GNN3 - D. Mancini, USA

8/14/2019 GNN3 - D. Mancini, USA

1/30

DOE NSRCs, GNN 2005, May 26thPioneeringScience andTechnology

Office of ScienceU.S. Department

of Energy

Department of EnergysDepartment of Energys

User Facilities forUser Facilities for

NanoscienceNanoscienceandandNanotechnologyNanotechnology

Derrick C. ManciniProject Manager and Nanofabrication Group Leader

Center for Nanoscale Materials

Argonne National Laboratory

http://nano.anl.gov

Global Nanotechnology NetworkMay 26, 2005, Saarbrucken, Germany


2/30



of Energy

DOE BES Initiative forDOE BES Initiative forNanoScienceNanoScience&&

Technology:Technology:NanoscaleNanoscaleScience Research CentersScience Research Centers

DOEs 5 NSRCs - http://www.sc.doe.gov/bes/NNI.htm

Center for Nanophase Materials Sciences (ORNL)

Molecular Foundry (LBNL)

Center for Functional Nanomaterials (BNL)

Center for Integrated Nanotechnologies (SNL-LANL)

Center for Nanoscale Materials (ANL)

QuickTime and aTIFF (Uncompressed) decompressor

are needed to see this picture.




3/30



of Energy

DOE BES Initiative forDOE BES Initiative forNanoScienceNanoScience&&

Technology:Technology:NanoscaleNanoscaleScience Research CentersScience Research Centers

DOEs 5 NSRCs Each is a National User Facility

Located at existing DOE National Laboratories Integrated with existing DOE National Facilities

Provides a regional resource East Coast (Brookhaven National Lab)

West Coast (Lawrence Berkeley National Lab)

Southwest (Sandia & Los Alamos National Labs)

South Central (Oak Ridge National Lab)

North Central (Argonne National Lab)

Scientific Research Mission - Themes

$18.5 M in DOE operating funds for each NSRC


4/30



of Energy

Center forCenter forNanophaseNanophaseMaterials SciencesMaterials Sciences

A collaborative nanoscience userresearch facility at Oak Ridge National

Laboratory in Tennessee for thesynthesis, characterization, modeling,simulation, and design of nanoscalematerials.

QuickTime and a

TIFF (Uncompressed) decompressorare needed to see this picture.

Integrated with:Spallation Neutron SourceHigh Flux Isotope ReactorMaterials Analysis User Center

Building completed in spring 2005.

http://www.cnms.ornl.gov/


5/30



of Energy

Molecular FoundryMolecular Foundry

World-class user facility atLawrence Berkeley NationalLaboratory in California for thedesign, synthesis, and

characterization of nanoscalematerials.

Integrated with:Advanced Light SourceNational Center for ElectronMicroscopyNational Energy Research ScientificComputing Center

Building to be completed inspring 2006.

http://foundry.lbl.gov/




6/30



of Energy

Center for IntegratedCenter for IntegratedNanoTechnologiesNanoTechnologies

World-class research facilities atSandia and Los Alamos NationalLaboratories in New Mexico fordeveloping the scientific principles

that govern the design,performance, and integration ofnanoscale materials.

Integrated with:

Integrated Materials Research LabLos Alamos Neutron Science CenterNational High Magnetic Field LabCompound Semicon Research LabMicroelectronics Development Lab

Building to be completed in fall2005.

http://cint.lanl.gov/






7/30



of Energy

Center for FunctionalCenter for FunctionalNanomaterialsNanomaterials

World class facility atBrookhaven National Laboratoryin New York for atomic leveltailoring of a material's response

to achieve a specific functionality.

Integrated with:National Synchrotron Light SourceLaser Electron Accelerator Facility

Building to be completed inspring 2007.

http://www.cfn.bnl.gov/




8/30



of Energy

Center for Nanoscale MaterialsCenter for Nanoscale Materials

World-class research facility atArgonne National Laboratory inIllinois for tackling the grand

challenges of nanoscience.

Unique $72M partnershipUnique $72M partnership

$36 M DOE funds $36 M State-of-Illinois funds Building to be completed inspring 2006 $18.5 M DOE operations fundsin FY 2007

http://nano.anl.gov/


9/30



of Energy

Argonnes Facilities forArgonnes Facilities forNanoscienceNanoscience

The Electron Microscopy Center

at Argonne National Laboratory Jazz Teraflop Cluster

Center for Nanoscale Materials

Electron MicroscopyCenter

One-stopUser access

to all ANLfacilities


10/30



of Energy

Center forCenter forNanoscaleNanoscaleMaterials MissionMaterials Mission

Enable world-class nanoscience aligned with theDepartment of Energys scientific vision.

Explore novel phenomena associated with the interplay between

spatial, physical and chemical length scales and proximity effects.

Transform the art of nanomaterial and nanodevice fabrication intoa science.

Understand the ultimate limits of miniaturization.

Lay foundations for new technologies based on the principles ofnanoscience.

Support users in doing outstanding science in a safeenvironment, by providing expertise and facilities to thenanoscience community.


11/30



of Energy

CNMs User ProgramCNMs User Program

Open access for all users. Best science via peer-reviewed proposals (http://nano.anl.gov)

Capabilities and facility shaped by CNM science.

Foster interactions across wide range of disciplines andprofessions.

Two phases

Early Access Provide users access to existing ANL nanoscience capabilities.

1st and 2nd Call for Proposals completed for time in 2004-2005

3rd Call for Proposals, July 15th deadline

New Facilities New building (funded by State of Illinois), to be constructed adjacent to the

Advanced Photon Source. Construction start in June. New equipment and Nanoprobe beamline (funded by DOE Nanoscale

Science Research Centers program).


12/30



of Energy

Opportunities at the CNM

User program. Individuals or group access to existing scientific

capabilities/equipment in CNM.

Rapid access. One-stop User access to all facilities at Argonne (APS,

IPNS, EMC, advanced computing).

CNMs world-class staff.

Leverage large complement of advanced tools fornanoscience and nanotechnology.

Joint initiatives including workshops and funding.

Workforce training.

Working on new model for IP and tech transfer. includes joint activities.

proprietary research at CNM (cost recovery fee).


13/30



of Energy

CNM Scientific ThemesCNM Scientific Themes

Novel functional

nanocomposites

Sub-wavelength photon confinement/propagation

Bio-inorganic interface (D. Tiede, T. Rajh, M. Firestone) Nanocarbon (D. Gruen, J. Carlisle) Nanomagnetism (S. Bader, A. Hoffmann) Complex oxides (O. Auciello, S. Streiffer)

Nanophotonics (G. Wiederrecht, S. Gray) Virtual Fab Lab (S. Gray, P. Zapol)

Nanopatterning (D. Mancini, L. Ocola) X-Ray Nanoprobe (J. Maser, B. Stephenson)

Self-assembled

functionalized arrays


14/30



of Energy

Bio-inspired/biomimetic materials andprocessesNanostructured 2D and 3D catalysis/photocatalysis; lightharvesting, sensing and energy transduction; Protein-basedmaterials for storage and transduction; Novel bio-inorganiccomposites; biomimetic; hydrogen production, storage and

conversion.

Hydrogen Fuel Initiative (DOEs BES)

Nanoscale catalysis designInorganic scaffolding for catalytic sites, eg., AAO membranes;Nanoscale phenomena size, shape and curvature effects

Nanostructured materials by design for

energy efficiencyUltra-strong magnets for efficient motors.Nanophotonics for > Tbps bandwidth.Nanocrystalline diamond for low-friction coatings.

Theory and Modeling.

NanomaterialsNanomaterialsfor Energy at Argonnefor Energy at Argonne

biomimetic H-production

Ultra-strong nanomagnet compositesmagnetic field

magnetization

coercivity,(Hc)

remanence(Mr)

saturation,(MS)

Co/CoPt core-shellnanoparticle array

Anodized Aluminum OxideM. Pellin, et al.

inorganic membranes


15/30



of Energy

Combined SEM/SPME-beam Lithography

Key Fabrication and Characterization ToolsKey Fabrication and Characterization Tools

LEO 1560XB CrossBeam

FIB/SEMPlasma-enhanced CVD for Carbon

The Center forThe Center for NanoscaleNanoscale MaterialsMaterials


16/30



of Energy

The Center forThe Center forNanoscaleNanoscaleMaterialsMaterials

Hard XHard X--rayrayNanoprobeNanoprobeat the APSat the APS

Unique instrument to study individual nanostructures30 nanometer spatial resolution or betterQuantitative structure, strain, magnetizationSensitive trace element and chemical state analysis

Ability to penetrate overlayers, environments, fields

Example of XExample of X ray Fluorescence Imaging at theray Fluorescence Imaging at the


17/30



of Energy

Example of XExample of X--ray Fluorescence Imaging at theray Fluorescence Imaging at the

APS: TiOAPS: TiO22--DNADNA NanocompositesNanocompositesin Cellsin Cells

TiO2-DNA Nanoparticlesfor in vivoGene Surgery

DNA-nanoparticlecrossing cell wall

X-ray elementalimaging of the cell

chromosomeshowing location ofthe single stranded

DNA-TiO2nanoparticle

Map Ti distribution usingXRF, to quantify the successof transfection and visualize

target of nanocomposite Affinity of transfected DNA

for ribosomes causeslocalization to the nucleolus.

CNMs Hard X-rayNanoprobe, at 30 nmresolution, will significantlyimproving applicability to cell

biology.

G. Woloschak, Nature Materials 2,

343 (2003). (Northwestern/ANL

collaboration)


18/30



of Energy

Advanced Photon SourceAdvanced Photon Source


19/30



of Energy

Advanced Photon SourceAdvanced Photon Source


20/30



of Energy

Adjacent to APS Sector 26Integrated with APS site design

Utilize APS site utilities

Center forCenter forNanoscaleNanoscaleMaterials BuildingMaterials Building


21/30



of Energy


~85,000 gross square feet, including:13,000 sq ft Laboratories

11,000 sq ft Cleanroom Facilities

33,000 sq ft Offices & Public Spaces


22/30



of Energy

CNM building complete in Spring 06 CNM Facility complete in Fall 07 85,000 sq. ft. lab + office space



23/30



of Energy

The Challenge: Enabling AccessThe Challenge: Enabling Access

Coordinated Access

Distributed Access Remote Access

Interactive Access

Telepresence

Telecollaboratory


24/30



of Energy

TelepresenceTelepresence&& TelecollaboratoryTelecollaboratory

Platform Independent

Intuitive User Interface Responsive to the User

Adaptable to Many Instruments

Provides user what they need to

execute their experiments


25/30



of Energy



26/30



of Energy


Neutron Residual Stress Facility at ORNL


27/30



of Energy


TelePresence Microscopy Collaboratory, Advanced Microscopy Center at ANLNestor Zalucek and Presistent Electronic Spaces

T l & T l ll b


28/30



of Energy


Materials MicroCharacterization LaboratoryAdoption of Web-based TPM Protocols

Univ. of IllinoisUniv. of Illinois

ORNLORNL

LBNLLBNL

NISTNIST

ANLANL

A G id N dA G id N d


29/30



of Energy

Access Grid NodesAccess Grid Nodes

Ambient mic

(tabletop)

Presentermic

Presenter

camera

Audience camera

Ambient mic

(tabletop)

Presenter

micPresenter

camera

Audience camera

GNN d DOE U F ilitiGNN d DOE U F iliti


30/30



of Energy

GNN and DOE User FacilitiesGNN and DOE User Facilities

Information

Coordination Education

Conferencing

Telepresence

Telecollaboratory

Documents

GNN3 - D. Mancini, USA