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EraW E S T COAST T e C H N l C A L S 6 R V 1 C G I N C . I N D U S T R I A L C A T E G O R Yf• S A M P L E I D 3 0 F - 1
L A B I D 22049V1D A T E I N J E C T E D 8 / 2 8 / 8 1S T D I D B F B 5 2 V O A 1 7 6C O N C . F A C T O R — — — — -
V o l a u l e s2 V i q j . i j I M i i ' ' " " " " ' " " "3V a c r y l o n i t r i l e4V benzene6V carbon t e t r a c h l o r i d e7V c h l o r o b e n z e n e10V l^rfr^iCiyrt^-iiftoiiiiAra11 V 1,1 , i - t r i c h l o r o e t h a n e13V 1» 1 - d i c h l o r o e t h a n e14V 1 , 1 , 2 - t r i c h l o r o e t h a n e15V 1. 1 , 2 , 2 - t e t r a c h l o r o e t h a n e16V c h l o r o e t h a n e
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. N O G O O D F I TN O G O O D F I TG E N E R A L F I TN O G O O D F I TN O G O O D F I TN O G O O D F I TN O G O O D F I TN O ' - . G O O D F I T
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D O S 3 4 9 6 - 0 3 3 3
BJyS> wesT COAST TECHNICAL SERVICE INC. iwo 'u s fRfl f f cATesoRY * ~ " 'S A M P L E I D 3 0 F - 5L A B I D _.... . 2 2 0 4 9 A 8D A T E E X T R A C T E D 8 / 3 0 / 8 ]D A T E I N J E C T E D 9 / _ 2 / 8 _ 1S T D I D S E N S 1 8 1 P H E N 3 5 8C O N C F A C T O R 1000
A c i d C o m p o u n d s21 A 2, L , S - t r i c h l o r o p h e n o l22A p-chloro-m-cresol
' 24 A 2-c h ". o r o p j i e nol31 A 2 , 4 - d i c h l o r o p h e n o l34A 2 , 4 — d i m e t h y l p h e n o l5 7 A 2 - n t t r o p h e n o l58A 4 - m i r o p h e n o l
; 59A 2 ,^-c in i t ropheno l60A 4 ,6~d in i t ro-o- cr e s o l6 4 A p e n t a c h l o r o p h e n o l65A p h e n o l
B a s e / N e u t r a l C o m p o u n d s
I B a c e n a o h t h e n eS B b e n z i d i n e88 1 ,2 ,4- t r i ch l c rob enzene9B h e x a c h l o r o b e n z e n e1 2 B h e x a c h l o r o e t h a n e18B b i s ( 2 - e h l o r o e t h y l ) e t h e r20B 2 - c h l o r o n a p t h a l e n e25B 1 , 2 - d i c h l o r o b e n z e n e26B 1 ,3-d i ch lorobenzene27B l , j i - d i c h l o r o b e n z e n e2 8 B 3 , 3 ' - d i c h l o r o b e n z i d i n e35B 2 t i - d i n i t r o t o l u e n e36B 2, 6 - d i n i t r c t o l u e n e37B 1 , 2 - d i p h e n y l h y d r a z i n e
(as azobenzene)39B f l u o r a n t h e n e40B i - c h l o r o p h e n y l p h e n y l
u g / 1N D„.,.. m
. N DN D
. .ND_ . _ N D. ._ ND
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S A M P L E I D 3 Q F - 5L A B I D 22049B8D A T E E X T R A C T E D 8 / 2 9 / 8 1D A T E I N J E C T E D 9 / 1 / 8 1S T D I D _ B E M Z 4 0 3 B N S T D 4 2 0C O W C F A C T O R 1000
B a s e / N e u t r a L C o m p o u n d s u4 1 B i -bromot>henyl p h e n y l e t h e r426 b i s ( 2 - c h l o r o i s o p r o p y l ) e ther^3B bi s ( 2 - c h l o r o e t h o x y ) m e t h a n e5 2 B h e x a c h l o r o b u t a d i e n e53B h e x a c h l o r o c y c l o p e n t a d i e n e54B i s o p h o r o n e5 5 B n a p h t h a l e n e56B ni trobenzene61 B N - n i t r o s o d i m e t h y l a m i n e6 2 B W - n i t r o s o d i p h e n y l a m i n e63B N - n i t r o s o d i - n - p ropy la mine66 B ^J*P»O u i . i ^ y ' ^ ^ j A i / ' ^ i ^ ^ / ^ i i . ^ ^ i j i6 7 B b u t y l b e n z y l p h t h a l a t e68B di-n-butyl p h t h a l a t e6 9 B d i - n - o c t y l p h t h a l a t e7 0 B d i e t h y l p h t h a l a t e7 1 B d i m e t h y l p h t h a l a t e7 2 B b e n z o ( a ) a n t h r a c e n e7 3 B b e n z o ( a ) p y r e n e74B 3 t 4 - b e n z o f l u o r a n t h e n e7 5 B b e n z o ( k ) f l u o r a n t h e n e76B c h r y s e n e77B a c e n a p h t h y l e n e78B a n t h r a c e n e7 9 B b e n z o ( g h i ) p e r y l c n eS O B f l u o r e n e8 1 B p h e n a n t h r e n e8 2 B d i b e n z o ( a , h ) a n t h r a c e n e83B i n d e n o ( l , 2 ( 3 - c d ) p y r e n e84B p y r e n e129B 2 , 3 . 7 , 8 - t e t r a c h l o r o d i b e n z o -p-diox in
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S A M P L E I D 3 0 F - 5L A B I D 2 2 0 4 9 V 5D A T E I N J E C T E D 8 / 2 8 / 3 1S T D I D B F B 5 2 V O A 1 7 6C O N C , F A C T O R
V o l a t i l e s2V a c r o l e i n3V a c r y l o n i t r i l e4V benzene6V carbon t e t r a c h l o r i d e7V c h l o r o b e n z e n e10V i l k ^ i U l i l l t l b h l ^ U i i r t M i L11V 1 , 1, l « - t r i c h l o r o e t h a n e13V 1 , 1 - d i c h l o r o e t h a n e14V 1 ,1 , 2 - t r i c h l o r o e t h a n e15V 1 , 1 ,2, 2 - t e t r a c h l o r o e t h a n e16V c h l o r o e t h a n emmxnUMmmtmmzmttMXnn19V 2 - c h l o r o e t h y l v i n y l e t h e r23V ^f f-S^i^&s fa,29V 1 , 1 - d i c h l o r o e t h y l e n e30V 1 , 2 - t r a n s - d i c h l o r o e t h y l e n e32V 1 , 2 - d i c h l o r o p r o p a n e33V 1 , 3 - d i c h l o r o p r o p y l e n e38V e t h v l b e n z e n e
N DN DN DN DN D
«*$*N DN DN DN DN D
X X X X XN D
tt&N D*N DN D
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S A M P L E I D 3 0 F - 5L A B I D T R A C E #4429D A T E E X T R A C T E D 8 / 2 8 / 8 1D A T E I N J E C T E D 8 / 3 1 / 8 1S T D I D T R A C E #4427C O N C . F A C T O R 5 0
P e s t i c i d e s89P a l d r i n90P d i e l d r i n91P c h l o r d a n e9 2 P 4 , 4 ' - D D T9 3 P 4 , 4 ' - D D E9 4 P 4 , 4 ' - D D D9 5 P a l p h a - e n d o s u l f a n96P be ta-en d o s u l f an9 7 P e n d o s u l f a n s u l f a t e98P e n d r i n9 9 P e n d r i n a l d e h y d e1 0 0 F h e p t a c h l o r1 0 1 P h e p t a c h l o r e p o x i d e1 0 2 P a l p h a - B H C103P b e t a - B H C1 0 4 P g a m m a - B H CI 0 5 P d e l t a - B H C106P P C B - 1 2 4 2107P P C B - 1 2 5 4
& 4430
H f i / LN DN DN DN DN D L HN D f AND 00N D °ON DN DN DN DN DN DN DN DN DN DN D
44V j n r t i m i i « . , M . . « . h ] n * r f T - - «£*> 108P P C B - 1 2 2 1 ND45V m e t h y l c h l o r i d e46V m e t h y l b r o m i d e47V b r o m o f o r m48V d i c h l o r o b r o m o m e t h a n e49V t r i c h l o r o f l u o r o m e t h a n e50V d i c h l o r o d i f l u o r o m e t h a n e51V c h l o r o d i b r o m o m e t h a n e85V t e t r a c h l o r o e t h y l e n e86V t o l u e n e87V t r i c h l o r o e t h y l e n e
N D_M
_ . N D-M. N D
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109P P C B - 1 2 3 2H O P P C B - 1 2 4 8U 1 P P C B - 1 2 6 0112P PCB-10161 1 3 P t o x a p h e n e
* = L e s s t h a n 10 ug/1( p e s t i c i d e s l e s s than 5 u g / 1 )
N D * N o t d e t e c t e d** « Not c o n f i r m e d by GCMS
- J U LUD_N D
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88V v i n y l c h l o r i d e _ N D
W 6 S T COAST T E C H N I C A L S 6 R V I C 6 I N CO R G A N I C S A N A L Y S I S D A T A S H E E T - P a g e 3QC Repor t No; S a m p l e N u m b e r
3 0 F - 5A . S U R R O G A T E S P I K E R E S U L T S —. . . . .—
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C O M P O U N DBenzene - d6l -Chloro-2-BromopropamT o l u e n e - d82 - F l u o r o p h e n o lP h e n o l - d5N i t r o b e n z e n e - d52 - F l u o r o b i p h e n v lN a p h t h a l e n e - 0 8
F r a c t i o nV G AV G AV G AA C I DA C I DB / NB/NB/N
Cone. ( u q / 1 )... M .__
5691
10898
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( S u r r o g a t e s o n l y )S p i k eA d d e d i u j / T J L. ___5.Q_. _
5050
L T O O103101100
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<y«Recovery_ _ U 0 _ _ _
96112
9i105
97120
N Ai — •*— ^ — "---I'-B . T E N T A T I V E L Y I D E N T I F I E D C O M P O U N D S
1.2.3.4.5.6 ,7.8.9.10.11.12.13,14.15.16.17.18.19.20.
CAS # C O M P O U N D N A M E
C H L O R O P R O P E N ET E T R A H Y D R O F U R A NT E T R A H Y O R O - 3 - M E T H Y L -
2 H - P Y R A NH Y D R O C A R B O NU N K N O W NU N K N O W NU N K N O W NU . - ; . : M O W NU N K N O W NU N K N O W NU N K N O W NU N K N O W N
F R A C T I O N
V G A # 8 4VOA 105
VOA #235A C I D # 6 0A C I D # 8 1A C I D #102A C I D #139A C I D #153A C I D #277B / N #198B / N #370B/N #444
% M a x i m u m S c o r e A t t a i n e dM a s s M a t c h i n g R o u t i n e : F I T...... ... _..... . (specify)
G E N E R A L F I T965
941G E N E R A L F I TN O G O O D F I TN O G O O D F I TN O G O O D F I TN O GOOD F I TN O G O O D F I TN O G O O D F I TN O G O O D F I TN O G O O D F I T
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x- 1I N O R G A N I C S A N A L Y S I S D A T A S H E E T D ™ ' ^ " Oivfe,<^
343 - 3o £"L A B O R A T O R Y N A M EL A B S A M P t £ I D N O *
1. A l u m i n u m2- Chromium3, Barium
Versar Inc. SAMPL5 NO. 3O £ S M^?3i QC REPORT NO.
TASK 1 - ( E l e i t i e T t s to be ident i f i ed and measured)4 U g / 1 U g / 1<£<?£. 10. N i c k e l ^ O-
<10, 11. Maji^aneae 2^7A 12- Zir.C <* / . ,r\
4. ServLnum <"£. 13. Boron 3O* to5. Cadmiumo* C c f a s i t7. CcooerS. I r a n
<"£ - 14. Vanadium 'C IL). ^<lQ, 1^. Calcium 351^300. o<5^), 16. M a z n e s i u m 2,900.
90. 17. S o d i u m IQIOO.9. Laad ^ ^0*
TASK 2 (Element!, to b« i d e n t i f i e d and measured)
u g / 1 f ' u g / 11. A r s « f i i c ^ /O' 5* Mcrcurv /2- Antimony3- Sel en ium
<2.O. 5. Tin ^^C).< / 0 - 7. S i l v e r <20 .
4. T h a l l i u m <7£>-:':
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3. S u l f i d e
TASK 3 (Elements to be i d en t i f i ed and measured)
ms/1 4. Cvanide m « / Im ? / l 5* pH U n i t sms/1 fi* TOC • m e / 1
C O M M E N T S t a )b)c)d )e)£)
with a detecticn limit of £&O. .with a d f i ta c t i cn liitiit of -with a detection l i jni t ofanalysed on a sarrole aliquot preserved with HC1 fron F/pH sarrple bottleaverage of two repHcata detaoiinatior^insuf f i c i ent sample aliquot i
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• ."" 41©Jig} west COAST TemwiCAu SGRVHS A M P L E I D 3 0 F - 6f * ft f tSL A o l u ? ? H d Q A < 3D A T E E X T R A C T E D f t / ^ f l / A lD A T E I N J E C T E D q / ? / f US T D I D _ _ _ _ _ S E N S l f l l P H P N . 1 5 f l _C O N C F A C T O R 1000
A c i d C o m p o u n d s21 A 2 , 4 , 6 - t r i c h l o r o p h e n o l22A p-chloro-m-cre so l24A 2 - c h I o r o p h e n o l31 A 2 , 4 - d i c h l o r o p h e n o l34 A 2 , 4 - d i m e t h y l p h e n o l57A 2-n i t r opheno l58A 4 - n i t r o p h e n c l59 A 2 , 4 - d i n i t r o p h e n o l60A 4 ,6-d in i t ro-o- cr e s o l64 A p e n t a c h l o r o p h e n o l65A p h e n o l
B a s e / N e u t r a l C o m p o u n d s
18 a c e n a p h t h e n eS B b e n z i d i n eSB 1 , 2 , 4 - t r i c h l o r o b e n z e n e9B h exa ch l o rob enz ene1 2 B h e x a c h l o r o e t h a n e
»aN DN DN DN DN DN HN DN nN Df i n
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1 8 B U W - f r ' * " ' 1 " " 1 i l i r i n n l i r T — — — — T T *2 0 B 2 - c h l o r o n a p t h a l e n e N D25B 1 f 2 - d i c h l o r o b e n z e n e26B 1 ,3-dichlorobenzene27B 1 , 4 - d i c h l o r o b e n z e n e
N D_.- . ND
N D28B 3 » 3 ' - d i c h l o r o b e n z i d i n e «n35B 2 , 4 - d i n i t r o t o l u e n e36B 2 , 6 - d i n i t r o t o l u e n e
. _ ND.__ . ND
37B 1 , 2 - d i p h e n y l h y d r a z i n e( a s a z o b e n z e n e ) N H
39B f l u o r a n t h e n e40B 4 - c h l o r o p h e n y l p h e n y l
NOe t h e r N D
B a s e / N e u t r a l C o m p o u n d s41B42B43B52B53B54B55B56B61B62 B63B66B67B68B69B70 B71B72873B74B75B76 B77B78B79880881 B82B83B84B
4-bromophenyl p h e n y l e therb i s ( 2 - c h l o r o i s o p r o p y l ) e t h e rb i s ( 2 - c h l o r o e t h o x y ) m e t h a n eh e x a c h l o r o b u t a d i e n eh e x a c h l o r o c y c l o p e n t a d i e n ei s ophoronen a p h t h a l e n en i t r o b e n z e n eN - n i t r o s o d i m e t h y l a m i n eN - n i t r o s o d i p h e n y l a m i n eN - n i t r o s o d i - n - p r o p v l a m i n eb i s ( 2 - e t h y l h e x y l ) p h t h a i a t eb u t y l b enzyl p h t h a i a t ed i - n - b u t y l p h t h a i a t ed i - n - o c t y l p h t h a l r . t ed i e t h y l p h t h a i a t ed i m e t h y l p h t h a i a t eb e n z o ( a ) a n t h r a c e n eb e n z o ( a ) p y r e n e3 , 4 - b e n z o f l u o r a n t h e n eb e n z o ( k ) f l u o r a n t h e n ec h r y s e n ea c e n a p h t h y l e n ea n t h r a c e n e •b e n z o ( g h i ) p e r y l e n ef l u o r e n ep h e n a n t h r e n ed i b e n 2 o ( a , h ) a n t h r a c e n ei n d e n o ( l , 2 , 3 - c d ) p y r e n ep y r e n e
gU^nn.
N DN DN DN DN DN DN DN ON ON ON D*N O***
N DN ON DN ON ON O
N PN OM f lN HmmN O
LP.
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1298 2 , 3 , 7 * 8 - t e t r a c h l o r o d i b e n z o -p - d i o x i nr- . _, -^-. . ,^-_-———-—.._,. . _ _ _ _ _ _ _._. . . . . ND_.
W 6 S T C O A S T T e m N I C A iS A M P L E I D 3 0 F - 6L A B I D 22049V8D A T E I N J E C T E D 8 / 2 8 / 8 1
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