Upload
others
View
3
Download
0
Embed Size (px)
Citation preview
~ Cambridge Analytical Associates ~ 1106 Commonwealth Avenue I Boston , Massachusetts 02215/ (817) 232-2207
FINAL REPORT
u.s. Env1 ronmental Protect1 on Agency Regton I
60 Westview Street Lexi ngton, MA. 02172
Attn: Ms . Mary Jane Mactejko
PROJECT NUMBER :
CUSTOMER ORDER NIJ4BER: S1D2S6 NNJA "';.i..-
REPORT NIJ4BER: 84-1478
PREPARED BY : Oavfd L. Fi est
DATE PREPARED: February 28, 198S
l> 0 :r HJ: zo HO u>o -<:r :00 l>Z -<o HO < ,.,,
0 :oz "'" 0
~
\
~ ~ Cambridge Analytical Associates
TABLE OF CONTENTS
I. INTROOUCTION
2. ANALYTICAl METHOOS
J 3. RESULTS
4. QUALITY ASSURANCE OOCUMENTATION
Cert1f1catton
1. INTRODUCT ION
This report s1.11111arizes results of chemical analyses performed on sampl es received by CAA on December 18, 1984. Analytical methods employed
for these analyses are described in Sect ton 2 and results are presented in
Section 3. The last section contains certtftcattons supporti ng the
analytical results.
2. ANALYTICAL METHOOS
Analytical Mthods uttltzed for s111ple analysts are sUI'MIIartzed tn
Toblo I.
3. RESULTS
Results of analyses are presented tn Table 2, 3, and 4. Quality
control results are reported tn Table 5.
,. 0
" H:I: zo HO <1>0
""'" :00 l> Z -< o :: o "'" 0 :oz mo 0 0
~
I I I I
Table 1. SU!IIIIary of Organic Analytical Methods
Const 1 tuent Method Reference Method Description
Volati le Method 624 (I) Purge and trap . gas Organi c chromatography/mass Compounds spectr0111etry
Smi volat tl e Method 8270 (2) Solvent ext racti on , Organics · capfll ary gas Acid/ Base/ Neut ral chroutography/111155 Extractabl es spectr0111etry
Pest tctdos/PC8s Method 608 (I) SOlvent extraction. gas chro.atography/electron capture detection
(l)~;.:·~~:~;t~r:~· _.::::::.~~r tUAg6&17.~~~6s;~ ~PA}~t o~,:~1!~!rt~ Ohio.
(2)U.S. EPA. 1982. Test Methods for Evaluating Soltd WastoPhxsfcal/ChMica1 MethOds. Sicona Ed1t1on. SW-846. Office of Solid Waste. U.S. EPA. Washington, D. C.
I I
.. I I
.I Jill 1 .. =1"1 . 'rr'•
( It ~·I f~"(l
1; "' ~J: zo ~n V>O -<:< " O l> Z -< n ~ o
<
"'" 0 "Z "' O n
~
I
Client : EPA~Ion I CM Proj.ct No. : 84~1471
-· S.,l• 101 CM 10:
en cntor~NM
121 ""-tMM Ul ¥111!1 cfllorlde C41 cfltoro.thene
~51 ..n lene chloride
~cfltorOIIfllyt ... ,,, .. lctll~
Cll trlfla-t,Miclltoro.tl'lyt-.
'" cblorofor-CIOI I,MICfll~ em 1,1,t•trlctllorM1'NM
1121 ~bon t.tr~~eltloriM em llr'.-.dlctlt~
(IU .crytOflltrlll IISJ ecrol•ln (Ill 1,2-odlctll~--
em tn••a-1,3-dlclllor~
1111 trldlloroetllyl-(191 chtorocllbr~t'NN
UOI 1,t,2=trtc:tltoroetNM
~ ~::~ r"--r~ "::'1---
CAMf!A IOGE ANALYTICAL ASSOCIATES, tiC~ U
..... ,., 1408148
Dlte S.ples Recelved 1 ~ 11, 19M Olte An•lytla Oc.pletech O.C.ber 22, 1984
Conc:.ntntlon - ug/1 lppbl
....... 8401151
1211 benzene mceot TRC901 _ 1221C:II•I,~Iclllor~ ffi)z:chi;o;ih;j;~;;;..---------------------------
n;r~;a---------
I:HI 1,1,2,2-'tltr.cl'ltoro.tf\WMI 1261 "tnchlor-o.tllyt.,. • 1271 toi...M ...
TRI401 ... TRI601
'"' __ TRUC)) TRUOI
I~ -· -~-1Co~~cMtr•tlont tnt thn the d•tec:tiOtl tl•lt .... l•tt biMk, Conc.tntlont bet-n I •nd 10 tl- the dltiiCt lon l l•lt ere listed 11 tree• ,..,.,,,Inti. O.tectlon ll•ltt tor ec:roleln ar~d •crylonltrll• •r• 100 ..,d 10 tl ... th• ~INI tMt-=tlon 11•1t ru,.etlv•ly.
l> 0
" H:J: zo HO <I>O -<J: :oo l>Z -< o HQ <
"'" 0 :oz ~0
~ 0
8 ..
CAMBRIDGE .v!AL'I'TICAL ASSOCIATES, IPC,
Cll.,.t1 EPA Region I CM Pl"oj.ct No,: 84·1478
O.te S..pl•• ReceiYedl O.O.bef' 18, 19&4 O.te An•lyll l C:O.pleted: Dlc•bef' 22, 19&4
S.ple ID: CM ID:
tO clllor .. thene
Conc:entntlon a ugfl lppbl
Mil• II 8408152
*·IOO 84081,
iirbr~-------------------------------
rn-~-----------------------
IU cl'lloroethane
Ul •tl'lyle~~e cl'llorlde --------------------·-----1)!•1-41cflloroetl'lyten. --------------------------._.LL_..!.Iaflcl'lloroefl\efte
tiJ tre~~s-1,2-dlcl'lloroetl'lyl--~~~~~~~~-~-~-~~~~~~~~~~~~~~~~~ C9J cl'llorotcww IIOJ 1,2-dlcllloroe~--- -------
1111 l,l,l*"'lci'IICW"'etMMI--------==------==--=---==--== iiz1 crbon tetr.cl'llorlde 1131 bt"a.dlcftiOI"''MMttl•iie------==:.:::..=:__ _____________ _
ll!LKryiOI'IItrlle ----------- -----------1151 KrO!eln iii)i;i:iiChi"oropropaine 117) trM~s•l,3-dlchloroprop;;;···------·----·-----------·----~~Chi'Qroettlyieft.-----·-----------------------
1 191 cl'llorodlbt'c.:.~t"-M
i20T'~oroei~n• 121) benzene iiiiCis:i;-~ior~----------------------------· iHIT-chl~~-----,.-------------·-----
~or;---- --··- -------------(2,, 1,1,2,2•tetrecl'lloroetllene - ··---------i2i)i;;r~'thYI.;---------ffi)Tol _______________________________ _
m;-~---------------------
m;-~~--==--=--========------------------1301 tot•! xyten.. TR!401
~~-·- =-==~==-------=-===.-::-no--===-=- -- -:::. -= · -- o.tec:tiOn-u;;;-:-_-:::::::::==:-.: _____ _:It-::-_-:==::..~-==
1eonc:entr•tlons less th•n tt••• dstectlon liMit sre left bl•nk. Concentr•tlons bet- I •nd 10 tl•e• the detection liMit.,.. listed •• trec:e leotels (TJII, O.t.ctlon liMits for ec:roleln and .c:rytonltrlle .,.. 100 •nd 10 tl ... the no-Ins I detection liMit r .. peet!Yely,
~ 0 :r H:l: zo HO <1>0 -<:r :00 ~z -<0 HO < ""' 0 :oz mo 0 0
"' 0
CAMBRIDGE ANALYTICAL ASSOCIATES, tiC.
Teble 2 Ccont 1d). Conc.ntretlont of Priority Pol lut1nt Vol1tlle Org1nlc Collpounds C~tttod 624)
Cll•t : EPA~Ion I CM ProJect No, : 14-1471
Sellple ID : CM ID:
Cll chlot"a.tfWII C21 --(]) vllllcttlor1de ... chloroetMM
"' -"'!'..,. clllorlde
J ~:::::::=. .... ... trelt ... 1,2-dlcti!Of"''etttyt-Ill ctllorotOI"'I C10) 1 ~lctiiOI"''e1'MMIe em 111•tl"lcfll~
ctn crtlolltetrectllorl• If)) ~lc:IIIO!"'a.e"'-
C14) 1Ct'l0111trfle em ecntll111 Cl6) 1,2-dlctlloropi"''P<<• {17) ,,. ...... 1,)-dlctlloropf'Oplrll Cll) trlctllot'Oittlyt .... {19) ctllorodl~llll
"'" 1,1 ,2•trlctllor"'t'ttleM {21)
... _ C221 cl .... l,)..cllchloropf"091M {2)) 2<tllot'Oittlylw111ytettllr' {24) ......... "" 1,1 2, 2•tetractlloroettlllle ,,., tetr.chloroethyiiM (27) tol~~~n~
"" ctll~z.,.
1291 lffl !benzene UOI totll 11 lenes
Dlte s. • .,, .. Rt>c. lwed : O.C.ber a, 1984 O.te Anllyth Collpletld : o.c.ber 22, 1984
ConC~t~tretlon ... ugfl hpb)
Sl~trt.Splke
8408141NS
.,.
••• ...
Anelytlc.IBienk 84ott4a a
1eoncentntlont IMI ttlen the detection ll•lt ere left blenk. ConC~t~tretlons betlfNII I 1nd ID ""' tt11 detection ll•lt .,.. listed •• t ree• , ..... ,. cnu. DltectiOI'I ll•lts tor .cro leln and ecry!Oflltrlll .,.. too lnd 10 tl ... ttll -In• I detection ll•tt ,...pectlwely.
:0 0 3 H::t zo HO <1'0 -13 :00 :oz -10 HO < "'" 0 :oz 1'10 n 0 :0 0
. \
CAMBRIDGE A~LY'TICAl ASSOCIATES, INC.
Tabla'· Coclc.ntr1tlon• of Acld/BIIe/M!Mitral Priority Pollutant Extractable• t ... tllod 12701
Cll.nt1 EPA Rlglon I CM ProJ.ct frb,r 14~1411
lllta S.piH R.cel¥t>d : DK..W 18, 1984
lllt. Anlly•l• Cotlpl1t1•h fabl"u.-y 26, 1915
-· ~
$Mpl1 IDr CM ID1 "' 1401141
0oM:Ifltrlt 1on - ua/1 <ppbl 1
" 1401149 "' 14011"'
.. 1401151
(11 pllrlrtol ---~---~--ktlloroptllnol --- -------- - - ------- -'" "' '" '"
2-fl1tf"'l)fferrol 2,4~1M'ttlyl,..;oo'-2,4~1clll~l
---~---noo Jtl pooc:lllor-~--------------------
! 2,4,6ootr1dllor~lllnol
__., 2,Winltrofhlftol (9) ~ltrofllrlftol
iiOi"' 4,6-41nltro-2-'11Yip1Mono_!.__ -===------·-CI1J !*ltiiCflloroptllflol
....
--~~.------------------nm-.,----,-~----H®-----._,"Y' phenol TRIIII- 1100 6100
,_ "
l> 0 :r HJ: zo Hn CI>O -<:r :oo l>Z -<n HQ <
"'" ,!£ f'10 n §l 0
I I
~ I I
CAMBRIDGE ANALYTICAL ASSOCIATES, UIC,
T•ble l Ccont 1d) , Conee~~tntlon of Acld/Bne/Neut,.•l P,.IOI"Ity Polh.1t•nt bt,..ct•bles CMttllod 12701
Cll.nt1 EPA Region I CM ProJect No,1 14•1461
IAKINEIJJRAL aii"'llGG Ccon 1t,l (Ill eceupMhyl.ne (19) ecen•ptltt~eM
1201 2 4•cltnltroto1Hn• C2H 2 6-dhltrvtol-1n1 dlethyl p!lthel•te CHI 4-octltCII"''OIf**yl "*'Y' •ffW' (241
.. _ J: Jtooflltn:IMdl,_.yt•T"'
I , Wiplleflylflydr-u:IM
~Y'"*'r' .. ...,. 1101 fleudiiOI"''benHM
1291 -.. -Ulll .... .._ (31) dl~tylpfltflel•t•
1321 tl..-..tMN (])) ben1ldiM1
"" • ,,, butyl a.nryl phtNI•t• 1361 3,3 1-dldiiOI"'OMzldiMI 1)7) benloC•Ienth,._
"" biiU~yl*yllplltNI•t•
"" .... 1401 dl-n-oc!yl pl'ltMI•n (41) benzoCb)tl~n~
,d)p -.nth,.eceM
O.tectlon Ll•lt
TR(!I)
TRC2001 TRClOOI
TRCIOI TR(2001
ntOOOI TRt2001
TRC200) TROOOI TRC401
1200 1100 TR(lOOI lR(2001
.. .. entl'lltlon• I•" th•n til• d•tectlon ll•lt .,.. T•ft bl•nk, Conc.nt,.•tlon• MtwHn I •nd 10 tl ... ttl• ll•lt of
d•tectlon •roe list*' •• t,.ace 1~•1• CTRI ,
2M.Iyllld •• •IObenleMo
'An•lyalld•sdlpllenyl .. ln•.
,. 0 J: MJ: zo MO v>o -<J: :00 l>Z -<0 MO <:
""' 0 :oz ~0
~ 0
CN&IIOGE ANALYTICAL ASSOCIATES, IPC.
Table 3, Concentration• of Acid/Base/Neutral Priority Pollutant Edrec:table• INett.od 12701
Client: EPA Region I CM Project No, : 14-1471
SeJIPI• 10 : -· 121
"' '" "' '" 111 ll)
Z..CIIIOI"'PMfiOI ~ltropllellol
2,WI..tllylpllenol 2,Wiclll~l
pooclll~l
2 4 6-trlciiiOI"'PIIellol 2,WIA1troptleftol
CM 10:
..,.,,ropbe!lol 4,6-ocllllltro-2.....,..ylpllenol
nn ,...teatot'Opftenot .,.....,pflelltol
benzoic ecld
MK/!!EIIl1W. QIPOUII)$
111 JW!Itro&odl .. tflyt•lne (2) bltl2~1oroetllyt)~tller
Ill I 3-odlcllloroben;r-C4) I,Wicl'llorol:lenzene (5) l,~ldi!OI"'benz-
!!!,_ bltC2~111oroltot>ropytletflf' 111 JW!ltr"'OICCI~-11ropyt•lne
Ill Mxec:IIIOI"'ttllane 19) nltroben;rene UOI hopllorone 111) blsl2~111oroettK»cyl .. tflane 1121 1,2,4-trlcllloroGenzene 1131 ~teplltllel•e
114) lleuclllorobllt•dl-1151 Mxeclllorocyclop-.,tedl(161 2-<llloron•plltii•I-
\.J~'~'M<~•~r•~~~·~~~'~"~'---------------
Dlte s .. plel Rec:elyecl: o.c-.r II, 1914 O.te Anelyalt CoMpleted : Februery 26, 1985
Concentntlon- ua / 1 lppb1 1
" 8408152
TRIIOI ,..
100 140815)
~ " HJ: zo HO <1'0 -IJ: :00 l>Z -10 HO < "'" 0 :oz mo 0 0
"' 0
Client : EPA Region I CM ProJect No. : 14 .. f.t78
S.IIPIIID : -· CM ID :
IASEJ!!U'ntAl CIDM"CCUHDS ccon•t.l (111 ecenepllttl leM
'"' eceneplltn-,,., 2 4--cllflltrotoluene 120 2,6-odlflltrotol-1221 dletft I pM'IIIIIete
'"' t-<MoropMftrt PNfirt ether 12<1 "--"" hltroeodl"*'rl•l., 1201 1,2-dl,...ylhyc!,..llfll
'"' ............ yl IIMnyl ether
J tt.ec:hl~a-_ .. _
1!01 .... .._ ()1) ........ ..,I ,..tlltilate ,,.,
fi~Dr'Mttl-
'"' biMzldh•
C:Ml ' (), butyl *zyl phtlltllate
"" 1,) 1 -dlehlorobMrldl~~e
'"' beiiiOIII.,.th~
"" b1112 .... tttyl~tny l)phtMI.te
"" .. .... 14D) dl""'ft't'Ctyl phtMiete (41) benrolblfluore~~tn-
(421 benro(kltluorefltn-COl Muo(elp r-.. 1441 1Mef10(1,2 1kdl,r-,., dlbellzo(e,lll.,.ttl~
1461 beruo(gllllper-yt-benz lelc:ohol
CAMBRIDGE ANALYTICAL ASSOC IATES, INC.
11 1408152
TRC61
100 8408151
1 Co~tce~~tr-st1onl IMI tlllfl the Ntectlon ll•lt er-e left bllflk 0 Conc.t~tr-etlons MtwMII 1 lfld 10 tl ... the 11•1t of l '\tectlon .,.. lhted II tr"IC. IIYIII CTRI.
~llyrediiiZOMftZ..,., 1AnllyZedlldlpllenyl•1fll,
~ " ~I zo ~0 11>0 -<:< :00 l>Z -<o ~o
<
"'" 0 :oz 1'10 0 0 :0 0
I I
.. I I
" I CANBAIOG£ ANALYTICAL ASSOCIATIS, IIC,
Teble 3 (c:ont 1dl, Oc:w!eentntiOI'!I of kld/BIIse/ Niutrel Priority Pollutant Elrtreetlbl•• IMithod 82701
Cll1111t 1 EPA A41glon I CM Project No, 1 84-1479
-~ Ill P'*'lol
"' "' ... "' J Ill ltl
2<odltoropflenot
2-.ltrOflhellol
2,&-c! IIWf'tly lpMflol 2, 4-41cfllorotll*lol ,-ct~ lor04-Ct'etOI
2,4, ... trlcti!Of'Otii*IOI 2,Winl~l
1101 4 ,6-dlnltro-~flyi!IMROI
1111 ,_tKMOI"'ttffenol
... ~-Ill M-nltro.od l..thyl • ln.
"' bii(:Z..Cflloroethy l ) .. t ....
"' J, l-dlclllorobeftHM
141 1 ,4~1 ch l orobeftr..
'" 1,2-cl l ch loro!MfiHN
161 bi1C2<h lorollo.,-opyt tethr 111 N-flltrCKOd l.n..,.opyt•ln~ Ill heiCKhloroetMne
191 l'lltrobeftZWII
(10) ltopPiorOM
111) bl112<hloroettlox'f)Mttlarle
Dltl S..plel Reee!Yedz Dtc•bw 11, 1984 Dlft Anllylll C:O.pleted : Febru..-y 26, 191!1'
Concentr1tlon - uo/1 lppbl 1
100 Mttrl~~: Sp ike Blenk
840815) MS 8408151
m ...
""
~TI~il=--~·~·'~··~~~'~'';'i~~~~~·:~::-::::::: ___________ '_"'-----------------------
l> 0
"' Hr zo H() 11'0 .... ,. :oo l> Z -<n H O <:
"'" 0 :oz 1'1 0 () 0
" 0
Client : EPA Region I CM. ProJ~~et No,: 14-1479
SMPI• 10: _.,.,, CM. 10:
IAS£/!!UlRAL CCII"CUUlS (COft 1t,)
(11) aceMPIItll 1-091 Ker~aplltlllfle ,,., 2,Winltrotol-(21) 2,6-dlnltrotol.,_
'"' dletllyl phtMiaft 12ll 4-oc:llloropllenyl pllenyl .,.._. ,,., .,_ C251 N-ftltroaoflpt~at~yl•l, ,,., 1,2-dlp'-ylfi,,Azlna
"" --~r'pfle!lrletfler"
J Jileuclll~zene _ .. _ .... .._
()1) dt.....e.utyl pfltMiete
"" flloiOI"'an,.,_ C))) •zldl~~a
"" . ()5) butyl MnzylolltMiaft .,., '"1 1 ""411clll~zldlne
U71 Mnzo(a)antllr-ec:Ma
"" blaC21tllyl"-yl1plltMiata
'"' cflryaena .... dl~tylohtflalaft
(41) baftzoCbltluorantMM (421 baftzoCkltluorantMM (41) beniO(alltr..
"" lnd•oCI,2,)-c:,d)pyr.M (45) dl benzoCa,ll1anthroaceM 146) bei'IZO(JIIIIperyl-
Oatec:tlon Ll•lt
CN4BRIOGE ANALYTICAL ASSOCIATES, INC,
Concentr-ation - ua/1 hpb) 1
100 .,.tr-1• Spike 1408153 MS
'" ""
iOi
...
Blank 1408151
1Coftcentratlona lass than ttla det~~etlon ll•lt are latt blank, Concantratlons batwMn 1 and 10 tl ... tlla ll•lt of 6atec:1'lon ara listed as traca l..,als CTRI,
elyzad as azobenzll!a,
1Malyzadndlphanyl•lna,
CAMBR IDGE AHAUTICAL ASSOC IATES, INC.
Cll«~t : EPA Region I O.t• 5.-pl•• R•c•lvM : o.c.-.ro II, 191, CM ProJKt No. : 14 .. 1411 O.t. A,.lysls Cosplet M: J1nuery 11, 198'
Conc.t~tr-1tlon .. !!51 / I Cl!l!b) 1
SeiiPII ID: "' " .. .. _..,,, CAA ID: 1408148 1408149 8408150 14oan1
'lSTICIDI:S NG Pall en liP~
l2l ... ....., I "' de lte..C
'" ,_..-.c etlnMnl)
"' "-'t.:tllor
"' .. .,.,,.
"' lleptKIIIor epGifl de Il l •l~ul ten
J dle ldr"lfl 4, 41...(10[
Clll .,.,,. C1 21 t.t-clolultM em
· · ·~ C14 1 .-r-111 lldeiiJ'dl em --.ulfMsultat. Cl61 ··•'4T em - "~ (181 ............ C19) --,,., f!C8..1016 e2H fiiC&o.1221 In I ...,..,, CUI f!C8..1242 (24) fiiC&o.l 248
"" PC&-1 254 ,,., ...... , ... o.t.ctiOft Ll•lt '·' '·' '·' '·'
1Conc.ntnttons '"' then till d1t.ctl0ft ll•lt 1r. l•tt blink. Conc•tretlons behtHII 1 •l'ld 10 tiNS tne detKtlon IT•It er. llst.d •• tr-ee. levels cnu. O.t~etlon ll•lts tor PC8s are t.n tt ... t"- -lnel d•tKtlon ll•lt.
l> 0 :r MJ: zo MO <1>0 -IJ: "O l>Z -co MQ < "'" ,!i! "'O 0
~ 0
'1
'. \
Client: EPA Region I CM ProJKt No. : 14·1478
CN411RIOGE NIALYTICAL ASSOCIATIS, IJC.
O.te S.plel RKehted 1 O.C.bw 18, 1914 O.te M1ly1l1 C.:.pleted : Jenu1ry 11, 1985
Cbftc~t~tntlon • ug/1 (ppb) 1
S.ple 10: 100 a.oal5l
..e:STICIOO Nil P'CII 111 121
o1-.... ..., ()) Rite~
(41 ,_~(llnclenel
'" MptiiCMor
:::1 ehllrln _! llepteclllor et1011lde I ll~lollfM
(9) dleldrht
(10) ··•'.oDE 1111 ..... 1'1
(121 ..,.......,.ultM (I))···'~
o•J INrlneiHtl.,cle (15) ..... lllfMIIIIfe ..
1111 ···'~ em ...._yct'lor CIIJ chlordene rn;-...,..... i20) P'C&-1016 (21) PCa-1221
mr ..:a-1212 iii)-;c...1242 rn;- PCB-1248 rn;-PC&-1254
~IHO
CM 10:
________ ,_.1 0.1
~ :r ~J: zo ~0 (/00 -1:< :00 l>Z -1 0 ~0 < "'" 0 :oz
"'" n 0
"' 0
Cllent1 £PA Regl011 I CM ProJect Mo. : 14-1411
S.•ple ID: -· CM ID:
f'UTICUIES NG f'C8I Ill ol-
"' ... ......,
"' Htt...ac 141 ,_...... (llrldanl)
"' -,tlld!ICII'" 161 •1411"111 111 Mlt~IOI"eporiM
: .............. lilt• dieldrin I 4 4 1--GIX
(11) eMirlll
C12l w......-.~~••• iii'r4 4'«11 114) M41rhetdetlyde
'") --lllfell&lllflt9 116) 4 4 1-«fT (11) 1 ... Ill) .. I...._ 119) -120) f!C&ool016 121) f'ICI-1221
"" f'ICI-1212 12,) f'ICI-1242 (24) f'ICI-1261
"'' f'ICI-1254 ,,., f'CB-o1260
Detection Ll•lt
CNIIRIOGE ANALYTICAL ASSOCIAT£5 , IJC,
lS Mltrhl: Spike 1401149145
.., ,,.
1oSi
tOll
'"'
Blenk 1408150 a
'·' 1eo..c.,.tretlona leaa t11111 1111 detection ll•lt .,.. lett blul!.. Ocwlcentntl011a betnen I 111d 10 tt.-s the detectiOII lf•lt .,.. llated n tree• teYela CTR) , Detection ll•lh tO!" PC8a ere ten tl•• tM _,,.., O.tectiOII ll•lt,
,. 0 3 ~:~: zo ~" V>O -<3 :00 l> Z -< n ~o
<: ,., ., :o !il 1'1 0
" 0 :0 0
Cllent1 EPA ~ion I CM Proj.ct No 1 14·1471
CNIIRIDOE AMALYTICAL ASSOC IATES, IIC,
Swrogate eo.pounc1 AKcwry Ill
Acceptlble S.,l• IDI "' " .. .. Anllylh ll•ltl CM IDr &401148 14011"9 1401150 1401151
~
Anely111 O.te "'· 22 Dtc:.22 "'· 22 Dtc:.22
10 2-Gic:M.-oettleM,cl" 71•120 "' 10, 109 100 TolweM,fl 16-119 101 102 100 101
~flmrobennne ,,_121 " n 71 10
~
bt .... c:tiCIII O.te o.c.21 o.c. 21 o.c. 21 DK. 21 ••• ,. •• O.t• ...... ... ... , •• 26 ...... 241~1 2l-121 .. " " .. P'tlenoi,O ,,_,0, .. " 124 120 2,,.,6-Trl.--opMnol IG-I:SO 121 .. 110 .. Nltrobeftnne, cl5 41-120 .. " 1" 104 241uoroblpflenyl 44-119 .. " 120 124 ,_, .. .,.,. •• ,ell" n-12e .. " 112 " ----------POTIC I Dl!l!!!!;
Extrectlon O.te Dtc:.21 Dtc:,21 Dtc:,21 DK. 21 Anely1l1 O.te .-n.ll .-n . ll Jln.l1 .Mn.ll
Dlwtyl chlorencl•t• 41-1)61 " 149 " 40
,.._..,._ &tnctlon O.te .. " .. NA
AnllyiiiO.t•
• frtltHI
1Aclvl10ry unltt only. NA- Not eppl lcebll ; tM ... ,,, w11 not enllyzld for thl1 11•r-'er.
l> 0 :I ~:r zo ~n <1>0 -!:I :00 l>Z -to ~0
< "'" "~ mo n jl 0
CNIIIIAIDGE '-HALYTIC"L .USOCI"T£5, INC,
Teble S Ccont'd), Quellty -'ta..rence S~ry for Orgenlc Me l yMI • IMt.,.
Cllent1 EP" Aeg 1011 I CM ProJect Ncu 84•1478
olccepteble
Melysls Ll•lts
1,2-0iclilloroetNM,dl 71·120 Toi~~M~e,d8 16--119 ~,,......... 8~121
-~ IJrtr.ctiOII Dlte ....... Dlte
2-11....,._., 2).121 PtiM!ot , tS 1).103
2,1,6-Trl~l 1~130
Nltrobefl&ene,d5 11·120 Hluoroblpftellyl 14-119
S..ple 101 CM 10:
11 8408152
Doc. n
109 104 ..
Dec. 21 ...... .,. ..
121
11 11 11
p..oT .. P"-'YI,dll )).128 ----------·----£xtrectl0fl Daft Met ysls O.t. ,.
100 8408155
Doc. n
109 100
"
Dec, 21
fM." "' "' 106
"' " .. Dec. 21 .len , II
142 01 bUtyl ctllorendet• ---------------------------------------[)ltrec'tiOfl Dlte Melylls Dlt•
...... •MYiaoryunlhonly, ""·Mot eppllceble; the a-pie wn not en11yzed tor thi s per .. ter ,
"' ..
~ ~I
zo ~o V>O -<:X :00 l>Z -<o ~0
<
"'" 0 :oz "'0 0 0
~
I I
" I I
..
4. QUALITY ASSURANCE D0Cli4ENTATION
Cert1f1 cat1on
This work has been checked for accuracy by the following staff
personnel :
D1 rector, Organt c CheMistry l aboratory
Oavtd L. Ft est
~ ~:t zo ~o 11>0 ... :r :0 0 l> Z ... 0 ~ o
< ,, 0
:oz mo
i