHETHANE VINYL CHLORIDE

C.M5 5)·~tCi·-, J09S2011

0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1

u u u u u u u u u u u u u u u u u u u u u u u

u u u u u u u u u

MATRIX: W(\TER f METHOD! 6011WOO RcVIEWER: .Jci:,,.5.. __ !,_

SAMPLE NUMBERS ·

UNITS! UG/L CASE! 2597G Df'\TE: 01/27/87

o.,~/ :c.c.-ic J0952011D

cw Z.:, .J09S2014

G'.-,:2.d J095201S

0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1

u u u u u u u u u u u. u u u u u u u u u u u u

u u u u u u u

u

0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0.1 1.,0 0.1 0.1


u u u u u u

u u

PROJ3329

0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 o.3 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0.1 :L20 0.1 0.1

u u u u u u u u u u u u u u u u u u

u u u u

u u u u u u

u u

ANALYSIS TYPE: VOLATILES BY 601 l 602

TI1LE: HASTINGS MATRIX: WATER 4 UNITS: UG/L LAB: AQUATECH METHOD: 6011WO CASE: 2597G SAMPLE PREP: _______ ANALYST/ENTRY! E72 REVIEWER: _6c{J ____ _7_ D~TE! 01/27/87

SAMPLE NUMBERS owJs M-, M-11 M-1s

J09S2016 J09S2023 J09S2024 J09S202S COMPOUND

BENZENE 0.1 u 0.1 u 0.1 u 0.1 u BROMDDICHLDROMETHANE 0.1 u 0.1 u 0.1 u 0.1 u BROHOFORM 0.1 u 0.1 u 0.1 u 0.1 u BROMDHETHANE 0.1 u 0.1 u 0.1 u 0.1 u CA~BON TETRACHLORIDE 0.1 u 0.1 u 0.1 u 0.1 u CHLOROBENZENE 0.1 u 0.1 u 0.1 u 0.1 u CHLOROETHANE 0. 1 u 0.1 u 0.1 u 0.1 u 2-CHLOROETHYL VINYL ETHER 0.1 u 0.1 u 0.1 u 0.1 u CHLOROFORM 0.1 u 0.1 u 0.1 u 0.1 u CHLOROMETHANE 0.1 u 0.1 u 0.1 u 0.1 u DIROMOCHLOROMETHANE 0.1 u 0.1 u 0.1 u 0.1 u 1,2-DICHLOROBENZENE 0.1 u 0.1 u 0.1 u 0.1 u 1,3-DICHLOROBENZENE 0.1 u 0.1 u 0.1 u 0.1 u 1,4-DICHLOROBENZENE 0.1 u 0.1 u 0.1 u 0.1 u 1,1-DICHLQROETHANE 0.1 u 0.1 u 0.1 u 0. 1 u 1,2-D!CHLOROETHANE 0.1 u 0.1 u 0.1 u 0.1 u

. -r1 I CHLOROETHENE 0.1 u 0.1 u 0.1 u 0.1 u ~ ~-1,2-DICHLOROETHENE 0.1 u 0.1 u 0.1 u 0.1 u TRANS-1,2-DICHLOROETHENE 0,1 u 0.1 u 0.1 u 0.1 u 1,2-DICHLOROPROPANE 0,1 u 0.1 u 0.1 u 0.1 u CIS-1,3-DICHLOROPROPENE 0.1 u 0.1 u 0.1 u 0.1 u TRANS-1,3-DICHLOROPROPENE 0.1 u 0.1 u 0.1 u 0.1 u ETHYLBENZENE 0.1 u 0.1 u 0.1 u 0.1 u METHYLENE CHLORIDE 1,00 u 1.00 u 1.00 u 1.00 u 1,1,2,2-TETRACHLOROETHANE 0.1 u 0,1 u 0,1 u 0,1 u TETRACHLOROETHENE 0,1 u 0,1 u 0,1 u 0.1 u TOLUENE 0.1 u 0.1 u 0,1 u 0,1 u 1,1,1-TRICHLOROETHANE o.4 0,1 u 0.1 u 0,4 1,1,2-TRICHLOROETHANE 0.1 u 0.1 u 0.1 u 0.1 u TRICHLOROETHENE 4.50 o.s 0.1 u 0.3 TRICHLOROFLUOROHETHANE 0.1 u 0.1 u 0.1 u 0.1 u VINYL CHLORIDE 0, 1· u 0.1 u 0.1 u 0.1 u

PROJ3330

ANALYSIS TYPE: VOLATILES BY 601 I 602

TLL. .iASTI NGS B: AOUATECH iPLE PREP: _______ ANALYST/ENTRY: E72

COMPOUND

NZENE .:OMODICHLOROMETHANE ROMOFORH

OMOMETHANE ,RBON TETRACHLORIDE

HLOROBENZENE YLOROETHANE

CHLOROETHYL VINYL ETHER riLOROFORM HLDROHETHANE

ROMOCHLOROMETHANE 2-DICHLDRDBENZENE

,3-DICHLORDBENZENE ·4-DICHLOROBENZENE

1-DICHLOROETHANE ,2-DICHLDRDETHANE ,1-nICHLOROETHENE

£ !-DICHLOROETHENE :ANb-1,2-DICHLOROETHENE ,2-DICHLOROPROPANE ·s-1,3-DICHLOROPROPENE :ANS-1,3-DICHLOROPROPENE t'HYLBENZENE ETHYLENE CHLORIDE

1,2,2-TETRACHLOROETHANE ...:TRACHLOROETHENE OLUENE

1,1-TRICHLOROETHANE 1,2-TRICHLOROETHANE

RICHLDRDETHENE RICHLOROFLUDROMETHANE

NYL CHLORII•E

f-",e. \c\ e, \ ·,, K"

J09S2027F

0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0.1 0,1 0,1 0,1


u u u u u u u u u

MATRIX: WtaTER METHOD: 601JWJ~,/, REVIEWER: ....trfJ>_-y:.._!r__

SAMPLE NUMBERS

UNITS: UG/L CASE: 2597G D~.TE: 01/27/87

r-c-'. .. -i ,~~·~-~ ~~?_1\:._:~~·.·p<. J09S2028F J69S2100

-t1·,_ ' ;. :_ ,;_•· .- . -r~~ J09S2101

0.1 (),1 0.1 0.1 0.1 0.1 0.1 0,1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1


u u u u u u u u u

0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0,1 0,1 0,1 0.1 0 .1 0,1 1.00 0.1 0.1 0.1 0.1 0.1 0.1 0,1 0.1


u u u u u u u u u

0.1 0.1 0,1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0,1 0.1 0.1 0.1 0.1 0,1 0.1 0.1 0.1 0.1 0.1 0.1 1.00 0.1 0.1 0.1 0.1 0,1 0.4 0,1 0.1

PROJ3331


u u u u u u

u u

ANALYSIS TYPE: VOLATILES BY 601 I 602

~ E: HASTINGS L, AQUATECH SAMPLE PREP: _______ ANALYST/ENTRY: E72

HATRIX: WATER METHOD: 6011WO~./ RtVIEWER: ~-~-7-

COHF'OUND

BENZENE BROMODICHLOROMETHANE BROMOFORM BF:OMOMETHANE CARBON TETRACHLORIDE CHLOROBENZENE CHLOROETHANE 2-CHLOROETHYL VINYL ETHER CHLOROFORM CHLOROMETHANE DIROMDCHLOROHETHANE 1,2-DICHLORDBENZENE 1,3-DICHLDROBENZENE 1,4-DICHLOROBENZENE 1,1-DICHLORDETHANE 1,2-DICHLDRDETHANE

•-DICHLORDETHENE -1,2-D!CHLOROETHENE

TRANS-1,2-D!CHLOROETHENE 1,2-DICHLDROPRDPANE CIS-1,3-DICHLOROPROPENE TRANS-1,3-DICHLOROPROPENE ETHYL BENZENE METHYLENE CHLORIDE 1,1,2,2-TETRACHLOROETHANE TETRACHLOROETHENE TOLUENE 1,1,1-TRICHLOROETHANE 1,1,2-TR!CHLOROETHANE TRICHLOROETHENE TRICHLOROFLUOROHETHANE VINYL CHLORIDE

SAHPLE NUMBERS /Yl - /1)

J09S2102

0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0. 1 . u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 0.1 u 1.00 u 0.1 u 0.1 u 0.1 u 0.3 0.1 u 1.40 0.1 u 0.1 u

UNITS: UG/L CASE: 2597G D(\TE: 01/27/87

PROJ3332

•

TITLE: HASTINGS LAB: AQUATECH INC. ANALYST/ENTRY: LT

MATRLX: !·WATER ME"FHOD :.·. 6011 WOO F(p.;U.El.ilER f. GCS {(- <;

UNITS: UG/L ,......__lJASE: SAS2~97G 't<)-~;ATE: 1-27-87

ANALYSIS TYPE= ETHYLENE DIBROMIDE

SAMPLE NO. COt'-IC.

J09S2009 6.2 J09S2010 0.1U J09S2011 O.lU

J09S2014 O. lU J09S2015 0.1U

J09S2028F o.1u

PROJ3333

1

ERRATA

This Page Was Intentionally Left Blank Due to an Errata, in Numbering.

PROJ3334

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