February 28, 2020 2020-112-64-MTM-A PUBLIC NOTICE · 2020-02-21 · Inc. (Wood) have completed the Final-Draft Sediment and Water Sampling and Analysis Report for Burns Waterway Harbor

Version 1.0 – 12/7/06

Indiana Department of Environmental Management Office of Water Quality

Wetlands Section

PUBLIC NOTICE

Publication Date: IDEM ID Number: February 28, 2020 2020-112-64-MTM-A

Closing Date: Corps of Engineers ID Number:

March 20, 2020

To all interested parties: This letter shall serve as a formal notice of the receipt of an application for Section 401 Water Quality Certification by the Indiana Department of Environmental Management (IDEM). The purpose of the notice is to inform the public of active applications submitted for water quality certification under Section 401 of the Clean Water Act (33 U.S.C. § 1341) and to solicit comments and information on any impacts to water quality related to the proposed project. IDEM will evaluate whether the project complies with Indiana’s water quality standards as set forth at 327 IAC 2.

1. Applicant:

U.S. Army Corps of Engineers 2. Agent: 231 S. LaSalle Street, Suite 1500 Chicago, IL 60604

3. Project location: Lake Michigan at Burns Waterway Harbor

4. Affected waterbody: Lake Michigan

5. Project Description: The applicant proposes to conduct annual maintenance dredging at Burns Waterway Harbor. Dredge areas will

potentially include the Approach Channel and Maintenance Area, the Outer Harbor, and the East and West Arms dependent on shoaling and Lake Michigan water levels. A maximum of 100,000 cyd of material would be hydraulically or mechanically dredged annually, as a total from all areas. Dredging is anticipated to occur on an annual basis, depending on funding. Two separate placement areas are proposed. For the Approach Channel and Maintenance Area, which have lower fines content, the proposed placement locations are either within the littoral zone (less than 18' water) along Ogden Dunes beach or onshore in the same area, depending on funding. For the Outer Harbor and East and West Arms, the proposed placement location is in deep water (>50') north of Burns Harbor. The inner harbor sediment has a higher fines content and is not well suited to beach nourishment. Because dredging is expected to occur on a nearly annual basis, a five year permit is requested. Additional information may be found on line at https://www.in.gov/idem/5474.htm

Comment period: Any person or entity who wishes to submit comments or information relevant to the aforementioned project may do so by the closing date noted above. Only comments or information related to water quality or potential impacts of the project on water quality can be considered by IDEM in the water quality certification review process.

Public Hearing: Any person may submit a written request that a public hearing be held to consider issues related to water quality

in connection with the project detailed in this notice. The request for a hearing should be submitted within the comment period to be considered timely. The request should also state the reason for the public hearing as specifically as possible to assist IDEM in determining whether a public hearing is warranted.

Indiana Department of Environmental Management 100 North Senate Avenue MC65-42 WQS IGCN 1255 Indianapolis, Indiana 46204-2251 FAX: 317/232-8406

Version 1.0 – 12/7/06

Version 1.0 – 12/7/06

Burns Waterway Harbor FINAL

Sediment and Water Sampling and Analysis

October 2019

Contract No. W912QR-14-D-0006 Delivery Order No. W912P619FCX10

Prepared For:

U.S. Army Corps of Engineers Chicago District

231 South LaSalle Street, Suite 1500 Chicago, Illinois 60604

Prepared By:

500 Horizon Drive, Suite 540 Robbinsville, New Jersey 08691

PARS Project No. 773-56

October 2019

U.S. Army Corps of Engineers, Chicago District Burns Waterway Harbor

FINAL-DRAFT Sediment and Water Sampling and Analysis Contract No. W912QR-14-D-0006

Delivery Order No. W912P619FCX10 October 2019

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CONTRACTOR STATEMENT OF TECHNICAL REVIEW

PARS Environmental, Inc. (PARS) and its subcontractor, Wood Environmental and Infrastructure Solutions,

Inc. (Wood) have completed the Final-Draft Sediment and Water Sampling and Analysis Report for Burns

Waterway Harbor at the Port of Indiana, located in Porter County, Indiana. Notice is hereby given that an

independent technical review (ITR) has been conducted that is appropriate to the level of risk and

complexity inherent in the project. All comments resulting from the ITR have been resolved and

incorporated into the document. During the ITR, compliance with established policy principles and

procedures was verified.

9/30/2019 Jay Mullett, PE, ITR Team Leader

10/14/19 Cody Postlethwait, PMP, Project Manager

CONTRACTOR CERTIFICATION OF INDEPENDENT TECHNICAL REVIEW

Significant concerns and the explanation of the resolution are as follows:

No major technical concerns were identified during the ITR.

10/14/2019 Constantine Tsentas, PG, Program Manager, Contractor




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TABLE OF CONTENTS

1.0 INTRODUCTION................................................................................................................................ 1-11.1 Project Objective .................................................................................................................... 1-2

2.0 SITE DESCRIPTION ......................................................................................................................... 2-13.0 FIELD SAMPLING ACTIVITIES ........................................................................................................ 3-1

3.1 Sampling Preparation ............................................................................................................. 3-13.2 Field Documentation .............................................................................................................. 3-13.3 Weather / Climatic Conditions ............................................................................................... 3-23.4 Water Level .............................................................................................................................. 3-33.5 Sample Locations ................................................................................................................... 3-33.6 Sample Collection ................................................................................................................... 3-33.6.1 Sediment Sampling Procedures ........................................................................................... 3-43.6.2 Volatile Organic Compound Sample Collection Procedures ................................................ 3-53.6.3 Water Sampling Procedures ................................................................................................. 3-63.6.4 Decontamination Procedures................................................................................................ 3-63.6.5 Field Logs..............................................................................................................................3-63.6.6 Sample Containers and Sample Preservation ...................................................................... 3-63.6.7 Sample Custody .................................................................................................................... 3-7

4.0 PERFORMANCE DATA REVIEW ..................................................................................................... 4-14.1 Chemical Data Review ............................................................................................................ 4-24.2 Quality Assurance / Quality Control ..................................................................................... 4-24.3 Data Qualifiers ........................................................................................................................ 4-4

5.0 RESULTS .......................................................................................................................................... 5-16.0 REFERENCES................................................................................................................................... 6-1




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FIGURESFigure 1: Site Location

Figure 2: Dredged Material Management Unit Locations

Figure 3: Reference Site and Disposal Area Locations

Figure 4: Dredged Material Management Unit Sample Locations

Figure 5: Reference Site Sample Locations

TABLESTable 1: Sample Summary

Table 2: Weather Conditions

Table 3: Sediment Sample Information

Table 4: Water Sample Information

Table 5: Sediment Chemical Analytical Results – Inorganics

Table 6: Sediment Chemical Analytical Results – VOCs, PAHs, PCBs

Table 7: Water Chemical Analytical Results – Inorganics, VOCs, and PCBs

Table 8: Water Chemical Analytical Results - SVOCs

Table 9: Sediment Grain Size Analysis

APPENDICES Appendix A - Field Sampling and Sediment Core Logs

Appendix B - Laboratory Reports

Appendix C - Data Validation Report




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ACRONYMS ASTM American Society for Testing and Materials

BLK Method Blank

BTEX Benzene, Toluene, Ethylbenzene, Xylenes

COC Chain-of-Custody

COD Chemical Oxygen Demand

CT Labs CT Laboratories, LLC

°C degrees Celsius

DO Delivery Order

DQO Data Quality Objective

EB Equipment Blank

FD Field Duplicate

ft. Feet

GLEC Great Lakes Environmental Center

GPS Global Positioning System

HCl Hydrochloric Acid

HNO3 Nitric Acid

H2SO4 Sulfuric Acid

ID Identification

IDW Investigative Derived Waste

IGLD International Great Lakes Datum

ITR Independent Technical Review

LCS Laboratory Control Sample

LCSD Laboratory Control Sample Duplicate

LOQ Level of Quantitation

LWD Low Water Datum

μg/kg microgram per kilogram

μg/L microgram per liter

mg/kg milligram per kilogram

m meter

ml milliliters

Mi-Tech Mi-Tech Services, Inc.

MPN/gTS Most Probable Number of Viable Cells per Gram of Solid

MS/MSD Matrix Spike/Matrix Spike Duplicate

MTBE Methyl tert-butyl ether

MU Management Unit

PAHs Polycyclic Aromatic Hydrocarbons




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PARS PARS Environmental Inc.

% Percent

PCB Polychlorinated Biphenyls

pH Potential of Hydrogen

PID Photoionization Detector

QA/QC Quality Assurance/Quality Control

RPD Relative Percent Difference

RS Reference Site

SDG Sample Delivery Group

SOW Scope of Work

SVOC Semi-Volatile Organic Compound

SIM Selected Ion Monitoring

SM Standard Methods for Examination of Water and Wastewater

TB Trip Blank

TDS Total Dissolved Solids

TOC Total Organic Carbon

TSS Total Suspended Solids

TVS Total Volatile Solids

USACE United States Army Corps of Engineers

USCS Unified Soil Classification System

USEPA United States Environmental Protection Agency

VOC Volatile Organic Compound

Wood Wood Environmental and Infrastructure Solutions, Inc.

Work Plan Final Burns Waterway Harbor Sediment and Water Sampling and Analysis Work

Plan




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1.0 INTRODUCTION

The U.S. Army Corps of Engineers, Chicago District (USACE) retained PARS to perform sediment and

water sampling and analysis at the Burns Waterway Harbor at the Port of Indiana, located in Porter County,

Indiana (Figure 1). The objective of the sample collection and analysis effort was to:

Obtain physical and chemical data for the sediments to be dredged in order to determine the suitability of the material for beach nourishment, littoral zone, or open water placement, and

Obtain chemical data for elutriate samples in order to determine water quality impacts related to sediment dredging and disposal.

The sampling activities consisted of the collection of sediment core samples, elutriate samples, sediment

grab samples, and site water samples in accordance with the USACE Scope of Work (SOW) Section C,

prepared by USACE and dated June 5, 2019, Contract No. W912QR-14-D-0006, Delivery Order (DO) No.

W912P619FCX10 and PARS Final Burns Waterway Harbor Sediment and Water Sampling and Analysis

Work Plan (Work Plan) dated August 6, 2019 (PARS, 2019).

PARS subcontracted field sample collection efforts to Wood. CT Laboratories, LLC (CT Labs) in Baraboo,

Wisconsin, provided chemical analysis services; CT Labs subcontracted geotechnical (grain size analysis)

services to Mi-Tech Services, Inc. (Mi-Tech) in Weston, Michigan. Great Lakes Environmental Center

(GLEC) provided and operated a 26-foot Pontoon Boat equipped with a pneumatic drivecore unit,

submersible pump, and ponar sampler to aid in the collection of samples.

Field sampling activities were completed from August 13 through August 16, 2019. The sampling events

were performed by the sampling crew consisting of Mr. Andrew Biehl and Mr. Chris Kapanowski from Wood,

Ms. Casey Pittman from USACE and Mr. Dave Johns and Mr. Carter Johns from GLEC. Sediment and

water samples were collected from within four (4) management units (MUs) within the dredging area

(Figure 2) and two (2) reference site (RS) locations (Figure 3). A composite of equal volumes of sediment

and site water were collected from each core within each MU which were used for preparation of an elutriate

sample. Background water samples from the RS were collected to compare the results of the elutriate

tests.

Sediment core sample locations within the MUs were adjusted in the field due to lack of shoaling at

proposed sample locations, the actual sample locations after field adjustment are presented in Figure 4.

Sediment grab samples were collected from the RS and are presented in Figure 5. Sample collection

activities are described in Section 3.6.

A total of twelve (12) sediment core samples, six (6) sediment composite grab samples, four (4) elutriate

samples and six (6) water samples, were collected at Burns Waterway Harbor. One (1) sediment duplicate

sample, one (1) sediment matrix spike/matrix spike duplicate (MS/MSD) sample, one (1) water equipment




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blank, and three (3) water trip blank samples were also collected for quality control/quality assurance

(QA/QC) analysis (Table 1).

Sampling, sample handling, and analytical techniques were conducted in accordance with the USACE

SOW, the PARS Work Plan, in addition to “Methods for Evaluating Solid Waste” 3rd ED, U.S. EPA No. SW-

846, and “Description of Soils (Visual-Manual Procedure)”, American Society for Testing and Materials

(ASTM) D2488-69 and particle size distribution of soils (Hydrometer Method), ASTM D 422.

1.1 Project Objective

This report aims to document activities completed for sediment and water sample collection and analysis

in Burns Waterway Harbor.

The objectives of this sample collection and analysis effort include the following:

Obtain physical and chemical data for the sediments to be dredged in order to determine the suitability of the material for beach nourishment, littoral zone, or open water placement, and

Obtain chemical data for elutriate samples in order to determine water quality impacts related to sediment dredging and disposal.

The information obtained is intended to be used to evaluate the removal and disposal practices for dredge

material from the dredging area, the disposal options for the sediment, and the water quality impacts of

dredging activities.




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2.0 SITE DESCRIPTION

Burns Waterway Harbor is located on the southern shore of Lake Michigan in Porter County, Indiana

(Figure 1). The port is divided between the municipalities of Burns Harbor and Portage. A curved, rubble

mound breakwater from the north and the ArcelorMittal facility in the south form Burns Harbor. The

breakwater protects the channel, which provides lake access to ferry boats, and commercial vessels. The

USACE, Chicago District, plans to dredge Burns Waterway Harbor in areas where shoaling is present in

the Federal Channel. For this project, samples were collected from four (4) MUs consisting of the West

Harbor Arm (MU1), the East Harbor Arm (MU2), the outer Harbor (MU3), and the approach channel (MU4)

(Figure 2). Potential dredge activities will include removal of shoaled material to the project depths in

feet (ft.) below low water datum (LWD) and are the following:

MU1 - West Harbor Arm (27 ft. LWD)

MU2 - East Harbor Arm (27 ft. LWD)

MU3 - Outer Harbor (28 ft. LWD)

MU4 - Approach channel (30 ft. LWD)

Potential dredge activities will include removal of shoaled material to the project depth(s) plus up to 2 ft. for

over dredge. In addition to the MUs, samples were collected from two (2) RSs to serve as a point of

comparison for evaluating sediment quality to the proposed disposal area(s) but have not been impacted

by previous dredge material disposition. RS1 is located close to the shore approximately 2.5 miles west of

Burns Waterway Harbor and RS2 is located in Lake Michigan approximately 1-mile north of the Harbor

(Figure 3).




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3.0 FIELD SAMPLING ACTIVITIES

The field sampling activities were conducted according to the SOW for the Burns Waterway Harbor, Indiana,

USACE contract order No. W912QR-14-D-0006, DO No. W912P619FCX10, as planned and submitted in

the PARS Work Plan, and upon discussions with the USACE Project Manager, Ms. Casey Pittman.

3.1 Sampling Preparation

The SOW provided by USACE required sediment and water sampling at eighteen (18) locations within the

four (4) MUs in the dredging area, RS1, and RS2 at Burns Waterway Harbor. In order to organize the

sampling effort, a Sediment and Water Sampling and Analysis Work Plan was developed to clearly define

the objective based on the SOW (PARS, 2019). The overall sampling plan summarized the following:

Project depth and elevation, amount of sediment required for chemical and physical analysis, sampling

equipment, sample locations, analytical parameters, containers required, sample preservation

requirements, chain-of-custody (COC), and planned shipment of samples to the laboratory.

Wood and GLEC coordinated with Port of Indiana authorities at the Burns Harbor and USACE for the

sampling activities, schedule, site access, and anticipated equipment that were to be used at the site.

The sampling crew confirmed with USACE and the Port of Indiana authorities, prior to mobilization and

sampling, the locations of any underground utilities crossing the sampling location at Burns Waterway

Harbor to ensure that no sample locations were located near any underground utility.

3.2 Field Documentation

Field data including conditions and site activities, field sediment coring logs, sediment grab sampling logs,

site water sampling logs, and sediment sampling logs are included in Appendix A. Information recorded

in the field logs includes:

Sediment Coring Logs

Sample location;

Sample collection date;

Depth at each sampling location;

Thickness of each core retrieved;

Project required sample collection interval;

Latitude and Longitude of station locations; and

Time of sample collection.

Sediment Grab Logs

Sample location;




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Depth at each sampling location;

Latitude and Longitude of sample location;

Time of sample collection; and

Description of material sample according to ASTM D 2488-69, “Description of Soils (Visual Manual

Procedure).

Sediment Sampling Logs

Sample core location;


Sample collection time;

Sample collection interval;

Description of material sample according to ASTM D 2488-69, “Description of Soils (Visual Manual

Procedure) and photoionization detector (PID) measurements; and

Relative QA/QC samples collected (if applicable).

Site Water Sample Logs

Sample location;


Sample collection time;

Depth of sampling location;

Latitude and Longitude of sample location; and

Applicable field parameter measurements (temperature and potential of Hydrogen [pH]).

Prior to collecting sediment and water samples, the sample coordinates were recorded using a

programmable Global Positioning Systems (GPS) (Trimble Geo7X) unit with 1 to 3-meter (m) accuracy.

The water depth at each sample location was measured using steel rods and confirmed with the Garmin

depth finder on the GLEC vessel.

3.3 Weather / Climatic Conditions

The weather conditions encountered during the sampling activities were generally sunny, with winds from

the north. Daily weather conditions during the sampling event are summarized in Table 2. Water clarity

was typically clear in the harbor (at MU locations), but poor at RS locations with 4 ft. or less visibility due to

the water turbidity.




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3.4 Water Level

Reference water level data were obtained each morning (prior to sample collection) and each afternoon

(after sample collection was complete) and were used to calculate the amount of sediment required at each

sample location. Reference water level data (in ft.) were obtained from the water level gauge located at

Calumet Harbor, Illinois (Station ID# 9087044). Water level data obtained was corrected based on the

LWD of Lake Michigan. The LWD of Lake Michigan is listed as 577.5 ft. from the International Great Lakes

Datum (IGLD) 1985 (IGLD, 1985). The water levels fluctuated between 581.98 ft. to 582.14 ft. during the

sampling activity periods (Table 3).

3.5 Sample Locations

Suggested sediment core and grab sample locations were pre-determined by USACE and provided in the

SOW. Sampling activities were initiated by navigating as close as possible to the coordinates of the pre-

determined sample locations using a preprogramed GPS unit. Sediment core sample locations within the

MU1, MU2, and MU3 were adjusted in the field, with USACE approval, due to lack of shoaling at proposed

sample locations. USACE requested to attempt collecting three sample cores from each MU, regardless

of proximity to the Federal Navigation Channel boarders and distance from other samples collected within

the MU. In dredging area MU4, sample locations did not require field adjustment; sample locations from

the four (4) MUs are located on Figure 4. Sediment grab sample locations from each RS were collected

from the pre-determined sample locations and are located on Figure 5. Background water samples were

collected from within each MU and RS. Water samples for elutriate procedure were collected from within

each MU. GPS coordinates of sample locations and locations of water samples are in Table 3 and Table 4.

3.6 Sample Collection

The purpose of sampling was to collect a representative, undisturbed sample of the sediment to the

maintenance dredge depths, in LWD, described in Section 2.0, plus 2 ft. for over-dredge. Three (3)

sediment cores and three (3) grab samples were collected from each MU and RS, respectively. The

sampling crew considered many factors in the selection of suitable sampling equipment, including physical

character of the sediments, required depth of penetration and weather conditions. A composite of equal

volume of sediment from each individual core within each MU and site water was collected for preparation

of elutriate sample. In addition, one (1) water sample for background analysis was collected in each MU

and RS for chemical analysis.

A total of twelve (12) sediment core samples, six (6) sediment grab samples, four (4) elutriate samples, and

six (6) water samples were collected at Burns Waterway Harbor. One (1) sediment duplicate sample, one

(1) sediment MS/MSD sample, one (1) water equipment blank, and three (3) water trip blank samples were




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also collected for QA/QC analysis. The four (4) elutriate samples consisted of equal volumes of sediment

and site water were collected from each individual core location within the MU for preparation of elutriate

samples.

Two (2) types of sediment samplers mounted on the pontoon boat were utilized to collect the sediment

samples based on the requirements for each sampling location, water conditions encountered, and/or

nature of the sediment surface. The types of sediment samplers used during the project included:

A pneumatic drivecore unit mounted on a 26-foot Pontoon Boat, which utilized a 29-pound

pneumatic piston to drive 4-inch lexan core tubes. This sampler was used to collect sediment

core samples from the MUs.

A ponar sampler was mounted on the 26-foot Pontoon Boat and was used primarily to collect the

sediment grab samples from RS1 and RS2. Sediment samples collected were thoroughly

homogenized before filling sample jars for analysis.

The sampling boat was equipped with a 40-horsepower motor, gasoline powered air compressor, and steel

spuds anchoring. The sampling boat was also equipped with additional life vest(s), portable light, portable

horn, guardrail, and tool box for emergency maintenance. Additional equipment on the workboat included

an ‘A-frame’ with an electric winch for core removal and to operate the ponar. The boat and the sampling

equipment were operated by GLEC. Prior to leaving the site, Wood cleaned the sample preparation area

on the boat and properly disposed of all used sample tubes and sample investigative derived waste (IDW).

3.6.1 Sediment Sampling Procedures

The sampling crew navigated to each pre-determined sampling location. The water depth at each sample

location was measured using steel rods and confirmed with the Garmin depth finder on the GLEC vessel.

Water depth was then corrected to the LWD, and the data obtained were used to determine the amount of

shoaling at each sample location. If a lack of shoaling was present at the pre-determined location, the

vessel navigated through the MU to find a location where shoaling was present and provided adequate

sediment for sample collection. The coordinates of the actual sample location(s) were recorded in the GPS

unit and the latitude and longitude were recorded in the field notes and on the sediment coring/grab

sampling logs (Appendix A and Table 3).

Based on the SOW and field conditions, different sediment sampling techniques were used to recover

representative, undisturbed, sub-bottom sediment samples from shoaled sample locations. The thickness

of the sediment cores varied for each sample location depending on the amount of shoaling, and was

documented on the sediment core logs (Appendix A).




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Sediment core sampling (MU locations) Based on the project depth and the amount of shoaling, the amount of sediment sample required to obtain

a representative sample of the shoaled material was calculated. The thickness of sediment collected varied

at each station depending on the project depth and nature of the sediment. Thickness of the sediment

cores ranged between 1.7 ft. and 6 ft. At each location, the sampling tube was lowered to the top of the

sediments, and then it was driven into the sediment using hydraulic force. The sediment cores were driven

below the project depth to refusal to ensure adequate sample recovery was obtained, which varied based

on sampling location.

Once retrieved, each sample core was capped and transferred to the designated sample preparation area

located on-shore. At the sample processing area, each sediment core was cut open and the sediment was

described in accordance with the Unified Soil Classification System (USCS) by a professional geoscientist.

The sediment was removed from the core, placed in the sampling pan, unwanted materials such as wood,

stones, and/or shells were removed, and the sample was thoroughly homogenized. Physical properties of

the sediment made through visual observations during field activities are summarized in Appendix A and

Table 3.The sediment samples were then placed in labeled sample jars and placed into a sturdy cooler

with ice for shipment to the laboratory.

Sediment grab sampling (RS locations)

Grab samples were collected at RS sample locations using a ponar sampler. In addition, within MU4, at

sample location MU4-C2, four (4) attempts were made to collect a sediment core, however, due to fine

sand/hard material, a core was unable to be collected and a sample was collected with the ponar sampler.

At each sample location, the ponar sampler was lowered to the top of the sediments to collect undisturbed

sediment from the surface; the sampler retrieved as many aliquots of sediment until sufficient sample

volume was obtained for chemical analyses. Sediment was removed from the sampler, placed in the

sampling pan, unwanted materials such as wood, stones, and/or shells were removed, the sample was

thoroughly homogenized, and described in accordance with the USCS. The sediment predominantly

consisted of fine sand with trace gravel. The sediment samples were then placed in labeled sample jars

and placed into a sturdy cooler with ice for shipment to the laboratory.

3.6.2 Volatile Organic Compound Sample Collection Procedures

Sediment samples collected for volatile organic compound (VOC) analysis were collected in general

accordance with United States Environmental Protection Agency (USEPA) Method 5035. This technique

requires collection of a sample that is as undisturbed as possible and is immediately preserved to limit loss

of volatiles from the sample as summarized below:




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Sub-samples of sediment from the retrieved sediment core or grab samples were collected immediately

upon homogenizing to avoid volatile loss of contaminants of concern. Two (2) pre-prepared and pre-

weighted vials containing 5 milliliters (ml) of methanol and a magnetic stir bar were used for VOC sample

preservation. For each sample, an aliquot of approximately 5 grams of sediment was weighed using an

electronic field scale and put into the vials. An additional unpreserved container was filled for each VOC

sample to complete dry-weight analysis per the analytical method. The samples collected were weighed

at CT Labs before analysis to confirm sample volume weight(s).

3.6.3 Water Sampling Procedures

The background water samples and the water samples used for the elutriate procedure were collected

using an electric pump and tubing. The tubing was lowered to the depth of half the water column (between

the surface water level and top of sediment) to collect the sample. Three (3) cube containers (1-gallon

cube container each) were filled with water from each MU for elutriate procedure. The six (6) background

samples were collected directly into the appropriate laboratory-provided containers. All water samples were

immediately placed in a sturdy cooler with ice until delivered to the laboratory. Temperature was obtained

in the field using a YSI-556 MPS (Table 4).

3.6.4 Decontamination Procedures

All non-disposable sampling equipment was decontaminated after each sample was collected. The

decontamination procedure included scrubbing and rinsing the sampling pans, and spoons with Alconox™

and site water followed by a distilled water rinse. New gloves were used for each sample location. IDW

consisted of used gloves, paper towels, and spent lexan core tubes and were placed in black trash bags

and deposited in a trash receptacle for disposal in a Type II landfill.

3.6.5 Field Logs

The field logs were filled out completely at each sample location; sample location coordinates and pertinent

sample information was recorded. Sediment coring and grab sampling logs, site water sampling logs, and

sediment sampling logs are included in Appendix A.

3.6.6 Sample Containers and Sample Preservation

All sediment samples were collected in pre-cleaned, laboratory supplied containers with Teflon® linings.

The background water samples were collected in laboratory supplied jars containing preservative as

mentioned below. The elutriate water samples were collected in pre-cleaned, laboratory supplied one-

gallon plastic cube containers.




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The sediment sample jars were placed in sealable plastic storage bags and wrapped in bubble wrap to

protect against breakage. All samples were then cooled to 4 C (degrees Celsius) using ice inside the

coolers. The samples were stored in darkness, except transiently, during handling operations. The COC

was maintained during sampling activities and transportation to the laboratory. Based on the proposed

analytical parameters, none of the samples (sediment or water) required additional chemical or physical

preservation other than ice and darkness with the exception of the background water sample and sediment

collected for VOCs analysis (as described in Section 3.6.2). The background water samples required

preservation for various analysis as summarized below:

125ml – Plastic container preserved with sulfuric acid (H2SO4) for Ammonia, chemical oxygen demand (COD), and Phosphorus;

250ml – Plastic container preserved with nitric acid (HNO3) for Priority Pollutant Metals; 1 Liter – Amber glass container preserved with hydrochloric acid (HCl) for Oil and Grease; and (3) 40 ml - vials preserved with HCl for VOCs.

Dissolved Iron samples were collected in unpreserved sample containers and filtered and preserved in the laboratory.

3.6.7 Sample Custody

COC protocol over samples was maintained at all times. The signed COC was stored in a sealable plastic

bag and attached to the cooler lid. The coolers with the sediment and water samples were shipped

overnight via Federal Express carrier to CT Labs. CT Labs maintained COC protocol when forwarding

sample aliquots to Mi-Tech for particle size distribution analysis.




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4.0 PERFORMANCE DATA REVIEW

Wood collected a total of nineteen (19) sediment samples (including one field duplicate) and fourteen (14)

water samples (including three [3] trip blanks and one [1] equipment blank) between August 13 and 16,

2019 from the Burns Waterway Harbor Site. Wood submitted the samples to CT Labs via overnight courier.

CT Labs logged in samples as sample delivery groups (SDG) 147285, 147337, 147378, and 147405 and

analyzed the samples for the parameters using USEPA and Standard Methods for Examination of Water

and Wastewater (SM) methods:

Organics Analyses

Polychlorinated Biphenyls (PCBs) by USEPA 8082A;

VOCs - Methyl tert-butyl ether (MTBE), Benzene, Toluene, Ethylbenzene, and Xylenes (BTEX) by USEPA 8260C; and/or

Polycyclic Aromatic Hydrocarbon (PAHs)/Semi-Volatile Organic Compounds (SVOCs) by USEPA 8270-selected ion monitoring (SIM).

Organics Analyses

Hexavalent Chromium by USEPA 3060A/7199 or 7196A;

Total Phosphorus by USEPA 365.1 or 365.4;

Ammonia Nitrogen by USEPA 350.1;

Oil and Grease by USEPA 1664A or 9071B;

Priority Pollutant Metals by Methods 6010D/7470A or 7471B;

COD by USEPA 410.4;

Total Organic Carbon (TOC) by Lloyd Kahn/USEPA 9060A;

Percent Total Solids by USEPA 8000C;

E Coli by SM 9223B;

Alkalinity by USEPA 310.2;

Hardness by SM 2340B;

pH by USEPA 9040C or 9045D;

Total dissolved solids (TDS) by SM 2540C;

Total suspended solids (TSS) by SM2540D; and/or

Total Volatile Solids (TVS) by SM 2540G

Additionally, sediment samples were subcontracted to MI-Tech, and were analyzed for particle size

distribution by ASTM International Method D 422. Laboratory analytical reports are located in Appendix B.

With USACE approval, the elutriation for samples from MU1 and MU2 were prepared in the laboratory using

the Inland Testing Manual – Modified (Aerated) Elutriate Preparation procedure and the elutriation for




Page 4-2

samples from MU3 and MU4 were prepared using the Inland Testing Manual – Standard Elutriate

Preparation procedure. Samples BWH-19-MU1-E1 and BWH-19-MU3-E1 required additional settling time

(4-hours) to obtain sufficient sample volume for analysis.

4.1 Chemical Data Review

Wood reviewed the chemical data generated during this project in accordance with USACE - EM 200-1-10

Guidance for Evaluating Performance-Based Chemical Data (Appendix C). The review was performed

based on the Data Quality Objectives (DQOs) of the project; screening of sediment and water data to

characterize sediment material in the Burns Waterway Harbor for the purpose of estimating environmental

impacts of disposal of the dredged material. The precision, accuracy, completeness, representativeness,

comparability, and sensitivity were reviewed for the compounds of concern in the environmental media of

interest and are evaluated with respect to acceptance limits prescribed by project DQOs.

Based on the review performed, the data generated during this project are appropriate for the use intended,

unless otherwise noted in the validation report. The analysis performed was complete and in accordance

with the SOW and Work Plan. Sample representativeness was not assessed as the SOW directed the

number and location of the samples. The precision and accuracy of the data, including data qualifiers, is

discussed in Section 4.2 and Section 4.3.

4.2 Quality Assurance / Quality Control

Data quality refers to the level of uncertainty associated with a particular data point. All elements of the

sampling event, from the sampling design through the laboratory analysis and reporting, affect the quality

of the data. Data quality associated with environmental measurement is a function of the sampling plan

rationale and procedures used to collect the samples, as well as, the analytical methods and

instrumentation used in making the measurements. Uncertainty cannot be eliminated from environmental

data. However, quality assurance programs effective in measuring uncertainty in data are employed to

monitor and control excursions from the desired data quality objectives.

Sources of uncertainty traced to the sampling component are poor sampling plan design, incorrect sample

handling, faulty sample transportation, and inconsistent use of standard operating procedures. The most

common sources of uncertainty that can be traced to the analytical component of the total measurement

system are problems associated with calibration and cross-contamination. To address this, the laboratory

performs the following laboratory QA/QC procedures:

Laboratory terms concerning quality control include:

Method Blank (BLK) (applies to whole batch)

Laboratory Control Sample (LCS) (applies to whole batch)




Page 4-3

Laboratory Control Duplicate Sample (LCSD) (applies to whole batch)

MS (only applies to the solid matrix spiked)

MSD (only applies to the solid matrix spiked)

Relative Percent Difference (RPD)

Field terms concerning quality control include:

Field Duplicate (FD)

Equipment Blank (EB)

Trip Blank (TB)

BLKs are used to monitor for contamination introduced by the laboratory during sample preparation and

analysis. The MBs are aliquots of analyte-free matrix that is processed by the laboratory using exactly the

same procedures as the field samples.

LCS and LCSD are used to determine the laboratories ability to successfully perform an analytical method

in an interference-free matrix and is measured by percent recoveries. LCS and LCSD are aliquots of

analyte-free matrix spiked with the analytes of interest for an analytical method. The spiked matrix is then

processed through the same preparation and analytical procedures as the samples they accompany.

MS/MSD samples measure percent recovery and precision and are an indicator of the laboratories ability

to successfully recover an analyte in the matrix of a specific sample or closely related sample matrices.

The MS/MSD are prepared in the laboratory by adding known amounts of the analytes of interest for an

analytical method, or a representative subset of those analytes, to an aliquot of sample. The spiked sample

is then processed through the same extraction, concentration, cleanup, and analytical procedure as the

unspiked samples in an analytical batch. The laboratory also spiked the organic samples with surrogate

organic compounds as part of the laboratory QA/QC procedures. The percent recovery equals the amount

detected divided by the amount added or spiked. RPD is the difference between the recovery for the MS

and the MSD or possibly as LCS and LCSD. QA/QC measures for this project include submitting MS/MSD

sample (BWH-19-MU1-C3) for internal laboratory QA/QC testing.

The FD is a sample prepared in the field to assess field variability and is collected at the same location,

using the same sampling methods, in the sample process. For this project, the FD was collected from

BWH-19-MU2-C1 and was labeled as “blind” as the laboratory would not know the primary/ ‘parent’ sample.

The EB is a sample that has been collected to ensure decontamination efforts are made and to ensure

there is not cross-contamination between samples from non-dedicated sampling equipment during the

sample collection process. For this project, analyte free water was pumped through non-dedicated




Page 4-4

sampling equipment (e.g., sample pump) directly into the container in the field, preserved and shipped to

the laboratory with the field samples (EB-1).

The TB is a clean sample of a matrix that is taken from the laboratory to the sampling site and transported

back to the laboratory without having been exposed to the sampling procedures. For this project, TB-

081319, TB-081419, and TB-081619 were submitted with samples delivery groups. The QA/QC review is

documented in Appendix C.

4.3 Data Qualifiers

Wood reviewed 2,265 data points from the field sampling effort. Qualifications concluded during the

validation process include:

10 data points were rejected because the analyte could not be recovered from the LCS or LCSD;

33 data points were qualified due to associated laboratory and/or equipment blanks; and

269 data points were qualified as estimated or estimated non-detect because of holding time

issues, low LCS recoveries, imprecision between laboratory duplicate results, high or low MS

recoveries, low surrogate recoveries, analyte concentrations less than the level of quantitation

(LOQ), and/or imprecision between primary (parent sample) and field duplicate results.

The detailed data qualifiers results are presented in the Data Validation Report (Appendix C) and have

been incorporated into the summary tables described in Section 5.0. It should be noted samples exceeded

hold times largely due to weather delays and sample submittal schedule. However, discussions where held

between USACE, PARS, and Wood regarding exceeding holding times due to the weather conditions and

sample collection/submittal schedule; USACE suggested to proceed with sample collection despite the

holding time issues.




Page 5-1

5.0 RESULTS

Chemical data results for field sediment samples are summarized in Table 5 and Table 6. Chemical data

results for site water and elutriate samples are presented in Table 7 and Table 8. Validation qualifiers have

been shown in these summaries. Table 9 presents the particle size analysis summary table for sediment

samples collected. Results from chemical analysis of sediments and water samples collected from the MU

and RS samples collected from the Burns Waterway Harbor indicate:

Sediments

Metals were detected in all samples collected, having the highest concentrations of iron, ranging

from 2,420 mg/kg (milligram per kilogram) in MU4 to 17,800 mg/kg in MU3;

MU3 generally contained the highest concentrations of metals compared to other MUs, whereas

MU4 contained the lowest concentrations;

Hexavalent Chromium was the only metal not detected in sediment samples;

Mercury was detected in MU1, MU2, MU3, and RS2, ranging in concentrations from

0.0039 mg/kg at RS1-G1 to 0.062 mg/kg at MU2-C1.

On average, ammonia nitrogen was the highest in MU3;

TOC was highest in MU2;

E. Coli was detected ranging from 5.97 most probable number of viable cells per gram of solid

(MPN/gTS) at MU3-C1 to 2,240 MPN/gTS at MU4-C2. E. Coli was also detected at RS1 with a

concentration of 2,270 MPN/gTS at RS1-G3;

PAHs were detected in samples collected from both the MUs and RSs, but contained the highest

concentrations in MU2;

Benzene and Toluene were the only VOCs detected, predominantly within MU2; and

Aroclor 1248 was the only PCB detected in samples collected, was detected in samples collected

from MU1, MU2, and MU3 and ranged from 29 milligram per kilogram (μg/kg) at MU2-C2 to 100

μg/kg at MU2-C1.

Water

All metals, with the exception of hexavalent chromium, mercury, and silver were detected in

samples collected from MUs and RSs;

In general, MU2 site water contained the fewest detections of metals or inorganics, but had the

highest concentrations detected in the elutriate sample;

VOCs or PCBs were not detected in site water collected from the MUs or RSs; and




Page 5-2

Low concentrations of SVOCs were detected in site water; MU2 contained the greatest number of

SVOCs detected, and pyrene was the only analyte detected in all site water and elutriate samples

collected.




Page 6-1

6.0 REFERENCES

ASTM, 1995. ASTM Standards. D2488-09a Standard Practice for Description and Identification of Soils (Visual-Manual Procedure), 1975.

USEPA. Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, USEPA publication SW-846, Third Edition, Final Updates I (1993, II (1995), IIA (1994), IIB (1995), III (1997), IIIA (1999), IIIB (2005), IV (2008), and V (2015).

IGLD, 1985. Brochure on The International Great Lakes Datum. 1985.

PARS, 2019. Final Burns Waterway Harbor Sediment and Water Sampling and Analysis Work Plan, August 2019.




FIGURES

_̂

Site Location

Burns Waterway Harbor, Indiana

Date: 6/19/2019Proj:

Figure 1

Prepared By: DJ Checked By: CK

_̂_̂

¯

Burns Waterway Harbor

MU1

MU3

MU2

MU4

Dredged Material Management Unit Locations


Date: 9/26/2019

Figure 2


_̂

¯

Contract:W912QR-14-D-0006Delivery Order: W912P619FCX10

RS1

RS2

Ogden Dunes

Disposal Area

Open WaterDisposal Area

Document Path: G:\USArmyCorp\a_MXD_PDFs\Burns Waterway Harbor\Work Plan\ReferenceAndDisposalAreas.mxd

Reference Site and Disposal Area Locations


Date: 10/14/2019

Figure 3


Disposal Area - Approximate LimitsReference Site_̂

010020050

Feet

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¯0 4,000

Feet

Burns Small Boat Harbor

Contract:W912QR-14-D-0006Delivery Order: W912P619FCX10

!(

!(

!(

!(

!(

!(

!( !(

!(

!(

!(

!(

Dredged Material Management Unit Sample Locations


Date: 9/25/2019Contract:W912QR-14-D-0006Delivery Order: W912P619FCX10

Figure 4


!(_̂

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!(

!(

!(

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RS2-G1

RS2-G2

RS2-G3

RS1-G1

RS1-G2RS1-G3

Document Path: G:\USArmyCorp\a_MXD_PDFs\Burns Waterway Harbor\Work Plan\PARSLOGO\ReferenceSiteSampleLocations.mxd

Reference Site Sample LocationsBurns Waterway Harbor, Indiana

Date: 9/26/2019Contract:W912QR-14-D-0006Delivery Order: W912P619FCX10

Figure 5


!( Sample Location_̂

010020050

Feet

Service Layer Credits: Source: Esr i, D ig italGlobe, GeoEye, Earthstar Geographic s, CNES /A irbus DS , USDA, US GS , Aer oGRID, IGN, and the GIS Us er Communi tySources: Esri , HERE , Gar min, Intermap, increment P Corp., GEBCO, USGS, FAO, NPS, NRCA N, GeoB ase, IGN, Kadaster NL, Ordnance Survey, Esri Japan, METI, Es ri China (HongKong), swisstopo, © OpenS treetMap contributor s, and the GIS User Comm unity

¯0 4,000

Feet

Burns Small Boat Harbor

U.S. Army Corps of Engineers, Chicago DistrictBurns Waterway Harbor

Sediment and Water Sampling and Analysis Contract No. W912QR-14-D-0006

Delivery Order No. W912P619FCX10 ber 2019

TABLES

Table 1Sample Summary

Burns Waterway HarborPort of Indiana, Porter County, Indiana

BWH-19-MU1-C1, BWH-19-MU1-C2, and BWH-19-MU1-C3 Sediment Core

BWH-19-MU1-W1 Site Water

BWH-19-MU1-E1Elutriate (composite sediment sample prepared from the three (3) sediment cores collected from MU1)










BWH-19-RS1-G1, BWH-19-RS1-G2, and BWH-19-RS1-G3, Sediment Grab

BWH-19-RS1-W1 Site Water

BWH-19-RS2-G1, BWH-19-RS2-G2, and BWH-19-RS2-G3 Sediment Grab

BWH-19-RS2-W2 Site Water

BWH-19-MU1-C3 MS/MSD Sediment MS/MSDFD-1 Sediment duplicateEB-1 Water equipment blankTB-081319, TB-081419, TB-081619 Water trip blank

Reference Site (RS)RS1

RS2

Quality Assurance/Quality Control (QA/QC) Samples

Dredging Management Unit (MU) AreaMU1

MU2

MU3

MU4

1 of 1

Table 2Weather Conditions


Day Date Sky ConditionAverage

Temperature (°F)

Wind Speed and Direction

Tuesday August 13, 2019 Partly Sunny 74 5-10 mph (N)

Wednesday August 14, 2019 Sunny 72 5-10 mph (N)

Thursday August 15, 2019 Mostly Sunny 71 15-20 mph (N)

Friday August 16, 2019 Mostly Sunny 5-10 mph (S)

1 of 1

Table 3Sediment Sample Information


Sample LocationWater

Elevation (msl)

Water Elevation (ft LWD)

Water Depth (ft)

Project Depth (LWD)

Maximum Sample

Depth (ft)

Sample Collected

(ft)

General Sediment Sample Material

BWH-19-MU1-C1 41°38'18.21709"N 87°09'38.57081"W 582.14 +4.7 30.7 27.0 3.0 3.0 Clay, gray, few medium sand

BWH-19-MU1-C2 41°38'20.71842"N 87°09'38.92510"W 582.14 +4.7 30.7 27.0 3.0 3.0 Silty-clay, gray

BWH-19-MU1-C3 41°38'24.44208"N 87°09'39.70549"W 582.14 +4.7 30.5 27.0 3.5 2.0 Clayey silt, gray, few fine sand

BWH-19-MU2-C1 41°38'11.21446"N 87°08'58.56886"W 582.06 +4.6 29.9 27.0 3.7 3.7 Silt, dark gray to gray, some sand

BWH-19-MU2-C2 41°38'17.66421"N 87°08'57.46432"W 582.06 +4.6 30.2 27.0 3.4 3.4 Silt and sand, gray, trace fine sand

BWH-19-MU2-C3 41°38'13.69256"N 87°08'58.44888"W 582.06 +4.6 30.2 27.0 3.4 3.0 Sandy silt to silty clay, gray to brown

BWH-19-MU3-C1 41°38'40.95932"N 87°09'32.53410"W 582.14 +4.7 31.5 28.0 3.2 3.2Silt to silty clay, gray, few medium sand

BWH-19-MU3-C2 41°38'41.76512"N 87°09'28.03219"W 582.17 +4.7 31.5 28.0 3.2 3.2 Clay, gray, few medium sand

BWH-19-MU3-C3 41°38'45.08534"N 87°09'15.10754"W 582.17 +4.7 31.4 28.0 3.3 3.3Sandy silt to silty clay, dark gray to gray

BWH-19-MU4-C1 41°38'48.02212"N 87°08'42.64950"W 581.98 +4.5 30.6 30.0 5.9 1.7Fine sand, gray, trace medium sand, trace gravel

BWH-19-MU4-C2 41°38'57.89282"N 87°08'15.12890"W 581.98 +4.5 29.5 30.0 7.0 Grab* Fine sand, tan, trace gravel

BWH-19-MU4-C3 41°39'08.08659"N 87°07'48.78968"W 581.98 +4.5 26 30.0 9.5 2.0 Fine sand, brown, trace gravel

BWH-19-RS1-G1 41°37'35.88735"N 87°13'14.91929"W 581.98 +4.5 12 NA NA Grab Fine sand, tan, trace gravel

BWH-19-RS1-G2 41°37'44.62611"N 87°13'04.49186"W 581.98 +4.5 23.8 NA NA GrabFine sand, tan w/some black grain, few gravel

BWH-19-RS1-G3 41°37'40.12005"N 87°12'51.22427"W 581.98 +4.5 17.0 NA NA Grab Fine sand, tan, trace gravel


BWH-19-RS2-G2 41°38'56.93802"N 87°10'16.27744"W 581.98 +4.5 52.6 NA NA GrabFine sand, tan w/some gray, trace gravel


ft - Feet

LWD - Low Water Datum

msl - Mean Sea Level

* - Sediment too hard for core collection, Ponar sampler used to collect sample

Sample Location (Actual)

1 of 1

Table 4Water Sample Information


Sample LocationSample

Temperature (°C)

BWH-19-MU1-W1 (BWH-19-MU1-C2) 41°38'20.71842"N 87°09'38.92510"W 23.87

BWH-19-MU2-W2 (BWH-19-MU2-C2) 41°38'17.66421"N 87°08'57.46432"W 23.47

BWH-19-MU3-W3 (BWH-19-MU3-C2) 41°38'41.76512"N 87°09'28.03219"W 23.88

BWH-19-MU4-W4 (BWH-19-MU4-C2) 41°38'57.89282"N 87°08'15.12890"W 24.26

BWH-19-RS1-W1 (BWH-19-RS1-G1) 41°37'35.88735"N 87°13'14.91929"W 23.77

BWH-19-RS2-W2 (BWH-19-RS2-G3) 41°39'08.01511"N 87°10'02.93248"W 24.00

°C - Degrees Celsius

Sample Location (Actual)

1 of 1

Table 5Sediment Chemical Analytical Results - Inorganics


Management UnitSample ID

Sample DateUnits

% Total Solids % 67.6 59.4 55.4 64.4 66.3 67.7 77 62 59.5 61.8Total Volatile Solids gVS/gTS 0.0228 0.0304 0.0324 0.0361 0.0328 0.0255 0.0232 0.0238 0.0266 0.0281pH S.U. 7.25 J 7.32 J 7.39 J 8.44 J 8.68 J 7.93 J 8.16 J 6.89 J 7.48 J 7.29 JE. Coli MPN/g_TS 13.8 4 U 4 U 3 U 3 U 3 U 3 U 5.97 3 U 3 UOil and Grease mg/kg 360 U 410 U 363 J 1320 884 548 J 449 J 269 J 420 U 559 JAmmonia Nitrogen mg/kg 33.5 39.5 66 8.7 8.97 70.7 J 4.16 80.6 J 83.9 J 68COD mg/kg 4150 47700 J 58100 84700 J 67200 J 24000 43900 21000 61300 51200Phosphorus mg/kg 198 J 202 J 229 J 148 J 157 J 175 J 111 J 235 J 268 J 236 JTotal Organic Carbon mg/kg 25300 45100 32200 51600 48200 45400 34200 33300 30700 33300Hexavalent Chromium mg/kg 0.16 U 0.16 UJ 0.16 U 0.25 U 0.24 U 0.24 U 0.2 U 0.16 U 0.16 U 0.16 UMercury mg/kg 0.018 0.032 0.033 0.062 J 0.032 J 0.022 0.018 0.03 0.031 0.031Aluminum mg/kg 5730 5950 5180 3190 J 1330 J 2680 M 2480 6840 7360 4630Arsenic mg/kg 4.5 4.9 4.4 4.3 2.9 3.2 3 5 5.4 4.4Barium mg/kg 34.8 36.6 34.2 28.4 22.1 21.4 19.4 39.5 44.4 30.7Cadmium mg/kg 0.03 U 0.034 U 0.038 U 0.21 0.3 0.056 J 0.21 0.033 U 0.035 U 0.033 UChromium mg/kg 13.8 17.3 23.2 25.7 16 17.4 15.3 18.8 23.1 21.8Copper mg/kg 13.7 16.6 18.1 39.5 32.4 18.9 J 25.7 17.2 19.2 15.0Iron mg/kg 14400 15600 M 15000 11500 J 6760 J 9510 M 8600 16400 17800 13700Lead mg/kg 11.3 14.6 Y 18.1 25.1 16.4 10.7 11.2 14.5 17.6 18.4Nickel mg/kg 15.8 16.6 J 14.1 9.6 J 4.8 J 7.5 7.3 19 19.8 12.6Selenium mg/kg 0.3 U 0.15 Q 0.11 B 0.48 J 0.33 J 0.18 J 0.14 J 0.33 U 0.35 U 0.18 BSilver mg/kg 0.74 0.83 0.83 0.078 J 0.08 J 0.092 J 0.083 J 0.85 0.93 0.74Zinc mg/kg 46.3 60.8 81.2 87.7 76.9 54.9 57.4 57.4 71.4 71.6

* E. coli Result is greater than result displayed

Analyte

% - Percent

gVS/gTS - Grams of Volatile Solids to grams of Total Solids.

mg/kg - Milligram per Kilogram

Notes:

J - The result is an estimated quantity. The associated numerical value is the approximate concentration in the sample.

U - The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.

B - A target analyte was detected in an associated blank QC sample. The detected sample result is less than five times the concentration detected in the blank.

COD - Chemical Oxygen Demand

MPN/gTS - Most probable number of viable cells per gram of solid.

M - Matrix spike and/or matrix Spike Duplicate recovery outside acceptance limits.

Q - The result was both B and J flagged during validation.

Y - Replicate/Duplicate precision outside of range.

Bold - Analyte detected above quantitation limit

8/14/2019 8/14/2019 8/14/2019 8/13/2019 8/13/2019 8/13/2019 8/13/2019 8/14/2019 8/15/2019 8/15/2019

MU1 MU2 MU3FD-1 BWH-19-MU2-C2 BWH-19-MU2-C3 BWH-19-MU3-C1 BWH-19-MU3-C2 BWH-19-MU3-C3BWH-19-MU1-C1 BWH-19-MU1-C2 BWH-19-MU1-C3 BWH-19-MU2-C1

1 of 2

Table 5Sediment Chemical Analytical Results - Inorganics



Sample DateUnits

% Total Solids %Total Volatile Solids gVS/gTSpH S.U.E. Coli MPN/g_TSOil and Grease mg/kgAmmonia Nitrogen mg/kgCOD mg/kgPhosphorus mg/kgTotal Organic Carbon mg/kgHexavalent Chromium mg/kgMercury mg/kgAluminum mg/kgArsenic mg/kgBarium mg/kgCadmium mg/kgChromium mg/kgCopper mg/kgIron mg/kgLead mg/kgNickel mg/kgSelenium mg/kgSilver mg/kgZinc mg/kg

* E. coli Result is greater than result displayed

Analyte

% - Percent

gVS/gTS - Grams of Volatile Solids to grams of Total Solids.

mg/kg - Milligram per Kilogram

Notes:


U - The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.


COD - Chemical Oxygen Demand

MPN/gTS - Most probable number of viable cells per gram of solid.



Y - Replicate/Duplicate precision outside of range.


83 78.4 81.7 78.1 79.1 77.5 77.2 78.4 80.10.024 0.0016 0.0026 0.0018 0.0031 0.0043 0.0059 0.0059 0.00639.66 J 8.94 J 7.81 J 8.87 J 8.56 J 8.94 J 8.47 J 8.33 J 8.42 J

2 UJ 2240 J 2 UJ 1300 J 751 J 2270 J 11.2 J 64.5 J 330 J300 U 214 J 169 J 165 J 310 U 320 U 320 U 310 U 300 U

6 U 6.3 U 6.1 U 6.4 U 6.3 U 6.4 U 6.3 U 2.57 J 6.2 U40400 1910 1280 1210 2160 1730 5490 11600 166044.4 J 65.8 J 92.7 J 91.5 J 133 J 175 J 185 J 176 J 68.4 J6010 614 2230 5940 5490 15300 17700 20700 42100.16 U 0.16 U 0.16 U 0.16 U 0.16 U 0.16 U 0.16 U 0.16 U 0.16 U

0.0051 U 0.0055 U 0.0054 U 0.0054 U 0.0058 U 0.0057 U 0.0039 J 0.0061 J 0.0054 U14600 711 496 572 658 642 943 1130 5070.49 U 1 J 1.2 1 1 0.95 J 3.8 4.4 2.6124 6.3 4 4.7 4.5 4.2 11.5 12.2 7.3

0.025 U 0.027 U 0.025 U 0.026 U 0.026 U 0.027 U 0.027 U 0.025 U 0.025 U23.5 3 1.6 1.6 2.1 2.1 3.6 4.8 2.20.69 B 0.64 B 1.5 J 0.74 B 0.64 B 1.4 1.6 1.7 0.69 B6460 2570 2420 M 2250 2930 2710 7870 8440 49406.6 2 2 1.7 2.2 2.2 8 9 5.32.2 1.8 1.6 1.6 1.8 1.8 4.5 4.9 3.1

0.89 B 0.084 B 0.11 B 0.26 U 0.26 U 0.27 U 0.14 B 0.25 U 0.25 U0.4 0.061 J 0.063 J 0.062 J 0.055 J 0.052 J 0.35 0.39 0.18

13.2 12.1 9.2 9.6 8.3 10.9 37.5 44.1 26.5

8/16/2019 8/16/2019 8/16/2019 8/16/2019 8/16/2019

RS2

8/16/2019 8/16/2019 8/16/2019 8/16/2019

MU4 RS1BWH-19-RS2-G3BWH-19-MU4-C2 BWH-19-MU4-C3 BWH-19-RS1-G1 BWH-19-RS1-G2 BWH-19-RS1-G3 BWH-19-RS2-G1 BWH-19-RS2-G2BWH-19-MU4-C1

2 of 2

Table 6Sediment Chemical Analytical Results - VOCs, PAHs, PCBs



Sample DateUnits

VOCsBenzene μg/kg 49 U 39 U 86 U 17 J 31 U 27 U 25 U 39 U 53 U 63 UEthylbenzene μg/kg 49 U 39 U 86 U 23 U 31 U 22 U 25 U 39 U 53 U 63 Um & p-Xylene μg/kg 97 U 78 U 170 U 45 U 61 U 54 U 50 U 77 U 110 U 130 UMethyl tert-butyl ether μg/kg 97 U 78 U 170 U 45 U 61 U 54 U 50 U 77 U 110 U 130 Uo-Xylene μg/kg 49 U 39 U 86 U 23 U 31 U 27 U 25 U 39 U 53 U 63 UToluene μg/kg 97 U 78 U 83.3 J 24.5 J 32 J 54 U 50 U 77 U 110 U 130 UPAHs1-Methylnaphthalene μg/kg 13.4 16.5 23.2 78.9 92.4 35.9 33.3 19.5 18.4 J 24.02-Methylnaphthalene μg/kg 18.6 27 48 170 196 76.9 66.8 34.4 36.0 J 45.0Acenaphthene μg/kg 6.83 10.2 16.4 96.1 101 27.2 40.4 13.8 13.1 J 23.7Acenaphthylene μg/kg 5.94 6.01 32.2 90.6 90.3 29.1 36.3 72.1 16.4 J 25.7Anthracene μg/kg 18.5 21.7 71.9 243 267 108 118 157 42.9 J 82.6Benzo(a)anthracene μg/kg 38.4 70 237 605 721 288 295 409 180 J 216Benzo(a)pyrene μg/kg 35.5 60.1 210 469 570 230 230 373 144 J 169Benzo(b)fluoranthene μg/kg 60.6 94.8 342 605 772 308 299 506 227 J 270Benzo(g,h,i)perylene μg/kg 49.4 58.9 181 361 437 178 178 250 117 J 143Benzo(k)fluoranthene μg/kg 15.3 30.7 85.7 165 193 88.7 89.3 130 62.3 J 68.2Chrysene μg/kg 46.3 72.8 259 514 631 275 273 407 174 J 218Dibenzo(a,h)anthracene μg/kg 11.5 8.32 45.1 108 121 47.6 58 70.1 32.8 J 37.0Fluoranthene μg/kg 71.8 118 519 1010 1080 444 478 410 291 J 386Fluorene μg/kg 15.2 26.1 57.3 193 207 74.1 102 33.7 44.3 J 51.9Indeno(1,2,3-cd)pyrene μg/kg 31.1 44.5 159 300 367 148 152 232 104 J 122Naphthalene μg/kg 14.5 25.8 58.5 504 526 118 206 122 41.1 J 83.5Phenanthrene μg/kg 62.3 87.3 337 876 891 394 439 174 186 J 275Pyrene μg/kg 66.2 107 394 815 863 356 384 332 266 J 284PCBsAroclor-1016 μg/kg 29 U 33 U,Y 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1221 μg/kg 29 U 33 U 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1232 μg/kg 29 U 33 U 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1242 μg/kg 29 U 33 U 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1248 μg/kg 35.1 J 71.4 54 100 J 33.9 J 29 J 38.3 42.9 J 40.4 J 46.4 JAroclor-1254 μg/kg 29 U 33 U 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1260 μg/kg 29 U 33 U,Y 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1262 μg/kg 29 U 33 U 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 UAroclor-1268 μg/kg 29 U 33 U 36 U 31 U 29 U 29 U 26 U 32 U 34 U 32 U


μg/kg - Microgram per Kilogram

VOCs - Volatile Organic CompoundsPAHs - Polycyclic Aromatic HydrocarbonsPCBs - Polychlorinated Biphenyls

J - The result is an estimated quantity. The associated numerical value is the approximate concentration in the sample.U - The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.

Y - Replicate/Duplicate precision outside acceptance limits.

8/14/2019

Notes:

Analyte8/13/2019 8/13/2019 8/13/2019 8/13/20198/14/2019 8/14/2019 8/15/2019 8/15/2019

MU1 MU2 MU3BWH-19-MU3-C1 BWH-19-MU3-C2 BWH-19-MU3-C3BWH-19-MU2-C3FD-1BWH-19-MU1-C1

8/14/2019BWH-19-MU1-C2 BWH-19-MU1-C3 BWH-19-MU2-C1 BWH-19-MU2-C2

1 of 2

Table 6Sediment Chemical Analytical Results - VOCs, PAHs, PCBs



Sample DateUnits

VOCsBenzene μg/kgEthylbenzene μg/kgm & p-Xylene μg/kgMethyl tert-butyl ether μg/kgo-Xylene μg/kgToluene μg/kgPAHs1-Methylnaphthalene μg/kg2-Methylnaphthalene μg/kgAcenaphthene μg/kgAcenaphthylene μg/kgAnthracene μg/kgBenzo(a)anthracene μg/kgBenzo(a)pyrene μg/kgBenzo(b)fluoranthene μg/kgBenzo(g,h,i)perylene μg/kgBenzo(k)fluoranthene μg/kgChrysene μg/kgDibenzo(a,h)anthracene μg/kgFluoranthene μg/kgFluorene μg/kgIndeno(1,2,3-cd)pyrene μg/kgNaphthalene μg/kgPhenanthrene μg/kgPyrene μg/kgPCBsAroclor-1016 μg/kgAroclor-1221 μg/kgAroclor-1232 μg/kgAroclor-1242 μg/kgAroclor-1248 μg/kgAroclor-1254 μg/kgAroclor-1260 μg/kgAroclor-1262 μg/kgAroclor-1268 μg/kg


μg/kg - Microgram per Kilogram

VOCs - Volatile Organic CompoundsPAHs - Polycyclic Aromatic HydrocarbonsPCBs - Polychlorinated Biphenyls

J - The result is an estimated quantity. The associated numerical value is the approximate concentration in the sample.U - The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.


Notes:

Analyte

29 U 33 U 29 U 29 U 27 U 32 U 28 U 32 U 26 U29 U 33 U 29 U 29 U 27 U 32 U 28 U 32 U 26 U58 U 66 U 57 U 58 U 54 U 64 U 56 U 64 U 51 U58 U 66 U 57 U 58 U 54 U 64 U 56 U 64 U 51 U29 U 33 U 29 U 29 U 27 U 32 U 28 U 32 U 26 U58 U 66 U 57 U 58 U 54 U 64 U 56 U 64 U 51 U

1.4 J 0.95 J 1.2 U 1.3 U 1.2 UJ 1.3 U 1.38 J 1.88 J 0.703 J2.76 1.23 J 1.2 U 1.3 U 1.2 UJ 0.901 J 1.83 J 2.73 0.877 J3.5 1.3 U 1.2 U 1.3 U 1.2 UJ 1.3 U 2.26 J 3.36 1.2 U

0.827 J 0.541 J 1.2 U 1.3 U 1.2 UJ 1.3 U 0.783 J 1.02 J 1.2 U9.58 1.66 J 1.2 U 1.3 U 1.2 UJ 1.3 U 5.77 8.72 1.29 J27.6 9.51 1.2 U 1.3 U 1.2 UJ 1.3 U 16.3 25.5 9.2121 7.6 1.2 U 5.63 4.91 J 5.01 10.8 16.3 7.38

26.4 9.91 4.27 6.9 4.59 J 5.28 14.8 25.7 8.0614.7 8.16 1.2 U 1.3 U 6.84 J 1.3 U 10.5 13.8 8.6410.2 2.46 J 0.809 J 2.48 J 0.984 J 1.21 J 4.19 J 7.45 2.31 J21.9 4.49 1.13 J 2.42 J 1.03 J 1.66 J 19.1 31.3 5.281.2 U 1.3 U 1.2 U 1.3 U 1.2 UJ 1.3 U 1.2 U 7.68 6.9153 9.7 1.94 J 3.98 J 1.73 J 3.28 J 34.4 56 8.69

4.43 1.36 J 1.2 U 1.3 U 1.2 UJ 1.3 U 3.97 7.2 1.2 U14.2 8.05 1.2 U 1.3 U 6.8 J 1.3 U 8.99 12.5 8.5110.9 1.86 J 0.885 J 1.02 J 0.898 J 1.14 J 4.79 5.5 1.03 J37.2 3.31 J 2.4 U 2.5 U 2.4 UJ 2.5 U 16.9 29.3 1.75 J40.4 8.25 2.46 J 4.14 J 2.36 J 3.38 J 34.2 51.4 9.66

24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U24 U 25 U 24 U 26 U 25 U 25 U 25 U 25 U 25 U

8/16/2019 8/16/2019

RS2BWH-19-RS2-G3

8/16/2019 8/16/2019BWH-19-RS1-G3 BWH-19-RS2-G1 BWH-19-RS2-G2

8/16/2019 8/16/2019 8/16/2019BWH-19-MU4-C3 BWH-19-RS1-G1

8/16/2019 8/16/2019

MU4 RS1BWH-19-MU4-C1 BWH-19-MU4-C2 BWH-19-RS1-G2

2 of 2

Table 7Water Chemical Analytical Results - Inorganics, VOCs, and PCBs


LocationSample ID

Sample DateSample Type

Units

pH S.U. 8.36 J 8.12 J 8.03 J 8.37 J 8.43 J 8.03 J 8.42 J 8.41 J 8.36 J 8.69 JOil and Grease mg/L 2.9 U 3.2 U 2.8 U 1.5 J 1.8 J 3.1 U 1.9 J 2.9 U 2.8 U 1.7 BHexavalent Chromium μg/L 12 U, M 12 U 12 U, M 12 U 12 U 12 U 12 U 12 U 12 U 12 UAmmonia Nitrogen mg/L 0.1 U 4.3 0.1 U 7.2 0.1 U 6.5 J 0.1 U 0.3 0.1 U 0.1 UAlkalinity mg/L 120 120 120 160 120 160 120 130 120 120COD mg/L 35 U 21 J 35 U, M, Y 17 J 35 U 29 J 35 U 24 J 35 U 35 UPhosphorus mg/L 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 UTotal Dissolved Solids mg/L 170 240 180 270 180 200 150 190 180 170Total Suspended Solids mg/L 2 UJ 2 UJ 2 U 24 2 UJ 2.2 J 2 UJ 43 2 UJ 2 UJMercury μg/L 0.06 U 0.06 U 0.06 U 0.06 U 0.06 U 0.06 U 0.06 U 0.06 U 0.06 U 0.06 UAluminum μg/L 25.4 J 359 6.7 J 1490 J 23.5 J 192 12.6 J 451 14.4 B 11.9 BArsenic μg/L 12 U 12 U 12 UJ 5.3 J 12 U 6.1 J 12 U 12 U 12 U 12 UBarium μg/L 20.8 56.4 12.2 J 50.3 21.5 64.9 21.2 61.1 20.6 B 21.4 BCadmium μg/L 1 U 1 U 1 UJ 0.34 J 1 U 1 U 1 U 1 U 1 U 1 UChromium μg/L 0.84 B 2 U 2 UJ 4.3 1.4 B 2 U 0.79 B 2 U 0.74 J 1.3 JCopper μg/L 3.5 U 4.5 J 3.5 UJ 5.8 J 4.3 J 2 J 1.2 J 5.6 J 3.5 U 3.5 UIron μg/L 50 U 538 50 UJ 2090 M 16.8 J 260 50 U 357 50 U 50 ULead μg/L 2 U 2.3 J 2 UJ 5.7 2 U 1.4 J 2 U 1.7 J 2 U 2 UNickel μg/L 3 U 3 U 3 UJ 2.2 J 3 U 1 J 3 U 3 U 3 U 3 USelenium μg/L 6.5 U 6.5 U 6.5 UJ 6.5 U 6.5 U 6.5 U 6.5 U 2.7 J 6.5 U 3.6 BSilver μg/L 2 U 2 U 2 UJ 2 U 2 U 2 U 2 U 2 U 2 U 2 UZinc μg/L 1.7 J 11.9 5 UJ 14.8 3 J 5 U 5 U 16.9 5 U 5 UTotal Hardness mg/L 130 110 81 Y 160 140 140 140 140 130 140Dissolved Iron μg/L 50 U 33.3 J 50 UJ 50 UJ 50 U 50 U 50 U 50 U 50 U 50 U

Benzene S.U. 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UEthylbenzene μg/L 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 Um & p-Xylene μg/L 1.2 U 1.2 U 1.2 U 1.2 U 1.2 U 1.2 U 1.2 U 1.2 U 1.2 U 1.2 UMethyl tert-butyl ether μg/L 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 Uo-Xylene μg/L 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 UToluene μg/L 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U 0.6 U

Aroclor-1016 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1221 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1232 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1242 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1248 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1254 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1260 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1262 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 UAroclor-1268 μg/L 0.3 U 0.31 U 0.3 U 0.3 U 0.3 U 0.3 U 0.3 U 0.29 U 0.3 U 0.3 U

S.U - Standard Unit

mg/L - Milligram per Liter

VOCs - Volatile Organic Compounds

SVOC - Semi-Volatile Organic Compounds

PCBs - Polychlorinated Biphenyls

μg/kg - Microgram per Liter


U - The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.UJ - The analyte was analyzed for, but was not detected. The reported quantitation limit is approximate and may be inaccurate or imprecise.




Inorganics

VOCs

PCBs

Notes:



RS2

Analyte

MU1 MU2 MU3 MU4

Site Water Elutriate Site Water Site Water Site Water Site Water Site WaterElutriate Elutriate Elutriate

RS1

8/16/2019BWH-19-MU1-W1 BWH-19-MU1-E1 BWH-19-MU2-W2 BWH-19-MU2-E1 BWH-19-MU3-W3 BWH-19-MU3-E1 BWH-19-MU4-W4 BWH-19-MU4-E1 BWH-19-RS1-W1 BWH-19-RS2-W2

8/14/2019 8/20/2019 8/14/2019 8/20/2019 8/16/20198/14/2019 8/19/2019 8/13/2019 8/19/2019

1 of 1

Table 8Water Analytical Results - SVOCs


LocationSample ID


Units1,1'-Biphenyl μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U1,2,4,5-Tetrachlorobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U1,2,4-Trichlorobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U1,2-Dichlorobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U1,3-Dichlorobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U1,4-Dichlorobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U2,3,4,6-Tetrachlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2,4,5-Trichlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2,4,6-Trichlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2,4-Dichlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2,4-Dimethylphenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2,4-Dinitrophenol μg/L 5 U 5.2 U 5 U 5.1 U 5 U 5.1 U 5.1 U 5 U 5 U 5 U2,4-Dinitrotoluene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U2,6-Dichlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2,6-Dinitrotoluene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U2-Chloronaphthalene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U2-Chlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2-Methylphenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U2-Nitroaniline μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U2-Nitrophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U3 & 4-Methylphenol μg/L 3.6 U 3.7 U 3.6 U 3.6 U 3.6 U 3.6 U 3.7 U 3.6 U 3.6 U 3.6 U3,3'-Dichlorobenzidine μg/L 1 UJ 1 UJ 1 UJ 1 UJ 1 UJ 1 UJ 1 UJ 1 UJ 1 UJ 1 UJ3-Nitroaniline μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U4,6-Dinitro-2-methylphenol μg/L 5 U 5.2 U 5 U 5.1 U 5 U 5.1 U 5.1 U 5 U 5 U 5 U4-Bromophenyl-phenyl ether μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U4-Chloro-3-methylphenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U4-Chloroaniline μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U4-Chlorophenyl-phenyl ether μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U4-Nitroaniline μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U4-Nitrophenol μg/L 5 U, Y 5.2 U, Y 5 U, Y 5.1 U, Y 5 U, Y 5.1 U, Y 5.1 U, Y 5 U, Y 5 U, Y 5 U, YAcetophenone μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UAniline μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 UAtrazine μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UAzobenzene & 1,2-Diphenylhydra μg/L 0.8 U 0.82 U 0.8 U 0.81 U 0.8 U 0.81 U 0.82 U 0.8 U 0.8 U 0.8 UBenzaldehyde μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UBenzidine μg/L 50 R 52 R 50 R 51 R 50 R 51 R 51 R 50 R 50 R 50 RBenzoic acid μg/L 25 U, Z 26 U, Z 25 U, Z 25 U, Z 25 U, Z 25 U, Z 26 U, Z 25 U, Z 25 U, Z 25 U, ZBenzyl alcohol μg/L 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, YBis(2-chloroethoxy)methane μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UBis(2-chloroethyl)ether μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UBis(2-chloroisopropyl)ether μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UBis(2-ethylhexyl)phthalate μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 2.7 1 U 1 UButylbenzylphthalate μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UCaprolactam μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UCarbazole μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UDi-n-butylphthalate μg/L 2 U 2.6 J 2 U 2 U 2 U 2 U 2 U 1.2 J 2 U 2 UDi-n-octylphthalate μg/L 1 U 1 U 1 U 1.2 J 1 U 1 U 1 U 0.67 J 1 U 1 UDibenzofuran μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UDiethylphthalate μg/L 1 U 0.62 J 1 U 0.6 J 1 U 1 U 1 U 1 U 1 U 1 U

Site Water Site WaterElutriate Elutriate ElutriateAnalyte

MU1 MU2 MU3 MU4

Site Water Elutriate Site Water Site Water Site Water

BWH-19-MU1-W1 BWH-19-MU1-E1 BWH-19-MU2-W2 BWH-19-MU2-E1 BWH-19-MU3-W38/20/2019

RS1 RS2BWH-19-MU3-E1 BWH-19-MU4-W4 BWH-19-MU4-E1 BWH-19-RS1-W1 BWH-19-RS2-W2

8/14/2019 8/20/2019 8/16/2019 8/16/20198/14/2019 8/19/2019 8/13/2019 8/19/2019 8/14/2019

1 of 2

Table 8Water Analytical Results - SVOCs


LocationSample ID


UnitsSite Water Site WaterElutriate Elutriate Elutriate

Analyte

MU1 MU2 MU3 MU4

Site Water Elutriate Site Water Site Water Site Water

BWH-19-MU1-W1 BWH-19-MU1-E1 BWH-19-MU2-W2 BWH-19-MU2-E1 BWH-19-MU3-W38/20/2019

RS1 RS2BWH-19-MU3-E1 BWH-19-MU4-W4 BWH-19-MU4-E1 BWH-19-RS1-W1 BWH-19-RS2-W2

8/14/2019 8/20/2019 8/16/2019 8/16/20198/14/2019 8/19/2019 8/13/2019 8/19/2019 8/14/2019

Dimethylphthalate μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UHexachlorobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UHexachlorobutadiene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UHexachlorocyclopentadiene μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UHexachloroethane μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UIsophorone μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UN-Nitroso-di-n-propylamine μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UN-Nitrosodimethylamine μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UN-Nitrosodiphenylamine & Diphn μg/L 0.8 U 0.82 U 0.8 U 0.81 U 0.8 U 0.81 U 0.82 U 0.8 U 0.8 U 0.8 UN-Nitrosopyrrolidine μg/L 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 U 1 UNitrobenzene μg/L 0.4 U 0.41 U 0.4 U 0.4 U 0.4 U 0.4 U 0.41 U 0.4 U 0.4 U 0.4 UPentachlorophenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 UPhenol μg/L 2 U 2.1 U 2 U 2 U 2 U 2 U 2 U 2 U 2 U 2 UPyridine μg/L 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y 1 U, Y1-Methylnaphthalene μg/L 0.02 U 0.021 U 0.0083 J 0.0073 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U2-Methylnaphthalene μg/L 0.02 U 0.021 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UAcenaphthene μg/L 0.02 U 0.021 U 0.02 U 0.022 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UAcenaphthylene μg/L 0.02 U 0.021 U 0.02 U 0.0077 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UAnthracene μg/L 0.02 U 0.021 U 0.02 U 0.017 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UBenzo(a)anthracene μg/L 0.02 U 0.021 U 0.02 U 0.076 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UBenzo(a)pyrene μg/L 0.02 U 0.021 U 0.02 U 0.056 B 0.02 U 0.039 B 0.02 U 0.041 B 0.02 U 0.02 UBenzo(b)fluoranthene μg/L 0.02 U 0.035 B 0.02 U 0.067 B 0.02 U 0.033 B 0.02 U 0.037 B 0.02 U 0.02 UBenzo(g,h,i)perylene μg/L 0.02 U 0.057 0.02 U 0.067 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UBenzo(k)fluoranthene μg/L 0.02 U 0.021 U 0.02 U 0.016 J 0.02 U 0.02 U 0.02 U 0.010 J 0.02 U 0.02 UChrysene μg/L 0.02 U 0.021 U 0.02 U 0.036 B 0.02 U 0.02 U 0.02 U 0.0086 B 0.02 U 0.02 UDibenzo(a,h)anthracene μg/L 0.02 U 0.021 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UFluoranthene μg/L 0.02 U 0.014 J 0.0098 J 0.09 0.02 U 0.011 J 0.02 U 0.012 J 0.02 U 0.02 UFluorene μg/L 0.02 U 0.010 J 0.02 U 0.034 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UIndeno(1,2,3-cd)pyrene μg/L 0.02 U 0.021 U 0.02 U 0.062 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UNaphthalene μg/L 0.02 U 0.021 U 0.02 U 0.02 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UPhenanthrene μg/L 0.02 U 0.021 U 0.02 U 0.063 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 UPyrene μg/L 0.012 B 0.023 B 0.017 B 0.077 B 0.022 B 0.023 B 0.014 B 0.015 B 0.015 B 0.016 B

μg/kg - Microgram per Liter

R - The data are unusable. The sample results are rejected due to serious deficiencies in meeting QC criteria. The analyte may or may not be present in the sample.

SVOC - Semi-Volatile Organic Compounds

Notes:

B - A target analyte was detected in an associated blank QC sample. The detected sample result is less than five times the concentration detected in the blank.J - The result is an estimated quantity. The associated numerical value is the approximate concentration in the sample.

U - The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.UJ - The analyte was analyzed for, but was not detected. The reported quantitation limit is approximate and may be inaccurate or imprecise.


Z - Specified calibtation criteria was not met.


2 of 2

Table 9Sediment Grain Size Analysis



Sample DateUnits

0.75 % Finer 100 100 NA 100 100 100 NA NA NA NA#4 % Finer 98.8 99.7 100 98.9 99.4 99.2 100 100 100 100#10 % Finer 91.7 64.2 93.6 96.7 90.3 98.2 95.6 96.4 93.6 95.9#40 % Finer 90.5 93.9 93.3 65.5 88.8 94.9 94.4 96.1 93 95.6#200 % Finer 81.7 90.3 74.1 44.7 47.1 39.4 51 71.1 79.2 62.40.0319 mm % Finer 75.2 82.1 71.3 33.1 33.2 29.4 36.3 58.1 69.5 48.90.0206 mm % Finer 69.0 70.1 67.5 28.6 29.4 24.9 31 52.8 67.2 46.60.0122 mm % Finer 56.0 56.7 60.6 22.6 21.1 18.1 22.7 42.2 62.6 38.20.0088 mm % Finer 48.3 49.2 55.2 18.1 17.4 15.1 18.2 37.7 56.5 34.40.0062 mm % Finer 40.7 42.5 48.3 14.3 14.3 13.6 14.4 31.7 53.5 30.50.0031 mm % Finer 30.7 30.6 35.3 9.8 9.8 9.8 9.8 22.6 40.5 22.90.0013 mm % Finer 23.0 22.4 26.1 7.5 6.0 6.8 5.3 15.1 29.8 16

NA - Not Available

8/13/20198/14/2019 8/14/2019 8/14/2019 8/13/2019 8/13/2019

MU1 MU2 MU3BWH-19-MU3-C3BWH-19-MU1-C1 BWH-19-MU1-C2 BWH-19-MU1-C3 BWH-19-MU2-C1 FD-1 BWH-19-MU2-C2 BWH-19-MU2-C3 BWH-19-MU3-C1 BWH-19-MU3-C2

Notes:

% - Percent

8/13/2019 8/14/2019 8/15/2019 8/15/2019Opening Size

1 of 2

Table 9Sediment Grain Size Analysis



Sample DateUnits

0.75 % Finer#4 % Finer#10 % Finer#40 % Finer#200 % Finer0.0319 mm % Finer0.0206 mm % Finer0.0122 mm % Finer0.0088 mm % Finer0.0062 mm % Finer0.0031 mm % Finer0.0013 mm % Finer

NA - Not Available

Notes:

% - Percent

Opening Size

NA NA NA NA 100 100 100 100 100100 100 100 100 99 99.6 99.5 99.4 10097.8 99.5 99.3 100 95.5 99.1 98.5 98.1 98.181.9 98.1 96.3 98.4 92.4 98.3 93.0 96.2 2.01.8 2.1 1.0 0.3 2.7 1.4 6.6 15.6 1.71.7 1.7 1.8 2.2 1.2 1.3 2.6 3.0 1.31.7 1.7 1.8 2.2 1.2 1.3 2.6 2.6 1.31.7 1.7 1.8 2.2 1.2 1.3 2.2 2.2 1.31.7 1.3 1.8 1.8 1.2 1.3 2.2 2.2 1.31.3 1.3 1.8 1.3 0.8 1.3 2.2 2.2 1.31.3 1.3 1.8 1.3 0.8 0.9 1.7 1.3 1.31.3 1.3 1.7 1.3 0.8 0.9 1.7 1.3 1.3

MU4BWH-19-MU4-C1 BWH-19-MU4-C2 BWH-19-MU4-C3 BWH-19-RS2-G2 BWH-19-RS2-G3

RS2RS1BWH-19-RS1-G1 BWH-19-RS1-G2 BWH-19-RS1-G3 BWH-19-RS2-G1

8/16/20198/16/2019 8/16/2019 8/16/2019 8/16/2019 8/16/2019 8/16/20198/16/2019 8/16/2019

2 of 2




APPENDIX A FIELD SAMPLING AND SEDIMENT CORE LOGS




APPENDIX B LABORATORY REPORTS

ANALYTICAL SUMMARY REPORT

This report at a minimum contains the following information:

Analytical Report of Test Results Description of QC Qualifiers Chain of Custody (copy) Quality Control Summary (if applicable) Case Narrative (if applicable) Correspondence with Client (if applicable)

This report has been specifically prepared to satisfy project or program requirements. These results are in compliance with NELAC requirements for parameters where accreditation is required or available, unless otherwise noted in the case narrative.

1230 Lange Court Baraboo, WI 53913 608-356-2760

www.ctlaboratories.com

Page 1 of 25

Unless specifically stated to the contrary, soil/sediment/sludge sample results reported on a Dry Weight Basis

147285 - Page 1 of 142

Page 2 of 25Project Name: BURNS HARBOR

Contract #: 3300 Folder #: 147285

Project #: 3293191855.02.****

WOOD E&I SOLUTIONS, INC.

Project Phase: BURNS HARBOR, IN

ANALYTICAL SAMPLE DATA

JOHN RALSTON

SUITE 190Purchase Order #:

Project Name: BURNS HARBOR

Contract #:

Folder #: 46850 MAGELLAN DRIVE Date Received: 08/14/2019

Arrival Temperature: 4.3Report Date: 09/09/2019

NOVI, MI 48377


Reprint Date:Project #:Project Phase:

09/09/2019

BURNS HARBOR, IN3293191855.02.****147285

3293191855.02.****3300

CT LAB#: 315103

Result Units DL DODLOQ

RL DF Qualifier PrepDate/Time

AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1150

Analyte

Sample Description: BWH-19-MU2-C2

DODLOD

Client Sample #:

Inorganic Results

%67.7 8/15/19 BMMSolids, Percent 13:040.1 EPA 8000C0.1 1.000.10.1

gVS/gTS0.0255 8/19/19 CLBTotal Volatile Solids 14:35 SM 2540G1.000.0001

S.U.7.93 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS<3 8/14/19 CLBE. coli 15:45U3 9223B3 1.0033

mg/kg548 8/19/19 JLHOil and Grease 08/19/2019 14:00 14:00J740 EPA 9071B370 1.00740190

mg/kg70.7 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 18:48 ^J73 EPA 350.136 5.007312

mg/kg24000 8/26/19 HLBCOD 08/23/2019 12:00 16:072700 EPA 410.41200 1.002700530

mg/kg175 8/22/19 JLHPhosphorus 08/21/2019 12:00 15:23 ^J280 EPA 365.4140 1.0028051

mg/kg45400 8/26/19 TMGTotal Organic Carbon 15:58440 L-Kahn/9060A220 1.0044053

mg/kg<0.24 8/26/19 DGSHexavalent Chromium 08/23/2019 10:00 11:35U0.47 EPA 3060A/71990.24 1.000.470.10

Metals Results

mg/kg0.022 8/22/19 MDSMercury 08/20/2019 09:59 09:470.013 EPA 7471B0.0066 1.000.0130.0033

mg/kg2680 M 8/20/19 NAHAluminum 08/15/2019 11:30 05:560.37 EPA 6010D0.19 1.000.370.062

mg/kg3.2 8/20/19 NAHArsenic 08/15/2019 11:30 05:561.2 EPA 6010D0.62 1.001.20.20

mg/kg21.4 8/20/19 NAHBarium 08/15/2019 11:30 05:560.077 EPA 6010D0.039 1.000.0770.014


147285 - Page 2 of 142



Project #: 3293191855.02.****



CT LAB#: 315103



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1150

Analyte


DODLOD

Client Sample #:

mg/kg0.056 8/20/19 NAHCadmium 08/15/2019 11:30 05:56J0.062 EPA 6010D0.031 1.000.0620.0093

mg/kg17.4 8/20/19 NAHChromium 08/15/2019 11:30 05:560.22 EPA 6010D0.11 1.000.220.036

mg/kg18.9 8/20/19 NAHCopper 08/15/2019 11:30 05:560.62 EPA 6010D0.31 1.000.620.11

mg/kg9510 M 8/20/19 NAHIron 08/15/2019 11:30 05:562.8 EPA 6010D1.4 1.002.80.46

mg/kg10.7 8/20/19 NAHLead 08/15/2019 11:30 05:560.39 EPA 6010D0.19 1.000.390.062

mg/kg7.5 8/20/19 NAHNickel 08/15/2019 11:30 05:560.19 EPA 6010D0.093 1.000.190.032

mg/kg0.18 8/20/19 NAHSelenium 08/15/2019 11:30 05:56J0.62 EPA 6010D0.31 1.000.620.093

mg/kg0.092 8/20/19 NAHSilver 08/15/2019 11:30 05:56J0.15 EPA 6010D0.077 1.000.150.026

mg/kg54.9 8/20/19 NAHZinc 08/15/2019 11:30 05:560.46 EPA 6010D0.23 1.000.460.077

Organic Results

ug/kg<27 8/22/19 RLDBenzene 08/22/2019 09:05 19:38U54 EPA 8260C27 1.005412

ug/kg<22 8/22/19 RLDEthylbenzene 08/22/2019 09:05 19:38U54 EPA 8260C22 1.005412

ug/kg<54 8/22/19 RLDm & p-Xylene 08/22/2019 09:05 19:38U110 EPA 8260C54 1.0011027

ug/kg<54 8/22/19 RLDMethyl tert-butyl ether 08/22/2019 09:05 19:38U110 EPA 8260C54 1.0011017

ug/kg<27 8/22/19 RLDo-Xylene 08/22/2019 09:05 19:38U54 EPA 8260C27 1.00547.6

ug/kg<54 8/22/19 RLDToluene 08/22/2019 09:05 19:38U110 EPA 8260C54 1.0011017

% Recovery103 8/22/19 RLD1,2 Dichloroethane-d4 08/22/2019 09:05 19:38 EPA 8260C1.0013671

% Recovery101 8/22/19 RLDBromofluorobenzene 08/22/2019 09:05 19:38 EPA 8260C1.0011979

% Recovery100 8/22/19 RLDd8-Toluene 08/22/2019 09:05 19:38 EPA 8260C1.0011685

% Recovery100 8/22/19 RLDDibromofluoromethane 08/22/2019 09:05 19:38 EPA 8260C1.0011978

ug/kg<29 8/23/19 AJZAroclor-1016 08/20/2019 14:20 16:09U43 EPA 8082A29 1.00437.2

ug/kg<29 8/23/19 AJZAroclor-1221 08/20/2019 14:20 16:09U43 EPA 8082A29 1.004310



ug/kg29.0 P 8/26/19 AJZAroclor-1248 08/20/2019 14:20 20:35J43 EPA 8082A29 1.004310




147285 - Page 3 of 142



Project #: 3293191855.02.****



CT LAB#: 315103



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1150

Analyte


DODLOD

Client Sample #:



% Recovery76 8/23/19 AJZSurr: 2,4,5,6-TCMX 08/20/2019 14:20 16:09 EPA 8082A1.0013044

% Recovery90 8/23/19 AJZSurr: DCBP 08/20/2019 14:20 16:09 EPA 8082A1.0014154

ug/kg35.9 8/27/19 JJY1-Methylnaphthalene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.2


ug/kg27.2 8/27/19 JJYAcenaphthene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.5

ug/kg29.1 8/27/19 JJYAcenaphthylene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.90.89

ug/kg108 8/27/19 JJYAnthracene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.2

ug/kg288 8/27/19 JJYBenzo(a)anthracene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.5

ug/kg230 8/27/19 JJYBenzo(a)pyrene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.90.89

ug/kg308 8/27/19 JJYBenzo(b)fluoranthene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.2

ug/kg178 8/27/19 JJYBenzo(g,h,i)perylene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.90.77

ug/kg88.7 8/27/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 19:4512 EPA 8270D-SIM5.9 2.00121.8

ug/kg275 8/27/19 JJYChrysene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.90.65

ug/kg47.6 8/27/19 JJYDibenzo(a,h)anthracene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.90.62

ug/kg444 8/27/19 JJYFluoranthene 08/16/2019 16:00 19:4512 EPA 8270D-SIM5.9 2.00122.1

ug/kg74.1 8/27/19 JJYFluorene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.2

ug/kg148 8/27/19 JJYIndeno(1,2,3-cd)pyrene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.2

ug/kg118 8/27/19 JJYNaphthalene 08/16/2019 16:00 19:455.9 EPA 8270D-SIM3.0 2.005.91.5

ug/kg394 8/27/19 JJYPhenanthrene 08/16/2019 16:00 19:4512 EPA 8270D-SIM5.9 2.00123.2

ug/kg356 8/27/19 JJYPyrene 08/16/2019 16:00 19:4512 EPA 8270D-SIM5.9 2.00121.8

% Recovery54 8/27/19 JJYSurr: 2-Methylnaphthalene-d10 08/16/2019 16:00 19:45 EPA 8270D-SIM2.0015050

% Recovery64 8/27/19 JJYSurr: Fluoranthene-d10 08/16/2019 16:00 19:45 EPA 8270D-SIM2.0015050

Sub Lab Results

ATTACHED 9/3/19 SUBHydrometer 00:001.00


147285 - Page 4 of 142



Project #: 3293191855.02.****



CT LAB#: 315114



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1340

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.44 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1


mg/kg1320 8/19/19 JLHOil and Grease 08/19/2019 14:00 14:00770 EPA 9071B390 1.00780200

mg/kg8.70 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 18:53 ^7.8 EPA 350.13.9 5.007.81.3

mg/kg84700 M 8/27/19 HLBCOD 08/23/2019 12:00 14:0011000 EPA 410.45300 1.00110002300




Metals Results


mg/kg3190 8/20/19 NAHAluminum 08/15/2019 11:30 06:530.39 EPA 6010D0.19 1.000.390.064



mg/kg0.21 8/20/19 NAHCadmium 08/15/2019 11:30 06:530.064 EPA 6010D0.032 1.000.0640.0097



mg/kg11500 8/20/19 NAHIron 08/15/2019 11:30 06:532.9 EPA 6010D1.4 1.002.90.48






Organic Results


147285 - Page 5 of 142



Project #: 3293191855.02.****



CT LAB#: 315114



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1340

Analyte


DODLOD

Client Sample #:

ug/kg17.0 8/22/19 RLDBenzene 08/22/2019 09:05 20:05J45 EPA 8260C23 1.00459.9

ug/kg<23 8/22/19 RLDEthylbenzene 08/22/2019 09:05 20:05U45 EPA 8260C23 1.00459.9




ug/kg24.5 8/22/19 RLDToluene 08/22/2019 09:05 20:05J90 EPA 8260C45 1.009014









ug/kg100 8/26/19 AJZAroclor-1248 08/20/2019 14:20 20:5646 EPA 8082A31 1.004611







ug/kg78.9 8/27/19 JJY1-Methylnaphthalene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.1

ug/kg170 8/27/19 JJY2-Methylnaphthalene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.8

ug/kg96.1 8/27/19 JJYAcenaphthene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.8

ug/kg90.6 8/27/19 JJYAcenaphthylene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00152.3

ug/kg243 8/27/19 JJYAnthracene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.1

ug/kg605 8/27/19 JJYBenzo(a)anthracene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.8

ug/kg469 8/27/19 JJYBenzo(a)pyrene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00152.3


147285 - Page 6 of 142



Project #: 3293191855.02.****



CT LAB#: 315114



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1340

Analyte


DODLOD

Client Sample #:

ug/kg605 8/27/19 JJYBenzo(b)fluoranthene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.1

ug/kg361 8/27/19 JJYBenzo(g,h,i)perylene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00152.0

ug/kg165 8/27/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 20:0531 EPA 8270D-SIM15 5.00314.6

ug/kg514 8/27/19 JJYChrysene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00151.7

ug/kg108 8/27/19 JJYDibenzo(a,h)anthracene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00151.6

ug/kg1010 8/27/19 JJYFluoranthene 08/16/2019 16:00 20:0531 EPA 8270D-SIM15 5.00315.4

ug/kg193 8/27/19 JJYFluorene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.1

ug/kg300 8/27/19 JJYIndeno(1,2,3-cd)pyrene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.1

ug/kg504 8/27/19 JJYNaphthalene 08/16/2019 16:00 20:0515 EPA 8270D-SIM7.7 5.00153.8

ug/kg876 8/27/19 JJYPhenanthrene 08/16/2019 16:00 20:0531 EPA 8270D-SIM15 5.00318.4

ug/kg815 8/27/19 JJYPyrene 08/16/2019 16:00 20:0531 EPA 8270D-SIM15 5.00314.6



Sub Lab Results


CT LAB#: 315115



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1445

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.16 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1




147285 - Page 7 of 142



Project #: 3293191855.02.****



CT LAB#: 315115



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1445

Analyte


DODLOD

Client Sample #:


mg/kg43900 8/27/19 HLBCOD 08/23/2019 12:00 14:0011000 EPA 410.45000 1.00110002200




Metals Results














Organic Results








147285 - Page 8 of 142



Project #: 3293191855.02.****



CT LAB#: 315115



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1445

Analyte


DODLOD

Client Sample #:









ug/kg38.3 8/26/19 AJZAroclor-1248 08/20/2019 14:20 21:1738 EPA 8082A26 1.00388.9









ug/kg40.4 8/27/19 JJYAcenaphthene 08/16/2019 16:00 20:2612 EPA 8270D-SIM5.9 5.00123.0







ug/kg89.3 8/27/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 20:2624 EPA 8270D-SIM12 5.00243.5


ug/kg58.0 8/27/19 JJYDibenzo(a,h)anthracene 08/16/2019 16:00 20:2612 EPA 8270D-SIM5.9 5.00121.2



147285 - Page 9 of 142



Project #: 3293191855.02.****



CT LAB#: 315115



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1445

Analyte


DODLOD

Client Sample #:








Sub Lab Results


CT LAB#: 315116



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1200

Analyte

Sample Description: FD-1

DODLOD

Client Sample #:

Inorganic Results



S.U.8.68 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1


mg/kg884 8/19/19 JLHOil and Grease 08/19/2019 14:00 14:00750 EPA 9071B370 1.00760190


mg/kg67200 8/27/19 HLBCOD 08/23/2019 12:00 14:0012000 EPA 410.45700 1.00120002400





147285 - Page 10 of 142



Project #: 3293191855.02.****



CT LAB#: 315116



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1200

Analyte


DODLOD

Client Sample #:

Metals Results














Organic Results













147285 - Page 11 of 142



Project #: 3293191855.02.****



CT LAB#: 315116



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1200

Analyte


DODLOD

Client Sample #:












ug/kg196 8/27/19 JJY2-Methylnaphthalene 08/16/2019 16:00 20:4614 EPA 8270D-SIM7.1 5.00143.5

ug/kg101 8/27/19 JJYAcenaphthene 08/16/2019 16:00 20:4614 EPA 8270D-SIM7.1 5.00143.5







ug/kg193 8/27/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 20:4628 EPA 8270D-SIM14 5.00284.3


ug/kg121 8/27/19 JJYDibenzo(a,h)anthracene 08/16/2019 16:00 20:4614 EPA 8270D-SIM7.1 5.00141.5








147285 - Page 12 of 142



Project #: 3293191855.02.****



CT LAB#: 315116



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1200

Analyte


DODLOD

Client Sample #:



Sub Lab Results


CT LAB#: 315117



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte

Sample Description: BWH-19-MU2-W2

DODLOD

Client Sample #:

Inorganic Results

S.U.8.03 8/16/19 HLBpH 08:00 ÊPA 9040C1.00

mg/L<2.8 8/26/19 JLHOil and Grease 08/26/2019 09:00 09:00 Û10 EPA 1664A2.8 1.00101.4

ug/L<12 M 8/14/19 HLBHexavalent Chromium 11:17 Û24 EPA 7196A12 1.00246.0

mg/L<0.10 8/19/19 HLBAmmonia Nitrogen 13:03 Û0.20 EPA 350.10.10 1.000.200.022

mg/L120 8/23/19 SRWAlkalinity 11:05 ^30 EPA 310.215 1.00306.0

mg/L<35 M,Y 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515

mg/L<0.50 8/21/19 SRWPhosphorus 16:54 Û1.0 EPA 365.10.50 1.001.00.30

mg/L180 8/16/19 SERTotal Dissolved Solids 15:3010 SM 2540C10 1.001010

mg/L<2.0 8/15/19 SERTotal Suspended Solids 15:30U2.0 SM 2540D2.0 1.002.02.0

Metals Results

ug/L<0.060 8/23/19 MDSTotal Mercury 08/21/2019 14:51 09:25U0.12 EPA 7470A0.060 1.000.120.030

ug/L6.7 8/20/19 NAHTotal Aluminum 08/14/2019 13:01 00:53J36 EPA 6010D18 1.00366.0

ug/L<12 8/20/19 NAHTotal Arsenic 08/14/2019 13:01 00:53U24 EPA 6010D12 1.00244.0

ug/L12.2 Y 8/20/19 NAHTotal Barium 08/14/2019 13:01 00:531.8 EPA 6010D0.90 1.001.80.29

ug/L<1.0 8/20/19 NAHTotal Cadmium 08/14/2019 13:01 00:53U2.0 EPA 6010D1.0 1.002.00.30


147285 - Page 13 of 142



Project #: 3293191855.02.****



CT LAB#: 315117



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte


DODLOD

Client Sample #:

ug/L<2.0 8/20/19 NAHTotal Chromium 08/14/2019 13:01 00:53U4.0 EPA 6010D2.0 1.004.00.60

ug/L<3.5 8/20/19 NAHTotal Copper 08/14/2019 13:01 00:53U7.0 EPA 6010D3.5 1.007.01.2

ug/L<50 8/20/19 NAHTotal Iron 08/14/2019 13:01 00:53U100 EPA 6010D50 1.0010016

ug/L<2.0 8/20/19 NAHTotal Lead 08/14/2019 13:01 00:53U4.0 EPA 6010D2.0 1.004.01.4

ug/L<3.0 8/20/19 NAHTotal Nickel 08/14/2019 13:01 00:53U6.0 EPA 6010D3.0 1.006.01.0

ug/L<6.5 8/20/19 NAHTotal Selenium 08/14/2019 13:01 00:53U13 EPA 6010D6.5 1.00132.2

ug/L<2.0 8/20/19 NAHTotal Silver 08/14/2019 13:01 00:53U4.0 EPA 6010D2.0 1.004.00.70

ug/L<5.0 8/20/19 NAHTotal Zinc 08/14/2019 13:01 00:53U10 EPA 6010D5.0 1.00101.6

mg/L81 Y 8/20/19 NAHTotal Hardness 08/19/2019 13:01 00:530.41 SM2340B/6010D0.21 1.000.410.067

Organic Results

ug/L<1.0 8/20/19 RLDBenzene 18:18U2.0 EPA 8260C1.0 1.002.00.40

ug/L<0.60 8/20/19 RLDEthylbenzene 18:18U1.0 EPA 8260C0.60 1.001.00.30

ug/L<1.2 8/20/19 RLDm & p-Xylene 18:18U2.0 EPA 8260C1.2 1.002.00.70

ug/L<0.60 8/20/19 RLDMethyl tert-butyl ether 18:18U1.0 EPA 8260C0.60 1.001.00.30

ug/L<0.60 8/20/19 RLDo-Xylene 18:18U1.0 EPA 8260C0.60 1.001.00.26

ug/L<0.60 8/20/19 RLDToluene 18:18U1.0 EPA 8260C0.60 1.001.00.21

% Recovery110 8/20/19 RLD1,2 Dichloroethane-d4 18:18 EPA 8260C1.0011881

% Recovery99 8/20/19 RLDBromofluorobenzene 18:18 EPA 8260C1.0011485

% Recovery100 8/20/19 RLDd8-Toluene 18:18 EPA 8260C1.0011289

% Recovery97 8/20/19 RLDDibromofluoromethane 18:18 EPA 8260C1.0011980

ug/L<0.30 8/22/19 AJZAroclor-1016 08/20/2019 09:00 18:57U1.0 EPA 8082A0.30 1.001.00.11








147285 - Page 14 of 142



Project #: 3293191855.02.****



CT LAB#: 315117



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte


DODLOD

Client Sample #:





ug/L<0.40 8/23/19 JJY1,1'-Biphenyl 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.15

ug/L<0.40 8/23/19 JJY1,2,4,5-Tetrachlorobenzene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.17

ug/L<0.40 8/23/19 JJY1,2,4-Trichlorobenzene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.17

ug/L<0.40 8/23/19 JJY1,2-Dichlorobenzene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.18



ug/L<2.0 8/23/19 JJY2,3,4,6-Tetrachlorophenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.01.1

ug/L<2.0 8/23/19 JJY2,4,5-Trichlorophenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.01.1


ug/L<2.0 8/23/19 JJY2,4-Dichlorophenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.01.0

ug/L<2.0 8/23/19 JJY2,4-Dimethylphenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.00.82

ug/L<5.0 8/23/19 JJY2,4-Dinitrophenol 08/19/2019 12:00 12:25U10 EPA 8270D5.0 1.00101.5

ug/L<0.40 8/23/19 JJY2,4-Dinitrotoluene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.21



ug/L<0.40 8/23/19 JJY2-Chloronaphthalene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.18

ug/L<2.0 8/23/19 JJY2-Chlorophenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.00.87

ug/L<2.0 8/23/19 JJY2-Methylphenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.00.86

ug/L<0.40 8/23/19 JJY2-Nitroaniline 08/19/2019 12:00 12:25U2.0 EPA 8270D0.40 1.002.00.22

ug/L<2.0 8/23/19 JJY2-Nitrophenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.00.90

ug/L<3.6 8/23/19 JJY3 & 4-Methylphenol 08/19/2019 12:00 12:25U9.0 EPA 8270D3.6 1.009.01.4

ug/L<1.0 Q,Y 8/23/19 JJY3,3'-Dichlorobenzidine 08/19/2019 12:00 12:25U2.5 EPA 8270D1.0 1.002.50.66


ug/L<5.0 8/23/19 JJY4,6-Dinitro-2-methylphenol 08/19/2019 12:00 12:25U10 EPA 8270D5.0 1.00101.6


147285 - Page 15 of 142



Project #: 3293191855.02.****



CT LAB#: 315117



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte


DODLOD

Client Sample #:

ug/L<0.40 8/23/19 JJY4-Bromophenyl-phenyl ether 08/19/2019 12:00 12:25U2.0 EPA 8270D0.40 1.002.00.20

ug/L<2.0 8/23/19 JJY4-Chloro-3-methylphenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.00.80

ug/L<0.40 8/23/19 JJY4-Chloroaniline 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.12

ug/L<0.40 8/23/19 JJY4-Chlorophenyl-phenyl ether 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.18


ug/L<5.0 Y 8/23/19 JJY4-Nitrophenol 08/19/2019 12:00 12:25U10 EPA 8270D5.0 1.00101.1

ug/L<0.40 8/23/19 JJYAcetophenone 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.27

ug/L<2.0 8/23/19 JJYAniline 08/19/2019 12:00 12:25U4.0 EPA 8270D2.0 1.004.00.72

ug/L<0.40 8/23/19 JJYAtrazine 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.26

ug/L<0.80 8/23/19 JJYAzobenzene & 1,2-Diphenylhydra

08/19/2019 12:00 12:25U2.0 EPA 8270D0.80 1.002.00.52

ug/L<0.40 8/23/19 JJYBenzaldehyde 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.25

ug/L<50 8/23/19 JJYBenzidine 08/19/2019 12:00 12:25U100 EPA 8270D50 1.0010029

ug/L<25 Z 8/23/19 JJYBenzoic acid 08/19/2019 12:00 12:25U50 EPA 8270D25 1.005011

ug/L<1.0 Y 8/23/19 JJYBenzyl alcohol 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.54

ug/L<0.40 8/23/19 JJYBis(2-chloroethoxy)methane 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.19

ug/L<0.40 8/23/19 JJYBis(2-chloroethyl)ether 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.21

ug/L<0.40 8/23/19 JJYBis(2-chloroisopropyl)ether 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.22

ug/L<1.0 8/23/19 JJYBis(2-ethylhexyl)phthalate 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.44

ug/L<1.0 8/23/19 JJYButylbenzylphthalate 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.47

ug/L<1.0 8/23/19 JJYCaprolactam 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.19

ug/L<0.40 8/23/19 JJYCarbazole 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.12

ug/L<2.0 8/23/19 JJYDi-n-butylphthalate 08/19/2019 12:00 12:25U4.0 EPA 8270D2.0 1.004.00.67

ug/L<1.0 8/23/19 JJYDi-n-octylphthalate 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.49

ug/L<0.40 8/23/19 JJYDibenzofuran 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.19

ug/L<1.0 8/23/19 JJYDiethylphthalate 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.45

ug/L<1.0 8/23/19 JJYDimethylphthalate 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.54

ug/L<0.40 8/23/19 JJYHexachlorobenzene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.27

ug/L<0.40 8/23/19 JJYHexachlorobutadiene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.18


147285 - Page 16 of 142



Project #: 3293191855.02.****



CT LAB#: 315117



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte


DODLOD

Client Sample #:

ug/L<1.0 8/23/19 JJYHexachlorocyclopentadiene 08/19/2019 12:00 12:25U4.0 EPA 8270D1.0 1.004.00.26

ug/L<0.40 8/23/19 JJYHexachloroethane 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.22

ug/L<0.40 8/23/19 JJYIsophorone 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.18

ug/L<0.40 8/23/19 JJYN-Nitroso-di-n-propylamine 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.18

ug/L<1.0 8/23/19 JJYN-Nitrosodimethylamine 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.47

ug/L<0.80 8/23/19 JJYN-Nitrosodiphenylamine & Diphn 08/19/2019 12:00 12:25U2.0 EPA 8270D0.80 1.002.00.36

ug/L<1.0 8/23/19 JJYN-Nitrosopyrrolidine 08/19/2019 12:00 12:25U2.0 EPA 8270D1.0 1.002.00.21

ug/L<0.40 8/23/19 JJYNitrobenzene 08/19/2019 12:00 12:25U1.0 EPA 8270D0.40 1.001.00.16

ug/L<2.0 8/23/19 JJYPentachlorophenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.01.1

ug/L<2.0 8/23/19 JJYPhenol 08/19/2019 12:00 12:25U5.0 EPA 8270D2.0 1.005.00.48

ug/L<1.0 Y 8/23/19 JJYPyridine 08/19/2019 12:00 12:25U4.0 EPA 8270D1.0 1.004.00.62

% Recovery82 8/23/19 JJYSurr: 2,4,6-Tribromophenol 08/19/2019 12:00 12:25 EPA 8270D1.0014043

% Recovery78 8/23/19 JJYSurr: 2-Fluorobiphenyl 08/19/2019 12:00 12:25 EPA 8270D1.0011944

% Recovery47 8/23/19 JJYSurr: 2-Fluorophenol 08/19/2019 12:00 12:25 EPA 8270D1.0011919

% Recovery75 8/23/19 JJYSurr: Nitrobenzene-d5 08/19/2019 12:00 12:25 EPA 8270D1.0012044

% Recovery31 8/23/19 JJYSurr: Phenol-d5 08/19/2019 12:00 12:25 EPA 8270D1.001141

% Recovery97 8/23/19 JJYSurr: Terphenyl-d14 08/19/2019 12:00 12:25 EPA 8270D1.0013450

ug/L0.0083 8/26/19 JJY1-Methylnaphthalene 08/19/2019 12:00 18:58J0.040 EPA 8270D-SIM0.020 1.000.0400.0070

ug/L<0.020 8/26/19 JJY2-Methylnaphthalene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.011

ug/L<0.020 8/26/19 JJYAcenaphthene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0070

ug/L<0.020 8/26/19 JJYAcenaphthylene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0060

ug/L<0.020 8/26/19 JJYAnthracene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0060

ug/L<0.020 8/26/19 JJYBenzo(a)anthracene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0070

ug/L<0.020 8/26/19 JJYBenzo(a)pyrene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0060

ug/L<0.020 8/26/19 JJYBenzo(b)fluoranthene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0070

ug/L<0.020 8/26/19 JJYBenzo(g,h,i)perylene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0060

ug/L<0.020 8/26/19 JJYBenzo(k)fluoranthene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.010

ug/L<0.020 8/26/19 JJYChrysene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0070


147285 - Page 17 of 142



Project #: 3293191855.02.****



CT LAB#: 315117



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte


DODLOD

Client Sample #:

ug/L<0.020 8/26/19 JJYDibenzo(a,h)anthracene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0060

ug/L0.0098 8/26/19 JJYFluoranthene 08/19/2019 12:00 18:58J0.040 EPA 8270D-SIM0.020 1.000.0400.0090

ug/L<0.020 8/26/19 JJYFluorene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0090

ug/L<0.020 8/26/19 JJYIndeno(1,2,3-cd)pyrene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.0060

ug/L<0.020 8/26/19 JJYNaphthalene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.011

ug/L<0.020 8/26/19 JJYPhenanthrene 08/19/2019 12:00 18:58U0.040 EPA 8270D-SIM0.020 1.000.0400.011

ug/L0.017 B 8/26/19 JJYPyrene 08/19/2019 12:00 18:58J0.040 EPA 8270D-SIM0.020 1.000.0400.0070



CT LAB#: 315136



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019 1555

Analyte


DODLOD

Client Sample #:

Inorganic Results

8/14/19 NAHSample Filtration 15:00 SOP #PR0071.00

Metals Results

ug/L<50 8/20/19 NAHDissolved Iron 08/14/2019 11:33 03:55U100 EPA 6010C50 1.0010016

CT LAB#: 315137



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019

Analyte

Sample Description: BWH-19-MU2-E1

DODLOD

Client Sample #:

Organic Results

COMPLETE 8/19/19 DABSediment Elutriate Prep 15:35 LAB SOP1.00


147285 - Page 18 of 142



Project #: 3293191855.02.****



CT LAB#: 315168



AnalysisDate/Time

Analyst Method

Sampled: 08/13/2019

Analyte

Sample Description: TB-081319

DODLOD

Client Sample #:

Organic Results











CT LAB#: 317012



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.37 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1

mg/L1.5 8/26/19 JLHOil and Grease 08/26/2019 09:00 09:00 ^J10 EPA 1664A2.9 1.00101.4

ug/L<12 8/20/19 HLBHexavalent Chromium 11:48 Û24 EPA 7196A12 1.00246.0

mg/L7.2 9/4/19 HLBAmmonia Nitrogen 13:24 ^1.0 EPA 350.10.50 5.001.00.11


mg/L17 8/26/19 HLBCOD 08/22/2019 12:00 15:50 ^J75 EPA 410.435 1.007515


mg/L270 8/22/19 CLBTotal Dissolved Solids 11:1010 SM 2540C10 1.001010

mg/L24 8/20/19 GMJTotal Suspended Solids 17:452.0 SM 2540D2.0 1.002.92.9


147285 - Page 19 of 142



Project #: 3293191855.02.****



CT LAB#: 317012



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:

Metals Results


ug/L1490 8/22/19 NAHTotal Aluminum 08/21/2019 11:24 17:2436 EPA 6010D18 1.00366.0

ug/L5.3 8/22/19 NAHTotal Arsenic 08/21/2019 11:24 17:24J24 EPA 6010D12 1.00244.0

ug/L50.3 8/22/19 NAHTotal Barium 08/21/2019 11:24 17:241.8 EPA 6010D0.90 1.001.80.29

ug/L0.34 8/22/19 NAHTotal Cadmium 08/21/2019 11:24 17:24J2.0 EPA 6010D1.0 1.002.00.30

ug/L4.3 8/22/19 NAHTotal Chromium 08/21/2019 11:24 17:244.0 EPA 6010D2.0 1.004.00.60

ug/L5.8 8/22/19 NAHTotal Copper 08/21/2019 11:24 17:24J7.0 EPA 6010D3.5 1.007.01.2

ug/L2090 M 8/22/19 NAHTotal Iron 08/21/2019 11:24 17:24100 EPA 6010D50 1.0010016

ug/L5.7 8/22/19 NAHTotal Lead 08/21/2019 11:24 17:244.0 EPA 6010D2.0 1.004.01.4

ug/L2.2 8/22/19 NAHTotal Nickel 08/21/2019 11:24 17:24J6.0 EPA 6010D3.0 1.006.01.0



ug/L14.8 8/22/19 NAHTotal Zinc 08/21/2019 11:24 17:2410 EPA 6010D5.0 1.00101.6

mg/L160 8/22/19 NAHTotal Hardness 08/21/2019 11:24 17:240.41 SM2340B/6010D0.21 1.000.410.067

Organic Results












147285 - Page 20 of 142



Project #: 3293191855.02.****



CT LAB#: 317012



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:






























147285 - Page 21 of 142



Project #: 3293191855.02.****



CT LAB#: 317012



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:


















08/19/2019 12:00 14:33U2.0 EPA 8270D0.81 1.002.00.53













147285 - Page 22 of 142



Project #: 3293191855.02.****



CT LAB#: 317012



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:


ug/L1.2 8/23/19 JJYDi-n-octylphthalate 08/19/2019 12:00 14:33J2.0 EPA 8270D1.0 1.002.00.49


ug/L0.60 8/23/19 JJYDiethylphthalate 08/19/2019 12:00 14:33J2.0 EPA 8270D1.0 1.002.00.45





















ug/L0.0073 8/26/19 JJY1-Methylnaphthalene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.0071


ug/L0.022 8/26/19 JJYAcenaphthene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.0071

ug/L0.0077 8/26/19 JJYAcenaphthylene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.0061


147285 - Page 23 of 142



Project #: 3293191855.02.****



CT LAB#: 317012



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:

ug/L0.017 8/26/19 JJYAnthracene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.0061

ug/L0.076 8/26/19 JJYBenzo(a)anthracene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0071

ug/L0.056 B 8/26/19 JJYBenzo(a)pyrene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0061

ug/L0.067 B 8/26/19 JJYBenzo(b)fluoranthene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0071

ug/L0.067 8/26/19 JJYBenzo(g,h,i)perylene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0061

ug/L0.016 8/26/19 JJYBenzo(k)fluoranthene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.010

ug/L0.036 B 8/26/19 JJYChrysene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.0071


ug/L0.090 8/26/19 JJYFluoranthene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0091

ug/L0.034 8/26/19 JJYFluorene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.0091

ug/L0.062 8/26/19 JJYIndeno(1,2,3-cd)pyrene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0061

ug/L0.020 8/26/19 JJYNaphthalene 08/19/2019 12:00 21:23J0.040 EPA 8270D-SIM0.020 1.000.0400.011

ug/L0.063 8/26/19 JJYPhenanthrene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.011

ug/L0.077 B 8/26/19 JJYPyrene 08/19/2019 12:00 21:230.040 EPA 8270D-SIM0.020 1.000.0400.0071



CT LAB#: 317093



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 15:30

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results



147285 - Page 24 of 142

Notes: ^ Indicates the laboratory is NELAP accredited for this analyte by the indicated matrix and method. DL (detection limit), LOD (limit of detection), loq (limit of quantitation) as defined by most recent DOD QSM version.

Submitted by: Brett M. SzymanskiProject Manager 608-356-2760

DescriptionCodeQC Qualifiers

B Analyte detected in the associated Method Blank.C Toxicity present in BOD sample.D Diluted Out.E Safe, No Total Coliform detected.F Unsafe, Total Coliform detected, no E. Coli detected.G Unsafe, Total Coliform detected and E. Coli detected.H Holding time exceeded.I Incubator temperature was outside acceptance limits during test period.J Estimated value.L Significant peaks were detected outside the chromatographic window.M Matrix spike and/or Matrix Spike Duplicate recovery outside acceptance limits.N Insufficient BOD oxygen depletion.O Complete BOD oxygen depletion.P Concentration of analyte differs more than 40% between primary and confirmation analysis.Q Laboratory Control Sample outside acceptance limits.R See Narrative at end of report.S Surrogate standard recovery outside acceptance limits due to apparent matrix effects.T Sample received with improper preservation or temperature.U Analyte concentration was below detection limit.V Raised Quantitation or Reporting Limit due to limited sample amount or dilution for matrix background interference.W Sample amount received was below program minimum.X Analyte exceeded calibration range.Y Replicate/Duplicate precision outside acceptance limits.Z Specified calibration criteria was not met.

Current CT Laboratories Certifications

Wisconsin (WDNR) Chemistry ID# 157066030Wisconsin (DATCP) Bacteriology ID# 289Louisiana NELAP (primary) ID# ACC20190002Illinois NELAP Lab ID# 200073Kansas NELAP Lab ID# E-10368Virginia NELAP Lab ID# 460203Maryland Lab ID# 344ISO/IEC 17025-2005 A2LA Cert # 3806.01DoD-ELAP A2LA 3806.01GA EPD Stipulation ID ACC20190002

All samples were received intact and properly preserved unless otherwise noted. The results reported relate only to the samples tested. This report shall not be reproduced, except in full, without written approval of this laboratory. The Chain of Custody is attached.

This report has been specifically prepared to satisfy project or program requirements. These results are in compliance with NELAC requirements for the parameters where accreditation is required or available, unless noted in the case narrative.

147285 - Page 25 of 142

1230 Lange Court Baraboo , W I 53913 608 -356-2760

www.ctlabor atories .com

QC SUMMARY REPORT

WOOD E&I SOLUTIONS, INC. Project Name: BURNS HARBOR

Project #: 3293191855.02.****SDG #: 0 Folder #: 147285

Duplicate

08/14/2019Analytical Run #: Analysis Date:11:18Analysis Time:315388DC

CTLab #:Analyst:

Prep Batch #:

315117Parent Sample #:Prep Date/Time:

GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded

Analyte Units %Recovery

ControlLimits

RPDQualifier(s)QCsampleresult

Parentsampleresult

163505Method: SW7196

Hexavalent Chromium ug/L U 0 206.00 <6.00

Date Printed: 09/09/2019

CTLaboratories LLC 1230 Lange Court Baraboo, WI 53913 608-356-2760


147285 - Page 26 of 142



Lab Control Spike Water

08/14/2019Analytical Run #: Analysis Date:11:15Analysis Time:315132HLB

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Hexavalent Chromium ug/L 97 11197.10 90 ---100.0




147285 - Page 27 of 142



Method Blank Water


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Hexavalent Chromium ug/L U 126 0




147285 - Page 28 of 142



Matrix Spike Duplicate Water


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Hexavalent Chromium ug/L 113 111 2 2056.5 BDL 90 ---50.0




147285 - Page 29 of 142



Matrix Spike Water


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Hexavalent Chromium ug/L 111 111 2055.4 BDL 90 ---50.0




147285 - Page 30 of 142



Duplicate

08/15/2019Analytical Run #: Analysis Date:15:30Analysis Time:319374SER

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163541Method: SM2540D

Total Suspended Solids mg/L U 0 464.00 <4.00




147285 - Page 31 of 142



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08/15/2019Analytical Run #: Analysis Date:13:04Analysis Time:317153BMM

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SOILMatrix:

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163549Method: SW8000C

Solids, Percent % 0 867.4 67.7




147285 - Page 32 of 142



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163646Method: E350.1

Ammonia Nitrogen mg/L U 0 200.0220 <0.0220




147285 - Page 33 of 142





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163646Method: E350.1

Ammonia Nitrogen mg/L 103 1101.29 90 ---1.25




147285 - Page 34 of 142



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163646Method: E350.1

Ammonia Nitrogen mg/L U 0.100.022 0




147285 - Page 35 of 142





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163646Method: E350.1

Ammonia Nitrogen mg/L 107 120 3 201.34 BDL 80 ---1.25




147285 - Page 36 of 142



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163646Method: E350.1

Ammonia Nitrogen mg/L 104 120 201.30 BDL 80 ---1.25




147285 - Page 37 of 142



LOQ Check Water

08/20/2019Analytical Run #: Analysis Date:17:45Analysis Time:317347GMJ

CTLab #:Analyst:

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Total Suspended Solids mg/L 60 1101.200 90 ---2.000




147285 - Page 38 of 142



Duplicate

08/19/2019Analytical Run #: Analysis Date:18:50Analysis Time:317116

73206

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SOIL

HLB

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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg 1 2569.8 70.7




147285 - Page 39 of 142



Lab Control Spike Soil


73206

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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg 102 12012.7 80 ---12.5




147285 - Page 40 of 142



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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg U 8.28.2 0.00




147285 - Page 41 of 142



Matrix Spike Duplicate Soil


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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg 112 120 2 2582.9 BDL 80 ---74.0




147285 - Page 42 of 142



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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg 100 12081.9 <12.2 80 ---74.5




147285 - Page 43 of 142



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147285 - Page 44 of 142





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147285 - Page 45 of 142



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147285 - Page 46 of 142





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147285 - Page 47 of 142



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147285 - Page 48 of 142




08/21/2019Analytical Run #: Analysis Date:16:50Analysis Time:317547SRW

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163717Method: E365.1

Phosphorus mg/L 96 1103.85 90 ---4.00




147285 - Page 49 of 142



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163717Method: E365.1

Phosphorus mg/L U 0.500.30 0




147285 - Page 50 of 142





73238

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163744Method: E365.408/21/201912:00

Phosphorus mg/kg 102 1101020 90 ---1000




147285 - Page 51 of 142



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163744Method: E365.408/21/201912:00

Phosphorus mg/kg U 12026 0.00




147285 - Page 52 of 142



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163789Method: E310.2

Alkalinity mg/L 1 20119 120




147285 - Page 53 of 142





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163789Method: E310.2

Alkalinity mg/L 102 110382.0 90 ---375.0




147285 - Page 54 of 142



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163789Method: E310.2

Alkalinity mg/L 103 11031.00 90 ---30.00




147285 - Page 55 of 142



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163789Method: E310.2

Alkalinity mg/L U 156 0




147285 - Page 56 of 142




08/26/2019Analytical Run #: Analysis Date:09:22Analysis Time:320574TMG

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163804Method: LYDKHN

Total Organic Carbon mg/kg 90 113358000 84 ---400000




147285 - Page 57 of 142



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Total Organic Carbon mg/kg U 15036 0




147285 - Page 58 of 142



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163838Method: E410.408/22/201912:00

COD mg/L U 0 2015.0 <15.0




147285 - Page 59 of 142





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163838Method: E410.408/23/201912:00

COD mg/L 98 110393.0 90 ---400.0




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163838Method: E410.408/23/201912:00

Total COD mg/L U 3515 0




147285 - Page 61 of 142





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163838Method: E410.408/22/201912:00

COD mg/L 111 110 1 20165 BDL 90 ---148




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163838Method: E410.408/22/201912:00

COD mg/L 110 110163 BDL 90 ---148




147285 - Page 63 of 142



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163842Method: E410.408/23/201912:00

COD mg/kg 19 4070200 84700




147285 - Page 64 of 142





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163842Method: E410.408/23/201912:00

COD mg/kg 98 1001950 90 ---2000




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163842Method: E410.408/23/201912:00

COD mg/kg U 3815 0




147285 - Page 66 of 142





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163842Method: E410.408/23/201912:00

COD mg/kg 0 110 13 3081700 84700 90 ---23600




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163842Method: E410.408/23/201912:00

COD mg/kg 9 11086700 84700 90 ---22100




147285 - Page 68 of 142





73155

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163908Method: SW166408/19/201914:00

Oil and Grease mg/kg 93 121 203720 68 ---4000




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163908Method: SW166408/19/201914:00

Oil and Grease mg/kg U 127127 0




147285 - Page 70 of 142





73284

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163925Method: SW166408/26/201909:00

Oil and Grease mg/L 98 114 3439.00 78 ---40.00




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163925Method: SW166408/26/201909:00

Oil and Grease mg/L U 5.01.4 0




147285 - Page 72 of 142





73271

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163949Method: SW719908/23/201910:00

Hexavalent Chromium mg/kg 92 1201.83 80 ---2.00




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163949Method: SW719908/23/201910:00

Hexavalent Chromium mg/kg U 0.160.07 0




147285 - Page 74 of 142





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164099Method: E350.1





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164099Method: E350.1





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163558Method: SW601008/14/201913:01

Total Aluminum ug/L 36 92 2018.2 6.7Total Arsenic ug/L U 24 0 204.00 <4.00Total Barium ug/L 1.80 29 2016.3 12.2Total Cadmium ug/L U 2.0 0 200.300 <0.300Total Chromium ug/L U 4.0 0 200.600 <0.600Total Copper ug/L 7.0 200 201.4 <1.20Total Iron ug/L 100 200 2017.0 <16.0Total Lead ug/L U 4.0 0 201.40 <1.40Total Nickel ug/L U 6.0 0 201.00 <1.00Total Selenium ug/L U 13.0 0 202.20 <2.20Total Silver ug/L U 4.0 0 200.700 <0.700Total Zinc ug/L U 10.0 0 201.60 <1.60




147285 - Page 77 of 142





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163558Method: SW601008/14/201913:01

Total Aluminum ug/L 96 115772.0 86 ---800.0Total Arsenic ug/L 98 113788.0 87 ---800.0Total Barium ug/L 95 113758.0 88 ---800.0Total Cadmium ug/L 98 11319.50 88 ---20.00Total Chromium ug/L 98 11378.50 90 ---80.00Total Copper ug/L 97 11497.40 86 ---100.0Total Iron ug/L 99 115397.0 87 ---400.0Total Lead ug/L 97 113194.0 86 ---200.0Total Nickel ug/L 92 113185.0 88 ---200.0Total Selenium ug/L 101 114805.0 83 ---800.0Total Silver ug/L 92 11518.30 84 ---20.00Total Zinc ug/L 102 115204.0 87 ---200.0




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163558Method: SW601008/14/201913:01

Total Aluminum ug/L U 186 0Total Arsenic ug/L U 124 0Total Barium ug/L U 0.900.29 0Total Cadmium ug/L U 1.00.3 0Total Chromium ug/L U 2.00.6 0Total Copper ug/L U 3.51.2 0Total Iron ug/L U 5016 0Total Lead ug/L U 2.01.4 0Total Nickel ug/L U 3.01.0 0Total Selenium ug/L U 6.52.2 0Total Silver ug/L U 2.00.7 0Total Zinc ug/L U 5.01.6 0




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163558Method: SW601008/14/201913:01

Total Aluminum ug/L 70 115 18 20566 6.7 86 ---800Total Arsenic ug/L 76 113 13 20611 BDL 87 ---800Total Barium ug/L 69 113 14 20562 12.2 88 ---800Total Cadmium ug/L 73 113 15 2014.6 BDL 88 ---20.0Total Chromium ug/L 70 113 16 2056.0 BDL 90 ---80.0Total Copper ug/L 72 114 17 2071.6 BDL 86 ---100Total Iron ug/L 74 115 16 20296 BDL 87 ---400Total Lead ug/L 72 113 12 20145 BDL 86 ---200Total Nickel ug/L 66 113 15 20133 BDL 88 ---200Total Selenium ug/L 80 114 11 20644 BDL 83 ---800Total Silver ug/L 80 115 6 2016.1 BDL 84 ---20.0Total Zinc ug/L 74 115 16 20148 BDL 87 ---200




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163558Method: SW601008/14/201913:01

Total Aluminum ug/L 58 115471 6.7 86 ---800Total Arsenic ug/L 67 113538 BDL 87 ---800Total Barium ug/L 59 113487 12.2 88 ---800Total Cadmium ug/L 63 11312.6 BDL 88 ---20.0Total Chromium ug/L 59 11347.5 BDL 90 ---80.0Total Copper ug/L 60 11460.5 BDL 86 ---100Total Iron ug/L 63 115252 BDL 87 ---400Total Lead ug/L 64 113128 BDL 86 ---200Total Nickel ug/L 57 113114 BDL 88 ---200Total Selenium ug/L 72 114578 BDL 83 ---800Total Silver ug/L 76 11515.1 BDL 84 ---20.0Total Zinc ug/L 63 115126 BDL 87 ---200




147285 - Page 81 of 142



Duplicate


73120

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Parentsampleresult

163559Method: SW601008/14/201911:33

Dissolved Iron ug/L U 100 0 2016.0 <16.0




147285 - Page 82 of 142





73120

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163559Method: SW601008/14/201911:33

Dissolved Iron ug/L 102 115 20408.0 87 ---400.0




147285 - Page 83 of 142



Method Blank Water


73120

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163559Method: SW601008/14/201911:33

Dissolved Iron ug/L U 5016 0




147285 - Page 84 of 142





73120

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163559Method: SW601008/14/201911:33

Dissolved Iron ug/L 61 115 9 20243 BDL 87 ---400




147285 - Page 85 of 142



Matrix Spike Water


73120

NAHCTLab #:

Analyst:

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GROUND WATER

NAH

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RPDLimit

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ControlLimits


Parentsampleresult

163559Method: SW601008/14/201911:33

Dissolved Iron ug/L 56 115223 BDL 87 ---400




147285 - Page 86 of 142



Duplicate


73124

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SOIL

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Parentsampleresult

163571Method: SW601008/15/201911:30

Aluminum mg/kg 9.6 5 202820 2680Arsenic mg/kg 32 9 203.5 3.2Barium mg/kg 2.0 1 2021.6 21.4Cadmium mg/kg 1.60 73 200.12 0.056Chromium mg/kg 5.6 4 2018.2 17.4Copper mg/kg 16.0 19 2022.8 18.9Iron mg/kg 72 3 209830 9510Lead mg/kg 10.0 6 2011.4 10.7Nickel mg/kg 4.8 5 207.9 7.5Selenium mg/kg U 16 200 200.0933 0.18Silver mg/kg 4.0 107 200.028 0.092Zinc mg/kg 12.0 7 2058.7 54.9




147285 - Page 87 of 142





73124

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Parentsampleresult

163571Method: SW601008/15/201911:30

Aluminum mg/kg 102 119102 74 ---100Arsenic mg/kg 98 11198.0 82 ---100Barium mg/kg 96 11396.5 83 ---100Cadmium mg/kg 104 1132.6 82 ---2.5Chromium mg/kg 100 11310.0 85 ---10.0Copper mg/kg 99 11712.4 81 ---12.5Iron mg/kg 107 11853.5 81 ---50.0Lead mg/kg 96 11224.1 81 ---25.0Nickel mg/kg 98 11324.5 83 ---25.0Selenium mg/kg 103 111103 78 ---100Silver mg/kg 96 1122.4 82 ---2.5Zinc mg/kg 102 11325.5 82 ---25.0




147285 - Page 88 of 142



Method Blank Soil


73124

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Parentsampleresult

163571Method: SW601008/15/201911:30

Aluminum mg/kg U 0.120.04 0Arsenic mg/kg U 0.400.13 0Barium mg/kg U 0.0250.009 0Cadmium mg/kg U 0.0200.006 0Chromium mg/kg 0.1250.023 0Copper mg/kg U 0.200.07 0Iron mg/kg U 0.90.3 0Lead mg/kg U 0.1250.04 0Nickel mg/kg U 0.0600.021 0Selenium mg/kg U 0.200.06 0Silver mg/kg U 0.0500.017 0Zinc mg/kg U 0.150.05 0




147285 - Page 89 of 142





73124

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SOIL

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Parentsampleresult

163571Method: SW601008/15/201911:30

Aluminum mg/kg 552 119 18 203530 2680 74 ---154Arsenic mg/kg 99 111 2 20155 3.2 82 ---154Barium mg/kg 95 113 2 20168 21.4 83 ---154Cadmium mg/kg 96 113 2 203.7 0.056 82 ---3.8Chromium mg/kg 97 113 0 2032.4 17.4 85 ---15.4Copper mg/kg 114 117 3 2040.8 18.9 81 ---19.2Iron mg/kg 0 118 2 209500 9510 81 ---76.9Lead mg/kg 104 112 2 2050.8 10.7 81 ---38.5Nickel mg/kg 90 113 2 2042.3 7.5 83 ---38.5Selenium mg/kg 84 111 1 20129 0.18 78 ---154Silver mg/kg 87 112 2 203.4 0.092 82 ---3.8Zinc mg/kg 95 113 1 2091.5 54.9 82 ---38.5




147285 - Page 90 of 142



Matrix Spike Soil


73124

NAHCTLab #:

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SOIL

NAH

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RPDLimit

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ControlLimits


Parentsampleresult

163571Method: SW601008/15/201911:30

Aluminum mg/kg 181 1192960 2680 74 ---155Arsenic mg/kg 97 111153 3.2 82 ---155Barium mg/kg 93 113166 21.4 83 ---155Cadmium mg/kg 91 1133.6 0.056 82 ---3.9Chromium mg/kg 97 11332.4 17.4 85 ---15.5Copper mg/kg 120 11742.1 18.9 81 ---19.3Iron mg/kg 0 1189400 9510 81 ---77.3Lead mg/kg 102 11250.3 10.7 81 ---38.7Nickel mg/kg 89 11341.8 7.5 83 ---38.7Selenium mg/kg 82 111128 0.18 78 ---155Silver mg/kg 85 1123.4 0.092 82 ---3.9Zinc mg/kg 98 11392.8 54.9 82 ---38.7




147285 - Page 91 of 142





73149

MDSCTLab #:

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SOLID

BMM

Matrix:

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RPDLimit

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ControlLimits


Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg 101 1240.084 82 ---0.083




147285 - Page 92 of 142



Method Blank Soil


73149

MDSCTLab #:

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Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg U 004150.0021 0




147285 - Page 93 of 142





73232

NAHCTLab #:

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LIQUID

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RPDLimit

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Parentsampleresult

163782Method: SW601008/21/201911:24





147285 - Page 94 of 142



Method Blank Water


73232

NAHCTLab #:

Analyst:

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Parentsampleresult

163782Method: SW601008/21/201911:24





147285 - Page 95 of 142



Duplicate


73233

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Parentsampleresult

163783Method: SW601008/21/201911:24

Total Aluminum ug/L 36 3 201440 1490Total Arsenic ug/L 24 12 206.0 5.3Total Barium ug/L 1.80 3 2051.7 50.3Total Cadmium ug/L 2.0 21 200.42 0.34Total Chromium ug/L 4.0 2 204.4 4.3Total Copper ug/L 7.0 5 205.5 5.8Total Iron ug/L 100 1 202110 2090Total Lead ug/L 4.0 5 205.4 5.7Total Nickel ug/L 6.0 13 202.5 2.2Total Selenium ug/L U 13.0 0 202.20 <2.20Total Silver ug/L U 4.0 0 200.700 <0.700Total Zinc ug/L 10.0 5 2015.5 14.8




147285 - Page 96 of 142





73233

NAHCTLab #:

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163783Method: SW601008/21/201911:24





147285 - Page 97 of 142



Method Blank Water


73233

NAHCTLab #:

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Parentsampleresult

163783Method: SW601008/21/201911:24





147285 - Page 98 of 142





73233

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Parentsampleresult

163783Method: SW601008/21/201911:24

Total Aluminum ug/L 175 115 1 202890 1490 86 ---800Total Arsenic ug/L 100 113 0 20808 5.3 87 ---800Total Barium ug/L 98 113 1 20838 50.3 88 ---800Total Cadmium ug/L 96 113 3 2019.5 0.34 88 ---20.0Total Chromium ug/L 101 113 0 2085.4 4.3 90 ---80.0Total Copper ug/L 119 114 1 20125 5.8 86 ---100Total Iron ug/L 62 115 1 202340 2090 87 ---400Total Lead ug/L 96 113 1 20198 5.7 86 ---200Total Nickel ug/L 96 113 1 20195 2.2 88 ---200Total Selenium ug/L 102 114 1 20813 BDL 83 ---800Total Silver ug/L 94 115 1 2018.8 BDL 84 ---20.0Total Zinc ug/L 105 115 0 20224 14.8 87 ---200




147285 - Page 99 of 142



Matrix Spike Water


73233

NAHCTLab #:

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RPDLimit

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ControlLimits


Parentsampleresult

163783Method: SW601008/21/201911:24

Total Aluminum ug/L 172 1152870 1490 86 ---800Total Arsenic ug/L 101 113811 5.3 87 ---800Total Barium ug/L 99 113844 50.3 88 ---800Total Cadmium ug/L 98 11320.0 0.34 88 ---20.0Total Chromium ug/L 101 11385.0 4.3 90 ---80.0Total Copper ug/L 120 114126 5.8 86 ---100Total Iron ug/L 58 1152320 2090 87 ---400Total Lead ug/L 96 113197 5.7 86 ---200Total Nickel ug/L 97 113196 2.2 88 ---200Total Selenium ug/L 102 114818 BDL 83 ---800Total Silver ug/L 94 11518.7 BDL 84 ---20.0Total Zinc ug/L 105 115225 14.8 87 ---200




147285 - Page 100 of 142



Duplicate


73152

MDSCTLab #:

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Parentsampleresult

163791Method: SW7470A08/21/201914:51

Total Mercury ug/L U 0.12 0 200.0300 <0.0300




147285 - Page 101 of 142





73152

MDSCTLab #:

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Parentsampleresult

163791Method: SW7470A08/21/201914:51

Total Mercury ug/L 98 1193.93 82 ---4.00




147285 - Page 102 of 142



Method Blank Water


73152

MDSCTLab #:

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163791Method: SW7470A08/21/201914:51

Total Mercury ug/L U 0.060.03 0




147285 - Page 103 of 142





73152

MDSCTLab #:

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GROUND WATER

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163791Method: SW7470A08/21/201914:51

Total Mercury ug/L 102 119 6 204.1 BDL 82 ---4.0




147285 - Page 104 of 142



Matrix Spike Water


73152

MDSCTLab #:

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GROUND WATER

BMM

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163791Method: SW7470A08/21/201914:51

Total Mercury ug/L 98 1193.9 BDL 82 ---4.0




147285 - Page 105 of 142



Lab Control Spike Duplicate Water

08/20/2019Analytical Run #: Analysis Date:18:46Analysis Time:317993RLD

CTLab #:Analyst:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult


Benzene ug/L 106 120 5 2010.6 79 ---10.0Ethylbenzene ug/L 99 121 6 209.86 79 ---10.0m & p-Xylene ug/L 98 121 9 2019.5 80 ---20.0Methyl tert-butyl ether ug/L 101 124 0 2010.1 71 ---10.0o-Xylene ug/L 100 122 0 209.95 78 ---10.0Toluene ug/L 98 121 6 209.80 80 ---10.0




147285 - Page 106 of 142





CTLab #:Analyst:

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Benzene ug/L 111 120 2011.1 79 ---10.0Ethylbenzene ug/L 105 121 2010.5 79 ---10.0m & p-Xylene ug/L 107 121 2021.4 80 ---20.0Methyl tert-butyl ether ug/L 101 124 2010.1 71 ---10.0o-Xylene ug/L 100 122 209.96 78 ---10.0Toluene ug/L 104 121 2010.4 80 ---10.0




147285 - Page 107 of 142



Method Blank Water


CTLab #:Analyst:

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Parentsampleresult


Benzene ug/L U 1.00.4 0Ethylbenzene ug/L U 0.50.3 0m & p-Xylene ug/L U 1.00.7 0Methyl tert-butyl ether ug/L U 0.50.3 0o-Xylene ug/L U 0.500.26 0Toluene ug/L U 0.500.21 0




147285 - Page 108 of 142





CTLab #:Analyst:

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LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147285 - Page 109 of 142



Method Blank Water


CTLab #:Analyst:

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Parentsampleresult






147285 - Page 110 of 142





73259

RLDCTLab #:

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SOLID

RLD

Matrix:

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RPDLimit

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Parentsampleresult

163774Method: SW8260C08/22/201909:05

Benzene ug/kg 103 125514 75 ---500Ethylbenzene ug/kg 99 125497 75 ---500m & p-Xylene ug/kg 98 125977 80 ---1000Methyl tert-butyl ether ug/kg 107 125535 65 ---500o-Xylene ug/kg 97 125484 75 ---500Toluene ug/kg 104 125520 70 ---500




147285 - Page 111 of 142



Method Blank Soil


73259

RLDCTLab #:

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RLD

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Parentsampleresult

163774Method: SW8260C08/22/201909:05

Benzene ug/kg U 2511 0Ethylbenzene ug/kg U 2511 0m & p-Xylene ug/kg U 5025 0Methyl tert-butyl ether ug/kg U 5016 0o-Xylene ug/kg U 257 0Toluene ug/kg U 5016 0




147285 - Page 112 of 142





73201

AJZCTLab #:

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Parentsampleresult

163780Method: SW808208/20/201909:00

Aroclor-1016 ug/L 75 129 2 303.76 46 ---5.00Aroclor-1260 ug/L 93 134 3 304.65 45 ---5.00




147285 - Page 113 of 142





73201

AJZCTLab #:

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Parentsampleresult

163780Method: SW808208/20/201909:00

Aroclor-1016 ug/L 76 129 303.82 46 ---5.00Aroclor-1260 ug/L 96 134 304.78 45 ---5.00




147285 - Page 114 of 142



Method Blank Water


73201

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Parentsampleresult

163780Method: SW808208/20/201909:00

Aroclor-1016 ug/L U 0.500.113 0Aroclor-1221 ug/L U 0.500.085 0Aroclor-1232 ug/L U 0.500.145 0Aroclor-1242 ug/L U 0.500.096 0Aroclor-1248 ug/L U 0.500.088 0Aroclor-1254 ug/L U 0.500.094 0Aroclor-1260 ug/L U 0.500.099 0Aroclor-1262 ug/L U 0.500.28 0Aroclor-1268 ug/L U 0.500.056 0




147285 - Page 115 of 142





73143

JJYCTLab #:

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Parentsampleresult

163812Method: SW8270SIM08/16/201916:00

1-Methylnaphthalene ug/kg 75 111 4075.1 43 ---1002-Methylnaphthalene ug/kg 85 114 4084.7 39 ---100Acenaphthene ug/kg 74 111 4073.5 44 ---100Acenaphthylene ug/kg 88 116 4088.0 39 ---100Anthracene ug/kg 93 114 4092.7 50 ---100Benzo(a)anthracene ug/kg 107 122 40107 54 ---100Benzo(a)pyrene ug/kg 99 125 4099.1 50 ---100Benzo(b)fluoranthene ug/kg 96 128 4096.3 53 ---100Benzo(g,h,i)perylene ug/kg 94 127 4094.0 49 ---100Benzo(k)fluoranthene ug/kg 91 123 4090.9 56 ---100Chrysene ug/kg 100 118 40100 57 ---100Dibenzo(a,h)anthracene ug/kg 97 129 4096.7 50 ---100Fluoranthene ug/kg 96 119 4095.5 55 ---100Fluorene ug/kg 83 114 4082.9 47 ---100Indeno(1,2,3-cd)pyrene ug/kg 99 130 4099.2 49 ---100Naphthalene ug/kg 77 111 4076.9 38 ---100Phenanthrene ug/kg 88 113 4087.8 49 ---100Pyrene ug/kg 94 117 4094.1 55 ---100




147285 - Page 116 of 142



Method Blank Soil


73143

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Parentsampleresult

163812Method: SW8270SIM08/16/201916:00

1-Methylnaphthalene ug/kg U 1.00.4 02-Methylnaphthalene ug/kg U 1.00.5 0Acenaphthene ug/kg U 1.00.5 0Acenaphthylene ug/kg U 1.00.3 0Anthracene ug/kg U 1.00.4 0Benzo(a)anthracene ug/kg U 1.00.51 0Benzo(a)pyrene ug/kg U 1.00.3 0Benzo(b)fluoranthene ug/kg U 1.00.4 0Benzo(g,h,i)perylene ug/kg U 1.000.26 0Benzo(k)fluoranthene ug/kg U 2.00.6 0Chrysene ug/kg U 1.000.22 0Dibenzo(a,h)anthracene ug/kg U 1.000.21 0Fluoranthene ug/kg U 2.00.7 0Fluorene ug/kg U 1.00.4 0Indeno(1,2,3-cd)pyrene ug/kg U 1.00.4 0Naphthalene ug/kg U 1.00.5 0Phenanthrene ug/kg U 2.01.1 0Pyrene ug/kg U 2.00.6 0




147285 - Page 117 of 142





73172

JJYCTLab #:

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Parentsampleresult

163814Method: SW8270SIM08/19/201912:00

1-Methylnaphthalene ug/L 70 115 2 400.695 41 ---1.002-Methylnaphthalene ug/L 76 114 3 400.755 39 ---1.00Acenaphthene ug/L 74 114 0 400.742 48 ---1.00Acenaphthylene ug/L 89 121 5 400.893 35 ---1.00Anthracene ug/L 92 119 2 400.917 53 ---1.00Benzo(a)anthracene ug/L 117 120 1 401.17 59 ---1.00Benzo(a)pyrene ug/L 104 120 4 401.04 53 ---1.00Benzo(b)fluoranthene ug/L 102 126 9 401.02 53 ---1.00Benzo(g,h,i)perylene ug/L 81 128 24 400.809 44 ---1.00Benzo(k)fluoranthene ug/L 105 125 5 401.05 54 ---1.00Chrysene ug/L 107 120 4 401.07 57 ---1.00Dibenzo(a,h)anthracene ug/L 88 131 17 400.882 44 ---1.00Fluoranthene ug/L 100 120 2 401.00 58 ---1.00Fluorene ug/L 86 118 3 400.864 50 ---1.00Indeno(1,2,3-cd)pyrene ug/L 90 130 17 400.905 48 ---1.00Naphthalene ug/L 69 114 2 400.689 43 ---1.00Phenanthrene ug/L 90 115 1 400.905 53 ---1.00Pyrene ug/L 104 121 1 401.04 53 ---1.00




147285 - Page 118 of 142





73172

JJYCTLab #:

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Parentsampleresult

163814Method: SW8270SIM08/19/201912:00

1-Methylnaphthalene ug/L 71 115 400.710 41 ---1.002-Methylnaphthalene ug/L 78 114 400.777 39 ---1.00Acenaphthene ug/L 74 114 400.739 48 ---1.00Acenaphthylene ug/L 85 121 400.852 35 ---1.00Anthracene ug/L 94 119 400.936 53 ---1.00Benzo(a)anthracene ug/L 116 120 401.16 59 ---1.00Benzo(a)pyrene ug/L 108 120 401.08 53 ---1.00Benzo(b)fluoranthene ug/L 112 126 401.12 53 ---1.00Benzo(g,h,i)perylene ug/L 103 128 401.03 44 ---1.00Benzo(k)fluoranthene ug/L 100 125 400.999 54 ---1.00Chrysene ug/L 111 120 401.11 57 ---1.00Dibenzo(a,h)anthracene ug/L 105 131 401.05 44 ---1.00Fluoranthene ug/L 102 120 401.02 58 ---1.00Fluorene ug/L 84 118 400.836 50 ---1.00Indeno(1,2,3-cd)pyrene ug/L 107 130 401.07 48 ---1.00Naphthalene ug/L 70 114 400.702 43 ---1.00Phenanthrene ug/L 92 115 400.918 53 ---1.00Pyrene ug/L 105 121 401.05 53 ---1.00




147285 - Page 119 of 142



Method Blank Water


73172

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163814Method: SW8270SIM08/19/201912:00

1-Methylnaphthalene ug/L U 0.0200.007 02-Methylnaphthalene ug/L U 0.0200.011 0Acenaphthene ug/L U 0.0200.007 0Acenaphthylene ug/L U 0.0200.006 0Anthracene ug/L U 0.0200.006 0Benzo(a)anthracene ug/L U 0.0200.007 0Benzo(a)pyrene ug/L 0.0200.0407 0Benzo(b)fluoranthene ug/L 0.0200.0343 0Benzo(g,h,i)perylene ug/L U 0.0200.006 0Benzo(k)fluoranthene ug/L U 0.0200.010 0Chrysene ug/L 0.0200.00764 0Dibenzo(a,h)anthracene ug/L U 0.0200.006 0Fluoranthene ug/L U 0.0200.009 0Fluorene ug/L U 0.0200.009 0Indeno(1,2,3-cd)pyrene ug/L U 0.0200.006 0Naphthalene ug/L U 0.0200.011 0Phenanthrene ug/L U 0.0200.011 0Pyrene ug/L 0.0200.0215 0




147285 - Page 120 of 142





73187

JJYCTLab #:

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Parentsampleresult

163815Method: SW8270D08/19/201912:00

1,1'-Biphenyl ug/L 69 115 4 2013.8 49 ---20.01,2,4,5-Tetrachlorobenzene ug/L 63 121 3 2012.6 35 ---20.01,2,4-Trichlorobenzene ug/L 56 116 5 2011.1 29 ---20.01,2-Dichlorobenzene ug/L 56 111 10 2011.2 32 ---20.01,3-Dichlorobenzene ug/L 53 110 9 2010.6 28 ---20.01,4-Dichlorobenzene ug/L 51 112 7 2010.2 29 ---20.01-Methylnaphthalene ug/L 68 119 4 2013.7 41 ---20.02,3,4,6-Tetrachlorophenol ug/L 96 128 1 2019.2 50 ---20.02,4,5-Trichlorophenol ug/L 88 123 2 2017.5 53 ---20.02,4,6-Trichlorophenol ug/L 79 125 6 2015.8 50 ---20.02,4-Dichlorophenol ug/L 69 121 5 2013.8 47 ---20.02,4-Dimethylphenol ug/L 47 124 17 209.36 31 ---20.02,4-Dinitrophenol ug/L 122 143 9 2024.3 23 ---20.02,4-Dinitrotoluene ug/L 96 128 2 2019.2 57 ---20.02,6-Dichlorophenol ug/L 66 118 7 2013.3 50 ---20.02,6-Dinitrotoluene ug/L 94 124 0 2018.9 57 ---20.02-Chloronaphthalene ug/L 66 116 4 2013.2 40 ---20.02-Chlorophenol ug/L 66 117 10 2013.2 38 ---20.02-Methylnaphthalene ug/L 62 121 4 2012.4 40 ---20.02-Methylphenol ug/L 64 117 5 2012.8 30 ---20.02-Nitroaniline ug/L 88 127 1 2017.7 55 ---20.02-Nitrophenol ug/L 70 123 4 2014.0 47 ---20.03 & 4-Methylphenol ug/L 56 110 9 2011.2 28 ---20.03,3'-Dichlorobenzidine ug/L 37 129 50 207.40 27 ---20.03-Nitroaniline ug/L 72 128 15 2014.5 41 ---20.04,6-Dinitro-2-methylphenol ug/L 98 137 5 2019.7 44 ---20.04-Bromophenyl-phenyl ether ug/L 92 124 0 2018.3 55 ---20.04-Chloro-3-methylphenol ug/L 77 119 4 2015.4 52 ---20.04-Chloroaniline ug/L 45 117 2 208.94 33 ---20.04-Chlorophenyl-phenyl ether ug/L 82 121 2 2016.3 53 ---20.04-Nitroaniline ug/L 77 130 2 2015.4 51 ---20.04-Nitrophenol ug/L 61 113 28 2012.2 0 ---20.0Acenaphthene ug/L 76 122 4 2015.1 47 ---20.0Acenaphthylene ug/L 78 130 1 2015.7 41 ---20.0Acetophenone ug/L 66 118 10 2013.2 46 ---20.0Aniline ug/L 36 101 2 207.26 18 ---20.0Anthracene ug/L 94 123 0 2018.7 57 ---20.0Atrazine ug/L 94 142 8 2018.9 44 ---20.0Azobenzene & 1,2-Diphenylhydra ug/L 92 116 2 2036.7 61 ---40.0Benzaldehyde ug/L 67 118 8 2013.4 15 ---20.0Benzidine ug/L 165 200 0 ---20.0Benzo(a)anthracene ug/L 104 125 2 2020.7 58 ---20.0Benzo(a)pyrene ug/L 99 128 1 2019.8 54 ---20.0




147285 - Page 121 of 142





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Parentsampleresult

163815Method: SW8270D08/19/201912:00

Benzo(b)fluoranthene ug/L 104 131 2 2020.9 53 ---20.0Benzo(g,h,i)perylene ug/L 70 134 20 2013.9 50 ---20.0Benzo(k)fluoranthene ug/L 98 129 3 2019.6 57 ---20.0Benzoic acid ug/L 58 125 4 2011.7 0 ---20.0Benzyl alcohol ug/L 42 112 41 208.32 31 ---20.0Bis(2-chloroethoxy)methane ug/L 64 120 6 2012.9 48 ---20.0Bis(2-chloroethyl)ether ug/L 71 118 9 2014.2 43 ---20.0Bis(2-chloroisopropyl)ether ug/L 60 130 7 2012.0 37 ---20.0Bis(2-ethylhexyl)phthalate ug/L 110 135 0 2021.9 55 ---20.0Butylbenzylphthalate ug/L 106 134 1 2021.1 53 ---20.0Caprolactam ug/L 30 120 4 206.05 10 ---20.0Carbazole ug/L 100 122 0 2020.0 60 ---20.0Chrysene ug/L 98 123 3 2019.5 59 ---20.0Di-n-butylphthalate ug/L 106 127 2 2021.2 59 ---20.0Di-n-octylphthalate ug/L 102 140 1 2020.5 51 ---20.0Dibenzo(a,h)anthracene ug/L 82 134 15 2016.3 51 ---20.0Dibenzofuran ug/L 78 118 2 2015.7 53 ---20.0Diethylphthalate ug/L 96 125 0 2019.2 56 ---20.0Dimethylphthalate ug/L 90 127 1 2018.0 45 ---20.0Fluoranthene ug/L 96 128 1 2019.3 57 ---20.0Fluorene ug/L 86 124 0 2017.1 52 ---20.0Hexachlorobenzene ug/L 94 125 2 2018.9 53 ---20.0Hexachlorobutadiene ug/L 50 124 0 2010.0 22 ---20.0Hexachlorocyclopentadiene ug/L 38 93 19 207.53 31 ---20.0Hexachloroethane ug/L 48 115 4 209.55 21 ---20.0Indeno(1,2,3-cd)pyrene ug/L 76 134 16 2015.1 52 ---20.0Isophorone ug/L 53 124 2 2010.6 42 ---20.0N-Nitroso-di-n-propylamine ug/L 73 119 9 2014.6 49 ---20.0N-Nitrosodimethylamine ug/L 46 104 10 209.24 9 ---20.0N-Nitrosodiphenylamine & Diphn ug/L 92 123 1 2037.0 51 ---40.0N-Nitrosopyrrolidine ug/L 63 113 8 2012.6 48 ---20.0Naphthalene ug/L 63 121 5 2012.6 40 ---20.0Nitrobenzene ug/L 70 121 5 2014.1 45 ---20.0Pentachlorophenol ug/L 97 138 6 2019.4 35 ---20.0Phenanthrene ug/L 94 120 1 2018.7 59 ---20.0Phenol ug/L 32 108 8 206.41 0 ---20.0Pyrene ug/L 102 126 3 2020.5 57 ---20.0Pyridine ug/L 36 106 33 207.10 0 ---20.0




147285 - Page 122 of 142





73187

JJYCTLab #:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163815Method: SW8270D08/19/201912:00

1,1'-Biphenyl ug/L 72 115 2014.4 49 ---20.01,2,4,5-Tetrachlorobenzene ug/L 65 121 2013.0 35 ---20.01,2,4-Trichlorobenzene ug/L 58 116 2011.7 29 ---20.01,2-Dichlorobenzene ug/L 62 111 2012.4 32 ---20.01,3-Dichlorobenzene ug/L 58 110 2011.6 28 ---20.01,4-Dichlorobenzene ug/L 54 112 2010.9 29 ---20.01-Methylnaphthalene ug/L 71 119 2014.2 41 ---20.02,3,4,6-Tetrachlorophenol ug/L 96 128 2019.1 50 ---20.02,4,5-Trichlorophenol ug/L 89 123 2017.8 53 ---20.02,4,6-Trichlorophenol ug/L 84 125 2016.8 50 ---20.02,4-Dichlorophenol ug/L 72 121 2014.5 47 ---20.02,4-Dimethylphenol ug/L 56 124 2011.1 31 ---20.02,4-Dinitrophenol ug/L 132 143 2026.5 23 ---20.02,4-Dinitrotoluene ug/L 98 128 2019.6 57 ---20.02,6-Dichlorophenol ug/L 71 118 2014.2 50 ---20.02,6-Dinitrotoluene ug/L 94 124 2018.9 57 ---20.02-Chloronaphthalene ug/L 68 116 2013.7 40 ---20.02-Chlorophenol ug/L 73 117 2014.6 38 ---20.02-Methylnaphthalene ug/L 64 121 2012.9 40 ---20.02-Methylphenol ug/L 68 117 2013.5 30 ---20.02-Nitroaniline ug/L 88 127 2017.6 55 ---20.02-Nitrophenol ug/L 73 123 2014.6 47 ---20.03 & 4-Methylphenol ug/L 62 110 2012.3 28 ---20.03,3'-Dichlorobenzidine ug/L 22 129 204.46 27 ---20.03-Nitroaniline ug/L 62 128 2012.5 41 ---20.04,6-Dinitro-2-methylphenol ug/L 104 137 2020.7 44 ---20.04-Bromophenyl-phenyl ether ug/L 92 124 2018.3 55 ---20.04-Chloro-3-methylphenol ug/L 80 119 2016.1 52 ---20.04-Chloroaniline ug/L 44 117 208.79 33 ---20.04-Chlorophenyl-phenyl ether ug/L 84 121 2016.7 53 ---20.04-Nitroaniline ug/L 76 130 2015.1 51 ---20.04-Nitrophenol ug/L 46 113 209.24 0 ---20.0Acenaphthene ug/L 78 122 2015.7 47 ---20.0Acenaphthylene ug/L 80 130 2015.9 41 ---20.0Acetophenone ug/L 73 118 2014.6 46 ---20.0Aniline ug/L 35 101 207.09 18 ---20.0Anthracene ug/L 94 123 2018.7 57 ---20.0Atrazine ug/L 88 142 2017.5 44 ---20.0Azobenzene & 1,2-Diphenylhydra ug/L 94 116 2037.4 61 ---40.0Benzaldehyde ug/L 72 118 2014.5 15 ---20.0Benzidine ug/L 0 165 200 0 ---20.0Benzo(a)anthracene ug/L 106 125 2021.2 58 ---20.0Benzo(a)pyrene ug/L 98 128 2019.7 54 ---20.0




147285 - Page 123 of 142





73187

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Parentsampleresult

163815Method: SW8270D08/19/201912:00

Benzo(b)fluoranthene ug/L 102 131 2020.4 53 ---20.0Benzo(g,h,i)perylene ug/L 85 134 2017.0 50 ---20.0Benzo(k)fluoranthene ug/L 95 129 2019.0 57 ---20.0Benzoic acid ug/L 61 125 2012.2 0 ---20.0Benzyl alcohol ug/L 63 112 2012.6 31 ---20.0Bis(2-chloroethoxy)methane ug/L 68 120 2013.7 48 ---20.0Bis(2-chloroethyl)ether ug/L 78 118 2015.5 43 ---20.0Bis(2-chloroisopropyl)ether ug/L 64 130 2012.9 37 ---20.0Bis(2-ethylhexyl)phthalate ug/L 109 135 2021.8 55 ---20.0Butylbenzylphthalate ug/L 106 134 2021.3 53 ---20.0Caprolactam ug/L 29 120 205.82 10 ---20.0Carbazole ug/L 100 122 2020.0 60 ---20.0Chrysene ug/L 100 123 2020.0 59 ---20.0Di-n-butylphthalate ug/L 108 127 2021.7 59 ---20.0Di-n-octylphthalate ug/L 104 140 2020.7 51 ---20.0Dibenzo(a,h)anthracene ug/L 95 134 2019.0 51 ---20.0Dibenzofuran ug/L 80 118 2016.0 53 ---20.0Diethylphthalate ug/L 96 125 2019.2 56 ---20.0Dimethylphthalate ug/L 91 127 2018.2 45 ---20.0Fluoranthene ug/L 98 128 2019.5 57 ---20.0Fluorene ug/L 86 124 2017.1 52 ---20.0Hexachlorobenzene ug/L 96 125 2019.3 53 ---20.0Hexachlorobutadiene ug/L 50 124 209.97 22 ---20.0Hexachlorocyclopentadiene ug/L 45 93 209.08 31 ---20.0Hexachloroethane ug/L 50 115 209.91 21 ---20.0Indeno(1,2,3-cd)pyrene ug/L 88 134 2017.7 52 ---20.0Isophorone ug/L 54 124 2010.8 42 ---20.0N-Nitroso-di-n-propylamine ug/L 80 119 2015.9 49 ---20.0N-Nitrosodimethylamine ug/L 51 104 2010.2 9 ---20.0N-Nitrosodiphenylamine & Diphn ug/L 93 123 2037.2 51 ---40.0N-Nitrosopyrrolidine ug/L 68 113 2013.7 48 ---20.0Naphthalene ug/L 66 121 2013.3 40 ---20.0Nitrobenzene ug/L 74 121 2014.8 45 ---20.0Pentachlorophenol ug/L 102 138 2020.5 35 ---20.0Phenanthrene ug/L 94 120 2018.8 59 ---20.0Phenol ug/L 35 108 206.92 0 ---20.0Pyrene ug/L 106 126 2021.1 57 ---20.0Pyridine ug/L 26 106 205.11 0 ---20.0




147285 - Page 124 of 142



Method Blank Water


73187

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Parentsampleresult

163815Method: SW8270D08/19/201912:00

1,1'-Biphenyl ug/L U 0.500.15 01,2,4,5-Tetrachlorobenzene ug/L U 0.500.17 01,2,4-Trichlorobenzene ug/L U 0.500.17 01,2-Dichlorobenzene ug/L U 0.500.18 01,3-Dichlorobenzene ug/L U 0.500.20 01,4-Dichlorobenzene ug/L U 0.500.19 01-Methylnaphthalene ug/L U 0.500.16 02,3,4,6-Tetrachlorophenol ug/L U 2.51.1 02,4,5-Trichlorophenol ug/L U 2.51.1 02,4,6-Trichlorophenol ug/L U 2.51.0 02,4-Dichlorophenol ug/L U 2.51.0 02,4-Dimethylphenol ug/L U 2.50.82 02,4-Dinitrophenol ug/L U 5.01.5 02,4-Dinitrotoluene ug/L U 0.500.21 02,6-Dichlorophenol ug/L U 2.51.2 02,6-Dinitrotoluene ug/L U 0.500.28 02-Chloronaphthalene ug/L U 0.500.18 02-Chlorophenol ug/L U 2.50.87 02-Methylnaphthalene ug/L U 0.500.17 02-Methylphenol ug/L U 2.50.86 02-Nitroaniline ug/L U 1.000.22 02-Nitrophenol ug/L U 2.50.90 03 & 4-Methylphenol ug/L U 4.51.4 03,3'-Dichlorobenzidine ug/L U 1.250.66 03-Nitroaniline ug/L U 1.000.26 04,6-Dinitro-2-methylphenol ug/L U 5.01.6 04-Bromophenyl-phenyl ether ug/L U 1.000.20 04-Chloro-3-methylphenol ug/L U 2.500.76 04-Chloroaniline ug/L U 0.500.12 04-Chlorophenyl-phenyl ether ug/L U 0.500.18 04-Nitroaniline ug/L U 1.000.15 04-Nitrophenol ug/L U 5.01.1 0Acenaphthene ug/L U 0.500.18 0Acenaphthylene ug/L U 0.500.17 0Acetophenone ug/L U 0.500.27 0Aniline ug/L U 2.000.72 0Anthracene ug/L U 0.500.11 0Atrazine ug/L U 0.500.26 0Azobenzene & 1,2-Diphenylhydra ug/L U 1.000.52 0Benzaldehyde ug/L U 0.500.25 0Benzidine ug/L U 5029 0Benzo(a)anthracene ug/L U 0.500.12 0Benzo(a)pyrene ug/L U 0.500.14 0




147285 - Page 125 of 142



Method Blank Water


73187

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Parentsampleresult

163815Method: SW8270D08/19/201912:00

Benzo(b)fluoranthene ug/L U 0.500.17 0Benzo(g,h,i)perylene ug/L U 0.500.21 0Benzo(k)fluoranthene ug/L U 0.500.20 0Benzoic acid ug/L U 2511 0Benzyl alcohol ug/L U 1.000.54 0Bis(2-chloroethoxy)methane ug/L U 0.500.19 0Bis(2-chloroethyl)ether ug/L U 0.500.21 0Bis(2-chloroisopropyl)ether ug/L U 0.500.22 0Bis(2-ethylhexyl)phthalate ug/L U 1.000.44 0Butylbenzylphthalate ug/L U 1.000.47 0Caprolactam ug/L U 1.000.19 0Carbazole ug/L U 0.500.12 0Chrysene ug/L U 0.500.16 0Di-n-butylphthalate ug/L U 2.000.67 0Di-n-octylphthalate ug/L U 1.000.49 0Dibenzo(a,h)anthracene ug/L U 0.500.17 0Dibenzofuran ug/L U 0.500.19 0Diethylphthalate ug/L U 1.000.45 0Dimethylphthalate ug/L U 1.000.54 0Fluoranthene ug/L U 0.500.13 0Fluorene ug/L U 0.500.19 0Hexachlorobenzene ug/L U 0.500.27 0Hexachlorobutadiene ug/L U 0.500.18 0Hexachlorocyclopentadiene ug/L U 2.000.26 0Hexachloroethane ug/L U 0.500.22 0Indeno(1,2,3-cd)pyrene ug/L U 0.500.18 0Isophorone ug/L U 0.500.18 0N-Nitroso-di-n-propylamine ug/L U 0.500.18 0N-Nitrosodimethylamine ug/L U 1.000.47 0N-Nitrosodiphenylamine & Diphn ug/L U 1.000.36 0N-Nitrosopyrrolidine ug/L U 1.000.21 0Naphthalene ug/L U 0.500.18 0Nitrobenzene ug/L U 0.500.16 0Pentachlorophenol ug/L U 2.51.1 0Phenanthrene ug/L U 0.500.30 0Phenol ug/L U 2.500.48 0Pyrene ug/L U 0.500.13 0Pyridine ug/L U 2.000.62 0




147285 - Page 126 of 142





73141

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AJZ

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Parentsampleresult

163834Method: SW808208/20/201914:20

Aroclor-1016 ug/kg 94 134 30472 47 ---500Aroclor-1260 ug/kg 107 140 30534 53 ---500




147285 - Page 127 of 142



Method Blank Soil


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Parentsampleresult

163834Method: SW808208/20/201914:20

Aroclor-1016 ug/kg U 155 0Aroclor-1221 ug/kg U 157 0Aroclor-1232 ug/kg U 159 0Aroclor-1242 ug/kg U 157 0Aroclor-1248 ug/kg U 157 0Aroclor-1254 ug/kg U 159 0Aroclor-1260 ug/kg U 156 0Aroclor-1262 ug/kg U 157 0Aroclor-1268 ug/kg U 155 0




147285 - Page 128 of 142

147285

Sample Condition Report

Folder #: 147285 Print Date / Time: 08/14/2019 11:35Client: WOOD E&I SOLUTIONS, INC. Received Date / Time / By: 08/14/2019 10:15 JLS

Project Name: BURNS HARBOR Log-In Date / Time / By: 08/14/2019 11:30 JLSProject Phase: BURNS HARBOR, IN Project #: 3293191855.02.**** PM: BMS

Coolers: 6176,6271 Temperature: 4.2,4.3 C On Ice: YCustody Seals Present : Y COC Present:? Y Complete? Y

Seal Intact? Y Numbers: DATED AND SIGNED Ship Method: FEDEX EXPRESS Tracking Number: 789114796454Adequate Packaging: Y Temp Blank Enclosed? Y

Notes: THE SAMPLES WERE RECEIVED IN GOOD CONDITION ON ICE.

ONE CUSTODY SEAL WAS PRESENT AND INTACT ON EACH COOLER UPON RECEIPT - BOTH WERE DATED 08/13/19 AND SIGNED.

TWO TRIP BLANKS WERE RECEIVED BUT WERE NOT LISTED ON THE COC. THE TRIP BLANKS WERE ADDED AND LOGGED FOR BTEX ANALYSIS, PER THE CLIENT'S REQUEST.

THE SITE WATER FOR THE ELUTRIATE SAMPLE WAS NOT RECEIVED WITH THIS SHIPMENT. THE CLIENT ADVISED THAT IT WOULD SHIP FOR 8/15 DELIVERY.

_________________________________________________________________________________________________________Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

_________________________________________________________________________________________________________315103 BWH-19-MU2-C2

SOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pSOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pTotal # of Containers of Type ( SOLIDS ) = 2

_________________________________________________________________________________________________________315103 BWH-19-MU2-C2

UNPRES GL 1 / 8270,PCBUNPRES GL 1 / 8270,PCBTotal # of Containers of Type ( UNPRES GL ) = 2

_________________________________________________________________________________________________________315103 BWH-19-MU2-C2

JAR GL 1 / O&G Total # of Containers of Type ( JAR GL ) = 1

_________________________________________________________________________________________________________315103 BWH-19-MU2-C2

MISC 1 / SUB HYD Total # of Containers of Type ( MISC ) = 1

_________________________________________________________________________________________________________315103 BWH-19-MU2-C2

TERRA CORE 1 / VOC TERRA CORE 1 / VOC Total # of Containers of Type ( TERRA CORE ) = 2


_________________________________________________________________________________________________________315114 BWH-19-MU2-C1


_________________________________________________________________________________________________________315114 BWH-19-MU2-C1

147285 - Page 129 of 142

147285


_________________________________________________________________________________________________________315114 BWH-19-MU2-C1


_________________________________________________________________________________________________________315114 BWH-19-MU2-C1


_________________________________________________________________________________________________________315114 BWH-19-MU2-C1



_________________________________________________________________________________________________________315115 BWH-19-MU2-C3


_________________________________________________________________________________________________________315115 BWH-19-MU2-C3

AMBER GL 1 / 8270Total # of Containers of Type ( AMBER GL ) = 1

_________________________________________________________________________________________________________315115 BWH-19-MU2-C3

UNPRES GL 1 / 8270,PCBTotal # of Containers of Type ( UNPRES GL ) = 1

_________________________________________________________________________________________________________315115 BWH-19-MU2-C3


_________________________________________________________________________________________________________315115 BWH-19-MU2-C3


_________________________________________________________________________________________________________315115 BWH-19-MU2-C3

TERRA CORE 1 / VOC Total # of Containers of Type ( TERRA CORE ) = 1

315115 BWH-19-MU2-C3TERRA CORE LL 1 / VOC Total # of Containers of Type ( TERRA CORE LL ) = 1


_________________________________________________________________________________________________________315116 FD-1


_________________________________________________________________________________________________________315116 FD-1

AMBER GL 1 / 8270Total # of Containers of Type ( AMBER GL ) = 1

_________________________________________________________________________________________________________315116 FD-1


_________________________________________________________________________________________________________315116 FD-1

JAR GL 1 / O&G

147285 - Page 130 of 142

147285

Total # of Containers of Type ( JAR GL ) = 1_________________________________________________________________________________________________________

315116 FD-1MISC 1 / SUB HYD Total # of Containers of Type ( MISC ) = 1

_________________________________________________________________________________________________________315116 FD-1



_________________________________________________________________________________________________________315117 BWH-19-MU2-W2

AMBER GL 1 / 8270,PCBAMBER GL 1 / 8270,PCBAMBER GL 1 / 8270,PCBTotal # of Containers of Type ( AMBER GL ) = 3

_________________________________________________________________________________________________________315117 BWH-19-MU2-W2

UNPRES PL 1 / ALK,CR6,pH,TDS,TSSUNPRES PL 1 / ALK,CR6,pH,TDS,TSSUNPRES PL 1 / ALK,CR6,pH,TDS,TSSTotal # of Containers of Type ( UNPRES PL ) = 3

_________________________________________________________________________________________________________315117 BWH-19-MU2-W2

H2SO4 PL 1 Y / COD,NH3N,PHOSTotal # of Containers of Type ( H2SO4 PL ) = 1

_________________________________________________________________________________________________________315117 BWH-19-MU2-W2

HNO3 1 Y / HG,HRD,ICPTotal # of Containers of Type ( HNO3 ) = 1

_________________________________________________________________________________________________________315117 BWH-19-MU2-W2

AMBER HCL 1 Y / O&G Total # of Containers of Type ( AMBER HCL ) = 1

_________________________________________________________________________________________________________315117 BWH-19-MU2-W2

VOA HCL 1 / VOC VOA HCL 1 / VOC VOA HCL 1 / VOC Total # of Containers of Type ( VOA HCL ) = 3


_________________________________________________________________________________________________________315136 BWH-19-MU2-W2

LABEL ONLY 1 / FILTRATIONTotal # of Containers of Type ( LABEL ONLY ) = 1

_________________________________________________________________________________________________________315136 BWH-19-MU2-W2

UNPRES PL 1 / ICPTotal # of Containers of Type ( UNPRES PL ) = 1


_________________________________________________________________________________________________________315137 BWH-19-MU2-E1

LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /Total # of Containers of Type ( LABEL ONLY ) = 3

_________________________________________________________________________________________________________315137 BWH-19-MU2-E1

UNPRES GL 1 / %SOLTotal # of Containers of Type ( UNPRES GL ) = 1

147285 - Page 131 of 142

147285

_________________________________________________________________________________________________________315137 BWH-19-MU2-E1

LABEL ONLY 1 / Sed. Elutirate Prep Total # of Containers of Type ( LABEL ONLY ) = 1

315137 BWH-19-MU2-E1UNPRES GL 1 / Sed. Elutirate Prep UNPRES GL 1 / Sed. Elutirate Prep Total # of Containers of Type ( UNPRES GL ) = 2


_________________________________________________________________________________________________________315168 TB-08132019

TRIP BLANK 1 / VOC TRIP BLANK 1 / VOC Total # of Containers of Type ( TRIP BLANK ) = 2

__________________________________________________________________________________________________________

Condition Code Condition Description 1 Sample Received OK

147285 - Page 132 of 142

147285 - Page 133 of 142

147285 - Page 134 of 142

147285 - Page 135 of 142

147285 - Page 136 of 142

ANALYTICAL REPORT

CT LaboratoriesAttn: Mr. Brett M. Szymanski1230 Lange CourtBaraboo, WI [email protected]

PROJECT NAME: BURNS HARBOR, IN

REPORT DATE: 08/30/19 CT LABS PO # 147285 MITECH

ANALYSIS: HYDROMETER MI-TECH # 10967

METHOD: ASTM D422 DATE RECEIVED: 08/19/19

Dear Mr. Szymanski:

Analytical results for the above referenced project are enclosed. Thank you for your business.

Sincerely,Mi-Tech Services, Inc.

Stephanie M. Finamore, M.S., P.G.Environmental Manager

147285 - Page 137 of 142

Particle Size Distribution Report - Hydrometer Method

PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100

% +3" Coarse% Gravel

Fine Coarse Medium% Sand

Fine Silt% Fines

Clay0.0 0.0 0.8 1.0 3.3 55.5 27.0 12.4

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200

Test Results (ASTM D 422-63 & ASTM D 2217)Opening Percent Spec.* Pass?

Size Finer (Percent) (X=Fail)

Client Sample Description

Atterberg Limits (ASTM D 4318)

Classification

Coefficients

Date Received: Date Tested:Tested By:

Checked By:Title:

Date Sampled:Sample Number: 315103

Client:Project:

Project No: Figure

BWH-19-MU2-C2

.75#4

#10#40#200

0.0319 mm.0.0206 mm.0.0122 mm.0.0088 mm.0.0062 mm.0.0031 mm.0.0013 mm.

100.099.298.294.939.429.424.918.115.113.6

9.86.8

NP NP NP

SM A-4(0)

0.3650 0.3122 0.14290.1046 0.0336 0.00860.0032 44.78 2.47

ATTERBERG LIMITS TESTING NOT PERFORMED ON THISSAMPLE

8-20-19 8-20-2019CLZ - ENVIRO. TECHNICIAN

SMFENVIRONMENTAL MANAGER

8-13-19

CT LABORATORIES BURNS HARBOR, IN (PO# 147285 MITECH)

MI-TECH # 10967

PL= LL= PI=

USCS (D 2487)= AASHTO (M 145)=

D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks

* (no specification provided)

Mi-Tech Services, Inc.

Weston, WI 1

147285 - Page 138 of 142


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 1.1 2.2 1.2 50.8 31.9 12.8

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU2-C1

.75#4

#10#40#200

0.0319 mm.0.0206 mm.0.0122 mm.0.0088 mm.0.0064 mm.0.0031 mm.0.0013 mm.

100.098.996.795.544.733.128.622.618.114.3

9.87.5

NP NP NP

SM A-4(0)

0.3524 0.2970 0.12640.0898 0.0236 0.00680.0033 38.86 1.35




8-13-19


MI-TECH # 10967

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 2

147285 - Page 139 of 142


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 4.4 1.2 43.4 38.2 12.8

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU2-C3

#4#10#40#200

0.0315 mm.0.0204 mm.0.0118 mm.0.0088 mm.0.0064 mm.0.0031 mm.0.0013 mm.

100.095.694.451.036.331.022.718.214.4

9.85.3

NP NP NP

ML A-4(0)

0.3565 0.2919 0.10750.0708 0.0191 0.00670.0032 33.29 1.05




8-13-19


MI-TECH # 10967

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 3

147285 - Page 140 of 142


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.6 9.1 1.5 41.7 34.3 12.8

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

FD-1

.75#4

#10#40#200

0.0320 mm.0.0206 mm.0.0123 mm.0.0089 mm.0.0064 mm.0.0031 mm.0.0013 mm.

100.099.490.388.847.133.229.421.117.414.3

9.86.0

NP NP NP

SM A-4(0)

1.5134 0.3635 0.12830.0846 0.0220 0.00680.0032 39.59 1.16




8-13-19


MI-TECH # 10967

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 4

147285 - Page 141 of 142

147285 - Page 142 of 142







Page 1 of 48


147337 - Page 1 of 208



Project #: 3293191855.02.****




JOHN RALSTON



Contract #:



NOVI, MI 48377



09/09/2019

BURNS HARBOR, IN3293191855.02.****147337

3293191855.02.****3300

CT LAB#: 315732



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1100

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.7.39 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1



mg/kg66.0 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 18:59 ^36 EPA 350.118 2.00365.9

mg/kg58100 8/27/19 HLBCOD 08/23/2019 12:00 14:0015000 EPA 410.46800 1.00150002900




Metals Results






147337 - Page 2 of 208



Project #: 3293191855.02.****



CT LAB#: 315732



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1100

Analyte


DODLOD

Client Sample #:

mg/kg<0.038 8/20/19 NAHCadmium 08/19/2019 11:16 21:29U0.076 EPA 6010D0.038 1.000.0760.011






mg/kg0.11 B 8/20/19 NAHSelenium 08/19/2019 11:16 21:29J0.76 EPA 6010D0.38 1.000.760.11

mg/kg0.83 8/20/19 NAHSilver 08/19/2019 11:16 21:290.19 EPA 6010D0.095 1.000.190.032


Organic Results





ug/kg<86 8/22/19 RLDo-Xylene 08/22/2019 09:05 21:29U170 EPA 8260C86 1.0017024










ug/kg54.0 8/26/19 AJZAroclor-1248 08/20/2019 14:20 22:2154 EPA 8082A36 1.005413




147337 - Page 3 of 208



Project #: 3293191855.02.****



CT LAB#: 315732



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1100

Analyte


DODLOD

Client Sample #:









ug/kg71.9 8/27/19 JJYAnthracene 08/16/2019 16:00 21:067.0 EPA 8270D-SIM3.5 2.007.01.4











ug/kg58.5 8/27/19 JJYNaphthalene 08/16/2019 16:00 21:067.0 EPA 8270D-SIM3.5 2.007.01.7





Sub Lab Results



147337 - Page 4 of 208



Project #: 3293191855.02.****



CT LAB#: 315764



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1140

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.7.32 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1


mg/kg<410 8/19/19 JLHOil and Grease 08/19/2019 14:00 14:00U830 EPA 9071B410 1.00860210

mg/kg39.5 9/4/19 HLBAmmonia Nitrogen 09/04/2019 10:00 14:16 ^17 EPA 350.18.3 1.00172.7

mg/kg47700 M 8/27/19 HLBCOD 08/23/2019 12:00 14:0013000 EPA 410.46300 1.00130002700

mg/kg202 M,Y 8/22/19 JLHPhosphorus 08/21/2019 12:00 15:30 ^J290 EPA 365.4150 1.0029053


mg/kg<0.16 M 8/26/19 DGSHexavalent Chromium 08/23/2019 10:00 12:37U0.31 EPA 3060A/71990.16 1.000.310.068

Metals Results









mg/kg14.6 Y 8/20/19 NAHLead 08/19/2019 11:16 21:350.43 EPA 6010D0.21 1.000.430.068

mg/kg16.6 M 8/20/19 NAHNickel 08/19/2019 11:16 21:350.20 EPA 6010D0.10 1.000.200.036




Organic Results


147337 - Page 5 of 208



Project #: 3293191855.02.****



CT LAB#: 315764



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1140

Analyte


DODLOD

Client Sample #:











ug/kg<33 Y 8/23/19 AJZAroclor-1016 08/20/2019 14:20 17:12U50 EPA 8082A33 1.00508.3




ug/kg71.4 8/26/19 AJZAroclor-1248 08/20/2019 14:20 21:3950 EPA 8082A33 1.005012


ug/kg<33 Y 8/23/19 AJZAroclor-1260 08/20/2019 14:20 17:12U50 EPA 8082A33 1.005010










ug/kg70.0 8/28/19 JJYBenzo(a)anthracene 08/16/2019 16:00 01:533.3 EPA 8270D-SIM1.6 1.003.30.82

ug/kg60.1 8/28/19 JJYBenzo(a)pyrene 08/16/2019 16:00 01:533.3 EPA 8270D-SIM1.6 1.003.30.49


147337 - Page 6 of 208



Project #: 3293191855.02.****



CT LAB#: 315764



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1140

Analyte


DODLOD

Client Sample #:

ug/kg94.8 8/28/19 JJYBenzo(b)fluoranthene 08/16/2019 16:00 01:533.3 EPA 8270D-SIM1.6 1.003.30.65

ug/kg58.9 8/28/19 JJYBenzo(g,h,i)perylene 08/16/2019 16:00 01:533.3 EPA 8270D-SIM1.6 1.003.30.42

ug/kg30.7 8/28/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 01:536.5 EPA 8270D-SIM3.3 1.006.50.98

ug/kg72.8 8/28/19 JJYChrysene 08/16/2019 16:00 01:533.3 EPA 8270D-SIM1.6 1.003.30.36


ug/kg118 8/28/19 JJYFluoranthene 08/16/2019 16:00 01:536.5 EPA 8270D-SIM3.3 1.006.51.1


ug/kg44.5 8/28/19 JJYIndeno(1,2,3-cd)pyrene 08/16/2019 16:00 01:533.3 EPA 8270D-SIM1.6 1.003.30.65


ug/kg87.3 8/28/19 JJYPhenanthrene 08/16/2019 16:00 01:536.5 EPA 8270D-SIM3.3 1.006.51.8

ug/kg107 8/28/19 JJYPyrene 08/16/2019 16:00 01:536.5 EPA 8270D-SIM3.3 1.006.50.98



Sub Lab Results


CT LAB#: 315765



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1305

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.7.25 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS13.8 8/15/19 CLBE. coli 14:453 9223B3 1.0033



147337 - Page 7 of 208



Project #: 3293191855.02.****



CT LAB#: 315765



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1305

Analyte


DODLOD

Client Sample #:

mg/kg33.5 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 18:16 ^15 EPA 350.17.3 1.00152.4

mg/kg4150 8/27/19 HLBCOD 08/23/2019 12:00 14:001100 EPA 410.4530 1.001100230




Metals Results











mg/kg<0.30 8/20/19 NAHSelenium 08/19/2019 11:16 22:33U0.61 EPA 6010D0.30 1.000.610.091



Organic Results








147337 - Page 8 of 208



Project #: 3293191855.02.****



CT LAB#: 315765



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1305

Analyte


DODLOD

Client Sample #:









ug/kg35.1 8/26/19 AJZAroclor-1248 08/20/2019 14:20 22:42J44 EPA 8082A29 1.004410



















ug/kg71.8 8/27/19 JJYFluoranthene 08/16/2019 16:00 21:275.5 EPA 8270D-SIM2.7 1.005.50.96


147337 - Page 9 of 208



Project #: 3293191855.02.****



CT LAB#: 315765



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1305

Analyte


DODLOD

Client Sample #:





ug/kg66.2 8/27/19 JJYPyrene 08/16/2019 16:00 21:275.5 EPA 8270D-SIM2.7 1.005.50.82



Sub Lab Results


CT LAB#: 315766



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1352

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.6.89 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS5.97 8/15/19 CLBE. coli 14:454 9223B4 1.0044



mg/kg21000 8/26/19 HLBCOD 08/23/2019 12:00 16:072600 EPA 410.41200 1.002600530





147337 - Page 10 of 208



Project #: 3293191855.02.****



CT LAB#: 315766



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1352

Analyte


DODLOD

Client Sample #:

Metals Results














Organic Results













147337 - Page 11 of 208



Project #: 3293191855.02.****



CT LAB#: 315766



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1352

Analyte


DODLOD

Client Sample #:















ug/kg157 8/27/19 JJYAnthracene 08/16/2019 16:00 21:486.2 EPA 8270D-SIM3.1 2.006.21.2





ug/kg130 8/27/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 21:4812 EPA 8270D-SIM6.2 2.00121.9






ug/kg122 8/27/19 JJYNaphthalene 08/16/2019 16:00 21:486.2 EPA 8270D-SIM3.1 2.006.21.5




147337 - Page 12 of 208



Project #: 3293191855.02.****



CT LAB#: 315766



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1352

Analyte


DODLOD

Client Sample #:



Sub Lab Results


CT LAB#: 315808



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:

Inorganic Results

8/15/19 BMMSample Filtration 14:00 SOP #PR0071.00

Metals Results


CT LAB#: 315810



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.36 8/16/19 HLBpH 08:00 ^0.1 EPA 9040C0.1 1.000.10.1


ug/L<12 M 8/15/19 HLBHexavalent Chromium 11:56 Û24 EPA 7196A12 1.00246.0



mg/L<35 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515


147337 - Page 13 of 208



Project #: 3293191855.02.****



CT LAB#: 315810



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:




Metals Results






ug/L0.84 B 8/20/19 NAHTotal Chromium 08/19/2019 09:54 20:07J4.0 EPA 6010D2.0 1.004.00.60







ug/L1.7 8/20/19 NAHTotal Zinc 08/19/2019 09:54 20:07J10 EPA 6010D5.0 1.00101.6

mg/L130 8/20/19 NAHTotal Hardness 08/19/2019 08: 20:070.41 SM2340B/6010D0.21 1.000.410.067

Organic Results









147337 - Page 14 of 208



Project #: 3293191855.02.****



CT LAB#: 315810



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:






























147337 - Page 15 of 208



Project #: 3293191855.02.****



CT LAB#: 315810



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:





















08/19/2019 12:00 12:43U2.0 EPA 8270D0.80 1.002.00.52










147337 - Page 16 of 208



Project #: 3293191855.02.****



CT LAB#: 315810



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:






























147337 - Page 17 of 208



Project #: 3293191855.02.****



CT LAB#: 315810



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1435

Analyte


DODLOD

Client Sample #:












ug/L<0.020 8/26/19 JJYFluoranthene 08/19/2019 12:00 19:19U0.040 EPA 8270D-SIM0.020 1.000.0400.0090








CT LAB#: 315815



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:

Inorganic Results



147337 - Page 18 of 208



Project #: 3293191855.02.****



CT LAB#: 315815



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:

Metals Results


CT LAB#: 315816



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.43 8/16/19 HLBpH 08:00 ^0.1 EPA 9040C0.1 1.000.10.1





mg/L<35 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515




Metals Results








ug/L16.8 8/20/19 NAHTotal Iron 08/19/2019 09:54 20:13J100 EPA 6010D50 1.0010016


147337 - Page 19 of 208



Project #: 3293191855.02.****



CT LAB#: 315816



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:





ug/L3.0 8/20/19 NAHTotal Zinc 08/19/2019 09:54 20:13J10 EPA 6010D5.0 1.00101.6


Organic Results






















147337 - Page 20 of 208



Project #: 3293191855.02.****



CT LAB#: 315816



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:






























147337 - Page 21 of 208



Project #: 3293191855.02.****



CT LAB#: 315816



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:








08/19/2019 12:00 13:02U2.0 EPA 8270D0.80 1.002.00.52























147337 - Page 22 of 208



Project #: 3293191855.02.****



CT LAB#: 315816



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:






























147337 - Page 23 of 208



Project #: 3293191855.02.****



CT LAB#: 315816



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1510

Analyte


DODLOD

Client Sample #:







CT LAB#: 315817



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results


CT LAB#: 315818



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.42 8/16/19 HLBpH 08:00 ^0.1 EPA 9040C0.1 1.000.10.1






147337 - Page 24 of 208



Project #: 3293191855.02.****



CT LAB#: 315818



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:

mg/L<35 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515




Metals Results















Organic Results








147337 - Page 25 of 208



Project #: 3293191855.02.****



CT LAB#: 315818



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:






























147337 - Page 26 of 208



Project #: 3293191855.02.****



CT LAB#: 315818



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:






















08/19/2019 12:00 13:20U2.0 EPA 8270D0.82 1.002.00.53









147337 - Page 27 of 208



Project #: 3293191855.02.****



CT LAB#: 315818



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:






























147337 - Page 28 of 208



Project #: 3293191855.02.****



CT LAB#: 315818



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019 1600

Analyte


DODLOD

Client Sample #:





















CT LAB#: 315825



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019

Analyte


DODLOD

Client Sample #:

Organic Results



147337 - Page 29 of 208



Project #: 3293191855.02.****



CT LAB#: 315827



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019

Analyte


DODLOD

Client Sample #:

Organic Results


CT LAB#: 315828



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019

Analyte


DODLOD

Client Sample #:

Organic Results


CT LAB#: 315829



AnalysisDate/Time

Analyst Method

Sampled: 08/14/2019

Analyte


DODLOD

Client Sample #:

Organic Results












147337 - Page 30 of 208



Project #: 3293191855.02.****



CT LAB#: 317096



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 1610

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.12 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1





mg/L21 8/26/19 HLBCOD 08/22/2019 12:00 15:50 ^J75 EPA 410.435 1.007515



mg/L<2.0 8/20/19 GMJTotal Suspended Solids 17:45U2.0 SM 2540D2.0 1.002.02.0

Metals Results








ug/L538 8/22/19 NAHTotal Iron 08/21/2019 11:24 18:20100 EPA 6010D50 1.0010016

ug/L2.3 8/22/19 NAHTotal Lead 08/21/2019 11:24 18:20J4.0 EPA 6010D2.0 1.004.01.4






Organic Results


147337 - Page 31 of 208



Project #: 3293191855.02.****



CT LAB#: 317096



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 1610

Analyte


DODLOD

Client Sample #:






























147337 - Page 32 of 208



Project #: 3293191855.02.****



CT LAB#: 317096



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 1610

Analyte


DODLOD

Client Sample #:




























08/19/2019 12:00 14:51U2.1 EPA 8270D0.82 1.002.10.54



147337 - Page 33 of 208



Project #: 3293191855.02.****



CT LAB#: 317096



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 1610

Analyte


DODLOD

Client Sample #:











ug/L2.6 8/23/19 JJYDi-n-butylphthalate 08/19/2019 12:00 14:51J4.1 EPA 8270D2.1 1.004.10.69



ug/L0.62 8/23/19 JJYDiethylphthalate 08/19/2019 12:00 14:51J2.1 EPA 8270D1.0 1.002.10.46
















147337 - Page 34 of 208



Project #: 3293191855.02.****



CT LAB#: 317096



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 1610

Analyte


DODLOD

Client Sample #:














ug/L0.035 B 8/26/19 JJYBenzo(b)fluoranthene 08/19/2019 12:00 21:44J0.041 EPA 8270D-SIM0.021 1.000.0410.0072

ug/L0.057 8/26/19 JJYBenzo(g,h,i)perylene 08/19/2019 12:00 21:440.041 EPA 8270D-SIM0.021 1.000.0410.0062





ug/L0.010 8/26/19 JJYFluorene 08/19/2019 12:00 21:44J0.041 EPA 8270D-SIM0.021 1.000.0410.0093








147337 - Page 35 of 208



Project #: 3293191855.02.****



CT LAB#: 317097



AnalysisDate/Time

Analyst Method

Sampled: 08/19/2019 1610

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results

ug/L33.3 8/22/19 NAHDissolved Iron 08/21/2019 11:24 19:17J100 EPA 6010C50 1.0010016

CT LAB#: 317100



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.03 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1



mg/L6.5 M 9/4/19 HLBAmmonia Nitrogen 13:29 ^1.0 EPA 350.10.50 5.001.00.11


mg/L29 M 8/26/19 HLBCOD 08/22/2019 12:00 15:50 ^J75 EPA 410.435 1.007515



mg/L2.2 8/23/19 GMJTotal Suspended Solids 15:002.0 SM 2540D2.0 1.002.02.0

Metals Results



ug/L6.1 8/22/19 NAHTotal Arsenic 08/21/2019 11:24 18:27J24 EPA 6010D12 1.00244.0




147337 - Page 36 of 208



Project #: 3293191855.02.****



CT LAB#: 317100



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:





ug/L1.0 8/22/19 NAHTotal Nickel 08/21/2019 11:24 18:27J6.0 EPA 6010D3.0 1.006.01.0





Organic Results



















147337 - Page 37 of 208



Project #: 3293191855.02.****



CT LAB#: 317100



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:






























147337 - Page 38 of 208



Project #: 3293191855.02.****



CT LAB#: 317100



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:











08/19/2019 12:00 15:09U2.0 EPA 8270D0.81 1.002.00.53




















147337 - Page 39 of 208



Project #: 3293191855.02.****



CT LAB#: 317100



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:
























ug/L0.039 B 8/26/19 JJYBenzo(a)pyrene 08/19/2019 12:00 22:05J0.040 EPA 8270D-SIM0.020 1.000.0400.0061






147337 - Page 40 of 208



Project #: 3293191855.02.****



CT LAB#: 317100



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:










CT LAB#: 317101



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1415

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results


CT LAB#: 317102



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.41 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1



147337 - Page 41 of 208



Project #: 3293191855.02.****



CT LAB#: 317102



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:




mg/L24 8/26/19 HLBCOD 08/22/2019 12:00 15:50 ^J75 EPA 410.435 1.007515



mg/L43 8/23/19 GMJTotal Suspended Solids 15:002.0 SM 2540D2.0 1.002.02.0

Metals Results











ug/L2.7 8/22/19 NAHTotal Selenium 08/21/2019 11:24 18:34J13 EPA 6010D6.5 1.00132.2




Organic Results





147337 - Page 42 of 208



Project #: 3293191855.02.****



CT LAB#: 317102



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:






























147337 - Page 43 of 208



Project #: 3293191855.02.****



CT LAB#: 317102



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:

























08/19/2019 12:00 15:27U2.0 EPA 8270D0.80 1.002.00.52






147337 - Page 44 of 208



Project #: 3293191855.02.****



CT LAB#: 317102



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:




ug/L2.7 8/23/19 JJYBis(2-ethylhexyl)phthalate 08/19/2019 12:00 15:272.0 EPA 8270D1.0 1.002.00.44





ug/L0.67 8/23/19 JJYDi-n-octylphthalate 08/19/2019 12:00 15:27J2.0 EPA 8270D1.0 1.002.00.49





















147337 - Page 45 of 208



Project #: 3293191855.02.****



CT LAB#: 317102



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:










ug/L0.041 B 8/26/19 JJYBenzo(a)pyrene 08/19/2019 12:00 22:260.040 EPA 8270D-SIM0.020 1.000.0400.0060



ug/L0.010 8/26/19 JJYBenzo(k)fluoranthene 08/19/2019 12:00 22:26J0.040 EPA 8270D-SIM0.020 1.000.0400.010

ug/L0.0086 B 8/26/19 JJYChrysene 08/19/2019 12:00 22:26J0.040 EPA 8270D-SIM0.020 1.000.0400.0070










CT LAB#: 317103



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:


147337 - Page 46 of 208



Project #: 3293191855.02.****



CT LAB#: 317103



AnalysisDate/Time

Analyst Method

Sampled: 08/20/2019 1500

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results



147337 - Page 47 of 208









147337 - Page 48 of 208



QC SUMMARY REPORT



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 49 of 208





CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 50 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 51 of 208





CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 52 of 208



Matrix Spike Water


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 53 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult


Total Suspended Solids mg/L U 0 464.00 <4.00




147337 - Page 54 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163619Method: SM2540C

Total Dissolved Solids mg/L 7 25182 170




147337 - Page 55 of 208



Duplicate

08/19/2019Analytical Run #: Analysis Date:09:30Analysis Time:317156CLB

CTLab #:Analyst:

Prep Batch #:


SOILMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult


pH S.U. 0 17.35 7.32




147337 - Page 56 of 208





CTLab #:Analyst:

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LIQUIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163646Method: E350.1





147337 - Page 57 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163646Method: E350.1





147337 - Page 58 of 208



LOQ Check Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 59 of 208





73206

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163670Method: E350.108/19/201912:00





147337 - Page 60 of 208



Method Blank Soil


73206

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163670Method: E350.108/19/201912:00





147337 - Page 61 of 208





CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 62 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 63 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1

Phosphorus mg/L U 0 250.300 <0.300




147337 - Page 64 of 208





CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1

Phosphorus mg/L 96 1103.85 90 ---4.00




147337 - Page 65 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1





147337 - Page 66 of 208





CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1

Phosphorus mg/L 98 120 7 253.9 BDL 80 ---4.0




147337 - Page 67 of 208





CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1

Phosphorus mg/L 100 120 1 254.0 BDL 80 ---4.0




147337 - Page 68 of 208



Matrix Spike Water


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1

Phosphorus mg/L 92 120 253.7 BDL 80 ---4.0




147337 - Page 69 of 208



Matrix Spike Water


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163717Method: E365.1

Phosphorus mg/L 100 120 254.0 BDL 80 ---4.0




147337 - Page 70 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 71 of 208





CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 72 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 73 of 208





CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 74 of 208



Matrix Spike Water


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 75 of 208



Duplicate


73238

JLHCTLab #:

Analyst:

Prep Batch #:


SOIL

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163744Method: E365.408/21/201912:00

Phosphorus mg/kg 28 20268 202




147337 - Page 76 of 208





73238

JLHCTLab #:

Analyst:

Prep Batch #:


SOLID

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163744Method: E365.408/21/201912:00

Phosphorus mg/kg 102 1101020 90 ---1000




147337 - Page 77 of 208



Method Blank Soil


73238

JLHCTLab #:

Analyst:

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SOLID

JLH

Matrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163744Method: E365.408/21/201912:00





147337 - Page 78 of 208





73238

JLHCTLab #:

Analyst:

Prep Batch #:


SOIL

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163744Method: E365.408/21/201912:00

Phosphorus mg/kg 56 110 8 20573 202 90 ---657




147337 - Page 79 of 208



Matrix Spike Soil


73238

JLHCTLab #:

Analyst:

Prep Batch #:


SOIL

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163744Method: E365.408/21/201912:00

Phosphorus mg/kg 50 110535 202 90 ---665




147337 - Page 80 of 208



Duplicate

08/22/2019Analytical Run #: Analysis Date:11:10Analysis Time:319749CLB

CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163747Method: SM2540C

Total Dissolved Solids mg/L 12 25215 190




147337 - Page 81 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 2 20123 120




147337 - Page 82 of 208





CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 102 110382.0 90 ---375.0




147337 - Page 83 of 208



LOQ Check Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 103 11031.00 90 ---30.00




147337 - Page 84 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2





147337 - Page 85 of 208





CTLab #:Analyst:

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GROUND WATERMatrix:

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ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 101 110 1 20221 120 90 ---100




147337 - Page 86 of 208





CTLab #:Analyst:

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GROUND WATERMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 103 110 1 20223 120 90 ---100




147337 - Page 87 of 208



Matrix Spike Water


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 103 110 20223 120 90 ---100




147337 - Page 88 of 208



Matrix Spike Water


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163789Method: E310.2

Alkalinity mg/L 101 110 20221 120 90 ---100




147337 - Page 89 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


SOILMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult


Total Organic Carbon mg/kg 8 3049000 45100




147337 - Page 90 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


SOILMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 91 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


SOILMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 92 of 208





CTLab #:Analyst:

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SOLIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 93 of 208



Method Blank Soil


CTLab #:Analyst:

Prep Batch #:


SOLIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 94 of 208



Duplicate


CTLab #:Analyst:

Prep Batch #:


GROUND WATERMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult


Total Suspended Solids mg/L 19 4635.6 43 W




147337 - Page 95 of 208



Duplicate


73266

HLBCTLab #:

Analyst:

Prep Batch #:


GROUND WATER

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163838Method: E410.408/22/201912:00

COD mg/L 1 2028.6 29




147337 - Page 96 of 208





73266

HLBCTLab #:

Analyst:

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LIQUID

HLB

Matrix:

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RPDLimit

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Parentsampleresult

163838Method: E410.408/23/201912:00

COD mg/L 98 110393.0 90 ---400.0




147337 - Page 97 of 208



Method Blank Water


73266

HLBCTLab #:

Analyst:

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HLB

Matrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163838Method: E410.408/23/201912:00





147337 - Page 98 of 208





73266

HLBCTLab #:

Analyst:

Prep Batch #:


GROUND WATER

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163838Method: E410.408/22/201912:00

COD mg/L 107 110 4 20187 29 90 ---148




147337 - Page 99 of 208



Matrix Spike Water


73266

HLBCTLab #:

Analyst:

Prep Batch #:


GROUND WATER

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163838Method: E410.408/22/201912:00

COD mg/L 111 110194 29 90 ---148




147337 - Page 100 of 208



Duplicate


73264

HLBCTLab #:

Analyst:

Prep Batch #:


SOIL

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg 17 4040200 47700




147337 - Page 101 of 208





73264

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

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Matrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg 98 1001950 90 ---2000




147337 - Page 102 of 208



Method Blank Soil


73264

HLBCTLab #:

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SOLID

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Matrix:

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Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg U 3815 0




147337 - Page 103 of 208





73264

HLBCTLab #:

Analyst:

Prep Batch #:


SOIL

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Matrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg 100 110 21 3075900 47700 90 ---28300




147337 - Page 104 of 208



Matrix Spike Soil


73264

HLBCTLab #:

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SOIL

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Matrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg 160 11092600 47700 90 ---28100




147337 - Page 105 of 208



Duplicate


73155

JLHCTLab #:

Analyst:

Prep Batch #:


SOIL

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163908Method: SW166408/19/201914:00

Oil and Grease mg/kg U 0 20200 <200




147337 - Page 106 of 208





73155

JLHCTLab #:

Analyst:

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RPDLimit

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163908Method: SW166408/19/201914:00





147337 - Page 107 of 208



Method Blank Soil


73155

JLHCTLab #:

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Parentsampleresult

163908Method: SW166408/19/201914:00





147337 - Page 108 of 208



Matrix Spike Soil


73155

JLHCTLab #:

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Prep Batch #:


SOIL

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163908Method: SW166408/19/201914:00

Oil and Grease mg/kg 105 1306910 BDL 70 ---6570




147337 - Page 109 of 208





73284

JLHCTLab #:

Analyst:

Prep Batch #:


LIQUID

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Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


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Parentsampleresult

163925Method: SW166408/26/201909:00





147337 - Page 110 of 208



Method Blank Water


73284

JLHCTLab #:

Analyst:

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Matrix:

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RPDLimit

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Parentsampleresult

163925Method: SW166408/26/201909:00





147337 - Page 111 of 208



Duplicate

08/27/2019Analytical Run #: Analysis Date:15:09Analysis Time:321065BMM

CTLab #:Analyst:

Prep Batch #:


SOILMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult


Solids, Percent % 1 859.0 59.4




147337 - Page 112 of 208



Duplicate


73271

DGSCTLab #:

Analyst:

Prep Batch #:


SOIL

DGS

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


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Parentsampleresult

163949Method: SW719908/23/201910:00

Hexavalent Chromium mg/kg U 0 200.0681 <0.0681




147337 - Page 113 of 208





73271

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163949Method: SW719908/23/201910:00





147337 - Page 114 of 208



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73271

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163949Method: SW719908/23/201910:00





147337 - Page 115 of 208





73271

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163949Method: SW719908/23/201910:00

Hexavalent Chromium mg/kg 30 125 2 201.01 BDL 75 ---3.33




147337 - Page 116 of 208



Matrix Spike Soil


73271

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Parentsampleresult

163949Method: SW719908/23/201910:00

Hexavalent Chromium mg/kg 30 1250.992 BDL 75 ---3.33




147337 - Page 117 of 208



Matrix Spike Soil


73271

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Parentsampleresult

163949Method: SW719908/23/201910:00

Hexavalent Chromium mg/kg 39 125520 BDL 75 ---1350




147337 - Page 118 of 208



Duplicate


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Prep Batch #:


GROUND WATERMatrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

164099Method: E350.1

Ammonia Nitrogen mg/L 2 206.40 6.5




147337 - Page 119 of 208





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164099Method: E350.1





147337 - Page 120 of 208



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164099Method: E350.1





147337 - Page 121 of 208





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Parentsampleresult

164099Method: E350.1

Ammonia Nitrogen mg/L 19 120 0 207.70 6.5 80 ---6.25




147337 - Page 122 of 208



Matrix Spike Water


CTLab #:Analyst:

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GROUND WATERMatrix:

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RPDLimit

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ControlLimits


Parentsampleresult

164099Method: E350.1

Ammonia Nitrogen mg/L 19 120 207.70 6.5 80 ---6.25




147337 - Page 123 of 208



Duplicate


73389

HLBCTLab #:

Analyst:

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SOIL

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

164100Method: E350.109/04/201910:00

Ammonia Nitrogen mg/kg 12 2544.7 39.5




147337 - Page 124 of 208





73389

HLBCTLab #:

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SOLID

HLB

Matrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

164100Method: E350.109/04/201910:00





147337 - Page 125 of 208



Method Blank Soil


73389

HLBCTLab #:

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HLB

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RPDLimit

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164100Method: E350.109/04/201910:00





147337 - Page 126 of 208





73389

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Parentsampleresult

164100Method: E350.109/04/201910:00

Ammonia Nitrogen mg/kg 84 120 2 2567.5 39.5 80 ---33.4




147337 - Page 127 of 208



Matrix Spike Soil


73389

HLBCTLab #:

Analyst:

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SOIL

HLB

Matrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

164100Method: E350.109/04/201910:00

Ammonia Nitrogen mg/kg 82 12067.2 39.5 80 ---33.9




147337 - Page 128 of 208



Duplicate


73157

NAHCTLab #:

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NAH

Matrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163656Method: SW601008/19/201909:54

Total Aluminum ug/L 36 8 2011.6 12.6Total Arsenic ug/L U 24 0 204.00 <4.00Total Barium ug/L 1.80 1 2021.4 21.2Total Cadmium ug/L U 2.0 0 200.300 <0.300Total Chromium ug/L 4.0 21 200.98 0.79Total Copper ug/L 7.0 22 201.5 1.2Total Iron ug/L U 100 0 2016.0 <16.0Total Lead ug/L U 4.0 0 201.40 <1.40Total Nickel ug/L U 6.0 0 201.00 <1.00Total Selenium ug/L U 13.0 0 202.20 <2.20Total Silver ug/L U 4.0 0 200.700 <0.700Total Zinc ug/L U 10.0 0 201.60 <1.60




147337 - Page 129 of 208





73157

NAHCTLab #:

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LIQUID

NAH

Matrix:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163656Method: SW601008/19/201909:54





147337 - Page 130 of 208



Method Blank Water


73157

NAHCTLab #:

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NAH

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Parentsampleresult

163656Method: SW601008/19/201909:54

Total Aluminum ug/L U 186 0Total Arsenic ug/L U 124 0Total Barium ug/L U 0.900.29 0Total Cadmium ug/L U 1.00.3 0Total Chromium ug/L 2.00.703 0Total Copper ug/L U 3.51.2 0Total Iron ug/L U 5016 0Total Lead ug/L U 2.01.4 0Total Nickel ug/L U 3.01.0 0Total Selenium ug/L 6.53.11 0Total Silver ug/L U 2.00.7 0Total Zinc ug/L U 5.01.6 0




147337 - Page 131 of 208





73157

NAHCTLab #:

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NAH

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Parentsampleresult

163656Method: SW601008/19/201909:54

Total Aluminum ug/L 107 115 1 20868 12.6 86 ---800Total Arsenic ug/L 99 113 0 20794 BDL 87 ---800Total Barium ug/L 101 113 1 20827 21.2 88 ---800Total Cadmium ug/L 98 113 1 2019.6 BDL 88 ---20.0Total Chromium ug/L 103 113 2 2083.1 0.79 90 ---80.0Total Copper ug/L 114 114 2 20115 1.2 86 ---100Total Iron ug/L 103 115 3 20413 BDL 87 ---400Total Lead ug/L 101 113 1 20202 BDL 86 ---200Total Nickel ug/L 96 113 1 20192 BDL 88 ---200Total Selenium ug/L 93 114 0 20743 BDL 83 ---800Total Silver ug/L 92 115 3 2018.3 BDL 84 ---20.0Total Zinc ug/L 100 115 0 20201 BDL 87 ---200




147337 - Page 132 of 208



Matrix Spike Water


73157

NAHCTLab #:

Analyst:

Prep Batch #:


GROUND WATER

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163656Method: SW601008/19/201909:54

Total Aluminum ug/L 108 115877 12.6 86 ---800Total Arsenic ug/L 100 113797 BDL 87 ---800Total Barium ug/L 101 113832 21.2 88 ---800Total Cadmium ug/L 99 11319.8 BDL 88 ---20.0Total Chromium ug/L 106 11385.2 0.79 90 ---80.0Total Copper ug/L 116 114117 1.2 86 ---100Total Iron ug/L 106 115426 BDL 87 ---400Total Lead ug/L 102 113204 BDL 86 ---200Total Nickel ug/L 96 113193 BDL 88 ---200Total Selenium ug/L 93 114745 BDL 83 ---800Total Silver ug/L 94 11518.8 BDL 84 ---20.0Total Zinc ug/L 101 115202 BDL 87 ---200




147337 - Page 133 of 208



Duplicate


73176

NAHCTLab #:

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Prep Batch #:


SOIL

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163668Method: SW601008/19/201911:16

Aluminum mg/kg 9.6 8 206470 5950Arsenic mg/kg 32 4 205.1 4.9Barium mg/kg 2.0 6 2038.8 36.6Cadmium mg/kg U 1.60 0 200.0102 <0.0102Chromium mg/kg 5.6 12 2019.5 17.3Copper mg/kg 16.0 16 2019.4 16.6Iron mg/kg 72 6 2016500 15600Lead mg/kg 10.0 22 2018.3 14.6Nickel mg/kg 4.8 8 2017.9 16.6Selenium mg/kg U 16 200 200.102 0.15Silver mg/kg 4.0 7 200.89 0.83Zinc mg/kg 12.0 12 2068.5 60.8




147337 - Page 134 of 208





73176

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Parentsampleresult

163668Method: SW601008/19/201911:16

Aluminum mg/kg 91 11991.3 74 ---100Arsenic mg/kg 90 11190.5 82 ---100Barium mg/kg 94 11394.0 83 ---100Cadmium mg/kg 104 1132.6 82 ---2.5Chromium mg/kg 98 1139.8 85 ---10.0Copper mg/kg 90 11711.2 81 ---12.5Iron mg/kg 98 11849.0 81 ---50.0Lead mg/kg 93 11223.3 81 ---25.0Nickel mg/kg 89 11322.2 83 ---25.0Selenium mg/kg 93 11192.8 78 ---100Silver mg/kg 88 1122.2 82 ---2.5Zinc mg/kg 92 11323.1 82 ---25.0




147337 - Page 135 of 208



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73176

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Parentsampleresult

163668Method: SW601008/19/201911:16

Aluminum mg/kg 0.120.23 0Arsenic mg/kg U 0.400.13 0Barium mg/kg U 0.0250.009 0Cadmium mg/kg U 0.0200.006 0Chromium mg/kg U 0.1250.023 0Copper mg/kg U 0.200.07 0Iron mg/kg 0.90.34 0Lead mg/kg U 0.1250.04 0Nickel mg/kg U 0.0600.021 0Selenium mg/kg 0.200.14 0Silver mg/kg U 0.0500.017 0Zinc mg/kg U 0.150.05 0




147337 - Page 136 of 208





73176

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Parentsampleresult

163668Method: SW601008/19/201911:16

Aluminum mg/kg 500 119 5 206800 5950 74 ---170Arsenic mg/kg 92 111 0 20161 4.9 82 ---170Barium mg/kg 93 113 0 20194 36.6 83 ---170Cadmium mg/kg 116 113 2 205.0 BDL 82 ---4.3Chromium mg/kg 106 113 3 2035.4 17.3 85 ---17.0Copper mg/kg 95 117 0 2036.9 16.6 81 ---21.3Iron mg/kg 1412 118 5 2016800 15600 81 ---85.0Lead mg/kg 112 112 1 2062.1 14.6 81 ---42.5Nickel mg/kg 80 113 2 2050.6 16.6 83 ---42.5Selenium mg/kg 73 111 4 20125 0.15 78 ---170Silver mg/kg 85 112 0 204.5 0.83 82 ---4.3Zinc mg/kg 104 113 4 20105 60.8 82 ---42.5




147337 - Page 137 of 208



Matrix Spike Soil


73176

NAHCTLab #:

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SOIL

NAH

Matrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163668Method: SW601008/19/201911:16

Aluminum mg/kg 300 1196460 5950 74 ---170Arsenic mg/kg 92 111161 4.9 82 ---170Barium mg/kg 92 113193 36.6 83 ---170Cadmium mg/kg 114 1134.9 BDL 82 ---4.3Chromium mg/kg 113 11336.5 17.3 85 ---17.0Copper mg/kg 94 11736.7 16.6 81 ---21.3Iron mg/kg 588 11816100 15600 81 ---85.0Lead mg/kg 110 11261.2 14.6 81 ---42.5Nickel mg/kg 78 11349.7 16.6 83 ---42.5Selenium mg/kg 77 111131 0.15 78 ---170Silver mg/kg 85 1124.5 0.83 82 ---4.3Zinc mg/kg 113 113109 60.8 82 ---42.5




147337 - Page 138 of 208



Duplicate


73149

MDSCTLab #:

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Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg 0.20 3 200.031 0.032




147337 - Page 139 of 208





73149

MDSCTLab #:

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Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg 101 1240.084 82 ---0.083




147337 - Page 140 of 208



Method Blank Soil


73149

MDSCTLab #:

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Parentsampleresult

163732Method: SW7471B08/20/201909:59





147337 - Page 141 of 208





73149

MDSCTLab #:

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SOIL

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RPDLimit

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Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg 92 124 1 200.17 0.032 82 ---0.15




147337 - Page 142 of 208



Matrix Spike Soil


73149

MDSCTLab #:

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SOIL

BMM

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg 92 1240.17 0.032 82 ---0.15




147337 - Page 143 of 208



Duplicate


73232

NAHCTLab #:

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GROUND WATER

NAH

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ControlLimits


Parentsampleresult

163782Method: SW601008/21/201911:24

Dissolved Iron ug/L 100 6 2035.4 33.3




147337 - Page 144 of 208





73232

NAHCTLab #:

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RPDLimit

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Parentsampleresult

163782Method: SW601008/21/201911:24





147337 - Page 145 of 208



Method Blank Water


73232

NAHCTLab #:

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SpikeAmountAdded


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Parentsampleresult

163782Method: SW601008/21/201911:24





147337 - Page 146 of 208





73232

NAHCTLab #:

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NAH

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RPDLimit

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Parentsampleresult

163782Method: SW601008/21/201911:24

Dissolved Iron ug/L 101 115 2 20438 33.3 87 ---400




147337 - Page 147 of 208



Matrix Spike Water


73232

NAHCTLab #:

Analyst:

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GROUND WATER

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163782Method: SW601008/21/201911:24

Dissolved Iron ug/L 99 115431 33.3 87 ---400




147337 - Page 148 of 208





73233

NAHCTLab #:

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163783Method: SW601008/21/201911:24





147337 - Page 149 of 208



Method Blank Water


73233

NAHCTLab #:

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RPDLimit

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Parentsampleresult

163783Method: SW601008/21/201911:24





147337 - Page 150 of 208





73152

MDSCTLab #:

Analyst:

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BMM

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Prep Analyst:

RPDLimit

SpikeAmountAdded


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Parentsampleresult

163791Method: SW7470A08/21/201914:51





147337 - Page 151 of 208



Method Blank Water


73152

MDSCTLab #:

Analyst:

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LIQUID

BMM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


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Parentsampleresult

163791Method: SW7470A08/21/201914:51





147337 - Page 152 of 208



Duplicate


73169

NAHCTLab #:

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NAH

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RPDLimit

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ControlLimits


Parentsampleresult

163830Method: SW601008/23/201909:47

Dissolved Iron ug/L U 100 0 2016.0 <16.0




147337 - Page 153 of 208





73169

NAHCTLab #:

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RPDLimit

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Parentsampleresult

163830Method: SW601008/23/201909:47





147337 - Page 154 of 208



Method Blank Water


73169

NAHCTLab #:

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163830Method: SW601008/23/201909:47





147337 - Page 155 of 208





73169

NAHCTLab #:

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GROUND WATER

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


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Parentsampleresult

163830Method: SW601008/23/201909:47





147337 - Page 156 of 208



Matrix Spike Water


73169

NAHCTLab #:

Analyst:

Prep Batch #:


GROUND WATER

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163830Method: SW601008/23/201909:47





147337 - Page 157 of 208





CTLab #:Analyst:

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Parentsampleresult


Benzene ug/L 108 120 0 2010.8 79 ---10.0Ethylbenzene ug/L 103 121 4 2010.3 79 ---10.0m & p-Xylene ug/L 104 121 6 2020.7 80 ---20.0Methyl tert-butyl ether ug/L 106 124 6 2010.6 71 ---10.0o-Xylene ug/L 105 122 5 2010.5 78 ---10.0Toluene ug/L 102 121 1 2010.2 80 ---10.0




147337 - Page 158 of 208





CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 159 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 160 of 208





CTLab #:Analyst:

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LIQUIDMatrix:

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ControlLimits


Parentsampleresult






147337 - Page 161 of 208



Method Blank Water


CTLab #:Analyst:

Prep Batch #:


LIQUIDMatrix:

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RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147337 - Page 162 of 208





73259

RLDCTLab #:

Analyst:

Prep Batch #:


SOLID

RLD

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RPDLimit

SpikeAmountAdded


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Parentsampleresult

163774Method: SW8260C08/22/201909:05





147337 - Page 163 of 208



Method Blank Soil


73259

RLDCTLab #:

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SOLID

RLD

Matrix:

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RPDLimit

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Parentsampleresult

163774Method: SW8260C08/22/201909:05





147337 - Page 164 of 208





73259

RLDCTLab #:

Analyst:

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SOIL

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RPDLimit

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Parentsampleresult

163774Method: SW8260C08/22/201909:05

1,2 Dichloroethane-d4 % Recovery 103 136103 71 ---100Benzene ug/kg 101 121 3 20604 BDL 77 ---596Bromofluorobenzene % Recovery 100 119100 79 ---100d8-Toluene % Recovery 99.0 11699.0 85 ---100Dibromofluoromethane % Recovery 101 119101 78 ---100Ethylbenzene ug/kg 99 122 2 20591 BDL 76 ---596m & p-Xylene ug/kg 97 124 2 201150 BDL 77 ---1190Methyl tert-butyl ether ug/kg 108 125 2 20643 BDL 73 ---596o-Xylene ug/kg 103 123 2 20613 BDL 77 ---596Toluene ug/kg 101 121 3 20602 BDL 77 ---596




147337 - Page 165 of 208



Matrix Spike Soil


73259

RLDCTLab #:

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SOIL

RLD

Matrix:

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RPDLimit

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Parentsampleresult

163774Method: SW8260C08/22/201909:05

1,2 Dichloroethane-d4 % Recovery 100 136100 71 ---100Benzene ug/kg 104 121621 BDL 77 ---596Bromofluorobenzene % Recovery 99.0 11999.0 79 ---100d8-Toluene % Recovery 99.0 11699.0 85 ---100Dibromofluoromethane % Recovery 100 119100 78 ---100Ethylbenzene ug/kg 101 122603 BDL 76 ---596m & p-Xylene ug/kg 99 1241180 BDL 77 ---1190Methyl tert-butyl ether ug/kg 106 125630 BDL 73 ---596o-Xylene ug/kg 105 123626 BDL 77 ---596Toluene ug/kg 104 121620 BDL 77 ---596




147337 - Page 166 of 208





73201

AJZCTLab #:

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Parentsampleresult

163780Method: SW808208/20/201909:00





147337 - Page 167 of 208





73201

AJZCTLab #:

Analyst:

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LIQUID

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RPDLimit

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Parentsampleresult

163780Method: SW808208/20/201909:00





147337 - Page 168 of 208



Method Blank Water


73201

AJZCTLab #:

Analyst:

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RPDLimit

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Parentsampleresult

163780Method: SW808208/20/201909:00





147337 - Page 169 of 208





73143

JJYCTLab #:

Analyst:

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SOLID

MCM

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RPDLimit

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Parentsampleresult

163812Method: SW8270SIM08/16/201916:00





147337 - Page 170 of 208



Method Blank Soil


73143

JJYCTLab #:

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RPDLimit

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Parentsampleresult

163812Method: SW8270SIM08/16/201916:00





147337 - Page 171 of 208





73143

JJYCTLab #:

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Parentsampleresult

163812Method: SW8270SIM08/16/201916:00

1-Methylnaphthalene ug/kg 62 111 12 40115 16.5 43 ---1602-Methylnaphthalene ug/kg 74 114 10 40146 27.0 39 ---160Acenaphthene ug/kg 66 111 10 40116 10.2 44 ---160Acenaphthylene ug/kg 89 116 4 40149 6.01 39 ---160Anthracene ug/kg 83 114 4 40155 21.7 50 ---160Benzo(a)anthracene ug/kg 104 122 2 40236 70.0 54 ---160Benzo(a)pyrene ug/kg 87 125 5 40199 60.1 50 ---160Benzo(b)fluoranthene ug/kg 96 128 4 40249 94.8 53 ---160Benzo(g,h,i)perylene ug/kg 68 127 0 40167 58.9 49 ---160Benzo(k)fluoranthene ug/kg 75 123 2 40150 30.7 56 ---160Chrysene ug/kg 94 118 1 40223 72.8 57 ---160Dibenzo(a,h)anthracene ug/kg 72 129 4 40124 8.32 50 ---160Fluoranthene ug/kg 97 119 4 40273 118 55 ---160Fluorene ug/kg 86 114 4 40163 26.1 47 ---160Indeno(1,2,3-cd)pyrene ug/kg 73 130 2 40161 44.5 49 ---160Naphthalene ug/kg 66 111 9 40131 25.8 38 ---160Phenanthrene ug/kg 102 113 1 40250 87.3 49 ---160Pyrene ug/kg 104 117 4 40274 107 55 ---160Surr: 2-Methylnaphthalene-d10 % Recovery 62.5 15062.5 50 ---100Surr: Fluoranthene-d10 % Recovery 79.6 15079.6 50 ---100




147337 - Page 172 of 208



Matrix Spike Soil


73143

JJYCTLab #:

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SOIL

MCM

Matrix:

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RPDLimit

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ControlLimits


Parentsampleresult

163812Method: SW8270SIM08/16/201916:00

1-Methylnaphthalene ug/kg 71 111133 16.5 43 ---1652-Methylnaphthalene ug/kg 84 114166 27.0 39 ---165Acenaphthene ug/kg 74 111132 10.2 44 ---165Acenaphthylene ug/kg 93 116159 6.01 39 ---165Anthracene ug/kg 88 114167 21.7 50 ---165Benzo(a)anthracene ug/kg 102 122238 70.0 54 ---165Benzo(a)pyrene ug/kg 81 125194 60.1 50 ---165Benzo(b)fluoranthene ug/kg 92 128247 94.8 53 ---165Benzo(g,h,i)perylene ug/kg 69 127172 58.9 49 ---165Benzo(k)fluoranthene ug/kg 73 123151 30.7 56 ---165Chrysene ug/kg 97 118233 72.8 57 ---165Dibenzo(a,h)anthracene ug/kg 76 129133 8.32 50 ---165Fluoranthene ug/kg 106 119293 118 55 ---165Fluorene ug/kg 91 114176 26.1 47 ---165Indeno(1,2,3-cd)pyrene ug/kg 76 130170 44.5 49 ---165Naphthalene ug/kg 74 111148 25.8 38 ---165Phenanthrene ug/kg 105 113261 87.3 49 ---165Pyrene ug/kg 101 117273 107 55 ---165Surr: 2-Methylnaphthalene-d10 % Recovery 74.6 15074.6 50 ---100Surr: Fluoranthene-d10 % Recovery 91.7 15091.7 50 ---100




147337 - Page 173 of 208





73172

JJYCTLab #:

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Parentsampleresult

163814Method: SW8270SIM08/19/201912:00





147337 - Page 174 of 208





73172

JJYCTLab #:

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Parentsampleresult

163814Method: SW8270SIM08/19/201912:00





147337 - Page 175 of 208



Method Blank Water


73172

JJYCTLab #:

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Parentsampleresult

163814Method: SW8270SIM08/19/201912:00





147337 - Page 176 of 208





73187

JJYCTLab #:

Analyst:

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MCM

Matrix:

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RPDLimit

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Parentsampleresult

163815Method: SW8270D08/19/201912:00





147337 - Page 177 of 208





73187

JJYCTLab #:

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ControlLimits


Parentsampleresult

163815Method: SW8270D08/19/201912:00





147337 - Page 178 of 208





73187

JJYCTLab #:

Analyst:

Prep Batch #:


LIQUID

MCM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163815Method: SW8270D08/19/201912:00





147337 - Page 179 of 208





73187

JJYCTLab #:

Analyst:

Prep Batch #:


LIQUID

MCM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163815Method: SW8270D08/19/201912:00





147337 - Page 180 of 208



Method Blank Water


73187

JJYCTLab #:

Analyst:

Prep Batch #:


LIQUID

MCM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163815Method: SW8270D08/19/201912:00





147337 - Page 181 of 208



Method Blank Water


73187

JJYCTLab #:

Analyst:

Prep Batch #:


LIQUID

MCM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163815Method: SW8270D08/19/201912:00





147337 - Page 182 of 208





73141

AJZCTLab #:

Analyst:

Prep Batch #:


SOLID

AJZ

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163834Method: SW808208/20/201914:20





147337 - Page 183 of 208



Method Blank Soil


73141

AJZCTLab #:

Analyst:

Prep Batch #:


SOLID

AJZ

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163834Method: SW808208/20/201914:20





147337 - Page 184 of 208





73141

AJZCTLab #:

Analyst:

Prep Batch #:


SOIL

AJZ

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163834Method: SW808208/20/201914:20

Aroclor-1016 ug/kg 63 134 38 30520 BDL 47 ---820Aroclor-1221 U 0 130 0 3011.5 BDL 70 ---820Aroclor-1232 U 0 130 0 3014.8 BDL 70 ---820Aroclor-1242 U 0 130 0 3011.5 BDL 70 ---820Aroclor-1248 U 0 130 0 3011.5 BDL 70 ---820Aroclor-1254 U 0 135 0 3014.8 BDL 67 ---820Aroclor-1260 ug/kg 76 140 32 30622 BDL 53 ---820Aroclor-1262 U 0 130 0 3011.5 BDL 70 ---820Aroclor-1268 U 0 130 0 308.20 BDL 70 ---820Surr: 2,4,5,6-TCMX % Recovery 62.0 13062.0 44 ---100Surr: DCBP % Recovery 68.9 14168.9 54 ---100




147337 - Page 185 of 208



Matrix Spike Soil


73141

AJZCTLab #:

Analyst:

Prep Batch #:


SOIL

AJZ

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163834Method: SW808208/20/201914:20

Aroclor-1016 ug/kg 93 134768 BDL 47 ---822Aroclor-1221 U 0 13011.5 BDL 70 ---822Aroclor-1232 U 0 13014.8 BDL 70 ---822Aroclor-1242 U 0 13011.5 BDL 70 ---822Aroclor-1248 U 0 13011.5 71.4 70 ---822Aroclor-1254 U 0 13514.8 BDL 67 ---822Aroclor-1260 ug/kg 105 140863 BDL 53 ---822Aroclor-1262 U 0 13011.5 BDL 70 ---822Aroclor-1268 U 0 1308.22 BDL 70 ---822Surr: 2,4,5,6-TCMX % Recovery 92.2 13092.2 44 ---100Surr: DCBP % Recovery 92.3 14192.3 54 ---100




147337 - Page 186 of 208

147337


Folder #: 147337 Print Date / Time: 08/15/2019 12:25Client: WOOD E&I SOLUTIONS, INC. Received Date / Time / By: 08/15/2019 10:00 DJL


Coolers: SEE BELOW Temperature: <4.9 C On Ice: YCustody Seals Present : Y COC Present:? Y Complete? Y

Seal Intact? Y Numbers: DATED AND SIGNED Ship Method: FEDEX EXPRESS Tracking Number: 789141903710- 7 COOLERS * Adequate Packaging: Temp Blank Enclosed? Y

Notes: *2ND MASTER TRACKING # 789141732940 1 COOLER

8 COOLERS: 5602,6272,5290,5542,6300,5853,5235,6249

THE SAMPLES WERE RECEIVED IN GOOD CONDITION ON ICE.

ONE CUSTODY SEAL WAS PRESENT AND INTACT ON EACH COOLER UPON RECEIPT - ALL WERE DATED 8/14/19 AND SIGNED.

THE COC INDICATED BWH-19-MU1-C3 AS A DESIGNATED MS/MSD SAMPLE; HOWEVER, THE EXTRA VOLUME WAS RECEIVED FOR SAMPLE BWH-19-MU1-C2. SAMPLE BWH-19-MU1-C2 WAS LOGGED FOR MS/MSD ANALYSIS, PER THE ADDITIONAL VOLUME RECEIVED.


_________________________________________________________________________________________________________315732 BWH-19-MU1-C3


_________________________________________________________________________________________________________315732 BWH-19-MU1-C3


_________________________________________________________________________________________________________315732 BWH-19-MU1-C3


_________________________________________________________________________________________________________315732 BWH-19-MU1-C3


_________________________________________________________________________________________________________315732 BWH-19-MU1-C3



_________________________________________________________________________________________________________315764 BWH-19-MU1-C2

SOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pSOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pSOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,p

147337 - Page 187 of 208

147337

SOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pSOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pSOLIDS 1 / %SOL,COD,CR6,ECOLI,HG,ICP,NH3N,pTotal # of Containers of Type ( SOLIDS ) = 6

_________________________________________________________________________________________________________315764 BWH-19-MU1-C2

UNPRES GL 1 / 8270,PCBUNPRES GL 1 / 8270,PCBUNPRES GL 1 / 8270,PCBUNPRES GL 1 / 8270,PCBUNPRES GL 1 / 8270,PCBUNPRES GL 1 / 8270,PCBTotal # of Containers of Type ( UNPRES GL ) = 6

_________________________________________________________________________________________________________315764 BWH-19-MU1-C2


315764 BWH-19-MU1-C2UNPRES GL 1 / O&G UNPRES GL 1 / O&G Total # of Containers of Type ( UNPRES GL ) = 2

_________________________________________________________________________________________________________315764 BWH-19-MU1-C2

MISC 1 / SUB HYD MISC 1 / SUB HYD MISC 1 / SUB HYD Total # of Containers of Type ( MISC ) = 3

_________________________________________________________________________________________________________315764 BWH-19-MU1-C2

TERRA CORE 1 / VOC TERRA CORE 1 / VOC TERRA CORE 1 / VOC TERRA CORE 1 / VOC TERRA CORE 1 / VOC TERRA CORE 1 / VOC Total # of Containers of Type ( TERRA CORE ) = 6


_________________________________________________________________________________________________________315765 BWH-19-MU1-C1


_________________________________________________________________________________________________________315765 BWH-19-MU1-C1


_________________________________________________________________________________________________________315765 BWH-19-MU1-C1


_________________________________________________________________________________________________________315765 BWH-19-MU1-C1


_________________________________________________________________________________________________________315765 BWH-19-MU1-C1



_________________________________________________________________________________________________________315766 BWH-19-MU3-C1

147337 - Page 188 of 208

147337


_________________________________________________________________________________________________________315766 BWH-19-MU3-C1


_________________________________________________________________________________________________________315766 BWH-19-MU3-C1


_________________________________________________________________________________________________________315766 BWH-19-MU3-C1


_________________________________________________________________________________________________________315766 BWH-19-MU3-C1



_________________________________________________________________________________________________________315808 BWH-19-MU1-W1


_________________________________________________________________________________________________________315808 BWH-19-MU1-W1



_________________________________________________________________________________________________________315810 BWH-19-MU1-W1


_________________________________________________________________________________________________________315810 BWH-19-MU1-W1

UNPRES PL 1 / ALK,CR6,pH,TDS,TSSUNPRES PL 1 / ALK,CR6,pH,TDS,TSSTotal # of Containers of Type ( UNPRES PL ) = 2

_________________________________________________________________________________________________________315810 BWH-19-MU1-W1


_________________________________________________________________________________________________________315810 BWH-19-MU1-W1


_________________________________________________________________________________________________________315810 BWH-19-MU1-W1


_________________________________________________________________________________________________________315810 BWH-19-MU1-W1



147337 - Page 189 of 208

147337

_________________________________________________________________________________________________________315815 BWH-19-MU3-W3


_________________________________________________________________________________________________________315815 BWH-19-MU3-W3



_________________________________________________________________________________________________________315816 BWH-19-MU3-W3

AMBER GL 1 / 8270AMBER GL 1 / 8270Total # of Containers of Type ( AMBER GL ) = 2

_________________________________________________________________________________________________________315816 BWH-19-MU3-W3

AMBER GL 1 / 8270,PCBTotal # of Containers of Type ( AMBER GL ) = 1

_________________________________________________________________________________________________________315816 BWH-19-MU3-W3

UNPRES PL 1 / ALK,CR6,pH,TDS,TSSUNPRES PL 1 / ALK,CR6,pH,TDS,TSSTotal # of Containers of Type ( UNPRES PL ) = 2

_________________________________________________________________________________________________________315816 BWH-19-MU3-W3


_________________________________________________________________________________________________________315816 BWH-19-MU3-W3


_________________________________________________________________________________________________________315816 BWH-19-MU3-W3


_________________________________________________________________________________________________________315816 BWH-19-MU3-W3



_________________________________________________________________________________________________________315817 BWH-19-MU4-W4


_________________________________________________________________________________________________________315817 BWH-19-MU4-W4



_________________________________________________________________________________________________________315818 BWH-19-MU4-W4


_________________________________________________________________________________________________________315818 BWH-19-MU4-W4

UNPRES PL 1 / ALK,CR6,pH,TDS,TSSUNPRES PL 1 / ALK,CR6,pH,TDS,TSS

147337 - Page 190 of 208

147337

Total # of Containers of Type ( UNPRES PL ) = 2_________________________________________________________________________________________________________

315818 BWH-19-MU4-W4H2SO4 PL 1 Y / COD,NH3N,PHOSTotal # of Containers of Type ( H2SO4 PL ) = 1

_________________________________________________________________________________________________________315818 BWH-19-MU4-W4


_________________________________________________________________________________________________________315818 BWH-19-MU4-W4


_________________________________________________________________________________________________________315818 BWH-19-MU4-W4



_________________________________________________________________________________________________________315825 BWH-19-MU1-E1

LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /Total # of Containers of Type ( LABEL ONLY ) = 6

_________________________________________________________________________________________________________315825 BWH-19-MU1-E1

SOLIDS 1 / %SOLTotal # of Containers of Type ( SOLIDS ) = 1

_________________________________________________________________________________________________________315825 BWH-19-MU1-E1

UNPRES 1 / Sed. Elutirate Prep Total # of Containers of Type ( UNPRES ) = 1


_________________________________________________________________________________________________________315827 BWH-19-MU3-E1

LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /Total # of Containers of Type ( LABEL ONLY ) = 8

_________________________________________________________________________________________________________315827 BWH-19-MU3-E1


_________________________________________________________________________________________________________315827 BWH-19-MU3-E1



_________________________________________________________________________________________________________315828 BWH-19-MU4-E1

LABEL ONLY 1 /

147337 - Page 191 of 208

147337

LABEL ONLY 1 /LABEL ONLY 1 /LABEL ONLY 1 /Total # of Containers of Type ( LABEL ONLY ) = 4

_________________________________________________________________________________________________________315828 BWH-19-MU4-E1


_________________________________________________________________________________________________________315828 BWH-19-MU4-E1



_________________________________________________________________________________________________________315829 TB-081419


__________________________________________________________________________________________________________


147337 - Page 192 of 208

147337 - Page 193 of 208

147337 - Page 194 of 208

147337 - Page 195 of 208

147337 - Page 196 of 208

147337 - Page 197 of 208

147337 - Page 198 of 208

147337 - Page 199 of 208

147337 - Page 200 of 208

147337 - Page 201 of 208

147337 - Page 202 of 208

ANALYTICAL REPORT






Dear Mr. Szymanski:




147337 - Page 203 of 208


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 6.4 0.3 19.2 27.0 47.1

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU1-C3

#4#10#40#200

0.0255 mm.0.0166 mm.0.0100 mm.0.0073 mm.0.0054 mm.0.0026 mm.0.0012 mm.

100.093.693.374.171.367.560.655.248.335.326.1

NP NP NP

ML A-4(0)

0.3167 0.2014 0.00960.0058 0.0017

ATTERBERG LIMIT TESTING NOT PERFORMED ON THISSAMPLE



8-14-19

CT LABORATORIESBURNS HARBOR, IN(PO# 147337 MITECH)

Mi-Tech #10965

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 1

147337 - Page 204 of 208


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.3 5.5 0.3 3.6 49.3 41.0

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU1-C2

.75#4

#10#40#200

0.0231 mm.0.0160 mm.0.0101 mm.0.0075 mm.0.0054 mm.0.0028 mm.0.0013 mm.

100.099.794.293.990.382.170.156.749.242.530.622.4

NP NP NP

ML A-4(0)

0.0723 0.0352 0.01130.0077 0.0027


8-20-19 8-20-2019CLZ - ENVIRO TECHNICIAN


8-14-19


Mi-Tech #10965

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 2

147337 - Page 205 of 208


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 1.2 7.1 1.2 8.8 42.6 39.1

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU1-C1

.75#4

#10#40#200

0.0249 mm.0.0164 mm.0.0103 mm.0.0076 mm.0.0056 mm.0.0028 mm.0.0013 mm.

100.098.891.790.581.775.269.056.048.340.730.723.0

NP NP NP

ML A-4(0)

0.3839 0.1444 0.01190.0081 0.0026




8-14-19


Mi-Tech #10965

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 3

147337 - Page 206 of 208


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 3.6 0.3 25.0 41.4 29.7

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU3-C1

#4#10#40#200

0.0276 mm.0.0180 mm.0.0110 mm.0.0079 mm.0.0058 mm.0.0029 mm.0.0013 mm.

100.096.496.171.158.152.842.237.731.722.615.1

NP NP NP

ML A-4(0)

0.2784 0.1967 0.03200.0158 0.0051




8-14-19


Mi-Tech #10965

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 4

147337 - Page 207 of 208

147337 - Page 208 of 208







Page 1 of 8


147378 - Page 1 of 39



Project #: 3293191855.02.****




JOHN RALSTON



Contract #:



NOVI, MI 48377



09/09/2019

BURNS HARBOR, IN3293191855.02.****147378

3293191855.02.****3300

CT LAB#: 316441



AnalysisDate/Time

Analyst Method

Sampled: 08/15/2019 1025

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.7.48 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1




mg/kg61300 8/27/19 HLBCOD 08/23/2019 12:00 14:0013000 EPA 410.46000 1.00130002600




Metals Results






147378 - Page 2 of 39



Project #: 3293191855.02.****



CT LAB#: 316441



AnalysisDate/Time

Analyst Method

Sampled: 08/15/2019 1025

Analyte


DODLOD

Client Sample #:










Organic Results



















147378 - Page 3 of 39



Project #: 3293191855.02.****



CT LAB#: 316441



AnalysisDate/Time

Analyst Method

Sampled: 08/15/2019 1025

Analyte


DODLOD

Client Sample #:























% Recovery45 S 8/27/19 JJYSurr: 2-Methylnaphthalene-d10 08/16/2019 16:00 22:08 EPA 8270D-SIM2.0015050

% Recovery47 S 8/27/19 JJYSurr: Fluoranthene-d10 08/16/2019 16:00 22:08 EPA 8270D-SIM2.0015050

Sub Lab Results



147378 - Page 4 of 39



Project #: 3293191855.02.****



CT LAB#: 316444



AnalysisDate/Time

Analyst Method

Sampled: 08/15/2019 1105

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.7.29 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1



mg/kg68.0 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 19:04 ^32 EPA 350.116 2.00325.3

mg/kg51200 8/27/19 HLBCOD 08/23/2019 12:00 14:0013000 EPA 410.46000 1.00130002600




Metals Results














Organic Results


147378 - Page 5 of 39



Project #: 3293191855.02.****



CT LAB#: 316444



AnalysisDate/Time

Analyst Method

Sampled: 08/15/2019 1105

Analyte


DODLOD

Client Sample #:






























147378 - Page 6 of 39



Project #: 3293191855.02.****



CT LAB#: 316444



AnalysisDate/Time

Analyst Method

Sampled: 08/15/2019 1105

Analyte


DODLOD

Client Sample #:














Sub Lab Results



147378 - Page 7 of 39









147378 - Page 8 of 39



QC SUMMARY REPORT





73206

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163670Method: E350.108/19/201912:00





147378 - Page 9 of 39



Method Blank Soil


73206

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163670Method: E350.108/19/201912:00





147378 - Page 10 of 39





73238

JLHCTLab #:

Analyst:

Prep Batch #:


SOLID

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163744Method: E365.408/21/201912:00

Phosphorus mg/kg 102 1101020 90 ---1000




147378 - Page 11 of 39



Method Blank Soil


73238

JLHCTLab #:

Analyst:

Prep Batch #:


SOLID

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163744Method: E365.408/21/201912:00





147378 - Page 12 of 39





CTLab #:Analyst:

Prep Batch #:


SOLIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147378 - Page 13 of 39



Method Blank Soil


CTLab #:Analyst:

Prep Batch #:


SOLIDMatrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult






147378 - Page 14 of 39





73264

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg 98 1001950 90 ---2000




147378 - Page 15 of 39



Method Blank Soil


73264

HLBCTLab #:

Analyst:

Prep Batch #:


SOLID

HLB

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163842Method: E410.408/23/201912:00

COD mg/kg U 3815 0




147378 - Page 16 of 39





73155

JLHCTLab #:

Analyst:

Prep Batch #:


SOLID

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163908Method: SW166408/19/201914:00





147378 - Page 17 of 39



Method Blank Soil


73155

JLHCTLab #:

Analyst:

Prep Batch #:


SOLID

JLH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163908Method: SW166408/19/201914:00





147378 - Page 18 of 39





73271

DGSCTLab #:

Analyst:

Prep Batch #:


SOLID

DGS

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163949Method: SW719908/23/201910:00





147378 - Page 19 of 39



Method Blank Soil


73271

DGSCTLab #:

Analyst:

Prep Batch #:


SOLID

DGS

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163949Method: SW719908/23/201910:00





147378 - Page 20 of 39





73176

NAHCTLab #:

Analyst:

Prep Batch #:


SOLID

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163668Method: SW601008/19/201911:16





147378 - Page 21 of 39



Method Blank Soil


73176

NAHCTLab #:

Analyst:

Prep Batch #:


SOLID

NAH

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163668Method: SW601008/19/201911:16

Aluminum mg/kg 0.120.23 0Arsenic mg/kg U 0.400.13 0Barium mg/kg U 0.0250.009 0Cadmium mg/kg U 0.0200.006 0Chromium mg/kg U 0.1250.023 0Copper mg/kg U 0.200.07 0Iron mg/kg 0.90.34 0Lead mg/kg U 0.1250.04 0Nickel mg/kg U 0.0600.021 0Selenium mg/kg 0.200.14 0Silver mg/kg U 0.0500.017 0Zinc mg/kg U 0.150.05 0




147378 - Page 22 of 39





73149

MDSCTLab #:

Analyst:

Prep Batch #:


SOLID

BMM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163732Method: SW7471B08/20/201909:59

Mercury mg/kg 101 1240.084 82 ---0.083




147378 - Page 23 of 39



Method Blank Soil


73149

MDSCTLab #:

Analyst:

Prep Batch #:


SOLID

BMM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163732Method: SW7471B08/20/201909:59





147378 - Page 24 of 39





73259

RLDCTLab #:

Analyst:

Prep Batch #:


SOLID

RLD

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163774Method: SW8260C08/22/201909:05





147378 - Page 25 of 39



Method Blank Soil


73259

RLDCTLab #:

Analyst:

Prep Batch #:


SOLID

RLD

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163774Method: SW8260C08/22/201909:05





147378 - Page 26 of 39





73143

JJYCTLab #:

Analyst:

Prep Batch #:


SOLID

MCM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163812Method: SW8270SIM08/16/201916:00





147378 - Page 27 of 39



Method Blank Soil


73143

JJYCTLab #:

Analyst:

Prep Batch #:


SOLID

MCM

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163812Method: SW8270SIM08/16/201916:00





147378 - Page 28 of 39





73141

AJZCTLab #:

Analyst:

Prep Batch #:


SOLID

AJZ

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163834Method: SW808208/20/201914:20





147378 - Page 29 of 39



Method Blank Soil


73141

AJZCTLab #:

Analyst:

Prep Batch #:


SOLID

AJZ

Matrix:

Prep Analyst:

RPDLimit

SpikeAmountAdded


ControlLimits


Parentsampleresult

163834Method: SW808208/20/201914:20





147378 - Page 30 of 39

147378


Folder #: 147378 Print Date / Time: 08/16/2019 11:05Client: WOOD E&I SOLUTIONS, INC. Received Date / Time / By: 08/16/2019 10:25 BMS


Coolers: 6322 Temperature: 5.2 C On Ice: YCustody Seals Present : Y COC Present:? Y Complete? Y

Seal Intact? Y Numbers: DATED AND SIGNED Ship Method: FEDEX EXPRESS Tracking Number: 789165155323Adequate Packaging: Y Temp Blank Enclosed? Y

Notes: THE SAMPLES WERE RECEIVED IN GOOD CONDITION ON ICE.

ONE CUSTODY SEAL WAS PRESENT AND INTACT UPON RECEIPT - DATED 8/15/19 AND SIGNED.

THE ELUTRIATE SEDIMENT RECEIVED FOR BWH-19-MU3-E1 WAS ADDED TO FOLDER 147337 (SAMPLES RECEIVED 08/15/2019).


_________________________________________________________________________________________________________316441 BWH-19-MU3-C2


_________________________________________________________________________________________________________316441 BWH-19-MU3-C2

UNPRES GL 1 / 8270Total # of Containers of Type ( UNPRES GL ) = 1

_________________________________________________________________________________________________________316441 BWH-19-MU3-C2


_________________________________________________________________________________________________________316441 BWH-19-MU3-C2


_________________________________________________________________________________________________________316441 BWH-19-MU3-C2


_________________________________________________________________________________________________________316441 BWH-19-MU3-C2



_________________________________________________________________________________________________________316444 BWH-19-MU3-C3


_________________________________________________________________________________________________________316444 BWH-19-MU3-C3

147378 - Page 31 of 39

147378

UNPRES GL 1 / 8270Total # of Containers of Type ( UNPRES GL ) = 1

_________________________________________________________________________________________________________316444 BWH-19-MU3-C3


_________________________________________________________________________________________________________316444 BWH-19-MU3-C3


_________________________________________________________________________________________________________316444 BWH-19-MU3-C3


_________________________________________________________________________________________________________316444 BWH-19-MU3-C3


__________________________________________________________________________________________________________


147378 - Page 32 of 39

147378 - Page 33 of 39

147378 - Page 34 of 39

147378 - Page 35 of 39

ANALYTICAL REPORT






Dear Mr. Szymanski:




147378 - Page 36 of 39


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 6.4 0.6 13.8 26.5 52.7

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU3-C2

#4#10#40#200

0.0257 mm.0.0165 mm.0.0098 mm.0.0072 mm.0.0052 mm.0.0027 mm.0.0012 mm.

100.093.693.079.269.567.262.656.553.540.529.8

NP NP NP

ML A-4(0)

0.2903 0.1548 0.00860.0044 0.0012




8-15-19


MI-TECH # 10966

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 1

147378 - Page 37 of 39


PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 4.1 0.3 33.2 33.5 28.9

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU3-C3

#4#10#40#200

0.0292 mm.0.0187 mm.0.0112 mm.0.0081 mm.0.0058 mm.0.0029 mm.0.0013 mm.

100.095.995.662.448.946.638.234.430.522.916.0

NP NP NP

ML A-4(0)

0.3175 0.2443 0.06330.0316 0.0055




8-15-19


MI-TECH # 10966

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 2

147378 - Page 38 of 39

147378 - Page 39 of 39




Revision Date 09/12/2019 Reason for Revision

The E. coli results were updated.




Page 1 of 45

REVISED


147405-Revised - Page 1 of 150



Project #: 3293191855.02.****




REVISED

JOHN RALSTON



Contract #:



NOVI, MI 48377



09/12/2019

BURNS HARBOR, IN3293191855.02.****147405

3293191855.02.****3300

CT LAB#: 316695



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 0815

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.7.81 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS<2 H 8/19/19 CLBE. coli 12:40U2 9223B2 1.0022


mg/kg<6.1 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 18:21 Û12 EPA 350.16.1 1.00122.0

mg/kg1280 8/26/19 HLBCOD 08/23/2019 12:00 16:07460 EPA 410.4210 1.0046091

mg/kg92.7 8/22/19 JLHPhosphorus 08/21/2019 12:00 15:42 ^J220 EPA 365.4110 1.0022040



Metals Results

mg/kg<0.0054 8/22/19 MDSMercury 08/20/2019 09:59 10:23U0.011 EPA 7471B0.0054 1.000.0110.0027








Project #: 3293191855.02.****



CT LAB#: 316695



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 0815

Analyte


DODLOD

Client Sample #:










Organic Results






















Project #: 3293191855.02.****



CT LAB#: 316695



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 0815

Analyte


DODLOD

Client Sample #:





ug/kg<1.2 8/27/19 JJY1-Methylnaphthalene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.48


ug/kg<1.2 8/27/19 JJYAcenaphthene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.60

ug/kg<1.2 8/27/19 JJYAcenaphthylene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.36

ug/kg<1.2 8/27/19 JJYAnthracene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.48

ug/kg<1.2 8/27/19 JJYBenzo(a)anthracene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.60

ug/kg<1.2 8/27/19 JJYBenzo(a)pyrene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.36


ug/kg<1.2 8/27/19 JJYBenzo(g,h,i)perylene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.31

ug/kg0.809 8/27/19 JJYBenzo(k)fluoranthene 08/16/2019 16:00 22:49J4.8 EPA 8270D-SIM2.4 1.004.80.72

ug/kg1.13 8/27/19 JJYChrysene 08/16/2019 16:00 22:49J2.4 EPA 8270D-SIM1.2 1.002.40.26

ug/kg<1.2 8/27/19 JJYDibenzo(a,h)anthracene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.25

ug/kg1.94 8/27/19 JJYFluoranthene 08/16/2019 16:00 22:49J4.8 EPA 8270D-SIM2.4 1.004.80.84

ug/kg<1.2 8/27/19 JJYFluorene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.48

ug/kg<1.2 8/27/19 JJYIndeno(1,2,3-cd)pyrene 08/16/2019 16:00 22:49U2.4 EPA 8270D-SIM1.2 1.002.40.48

ug/kg0.885 8/27/19 JJYNaphthalene 08/16/2019 16:00 22:49J2.4 EPA 8270D-SIM1.2 1.002.40.60

ug/kg<2.4 8/27/19 JJYPhenanthrene 08/16/2019 16:00 22:49U4.8 EPA 8270D-SIM2.4 1.004.81.3

ug/kg2.46 8/27/19 JJYPyrene 08/16/2019 16:00 22:49J4.8 EPA 8270D-SIM2.4 1.004.80.72



Sub Lab Results






Project #: 3293191855.02.****



CT LAB#: 316696



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1000

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.9.66 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS<2 H 8/19/19 CLBE. coli 12:40U2 9223B2 1.0022



mg/kg40400 8/27/19 HLBCOD 08/23/2019 12:00 14:0010000 EPA 410.44700 1.00100002000




Metals Results



mg/kg<0.49 8/21/19 NAHArsenic 08/19/2019 11:16 00:06U0.99 EPA 6010D0.49 1.000.990.16

mg/kg124 8/21/19 NAHBarium 08/19/2019 11:16 00:060.062 EPA 6010D0.031 1.000.0620.011



mg/kg0.69 B 8/21/19 NAHCopper 08/19/2019 11:16 00:060.49 EPA 6010D0.25 1.000.490.086




mg/kg0.89 B 8/21/19 NAHSelenium 08/19/2019 11:16 00:060.49 EPA 6010D0.25 1.000.490.074



Organic Results





Project #: 3293191855.02.****



CT LAB#: 316696



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1000

Analyte


DODLOD

Client Sample #:






















ug/kg1.40 8/27/19 JJY1-Methylnaphthalene 08/16/2019 16:00 23:09J2.4 EPA 8270D-SIM1.2 1.002.40.47



ug/kg0.827 8/27/19 JJYAcenaphthylene 08/16/2019 16:00 23:09J2.4 EPA 8270D-SIM1.2 1.002.40.35








Project #: 3293191855.02.****



CT LAB#: 316696



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1000

Analyte


DODLOD

Client Sample #:














Sub Lab Results


CT LAB#: 316697



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1115

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.94 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1E. coli Comments: result is greater than 2240 MPN/g_TS





Project #: 3293191855.02.****



CT LAB#: 316697



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1115

Analyte


DODLOD

Client Sample #:

E. coli Comments: result is greater than 2240 MPN/g_TS

MPN/g_TS2240 H 8/19/19 CLBE. coli 12:402 9223B2 1.0022



mg/kg1910 8/26/19 HLBCOD 08/23/2019 12:00 16:07470 EPA 410.4220 1.0047094




Metals Results



mg/kg1.0 8/21/19 NAHArsenic 08/19/2019 11:16 00:13J1.1 EPA 6010D0.53 1.001.10.17











Organic Results







Project #: 3293191855.02.****



CT LAB#: 316697



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1115

Analyte


DODLOD

Client Sample #:
























ug/kg1.66 8/27/19 JJYAnthracene 08/16/2019 16:00 23:30J2.5 EPA 8270D-SIM1.3 1.002.50.50









Project #: 3293191855.02.****



CT LAB#: 316697



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1115

Analyte


DODLOD

Client Sample #:





ug/kg1.36 8/27/19 JJYFluorene 08/16/2019 16:00 23:30J2.5 EPA 8270D-SIM1.3 1.002.50.50



ug/kg3.31 8/27/19 JJYPhenanthrene 08/16/2019 16:00 23:30J5.0 EPA 8270D-SIM2.5 1.005.01.4




Sub Lab Results


CT LAB#: 316699



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1305

Analyte

Sample Description: BWH-19-RS1-G1

DODLOD

Client Sample #:

Inorganic Results



S.U.8.87 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1




mg/kg1210 8/26/19 HLBCOD 08/23/2019 12:00 16:07430 EPA 410.4200 1.0043086





Project #: 3293191855.02.****



CT LAB#: 316699



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1305

Analyte


DODLOD

Client Sample #:




Metals Results














Organic Results













Project #: 3293191855.02.****



CT LAB#: 316699



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1305

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316699



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1305

Analyte


DODLOD

Client Sample #:






Sub Lab Results


CT LAB#: 316700



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte

Sample Description: BWH-19-RS1-W1

DODLOD

Client Sample #:

Inorganic Results

S.U.8.36 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1





mg/L<35 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515




Metals Results







Project #: 3293191855.02.****



CT LAB#: 316700



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte


DODLOD

Client Sample #:




ug/L0.74 8/20/19 NAHTotal Chromium 08/19/2019 09:54 18:45J4.0 EPA 6010D2.0 1.004.00.60









Organic Results



















Project #: 3293191855.02.****



CT LAB#: 316700



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316700



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte


DODLOD

Client Sample #:














08/19/2019 12:00 13:38U2.0 EPA 8270D0.80 1.002.00.52




















Project #: 3293191855.02.****



CT LAB#: 316700



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316700



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte


DODLOD

Client Sample #:













CT LAB#: 316701



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1320

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results


CT LAB#: 316702



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1350

Analyte


DODLOD

Client Sample #:





Project #: 3293191855.02.****



CT LAB#: 316702



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1350

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.56 8/19/19 CLBpH 09:30 ^0.1 EPA 9045D0.1 1.000.10.1




mg/kg2160 8/26/19 HLBCOD 08/23/2019 12:00 16:07460 EPA 410.4210 1.0046092

mg/kg133 M,Y 8/22/19 JLHPhosphorus 08/21/2019 12:00 15:47 ^J230 EPA 365.4110 1.0023041



Metals Results














Organic Results





Project #: 3293191855.02.****



CT LAB#: 316702



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1350

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316702



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1350

Analyte


DODLOD

Client Sample #:












% Recovery49 S 8/28/19 JJYSurr: 2-Methylnaphthalene-d10 08/16/2019 16:00 00:11 EPA 8270D-SIM1.0015050


Sub Lab Results


CT LAB#: 316703



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1415

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.94 8/23/19 SRWpH 15:30 ^0.1 EPA 9045D0.1 1.000.10.1E. coli Comments: value is greater than 2270 MPN/g TS





Project #: 3293191855.02.****



CT LAB#: 316703



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1415

Analyte


DODLOD

Client Sample #:

E. coli Comments: value is greater than 2270 MPN/g TS




mg/kg1730 8/26/19 HLBCOD 08/23/2019 12:00 16:07490 EPA 410.4230 1.0049097




Metals Results



mg/kg0.95 8/21/19 NAHArsenic 08/19/2019 11:16 00:31J1.1 EPA 6010D0.53 1.001.10.17











Organic Results







Project #: 3293191855.02.****



CT LAB#: 316703



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1415

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316703



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1415

Analyte


DODLOD

Client Sample #:












Sub Lab Results


CT LAB#: 316704



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1450

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.42 8/23/19 SRWpH 15:30 ^0.1 EPA 9045D0.1 1.000.10.1




mg/kg1660 8/26/19 HLBCOD 08/23/2019 12:00 16:07420 EPA 410.4200 1.0042084





Project #: 3293191855.02.****



CT LAB#: 316704



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1450

Analyte


DODLOD

Client Sample #:




Metals Results














Organic Results













Project #: 3293191855.02.****



CT LAB#: 316704



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1450

Analyte


DODLOD

Client Sample #:


















ug/kg1.29 8/28/19 JJYAnthracene 08/16/2019 16:00 00:52J2.5 EPA 8270D-SIM1.2 1.002.50.49















Project #: 3293191855.02.****



CT LAB#: 316704



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1450

Analyte


DODLOD

Client Sample #:


ug/kg1.75 8/28/19 JJYPhenanthrene 08/16/2019 16:00 00:52J4.9 EPA 8270D-SIM2.5 1.004.91.4




Sub Lab Results


CT LAB#: 316705



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:

Inorganic Results

S.U.8.69 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1





mg/L<35 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515




Metals Results







Project #: 3293191855.02.****



CT LAB#: 316705



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:




ug/L1.3 8/20/19 NAHTotal Chromium 08/19/2019 09:54 18:52J4.0 EPA 6010D2.0 1.004.00.60









Organic Results



















Project #: 3293191855.02.****



CT LAB#: 316705



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316705



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:














08/19/2019 12:00 13:56U2.0 EPA 8270D0.80 1.002.00.52




















Project #: 3293191855.02.****



CT LAB#: 316705



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316705



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:













CT LAB#: 316706



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1505

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results


CT LAB#: 316707



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1535

Analyte


DODLOD

Client Sample #:





Project #: 3293191855.02.****



CT LAB#: 316707



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1535

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.33 8/23/19 SRWpH 15:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS64.5 H 8/19/19 CLBE. coli 12:402 9223B2 1.0022


mg/kg2.57 8/19/19 HLBAmmonia Nitrogen 08/19/2019 12:00 18:36 ^J13 EPA 350.16.3 1.00132.1

mg/kg11600 8/27/19 HLBCOD 08/23/2019 12:00 14:0410000 EPA 410.44900 1.00100002100




Metals Results

mg/kg0.0061 8/22/19 MDSMercury 08/20/2019 09:59 10:52J0.011 EPA 7471B0.0057 1.000.0110.0029













Organic Results





Project #: 3293191855.02.****



CT LAB#: 316707



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1535

Analyte


DODLOD

Client Sample #:

































Project #: 3293191855.02.****



CT LAB#: 316707



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1535

Analyte


DODLOD

Client Sample #:














Sub Lab Results


CT LAB#: 316708



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1600

Analyte


DODLOD

Client Sample #:

Inorganic Results



S.U.8.47 8/23/19 SRWpH 15:30 ^0.1 EPA 9045D0.1 1.000.10.1

MPN/g_TS11.2 H 8/19/19 CLBE. coli 12:402 9223B2 1.0022






Project #: 3293191855.02.****



CT LAB#: 316708



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1600

Analyte


DODLOD

Client Sample #:


mg/kg5490 8/27/19 HLBCOD 08/23/2019 12:00 14:001100 EPA 410.4510 1.001100220




Metals Results

mg/kg0.0039 8/22/19 MDSMercury 08/20/2019 09:59 10:54J0.011 EPA 7471B0.0057 1.000.0110.0029













Organic Results











Project #: 3293191855.02.****



CT LAB#: 316708



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1600

Analyte


DODLOD

Client Sample #:


















ug/kg2.26 8/28/19 JJYAcenaphthene 08/16/2019 16:00 01:33J2.5 EPA 8270D-SIM1.2 1.002.50.62















Project #: 3293191855.02.****



CT LAB#: 316708



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1600

Analyte


DODLOD

Client Sample #:








Sub Lab Results


CT LAB#: 316709



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019

Analyte


DODLOD

Client Sample #:

Organic Results















Project #: 3293191855.02.****



CT LAB#: 316710



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1705

Analyte

Sample Description: EB-1

DODLOD

Client Sample #:

Inorganic Results

S.U.6.87 8/23/19 SRWpH 15:30 ^0.1 EPA 9040C0.1 1.000.10.1




mg/L<15 8/23/19 SRWAlkalinity 11:24 Û30 EPA 310.215 1.00306.0

mg/L<35 8/26/19 HLBCOD 08/22/2019 12:00 15:50 Û75 EPA 410.435 1.007515




Metals Results




ug/L0.63 8/20/19 NAHTotal Barium 08/19/2019 09:54 19:48J1.8 EPA 6010D0.90 1.001.80.29




ug/L22.1 8/20/19 NAHTotal Iron 08/19/2019 09:54 19:48J100 EPA 6010D50 1.0010016






mg/L3.8 8/20/19 NAHTotal Hardness 08/19/2019 09:54 19:480.41 SM2340B/6010D0.21 1.000.410.067

Organic Results





Project #: 3293191855.02.****



CT LAB#: 316710



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1705

Analyte


DODLOD

Client Sample #:






ug/L0.32 8/29/19 RLDToluene 14:32J1.0 EPA 8260C0.60 1.001.00.21



























Project #: 3293191855.02.****



CT LAB#: 316710



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1705

Analyte


DODLOD

Client Sample #:




























08/19/2019 12:00 14:15U2.1 EPA 8270D0.82 1.002.10.54

ug/L1.0 8/23/19 JJYBenzaldehyde 08/19/2019 12:00 14:151.0 EPA 8270D0.41 1.001.00.26





Project #: 3293191855.02.****



CT LAB#: 316710



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1705

Analyte


DODLOD

Client Sample #:







ug/L0.57 8/23/19 JJYBis(2-ethylhexyl)phthalate 08/19/2019 12:00 14:15J2.1 EPA 8270D1.0 1.002.10.45


























Project #: 3293191855.02.****



CT LAB#: 316710



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1705

Analyte


DODLOD

Client Sample #:






















ug/L0.015 8/26/19 JJYNaphthalene 08/19/2019 12:00 21:03J0.041 EPA 8270D-SIM0.021 1.000.0410.011









Project #: 3293191855.02.****



CT LAB#: 316711



AnalysisDate/Time

Analyst Method

Sampled: 08/16/2019 1705

Analyte


DODLOD

Client Sample #:

Inorganic Results


Metals Results















QC SUMMARY REPORT



Duplicate


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163646Method: E350.1








Method Blank Water


CTLab #:Analyst:

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163646Method: E350.1








LOQ Check Water


CTLab #:Analyst:

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73206

HLBCTLab #:

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SOIL

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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg U 0 251.63 <1.63









73206

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163670Method: E350.108/19/201912:00








Method Blank Soil


73206

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163670Method: E350.108/19/201912:00










73206

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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg 100 120 1 259.81 BDL 80 ---9.82







Matrix Spike Soil


73206

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163670Method: E350.108/19/201912:00

Ammonia Nitrogen mg/kg 101 12010.1 BDL 80 ---10.0







Duplicate


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163717Method: E365.1

Phosphorus mg/L U 0 250.300 <0.300









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163717Method: E365.1

Phosphorus mg/L 96 1103.85 90 ---4.00







Method Blank Water


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163717Method: E365.1








Duplicate


73238

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163744Method: E365.408/21/201912:00

Phosphorus mg/kg 79 20307 133









73238

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163744Method: E365.408/21/201912:00

Phosphorus mg/kg 102 1101020 90 ---1000







Method Blank Soil


73238

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163744Method: E365.408/21/201912:00










73238

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163744Method: E365.408/21/201912:00

Phosphorus mg/kg 116 110 9 20714 133 90 ---502







Matrix Spike Soil


73238

JLHCTLab #:

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163744Method: E365.408/21/201912:00

Phosphorus mg/kg 100 110589 133 90 ---455









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163789Method: E310.2

Alkalinity mg/L 102 110382.0 90 ---375.0







LOQ Check Water


CTLab #:Analyst:

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163789Method: E310.2

Alkalinity mg/L 103 11031.00 90 ---30.00







Method Blank Water


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163789Method: E310.2










CTLab #:Analyst:

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Method Blank Soil


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73266

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163838Method: E410.408/23/201912:00

COD mg/L 98 110393.0 90 ---400.0







Method Blank Water


73266

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163838Method: E410.408/23/201912:00










73264

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163842Method: E410.408/23/201912:00

COD mg/kg 98 1001950 90 ---2000







Method Blank Soil


73264

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163842Method: E410.408/23/201912:00

COD mg/kg U 3815 0









73155

JLHCTLab #:

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163908Method: SW166408/19/201914:00








Method Blank Soil


73155

JLHCTLab #:

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163908Method: SW166408/19/201914:00










73284

JLHCTLab #:

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163925Method: SW166408/26/201909:00








Method Blank Water


73284

JLHCTLab #:

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163925Method: SW166408/26/201909:00










73271

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163949Method: SW719908/23/201910:00








Method Blank Soil


73271

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163949Method: SW719908/23/201910:00








Duplicate


73156

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163661Method: SW601008/19/201909:54

Total Aluminum ug/L 36 14 2010.3 11.9Total Arsenic ug/L U 24 0 204.00 <4.00Total Barium ug/L 1.80 1 2021.2 21.4Total Cadmium ug/L U 2.0 0 200.300 <0.300Total Chromium ug/L U 4.0 200 200.600 1.3Total Copper ug/L U 7.0 0 201.20 <1.20Total Iron ug/L U 100 0 2016.0 <16.0Total Lead ug/L U 4.0 0 201.40 <1.40Total Nickel ug/L U 6.0 0 201.00 <1.00Total Selenium ug/L U 13.0 200 202.20 3.6Total Silver ug/L U 4.0 0 200.700 <0.700Total Zinc ug/L U 10.0 0 201.60 <1.60









73156

NAHCTLab #:

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163661Method: SW601008/19/201909:54








Method Blank Water


73156

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163661Method: SW601008/19/201909:54










73156

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163661Method: SW601008/19/201909:54

Total Aluminum ug/L 106 115 0 20862 11.9 86 ---800Total Arsenic ug/L 100 113 1 20799 BDL 87 ---800Total Barium ug/L 100 113 0 20825 21.4 88 ---800Total Cadmium ug/L 98 113 1 2019.7 BDL 88 ---20.0Total Chromium ug/L 101 113 1 2081.9 1.3 90 ---80.0Total Copper ug/L 114 114 2 20114 BDL 86 ---100Total Iron ug/L 104 115 1 20417 BDL 87 ---400Total Lead ug/L 100 113 0 20201 BDL 86 ---200Total Nickel ug/L 96 113 0 20191 BDL 88 ---200Total Selenium ug/L 94 114 0 20756 3.6 83 ---800Total Silver ug/L 96 115 1 2019.3 BDL 84 ---20.0Total Zinc ug/L 102 115 0 20203 BDL 87 ---200







Matrix Spike Water


73156

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163661Method: SW601008/19/201909:54

Total Aluminum ug/L 106 115859 11.9 86 ---800Total Arsenic ug/L 99 113789 BDL 87 ---800Total Barium ug/L 100 113825 21.4 88 ---800Total Cadmium ug/L 98 11319.6 BDL 88 ---20.0Total Chromium ug/L 100 11381.3 1.3 90 ---80.0Total Copper ug/L 116 114116 BDL 86 ---100Total Iron ug/L 103 115413 BDL 87 ---400Total Lead ug/L 100 113200 BDL 86 ---200Total Nickel ug/L 96 113191 BDL 88 ---200Total Selenium ug/L 94 114753 3.6 83 ---800Total Silver ug/L 97 11519.4 BDL 84 ---20.0Total Zinc ug/L 102 115203 BDL 87 ---200







Duplicate


73167

NAHCTLab #:

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163662Method: SW601008/19/201909:54

Dissolved Iron ug/L 100 200 2024.7 <16.0









73167

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163662Method: SW601008/19/201909:54








Method Blank Water


73167

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163662Method: SW601008/19/201909:54










73167

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163662Method: SW601008/19/201909:54








Matrix Spike Water


73167

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163662Method: SW601008/19/201909:54








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73177

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163669Method: SW601008/19/201911:16

Aluminum mg/kg 9.6 0 20496 496Arsenic mg/kg 32 0 201.2 1.2Barium mg/kg 2.0 16 203.4 4.0Cadmium mg/kg U 1.60 0 200.00749 <0.00749Chromium mg/kg 5.6 6 201.7 1.6Copper mg/kg 16.0 93 200.55 1.5Iron mg/kg 72 1 202440 2420Lead mg/kg 10.0 0 202.0 2.0Nickel mg/kg 4.8 0 201.6 1.6Selenium mg/kg U 16 200 200.0749 0.11Silver mg/kg 4.0 6 200.067 0.063Zinc mg/kg 12.0 2 209.4 9.2









73177

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163669Method: SW601008/19/201911:16








Method Blank Soil


73177

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163669Method: SW601008/19/201911:16

Aluminum mg/kg 0.120.48 0Arsenic mg/kg U 0.400.13 0Barium mg/kg U 0.0250.009 0Cadmium mg/kg U 0.0200.006 0Chromium mg/kg U 0.1250.023 0Copper mg/kg 0.200.084 0Iron mg/kg 0.90.44 0Lead mg/kg U 0.1250.04 0Nickel mg/kg U 0.0600.021 0Selenium mg/kg 0.200.11 0Silver mg/kg U 0.0500.017 0Zinc mg/kg U 0.150.05 0









73177

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163669Method: SW601008/19/201911:16

Aluminum mg/kg 125 119 1 20653 496 74 ---126Arsenic mg/kg 92 111 4 20117 1.2 82 ---126Barium mg/kg 95 113 4 20124 4.0 83 ---126Cadmium mg/kg 106 113 4 203.3 BDL 82 ---3.1Chromium mg/kg 99 113 6 2014.1 1.6 85 ---12.6Copper mg/kg 83 117 2 2014.6 1.5 81 ---15.7Iron mg/kg 0 118 2 202220 2420 81 ---62.8Lead mg/kg 92 112 4 2030.8 2.0 81 ---31.4Nickel mg/kg 87 113 4 2028.8 1.6 83 ---31.4Selenium mg/kg 91 111 3 20115 0.11 78 ---126Silver mg/kg 88 112 5 202.8 0.063 82 ---3.1Zinc mg/kg 89 113 3 2037.3 9.2 82 ---31.4







Matrix Spike Soil


73177

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163669Method: SW601008/19/201911:16

Aluminum mg/kg 118 119643 496 74 ---125Arsenic mg/kg 88 111111 1.2 82 ---125Barium mg/kg 91 113118 4.0 83 ---125Cadmium mg/kg 103 1133.2 BDL 82 ---3.1Chromium mg/kg 93 11313.2 1.6 85 ---12.5Copper mg/kg 81 11714.1 1.5 81 ---15.6Iron mg/kg 0 1182160 2420 81 ---62.4Lead mg/kg 88 11229.4 2.0 81 ---31.2Nickel mg/kg 83 11327.6 1.6 83 ---31.2Selenium mg/kg 89 111111 0.11 78 ---125Silver mg/kg 85 1122.7 0.063 82 ---3.1Zinc mg/kg 87 11336.2 9.2 82 ---31.2







Duplicate


73150

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163733Method: SW7471B08/20/201909:59

Mercury mg/kg U 0.20 0 200.00266 <0.00266









73150

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163733Method: SW7471B08/20/201909:59

Mercury mg/kg 99 1240.082 82 ---0.083







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73150

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163733Method: SW7471B08/20/201909:59










73150

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163733Method: SW7471B08/20/201909:59

Mercury mg/kg 100 124 3 200.11 BDL 82 ---0.11







Matrix Spike Soil


73150

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163733Method: SW7471B08/20/201909:59

Mercury mg/kg 100 1240.11 BDL 82 ---0.11









73152

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163791Method: SW7470A08/21/201914:51








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73152

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163791Method: SW7470A08/21/201914:51










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1,2 Dichloroethane-d4 % Recovery 104 118104 81 ---100Benzene ug/L 106 120 0 2010.6 BDL 79 ---10.0Bromofluorobenzene % Recovery 100 114100 85 ---100d8-Toluene % Recovery 101 112101 89 ---100Dibromofluoromethane % Recovery 102 119102 80 ---100Ethylbenzene ug/L 106 121 0 2010.6 BDL 79 ---10.0m & p-Xylene ug/L 105 121 2 2021.0 BDL 80 ---20.0Methyl tert-butyl ether ug/L 101 124 4 2010.1 BDL 71 ---10.0o-Xylene ug/L 103 122 0 2010.3 BDL 78 ---10.0Toluene ug/L 105 121 1 2010.5 BDL 80 ---10.0







Matrix Spike Water


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1,2 Dichloroethane-d4 % Recovery 103 118103 81 ---100Benzene ug/L 105 120 2010.5 BDL 79 ---10.0Bromofluorobenzene % Recovery 94.0 11494.0 85 ---100d8-Toluene % Recovery 101 112101 89 ---100Dibromofluoromethane % Recovery 102 119102 80 ---100Ethylbenzene ug/L 107 121 2010.7 BDL 79 ---10.0m & p-Xylene ug/L 108 121 2021.5 BDL 80 ---20.0Methyl tert-butyl ether ug/L 97 124 209.71 BDL 71 ---10.0o-Xylene ug/L 103 122 2010.3 BDL 78 ---10.0Toluene ug/L 106 121 2010.6 BDL 80 ---10.0









73259

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163774Method: SW8260C08/22/201909:05








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73259

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163774Method: SW8260C08/22/201909:05










73201

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163780Method: SW808208/20/201909:00










73201

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163780Method: SW808208/20/201909:00








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73201

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163780Method: SW808208/20/201909:00










73143

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163812Method: SW8270SIM08/16/201916:00








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73143

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163812Method: SW8270SIM08/16/201916:00










73172

JJYCTLab #:

Analyst:

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LIQUID

MCM

Matrix:

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RPDLimit

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163814Method: SW8270SIM08/19/201912:00










73172

JJYCTLab #:

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163814Method: SW8270SIM08/19/201912:00








Method Blank Water


73172

JJYCTLab #:

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163814Method: SW8270SIM08/19/201912:00










73187

JJYCTLab #:

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163815Method: SW8270D08/19/201912:00










73187

JJYCTLab #:

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RPDLimit

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163815Method: SW8270D08/19/201912:00










73187

JJYCTLab #:

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MCM

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163815Method: SW8270D08/19/201912:00










73187

JJYCTLab #:

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MCM

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163815Method: SW8270D08/19/201912:00








Method Blank Water


73187

JJYCTLab #:

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163815Method: SW8270D08/19/201912:00








Method Blank Water


73187

JJYCTLab #:

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163815Method: SW8270D08/19/201912:00










73141

AJZCTLab #:

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SOLID

AJZ

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RPDLimit

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163834Method: SW808208/20/201914:20








Method Blank Soil


73141

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AJZ

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163834Method: SW808208/20/201914:20






147405


Folder #: 147405 Print Date / Time: 08/19/2019 18:25Client: WOOD E&I SOLUTIONS, INC. Received Date / Time / By: 08/17/2019 10:20 BMS

Project Name: BURNS HARBOR Log-In Date / Time / By: 08/17/2019 11:10 BMSProject Phase: BURNS HARBOR, IN Project #: 3293191855.02.**** PM: BMS

Coolers: SEE BELOW Temperature: <4.9 C On Ice: YCustody Seals Present : Y COC Present:? Y Complete? Y

Seal Intact? Y Numbers: SIGNED AND DATED Ship Method: FEDEX EXPRESS Tracking Number: 789191711361Adequate Packaging: Y Temp Blank Enclosed? Y

Notes: COOLERS: 5283, 6000, 6338, 6331, 6360

THE SAMPLES WERE RECEIVED IN GOOD CONDITION ON ICE.

A TERRACORE KIT WAS NOT RECEIVED FOR SAMPLE BWH-19-RS2-G2. TWO 5-GRAM ALIQUOTS WERE SUBSAMPLED FROM THE PACKED, 4-OZ AMBER GLASS JAR AND PUT INTO 5-ML METHANOL-VIALS FOR THE BTEX ANALYSIS.

ONE CUSTODY SEAL WAS PRESENT AND INTACT ON EACH COOLER UPON RECEIPT - ALL WERE DATED 8/16/19 AND SIGNED.


_________________________________________________________________________________________________________316695 BWH-19-MU4-C3


_________________________________________________________________________________________________________316695 BWH-19-MU4-C3


_________________________________________________________________________________________________________316695 BWH-19-MU4-C3


_________________________________________________________________________________________________________316695 BWH-19-MU4-C3

MISC 1 / SUB HYDROMETER Total # of Containers of Type ( MISC ) = 1

_________________________________________________________________________________________________________316695 BWH-19-MU4-C3



_________________________________________________________________________________________________________316696 BWH-19-MU4-C1


_________________________________________________________________________________________________________316696 BWH-19-MU4-C1


147405


_________________________________________________________________________________________________________316696 BWH-19-MU4-C1


_________________________________________________________________________________________________________316696 BWH-19-MU4-C1


_________________________________________________________________________________________________________316696 BWH-19-MU4-C1



_________________________________________________________________________________________________________316697 BWH-19-MU4-C2


_________________________________________________________________________________________________________316697 BWH-19-MU4-C2


_________________________________________________________________________________________________________316697 BWH-19-MU4-C2


_________________________________________________________________________________________________________316697 BWH-19-MU4-C2


_________________________________________________________________________________________________________316697 BWH-19-MU4-C2



_________________________________________________________________________________________________________316699 BWH-19-RS1-G1


_________________________________________________________________________________________________________316699 BWH-19-RS1-G1


_________________________________________________________________________________________________________316699 BWH-19-RS1-G1


_________________________________________________________________________________________________________316699 BWH-19-RS1-G1


_________________________________________________________________________________________________________316699 BWH-19-RS1-G1

TERRA CORE 1 / VOC TERRA CORE 1 / VOC


147405

Total # of Containers of Type ( TERRA CORE ) = 2_________________________________________________________________________________________________________Sample ID / Description Container Type Cond. Code pH OK?/Filtered? Tests

_________________________________________________________________________________________________________316700 BWH-19-RS1-W1


_________________________________________________________________________________________________________316700 BWH-19-RS1-W1


_________________________________________________________________________________________________________316700 BWH-19-RS1-W1


_________________________________________________________________________________________________________316700 BWH-19-RS1-W1


_________________________________________________________________________________________________________316700 BWH-19-RS1-W1

AMBER HCL 1 / O&G Total # of Containers of Type ( AMBER HCL ) = 1

_________________________________________________________________________________________________________316700 BWH-19-RS1-W1



_________________________________________________________________________________________________________316701 BWH-19-RS1-W1

UNPRES PL 1 / FILTRATIONTotal # of Containers of Type ( UNPRES PL ) = 1

_________________________________________________________________________________________________________316701 BWH-19-RS1-W1

HNO3 1 Y / ICPTotal # of Containers of Type ( HNO3 ) = 1


_________________________________________________________________________________________________________316702 BWH-19-RS1-G2


_________________________________________________________________________________________________________316702 BWH-19-RS1-G2


_________________________________________________________________________________________________________316702 BWH-19-RS1-G2


_________________________________________________________________________________________________________316702 BWH-19-RS1-G2


_________________________________________________________________________________________________________


147405

316702 BWH-19-RS1-G2TERRA CORE 1 / VOC TERRA CORE 1 / VOC Total # of Containers of Type ( TERRA CORE ) = 2


_________________________________________________________________________________________________________316703 BWH-19-RS1-G3


_________________________________________________________________________________________________________316703 BWH-19-RS1-G3


_________________________________________________________________________________________________________316703 BWH-19-RS1-G3


_________________________________________________________________________________________________________316703 BWH-19-RS1-G3


_________________________________________________________________________________________________________316703 BWH-19-RS1-G3



_________________________________________________________________________________________________________316704 BWH-19-RS2-G3


_________________________________________________________________________________________________________316704 BWH-19-RS2-G3


_________________________________________________________________________________________________________316704 BWH-19-RS2-G3


_________________________________________________________________________________________________________316704 BWH-19-RS2-G3


_________________________________________________________________________________________________________316704 BWH-19-RS2-G3



_________________________________________________________________________________________________________316705 BWH-19-RS2-W2


_________________________________________________________________________________________________________316705 BWH-19-RS2-W2


147405


_________________________________________________________________________________________________________316705 BWH-19-RS2-W2


_________________________________________________________________________________________________________316705 BWH-19-RS2-W2


_________________________________________________________________________________________________________316705 BWH-19-RS2-W2


_________________________________________________________________________________________________________316705 BWH-19-RS2-W2



_________________________________________________________________________________________________________316706 BWH-19-RS2-W2


_________________________________________________________________________________________________________316706 BWH-19-RS2-W2

HNO3 1 Y / ICPTotal # of Containers of Type ( HNO3 ) = 1


_________________________________________________________________________________________________________316707 BWH-19-RS2-G2


_________________________________________________________________________________________________________316707 BWH-19-RS2-G2


_________________________________________________________________________________________________________316707 BWH-19-RS2-G2


_________________________________________________________________________________________________________316707 BWH-19-RS2-G2


_________________________________________________________________________________________________________316707 BWH-19-RS2-G2



_________________________________________________________________________________________________________316708 BWH-19-RS2-G1



147405

_________________________________________________________________________________________________________316708 BWH-19-RS2-G1


_________________________________________________________________________________________________________316708 BWH-19-RS2-G1


_________________________________________________________________________________________________________316708 BWH-19-RS2-G1


_________________________________________________________________________________________________________316708 BWH-19-RS2-G1



_________________________________________________________________________________________________________316709 TB-081619



_________________________________________________________________________________________________________316710 EB-1


_________________________________________________________________________________________________________316710 EB-1


_________________________________________________________________________________________________________316710 EB-1


_________________________________________________________________________________________________________316710 EB-1


_________________________________________________________________________________________________________316710 EB-1


_________________________________________________________________________________________________________316710 EB-1



_________________________________________________________________________________________________________316711 EB-1


_________________________________________________________________________________________________________


147405

316711 EB-1HNO3 1 Y / ICPTotal # of Containers of Type ( HNO3 ) = 1

__________________________________________________________________________________________________________










ANALYTICAL REPORT






Dear Mr. Szymanski:






PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 0.7 3.0 95.3 1.0

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU4-C3

#4#10#40#200

0.0364 mm.0.0230 mm.0.0133 mm.0.0092 mm.0.0066 mm.0.0032 mm.0.0014 mm.

100.099.396.3

1.01.81.81.81.81.81.81.7

NP NP NP

SP A-3

0.3791 0.3462 0.21960.1831 0.1272 0.09680.0884 2.48 0.83

ATTERBERG LIMITS NOT ANALYZED FOR IN THIS SAMPLE


SFENVIROMENTAL MANAGER

8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 1



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 2.2 15.9 80.1 0.5 1.3

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU4-C1

#4#10#40#200

0.0364 mm.0.0230 mm.0.0133 mm.0.0094 mm.0.0066 mm.0.0032 mm.0.0014 mm.

100.097.881.9

1.81.71.71.71.71.31.31.3

NP NP NP

SP A-3

0.9337 0.5742 0.26450.2130 0.1381 0.09980.0895 2.95 0.81




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 2



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 0.5 1.4 96.0 0.8 1.3

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-MU4-C2

#4#10#40#200

0.0364 mm.0.0230 mm.0.0133 mm.0.0094 mm.0.0066 mm.0.0032 mm.0.0014 mm.

100.099.598.1

2.11.71.71.71.31.31.31.3

NP NP NP

SP A-3

0.3672 0.3355 0.21360.1783 0.1242 0.09470.0865 2.47 0.83




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 3



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 0.0 1.6 98.1 0.3

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-RS1-G1

#4#10#40#200

0.0363 mm.0.0230 mm.0.0133 mm.0.0094 mm.0.0066 mm.0.0032 mm.0.0014 mm.

100.0100.0

98.40.32.22.22.21.81.31.31.3

NP NP NP

SP A-3

0.3662 0.3352 0.21550.1806 0.1268 0.09730.0891 2.42 0.84




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 4



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 1.0 3.5 3.1 89.7 1.9 0.8

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-RS1-G2

.75#4

#10#40#200

0.0359 mm.0.0227 mm.0.0131 mm.0.0092 mm.0.0065 mm.0.0032 mm.0.0014 mm.

100.099.095.592.4

2.71.21.21.21.20.80.80.8

NP NP NP

SP A-3

0.4060 0.3686 0.22720.1872 0.1271 0.09510.0863 2.63 0.82




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 5



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.4 0.5 0.8 96.9 0.3 1.1

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-RS1-G3

.75#4

#10#40#200

0.0359 mm.0.0227 mm.0.0131 mm.0.0091 mm.0.0065 mm.0.0032 mm.0.0014 mm.

100.099.699.198.3

1.41.31.31.31.31.30.90.9

NP NP NP

SP A-3

0.3665 0.3351 0.21420.1791 0.1252 0.09570.0875 2.45 0.84




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 6



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.0 0.0 1.9 96.1 0.7 1.3

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-RS2-G3

#4#10#40#200

0.0364 mm.0.0231 mm.0.0133 mm.0.0094 mm.0.0066 mm.0.0032 mm.0.0014 mm.

100.0100.0

98.12.01.71.31.31.31.31.31.3

NP NP NP

SP A-3

0.3673 0.3356 0.21370.1784 0.1243 0.09480.0867 2.47 0.83




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 7



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.6 1.3 1.9 80.6 13.8 1.8

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-RS2-G2

.75#4

#10#40#200

0.0354 mm.0.0225 mm.0.0130 mm.0.0092 mm.0.0065 mm.0.0032 mm.0.0014 mm.

100.099.498.196.215.6

3.02.62.22.22.21.31.3

NP NP NP

SM A-2-4(0)

0.3719 0.3339 0.19490.1572 0.1022 0.07220.0536 3.63 1.00




8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 8



PER

CEN

T FI

NER

0

10

20

30

40

50

60

70

80

90

100

GRAIN SIZE - mm.

0.0010.010.1110100



Fine Silt% Fines

Clay0.0 0.0 0.5 1.0 5.5 86.4 4.6 2.0

6 in

.

3 in

.

2 in

.

1½ in

.

1 in

.

¾ in

.

½ in

.

3/8

in.

#4 #10

#20

#30

#40

#60

#100

#140

#200





Classification

Coefficients


Checked By:Title:


Client:Project:

Project No: Figure

BWH-19-RS2-G1

.75#4

#10#40#200

0.0362 mm.0.0229 mm.0.0133 mm.0.0094 mm.0.0066 mm.0.0032 mm.0.0014 mm.

100.099.598.593.0

6.62.62.62.22.22.21.71.7

NP NP NP

SP-SM A-3

0.3998 0.3616 0.21900.1792 0.1199 0.08880.0803 2.73 0.82



SMFENVIRONMENTAL MANAAGER

8-16-19


MI-TECH # 10968

PL= LL= PI=


D90= D85= D60=D50= D30= D15=D10= Cu= Cc=

Remarks



Weston, WI 9


147405-Revised - P

age 150 of 150



Delivery Order No. W912P619FCX10 er 2019

APPENDIX C DATA VALIDATION REPORT

Prepared for:

US Army Corps of Engineers, Chicago District 231 South LaSalle street, Suite 1500, Chicago, Illinois 60604

Prepared by:

Wood Environment & Infrastructure Solutions, Inc. 7376 SW Durham Road, Portland, Oregon, 97224 T: 503-639-3400 9/13/2019

Data Validation Report Burns Waterway Harbor Port of Indiana-Burns Harbor Porter County, Indiana Project # 3293191855.05.****

Data Validation Report Burns Waterway Harbor

Project # 3293191855.05.**** | 9/13/2019 Page i of ii

Table of Contents 1.0 Introduction ........................................................................................................................................................................... 1 2.0 Data Validation Methodology ........................................................................................................................................ 2 3.0 Definition of Qualifiers that May be Added During Validation ......................................................................... 2 4.0 Qualification Reason Codes ............................................................................................................................................. 3 5.0 Explanation of Data Quality indicators ........................................................................................................................ 3

5.1 Blank Samples ...................................................................................................................................................... 3 5.2 Laboratory Control Sample Recoveries ...................................................................................................... 4 5.3 Matrix Spike Recoveries .................................................................................................................................... 4 5.4 Surrogate Recoveries ......................................................................................................................................... 4

6.0 Chain of Custody and Sample Receipt Condition Documentation.................................................................. 4 7.0 Specific Data Validation Findings .................................................................................................................................. 4

7.1 Inorganic Analyses .............................................................................................................................................. 4 7.1.1 Holding Times ...................................................................................................................................... 5 7.1.2 Laboratory Blank Detections .......................................................................................................... 5 7.1.3 Equipment Blank Detections .......................................................................................................... 6 7.1.4 Laboratory Control Sample Recoveries ..................................................................................... 7 7.1.5 Matrix Spike Recoveries ................................................................................................................... 7 7.1.6 Laboratory Duplicate Precision ..................................................................................................... 9 7.1.7 Data Reporting and Analytical Procedures ............................................................................10

7.2 Organic Analyses ...............................................................................................................................................10 7.2.1 Holding Times ....................................................................................................................................10 7.2.2 Laboratory Blank Detections ........................................................................................................11 7.2.3 Equipment Blank Detections ........................................................................................................11 7.2.4 Laboratory Control Sample Recoveries and Precision .......................................................12 7.2.5 Matrix Spike Recoveries .................................................................................................................12 7.2.6 Surrogate Recoveries ......................................................................................................................12 7.2.7 Data Reporting and Analytical Procedures ............................................................................12

8.0 Field Duplicates ..................................................................................................................................................................12 9.0 Summary and Conclusions .............................................................................................................................................13 10.0 References ............................................................................................................................................................................14 11.0 Limitations ............................................................................................................................................................................15

Tables Table 1: Field Samples Submitted to CT Laboratories Table 2: Field Duplicate DetectionsTable 3: Qualifiers Added During Validation


Project # 3293191855.05.**** | 9/13/2019 Page ii of ii

List of Acronyms μg/L % BTEX COC COD CT Labs EPA ID LCS LCSD LOQ mg/kg mg/L MS MTBE PAH PCB

S S M S S T T T S

micrograms per liter percent benzene, toluene, ethylbenzene, m,p-xylene, and o-xylene chain of custody chemical oxygen demand CT Laboratories United States Environmental Protection Agency identification laboratory control sample laboratory control sample duplicate limit of quantification milligram per kilogram milligram per liter matrix spike methyl tert-butyl ether polycyclic aromatic hydrocarbon polychlorinated biphenyl

quality control sample delivery group selected ion monitoring Standard Methods for the Examination of Water and Wastewater semivolatile organic compound total dissolved solids total organic carbon total suspended solids total volatile solids Wood Environment & Infrastructure Solutions, Inc.


Project # 3293191855.05.**** | 9/13/2019 Page 1 of

1.0 Introduction Wood Environment & Infrastructure Solutions, Inc. (Wood), collected 19 soil samples (including one field duplicate) and 14 water samples (including three trip blanks and one equipment blank) between August 13 and 16, 2019 from the Burns Harbor Waterway Site located in Porter County, Indiana. Wood submitted the samples to CT Laboratories (CT Labs) in Baraboo, Wisconsin, where they were received between August 14 and 17, 2019. CT Labs assigned the samples to sample delivery groups (SDGs) 147285, 147337, 147378, and 147405 and analyzed the samples for the following parameters using United States Environmental Protection Agency ( EPA) and Standard Methods for the Examination of Water and Wastewater (SM) methods:

Inorganic Analyses:

- Alkalinity by EPA 310.2,

- Ammonia by EPA 350.1,

- Phosphorus by EPA 365.1 or 365.4,

- Chemical oxygen demand (COD) by EPA 410.4,

- Oil and grease by EPA 1664A or 9071B,

- Hexavalent chromium by EPA 3060A/7199 or 7196A,

- Metals by EPA 6010D,

- Mercury by EPA 7470A or 7471B,

- pH by EPA 9040C or 9045D,

- Total organic carbon (TOC) by Lloyd Kahn/EPA 9060A,

- Hardness by SM 2340B,

- Total dissolved solids (TDS) by SM 2540C,

- Total suspended solids (TSS) by SM 2540D,

- Total volatile solids (TVS) by SM 2540G, and/or

- by SM 9223B.

Organic Analyses:

- Polychlorinated biphenyls (PCBs) by EPA 8082A,

- Methyl tert-butyl ether (MTBE) and benzene, toluene, ethylbenzene, m,p-xylene, and o-xylene(BTEX) by EPA 8260C,

- Semivolatile organic compounds (SVOCs) by EPA 8270D, and/or

- Polycyclic aromatic hydrocarbons (PAHs) by EPA 8270D-selected ion monitoring (SIM).

Additionally, soil samples were subcontracted to Mi-Tech Services, Inc., where they were analyzed for particle size distribution by ASTM International Method D 422.

A list of these samples by field sample identification (ID), sample collection date, matrix, SDG, and CT Lab’s sample ID is presented in Table 1.


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2.0 Data Validation Methodology Wood performed an EPA Stage 2A data validation on the data from the EPA and SM method analyses of these samples. Particle size distribution data was not reviewed or validated. This data validation has been performed in accordance with:

Wood, 2019. Final Work Plan, Burns Waterway Harbor Sediment and Water Sampling and Analysis.August 6.

Department of Defense, 2019. Quality System Manual for Environmental Laboratories, Version 5.3.May.

EPA. Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, EPA publication SW-846,Third Edition, Final Updates I (1993), II (1995), IIA (1994), IIB (1995), III (1997), IIIA (1999), IIIB (2005), IV(2008), and V (2015).

EPA, 2009. Guidance for Labeling externally Validated Laboratory Analytical Data for Superfund Use.EPA-540-R-08-005, January 13.

The analytical methods referenced by the laboratory.

The laboratory's certified analytical report and supporting documentation were reviewed to assess the following:

Data package and electronic data deliverable completeness;

Laboratory case narrative review;

Chain of custody (COC) compliance;

Holding time compliance;

Presence or absence of laboratory contamination as demonstrated by laboratory blanks;

Accuracy and bias as demonstrated by recovery of surrogate spikes, laboratory control sample (LCS),and matrix spike (MS) samples;

Analytical precision as relative percent difference (RPD) of analyte concentration between laboratoryduplicates or LCS/LCS duplicate (LCSD);

Sampling and analytical precision as RPD of analyte concentration between field duplicates;

Assessment of field contamination as demonstrated by equipment and trip blanks;

Insofar as possible, the degree of conformance to method requirements and good laboratorypractices.

In general, it is important to recognize that no analytical data are guaranteed to be correct, even if all quality control (QC) audits are passed. Strict QC serves to increase confidence in data, but any reported value may potentially contain error

3.0 Definition of Qualifiers that May be Added During Validation B A target analyte was detected in an associated blank QC sample. The detected sample result is

less than five times the concentration detected in the blank, or less than ten times the concentration detected in the blank for common laboratory contaminants.


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J The result is an estimated quantity. The associated numerical value is the approximate concentration of the analyte in the sample.

U The analyte was analyzed for, but was not detected at a concentration greater than the reported sample quantitation limit.

UJ The analyte was analyzed for, but was not detected. The reported quantitation limit is approximate and may be inaccurate or imprecise.

Q The result was both B and J qualified during validation.

R The data are unusable. The sample results are rejected due to serious deficiencies in meeting QC criteria. The anlayte may or may not be present in the sample.

4.0 Qualification Reason Codes The following reason codes were applied to the data during validation:

EBL A target analyte was detected in the associated equipment blank and the concentration detected in the sample is less than five times the concentration detected in the blank.

FDD Imprecision between primary and field duplicate results.

HHL Hold time was exceeded.

LBM A target analyte was detected in the associated laboratory blank and the concentration detected in the sample is less than five times the concentration detected in the blank.

LCL Low LCS recovery. Result may be biased low.

LDD Imprecision between laboratory duplicate results.

MSH High MS recovery. Result may be biased high.

MSL Low MS recovery. Result may be biased low.

SGL Low surrogate recovery. Result may be biased low.

TR The detected concentration is less than the limit of quantification (LOQ).

5.0 Explanation of Data Quality indicators Summary explanations of the specific data quality indicators reviewed during this data validation are presented in the sections below.

5.1 Blank Samples Blank samples are aliquots of analyte free matrix that are used as negative controls to verify that the sample collection, storage, preparation, and analytical system does not produce false positive results.

Equipment blanks are prepared by passing analyte free water through or over sample collectionequipment and collecting the water in sample containers. Equipment blanks are analyzed for theanalytical suite required for the project and are used to monitor for possible sample contaminationduring the sample collection process and serve as a check on the effectiveness of fielddecontamination procedures.

Trip blanks are vials of analyte free water that accompany sample bottles shipped to the field andback to the laboratory with field samples. Trip blanks assess contamination attributed to shipping and


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handling procedures, as well as contamination from containers. Target analytes should not be found in trip blanks.

Laboratory blanks are aliquots of analyte free matrix that are processed by the laboratory usingexactly the same procedures as the field samples. Laboratory blanks are used to monitor forcontamination introduced by the laboratory during sample preparation and analysis.

Target analytes should not be found in blank samples and blank detections may result in results from field samples being B qualified if the concentration detected in the sample is less than five, or ten for common laboratory contaminants, times the concentration detected in the blank.

5.2 Laboratory Control Sample Recoveries LCSs are aliquots of analyte-free matrix that are spiked with the analytes of interest for an analytical method. The spiked matrix is then processed through the same preparation and analytical procedures as the samples they accompany. LCS recovery is an indication of a laboratory’s ability to successfully perform an analytical method in an interference-free matrix.

5.3 Matrix Spike Recoveries MSs are prepared by adding known amounts of the analytes of interest for an analytical method, or a representative subset of those analytes, to an aliquot of sample. The spiked sample is then processed through the same extraction, concentration, cleanup, and analytical procedures as the unspiked samples in an analytical batch.

MS recovery and precision are an indication of a laboratory’s ability to successfully recover an analyte in the matrix of a specific sample or closely related sample matrices. It is important not to apply MS results for any specific sample to other samples without understanding how the sample matrices are related.

5.4 Surrogate Recoveries Surrogate standards are compounds that are not normally found in environmental samples but are similar to target analytes in chemical composition and analytical behavior. Surrogates are added to a sample before extraction to monitor extraction and analytical efficiency.

6.0 Chain of Custody and Sample Receipt Condition Documentation The samples were received by CT Labs under proper COC, intact, in good condition, and at temperatures less than the EPA-recommended maximum of 6 degrees Celsius, with the following exception:

The trip blank was not listed on the COC associated with SDG 147285. CT labs added the trip blank tothe COC and analyzed it for BTEX and MTBE.

7.0 Specific Data Validation Findings Sections 7.1 through 8.0 contain narrative descriptions of the data validation findings and data quality limitations.

7.1 Inorganic Analyses Inorganic results generated by CT Labs may be considered usable with the limitations summarized in Sections 7.1.1 through 7.1.7.


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7.1.1 Holding Times Samples were analyzed within the method-specified maximum holding times of:

15 minutes for pH in water;

24 hours for E. coli, hexavalent chromium in water, and pH in soil;

7 days for TDS, TSS, and TVS;

14 days for alkalinity;

28 days for ammonia, COD, mercury, oil and grease, phosphorus, and TOC;

30 days for hexavalent chromium in soil; and

180 days for hardness and metals.

Hold time exceedances are summarized below.

All pH analyses were performed outside the EPA-recommended maximum hold times of 15 minutesfor water samples and 24 hours for soil samples. Wood J qualified all pH results because of the missedhold times. (J-HHL)

Samples BWH-19-MU4-C1, BWH-19-MU4-C2, BWH-19-MU4-C3, BWH-19-RS1-G1, BWH-19-RS1-G2,BWH-19-RS1-G3, BWH-19-RS2-G1, BWH-19-RS2-G2, and BWH-19-RS2-G3 were collected August 16,but were not analyzed for E. coli until August 19. Wood J qualified the detected and UJ qualified thenon-detected E. coli results from these samples because of the missed hold times. (J/UJ-HHL)

7.1.2 Laboratory Blank Detections Target analytes were not detected in the laboratory blanks associated with the analysis of these samples, with the following exceptions:

Chromium and selenium were detected at concentrations of 0.703 micrograms per liter (μg/L) and3.11 μg/L, respectively, in the laboratory blank associated with the metal analysis of samplesBWH-19-MU1-W1, BWH-19-MU3-W3, and BWH-19-MU4-W4. Data limitations are summarizedbelow.

- Wood B qualified the detected chromium results from the associated samples because theconcentrations detected in the samples were less than five times the concentration detected in the blank. (B-LBM)

- Selenium was not detected in the associated samples and data usability is not adversely affected by the blank detection.

Aluminum (0.23 milligrams per kilogram [mg/kg]), iron (0.34 mg/kg), and selenium (0.14 mg/kg) weredetected in the laboratory blank associated with the metal analysis of samples BWH-19-MU1-C1,BWH-19-MU1-C2, BWH-19-MU1-C3, BWH-19-MU3-C1, BWH-19-MU3-C2, and BWH-19-MU3-C3.Data limitations are summarized below.

- Wood B qualified the detected selenium results from samples BWH-19-MU1-C2,BWH-19-MU1-C3, and BWH-19-MU3-C3 because the concentrations detected in the samples were less than five times the concentration detected in the blank. (B-LBM)

- Aluminum and iron concentrations detected in the associated samples were greater than five times the concentration detected in the blank and selenium was not detected in samples


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BWH-19-MU1-C1, BWH-19-MU3-C1, and BWH-19-MU3-C2. Data usability is not adversely affected by the blank detections.

Aluminum and barium were detected at concentrations of 11.9 μg/L and 21.4 μg/L, respectively, in thelaboratory blank associated with the metal analysis of samples BWH-19-RS1-W1 andBWH-19-RS2-W2. Wood B qualified the detected aluminum and barium results from the associatedsamples because the concentration detected in the samples were less than five times theconcentrations detected in the blank. (B-LBM)

Aluminum (0.48 mg/kg), copper (0.084 mg/kg), iron (0.44 mg/kg), and selenium (0.11 mg/kg) weredetected in the laboratory blank associated with the metal analysis of samples BWH-19-MU4-C1,BWH-19-MU4-C2, BWH-19-MU4-C3, BWH-19-RS1-G1, BWH-19-RS1-G2, BWH-19-RS1-G3,BWH-19-RS2-G1, BWH-19-RS2-G2, and BWH-19-RS2-G3. Data limitations are summarized below.

- Wood B qualified the detected selenium results from samples BWH-19-MU4-C2,BWH-19-MU4-C3, and BWH-19-RS2-G1 because the concentration detected in the samples were less than five times the concentration detected in the blank. (B-LBM)

- Selenium was detected in sample BWH-19-MU4-C1 at a concentration greater than five times the concentration detected in the blank and was not detected in the remaining associated samples. Data usability is not adversely affected by the blank detection.

- The remaining analytes were detected in the associated samples at concentrations greater than five times the concentrations detected in the blank and data usability is not adversely affected by the blank detections.

Chromium was detected at a concentration of 0.023 mg/kg in the laboratory blank associated withthe metal analysis of samples BWH-19-MU2-C1, BWH-19-MU2-C2, BWH-19-MU2-C3, and FD-1.Chromium concentrations detected in the associated samples were greater than five times theconcentration detected in the blank and data usability is not adversely affected by the blankdetection.

7.1.3 Equipment Blank Detections Equipment blank EB-1 was collected on August 16, 2019 and Wood evaluated detections in the equipment blank against samples collected the same day as the blank.

Target analytes were not detected in the equipment blank, with the following exceptions:

Aluminum (35.6 μg/L), barium (0.63 μg/L), hardness (3.8 milligrams per liter [mg/L]), iron (22.1 μg/L),oil and grease (1.7 mg/L), selenium (4.5 μg/L), TDS (27 mg/L), and zinc (25.9 μg/L) were detected inequipment blank EB-1. Data limitations are summarized below.

- Wood B qualified the detected aluminum results from samples BWH-19-RS1-W1 andBWH-19-RS2-W2 because the concentrations detected in the samples were less than five times the concentration detected in the blank. (B-EBL)

- Wood B qualified the detected oil and grease and selenium results from sample BWH-19-RS2-W2 because the concentrations detected in the sample were less than five times the concentrations detected in the blank. (B-EBL)

- The remaining analytes either were not detected in the associated samples or were detected at concentrations greater than five times the concentrations detected in the blank and data usability is not adversely affected by the blank detections.


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7.1.4 Laboratory Control Sample Recoveries LCS recoveries were within laboratory-specified limits, with the following exceptions:

TSS recovery was low at 60 percent (%) in the LOQ check sample associated with the analysis ofsamples BWH-19-MU1-E1, BWH-19-MU1-W1, BWH-19-MU3-E1, BWH-19-MU3-W3,BWH-19-MU4-E1, BWH-19-MU4-W4, BWH-19-RS1-W1, and BWH-19-RS2-W2. Data limitations aresummarized below.

- Wood J qualified the detected TSS result from sample BWH-19-MU3-E1 and UJ qualified thenon-detected TSS results from samples BWH-19-MU1-E1, BWH-19-MU1-W1, BWH-19-MU3-W3, BWH-19-MU4-W4, BWH-19-RS1-W1, and BWH-19-RS2-W2 because of potential low analytical bias. (J/UJ-LCL)

- The TSS concentration detected in sample BWH-19-MU4-E1 was greater than five times the LOQ and in Wood’s professional opinion, data usability is not adversely affected by the low LOQ check recovery.

7.1.5 Matrix Spike Recoveries CT Labs performed MS analyses on the following samples for the following parameters:

BWH-19-MU1-C2 for ammonia, COD, hexavalent chromium, mercury, metals, oil and grease, andphosphorus;

BWH-19-MU1-E1 for dissolved iron;

BWH-19-MU1-W1 for alkalinity, dissolved iron, hexavalent chromium, and phosphorus;

BWH-19-MU2-C1 for COD;

BWH-19-MU2-C2 for ammonia and metals;

BWH-19-MU2-E1 for hexavalent chromium and metals;

BWH-19-MU2-W2 for COD, dissolved iron, hexavalent chromium, mercury, and metals;

BWH-19-MU3-E1 for ammonia and COD;

BWH-19-MU3-W3 for alkalinity and phosphorus;

BWH-19-MU4-C3 (316695) for ammonia, mercury, and metals;

BWH-19-MU4-W4 for metals;

BWH-19-RS1-G2 (316702) for phosphorus;

BWH-19-RS1-W1 for dissolved iron and hexavalent chromium; and

BWH-19-RS2-W2 for metals.

Recoveries were within laboratory-specified limits, with the following exceptions:

Aluminum (300%), cadmium (114%), COD (163%), and iron (588%) recoveries were high; andhexavalent chromium (30%), nickel (78%), phosphorus (50%), and selenium (77%) recoveries were lowin the MSs performed on sample BWH-19-MU1-C2. Data limitations are summarized below.

- Wood J qualified the detected COD result from the unspiked native sample because of potentialhigh analytical bias. (J-MSH)


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- Wood UJ qualified the non-detected hexavalent chromium result and J qualified the detected nickel and phosphorus results from the unspiked native sample because of potential low analytical bias. (UJ/J-MSL)

- The selenium result from the unspiked native sample was previously B qualified due to a detection in the associated laboratory blank and it is not possible to apply combined qualifiers to the data. Wood Q qualified the selenium result to indicate that it should be both B qualified due to the blank detection and J qualified due to low MS recovery, indicating potential low analytical bias. (Q-MSL)

- Aluminum and iron concentrations detected in the unspiked native sample were greater than four times the spike concentrations and it is not possible to assess data usability for these analytes in this sample based on MS recoveries.

- Cadmium recovery was high and cadmium was not detected in the unspiked native sample. Data usability is not adversely affected by the potential high analytical bias.

COD recovery was low at 9% in the MS performed on sample BWH-19-MU2-C1. Wood J qualified theCOD results from this sample and its field duplicate DUP-1 because of potential low analytical bias.(J-MSL)

Aluminum (181%), copper (120%) and iron (0%) recoveries were outside of limits in the MS performedon sample BWH-19-MU2-C2. Data limitations are summarized below.

- Wood J qualified the detected copper result from sample BWH-19-MU2-C2 because of potentialhigh analytical bias. (J-MSH)

- Aluminum and iron concentrations in the unspiked native sample were greater than four times the spike concentrations and it is not possible to assess data usability for these analytes in this sample based on MS recoveries.

Aluminum (172%), copper (120%), and iron (58%) recoveries were outside of limits in the MSperformed on sample BWH-19-MU2-E1. Data limitations are summarized below.

- Wood J qualified the detected aluminum and copper results from the unspiked native sample dueto potential high analytical bias. (J-MSH)

- The iron concentration in the unspiked native sample was greater than four times the spike concentration and it is not possible to assess data usability for this analyte in this sample based on MS recovery.

Aluminum (58%), arsenic (67%), barium (59%), cadmium (63%), chromium (59%), copper (60%), iron(63%), lead (64%), nickel (57%), selenium (72%), silver (76%), zinc (63%), and dissolved iron (56%)recoveries were low in the MS performed on sample BWH-19-MU2-W2. Wood J qualified thedetected and UJ qualified the non-detected metal and dissolved iron results from this sample becauseof potential low analytical bias. (J/UJ-MSL)

Ammonia recovery was low at 19% and COD recovery was high at 111% in the MSs performed onsample BWH-19-MU3-E1. Data limitations are summarized below.

- Wood J qualified the detected ammonia result from the unspiked native sample because ofpotential low analytical bias. (J-MSL)

- Wood J qualified the detected COD result from the unspiked native sample due to potential high analytical bias. (J-MSH)


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Copper recovery was high at 116% in the MS performed on sample BWH-19-MU4-W4. Wood Jqualified the detected copper result from the unspiked native sample due to potential high analyticalbias. (J-MSH)

Iron was not recovered from the MS performed on sample BWH-19-MU4-C3. The iron concentrationin the unspiked native sample was greater than four times the spike concentration and it is notpossible to assess data usability for this analyte in this sample based on MS recovery.

Copper recovery was high at 116% in the MS performed on sample BWH-19-RS2-W2. Copper was notdetected in the unspiked native sample and data usability is not adversely affected by the potentialhigh analytical bias.

7.1.6 Laboratory Duplicate Precision CT Labs performed duplicate analyses on the following samples for the following analyses:

BWH-19-MU1-C2 for ammonia, COD, hexavalent chromium, mercury, oil and grease, pH, phosphorus,solids, and TOC;

BWH-19-MU1-E1 for mercury;

BWH-19-MU1-W1 for hexavalent chromium, mercury, and TDS;

BWH-19-MU2-C1 for COD;

BWH-19-MU2-C2 for ammonia, percent solids, and metals;

BWH-19-MU2-E1 for hexavalent chromium and metals;

BWH-19-MU2-W2 for alkalinity, ammonia, COD, dissolved iron, hexavalent chromium, mercury,metals, and TSS;

BWH-19-MU3-E1 for ammonia and COD;

BWH-19-MU4-C3 for ammonia, mercury, and metals;

BWH-19-MU4-E1 for TDS and TSS;

BWH-19-MU4-W4 for alkalinity, metals, phosphorus, and TSS;

BWH-19-RS1-G2 for phosphorus;

BWH-19-RS1-W1 for dissolved iron, hexavalent chromium, and phosphorus; and

BWH-19-RS2-W2 for metals.

RPDs between primary and duplicate results were less than laboratory-specified maximum limits, with the following exceptions:

RPDs between primary and duplicate aluminum and barium results were high at 92% and 29%,respectively, in the duplicate analysis performed on sample BWH-19-MU2-W2. Data limitations aresummarized below.

- Wood J qualified the barium result from this sample because of potential analytical imprecision.(J-LDD)

- The difference between aluminum results was less than the LOQ, indicating acceptable analytical precision.


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RPDs between copper and selenium results from the primary and duplicate analyses of sampleBWH-19-MU4-C3 were high at 93% and 200% respectively. Data limitations are summarized below.

- The difference between primary and duplicate copper results was greater than the LOQ. Wood Jqualified the detected copper result from this sample because of potential analytical imprecision. (J-LDD)

- Selenium was not detected in the primary analysis but it was detected in the duplicate analysis. The difference between results was less than the applicable LOQ, indicating acceptable analytical precision.

RPDs between cadmium results were high in the duplicate analyses performed on samplesBWH-19-MU2-C2 and BWH-19-MU2-E1 at 73% and 21%, respectively. The differences betweenprimary and duplicate cadmium results were less than the applicable LOQs, indicating acceptableanalytical precision.

The RPD between phosphorus results was high at 28% in the duplicate analysis performed on sampleBWH-19-MU1-C2. The difference between primary and duplicate phosphorus results was less than theapplicable LOQ, indicating acceptable analytical precision.

The RPD between phosphorus results was high at 79% in the duplicate analysis performed on sampleBWH-9-RS1-G2. The difference between primary and duplicate phosphorus results was less than theapplicable LOQ, indicating acceptable analytical precision.

Dissolved iron was not detected in the primary analysis of sample BWH-19-RS1-W1 but it wasdetected in the duplicate analysis. The differences between the primary and duplicate results was lessthan the applicable LOQ, indicating acceptable analytical precision.

Chromium and selenium were not detected in the primary analysis of sample BWH-19-RS2-W2, butthey were detected in the duplicate analysis. The differences between primary and duplicate resultswere less than the applicable LOQs, indicating acceptable analytical precision.

7.1.7 Data Reporting and Analytical Procedures CT Labs J qualified results with detected concentrations less than the LOQ. Wood agrees that these results are quantitatively uncertain and has maintained the laboratory’s J qualifiers. (J-TR)

7.2 Organic Analyses Organic results generated by CT Labs may be considered usable with the limitations summarized in Sections 7.2.1 through 7.2.7.

7.2.1 Holding Times Samples were extracted and analyzed within the method-specified maximum holding times of:

Extraction within 7 days of sampling and analysis within 40 days from extraction for PAHs and SVOCsin water;

Analysis within 14 days from sampling for BTEX and MTBE;

Extraction within 14 days and analysis within 40 days from extraction for PAHs in soil; and

Extraction within one year of collection and analysis within one year of extraction for PCBs.


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7.2.2 Laboratory Blank Detections Target analytes were not detected in the laboratory blanks associated with the analysis of these samples, with the following exceptions:

Benzo(a)pyrene (0.0407 μg/L), benzo(b)fluoranthene (0.0343 μg/L), chrysene (0.00764 μg/L), andpyrene (0.0215 μg/L) were detected in the laboratory blank associated with the PAH analysis ofsamples BWH-19-MU1-E1, BWH-19-MU1-W1, BWH-19-MU2-E1, BWH-19-MU2-W2,BWH-19-MU3-E1, BWH-19-MU3-W3, BWH-19-MU4-E1, BWH-19-MU4-W4, BWH-19-RS1-W1, andBWH-19-RS2-W2. Data limitations are summarized below.

- Wood B qualified the detected benzo(a)pyrene results from samples BWH-19-MU2-E1 andBWH-19-MU4-E1 because the concentrations detected in the samples were less than five times the concentration detected in the blank. (B-LBM)

- Wood B qualified the detected benzo(a)pyrene, benzo(b)fluoranthene, and pyrene results from sample BWH-19-MU3-E1 because the concentrations detected in the sample were less than five times the concentration detected in the blank. (B-LBM)

- Wood B qualified the detected benzo(b)fluoranthene and pyrene results from sample BWH-19-MU1-E1 because the concentrations detected in the sample were less than five times the concentrations detected in the blank. (B-LBM)

- Wood B qualified the detected benzo(b)fluoranthene, chrysene, and pyrene results from samples BWH-19-MU2-E1 and BWH-19-MU4-E1 because the concentrations detected in the samples were less than five times the concentrations detected in the blank. (B-LBM)

- Wood B qualified the detected pyrene results from samples BWH-19-MU1-W1, BWH-19-MU2-W2, BWH-19-MU3-W3, BWH-19-MU4-W4, BWH-19-RS1-W1, and BWH-19-RS2-W2 because the concentrations detected in the samples were less than five times the concentration detected in the blank. (B-LBM)

- Benzo(a)pyrene, benzo(b)fluoranthene, and chrysene were not detected in the remaining samples and data usability is not adversely affected by the blank detections.

7.2.3 Equipment Blank Detections Equipment blank EB-1 was collected on August 16, 2019 and Wood evaluated detections in the equipment blank against samples collected the same day as the blank.

Target analytes were not detected in the equipment blank, with the following exceptions:

Benzaldehyde (1.0 μg/L), benzo(b)fluoranthene (0.033 μg/L), bis(2-ethylhexyl)phthalate (0.57 μg/L),di-n-butylphthalate (0.69 μg/L), naphthalene (0.015 μg/L), pyrene (0.018 μg/L), and toluene(0.32 μg/L) were detected in equipment blank EB-1. Data limitations are summarized below.

- Wood B qualified the detected pyrene results from samples BWH-19-RS1-W1 andBWH-19-RS2-W2 because the concentrations detected in the samples were less than five times the concentration detected in the blank. (B-EBL)

- The remaining analytes either were not detected in the associated samples or were detected at concentrations greater than five times the concentration detected in the blank. Data usability is not adversely affected by the blank detections.


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7.2.4 Laboratory Control Sample Recoveries and Precision LCS recoveries were within laboratory-specified limits and RPDs between LCS and LCSD results were less than laboratory-specified maximum values, with the following exceptions:

3,3’-Dichlorobenzidine recovery was low at 22% in the LCS and benzidine was not recovered from theLCS and LCSD associated with the SVOC analysis of samples BWH-19-MU1-E1, BWH-19-MU1-W1,BWH-19-MU2-E1, BWH-19-MU2-W2, BWH-19-MU3-E1, BWH-19-MU3-W3, BWH-19-MU4-E1,BWH-19-MU4-W4, BWH-19-RS1-W1, and BWH-19-RS2-W2. Additionally, RPDs between LCS andLCSD results were high for benzyl alcohol (41%), 4-nitrophenol (28%), and pyridine (33%). Datalimitations are summarized below.

- Wood R qualified and rejected the non-detected benzidine results from the associated samplesbecause the analyte could not be recovered from the LCS or LCSD. (R-LCL)

- Wood UJ qualified the non-detected 3,3’-dichlorobenzidine results from the associated samples because of potentially low analytical bias. (UJ-LCL)

- Benzyl alcohol, 4-nitrophenol, and pyridine were not detected in the associated samples and data usability is not adversely affected by the potential analytical imprecision.

7.2.5 Matrix Spike Recoveries CT Labs performed MS analyses on the following samples for the following parameters:

BWH-19-MU1-C2 for BTEX and MTBE, PAHs, and PCBs; and

BWH-19-RS1-W1 for BTEX and MTBE.

Recoveries were within laboratory-specified limits.

7.2.6 Surrogate Recoveries Surrogate recoveries were within laboratory-specified limits, except as described below:

Recoveries of the surrogate compounds 2-methylnaphthalene-d10 and fluoranthene-d10 were low at45% and 47%, respectively, in the PAH analysis of sample BWH-19-MU3-C2. Wood J qualified the PAHresults from this sample because of potential low analytical bias. (J-SGL)

Recovery of the surrogate compound 2-methylnaphthalene-d10 was low at 49% in the PAH analysis ofsample BWH-19-RS1-G2. Wood J qualified the detected and UJ qualified the non-detected PAHresults from this sample because of potential low analytical bias. (J/UJ-SGL)

7.2.7 Data Reporting and Analytical Procedures CT Labs J qualified results with detected concentrations less than the LOQ. Wood agrees that these results are quantitatively uncertain and has maintained the laboratory’s J qualifiers. (J-TR)

8.0 Field Duplicates Wood collected a field duplicate (FD-1) with primary sample BWH-19-MU2-C1. RPDs between primary and field duplicate results were less than 50% or differences between primary and field duplicate results were less than the LOQ, with the following exceptions:

RPDs between mercury (64%), aluminum (82%), iron (52%), nickel (67%), and Aroclor 1248 (99%)results from sample BWH-19-MU2-C1 and its field duplicate FD-1 were high. Wood J qualified the


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result for these analytes in the primary and field duplicate samples because of potential sampling and/or analytical imprecision. (J-FDD)

Detections in the primary and field duplicate samples are summarized in Table 2.

9.0 Summary and Conclusions Wood reviewed 2,265 data points from field samples during this validation. Qualification statistics are summarized below.

Wood R qualified and rejected 10 data points (0.44%) because the analyte could not be recoveredfrom the LCS or LCSD.

Wood B qualified 33 data points (1.5%) because of detections in the associated laboratory and/orequipment blanks.

Wood J or UJ qualified 269 data points (12%) because of missed hold times, low LCS recoveries,imprecision between laboratory duplicate results, high or low MS recoveries, low surrogate recoveries,analyte concentrations less than the LOQ, and/or imprecision between primary and field duplicateresults.

Wood Q qualified one result to indicate that it should be both B qualified because of a detection inthe associated laboratory blank and J qualified because of low MS recovery.

The data are more than 99% usable with the addition of the qualifiers summarized in Table 3.


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10.0 References Wood, 2019. Final Work Plan, Burns Waterway Harbor Sediment and Water Sampling and Analysis. August

6.

Department of Defense, 2019. Quality System Manual for Environmental Laboratories, Version 5.3. May.

EPA. Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, EPA publication SW-846, Third Edition, Final Updates I (1993), II (1995), IIA (1994), IIB (1995), III (1997), IIIA (1999), IIIB (2005), IV (2008), and V (2015).

EPA, 2009. Guidance for Labeling externally Validated Laboratory Analytical Data for Superfund Use. EPA-540-R-08-005, January 13.


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11.0 Limitations This report was prepared exclusively for US Army Corps of Engineers by Wood Environment & Infrastructure Solutions, Inc. The quality of information, conclusions, and estimates contained herein is consistent with the level of effort involved in Wood services and based on: i) information available at the time of preparation, ii) data supplied by outside sources, and iii) the assumptions, conditions, and qualifications set forth in this report. This data validation report is intended to be used by US Army Corps of Engineers for the Burns Harbor Waterway Site only, subject to the terms and conditions of its contract with Wood. Any other use of, or reliance on, this report by any third party is at that party’s sole risk.

Tables

TABLE 1Field Samples Submitted to CT Laboratories

Burns Harbor Waterway

Field Sample Identification

Collection Date Matrix Sample Delivery

Group

Laboratory Sample

IdentificationNotes

BWH-19-MU2-C2 8/13/2019 Soil 147285 315103BWH-19-MU2-C1 8/13/2019 Soil 147285 315114BWH-19-MU2-C3 8/13/2019 Soil 147285 315115FD-1 8/13/2019 Soil 147285 315116 Field duplicate of BWH-19-MU2-C1BWH-19-MU2-W2 8/13/2019 Groundwater 147285 315117/315136TB-081319 8/13/2019 Water 147285 315168 Trip blankBWH-19-MU2-E1 8/19/2019 Groundwater 147285 317012/317093BWH-19-MU1-C3 8/14/2019 Soil 147337 315732BWH-19-MU1-C2 8/14/2019 Soil 147337 315764BWH-19-MU1-C1 8/14/2019 Soil 147337 315765BWH-19-MU3-C1 8/14/2019 Soil 147337 315766BWH-19-MU1-W1 8/14/2019 Groundwater 147337 315808/315810BWH-19-MU3-W3 8/14/2019 Groundwater 147337 315815/315816BWH-19-MU4-W4 8/14/2019 Groundwater 147337 315817/315818TB-081419 8/14/2019 Water 147337 315829 Trip blankBWH-19-MU1-E1 8/19/2019 Groundwater 147337 317096/317097BWH-19-MU3-E1 8/20/2019 Groundwater 147337 317100/317101BWH-19-MU4-E1 8/20/2019 Groundwater 147337 317102/317103BWH-19-MU3-C2 8/15/2019 Soil 147378 316441BWH-19-MU3-C3 8/15/2019 Soil 147378 316444BWH-19-MU4-C3 8/16/2019 Soil 147405 316695BWH-19-MU4-C1 8/16/2019 Soil 147405 316696BWH-19-MU4-C2 8/16/2019 Soil 147405 316697BWH-19-RS1-G1 8/16/2019 Soil 147405 316699BWH-19-RS1-W1 8/16/2019 Groundwater 147405 316700/316701BWH-19-RS1-G2 8/16/2019 Soil 147405 316702BWH-19-RS1-G3 8/16/2019 Soil 147405 316703BWH-19-RS2-G3 8/16/2019 Soil 147405 316704BWH-19-RS2-W2 8/16/2019 Groundwater 147405 316705/316706BWH-19-RS2-G2 8/16/2019 Soil 147405 316707BWH-19-RS2-G1 8/16/2019 Soil 147405 316708TB-081619 8/16/2019 Water 147405 316709 Trip blankEB-1 8/16/2019 Water 147405 316710/316711 Equipment blank

Burns Harbor WaterwayData Validation ReportS:\Data\Burns Harbor Waterway\Burns Harbor Waterway Data Validation Tables

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TABLE 2Field Duplicate Detections


AnalyteAverage Limit

ofQuantification

Primary Result

Duplicate Result

Relative Percent

DifferenceNotes

Samples BWH-19-MU2-C1 and FD-1Percent Solids 0.1 % 64.4 66.3 2.9%Total Volatile Solids 0.0001 gVS/gTS 0.0361 0.0328 9.6%pH 0.1 S.U. 8.44 8.68 2.8%Oil and Grease 765 mg/kg 1,320 884 40%Ammonia 7.7 mg/kg 8.70 8.97 3.1%COD 11,500 mg/kg 84,700 67,200 23%Phosphorus 280 mg/kg 148 J 157 J 5.9%Total Organic Carbon 460 mg/kg 51,600 48,200 6.8%Mercury 0.014 mg/kg 0.062 0.032 64% J-FDDAluminum 0.38 mg/kg 3,190 1,330 82% J-FDDArsenic 1.3 mg/kg 4.3 2.9 39%Barium 0.078 mg/kg 28.4 22.1 25%Cadmium 0.062 mg/kg 0.21 0.30 35%Chromium 0.22 mg/kg 25.7 16.0 47%Copper 0.62 mg/kg 39.5 32.4 20%Iron 2.8 mg/kg 11,500 6,760 52% J-FDDLead 0.39 mg/kg 25.1 16.4 42%Nickel 0.19 mg/kg 9.6 4.8 67% J-FDDSelenium 0.62 mg/kg 0.48 J 0.33 J 37%Silver 0.16 mg/kg 0.078 J 0.080 J 2.5%Zinc 0.47 mg/kg 87.7 76.9 13%Benzene 53 μg/kg 17.0 J 31 U NC ± LOQToluene 105 μg/kg 24.5 J 32.0 J 27%Aroclor-1248 45 μg/kg 100 33.9 J 99% J-FDD1-Methylnaphthalene 15 μg/kg 78.9 92.4 16%2-Methylnaphthalene 15 μg/kg 170 196 14%Acenaphthene 15 μg/kg 96.1 101 5.0%Acenaphthylene 15 μg/kg 90.6 90.3 0.33%Anthracene 15 μg/kg 243 267 9.4%Benzo(a)anthracene 15 μg/kg 605 721 17%Benzo(a)pyrene 15 μg/kg 469 570 19%Benzo(b)fluoranthene 15 μg/kg 605 772 24%Benzo(g,h,i)perylene 15 μg/kg 361 437 19%Benzo(k)fluoranthene 30 μg/kg 165 193 16%Chrysene 15 μg/kg 514 631 20%Dibenzo(a,h)anthracene 15 μg/kg 108 121 11%Fluoranthene 30 μg/kg 1,010 1,080 6.7%Fluorene 15 μg/kg 193 207 7.0%Indeno(1,2,3-cd)pyrene 15 μg/kg 300 367 20%Naphthalene 15 μg/kg 504 526 4.3%Phenanthrene 30 μg/kg 876 891 1.7%Pyrene 30 μg/kg 815 863 5.7%

Notes:% = percentμg/kg = micrograms per kilogramgVS/gTS = grams volatile solids per gram total solidsmg/kg = milligrams per kilogramNC = not calculableS.U. = standard units


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TABLE 2Field Duplicate Detections


Qualifier Definitions:J = The result is an estimated quantity. The associated numerical value is the approximate concentration of

the analyte in the sample.U = The analyte was analyzed for, but was not detected at a concentration greater than the reported sample

quantitation limit.

Reason Codes:± LOQ = The difference between concentrations is less than the limit of quantification, indicating acceptable

sampling and analytical precision.FDD = Imprecision between primary and field duplicate results.


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TABLE 3Qualifiers Added During Validation


Sample Identification Method Analyte Concentration Qualifier and Reason Code

BWH-19-MU1-C1 EPA 365.4 Phosphorus 198 mg/kg J TRBWH-19-MU1-C1 EPA 8082 Aroclor-1248 35.1 μg/kg J TRBWH-19-MU1-C1 EPA 9045 pH 7.25 S.U. J HHLBWH-19-MU1-C2 EPA 365.4 Phosphorus 202 mg/kg J MSL, TRBWH-19-MU1-C2 EPA 410.4 COD 47,700 mg/kg J MSHBWH-19-MU1-C2 EPA 6010 Nickel 16.6 mg/kg J MSLBWH-19-MU1-C2 EPA 6010 Selenium 0.15 mg/kg Q LBM, MSLBWH-19-MU1-C2 EPA 7199 Hexavalent Chromium 0.16 mg/kg UJ MSLBWH-19-MU1-C2 EPA 9045 pH 7.32 S.U. J HHLBWH-19-MU1-C3 EPA 365.4 Phosphorus 229 mg/kg J TRBWH-19-MU1-C3 EPA 6010 Selenium 0.11 mg/kg B LBMBWH-19-MU1-C3 EPA 8260C Toluene 83.3 μg/kg J TRBWH-19-MU1-C3 EPA 9045 pH 7.39 S.U. J HHLBWH-19-MU1-C3 EPA 9071 Oil and Grease 363 mg/kg J TRBWH-19-MU1-E1 EPA 410.4 COD 21 mg/L J TRBWH-19-MU1-E1 EPA 6010 Dissolved Iron 33.3 μg/L J TRBWH-19-MU1-E1 EPA 6010 Total Copper 4.5 μg/L J TRBWH-19-MU1-E1 EPA 6010 Total Lead 2.3 μg/L J TRBWH-19-MU1-E1 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU1-E1 EPA 8270D Benzidine 52 μg/L R LCLBWH-19-MU1-E1 EPA 8270D Diethylphthalate 0.62 μg/L J TRBWH-19-MU1-E1 EPA 8270D Di-n-butylphthalate 2.6 μg/L J TRBWH-19-MU1-E1 EPA 8270D-SIM Benzo(b)fluoranthene 0.035 μg/L B LBMBWH-19-MU1-E1 EPA 8270D-SIM Fluoranthene 0.014 μg/L J TRBWH-19-MU1-E1 EPA 8270D-SIM Fluorene 0.01 μg/L J TRBWH-19-MU1-E1 EPA 8270D-SIM Pyrene 0.023 μg/L B LBMBWH-19-MU1-E1 EPA 9040 pH 8.12 S.U. J HHLBWH-19-MU1-E1 SM 2540D Total Suspended Solids 2.0 mg/L UJ LCLBWH-19-MU1-W1 EPA 6010 Total Aluminum 25.4 μg/L J TRBWH-19-MU1-W1 EPA 6010 Total Chromium 0.84 μg/L B LBMBWH-19-MU1-W1 EPA 6010 Total Zinc 1.7 μg/L J TRBWH-19-MU1-W1 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU1-W1 EPA 8270D Benzidine 50 μg/L R LCLBWH-19-MU1-W1 EPA 8270D-SIM Pyrene 0.012 μg/L B LBMBWH-19-MU1-W1 EPA 9040 pH 8.36 S.U. J HHLBWH-19-MU1-W1 SM 2540D Total Suspended Solids 2.0 mg/L UJ LCLBWH-19-MU2-C1 EPA 365.4 Phosphorus 148 mg/kg J TRBWH-19-MU2-C1 EPA 410.4 COD 84,700 mg/kg J MSLBWH-19-MU2-C1 EPA 6010 Aluminum 3,190 mg/kg J FDDBWH-19-MU2-C1 EPA 6010 Iron 11,500 mg/kg J FDDBWH-19-MU2-C1 EPA 6010 Nickel 9.6 mg/kg J FDDBWH-19-MU2-C1 EPA 6010 Selenium 0.48 mg/kg J TRBWH-19-MU2-C1 EPA 6010 Silver 0.078 mg/kg J TRBWH-19-MU2-C1 EPA 7471B Mercury 0.062 mg/kg J FDDBWH-19-MU2-C1 EPA 8082 Aroclor-1248 100 μg/kg J FDDBWH-19-MU2-C1 EPA 8260C Benzene 17 μg/kg J TRBWH-19-MU2-C1 EPA 8260C Toluene 24.5 μg/kg J TRBWH-19-MU2-C1 EPA 9045 pH 8.44 S.U. J HHLBWH-19-MU2-C2 EPA 350.1 Ammonia Nitrogen 70.7 mg/kg J TRBWH-19-MU2-C2 EPA 365.4 Phosphorus 175 mg/kg J TRBWH-19-MU2-C2 EPA 6010 Cadmium 0.056 mg/kg J TRBWH-19-MU2-C2 EPA 6010 Copper 18.9 mg/kg J MSHBWH-19-MU2-C2 EPA 6010 Selenium 0.18 mg/kg J TRBWH-19-MU2-C2 EPA 6010 Silver 0.092 mg/kg J TR


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BWH-19-MU2-C2 EPA 8082 Aroclor-1248 29 μg/kg J TRBWH-19-MU2-C2 EPA 9045 pH 7.93 S.U. J HHLBWH-19-MU2-C2 EPA 9071 Oil and Grease 548 mg/kg J TRBWH-19-MU2-C3 EPA 365.4 Phosphorus 111 mg/kg J TRBWH-19-MU2-C3 EPA 6010 Selenium 0.14 mg/kg J TRBWH-19-MU2-C3 EPA 6010 Silver 0.083 mg/kg J TRBWH-19-MU2-C3 EPA 9045 pH 8.16 S.U. J HHLBWH-19-MU2-C3 EPA 9071 Oil and Grease 449 mg/kg J TRBWH-19-MU2-E1 EPA 1664 Oil and Grease 1.5 mg/L J TRBWH-19-MU2-E1 EPA 410.4 COD 17 mg/L J TRBWH-19-MU2-E1 EPA 6010 Total Aluminum 1490 μg/L J MSHBWH-19-MU2-E1 EPA 6010 Total Arsenic 5.3 μg/L J TRBWH-19-MU2-E1 EPA 6010 Total Cadmium 0.34 μg/L J TRBWH-19-MU2-E1 EPA 6010 Total Copper 5.8 μg/L J MSH, TRBWH-19-MU2-E1 EPA 6010 Total Nickel 2.2 μg/L J TRBWH-19-MU2-E1 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/l UJ LCLBWH-19-MU2-E1 EPA 8270D Benzidine 51 μg/L R LCLBWH-19-MU2-E1 EPA 8270D Diethylphthalate 0.6 μg/L J TRBWH-19-MU2-E1 EPA 8270D Di-n-octylphthalate 1.2 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM 1-Methylnaphthalene 0.0073 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Acenaphthene 0.022 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Acenaphthylene 0.0077 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Anthracene 0.017 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Benzo(a)pyrene 0.056 μg/L B LBMBWH-19-MU2-E1 EPA 8270D-SIM Benzo(b)fluoranthene 0.067 μg/L B LBMBWH-19-MU2-E1 EPA 8270D-SIM Benzo(k)fluoranthene 0.016 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Chrysene 0.036 μg/L B LBMBWH-19-MU2-E1 EPA 8270D-SIM Fluorene 0.034 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Naphthalene 0.02 μg/L J TRBWH-19-MU2-E1 EPA 8270D-SIM Pyrene 0.077 μg/L B LBMBWH-19-MU2-E1 EPA 9040 pH 8.37 S.U. J HHLBWH-19-MU2-W2 EPA 6010 Dissolved Iron 50 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Aluminum 6.7 μg/L J MSL, TRBWH-19-MU2-W2 EPA 6010 Total Arsenic 12 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Barium 12.2 μg/L J MSL, LDDBWH-19-MU2-W2 EPA 6010 Total Cadmium 1 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Chromium 2 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Copper 3.5 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Iron 50 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Lead 2 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Nickel 3 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Selenium 6.5 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Silver 2 μg/L UJ MSLBWH-19-MU2-W2 EPA 6010 Total Zinc 5 μg/L UJ MSLBWH-19-MU2-W2 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU2-W2 EPA 8270D Benzidine 50 μg/L R LCLBWH-19-MU2-W2 EPA 8270D-SIM 1-Methylnaphthalene 0.0083 μg/L J TRBWH-19-MU2-W2 EPA 8270D-SIM Fluoranthene 0.0098 μg/L J TRBWH-19-MU2-W2 EPA 8270D-SIM Pyrene 0.017 μg/L B LBMBWH-19-MU2-W2 EPA 9040 pH 8.03 S.U. J HHLBWH-19-MU3-C1 EPA 350.1 Ammonia Nitrogen 80.6 mg/kg J TRBWH-19-MU3-C1 EPA 365.4 Phosphorus 235 mg/kg J TRBWH-19-MU3-C1 EPA 8082 Aroclor-1248 42.9 μg/kg J TRBWH-19-MU3-C1 EPA 9045 pH 6.89 S.U. J HHL


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BWH-19-MU3-C1 EPA 9071 Oil and Grease 269 mg/kg J TRBWH-19-MU3-C2 EPA 350.1 Ammonia Nitrogen 83.9 mg/kg J TRBWH-19-MU3-C2 EPA 365.4 Phosphorus 268 mg/kg J TRBWH-19-MU3-C2 EPA 8082 Aroclor-1248 40.4 μg/kg J TRBWH-19-MU3-C2 EPA 8270D-SIM 1-Methylnaphthalene 18.4 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM 2-Methylnaphthalene 36 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Acenaphthene 13.1 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Acenaphthylene 16.4 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Anthracene 42.9 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Benzo(a)anthracene 180 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Benzo(a)pyrene 144 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Benzo(b)fluoranthene 227 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Benzo(g,h,i)perylene 117 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Benzo(k)fluoranthene 62.3 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Chrysene 174 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Dibenzo(a,h)anthracene 32.8 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Fluoranthene 291 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Fluorene 44.3 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Indeno(1,2,3-cd)pyrene 104 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Naphthalene 41.1 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Phenanthrene 186 μg/kg J SGLBWH-19-MU3-C2 EPA 8270D-SIM Pyrene 266 μg/kg J SGLBWH-19-MU3-C2 EPA 9045 pH 7.48 S.U. J HHLBWH-19-MU3-C3 EPA 365.4 Phosphorus 236 mg/kg J TRBWH-19-MU3-C3 EPA 6010 Selenium 0.18 mg/kg B LBMBWH-19-MU3-C3 EPA 8082 Aroclor-1248 46.4 μg/kg J TRBWH-19-MU3-C3 EPA 9045 pH 7.29 S.U. J HHLBWH-19-MU3-C3 EPA 9071 Oil and Grease 559 mg/kg J TRBWH-19-MU3-E1 EPA 350.1 Ammonia Nitrogen 6.5 mg/L J MSLBWH-19-MU3-E1 EPA 410.4 COD 29 mg/L J MSH, TRBWH-19-MU3-E1 EPA 6010 Total Arsenic 6.1 μg/L J TRBWH-19-MU3-E1 EPA 6010 Total Copper 2 μg/L J TRBWH-19-MU3-E1 EPA 6010 Total Nickel 1 μg/L J TRBWH-19-MU3-E1 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU3-E1 EPA 8270D Benzidine 51 μg/L R LCLBWH-19-MU3-E1 EPA 8270D-SIM Benzo(a)pyrene 0.039 μg/L B LBMBWH-19-MU3-E1 EPA 8270D-SIM Benzo(b)fluoranthene 0.033 μg/L B LBMBWH-19-MU3-E1 EPA 8270D-SIM Fluoranthene 0.011 μg/L J TRBWH-19-MU3-E1 EPA 8270D-SIM Pyrene 0.023 μg/L B LBMBWH-19-MU3-E1 EPA 9040 pH 8.03 S.U. J HHLBWH-19-MU3-E1 SM 2540D Total Suspended Solids 2.2 mg/L J LCLBWH-19-MU3-W3 EPA 1664 Oil and Grease 1.8 mg/L J TRBWH-19-MU3-W3 EPA 6010 Total Aluminum 23.5 μg/L J TRBWH-19-MU3-W3 EPA 6010 Total Chromium 1.4 μg/L B LBMBWH-19-MU3-W3 EPA 6010 Total Copper 4.3 μg/L J TRBWH-19-MU3-W3 EPA 6010 Total Iron 16.8 μg/L J TRBWH-19-MU3-W3 EPA 6010 Total Zinc 3 μg/L J TRBWH-19-MU3-W3 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU3-W3 EPA 8270D Benzidine 50 μg/L R LCLBWH-19-MU3-W3 EPA 8270D-SIM Pyrene 0.022 μg/L B LBMBWH-19-MU3-W3 EPA 9040 pH 8.43 S.U. J HHLBWH-19-MU3-W3 SM 2540D Total Suspended Solids 2.0 mg/L UJ LCLBWH-19-MU4-C1 EPA 365.4 Phosphorus 44.4 mg/kg J TR


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BWH-19-MU4-C1 EPA 8270D-SIM 1-Methylnaphthalene 1.40 μg/kg J TRBWH-19-MU4-C1 EPA 8270D-SIM Acenaphthylene 0.827 μg/kg J TRBWH-19-MU4-C1 EPA 9045 pH 9.66 S.U. J HHLBWH-19-MU4-C1 SM 9223B E. coli 2 MPN/g_TS UJ HHLBWH-19-MU4-C2 EPA 365.4 Phosphorus 65.8 mg/kg J TRBWH-19-MU4-C2 EPA 6010 Arsenic 1 mg/kg J TRBWH-19-MU4-C2 EPA 6010 Selenium 0.084 mg/kg B LBMBWH-19-MU4-C2 EPA 6010 Silver 0.061 mg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM 1-Methylnaphthalene 0.950 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM 2-Methylnaphthalene 1.23 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM Acenaphthylene 0.541 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM Anthracene 1.66 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM Benzo(k)fluoranthene 2.46 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM Fluorene 1.36 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM Naphthalene 1.86 μg/kg J TRBWH-19-MU4-C2 EPA 8270D-SIM Phenanthrene 3.31 μg/kg J TRBWH-19-MU4-C2 EPA 9045 pH 8.94 S.U. J HHLBWH-19-MU4-C2 EPA 9071 Oil and Grease 214 mg/kg J TRBWH-19-MU4-C2 SM 9223B E. coli 2,240 MPN/g_TS J HHLBWH-19-MU4-C3 EPA 365.4 Phosphorus 92.7 mg/kg J TRBWH-19-MU4-C3 EPA 6010 Copper 1.5 mg/kg J LDDBWH-19-MU4-C3 EPA 6010 Selenium 0.11 mg/kg B LBMBWH-19-MU4-C3 EPA 6010 Silver 0.063 mg/kg J TRBWH-19-MU4-C3 EPA 8270D-SIM Benzo(k)fluoranthene 0.809 μg/kg J TRBWH-19-MU4-C3 EPA 8270D-SIM Chrysene 1.13 μg/kg J TRBWH-19-MU4-C3 EPA 8270D-SIM Fluoranthene 1.94 μg/kg J TRBWH-19-MU4-C3 EPA 8270D-SIM Naphthalene 0.885 μg/kg J TRBWH-19-MU4-C3 EPA 8270D-SIM Pyrene 2.46 μg/kg J TRBWH-19-MU4-C3 EPA 9045 pH 7.81 S.U. J HHLBWH-19-MU4-C3 EPA 9071 Oil and Grease 169 mg/kg J TRBWH-19-MU4-C3 SM 9223B E. coli 2 MPN/g_TS UJ HHLBWH-19-MU4-E1 EPA 410.4 COD 24 mg/L J TRBWH-19-MU4-E1 EPA 6010 Total Copper 5.6 μg/L J TRBWH-19-MU4-E1 EPA 6010 Total Lead 1.7 μg/L J TRBWH-19-MU4-E1 EPA 6010 Total Selenium 2.7 μg/L J TRBWH-19-MU4-E1 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU4-E1 EPA 8270D Benzidine 50 μg/L R LCLBWH-19-MU4-E1 EPA 8270D Di-n-butylphthalate 1.2 μg/L J TRBWH-19-MU4-E1 EPA 8270D Di-n-octylphthalate 0.67 μg/L J TRBWH-19-MU4-E1 EPA 8270D-SIM Benzo(a)pyrene 0.041 μg/L B LBMBWH-19-MU4-E1 EPA 8270D-SIM Benzo(b)fluoranthene 0.037 μg/L B LBMBWH-19-MU4-E1 EPA 8270D-SIM Chrysene 0.0086 μg/L B LBMBWH-19-MU4-E1 EPA 8270D-SIM Fluoranthene 0.012 μg/L J TRBWH-19-MU4-E1 EPA 8270D-SIM Pyrene 0.015 μg/L B LBMBWH-19-MU4-E1 EPA 9040 pH 8.41 S.U. J HHLBWH-19-MU4-W4 EPA 1664 Oil and Grease 1.9 mg/L J TRBWH-19-MU4-W4 EPA 6010 Total Aluminum 12.6 μg/L J TRBWH-19-MU4-W4 EPA 6010 Total Chromium 0.79 μg/L B LBMBWH-19-MU4-W4 EPA 6010 Total Copper 1.2 μg/L J MSH, TRBWH-19-MU4-W4 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-MU4-W4 EPA 8270D Benzidine 51 μg/L R LCLBWH-19-MU4-W4 EPA 8270D-SIM Pyrene 0.014 μg/L B LBMBWH-19-MU4-W4 EPA 9040 pH 8.42 S.U. J HHLBWH-19-MU4-W4 SM 2540D Total Suspended Solids 2.0 mg/L UJ LCL


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BWH-19-RS1-G1 EPA 365.4 Phosphorus 91.5 mg/kg J TRBWH-19-RS1-G1 EPA 6010 Silver 0.062 mg/kg J TRBWH-19-RS1-G1 EPA 8270D-SIM Benzo(k)fluoranthene 2.48 μg/kg J TRBWH-19-RS1-G1 EPA 8270D-SIM Chrysene 2.42 μg/kg J TRBWH-19-RS1-G1 EPA 8270D-SIM Fluoranthene 3.98 μg/kg J TRBWH-19-RS1-G1 EPA 8270D-SIM Naphthalene 1.02 μg/kg J TRBWH-19-RS1-G1 EPA 8270D-SIM Pyrene 4.14 μg/kg J TRBWH-19-RS1-G1 EPA 9045 pH 8.87 S.U. J HHLBWH-19-RS1-G1 EPA 9071 Oil and Grease 165 mg/kg J TRBWH-19-RS1-G1 SM 9223B E. coli 1,300 MPN/g_TS J HHLBWH-19-RS1-G2 EPA 365.4 Phosphorus 133 mg/kg J TRBWH-19-RS1-G2 EPA 6010 Silver 0.055 mg/kg J TRBWH-19-RS1-G2 EPA 8270D-SIM 1-Methylnaphthalene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM 2-Methylnaphthalene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Acenaphthene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Acenaphthylene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Anthracene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Benzo(a)anthracene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Benzo(a)pyrene 4.91 μg/kg J SGLBWH-19-RS1-G2 EPA 8270D-SIM Benzo(b)fluoranthene 4.59 μg/kg J SGLBWH-19-RS1-G2 EPA 8270D-SIM Benzo(g,h,i)perylene 6.84 μg/kg J SGLBWH-19-RS1-G2 EPA 8270D-SIM Benzo(k)fluoranthene 0.984 μg/kg J SGL, TRBWH-19-RS1-G2 EPA 8270D-SIM Chrysene 1.03 μg/kg J SGL, TRBWH-19-RS1-G2 EPA 8270D-SIM Dibenzo(a,h)anthracene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Fluoranthene 1.73 μg/kg J SGL, TRBWH-19-RS1-G2 EPA 8270D-SIM Fluorene 1.2 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Indeno(1,2,3-cd)pyrene 6.80 μg/kg J SGLBWH-19-RS1-G2 EPA 8270D-SIM Naphthalene 0.898 μg/kg J SGL, TRBWH-19-RS1-G2 EPA 8270D-SIM Phenanthrene 2.4 μg/kg UJ SGLBWH-19-RS1-G2 EPA 8270D-SIM Pyrene 2.36 μg/kg J SGL, TRBWH-19-RS1-G2 EPA 9045 pH 8.56 S.U. J HHLBWH-19-RS1-G2 SM 9223B E. coli 751 MPN/g_TS J HHLBWH-19-RS1-G3 EPA 365.4 Phosphorus 175 mg/kg J TRBWH-19-RS1-G3 EPA 6010 Arsenic 0.95 mg/kg J TRBWH-19-RS1-G3 EPA 6010 Silver 0.052 mg/kg J TRBWH-19-RS1-G3 EPA 8270D-SIM 2-Methylnaphthalene 0.901 μg/kg J TRBWH-19-RS1-G3 EPA 8270D-SIM Benzo(k)fluoranthene 1.21 μg/kg J TRBWH-19-RS1-G3 EPA 8270D-SIM Chrysene 1.66 μg/kg J TRBWH-19-RS1-G3 EPA 8270D-SIM Fluoranthene 3.28 μg/kg J TRBWH-19-RS1-G3 EPA 8270D-SIM Naphthalene 1.14 μg/kg J TRBWH-19-RS1-G3 EPA 8270D-SIM Pyrene 3.38 μg/kg J TRBWH-19-RS1-G3 EPA 9045 pH 8.94 S.U. J HHLBWH-19-RS1-G3 SM 9223B E. coli 2,270 MPN/g_TS J HHLBWH-19-RS1-W1 EPA 6010 Total Aluminum 14.4 μg/L B LBM, EBLBWH-19-RS1-W1 EPA 6010 Total Barium 20.6 μg/L B LBMBWH-19-RS1-W1 EPA 6010 Total Chromium 0.74 μg/L J TRBWH-19-RS1-W1 EPA 8270D 3,3'-Dichlorobenzidine 1 μg/L UJ LCLBWH-19-RS1-W1 EPA 8270D Benzidine 50 μg/L R LCLBWH-19-RS1-W1 EPA 8270D-SIM Pyrene 0.015 μg/L B LBM, EBLBWH-19-RS1-W1 EPA 9040 pH 8.36 S.U. J HHLBWH-19-RS1-W1 SM 2540D Total Suspended Solids 2.0 mg/L UJ LCLBWH-19-RS2-G1 EPA 365.4 Phosphorus 185 mg/kg J TRBWH-19-RS2-G1 EPA 6010 Selenium 0.14 mg/kg B LBMBWH-19-RS2-G1 EPA 7471B Mercury 0.0039 mg/kg J TR


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BWH-19-RS2-G1 EPA 8270D-SIM 1-Methylnaphthalene 1.38 μg/kg J TRBWH-19-RS2-G1 EPA 8270D-SIM 2-Methylnaphthalene 1.83 μg/kg J TRBWH-19-RS2-G1 EPA 8270D-SIM Acenaphthene 2.26 μg/kg J TRBWH-19-RS2-G1 EPA 8270D-SIM Acenaphthylene 0.783 μg/kg J TRBWH-19-RS2-G1 EPA 8270D-SIM Benzo(k)fluoranthene 4.19 μg/kg J TRBWH-19-RS2-G1 EPA 9045 pH 8.47 S.U. J HHLBWH-19-RS2-G1 SM 9223B E. coli 11.2 MPN/g_TS J HHLBWH-19-RS2-G2 EPA 350.1 Ammonia Nitrogen 2.57 mg/kg J TRBWH-19-RS2-G2 EPA 365.4 Phosphorus 176 mg/kg J TRBWH-19-RS2-G2 EPA 7471B Mercury 0.0061 mg/kg J TRBWH-19-RS2-G2 EPA 8270D-SIM 1-Methylnaphthalene 1.88 μg/kg J TRBWH-19-RS2-G2 EPA 8270D-SIM Acenaphthylene 1.02 μg/kg J TRBWH-19-RS2-G2 EPA 9045 pH 8.33 S.U. J HHLBWH-19-RS2-G2 SM 9223B E. coli 64.5 MPN/g_TS J HHLBWH-19-RS2-G3 EPA 365.4 Phosphorus 68.4 mg/kg J TRBWH-19-RS2-G3 EPA 8270D-SIM 1-Methylnaphthalene 0.703 μg/kg J TRBWH-19-RS2-G3 EPA 8270D-SIM 2-Methylnaphthalene 0.877 μg/kg J TRBWH-19-RS2-G3 EPA 8270D-SIM Anthracene 1.29 μg/kg J TRBWH-19-RS2-G3 EPA 8270D-SIM Benzo(k)fluoranthene 2.31 μg/kg J TRBWH-19-RS2-G3 EPA 8270D-SIM Naphthalene 1.03 μg/kg J TRBWH-19-RS2-G3 EPA 8270D-SIM Phenanthrene 1.75 μg/kg J TRBWH-19-RS2-G3 EPA 9045 pH 8.42 S.U. J HHLBWH-19-RS2-G3 SM 9223B E. coli 330 MPN/g_TS J HHLBWH-19-RS2-W2 EPA 1664 Oil and Grease 1.7 mg/L B EBLBWH-19-RS2-W2 EPA 6010 Total Aluminum 11.9 μg/L B LBM, EBLBWH-19-RS2-W2 EPA 6010 Total Barium 21.4 μg/L B LBMBWH-19-RS2-W2 EPA 6010 Total Chromium 1.3 μg/L J TRBWH-19-RS2-W2 EPA 6010 Total Selenium 3.6 μg/L B EBLBWH-19-RS2-W2 EPA 8270D 3,3'-Dichlorobenzidine 1.0 μg/L UJ LCLBWH-19-RS2-W2 EPA 8270D Benzidine 50 μg/L R LCLBWH-19-RS2-W2 EPA 8270D-SIM Pyrene 0.016 μg/L B LBM, EBLBWH-19-RS2-W2 EPA 9040 pH 8.69 S.U. J HHLBWH-19-RS2-W2 SM 2540D Total Suspended Solids 2.0 mg/L UJ LCLFD-1 EPA 365.4 Phosphorus 157 mg/kg J TRFD-1 EPA 410.4 COD 67,200 mg/kg J MSLFD-1 EPA 6010 Aluminum 1,330 mg/kg J FDDFD-1 EPA 6010 Iron 6,760 mg/kg J FDDFD-1 EPA 6010 Nickel 4.8 mg/kg J FDDFD-1 EPA 6010 Selenium 0.33 mg/kg J TRFD-1 EPA 6010 Silver 0.08 mg/kg J TRFD-1 EPA 7471B Mercury 0.032 mg/kg J FDDFD-1 EPA 8082 Aroclor-1248 33.9 μg/kg J TR, FDDFD-1 EPA 8260C Toluene 32 μg/kg J TRFD-1 EPA 9045 pH 8.68 S.U. J HHL

Notes:μg/kg = micrograms per kilogram μg/L = micrograms per litermg/kg = milligrams per kilogram mg/L = milligrams per literMPN/g_TS = most probable number per gram total solids S.U. = standard units


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Qualifier Definitions:B = A target analyte was detected in an associated blank quality control (QC) sample. The detected sample

result is less than five times the concentration detected in the blank, or less than ten times the concentration detected in the blank for common laboratory contaminants.

J = The result is an estimated quantity. The associated numerical value is the approximate concentration ofthe analyte in the sample.

Q = The result was both B and J qualified during validation.R = The data are unusable. The sample results are rejected due to serious deficiencies in meeting quality

control criteria. The anlayte may or may not be present in the sample.UJ = The analyte was analyzed for, but was not detected. The reported quantitation limit is approximate and

may be inaccurate or imprecise.

Reason Codes:EBL = A target analyte was detected in the associated equipment blank and the concentration detected in the

sample is less than five times the concentration detected in the blank.FDD = Imprecision between primary and field duplicate results.HHL = Hold time was exceeded.LBL = A target analyte was detected in the associated laboratory blank and the concentration detected in the

sample is less than five times the concentration detected in the blank.LCL = Low laboratory control sample recovery. Result may be biased low.LDD = Imprecision between laboratory duplicate results. MSH = High matrix spike (MS) recovery. Result may be biased high.MSL = Low MS recovery. Result may be biased low.SGL = Low surrogate recovery. Result may be biased low.TR = The detected concentration is less than the limit of quantification.


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Documents

February 28, 2020 2020-112-64-MTM-A PUBLIC NOTICE · 2020-02-21 · Inc. (Wood) have completed the Final-Draft Sediment and Water Sampling and Analysis Report for Burns Waterway Harbor