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89 CHAPTER - 5 EN Series Steels Surface finish and surface hardness of the components play vital role in quality of products/components, in general and failure resistance, in particular. One of the finishing process involving surface plastic deformation that introduce compressive residual stresses and thereby improve fatigue resistance is “Burnishing”. Even though the burnishing process is widely employed, its process parameters were not systematically studied till date and not fully established for various important structural materials. The burnishing process parameters include force, speed, feed, and number of tool passes. In the present study, the data obtained from systematically conducted burnishing experiments are correlated with theoretical design using Taguchi method in case of EN series steels (EN 8, EN 24 and EN 31). The surface characterization employed includes optical microscopy, micro hardness and magnitude of residual stress. The study revealed a one- to-one correlation between burnishing depth, increase in average micro hardness and magnitude of compressive residual stresses and a peak in all these three at intermittent extent of burnishing (either after first or second pass) in all the three alloy steels. One of the characterization of materials that was study in the present thesis pertained to alloy steels. Alloy steels are defined as a steels alloyed with variety of elements in total amounts ranging from

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CHAPTER - 5

EN Series Steels

Surface finish and surface hardness of the components play vital

role in quality of products/components, in general and failure

resistance, in particular. One of the finishing process involving surface

plastic deformation that introduce compressive residual stresses and

thereby improve fatigue resistance is “Burnishing”. Even though the

burnishing process is widely employed, its process parameters were

not systematically studied till date and not fully established for various

important structural materials. The burnishing process parameters

include force, speed, feed, and number of tool passes. In the present

study, the data obtained from systematically conducted burnishing

experiments are correlated with theoretical design using Taguchi

method in case of EN series steels (EN 8, EN 24 and EN 31). The

surface characterization employed includes optical microscopy, micro

hardness and magnitude of residual stress. The study revealed a one-

to-one correlation between burnishing depth, increase in average

micro hardness and magnitude of compressive residual stresses and a

peak in all these three at intermittent extent of burnishing (either after

first or second pass) in all the three alloy steels.

One of the characterization of materials that was study in the

present thesis pertained to alloy steels. Alloy steels are defined as a

steels alloyed with variety of elements in total amounts ranging from

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90

1% to 50% by weight to improve their mechanical properties. These

are classified as low alloy and high alloy steels. The steels with alloy

contains lower than 4-5% are considered as low alloy steels while

those higher than 8% alloying elements are called high alloy steels.

The commonly employed elements in these steels include Mn (most

common), Ni, Cr, Mo, V, Si and Boron, less commonly used alloying

elements include Al, Co, Cu, Ce, Nb, Ti, W, Sn and Zr. These steels

find wide range of applications such as turbine blades in jet engines,

space crafts and components for nuclear reactors and also find

applications in electrical motors and transformers. Some of the

commonly used alloy steels and their equivalent grades are given in

Table 5.1. The standard chemical composition of EN series steels are

given in table 5.2.

Table 5.1: Alloy designations of select Engineering Materials

Equivalent Grades

InternalStandard BS DIN IS EN SAE/AISI

EN18 530A40 37Cr4 40Cr1 EN18 5140

EN24 817M40 34CrNiMo6 40NiCr4Mo3 EN24 4340

EN19C 709M40 - 40Cr4Mo3 EN19C 4140, 4142

EN19 709M40 42Cr4Mo2 40Cr4Mo3 EN19 4140, 4142

EN18D 530A40 37Cr4 40Cr1 EN18D 5140

EN18C 530A40 37Cr4 40Cr1 EN18C 5140

EN353 815M17 - 15NiCr1Mo12 EN353 -

EN18A 530A40 37Cr4 40Cr1 EN18A 5140

EN354 820M17 - 15NIVCr1Mo15 EN354 4320

27C15 - 28Mn6 27C15 - 1527

20MnCr5 - 20MnCr5 20MnCr1 - -

20Mn2 150M28 - 20Mn2 EN14A 1524

16MnCr5 - 16MnCr5 17Mn1Cr95 - 5120

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15Cr3 523A14 15Cr3 15Cr65 EN206 5015

FILESTEEL - - - - -

EN18B 530A40 37Cr4 40Cr1 EN18B 5140

SCM420 708M20 - - - -

SAE8620 805M20 - 20NiCrMo2 EN362 SAE8620

Table 5.2: Chemical composition of EN series steels

C Mn Si S P Cr Ni Mo

EN 8 0.35 - 0.45 0.60 -1.0 0.10 0.35 0.05 max 0.05 max - - -

EN 8D 0.40 -0.45 0.7 - 0.9 0.05 - .35 0.06 max 0.06 max - - -

EN 9 0.50 - 0.60 0.5 - 0.8 0.05 - .35 0.04 max 0.04 max - - -

EN 15 0.30 - 0.40 1.3 - 1.7 0.10 - .35 0.04 max 0.04 max - - -

EN 16 0.30 - 0.40 1.3 - 1.8 0.10 - .35 0.04 0.04 - - 0.2 - 0.3

EN 18 0.35 - 0.45 0.6 - 0.95 0.10 - .35 0.04 0.04 0.85 - 1.15 - -

EN 19 0.35 - 0.45 0.5 - 0.8 0.10 - .35 0.04 0.04 0.90 - 1.4 - 0.2 - 0.4

EN 24 0.35 - 0.45 0.45 - 0.7 0.10 - .35 0.04 0.04 0.90 - 1.4 1.30 - 1.8 0.2 - 0.4

EN 25 0.27 - 0.35 0.5 - 0.7 0.10 - .35 0.04 0.04 0.50 - 0.80 2.3 - 2.8 0.4 - 0.7

EN 31 0.90 - 1.2 0.3 - 0.75 0.10 - .35 0.04 0.04 1.0 - 1.6 - -

EN 36B 0.12 - 0.18 0.30 - 0.60 0.10 - .35 0.04 0.04 0.60 - 1.1 3.0 - 3.75

EN 36C 0.12 - 0.18 0.3 - 0.6 0.10 - .35 0.04 0.04 0.60 - 1.1 3.0 - 3.75 0.10 - 0.25

EN 41B 0.35 - 0.45 0.6 max 0.10 - .45 0.04 0.04 1.5 - 1.8 0.40 max 0.10 - 0.25

EN 42 0.70 - 0.85 0.55 - 0.75 0.10 - .40 0.04 0.04 - - -

EN 45A 0.55 - 0.65 0.7 - 1.0 1.70 - 2.0 0.04 0.04 - - -

EN 47 0.45 - 0.55 0.5 - 0.8 0.50 max 0.04 0.04 0.80 - 1.2 - -

EN 48A 0.50 - 0.60 0.6 - 0.9 1.35 - 1.65 0.04 0.04 0.55 - 0.85 - -

EN 353 0.20 max 0.5 - 1.0 0.35 max 0.04 0.04 0.75 - 1.25 1.0 - 1.5 0.08 - 0.15

EN 354 0.20 max 0.5 - 1.0 0.35 max 0.04 0.04 0.75 - 1.25 1.5 - 2.0 0.1 -0 .2

5.1. Experimental Details

In order to establish the clear picture of burnishing process, a

series of experiments were conducted on metals which find wide range

of industrial applications, such as EN 8, EN 24 and EN 31 alloy steels.

In these experiments, the work pieces were burnished after turning on

lathe, keeping the roller burnishing tool fixed in the lathe tool

dynamometer. The dynamometer is employed to measure three force

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components, along x, y and z directions (force in z direction is taken

as burnishing force).

5.1.1. Materials

The work piece materials are EN 8, EN 24 and EN 31 (alloy

steels) and the nominal composition of the experimental materials is

given in Table 5.3. All the three alloy steels are in quenched

(hardened) and tempered condition.

Table 5.3: Chemical composition of the experimental materials

MaterialComposition, in Wt. %

C Si Mn Cr Ni S P

EN 8 0.41 0.204 0.70 - - 0.02 0.026

EN 24 0.37 0.265 0.64 1.1 0.225 0.023 0.025

EN 31 1.01 0.30 0.78 0.76 - 0.024 0.028

5.2. Results and Discussion

5.2.1. Surface roughness

The values of surface finish, a direct measurement of surface

roughness before and after burnishing as a function of burnishing

speed and burnishing feed are given in Table 5.4 and 5.5, respectively.

The optimal forces for EN 8, EN 24 and EN 31 are 210N, 170N and

200N respectively. The feed for all materials is taken as 0.032 mm/rev

From these data (data in Tables 5.4 and 5.5 and Figs. 5.1 and 5.2)

optimal speed and feed values which result in highest increase in

surface finish are determined and the same are given in Table 5.6. The

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variation in the extent of improvement in the surface finish for EN

series steels obtained in the present investigation (for that matter, for

any other material) depends upon microstructural features and the

levels of hardness and/or strength (in the present case microhardness

values).

Table 5.4: Comparison of surface finish values before and afterburnishing for a 30 mm diameter work piece of alloy steels as afunction of burnishing speed.

MaterialBurnishing

speed(m/min)

Surfacefinish beforeburnishing

Ra (µm)

Surface finish afterburnishing Ra (µm)

% increase insurface finish

Firstpass

Secondpass

Thirdpass

Firstpass

Secondpass

Thirdpass

EN 8

51 1.32 0.10 0.11 0.17 92.42 91.66 87.121

34 1.62 0.43 0.38 0.23 91.98 76.54 85.80

22 1.39 0.33 0.34 0.19 76.26 75.54 86.34

14 1.31 1.04 0.92 0.35 20.61 29.77 73.28

9 1.32 0.24 0.19 0.22 81.81 85.60 83.33

EN 24

51 2.00 0.25 0.27 0.56 87.50 86.50 72.00

34 3.88 0.36 0.15 0.26 90.72 96.13 93.30

22 3.92 0.18 0.17 0.27 95.41 95.66 93.11

14 3.48 0.48 0.62 0.90 86.20 82.18 74.14

9 3.71 0.53 0.51 0.92 85.72 86.25 75.20

EN 31

51 0.99 0.62 0.38 0.92 37.37 61.61 07.07

34 0.81 0.11 0.13 0.18 86.45 84.00 77.77

22 0.98 0.28 0.20 0.12 71.43 79.60 87.75

14 1.18 0.23 0.19 0.21 80.51 83.90 82.20

9 0.77 0.20 0.22 0.70 74.02 71.43 09.09

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Table 5.5 Comparison of surface finish values before and afterburnishing for a 30 mm diameter work piece of alloy steels as afunction of burnishing feed.

MaterialBurnishing

feedmm/rev

Surfacefinish beforeburnishing

Ra (µm)

Surface finish afterburnishing Ra (µm)

% increase insurface finish

22m/min

34m/min

51m/min

22m/min

34m/min

51m/min

EN 8

0.111 1.32 0.75 1.11 0.67 43.18 15.90 49.24

0.095 1.62 0.33 1.08 0.92 79.63 33.33 43.21

0.063 1.31 0.57 0.77 1.09 56.48 41.22 16.80

0.032 1.32 0.19 0.43 0.10 85.60 67.42 92.42

EN 24

0.111 2.00 0.25 0.37 1.70 87.5 81.50 15.00

0.095 3.88 0.54 0.22 0.97 86.08 94.32 75.00

0.063 3.92 0.42 0.32 2.18 89.28 90.45 44.39

0.032 1.8 0.18 0.36 0.25 90.00 80.00 86.11

EN 31

0.111 0.99 0.33 0.19 0.75 66.66 80.80 24.24

0.095 0.81 0.34 0.13 0.44 58.02 83.95 45.68

0.063 0.98 0.72 0.20 0.51 26.53 79.59 47.95

0.032 1.18 0.28 0.11 0.62 76.27 90.67 47.45

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Fig. 5.1: Variation of burnishing speed with % increase in surface finishfor different passes in (a) EN 8 (b) EN 24 and (c) EN 31 alloy steels.

10 20 30 40 5060

70

80

90

100 1st pass 2nd pass 3rd pass

Speed, m/min

% in

crea

se in

sur

face

fini

sh

(b) EN 24

10 20 30 40 500

10

20

30

40

50

60

70

80

90

100 1st pass 2nd pass 3rd pass

Speed, m/min

% in

crea

se in

sur

face

fini

sh

(c) EN 31

10 20 30 40 5010

20

30

40

50

60

70

80

90

100

1st pass 2nd pass 3rd pass

Speed, m/min

% in

crea

se in

sur

face

fini

sh(a) EN 8

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Fig. 5.2: Variation of burnishing feed with % increase in surface finishat different speeds in (a) EN 8 (b) EN 24 and (c) EN 31 alloy steels.

0.02 0.04 0.06 0.08 0.10 0.1210

20

30

40

50

60

70

80

90

100 22 m/min 34 m/min 51 m/min

(a) EN 8

Feed, mm/rev

% in

crea

se in

sur

face

fini

sh

0.02 0.04 0.06 0.08 0.10 0.1240

50

60

70

80

90

100

22 m/min 34 m/min 51 m/min

(b) EN 24

Feed, mm/rev

% in

crea

se in

sur

face

fini

sh

0.02 0.04 0.06 0.08 0.10 0.120

10

20

30

40

50

60

70

80

90

100

22 m/min 34 m/min 51 m/min(c) EN 31

Feed, mm/rev

% in

crea

se in

sur

face

fini

sh

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Table 5.6 Optimal values of burnishing parameters for the alloysteels, EN 8, EN 24 and EN 31.

Material Speed(m/min)

No ofpasses

Force(N)

Feed(mm/rev)

Ra

(µm)

EN 8 51 1 210 0.032 0.10

EN 24 34 2 170 0.095 0.15

EN 31 34 1 200 0.032 0.11

5.2.2. Microstructure

Figure 5.3 to 5.5 shows the typical set of optical micrographs

obtained from EN 8, En 24 and EN 31 alloy steels in the unburnished

(Fig. 5.3a) and burnished (Fig. 5.3b for first pass, Fig. 5.3c for second

pass, Fig. 5.3d for third pass) conditions. The optical micrographs

(corresponding to surfaces from periphery to inner cross section of the

cylindrical specimens) show similar structure with varied burnished

depths for different burnishing conditions in all the three alloy sheets.

These figures clearly show a distinct variation in the thickness of

burnishing affected zone with each of the burnished pass. The

variation in depth of these zones is measured from micrographs and

the same are given in Fig. 5.6 and Table 5.7. These data clearly reveal

that highest burnishing depth occurs at 1st pass in EN 8 and EN 31

while the same occurs at 2nd pass in EN 24 alloy steel. It should be

noted here that the highest depth of burnishing presumably provides

maximum effectiveness in surface modification. The actual values of

burnishing layer thickness are obtained experimentally. The variation

of burnishing layer thickness which is different for different EN series

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steels is a function of many microstructural and surface condition

dependent properties. The principal reasons for such variation

observed in the present study was not investigated in the present

thesis as this requires detailed microstructural analysis involving

transmission electron microscopy.

(a) (b)

(c) (d)

Fig. 5.3: Optical micrographs of EN 8 showing the depth of burnishingin (a) Unburnished (b) Burnished – 1st pass (c) Burnished – 2nd pass(d) Burnished – 3rd pass conditions

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(a) (b)

(c) (d)

Fig. 5.4: Optical micrographs of EN 24 showing the depth ofburnishing in (a) Unburnished (b) Burnished – 1st pass (c) Burnished –2nd pass (d) Burnished – 3rd pass conditions

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(a) (b)

(c) (d)

Fig. 5.5: Optical micrographs of EN 31 showing the depth ofburnishing in (a) Unburnished (b) Burnished – 1st pass (c) Burnished –2nd pass(d) burnished – 3rd pass conditions

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Table 5.7: Variation of burnishing layer thickness in theburnishing zone for three alloy steels.

Material Characteristic Burnishing ProcessBB B1 B2 B3

EN 8 Burnishing layer thickness 260.0 475.0 425.0 350.0

EN 24 Burnishing layer thickness 250.0 350.0 450.0 430.0

EN 31 Burnishing layer thickness 400.0 650.0 700.0 675.0[BB – Before burnishing, B1 – Burnished-1st pass, B2 – Burnished-2nd pass andB3 – Burnished-3rd pass]

5.2.3. Micro hardnessThe specimens polished to obtain microstructure were further used

to determine the variation in micro hardness as a function of distance

from the surface. The micro hardness values are found to be almost

similar with no systematic variation with the burnishing distance.

Hence, an average value of micro hardness is taken as a

representative value for each of the experimental condition such as

Fig. 5.6: Correlation of burnishing layerthickness with burnishing parameters

B B1 B2 B3200

300

400

500

600

700

800 EN 8 EN 24 EN 31

No of Passes

Burn

ishi

ng la

yer t

hick

ness

,m

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unburnished, burnished-1st pass, burnished-2nd pass and burnished-

3rd pass. These data are summarized and given in Table 5.8 and are

shown in Fig. 5.7. It is interesting to note that maximum burnished

depth (as obtained from optical micrographs) also results in highest

values of average micro hardness. The micro hardness variation

depends on nature and magnitude of residua stresses that arise due

to different extents of burnishing. It should be noted here that in all

the three EN series steels highest micro hardness were obtained either

at B1 or B2 (depending upon the extent of burnishing in each stage)

and comparatively lower micro hardness values in B and B3, the first

(B) for the lack of any surface modification and the later for the effects

of flaking like microstructural degradation.

Table 5.8: Variation of average micro hardness values in theburnishing zone for three alloy steels.

Material CharacteristicBurnishing Process

BB B1 B2 B3

EN 8 Micro Hardness 251.2 303.5 279.4 294.3

EN 24 Micro Hardness 297.2 312.7 339.6 335.1

EN 31 Micro Hardness 196.1 251.6 254.1 223.9

[BB – Before burnishing, B1 – Burnished-1st pass, B2 – Burnished-2nd pass andB3 – Burnished-3rd pass]

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5.2.4. Residual stress

The residual stresses that are determined by XRD for EN series

steels are given in Table 5.9 and the data are shown in Fig. 5.8 as a

function of number of passes for the three alloy steels. The data in

Fig. 5.8 show that the residual stresses gradually build up with

burnishing and exhibit a peak in residual stresses at 1st or 2nd

burnishing pass. Unlike in EN 8 steel the other two alloy steels

namely EN 24 and EN 31 show significant decrease in the magnitude

of compressive residual stresses. The magnitude of compressive

residual stress is also found to be strongly dependent on nature of

alloy steel. The harder is the alloy steel; the highest is the magnitude

of compressive residual stresses.

Fig. 5.7: Correlation of surface micro-hardnesswith burnishing parameters

0

50

100

150

200

250

300

350

400

B3

B3

B3

B2

B2

B2

B1

B1

B

BB1

B

EN 31EN 24EN 8

Mic

ro h

ardn

ess

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Table 5.9: Compressive residual stresses for EN series steels

Material Burnishingcondition

PrincipalStress(max)(MPa)

PrincipalStress(min)(MPa)

Directionof

PrincipalStress *

Maxshearstress(MPa)

Equivalentstress(MPa)

EN 8

BB -171 -331 14.4 80 286.9

B1 -223 -368 6.6 72.4 323

B2 -203 -369 4.6 83 323.4

B3 -205 -358 2.9 76.6 314.5

EN 24

BB -208 -285 5.7 38.5 258.6

B1 -272 -667 11.4 197.4 582.7

B2 -293 -598 2.2 152.5 519.7

B3 -249 -628 10.8 189.4 549.4

EN 31

BB -160 -317 8.1 78.8 311.7

B1 -208 -285 5.7 38.5 258.6

B2 -175 -275 6.3 49.8 241.8

B3 -171 -331 14.4 80 286.8[BB – Before burnishing, B1 – Burnished-1st pass, B2 – Burnished-2nd pass and

B3 – Burnished-3rd pass];* Angle in degrees from the axial direction of the cylindrical sample

Burnishing depth too revealed a systematic correlation with the

average hardness of the alloy steel. According to the expected lines,

softest alloy steel of the three exhibited the highest burnishing depth.

Parameters chosen for XRD analysis are wave length: 2.291 A° and

Bragg angle: 156°.

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5.3. Technological Implication

Surface compressive residual stresses have been found to be

beneficial for tensile mean stress controlled fatigue as well as creep.

The same would be grossly detrimental to the conditions where

compressive mean stress is in vogue. However, in most engineering

applications the rotary parts grossly experience tensile loading

conditions and compressive residual stresses are desirable and they

effectively enhance fatigue resistance. Hence, burnishing is highly

beneficial for most rotating structural components in improving their

service life. Further studies are required to evaluate the effectiveness

Fig. 5.8: Variation of magnitude of residual compressivestresses with burnishing pass in case of the three alloy steels.

B B1 B2 B3150

200

250

300 EN 8 EN 24 EN 31

No of passes

Com

pres

sive

resi

dual

stre

ss, M

Pa

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of compressive residual stresses that result an industrial burnishing

process by extending the present studies to at least high cycle fatigue

loading. Such studies also need to address the progressive relaxation

in the net compressive residual stresses with the extent of high cycle

fatigue damage as occurs with number of such fatigue cycles. Such

studies have not been attempted till date and should be of significant

technological value in case of present low cost EN series alloy steels.

5.4. Conclusions

1. Burnishing results in significant surface finish depth of

burnishing and increase in micro hardness and residual stresses.

2. The present systematic study reveals that the burnishing depth,

increase in micro hardness or increase in magnitude of

compressive residual stresses, is higher in case of softer alloy

steels EN 8 and EN 24 as compared to the relatively harder EN 31

alloy steel.

3. In all the three alloy steels, higher extent of burnishing resulted in

different extents of micro structural modification (as reflected by

the magnitude of compressive residual stresses) and in general,

showed a maximum at intermediate burnishing pass – First in

case of EN 8, EN 31 and second in case of EN 24 steel.

4. The present study revealed one-to-one correlation between

burnishing depth, increase in micro hardness and magnitude of

compressive residual stresses.