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Environmental Laboratory Accreditation Program

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Environmental Laboratory Accreditation Program

Oregon

Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division

NELAP Recognized

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

MATRIX :Reference Code Description

Non-Potable Water

AK101 GRO Determination of Gasoline Range Organics - Alaska Department ofEnvironmental Conservation

90015002

AnalyteAnalyte CodeGasoline range organics (GRO)9408

AK102 DRO Determination of Diesel Range Organics - Alaska Department ofEnvironmental Conservation

90015206

AnalyteAnalyte CodeDiesel range organics (DRO)9369

AK103 RRO Determination of Residual Range Organics - Alaska Department ofEnvironmental Conservation

90015400

AnalyteAnalyte CodeMotor Oil9499

CA HML 939-M Determination of Organic Lead Compounds by Graphite FurnaceAbsorption Spectrometry

90016765

AnalyteAnalyte CodeOrganic Lead1208

EPA 1010 Pensky-Martens Closed-Cup Method for Determining Ignitability10116606

AnalyteAnalyte CodeIgnitability1780

EPA 120.1 Conductance - Specific @ 25 C10006209

AnalyteAnalyte CodeConductivity1610

EPA 1311 Toxicity Characteristic Leaching Procedure10118806

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 1312 Synthetic Precipitation Leaching Procedure10119003

AnalyteAnalyte CodeExtraction/Preparation8031

Page 1 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 160.4 Total Volatile Solids, ignition @ 550 C.10010409

AnalyteAnalyte CodeResidue-volatile1970Volatile suspended solids2070

EPA 1613B Tetra- through Octa-Chlorinated Dioxins and Furans by IsotopeDilution GC/HRMS

10120602

AnalyteAnalyte Code1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)95161,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)95191,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-hpcdf)94201,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)94261,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-hpcdf)94231,2,3,4,7,8-Hexachlorodibenzofuran (1,2,3,4,7,8-Hxcdf)94711,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (1,2,3,4,7,8-Hxcdd)94531,2,3,6,7,8-Hexachlorodibenzofuran (1,2,3,6,7,8-Hxcdf)94741,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)94561,2,3,7,8,9-Hexachlorodibenzofuran (1,2,3,7,8,9-Hxcdf)94771,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (1,2,3,7,8,9-Hxcdd)94591,2,3,7,8-Pentachlorodibenzofuran (1,2,3,7,8-Pecdf)95431,2,3,7,8-Pentachlorodibenzo-p-dioxin (1,2,3,7,8-Pecdd)95402,3,4,6,7,8-Hexachlorodibenzofuran94802,3,4,7,8-Pentachlorodibenzofuran95492,3,7,8-Tetrachlorodibenzo- p-dioxin (2,3,7,8-TCDD)96182,3,7,8-Tetrachlorodibenzofuran9612Hpcdd, total9438Hpcdf, total9444Hxcdd, total9468Hxcdf, total9483Pecdd, total9555Pecdf, total9552TCDD, total9609TCDF, total9615

EPA 1631E Mercury in Water by Oxidation, Purge & Trap, and Cold Vapor AtomicFluorescence

10237204

AnalyteAnalyte CodeMercury1095

EPA 1664A Silica Gen Treated N-Hexane Extractable Material (Oil and Grease)10127603

AnalyteAnalyte CodeOil & Grease1860

EPA 180.1 Turbidity - Nephelometric10011402

AnalyteAnalyte CodeTurbidity2055

EPA 200.7 4.4 ICP - metals10013806

AnalyteAnalyte CodeAluminum1000Antimony1005Arsenic1010Barium1015Beryllium1020Bismuth1023Boron1025Cadmium1030

Page 2 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeCalcium1035Chromium1040Cobalt1050Copper1055Hardness (calc.)1760Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Molybdenum1100Nickel1105Potassium1125Selenium1140Silica as SiO21990Silicon1145Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190Zirconium1192

EPA 200.8 5.4 Metals by ICP-MS10014605

AnalyteAnalyte CodeAluminum1000Antimony1005Arsenic1010Barium1015Beryllium1020Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Hardness (calc.)1760Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Mercury1095Molybdenum1100Nickel1105Potassium1125Selenium1140Silicon1145Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190

Page 3 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 218.6 Dissolved Hexavalent Chromium by Ion Chromatography10027802

AnalyteAnalyte CodeChromium VI1045

EPA 245.2 Mercury by Cold Vapor Atomic Absorption10037000

AnalyteAnalyte CodeMercury1095

EPA 300.0 Ion chromatography - anions.10053006

AnalyteAnalyte CodeBromate1535Bromide1540Chlorate1570Chloride1575Chlorite1595Fluoride1730Nitrate as N1810Nitrate-nitrite1820Nitrite1835Nitrite as N1840Orthophosphate as P1870Phosphorus, total1910Sulfate2000

EPA 300.1 Ion chromatography - anions.10053608

AnalyteAnalyte CodeBromate1535Bromide1540Chlorate1570Chloride1575Chlorite1595Fluoride1730Nitrate as N1810Nitrite as N1840Orthophosphate as P1870Sulfate2000

EPA 3005A Acid Digestion of waters for Total Recoverable or Dissolved Metals10133207

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3010A Acid Digestion of Aqueous samples and Extracts for Total Metals10133605

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3050A Acid Digestion of Sediments, Sludges, and soils10135407

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3060A Alkaline Digestion for Hexavalent Chromium10136604

AnalyteAnalyte CodeExtraction/Preparation8031

Page 4 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 310.2 Alkalinity as CaCO3 - Colorimetric, Automated10055002

AnalyteAnalyte CodeAlkalinity as CaCO31505

EPA 335.4 Methods for the Determination of Inorganic Substances inEnvironmental Samples

10061208

AnalyteAnalyte CodeTotal cyanide1645

EPA 350.1 Ammonia Nitrogen - Colorimetric, Auto Phenate10063204

AnalyteAnalyte CodeAmmonia as N1515

EPA 3510 Separatory Funnel Liquid-liquid extraction10137607

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3520 Continuous Liquid-liquid extraction10138406

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 353.2 Nitrate/Nitrite Nitrogen - Automated, Cadmium10067206

AnalyteAnalyte CodeKjeldahl nitrogen1790Nitrate as N1810Nitrate-nitrite1820Nitrite as N1840Total nitrate+nitrite1825

EPA 3535 Solid-Phase Extraction (SPE)10139205

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3540B Soxhlet Extraction10140008

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3550 Ultrasonic Extraction10141409

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 365.1 Phosphorous - Colorimetric, Automated persulfate10069600

AnalyteAnalyte CodeOrthophosphate as P1870Phosphorus, total1910

EPA 420.1 Phenolics - Spectrophotometric, manual.10079206

AnalyteAnalyte CodeTotal phenolics1905

Page 5 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 420.4 Phenolics, Total Recoverable by Semi-Automated Colorimetry10080203

AnalyteAnalyte CodeTotal phenolics1905

EPA 5030B Purge and trap for aqueous samples10153409

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 6010B ICP - AES10155609

AnalyteAnalyte CodeAluminum1000Antimony1005Arsenic1010Barium1015Beryllium1020Bismuth1023Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Hardness (calc.)1760Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Molybdenum1100Nickel1105Potassium1125Selenium1140Silica as SiO21990Silicon1145Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190

EPA 602 Purgeable Aromatics by GC/PID Purge & Trap10102202

AnalyteAnalyte CodeBenzene4375Ethylbenzene4765m+p-xylene5240Methyl tert-butyl ether (MTBE)5000o-Xylene5250Toluene5140Xylene (total)5260

EPA 6020 Inductively Coupled Plasma-Mass Spectrometry10156000

AnalyteAnalyte CodeAluminum1000

Page 6 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeAntimony1005Arsenic1010Barium1015Beryllium1020Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Mercury1095Molybdenum1100Nickel1105Potassium1125Selenium1140Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190Zirconium1192

EPA 608 Organochlorine Pesticides & PCBs by GC/ECD10103603

AnalyteAnalyte Code4,4'-DDD73554,4'-DDE73604,4'-DDT7365Alachlor7005Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110alpha-Chlordane7240Aroclor-1016 (PCB-1016)8880Aroclor-1221 (PCB-1221)8885Aroclor-1232 (PCB-1232)8890Aroclor-1242 (PCB-1242)8895Aroclor-1248 (PCB-1248)8900Aroclor-1254 (PCB-1254)8905Aroclor-1260 (PCB-1260)8910Aroclor-1262 (PCB-1262)8912Aroclor-1268 (PCB-1268)8913Atrazine7065beta-BHC (beta-Hexachlorocyclohexane)7115Butachlor7160Chlordane (tech.)7250Chloroneb7265Chlorthalonil (Daconil)7310Dacthal (DCPA)8550delta-BHC7105Dieldrin7470Dimethazone (Clomazone)7473Endosulfan I7510Endosulfan II7515

Page 7 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeEndosulfan sulfate7520Endrin7540Endrin aldehyde7530Endrin ketone7535gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120gamma-Chlordane7245Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorocyclopentadiene6285Isodrin7725Kepone7740Malathion7770Methoxychlor7810Methyl parathion (Parathion, methyl)7825Metolachlor7835Metribuzin7845Mirex7870Parathion, ethyl7955Propachlor (Ramrod)8045Simazine8125Toxaphene (Chlorinated camphene)8250Trifluralin (Treflan)8295

EPA 610 (HPLC) Polynuclear Hydrocarbons by HPLC/UV-VIS10297004

AnalyteAnalyte Code1-Methylnaphthalene63802-Methylnaphthalene6385Acenaphthene5500Acenaphthylene5505Anthracene5555Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Chrysene5855Dibenz(a,h) anthracene5895Fluoranthene6265Fluorene6270Indeno(1,2,3-cd) pyrene6315Naphthalene5005Phenanthrene6615Pyrene6665

EPA 624 Volatile Organic Compounds by purge and trap GC/MS10107207

AnalyteAnalyte Code1,1,1,2-Tetrachloroethane51051,1,1-Trichloroethane51601,1,2,2-Tetrachloroethane51101,1,2-Trichloroethane51651,1-Dichloroethane46301,1-Dichloroethylene46401,1-Dichloropropene46701,2,3-Trichlorobenzene51501,2,3-Trichloropropane51801,2,4-Trichlorobenzene51551,2,4-Trimethylbenzene52101,2-Dibromoethane (EDB, Ethylene dibromide)4585

Page 8 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code1,2-Dichlorobenzene46101,2-Dichloroethane (Ethylene dichloride)46351,2-Dichloropropane46551,3,5-Trimethylbenzene52151,3-Dichlorobenzene46151,3-Dichloropropane46601,4-Dichlorobenzene46201,4-Dioxane (1,4- Diethyleneoxide)47352,2-Dichloropropane46652-Butanone (Methyl ethyl ketone, MEK)44102-Chloroethyl vinyl ether45002-Chlorotoluene45352-Hexanone (MBK)48604-Chlorotoluene45404-Methyl-2-pentanone (MIBK)4995Acetone4315Acetonitrile4320Acrolein (Propenal)4325Acrylonitrile4340Allyl chloride (3-Chloropropene)4355Benzene4375Bromobenzene4385Bromochloromethane4390Bromodichloromethane4395Bromoform4400Carbon disulfide4450Carbon tetrachloride4455Chlorobenzene4475Chloroethane (Ethyl chloride)4485Chloroform4505cis-1,2-Dichloroethylene4645cis-1,3-Dichloropropene4680Dibromochloropropane4580Dibromofluoromethane4590Dibromomethane (Methylene bromide)4595Dichlorodifluoromethane (Freon-12)4625Ethyl methacrylate4810Ethylbenzene4765Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)4770Hexachlorobutadiene4835Hexachloroethane4840Iodomethane (Methyl iodide)4870Isobutyl alcohol (2-Methyl-1-propanol)4875Isopropylbenzene4900Methanol4930Methyl methacrylate4990Methyl tert-butyl ether (MTBE)5000Methylene chloride (Dichloromethane)4975Naphthalene5005n-Butyl alcohol (1-Butanol, n-Butanol)4425n-Butylbenzene4435Nitrobenzene5015n-Propylbenzene5090Pentachloroethane5035sec-Butylbenzene4440Styrene5100T-amylmethylether (TAME)4370tert-Butyl alcohol4420tert-Butylbenzene4445Tetrachloroethylene (Perchloroethylene)5115Toluene5140

Page 9 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeTotal trihalomethanes5205trans-1,2-Dichloroethylene4700trans-1,3-Dichloropropylene4685Trichloroethene (Trichloroethylene)5170Trichlorofluoromethane (Fluorotrichloromethane, Freon 11)5175Vinyl acetate5225Vinyl chloride5235Xylene (total)5260

EPA 625 Base/Neutrals and Acids by GC/MS10300002

AnalyteAnalyte Code1,2,4,5-Tetrachlorobenzene67151,2,4-Trichlorobenzene51551,2-Dichlorobenzene46101,2-Diphenylhydrazine62211,3-Dichlorobenzene46151,4-Dichlorobenzene46201-Chloronaphthalene57901-Naphthylamine64252,3,4,6-Tetrachlorophenol67352,4,5-Trichlorophenol68352,4,6-Trichlorophenol68402,4-Dichlorophenol60002,4-Dimethylphenol61302,4-Dinitrophenol61752,4-Dinitrotoluene (2,4-DNT)61852,6-Dichlorophenol60052,6-Dinitrotoluene (2,6-DNT)61902-Chloronaphthalene57952-Chlorophenol58002-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)63602-Methylnaphthalene63852-Methylphenol (o-Cresol)64002-Naphthylamine64302-Nitroaniline64602-Nitrophenol64903 & 4 Methylphenol64123,3'-Dichlorobenzidine59453-Methylcholanthrene63553-Methylphenol (m-Cresol)64053-Nitroaniline64654,4'-DDD73554,4'-DDE73604,4'-DDT73654-Aminobiphenyl55404-Bromophenyl phenyl ether (BDE-3)56604-Chloro-3-methylphenol57004-Chloroaniline57454-Chlorophenyl phenylether58254-Dimethyl aminoazobenzene61054-Methylphenol (p-Cresol)64104-Nitroaniline64704-Nitrophenol65007,12-Dimethylbenz(a) anthracene6115Acenaphthene5500Acenaphthylene5505Acetophenone5510Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110Aniline5545

Page 10 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeAnthracene5555Benzidine5595Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Benzoic acid5610Benzyl alcohol5630beta-BHC (beta-Hexachlorocyclohexane)7115bis(2-Chloroethoxy)methane5760bis(2-Chloroethyl) ether5765bis(2-Chloroisopropyl) ether5780bis(2-Ethylhexyl)adipate6062Butyl benzyl phthalate5670Carbazole5680Carbofuran (Furaden)7205Chrysene5855Coelution - 3-Chlorophenol + 4-Chlorophenol8906delta-BHC7105Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)6065Diallate7405Dibenz(a,h) anthracene5895Dibenzofuran5905Dieldrin7470Diethyl phthalate6070Dimethoate7475Dimethyl phthalate6135Di-n-butyl phthalate5925Di-n-octyl phthalate6200Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)8620Diphenylamine6205Disulfoton8625Endosulfan I7510Endosulfan II7515Endosulfan sulfate7520Endrin7540Ethyl methanesulfonate6260Fluoranthene6265Fluorene6270gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorobutadiene4835Hexachlorocyclopentadiene6285Hexachloroethane4840Indeno(1,2,3-cd) pyrene6315Isophorone6320Methoxychlor7810Methyl methanesulfonate6375Methyl parathion (Parathion, methyl)7825Naphthalene5005Nitrobenzene5015n-Nitrosodimethylamine6530n-Nitroso-di-n-butylamine5025n-Nitrosodi-n-propylamine6545n-Nitrosodiphenylamine6535n-Nitrosomethylethalamine6550n-Nitrosopiperidine6560Parathion, ethyl7955

Page 11 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodePentachlorobenzene6590Pentachloronitrobenzene6600Pentachlorophenol6605Phenacetin6610Phenanthrene6615Phenol6625Phorate7985Pronamide (Kerb)6650Pyrene6665Pyridine5095

EPA 7199 Determination of Hexavalent Chromium in Drinking Water,Groundwater and Industrial Wastewater Effluents by IonChromatography

10163005

AnalyteAnalyte CodeChromium VI1045

EPA 7470A Mercury in Liquid Waste by Cold Vapor Atomic Absorption10165807

AnalyteAnalyte CodeMercury1095

EPA 7471A Mercury in Solid Waste by Cold Vapor Atomic Absorption10166208

AnalyteAnalyte CodeMercury1095

EPA 8015B Non-halogenated organics using GC/FID10173601

AnalyteAnalyte CodeDiesel range organics (DRO)9369Gasoline range organics (GRO)9408Jet Fuel9488Kerosene9409

EPA 8021B Aromatic and Halogenated Volatiles by GC with PID and/or ECD Purge& Trap

10174808

AnalyteAnalyte CodeBenzene4375Ethylbenzene4765m+p-xylene5240Methyl tert-butyl ether (MTBE)5000o-Xylene5250Toluene5140Xylene (total)5260

EPA 8081A Organochlorine Pesticides by GC/ECD10178606

AnalyteAnalyte Code4,4'-DDD73554,4'-DDE73604,4'-DDT7365Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110alpha-Chlordane7240beta-BHC (beta-Hexachlorocyclohexane)7115Chlordane (tech.)7250delta-BHC7105Dieldrin7470Endosulfan I7510Endosulfan II7515

Page 12 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeEndosulfan sulfate7520Endrin7540Endrin aldehyde7530Endrin ketone7535gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120gamma-Chlordane7245Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorocyclopentadiene6285Methoxychlor7810Toxaphene (Chlorinated camphene)8250

EPA 8082 Polychlorinated Biphenyls (PCBs) by GC/ECD10179007

AnalyteAnalyte CodeAroclor-1016 (PCB-1016)8880Aroclor-1221 (PCB-1221)8885Aroclor-1232 (PCB-1232)8890Aroclor-1242 (PCB-1242)8895Aroclor-1248 (PCB-1248)8900Aroclor-1254 (PCB-1254)8905Aroclor-1260 (PCB-1260)8910Aroclor-1262 (PCB-1262)8912Aroclor-1268 (PCB-1268)8913Decachlorobiphenyl (BZ-209)9105

EPA 8151A Chlorinated Herbicides by GC/ECD10183207

AnalyteAnalyte Code2,4,5-T86552,4-D85452,4-DB85603,5-Dichlorobenzoic acid86004-Nitrophenol6500Acifluorfen8505Bentazon8530Chloramben8540Dacthal (DCPA)8550Dalapon8555Dicamba8595Dichloroprop (Dichlorprop)8605Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)8620Garlon (Triclopyr)7650MCPA7775MCPP7780Pentachlorophenol6605Picloram8645Silvex (2,4,5-TP)8650

EPA 8260B Volatile Organic Compounds by purge and trap GC/MS10184802

AnalyteAnalyte Code1,1,1,2-Tetrachloroethane51051,1,1-Trichloroethane51601,1,2,2-Tetrachloroethane51101,1,2-Trichloroethane51651,1-Dichloroethane46301,1-Dichloroethylene46401,1-Dichloropropene4670

Page 13 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code1,2,3-Trichlorobenzene51501,2,3-Trichloropropane51801,2,4-Trichlorobenzene51551,2,4-Trimethylbenzene52101,2-Dibromoethane (EDB, Ethylene dibromide)45851,2-Dichlorobenzene46101,2-Dichloroethane (Ethylene dichloride)46351,2-Dichloropropane46551,3,5-Trimethylbenzene52151,3-Dichlorobenzene46151,3-Dichloropropane46601,4-Dichlorobenzene46201,4-Dioxane (1,4- Diethyleneoxide)47352,2-Dichloropropane46652-Butanone (Methyl ethyl ketone, MEK)44102-Chloroethyl vinyl ether45002-Chlorotoluene45352-Hexanone (MBK)48604-Chlorotoluene45404-Methyl-2-pentanone (MIBK)4995Acetone4315Acetonitrile4320Acrolein (Propenal)4325Acrylonitrile4340Allyl chloride (3-Chloropropene)4355Benzene4375Bromobenzene4385Bromochloromethane4390Bromodichloromethane4395Bromoethane (Ethyl Bromide)4397Bromoform4400Carbon disulfide4450Carbon tetrachloride4455Chlorobenzene4475Chlorodibromomethane4575Chloroethane (Ethyl chloride)4485Chloroform4505cis-1,2-Dichloroethylene4645cis-1,3-Dichloropropene4680Dibromochloropropane4580Dibromomethane (Methylene bromide)4595Dichlorofluoromethane (Freon 21)4627Ethyl methacrylate4810Ethylbenzene4765Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)4770Gasoline range organics (GRO)9408Hexachlorobutadiene4835Hexachloroethane4840Iodomethane (Methyl iodide)4870Isobutyl alcohol (2-Methyl-1-propanol)4875Isopropylbenzene4900Methanol4930Methyl acrylate4945Methyl chloride (Chloromethane)4960Methyl tert-butyl ether (MTBE)5000Methylene chloride (Dichloromethane)4975Naphthalene5005n-Butyl alcohol (1-Butanol, n-Butanol)4425n-Butylbenzene4435Nitrobenzene5015n-Propylbenzene5090

Page 14 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodePentachloroethane5035sec-Butylbenzene4440Styrene5100T-amylmethylether (TAME)4370tert-Butyl alcohol4420tert-Butylbenzene4445Tetrachloroethylene (Perchloroethylene)5115Toluene5140trans-1,2-Dichloroethylene4700trans-1,3-Dichloropropylene4685Trichloroethene (Trichloroethylene)5170Trichlorofluoromethane (Fluorotrichloromethane, Freon 11)5175Vinyl acetate5225Vinyl chloride5235Xylene (total)5260

EPA 8270C Semivolatile Organic compounds by GC/MS10185805

AnalyteAnalyte Code1,2,4,5-Tetrachlorobenzene67151,2,4-Trichlorobenzene51551,2-Dichlorobenzene46101,2-Diphenylhydrazine62211,3-Dichlorobenzene46151,4-Dichlorobenzene46201-Chloronaphthalene57901-Naphthylamine64252,3,4,6-Tetrachlorophenol67352,4,5-Trichlorophenol68352,4,6-Trichlorophenol68402,4-Dichlorophenol60002,4-Dimethylphenol61302,4-Dinitrophenol61752,4-Dinitrotoluene (2,4-DNT)61852,6-Dichlorophenol60052,6-Dinitrotoluene (2,6-DNT)61902-Chloronaphthalene57952-Chlorophenol58002-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)63602-Methylnaphthalene63852-Methylphenol (o-Cresol)64002-Naphthylamine64302-Nitroaniline64602-Nitrophenol64902-Picoline (2-Methylpyridine)50503,3'-Dichlorobenzidine59453-Methylcholanthrene63553-Methylphenol (m-Cresol)64053-Nitroaniline64654,4'-DDD73554,4'-DDE73604,4'-DDT73654-Aminobiphenyl55404-Bromophenyl phenyl ether (BDE-3)56604-Chloro-3-methylphenol57004-Chloroaniline57454-Chlorophenyl phenylether58254-Dimethyl aminoazobenzene61054-Methylphenol (p-Cresol)64104-Nitroaniline64704-Nitrophenol6500

Page 15 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code7,12-Dimethylbenz(a) anthracene6115a-a-Dimethylphenethylamine6125Acenaphthene5500Acenaphthylene5505Acetophenone5510Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110alpha-Chlordane7240Aniline5545Anthracene5555Benzidine5595Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Benzoic acid5610Benzyl alcohol5630beta-BHC (beta-Hexachlorocyclohexane)7115bis(2-Chloroethoxy)methane5760bis(2-Chloroethyl) ether5765bis(2-Chloroisopropyl) ether5780Butyl benzyl phthalate5670Captafol7185Captan7190Carbaryl (Sevin)7195Carbazole5680Carbofuran (Furaden)7205Carbophenothion7220Chrysene5855delta-BHC7105Demeton-o7395Demeton-s7385Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)6065Diallate7405Dibenz(a, j) acridine5900Dibenz(a,h) anthracene5895Dibenzofuran5905Dichlone7430Dieldrin7470Diethyl phthalate6070Dimethoate7475Dimethyl phthalate6135Di-n-butyl phthalate5925Di-n-octyl phthalate6200Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)8620Diphenylamine6205Disulfoton8625Endosulfan I7510Endosulfan II7515Endosulfan sulfate7520Endrin7540Endrin aldehyde7530Endrin ketone7535EPN7550Ethion7565Ethyl methanesulfonate6260Fluoranthene6265Fluorene6270gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120gamma-Chlordane7245

Page 16 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeHeptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorobutadiene4835Hexachlorocyclopentadiene6285Hexachloroethane4840Indeno(1,2,3-cd) pyrene6315Isophorone6320Malathion7770Methoxychlor7810Methyl methanesulfonate6375Methyl parathion (Parathion, methyl)7825Mevinphos7850Naphthalene5005Nitrobenzene5015n-Nitrosodimethylamine6530n-Nitroso-di-n-butylamine5025n-Nitrosodi-n-propylamine6545n-Nitrosodiphenylamine6535n-Nitrosomethylethalamine6550n-Nitrosopiperidine6560Parathion, ethyl7955Pentachlorobenzene6590Pentachloronitrobenzene6600Pentachlorophenol6605Phenacetin6610Phenanthrene6615Phenol6625Phorate7985Pronamide (Kerb)6650Pyrene6665Pyridine5095Sulfotepp8155Tetraethyl pyrophosphate (TEPP)8210Trifluralin (Treflan)8295

EPA 8280A Polychlorinated Dibenzo-p-Dioxins and PolychlorinatedDibenzofurans by GC/HRMS

10186808

AnalyteAnalyte Code1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)95161,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)95191,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-hpcdf)94201,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)94261,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-hpcdf)94231,2,3,4,7,8-Hexachlorodibenzofuran (1,2,3,4,7,8-Hxcdf)94711,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (1,2,3,4,7,8-Hxcdd)94531,2,3,6,7,8-Hexachlorodibenzofuran (1,2,3,6,7,8-Hxcdf)94741,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)94561,2,3,7,8,9-Hexachlorodibenzofuran (1,2,3,7,8,9-Hxcdf)94771,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (1,2,3,7,8,9-Hxcdd)94591,2,3,7,8-Pentachlorodibenzofuran (1,2,3,7,8-Pecdf)95431,2,3,7,8-Pentachlorodibenzo-p-dioxin (1,2,3,7,8-Pecdd)95402,3,4,6,7,8-Hexachlorodibenzofuran94802,3,4,7,8-Pentachlorodibenzofuran95492,3,7,8-Tetrachlorodibenzo- p-dioxin (2,3,7,8-TCDD)96182,3,7,8-Tetrachlorodibenzofuran9612Hpcdd, total9438Hpcdf, total9444Hxcdd, total9468Hxcdf, total9483Pecdd, total9555

Page 17 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodePecdf, total9552TCDD, total9609TCDF, total9615

EPA 8290 Polychlorinated Dibenzodioxins (PCDDs) and PolychlorinatedDibenzofurans (PCDFs) by GC/HRMS

10187209

AnalyteAnalyte Code1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)95161,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)95191,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-hpcdf)94201,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)94261,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-hpcdf)94231,2,3,4,7,8-Hexachlorodibenzofuran (1,2,3,4,7,8-Hxcdf)94711,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (1,2,3,4,7,8-Hxcdd)94531,2,3,6,7,8-Hexachlorodibenzofuran (1,2,3,6,7,8-Hxcdf)94741,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)94561,2,3,7,8,9-Hexachlorodibenzofuran (1,2,3,7,8,9-Hxcdf)94771,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (1,2,3,7,8,9-Hxcdd)94591,2,3,7,8-Pentachlorodibenzofuran (1,2,3,7,8-Pecdf)95431,2,3,7,8-Pentachlorodibenzo-p-dioxin (1,2,3,7,8-Pecdd)95402,3,4,6,7,8-Hexachlorodibenzofuran94802,3,4,7,8-Pentachlorodibenzofuran95492,3,7,8-Tetrachlorodibenzo- p-dioxin (2,3,7,8-TCDD)96182,3,7,8-Tetrachlorodibenzofuran9612Hpcdd, total9438Hpcdf, total9444Hxcdd, total9468Hxcdf, total9483Pecdd, total9555Pecdf, total9552TCDD, total9609TCDF, total9615

EPA 8310 Polynuclear Aromatic Hydrocarbons by HPLC/UV-VIS10187607

AnalyteAnalyte Code1-Methylnaphthalene63802-Methylnaphthalene6385Acenaphthene5500Acenaphthylene5505Anthracene5555Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Chrysene5855Dibenz(a,h) anthracene5895Fluoranthene6265Fluorene6270Indeno(1,2,3-cd) pyrene6315Naphthalene5005Phenanthrene6615Pyrene6665

EPA 8315A Determination of Carbonyl Compounds by HPLC/UV-VIS10188008

AnalyteAnalyte Code2,5-Dimethylbenzaldehyde6110Acetaldehyde4300

Page 18 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeAcetone4315Acrolein (Propenal)4325Benzaldehyde5570Butylaldehyde (Butanal)4430Crotonaldehyde4545Cyclohexanone4560Decanal4565Formaldehyde4815Heptanal4820Hexanaldehyde (Hexanal)3825Isovaleraldehyde6330m-Tolualdehyde (1,3-Tolualdehyde)5125n-Octaldehyde (Octanal)9525Nonanal6575o-Tolualdehyde (1,2-Tolualdehyde)6755Propanal (Propionaldehyde)6935p-Tolualdehyde (1,4-Tolualdehyde)6760Valeraldehyde (Pentanal, Pentanaldehyde)4040

EPA 8316 Acrylamide, Acrylonitrile and Acrolein by High Performance LiquidChromatography (HPLC)

10188202

AnalyteAnalyte CodeAcrolein (Propenal)4325Acrylamide4330Acrylonitrile4340

EPA 8318 N-Methylcarbamates by HPLC/UV-VIS10188406

AnalyteAnalyte Code3-Hydroxycarbofuran7710Aldicarb (Temik)7010Aldicarb sulfone7015Aldicarb sulfoxide7020Bendiocarb7085Carbaryl (Sevin)7195Carbofuran (Furaden)7205Dioxacarb9384Formetanate hydrochloride9405m-Cumenyl methylcarbamate7335Methiocarb (Mesurol)7800Methomyl (Lannate)7805Metolcarb7840Oxamyl7940Promecarb8025Propoxur (Baygon)8080Thiodicarb8225

EPA 8330A Nitroaromatics and Nitramines by High Performance LiquidChromatography (HPLC)

10190008

AnalyteAnalyte Code1,3,5-Trinitrobenzene (1,3,5-TNB)68851,3-Dinitrobenzene (1,3-DNB)61602,4,6-Trinitrotoluene (2,4,6-TNT)96512,4-Dinitrotoluene (2,4-DNT)61852,6-Dinitrotoluene (2,6-DNT)61902-Amino-4,6-dinitrotoluene (2-am-dnt)93032-Nitrotoluene95073-Nitrotoluene95104-Amino-2,6-dinitrotoluene (4-am-dnt)93064-Nitrotoluene9513

Page 19 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeMethyl-2,4,6-trinitrophenylnitramine (tetryl)6415Nitrobenzene5015Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX)9522RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine)9432

EPA 9012A Total and Amenable Cyanide (automated colorimetric with off-linedistillation)

10193405

AnalyteAnalyte CodeAmenable cyanide1510Cyanide1635Total cyanide1645

EPA 9040B pH Electrometric Measurement10197203

AnalyteAnalyte CodepH1900

EPA 9045C Soil and Waste pH10198400

AnalyteAnalyte CodepH1900

SM 2120 B 20th ED Color by Visual Comparison20224004

AnalyteAnalyte CodeColor1605

SM 2130 B 20th ED Turbidity by Nephelometric Determination20042404

AnalyteAnalyte CodeTurbidity2055

SM 2310 B 20th ED Acidity by Titration20044206

AnalyteAnalyte CodeAcidity, as CaCO31500

SM 2320 B 20th ED Alkalinity by Titration20045209

AnalyteAnalyte CodeAlkalinity as CaCO31505Corrosivity1615

SM 2340 B 20th ED Hardness by calculation20046202

AnalyteAnalyte CodeCalcium hardness as CaCO31550Hardness1750Total hardness as CaCO31755

SM 2510 B 20th ED Conductivity by Probe20048208

AnalyteAnalyte CodeConductivity1610

SM 2540 B 20th ED Total Solids20049007

AnalyteAnalyte CodeResidue-total1950

Page 20 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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01/30/2014 01/29/2015

4033 - 001

01/30/2014

SM 2540 C 20th ED Total Dissolved Solids20050004

AnalyteAnalyte CodeResidue-filterable (TDS)1955

SM 2540 D 20th ED Total Suspended Solids20050800

AnalyteAnalyte CodeResidue-nonfilterable (TSS)1960

SM 2540 F 20th ED Settleable Solids20051803

AnalyteAnalyte CodeResidue-settleable1965

SM 4500-Cl D 20th ED Chlorine by Potentiometry20079601

AnalyteAnalyte CodeChloride1575Residual free chlorine1945

SM 4500-Cl G 20th ED Residual Chlorine by DPD Colorimetric Determination20081203

AnalyteAnalyte CodeChlorine1580Residual free chlorine1945Total residual chlorine1940

SM 4500-Cl¯ E 19th ED Chloride by Automated Ferricyanide Method20086004

AnalyteAnalyte CodeChloride1575

SM 4500-CN E 20th ED Cyanide by Colorimetric Determination20092404

AnalyteAnalyte CodeCyanide1635Total cyanide1645

SM 4500-CN¯ C 21st ED Cyanide by Total Cyanide after Distillation20095403

AnalyteAnalyte CodeCyanide1635

SM 4500-CN¯ G 21st ED Cyanide by Cyanides Amenable to Chlorination after Distillation20097001

AnalyteAnalyte CodeAmenable cyanide1510

SM 4500-H+ B 20th ED pH by Probe20104807

AnalyteAnalyte CodepH1900

SM 4500-O G 20th ED Dissolved Oxygen by Membrane Electrode Method20121204

AnalyteAnalyte CodeOxygen, dissolved1880

Page 21 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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01/30/2014 01/29/2015

4033 - 001

01/30/2014

SM 4500-S2¯ D 20th ED Sulfide by Methylene Blue Method20125400

AnalyteAnalyte CodeSulfide2005

SM 5210 B 20th ED Biochemical Oxygen Demand, 5-Day (BOD5)20134809

AnalyteAnalyte CodeBiochemical oxygen demand1530Carbonaceous BOD, CBOD1555

SM 5220 D 20th ED Chemical Oxygen Demand by Closed Reflux and ColorimetricDetermination

20136407

AnalyteAnalyte CodeChemical oxygen demand1565

SM 5310 B 20th ED Total Organic Carbon by Combustion Infra-red Method20137400

AnalyteAnalyte CodeDissolved organic carbon (DOC)1710Total organic carbon2040

SM 5520 B 20th ED Oil and Grease by Extraction and Gravimetric Determination20141202

AnalyteAnalyte Coden-Hexane Extractable Material (O&G)1803Oil & Grease1860

SM 5540 C 20th ED Surfactants as MBAS20144609

AnalyteAnalyte CodeSurfactants - MBAS2025

SM 5550 B 20th ED Tannin and Lignin20145306

AnalyteAnalyte CodeTannin & Lignin9597

WA EPH Extractable Petroleum Hydrocarbons60015001

AnalyteAnalyte CodeDiesel range organics (DRO)9369EPH Aliphatic >C10-C126211EPH Aliphatic >C12-C166212EPH Aliphatic >C16-C216214EPH Aliphatic >C21-C346216EPH Aliphatic C8-C106220EPH Aliphatic C9-C186222EPH Aromatic >C10-C126224EPH Aromatic >C12-C166226EPH Aromatic >C16-C216228EPH Aromatic >C21-C346231EPH Aromatic C8-C106236

WA VPH Volatile Petroleum Hydrocarbons (VPH) by GC/PID Purge & Trap60015056

AnalyteAnalyte CodeBenzene4375Ethylbenzene4765Gasoline range organics (GRO)9408m+p-xylene5240

Page 22 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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4033 - 001

01/30/2014

AnalyteAnalyte CodeMethyl tert-butyl ether (MTBE)5000n-Hexane4855o-Xylene5250Toluene5140VPH Aliphatic >C10-C125300VPH Aliphatic >C6-C85301VPH Aliphatic >C8-C105302VPH Aliphatic C5-C65303VPH Aromatic >C10-C125308VPH Aromatic >C12-C135309VPH Aromatic >C8-C105310Xylene (total)5260

Page 23 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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4033 - 001

01/30/2014

MATRIX :Reference Code Description

Solids

AK101 GRO Determination of Gasoline Range Organics - Alaska Department ofEnvironmental Conservation

90015002

AnalyteAnalyte CodeGasoline range organics (GRO)9408

AK102 DRO Determination of Diesel Range Organics - Alaska Department ofEnvironmental Conservation

90015206

AnalyteAnalyte CodeDiesel range organics (DRO)9369

AK103 RRO Determination of Residual Range Organics - Alaska Department ofEnvironmental Conservation

90015400

AnalyteAnalyte CodeMotor Oil9499

CA HML 939-M Determination of Organic Lead Compounds by Graphite FurnaceAbsorption Spectrometry

90016765

AnalyteAnalyte CodeOrganic Lead1208

EPA 1010 Pensky-Martens Closed-Cup Method for Determining Ignitability10116606

AnalyteAnalyte CodeIgnitability1780

EPA 120.1 Conductance - Specific @ 25 C10006209

AnalyteAnalyte CodeConductivity1610

EPA 1311 Toxicity Characteristic Leaching Procedure10118806

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 1312 Synthetic Precipitation Leaching Procedure10119003

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 160.4 Total Volatile Solids, ignition @ 550 C.10010409

AnalyteAnalyte CodeResidue-volatile1970Volatile suspended solids2070

EPA 1613B Tetra- through Octa-Chlorinated Dioxins and Furans by IsotopeDilution GC/HRMS

10120602

AnalyteAnalyte Code1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)95161,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)95191,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-hpcdf)94201,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)94261,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-hpcdf)94231,2,3,4,7,8-Hexachlorodibenzofuran (1,2,3,4,7,8-Hxcdf)94711,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (1,2,3,4,7,8-Hxcdd)94531,2,3,6,7,8-Hexachlorodibenzofuran (1,2,3,6,7,8-Hxcdf)9474

Page 24 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)94561,2,3,7,8,9-Hexachlorodibenzofuran (1,2,3,7,8,9-Hxcdf)94771,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (1,2,3,7,8,9-Hxcdd)94591,2,3,7,8-Pentachlorodibenzofuran (1,2,3,7,8-Pecdf)95431,2,3,7,8-Pentachlorodibenzo-p-dioxin (1,2,3,7,8-Pecdd)95402,3,4,6,7,8-Hexachlorodibenzofuran94802,3,4,7,8-Pentachlorodibenzofuran95492,3,7,8-Tetrachlorodibenzo- p-dioxin (2,3,7,8-TCDD)96182,3,7,8-Tetrachlorodibenzofuran9612Hpcdd, total9438Hpcdf, total9444Hxcdd, total9468Hxcdf, total9483Pecdd, total9555Pecdf, total9552TCDD, total9609TCDF, total9615

EPA 1631E Mercury in Water by Oxidation, Purge & Trap, and Cold Vapor AtomicFluorescence

10237204

AnalyteAnalyte CodeMercury1095

EPA 1664A Silica Gen Treated N-Hexane Extractable Material (Oil and Grease)10127603

AnalyteAnalyte CodeOil & Grease1860

EPA 180.1 Turbidity - Nephelometric10011402

AnalyteAnalyte CodeTurbidity2055

EPA 200.7 4.4 ICP - metals10013806

AnalyteAnalyte CodeAluminum1000Antimony1005Arsenic1010Barium1015Beryllium1020Bismuth1023Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Hardness (calc.)1760Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Molybdenum1100Nickel1105Potassium1125Selenium1140Silica as SiO21990Silicon1145

Page 25 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeSilver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190Zirconium1192

EPA 200.8 5.4 Metals by ICP-MS10014605

AnalyteAnalyte CodeAluminum1000Antimony1005Arsenic1010Barium1015Beryllium1020Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Hardness (calc.)1760Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Mercury1095Molybdenum1100Nickel1105Potassium1125Selenium1140Silicon1145Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190

EPA 218.6 Dissolved Hexavalent Chromium by Ion Chromatography10027802

AnalyteAnalyte CodeChromium VI1045

EPA 245.2 Mercury by Cold Vapor Atomic Absorption10037000

AnalyteAnalyte CodeMercury1095

EPA 300.0 Ion chromatography - anions.10053006

AnalyteAnalyte CodeBromate1535Bromide1540

Page 26 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeChlorate1570Chloride1575Chlorite1595Fluoride1730Nitrate as N1810Nitrate-nitrite1820Nitrite1835Nitrite as N1840Orthophosphate as P1870Phosphorus, total1910Sulfate2000

EPA 300.1 Ion chromatography - anions.10053608

AnalyteAnalyte CodeBromate1535Bromide1540Chlorate1570Chloride1575Chlorite1595Fluoride1730Nitrate as N1810Nitrite as N1840Orthophosphate as P1870Sulfate2000

EPA 3005A Acid Digestion of waters for Total Recoverable or Dissolved Metals10133207

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3010A Acid Digestion of Aqueous samples and Extracts for Total Metals10133605

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3050A Acid Digestion of Sediments, Sludges, and soils10135407

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3060A Alkaline Digestion for Hexavalent Chromium10136604

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 310.2 Alkalinity as CaCO3 - Colorimetric, Automated10055002

AnalyteAnalyte CodeAlkalinity as CaCO31505

EPA 335.4 Methods for the Determination of Inorganic Substances inEnvironmental Samples

10061208

AnalyteAnalyte CodeTotal cyanide1645

EPA 350.1 Ammonia Nitrogen - Colorimetric, Auto Phenate10063204

AnalyteAnalyte CodeAmmonia as N1515

Page 27 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 3510 Separatory Funnel Liquid-liquid extraction10137607

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3520 Continuous Liquid-liquid extraction10138406

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 353.2 Nitrate/Nitrite Nitrogen - Automated, Cadmium10067206

AnalyteAnalyte CodeKjeldahl nitrogen1790Nitrate as N1810Nitrate-nitrite1820Nitrite as N1840Total nitrate+nitrite1825

EPA 3535 Solid-Phase Extraction (SPE)10139205

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3540B Soxhlet Extraction10140008

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 3550 Ultrasonic Extraction10141409

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 365.1 Phosphorous - Colorimetric, Automated persulfate10069600

AnalyteAnalyte CodeOrthophosphate as P1870Phosphorus, total1910

EPA 420.1 Phenolics - Spectrophotometric, manual.10079206

AnalyteAnalyte CodeTotal phenolics1905

EPA 420.4 Phenolics, Total Recoverable by Semi-Automated Colorimetry10080203

AnalyteAnalyte CodeTotal phenolics1905

EPA 5030B Purge and trap for aqueous samples10153409

AnalyteAnalyte CodeExtraction/Preparation8031

EPA 6010B ICP - AES10155609

AnalyteAnalyte CodeAluminum1000Antimony1005

Page 28 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeArsenic1010Barium1015Beryllium1020Bismuth1023Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Hardness (calc.)1760Iron1070Lead1075Lithium1080Magnesium1085Manganese1090Molybdenum1100Nickel1105Potassium1125Selenium1140Silica as SiO21990Silicon1145Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190

EPA 602 Purgeable Aromatics by GC/PID Purge & Trap10102202

AnalyteAnalyte CodeBenzene4375Ethylbenzene4765m+p-xylene5240Methyl tert-butyl ether (MTBE)5000o-Xylene5250Toluene5140Xylene (total)5260

EPA 6020 Inductively Coupled Plasma-Mass Spectrometry10156000

AnalyteAnalyte CodeAluminum1000Antimony1005Arsenic1010Barium1015Beryllium1020Boron1025Cadmium1030Calcium1035Chromium1040Cobalt1050Copper1055Iron1070Lead1075Lithium1080Magnesium1085Manganese1090

Page 29 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeMercury1095Molybdenum1100Nickel1105Potassium1125Selenium1140Silver1150Sodium1155Strontium1160Thallium1165Tin1175Titanium1180Vanadium1185Zinc1190Zirconium1192

EPA 608 Organochlorine Pesticides & PCBs by GC/ECD10103603

AnalyteAnalyte Code4,4'-DDD73554,4'-DDE73604,4'-DDT7365Alachlor7005Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110alpha-Chlordane7240Aroclor-1016 (PCB-1016)8880Aroclor-1221 (PCB-1221)8885Aroclor-1232 (PCB-1232)8890Aroclor-1242 (PCB-1242)8895Aroclor-1248 (PCB-1248)8900Aroclor-1254 (PCB-1254)8905Aroclor-1260 (PCB-1260)8910Aroclor-1262 (PCB-1262)8912Aroclor-1268 (PCB-1268)8913Atrazine7065beta-BHC (beta-Hexachlorocyclohexane)7115Butachlor7160Chlordane (tech.)7250Chloroneb7265Chlorthalonil (Daconil)7310Dacthal (DCPA)8550delta-BHC7105Dieldrin7470Dimethazone (Clomazone)7473Endosulfan I7510Endosulfan II7515Endosulfan sulfate7520Endrin7540Endrin aldehyde7530Endrin ketone7535gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120gamma-Chlordane7245Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorocyclopentadiene6285Isodrin7725Kepone7740Malathion7770Methoxychlor7810Methyl parathion (Parathion, methyl)7825

Page 30 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeMetolachlor7835Metribuzin7845Mirex7870Parathion, ethyl7955Propachlor (Ramrod)8045Simazine8125Toxaphene (Chlorinated camphene)8250Trifluralin (Treflan)8295

EPA 610 (HPLC) Polynuclear Hydrocarbons by HPLC/UV-VIS10297004

AnalyteAnalyte Code1-Methylnaphthalene63802-Methylnaphthalene6385Acenaphthene5500Acenaphthylene5505Anthracene5555Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Chrysene5855Dibenz(a,h) anthracene5895Fluoranthene6265Fluorene6270Indeno(1,2,3-cd) pyrene6315Naphthalene5005Phenanthrene6615Pyrene6665

EPA 624 Volatile Organic Compounds by purge and trap GC/MS10107207

AnalyteAnalyte Code1,1,1,2-Tetrachloroethane51051,1,1-Trichloroethane51601,1,2,2-Tetrachloroethane51101,1,2-Trichloroethane51651,1-Dichloroethane46301,1-Dichloroethylene46401,1-Dichloropropene46701,2,3-Trichlorobenzene51501,2,3-Trichloropropane51801,2,4-Trichlorobenzene51551,2,4-Trimethylbenzene52101,2-Dibromoethane (EDB, Ethylene dibromide)45851,2-Dichlorobenzene46101,2-Dichloroethane (Ethylene dichloride)46351,2-Dichloropropane46551,3,5-Trimethylbenzene52151,3-Dichlorobenzene46151,3-Dichloropropane46601,4-Dichlorobenzene46201,4-Dioxane (1,4- Diethyleneoxide)47352,2-Dichloropropane46652-Butanone (Methyl ethyl ketone, MEK)44102-Chloroethyl vinyl ether45002-Chlorotoluene45352-Hexanone (MBK)48604-Chlorotoluene45404-Methyl-2-pentanone (MIBK)4995

Page 31 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeAcetone4315Acetonitrile4320Acrolein (Propenal)4325Acrylonitrile4340Allyl chloride (3-Chloropropene)4355Benzene4375Bromobenzene4385Bromochloromethane4390Bromodichloromethane4395Bromoform4400Carbon disulfide4450Carbon tetrachloride4455Chlorobenzene4475Chloroethane (Ethyl chloride)4485Chloroform4505cis-1,2-Dichloroethylene4645cis-1,3-Dichloropropene4680Dibromochloropropane4580Dibromofluoromethane4590Dibromomethane (Methylene bromide)4595Dichlorodifluoromethane (Freon-12)4625Ethyl methacrylate4810Ethylbenzene4765Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)4770Hexachlorobutadiene4835Hexachloroethane4840Iodomethane (Methyl iodide)4870Isobutyl alcohol (2-Methyl-1-propanol)4875Isopropylbenzene4900Methanol4930Methyl methacrylate4990Methyl tert-butyl ether (MTBE)5000Methylene chloride (Dichloromethane)4975Naphthalene5005n-Butyl alcohol (1-Butanol, n-Butanol)4425n-Butylbenzene4435Nitrobenzene5015n-Propylbenzene5090Pentachloroethane5035sec-Butylbenzene4440Styrene5100T-amylmethylether (TAME)4370tert-Butyl alcohol4420tert-Butylbenzene4445Tetrachloroethylene (Perchloroethylene)5115Toluene5140Total trihalomethanes5205trans-1,2-Dichloroethylene4700trans-1,3-Dichloropropylene4685Trichloroethene (Trichloroethylene)5170Trichlorofluoromethane (Fluorotrichloromethane, Freon 11)5175Vinyl acetate5225Vinyl chloride5235Xylene (total)5260

EPA 625 Base/Neutrals and Acids by GC/MS10300002

AnalyteAnalyte Code1,2,4,5-Tetrachlorobenzene67151,2,4-Trichlorobenzene51551,2-Dichlorobenzene4610

Page 32 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code1,2-Diphenylhydrazine62211,3-Dichlorobenzene46151,4-Dichlorobenzene46201-Chloronaphthalene57901-Naphthylamine64252,3,4,6-Tetrachlorophenol67352,4,5-Trichlorophenol68352,4,6-Trichlorophenol68402,4-Dichlorophenol60002,4-Dimethylphenol61302,4-Dinitrophenol61752,4-Dinitrotoluene (2,4-DNT)61852,6-Dichlorophenol60052,6-Dinitrotoluene (2,6-DNT)61902-Chloronaphthalene57952-Chlorophenol58002-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)63602-Methylnaphthalene63852-Methylphenol (o-Cresol)64002-Naphthylamine64302-Nitroaniline64602-Nitrophenol64903 & 4 Methylphenol64123,3'-Dichlorobenzidine59453-Methylcholanthrene63553-Methylphenol (m-Cresol)64053-Nitroaniline64654,4'-DDD73554,4'-DDE73604,4'-DDT73654-Aminobiphenyl55404-Bromophenyl phenyl ether (BDE-3)56604-Chloro-3-methylphenol57004-Chloroaniline57454-Chlorophenyl phenylether58254-Dimethyl aminoazobenzene61054-Methylphenol (p-Cresol)64104-Nitroaniline64704-Nitrophenol65007,12-Dimethylbenz(a) anthracene6115Acenaphthene5500Acenaphthylene5505Acetophenone5510Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110Aniline5545Anthracene5555Benzidine5595Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Benzoic acid5610Benzyl alcohol5630beta-BHC (beta-Hexachlorocyclohexane)7115bis(2-Chloroethoxy)methane5760bis(2-Chloroethyl) ether5765bis(2-Chloroisopropyl) ether5780bis(2-Ethylhexyl)adipate6062Butyl benzyl phthalate5670

Page 33 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeCarbazole5680Carbofuran (Furaden)7205Chrysene5855Coelution - 3-Chlorophenol + 4-Chlorophenol8906delta-BHC7105Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)6065Diallate7405Dibenz(a,h) anthracene5895Dibenzofuran5905Dieldrin7470Diethyl phthalate6070Dimethoate7475Dimethyl phthalate6135Di-n-butyl phthalate5925Di-n-octyl phthalate6200Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)8620Diphenylamine6205Disulfoton8625Endosulfan I7510Endosulfan II7515Endosulfan sulfate7520Endrin7540Ethyl methanesulfonate6260Fluoranthene6265Fluorene6270gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorobutadiene4835Hexachlorocyclopentadiene6285Hexachloroethane4840Indeno(1,2,3-cd) pyrene6315Isophorone6320Methoxychlor7810Methyl methanesulfonate6375Methyl parathion (Parathion, methyl)7825Naphthalene5005Nitrobenzene5015n-Nitrosodimethylamine6530n-Nitroso-di-n-butylamine5025n-Nitrosodi-n-propylamine6545n-Nitrosodiphenylamine6535n-Nitrosomethylethalamine6550n-Nitrosopiperidine6560Parathion, ethyl7955Pentachlorobenzene6590Pentachloronitrobenzene6600Pentachlorophenol6605Phenacetin6610Phenanthrene6615Phenol6625Phorate7985Pronamide (Kerb)6650Pyrene6665Pyridine5095

EPA 7199 Determination of Hexavalent Chromium in Drinking Water,Groundwater and Industrial Wastewater Effluents by IonChromatography

10163005

AnalyteAnalyte CodeChromium VI1045

Page 34 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

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01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 7470A Mercury in Liquid Waste by Cold Vapor Atomic Absorption10165807

AnalyteAnalyte CodeMercury1095

EPA 7471A Mercury in Solid Waste by Cold Vapor Atomic Absorption10166208

AnalyteAnalyte CodeMercury1095

EPA 8015B Non-halogenated organics using GC/FID10173601

AnalyteAnalyte CodeDiesel range organics (DRO)9369Gasoline range organics (GRO)9408Jet Fuel9488Kerosene9409

EPA 8021B Aromatic and Halogenated Volatiles by GC with PID and/or ECD Purge& Trap

10174808

AnalyteAnalyte CodeBenzene4375Ethylbenzene4765m+p-xylene5240Methyl tert-butyl ether (MTBE)5000o-Xylene5250Toluene5140Xylene (total)5260

EPA 8081A Organochlorine Pesticides by GC/ECD10178606

AnalyteAnalyte Code4,4'-DDD73554,4'-DDE73604,4'-DDT7365Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110alpha-Chlordane7240beta-BHC (beta-Hexachlorocyclohexane)7115Chlordane (tech.)7250delta-BHC7105Dieldrin7470Endosulfan I7510Endosulfan II7515Endosulfan sulfate7520Endrin7540Endrin aldehyde7530Endrin ketone7535gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120gamma-Chlordane7245Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorocyclopentadiene6285Methoxychlor7810Toxaphene (Chlorinated camphene)8250

EPA 8082 Polychlorinated Biphenyls (PCBs) by GC/ECD10179007

AnalyteAnalyte CodeAroclor-1016 (PCB-1016)8880

Page 35 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeAroclor-1221 (PCB-1221)8885Aroclor-1232 (PCB-1232)8890Aroclor-1242 (PCB-1242)8895Aroclor-1248 (PCB-1248)8900Aroclor-1254 (PCB-1254)8905Aroclor-1260 (PCB-1260)8910Aroclor-1262 (PCB-1262)8912Aroclor-1268 (PCB-1268)8913Decachlorobiphenyl (BZ-209)9105

EPA 8151A Chlorinated Herbicides by GC/ECD10183207

AnalyteAnalyte Code2,4,5-T86552,4-D85452,4-DB85603,5-Dichlorobenzoic acid86004-Nitrophenol6500Acifluorfen8505Bentazon8530Chloramben8540Dacthal (DCPA)8550Dalapon8555Dicamba8595Dichloroprop (Dichlorprop)8605Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)8620Garlon (Triclopyr)7650MCPA7775MCPP7780Pentachlorophenol6605Picloram8645Silvex (2,4,5-TP)8650

EPA 8260B Volatile Organic Compounds by purge and trap GC/MS10184802

AnalyteAnalyte Code1,1,1,2-Tetrachloroethane51051,1,1-Trichloroethane51601,1,2,2-Tetrachloroethane51101,1,2-Trichloroethane51651,1-Dichloroethane46301,1-Dichloroethylene46401,1-Dichloropropene46701,2,3-Trichlorobenzene51501,2,3-Trichloropropane51801,2,4-Trichlorobenzene51551,2,4-Trimethylbenzene52101,2-Dibromoethane (EDB, Ethylene dibromide)45851,2-Dichlorobenzene46101,2-Dichloroethane (Ethylene dichloride)46351,2-Dichloropropane46551,3,5-Trimethylbenzene52151,3-Dichlorobenzene46151,3-Dichloropropane46601,4-Dichlorobenzene46201,4-Dioxane (1,4- Diethyleneoxide)47352,2-Dichloropropane46652-Butanone (Methyl ethyl ketone, MEK)44102-Chloroethyl vinyl ether45002-Chlorotoluene45352-Hexanone (MBK)4860

Page 36 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code4-Chlorotoluene45404-Methyl-2-pentanone (MIBK)4995Acetone4315Acetonitrile4320Acrolein (Propenal)4325Acrylonitrile4340Allyl chloride (3-Chloropropene)4355Benzene4375Bromobenzene4385Bromochloromethane4390Bromodichloromethane4395Bromoethane (Ethyl Bromide)4397Bromoform4400Carbon disulfide4450Carbon tetrachloride4455Chlorobenzene4475Chlorodibromomethane4575Chloroethane (Ethyl chloride)4485Chloroform4505cis-1,2-Dichloroethylene4645cis-1,3-Dichloropropene4680Dibromochloropropane4580Dibromomethane (Methylene bromide)4595Dichlorodifluoromethane (Freon-12)4625Dichlorofluoromethane (Freon 21)4627Ethyl methacrylate4810Ethylbenzene4765Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane)4770Gasoline range organics (GRO)9408Hexachlorobutadiene4835Hexachloroethane4840Iodomethane (Methyl iodide)4870Isobutyl alcohol (2-Methyl-1-propanol)4875Isopropylbenzene4900Methanol4930Methyl acrylate4945Methyl chloride (Chloromethane)4960Methyl methacrylate4990Methyl tert-butyl ether (MTBE)5000Methylene chloride (Dichloromethane)4975Naphthalene5005n-Butyl alcohol (1-Butanol, n-Butanol)4425n-Butylbenzene4435Nitrobenzene5015n-Propylbenzene5090Pentachloroethane5035sec-Butylbenzene4440Styrene5100T-amylmethylether (TAME)4370tert-Butyl alcohol4420tert-Butylbenzene4445Tetrachloroethylene (Perchloroethylene)5115Toluene5140trans-1,2-Dichloroethylene4700trans-1,3-Dichloropropylene4685Trichloroethene (Trichloroethylene)5170Trichlorofluoromethane (Fluorotrichloromethane, Freon 11)5175Vinyl acetate5225Vinyl chloride5235Xylene (total)5260

Page 37 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 8270C Semivolatile Organic compounds by GC/MS10185805

AnalyteAnalyte Code1,2,4,5-Tetrachlorobenzene67151,2,4-Trichlorobenzene51551,2-Dichlorobenzene46101,2-Diphenylhydrazine62211,3-Dichlorobenzene46151,4-Dichlorobenzene46201-Chloronaphthalene57901-Naphthylamine64252,3,4,6-Tetrachlorophenol67352,4,5-Trichlorophenol68352,4,6-Trichlorophenol68402,4-Dichlorophenol60002,4-Dimethylphenol61302,4-Dinitrophenol61752,4-Dinitrotoluene (2,4-DNT)61852,6-Dichlorophenol60052,6-Dinitrotoluene (2,6-DNT)61902-Chloronaphthalene57952-Chlorophenol58002-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)63602-Methylnaphthalene63852-Methylphenol (o-Cresol)64002-Naphthylamine64302-Nitroaniline64602-Nitrophenol64902-Picoline (2-Methylpyridine)50503,3'-Dichlorobenzidine59453-Methylcholanthrene63553-Methylphenol (m-Cresol)64053-Nitroaniline64654,4'-DDD73554,4'-DDE73604,4'-DDT73654-Aminobiphenyl55404-Bromophenyl phenyl ether (BDE-3)56604-Chloro-3-methylphenol57004-Chloroaniline57454-Chlorophenyl phenylether58254-Dimethyl aminoazobenzene61054-Methylphenol (p-Cresol)64104-Nitroaniline64704-Nitrophenol65007,12-Dimethylbenz(a) anthracene6115a-a-Dimethylphenethylamine6125Acenaphthene5500Acenaphthylene5505Acetophenone5510Aldrin7025alpha-BHC (alpha-Hexachlorocyclohexane)7110alpha-Chlordane7240Aniline5545Anthracene5555Benzidine5595Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585

Page 38 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeBenzoic acid5610Benzyl alcohol5630beta-BHC (beta-Hexachlorocyclohexane)7115bis(2-Chloroethoxy)methane5760bis(2-Chloroethyl) ether5765bis(2-Chloroisopropyl) ether5780Butyl benzyl phthalate5670Captafol7185Captan7190Carbaryl (Sevin)7195Carbazole5680Carbofuran (Furaden)7205Carbophenothion7220Chrysene5855delta-BHC7105Demeton-o7395Demeton-s7385Di(2-ethylhexyl) phthalate (bis(2-Ethylhexyl)phthalate, DEHP)6065Diallate7405Dibenz(a, j) acridine5900Dibenz(a,h) anthracene5895Dibenzofuran5905Dichlone7430Dieldrin7470Diethyl phthalate6070Dimethoate7475Dimethyl phthalate6135Di-n-butyl phthalate5925Di-n-octyl phthalate6200Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)8620Diphenylamine6205Disulfoton8625Endosulfan I7510Endosulfan II7515Endosulfan sulfate7520Endrin7540Endrin aldehyde7530Endrin ketone7535EPN7550Ethion7565Ethyl methanesulfonate6260Fluoranthene6265Fluorene6270gamma-BHC (Lindane, gamma-HexachlorocyclohexanE)7120gamma-Chlordane7245Heptachlor7685Heptachlor epoxide7690Hexachlorobenzene6275Hexachlorobutadiene4835Hexachlorocyclopentadiene6285Hexachloroethane4840Indeno(1,2,3-cd) pyrene6315Isophorone6320Malathion7770Methoxychlor7810Methyl methanesulfonate6375Methyl parathion (Parathion, methyl)7825Mevinphos7850Naphthalene5005Nitrobenzene5015n-Nitrosodimethylamine6530

Page 39 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Coden-Nitroso-di-n-butylamine5025n-Nitrosodi-n-propylamine6545n-Nitrosodiphenylamine6535n-Nitrosomethylethalamine6550n-Nitrosopiperidine6560Parathion, ethyl7955Pentachlorobenzene6590Pentachloronitrobenzene6600Pentachlorophenol6605Phenacetin6610Phenanthrene6615Phenol6625Phorate7985Pronamide (Kerb)6650Pyrene6665Pyridine5095Sulfotepp8155Tetraethyl pyrophosphate (TEPP)8210Trifluralin (Treflan)8295

EPA 8280A Polychlorinated Dibenzo-p-Dioxins and PolychlorinatedDibenzofurans by GC/HRMS

10186808

AnalyteAnalyte Code1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)95161,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)95191,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-hpcdf)94201,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)94261,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-hpcdf)94231,2,3,4,7,8-Hexachlorodibenzofuran (1,2,3,4,7,8-Hxcdf)94711,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (1,2,3,4,7,8-Hxcdd)94531,2,3,6,7,8-Hexachlorodibenzofuran (1,2,3,6,7,8-Hxcdf)94741,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)94561,2,3,7,8,9-Hexachlorodibenzofuran (1,2,3,7,8,9-Hxcdf)94771,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (1,2,3,7,8,9-Hxcdd)94591,2,3,7,8-Pentachlorodibenzofuran (1,2,3,7,8-Pecdf)95431,2,3,7,8-Pentachlorodibenzo-p-dioxin (1,2,3,7,8-Pecdd)95402,3,4,6,7,8-Hexachlorodibenzofuran94802,3,4,7,8-Pentachlorodibenzofuran95492,3,7,8-Tetrachlorodibenzo- p-dioxin (2,3,7,8-TCDD)96182,3,7,8-Tetrachlorodibenzofuran9612Hpcdd, total9438Hpcdf, total9444Hxcdd, total9468Hxcdf, total9483Pecdd, total9555Pecdf, total9552TCDD, total9609TCDF, total9615

EPA 8290 Polychlorinated Dibenzodioxins (PCDDs) and PolychlorinatedDibenzofurans (PCDFs) by GC/HRMS

10187209

AnalyteAnalyte Code1,2,3,4,6,7,8,9-Octachlorodibenzofuran (OCDF)95161,2,3,4,6,7,8,9-Octachlorodibenzo-p-dioxin (OCDD)95191,2,3,4,6,7,8-Heptachlorodibenzofuran (1,2,3,4,6,7,8-hpcdf)94201,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin (1,2,3,4,6,7,8-hpcdd)94261,2,3,4,7,8,9-Heptachlorodibenzofuran (1,2,3,4,7,8,9-hpcdf)94231,2,3,4,7,8-Hexachlorodibenzofuran (1,2,3,4,7,8-Hxcdf)94711,2,3,4,7,8-Hexachlorodibenzo-p-dioxin (1,2,3,4,7,8-Hxcdd)94531,2,3,6,7,8-Hexachlorodibenzofuran (1,2,3,6,7,8-Hxcdf)94741,2,3,6,7,8-Hexachlorodibenzo-p-dioxin(1,2,3,6,7,8-Hxcdd)9456

Page 40 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte Code1,2,3,7,8,9-Hexachlorodibenzofuran (1,2,3,7,8,9-Hxcdf)94771,2,3,7,8,9-Hexachlorodibenzo-p-dioxin (1,2,3,7,8,9-Hxcdd)94591,2,3,7,8-Pentachlorodibenzofuran (1,2,3,7,8-Pecdf)95431,2,3,7,8-Pentachlorodibenzo-p-dioxin (1,2,3,7,8-Pecdd)95402,3,4,6,7,8-Hexachlorodibenzofuran94802,3,4,7,8-Pentachlorodibenzofuran95492,3,7,8-Tetrachlorodibenzo- p-dioxin (2,3,7,8-TCDD)96182,3,7,8-Tetrachlorodibenzofuran9612Hpcdd, total9438Hpcdf, total9444Hxcdd, total9468Hxcdf, total9483Pecdd, total9555Pecdf, total9552TCDD, total9609TCDF, total9615

EPA 8310 Polynuclear Aromatic Hydrocarbons by HPLC/UV-VIS10187607

AnalyteAnalyte Code1-Methylnaphthalene63802-Methylnaphthalene6385Acenaphthene5500Acenaphthylene5505Anthracene5555Benzo(a)anthracene5575Benzo(a)pyrene5580Benzo(g,h,i)perylene5590Benzo(k)fluoranthene5600Benzo[b]fluoranthene5585Chrysene5855Dibenz(a,h) anthracene5895Fluoranthene6265Fluorene6270Indeno(1,2,3-cd) pyrene6315Naphthalene5005Phenanthrene6615Pyrene6665

EPA 8315A Determination of Carbonyl Compounds by HPLC/UV-VIS10188008

AnalyteAnalyte Code2,5-Dimethylbenzaldehyde6110Acetaldehyde4300Acetone4315Acrolein (Propenal)4325Benzaldehyde5570Butylaldehyde (Butanal)4430Crotonaldehyde4545Cyclohexanone4560Decanal4565Formaldehyde4815Heptanal4820Hexanaldehyde (Hexanal)3825Isovaleraldehyde6330m-Tolualdehyde (1,3-Tolualdehyde)5125n-Octaldehyde (Octanal)9525Nonanal6575o-Tolualdehyde (1,2-Tolualdehyde)6755Propanal (Propionaldehyde)6935p-Tolualdehyde (1,4-Tolualdehyde)6760

Page 41 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

AnalyteAnalyte CodeValeraldehyde (Pentanal, Pentanaldehyde)4040

EPA 8316 Acrylamide, Acrylonitrile and Acrolein by High Performance LiquidChromatography (HPLC)

10188202

AnalyteAnalyte CodeAcrolein (Propenal)4325Acrylamide4330Acrylonitrile4340

EPA 8318 N-Methylcarbamates by HPLC/UV-VIS10188406

AnalyteAnalyte Code3-Hydroxycarbofuran7710Aldicarb (Temik)7010Aldicarb sulfone7015Aldicarb sulfoxide7020Bendiocarb7085Carbaryl (Sevin)7195Carbofuran (Furaden)7205Dioxacarb9384Formetanate hydrochloride9405m-Cumenyl methylcarbamate7335Methiocarb (Mesurol)7800Methomyl (Lannate)7805Metolcarb7840Oxamyl7940Promecarb8025Propoxur (Baygon)8080Thiodicarb8225

EPA 8330A Nitroaromatics and Nitramines by High Performance LiquidChromatography (HPLC)

10190008

AnalyteAnalyte Code1,3,5-Trinitrobenzene (1,3,5-TNB)68851,3-Dinitrobenzene (1,3-DNB)61602,4,6-Trinitrotoluene (2,4,6-TNT)96512,4-Dinitrotoluene (2,4-DNT)61852,6-Dinitrotoluene (2,6-DNT)61902-Amino-4,6-dinitrotoluene (2-am-dnt)93032-Nitrotoluene95073-Nitrotoluene95104-Amino-2,6-dinitrotoluene (4-am-dnt)93064-Nitrotoluene9513Methyl-2,4,6-trinitrophenylnitramine (tetryl)6415Nitrobenzene5015Octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine (HMX)9522RDX (hexahydro-1,3,5-trinitro-1,3,5-triazine)9432

EPA 9012A Total and Amenable Cyanide (automated colorimetric with off-linedistillation)

10193405

AnalyteAnalyte CodeAmenable cyanide1510Cyanide1635Total cyanide1645

EPA 9040B pH Electrometric Measurement10197203

AnalyteAnalyte CodepH1900

Page 42 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

EPA 9045C Soil and Waste pH10198400

AnalyteAnalyte CodepH1900

SM 2120 B 20th ED Color by Visual Comparison20224004

AnalyteAnalyte CodeColor1605

SM 2130 B 20th ED Turbidity by Nephelometric Determination20042404

AnalyteAnalyte CodeTurbidity2055

SM 2310 B 20th ED Acidity by Titration20044206

AnalyteAnalyte CodeAcidity, as CaCO31500

SM 2320 B 20th ED Alkalinity by Titration20045209

AnalyteAnalyte CodeAlkalinity as CaCO31505Corrosivity1615

SM 2340 B 20th ED Hardness by calculation20046202

AnalyteAnalyte CodeCalcium hardness as CaCO31550Hardness1750Total hardness as CaCO31755

SM 2510 B 20th ED Conductivity by Probe20048208

AnalyteAnalyte CodeConductivity1610

SM 2540 B 20th ED Total Solids20049007

AnalyteAnalyte CodeResidue-total1950

SM 2540 C 20th ED Total Dissolved Solids20050004

AnalyteAnalyte CodeResidue-filterable (TDS)1955

SM 2540 D 20th ED Total Suspended Solids20050800

AnalyteAnalyte CodeResidue-nonfilterable (TSS)1960

SM 2540 F 20th ED Settleable Solids20051803

AnalyteAnalyte CodeResidue-settleable1965

Page 43 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

SM 4500-Cl D 20th ED Chlorine by Potentiometry20079601

AnalyteAnalyte CodeChloride1575Residual free chlorine1945

SM 4500-Cl G 20th ED Residual Chlorine by DPD Colorimetric Determination20081203

AnalyteAnalyte CodeChlorine1580Residual free chlorine1945Total residual chlorine1940

SM 4500-Cl¯ E 19th ED Chloride by Automated Ferricyanide Method20086004

AnalyteAnalyte CodeChloride1575

SM 4500-CN E 20th ED Cyanide by Colorimetric Determination20092404

AnalyteAnalyte CodeCyanide1635Total cyanide1645

SM 4500-CN¯ C 21st ED Cyanide by Total Cyanide after Distillation20095403

AnalyteAnalyte CodeCyanide1635

SM 4500-CN¯ G 21st ED Cyanide by Cyanides Amenable to Chlorination after Distillation20097001

AnalyteAnalyte CodeAmenable cyanide1510

SM 4500-H+ B 20th ED pH by Probe20104807

AnalyteAnalyte CodepH1900

SM 4500-O G 20th ED Dissolved Oxygen by Membrane Electrode Method20121204

AnalyteAnalyte CodeOxygen, dissolved1880

SM 4500-S2¯ D 20th ED Sulfide by Methylene Blue Method20125400

AnalyteAnalyte CodeSulfide2005

SM 5210 B 20th ED Biochemical Oxygen Demand, 5-Day (BOD5)20134809

AnalyteAnalyte CodeBiochemical oxygen demand1530Carbonaceous BOD, CBOD1555

SM 5220 D 20th ED Chemical Oxygen Demand by Closed Reflux and ColorimetricDetermination

20136407

AnalyteAnalyte CodeChemical oxygen demand1565

Page 44 of 45

ORELAP Fields of Accreditation

Mccampbell Analytical Inc.1534 Willow Pass RoadPittsburg CA 94565

4033ORELAP ID:

EPA CODE: CA00371

Certificate:

Issue Date: Expiration Date:

this list supercedes all previous lists for this certificate number.Customers. Please verify the current accreditation standing with ORELAP.As of

01/30/2014 01/29/2015

4033 - 001

01/30/2014

SM 5310 B 20th ED Total Organic Carbon by Combustion Infra-red Method20137400

AnalyteAnalyte CodeDissolved organic carbon (DOC)1710Total organic carbon2040

SM 5520 B 20th ED Oil and Grease by Extraction and Gravimetric Determination20141202

AnalyteAnalyte Coden-Hexane Extractable Material (O&G)1803Oil & Grease1860

SM 5540 C 20th ED Surfactants as MBAS20144609

AnalyteAnalyte CodeSurfactants - MBAS2025

SM 5550 B 20th ED Tannin and Lignin20145306

AnalyteAnalyte CodeTannin & Lignin9597

WA EPH Extractable Petroleum Hydrocarbons60015001

AnalyteAnalyte CodeDiesel range organics (DRO)9369EPH Aliphatic >C10-C126211EPH Aliphatic >C12-C166212EPH Aliphatic >C16-C216214EPH Aliphatic >C21-C346216EPH Aliphatic C8-C106220EPH Aliphatic C9-C186222EPH Aromatic >C10-C126224EPH Aromatic >C12-C166226EPH Aromatic >C16-C216228EPH Aromatic >C21-C346231EPH Aromatic C8-C106236

WA VPH Volatile Petroleum Hydrocarbons (VPH) by GC/PID Purge & Trap60015056

AnalyteAnalyte CodeBenzene4375Ethylbenzene4765Gasoline range organics (GRO)9408m+p-xylene5240Methyl tert-butyl ether (MTBE)5000n-Hexane4855o-Xylene5250Toluene5140VPH Aliphatic >C10-C125300VPH Aliphatic >C6-C85301VPH Aliphatic >C8-C105302VPH Aliphatic C5-C65303VPH Aromatic >C10-C125308VPH Aromatic >C12-C135309VPH Aromatic >C8-C105310Xylene (total)5260

Page 45 of 45