Evaporation - mail2.gaiascience.com.mymail2.gaiascience.com.my/Images/heidolph/catalogue/Heidolph Rotary... · • Only the Hei-VAP heating bath reaches a temperature of 210 °C •

EvaporationIntelligent

Premium Safety Standards Superior Ease of Use Reduced Cost of Ownership

HeiVAP_GB_0612_internet.indd 1 06.12.11 09:50

... stands for an overheat protection design that prevents water baths running dry, provides a detachable panel for superior ease of use outside a fume hood, and offers a proven vacuum seal and vapour tube system guaranteed for years of operation!

• Two independent safety circuits avoid an overheat situation of your heating bath: If bath temperature overshoots by 5 °C and if your water bath runs dry, heating will be switched off automatically

• To avoid an overtemperature situation and potential thermal damage to your sample, you can individually pre-program a maximum temperature on the Precision model, at which the bath shuts off

• In case of a power cut, all motor lift models will remove the fl ask from the heating bath preventing safety hazards and potential thermal damage to your sample

• To protect you from splashes and scalding, the Hei-VAP heating bath features a pour spout to remove bath fl uid safely

• Heating bath is constructed with adouble wall for your protection against burns and scalding

• The guard hood covers the entire bath completely even if the heating bath is adjusted horizontally to its most extreme limit

• A metal support between the heating bath and the base unit prevents bath instability

• To protect your heating bath against short-circuits and systematic corrosion, the electrical cable coupling complies with the high protection class IP 67

• For your protection, the operating panel is located near the base so as to keep your hands out of the dangerous zone of rotating fl asks, steam and splashing bath fl uids

• All heating baths feature non-slip handles with safety grip to protect you from scalding bath liquids and allow for easy installation/removal of the bath

• A separate on/off switch for heating prevents unintentional heat-up. The button is illuminated for visual control

• In case of an overshoot of any parameter setting, all models will show a warning on the operating panel

• Glassware assemblies are optionally available with transparent plastic safety coating ensuring ultimate protection while allowing visual control at all times

• Only the Hei-VAP heating bath reaches a temperature of 210 °C

• The heating bath can be adjusted horizontally up to 200 mm

• The universal heating bath can even accommodate 5-liter fl asks

• To prevent short circuits and corrosion, the electrical cable coupling complies with the high protection class IP 67

• Non-slip handles for safe transportation eliminate the risk of scalding

• Pour spout to remove bath fl uid safely

YOUR ADVANTAGES

Intelligent Evaporation...

Safety heating bathDo you demand the highest safety standards, perfectly engineered ease of use and reduced cost of ownership?

Premium Safety Standards

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• The detachable operating panel can be attached via Velcro or with a special suspension at eye level for your convenience outside of closed fume hoods

• The evaporating fl ask clamp cannot be lost due to a connection to the vapor tube coupling ring

• A fl ask ejector feature of the vapor tube coupling ring allows you to remove sticking evaporating fl asks from the vapor tube just in seconds in a safe manner

• The universal heating bath can be adjusted horizontally up to 200 mm and offers effi cient space to accommodate even 5-liter fl asks

• For your convenience, the height of 160 mm and the angle of the evaporating fl ask can be adjusted easily from 20° to 80°

• Reduce your process times depending on your model and periphery up to 30 %

• The chemical-resistant vacuum seal reduces your spare parts budget up to 75 % with prolonged operational lifespan

• Savings at the same high level are possible due to the long service-life vapor tube

• Increase your range of applications by using 5-liter fl asks in the universal bath at no added costs

• The fl ange on the condenser side of the drive is made of PPS (Polyphenylene sulfi de), a robust industrial-designed resin with superior chemical resistance which provides more chemical resistance than stainless steel or welded aluminum.

This reduces corrosion to a minimum which results in additional savings on maintenance and replacement components associated with corrosion effects of moisture condensation from condenser coupled with common corrosive reagents used in daily laboratory activities

• Only Hei-VAP heating baths reach a temperature of 210 °C which is 30 °C higher than other evaporators on the market and allow for a broader range of applications which previously could not be performed on any rotary evaporator

(for example bitumen distillation). Thus, increasing the range of applications eliminates the need for investments in other equipment

• Reduce your maintenance costs. The sealed housing protects your rotary evaporator from aggressive fumes, liquids and vapors to prevent internal corrosion. This results in an increased lifespan of 10 years on average at a reduced maintenance and repair cost

Superior Ease of Use

Reduced Cost of Ownership


5


The average operational lifespan of 10 years is backed by a 3 year warranty and makes your purchase a truly worthwhile investment.

Non sticking vapor tube eliminates broken glass and reduces spare parts cost signifi cantly

Safety bath will power off if temperature overshoots by 5 °C or runs dry

A metal support between the heating bath and the base unit prevents bath instability

A separate ON/OFF switch for heating prevents unintentional heat-up – the button is illuminated for visual control

210 °C heating bath with safety handles and pour spout accommodates 5-liter fl asks

Bath power cable coupling complies with protection class IP 67 to prevent corrosion and short circuits

Detachable panel allows for thehighest operational safetyfrom outside closed fumehoods

The fl ange made of chemical-resistantPPS reduces corrosion, maintenance and spare parts cost to a minimum

Chemical-resistant vacuum seal allows for years of operation and reduces spare parts budget up to 75 %

EvaporationIntelligent

Operating Panel

Are safety, convenience and fl exibility top priorities for you? The detachable operating panel offers all in one.

Vapor Tube

Are safety, convenience, cost savings and time top priorities for you?The vapor tube of the Hei-VAP series offers all in one.

• The vapor tube can easily be removed from the drive and is designed for years of service life.

• Years of performance life reduce your spare parts budget up to 75 %

• Highest safety: The Hei-VAP vapor tube does not get stuck in the drive, thus eliminating the risk of broken glass

• Immediate removal of the vapor tube from the drive facilitates your work

• Changing all parameters outside the closed fume hood guarantees the highest safety level

• Standard for all models is a panel with 1 m cable connection. Thus data security is guaranteed at any time

• Hei-GUIDE, the button with a turn and push function navigates you easily through the menu

• Immediate access to the panel ensures ultimate control of the process while increasing your ease of use

YOUR ADVANTAGES

YOUR ADVANTAGES


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• The convenience of large dial controls for adjustment of rotation speed and bath temperature

• For limited budgets, we recommend the optional Manual Vacuum Controller

• Hei-VAP Value models have no digital display

Affordable model with hand lift for all standard applicationsIncludes premium safety standards and features for superior ease of use and reduced cost of ownership, plus:

For your routine distillation applications and reproducible resultsIncludes premium safety standards and features for superior ease of use and reduced cost of ownership, plus:

• Available in hand lift or motor lift configurations

• Experience the advantages of our large digital 3.5“ LCDdisplay which indicates rotation speed, heating bath andvapor temperature

• We recommend the optional Manual Vacuum Controller

• Experience the advantages of the automatic process timer whichturns off your evaporator at a pre-programmed time and removesevaporating flasks from bath on motor lift models

• Upgrade your Hei-VAP Advantage to a Hei-VAP Precision:

Upgrade-KIT Advantage Precision-HLP/N 569-30009-00Upgrade-KIT Advantage Precision-MLP/N 569-40009-00

Hei-VAP Value HL/G3P/N 560-01300-00

Hei-VAP Advantage ML/G3P/N 562-01300-00

Hei-VAP Value Hei-VAP Advantage

Large digital LCD display which allowsyou to monitor all parameterseven from a distance

The evaporating flask clampcannot be lost due to a connectionto the vapor tube coupling ring

Adjust the required angleof the evaporating flask individually

Limit the height of yourevaporating flask just in seconds

Convenient motor lift adjusts heightby the press of a button

For your protection the detachableoperating panel is located belowthe bath and thus outside thedangerous zone

Hei-GUIDE control knob to navigate themenu and confirm parameters

Easy operating hand lift forfast height adjustment

Hei-VAP Value

Hei-VAP Value

Hei-VAP Value

Hei-VAP Value

standard coated

560-01100-00

560-01300-00

560-01500-00

560-01600-00

Glassware

Models

G1 Diagonal

G3 Vertical

G5 Dry Ice Condenser

G6 Vertical for Reflux

560-01110-00

560-01310-00

560-01510-00

560-01610-00

Hei-VAP Advantage

Hei-VAP Advantage

Hei-VAP Advantage

Hei-VAP Advantage

standard coated

561-01100-00

561-01300-00

561-01500-00

561-01600-00

Glassware

Models

G1 Diagonal

G3 Vertical



561-01110-00

561-01310-00

561-01510-00

561-01610-00

562-01100-00

562-01300-00

562-01500-00

562-01600-00

562-01110-00

562-01310-00

562-01510-00

562-01610-00

standard coated

Hand lift (HL) Motor lift (ML)

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• Available in hand lift or motor lift configurations

• Experience the advantages of our large 4.3” color graphicdisplay which features all parameters, integrated vacuumcontroller and includes programs for automated distillations

• Make your life easier by utilizing the integrated software supportwhich leads you through the capabilities of the evaporator

• For data management Hei-VAP Precision models feature aUSB interface

• Save time by configuring the unit - all connected componentsand periphery devices will be recognized by the evaporator,which eliminates the need to configure the unit manually

• Now you can manage even the most demanding applicationseasily and prevent foaming, excessive bubbling or bumping

• Save time with your individualized pre-programmed parametersettings for your 30 most common applications used on adaily basis by saving them as a ramp in ”Favorites” section.Each ramp offers 20 separate steps for demanding applications

• Apply an individual name to those ramps to avoid a mix-up

• Experience the advantages of the automatic process timerwhich turns off your evaporator at a pre-programmed timeby raising the flask on motor lift models and releasing vacuum

• Control your process individually by pre-programmingvacuum gradients

• Hei-VAP Precision models feature a built-in vacuum controlleras a standard

Even from a distance you willbe able to monitor thenumbers on the display easily

For increased safety allbath temperatureadjustments can belimited

AUTOaccurate

Supports very precise automatic pressure control for solventseparations. This program works similar to AUTOeasy but inaddition is able to identify multiple boiling points automaticallyby reducing vacuum accordingly. Also the AUTOaccurate programdelivers the finest and most precise vacuum control. To takeadvantage of this program, the optional AUTOaccurate-sensor isrequired. Also, this program cannot be used on Heidolph G1 andG5 glassware assemblies. Leading parameter of this program isthe vapor temperature (AUTOaccurate is a combination of theprevious programs Tauto and Pauto)

Most demanding applications and the finest integrated vacuum control capabilitiesIncludes premium safety standards and features for superior ease of use and reduced cost of ownership, plus:

Hei-VAP Precision ML/G3P/N 564-01300-00

Programs facilitate process control

Reduce your process times significantly by using these three programs for automated distillation

Hei-VAP Precision

Large color graphicdisplay for all parametersand automated programs

Save your commonapplications underan individual name

SETpressure

Program for solvent separations. This program holds a pre-setvacuum constant. During the evacuation you have the fullflexibility to choose any other level of vacuum by the press ofa button

AUTOeasy

Supports the automatic pressure control for solvent separations.The pressure level for the first boiling point is foundautomatically. This program can be used with all Heidolphglassware assemblies and does not require any accessories

Reduce your process times via automated distillation programs

Program: SETpressure

Control parameter: manually set pressure1000 mbar

Manually set vacuum

Program: AUTOeasy

Control parameter: Pressure1000 mbar

Finds boiling point automatically and holds vacuum constant

Stop

Program: AUTOaccurate

Control parameter: Vapor temperature1000 mbar

Finds multiple boiling points automatically

Final vacuum individually adjustable

Hei-VAP Precision

Hei-VAP Precision

Hei-VAP Precision

Hei-VAP Precision

standard coated

563-01100-00

563-01300-00

563-01500-00

563-01600-00

Glassware

Models

G1 Diagonal

G3 Vertical



563-01110-00

563-01310-00

563-01510-00

563-01610-00

564-01100-00

564-01300-00

564-01500-00

564-01600-00

564-01110-00

564-01310-00

564-01510-00

564-01610-00

standard coated

Hand lift (HL) Motor lift (ML)

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The Modular Concept consists of rotary evaporator, vacuum pump, controller and chiller Most precise vacuum due to fully automatic speed control

Reduce your process times up to 30 %The Modular Concept

30 % reduced process times

Cost reduction

Superior ease of use

The figures prove significant time saving when using a speed-controlled system with boil pressure follow-up in comparison witha conventional ”open/close” valve control system. Usedconfiguration:Hei-VAP Precision with program AUTOaccurate

Time to evaporate400 grams of ethanol

0

20

40

60

80

100

120

Min

utes

valve-controlled vacuumwithout

boil pressure follow-up

speed-controlledpressure regulation withboil pressure follow-up

recovery rate

=

pres

sure

Time

Valve regulated

= intermittant evaporation

= continuous evaporation

Fully automatic control with speed adjustment

Time

pres

sure

=

recovery rate

• The integrated vacuum controller exactlycontrols pressure by the specific boilingpoint no hysteresis

• The evaporating process is increasedsignificantly

• The solvent recovery rate is close to 100 %

• High efficiency as the time saving will cutdown process times, and hence cost

• Reduced process times lead to sustainableeconomic benefits and measurableincreased efficiency

Your advantages

• All components are technically designedto function perfectly together

• Self-contained system eliminates the needfor water, dry ice and vacuum source

• For higher requirements you can upgradeyour Hei-VAP model at any time

• Heidolph offers you a complete systemavailable from one manufacturer

• Use your lab space efficiently:The Modular Concept has a footprint of470 x 580 mm only

Your advantages

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• Glassware set includes one 1,000-ml evaporating flask and one1,000-ml receiving flask

• All glassware sets are also available with transparent plasticcoating (Surlyn®-coated) for added safety, except for glasswareset G5 which is Halar-coated

• Evaporating flasks and vapor tubes which come with a standardNS 29/32 joint size are also available with NS 24/29 ground joints(available upon request)

• Also available upon request: glassware sets for Soxhletextraction and descending condenser system

• All glassware sets feature GL 10 thread; the inlettube can be connected with a threaded fitting

• Glassware G3 and G6 allow for the automated distillationprogram AUTOaccurate on Hei-VAP Precision models

Glassware set G1

• Diagonal condenser for all standarddistillations; the option with themost affordable price

Glassware set G3

• Vertical condenser for all standarddistillations; the option withthe smallest space requirement

Glassware set G5

• Dry Ice Condenser for low-boilingsolvents

Glassware set G6

• Vertical condenser; centerpiecewith valve for reflux distillation

Glassware - Hei-VAP Series

Guard hoodStrong and super-transparent guard hoodto protect you from implosions. Excellentvisibility to flask. Provides easy andimmediate access to flask and bathP/N 569-00010-00

Guard shieldStrong and super-transparent guard shield foryour protection while changing flasks.Attached at the edge of the bathP/N 569-00020-00

Vapor temperature sensorFor Hei-VAP Advantageand Hei-VAP Precision modelsP/N 569-00030-00

AUTOaccurate-sensorFor Hei-VAP Precision models, only incombination with glassware set G3 and G6P/N 569-00040-00

Heating bath liquid (5 l)Heating bath liquid for temperatures upto 240 °C, mixes with waterP/N 515-31000-00

Tube set6.25 meter vacuum tubing and6.25 meter water tubingP/N 591-35000-00

Accessories - Hei-VAP Series

Aqua-StopSafety mechanism - in the event of a water leakage the valve closes and thus avoids floodingin your laboratory (can only be used in combination with the chiller model Rotacool)P/N 569-00500-00

Spare PTFE vacuum sealP/N 23-30-01-01-30

Spare clamping sleeveP/N 23-30-01-05-31

Spare vapor tube NS 29/32P/N 514-00000-01

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SwitchboxP/N 569-00400-00

Manual Vacuum ControllerP/N 591-26000-00 Vacuum valve

P/N 569-00060-00Woulff BottleP/N 569-00070-00

Vacuum Accessories - Hei-VAP SeriesAccessories - Hei-VAP Series

Connect up to 3 rotary evaporators to one pumpand control vacuum individually

• Pump switches off automatically at required vacuum

• Reduces energy consumption of pump

• Increases performance life of the pump due to acomplete switch-off if vacuum is reached

• Vacuum valve and non-return valve are required forevery evaporator if you work with different pressuresat the same time

• Delivery includes 3 non-return valves

• Weight: 0.6 kg

• Dimensions: 80 x 160 x 45 (l x w x h / mm)

• Designed for all Hei-VAP models with valve-regulatedvacuum pumps

Switchbox

Required to control vacuum for Hei-VAP models with valveregulated pumps

• External attachment design for easy cleaning

• Can be combined with the Woulff Bottle to one unit

• Not required if you utilize a manual vacuum controller

Woulff Bottle (optional)

• Additional recovery of solvent to protect vacuum valveand vacuum pump

• Direct connection to the vacuum valve

• Features connection to vacuum controller

• Volume of 250 ml

Vacuum valveManual vacuum controllerFor Hei-VAP Value and Hei-VAP Advantage models

• Control your house vacuum or any other vacuum source

• Pressure range from 0 to 1,020 mbar

• Scaling on display in steps of 50 mbar

• Adapter for the tube with 8 mm inner diameter

• Support rod included

• Attaches safely to evaporator


• A vacuum valve is not required

Evaporating flask* 50 ml

Evaporating flask 100 ml



Evaporating flask 1,000 ml




NS 29/32 NS 24/29

514-70000-00

514-71000-00

514-72000-00

514-73000-00

514-74000-00

514-75000-00

514-76300-00

514-78000-00

514-70000-01

514-71000-01

514-72000-01

514-73000-01

514-74000-01

514-75000-01

514-76300-01

514-78000-03

* Evaporating flask NS 14.5 incl. adapter (NS 29 or NS 24)

Evaporating flasks

Receiving flask - NS 35/20 100 ml



Receiving flask - NS 35/20 1,000 ml



standard coated

514-81000-00

514-82000-00

514-83000-00

514-84000-00

514-85000-00

514-87000-00

Receiving flasks

514-81000-02

514-82000-02

514-83000-02

514-84000-02

514-85000-02

514-87000-02

Powder flask 500 ml

Powder flask 1,000 ml

Powder flask 2,000 ml

NS 29/32 NS 24/29

514-73200-00

514-74200-00

514-75300-00

514-73200-01

514-74200-01

514-75300-01

Powder flasks

Spider with 6 distillation sleeves NS 14.5 20 ml



NS 29/32 NS 24/29

15-300-005-09

15-300-005-10

15-300-005-11

15-300-005-12

15-300-005-13

15-300-005-06

15-300-005-04

15-300-005-07

Spider with 5 flasks NS 24 50 ml

Spider with 5 flasks NS 24 100 ml

NS 29/32

15-300-005-08

15-300-005-05

NS 24/29

514-00070-00

514-00071-00

Evaporating cylinder 500 ml

Evaporating cylinder 1,500 ml

NS 29/32

514-00070-01

514-00071-01

NS 24/29

514-00004-00Foam brake with flask clamp

NS 29/32

514-00005-00

NS 24/29

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Rotavac Vario ControlP/N 591-00141-00Condenser(not shown)P/N 591-00084-00

Rotavac Vario TecP/N 591-00171-00CondenserP/N 591-00084-00

• All components which come in contact with media are built from chemically resistant fluoropolyemer

• The durable PTFE sandwich design guarantees an exceptional diaphragm lifespan

• The head cover and clamping disc have a stable core made of metal which offers unsurpassedlong-term performance of your operational parameters

• The direct pump drive (without belt) is exceptionally quiet, creates a very low vibrational environmentand reduces the need of wear and tear parts to a minimum

• The gas ballast valve has been optimized, prevents media condensing in the pump

For all Hei-VAP Precision models

• Two-stage diaphragm pump is made from chemical-resistant material

• Recommended for solvents with low or medium boiling points

• Suction capacity of 1.0 m3/h

• Achieves an ultimate vacuum of 12 mbar

• Can be combined with a condenser

• Power input: 160 W, Weight: 4.3 kg


Rotavac Vario Tec

RPM Regulated Vacuum Pumps

General advantages of all chemical-resistantdiaphragm vacuum pumps For all Hei-VAP Precision models

• Three-stage diaphragm pump is made from chemical-resistant material

• High suction capacity of 1.7 m3/h for fastest evacuation


• Even if the gas ballast valve is open an excellent ultimate vacuum is reached whenworking with easily condensable vapors. This makes distilling high boiling pointsolvents such as DMF or DMSO possible at low bath temperatures




Rotavac Vario Control

Highest distillation rates possible while reducing process time by 30 %

Stable distillation conditions accounts for solvent recovery up to 100 %

Significant time and energy savings

= continuous evaporation

Fully automatic control with speed adjustment

Time

Pre

ssur

e

=

recovery rate

RPM regulated pumps adjust their speed individually and come to a complete stop whenthe required vacuum level is reached

Rotavac Vario Pumping UnitP/N 591-00142-00Condenser(not shown)P/N 591-00084-00

Fully controllable stand-alone pumping unit including vacuum controller – for allHei-VAP Value and Hei-VAP Advantage models

• Three-stage diaphragm pump is made from chemical-resistant material

• Precise vacuum control avoids bumping and eliminates foaming of your evaporation solution

• Due to automatic vacuum supply to the process parameters you have more time forimportant laboratory activities


• The Rotavac Vario Pumping Unit achieves an ultimate vacuumof 5 mbar

• The Rotavac Vario Pumping Unit can be combined witha condenser



Rotavac Vario Pumping Unit

• Speed adjustment stops completelyif vacuum is reached and runs intermittentlyat very low speed to hold vacuum constant

• Increased diaphragm performance life dueto periods of non-operation

• Significant noise and vibration reductiondue to periods of non-operation

• Low energy consumption due to intermittentoperation

• Operates without vacuum valve

• Most precise vacuum level at all times

Your advantages

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Rotavac Valve ControlP/N 591-00130-00CondenserP/N 591-00083-00

Rotavac Valve TecP/N 591-00160-00Condenser (not shown)P/N 591-00083-00

Standard vacuum pumps which close a valve when the requiredvacuum level is reached

AUTOaccuratesensor

For all Hei-VAP models

• 2-gear diaphragm vacuum pump made of chemically-resistant materialguarantees working with solvents of low to medium boiling temperature

• Vacuum can be controlled manually or via valve operated vacuum controllers

• Suction capacity of 0.75 m3/h



• Power input: 80 W, Weight: 6 kg


Rotavac Valve Tec

For all Hei-VAP models

• Two-stage diaphragm pump made from chemical-resistant material


• Suction capacity for up to 3 rotary evaporators at the same time


• Vacuum can be controlled manually or via valve operated vacuum controllers

• Depending on your application you can switch on and off the vacuumpump via switchbox




Rotavac Valve Control

Valve-Regulated Vacuum Pumps

Rotavac Valce Controlwith condenser

Rotavac ValveTec

Rotavac VarioControl

Rotavac Vario Tecwith condenser

Manual vacuumcontroller

Vacuum valvewith Woulff Bottle

Vaportemperature sensor

recovery rate=

Pre

ssur

e

Time

Valve-regulated vacuum pump

Rotavac VarioPumping Unit

Hei-VAP Models Vacuum source Accessories

Equipment Combinations

Hei-VAP Advantage

Hei-VAP Value

Hei-VAP Precision



Rotavac Valve Tec

House vacuum

Vacuum controller

optional

Rotavac Vario Control

Rotavac Vario Tec

optional


Rotavac Valve Tec

House vacuum


included

not requiredVacuum valve



Rotavac Valve Tec

House vacuum

Vacuum controller

optional


included

optional Vapor temperature sensor(all glassware sets)

Vacuum valvenot required

Vacuum controller

Vacuum valve

AUTOaccurate-sensor(glassware G3/G6 only)optionalVapor temperature sensor(all glassware sets)

Vapor temperature sensor(all glassware sets)

included

required

Vacuum controller

Vacuum valve

AUTOaccurate-sensor(glassware G3/G6 only)optionalVapor temperature sensor(all glassware sets)

included

not required

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High cooling capacity - minimal bench space

• The only chiller designed specifically for rotary evaporators

• Minimal bench space due to unique ”L-shape design”

• Long-lasting service life

• Footprint of chiller: 470 x 580 x 443 mm

• Provides space of 470 x 405 mm for evaporator

• Temperature range: -10 °C to +40 °C

• Small quantity of circulating coolant required dueto innovative technology

• Precise temperature control of ± 0.5 °C

• Display for setting temperature and reading outactual temperature

SUPERIOR 1 THei-VAP Precision with a 210 °C heating bath incl. coatedglassware G1B, vapor temperature sensor, vacuum valve, vacuumpump Rotavac Valve Tec with condenserand tube setP/N 563-61110-00

RotacoolP/N 591-00200-00

Rotacool

Rotacool MiniP/N 591-00210-00

RotaChillP/N 591-00220-00

Chillers

Automated distillation with Hei-VAP Precision motor lift models and rpm-regulated vacuum control

Rotary evaporator with motor lift, a 210 °C heating bath, glassware set, vacuum pump Rotavac Vario Controlwith condenser, AUTOaccurate-sensor and tube set

PREMIUM 7 Hei-VAP Precision with glassware set G3 P/N 564-71300-00

PREMIUM 10 Hei-VAP Precision with coated glassware set G3B P/N 564-71310-00

PREMIUM 10 cool Same as PREMIUM 10, but with chiller Rotacool P/N 564-71318-00

PREMIUM 12 Hei-VAP Precision with coated glassware set G6B P/N 564-71610-00

Complete Packages PREMIUM

Complete Packages at a special price

Ideal for routine applications

• Chiller for all bench-top evaporators

• Small footprint of chiller: 225 x 450 x 400 mm

• Cooling temperature: 7 °C (not adjustable)

• Cooling capacity at 7 °C: 370 W

• No digital display

Rotacool Mini

The affordable model

• Temperature range: 0 °C to +100 °C

• Temperature control: ± 0.2 °C

• Footprint of chiller: 210 x 450 x 570 mm

• No digital display

RotaChill

Rotacool Rotacool Mini RotaChill

Temperature range [°C]

Coolant volume [L]

Cooling capacity* at: +20 °C [W]

0 °C

- 10 °C

-10° to +40°

2

420

350

220

7° (constant)

3

370

0° to +100°

6

200

140

100

* at 20 °C ambient temperature

SUPERIOR 1Hei-VAP Precision with a 210 °C heating bath incl. coatedglassware set G3B, AUTOaccurate-sensor, vacuum valve,vacuum pump Rotavac Valve Control with condenserand tube setP/N 563-51310-00

Automated distillation with Hei-VAP Precision hand lift models and valve-regulated vacuum control

Complete Packages SUPERIOR

BASIC 1Hei-VAP Value with a 210 °C heating bath and hand lift incl.coated glassware set G1B, vacuum pump Rotavac Valve Controland tube setP/N 560-81110-00

BASIC 1 THei-VAP Value with a 210 °C heating bath and hand liftincl. coated glassware set G1B, vacuum pump RotavacValve Tec and tube setP/N 560-91110-00

Complete Packages BASICStandard equipment for your lab

STANDARD 4Hei-VAP Advantage with a 210 °C heating bath and hand liftincl. coated glassware set G3B, vapor temperature sensor,vacuum pump Rotavac Valve Control and tube setP/N 561-81310-00

STANDARD 3 THei-VAP Advantage with a 210 °C heating bath and hand liftincl. glassware set G1, vapor temperature sensor,vacuum pump Rotavac Valve Tec and tube setP/N 561-91100-00

Complete Packages STANDARDFor standard distillations without vacuum control

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Cert i f icate

Hei-VAP Series Rotary Evaporators feature overtemperature safety circuits according

to DIN EN 61010-1:2001 and DIN EN 61010-2-010:2003 and therefore, are designed for

continuous operation.

This statement is made under the precondition that all units are operated in

accordance with the operation manual and in accordance with good practice standards

for safety in laboratories, rules for accident preventions, and compliance with directions

on hazardous materials.

S c h w a b a c h , O c t o b e r 2 0 1 1

i. V. Jan WelzienTechnical Director

i. V. Stefan RichterQuality Control Director

To confi rm the ability for

continuous operationof the Hei-VAP Series Rotary Evaporators

i. V. Jan WelzienTechnical Director

i. V. Stefan Richter

Zertifikate_GB_alle_15112011.indd 1 25.11.11 12:18


Probedruck


hand lift

manual

155

20 - 280

scale

1,300

20 - 210

± 1

scale

electronic/digital

250

stainless steel AISI 316L

255

4.5

no

no

no

no

no

no

noyesnoyes

no

1,400

16

395 x 490 x 430

IP 20

0 - 40 at 80 %rel. humidity

8.55.83.51.2

1,200

230 / 50/60115 / 60

Hand / Motor lift

Height adjustment speed

Height adjustment (mm)

Rotation speed (rpm)

Rotation speed setting

Drive

Heating capacity (W)

Temp. range heating bath (°C)

Temperature accuracy bath (°C)

Overheat protection bath (°C)

Bath temperature setting

Heating bath temperature control

Secondary overtemp. cut-off (°C)

Material heating bath

Diameter heating bath (mm)

Volume heating bath (l)

Display vapor temperaturerequired accessories

Integrated vacuum controller

Timer

Vacuum program Setpressure**

Vacuum program AUTOeasy**

Vacuum program AUTOaccurate**requires AUTOaccurate-sensor

Remote control function- Lift- Start rotation- Start vacuum- Start heating bath

Programmable ramps

Supply power (W)

Weight (w/o glass assembly) (kg)

Dimensions (l x w x h) (mm)

Protection class**** (DIN EN 60529)

Operating conditions (°C)

Rate of evaporation* (L/h)- Toluene- Acetone- Ethanol- Water

Condensing surface (cm2)

Supply voltage *** (V/Hz)

hand lift

manual

155

20 - 280

4.3” LCD color graphic display

1,300

20 - 210

± 1


electronic/digital

250


255

4.5

yesvapor temperature sensor

yes

yes

yes

yes

yes

noyesyesyes

yes

1,400

17

395 x 490 x 430

IP 20


8.55.83.51.2

1,200

230 / 50/60115 / 60

hand lift

manual

155

20 - 280

3.5” LCD display

1,300

20 - 210

± 1

3.5” LCD display

electronic/digital

250


255

4.5


no

yes

no

no

no

noyesnoyes

no

1,400

16

395 x 490 x 430

IP 20


8.55.83.51.2

1,200

230 / 50/60115 / 60

motor lift

30 mm/s

155

20 - 280

3.5” LCD display

1,300

20 - 210

± 1

3.5” LCD display

electronic/digital

250


255

4.5


no

yes

no

no

no

yesyesnoyes

no

1,400

16

395 x 420 x 430

IP 20


8.55.83.51.2

1,200

230 / 50/60115 / 60

motor lift

30 mm/s

155

20 - 280


1,300

20 - 210

± 1


electronic/digital

250


255

4.5


yes

yes

yes

yes

yes

yesyesyesyes

yes

1,400

17

395 x 420 x 430

IP 20


8.55.83.51.2

1,200

230 / 50/60115 / 60

Technical Specifications - Rotary Evaporators

Hei-VAPPrecision (HL)

Hei-VAPPrecision (ML)

Hei-VAPValue (HL)

Model Hei-VAPAdvantage (ML)

Hei-VAPAdvantage (HL)

* ΔT of 40 °C between heating bath temperature and boiling temperature

** Only in combination with vacuum systems*** Standard 230 V / 50/60 Hz: other voltages upon request, please specify for order

**** IP 67 cable connection on heating bath

cut-off at 5 °C over set temperature via separate PT 1000

brushless DC motor with electronic speed control

24 26


Heidolph Instruments GmbH & Co. KG

Walpersdorfer Str. 12 • 91126 Schwabach/Germany

Phone +49 (0) 91 22/99 20 68 • Fax +49 (0) 91 22/99 20 65

[email protected] • www.heidolph.com


Documents

Evaporation - mail2.gaiascience.com.mymail2.gaiascience.com.my/Images/heidolph/catalogue/Heidolph Rotary... · • Only the Hei-VAP heating bath reaches a temperature of 210 °C •