Elemental Analyzer Consumables and Spare Parts Catalog · 6 Consumables and Spare Parts Catalog 1 CHN Determination Table 1-1. Consumables and Spare Parts for CHN Determination Refer

FlashEA® 1112Elementa l Ana lyzer

Consumables and Spare Parts CatalogNinth Edition

FlashEA® 1112 Elemental Analyzer Consumables and Spare Parts CatalogJanuary 2007 NL EditionPart Number 317 082 50© 1999-2007 Thermo Fisher Scientific Inc. All rights reserved.Printed in Italy

Published by Thermo Fisher Scientific., Voltaweg 22, 2627 BC Delft, the NetherlandsTel: +31 15 257 13 14 Fax: +31 15 257 22 97

Printing History: First Edition, released September 1999.Second Edition, released October 2000Third Edition, released November 2001Fourth Edition, released January 2003Fifth Edition, released September 2003Sixth Edition, released January 2004Seventh Edition, released June 2005Eighth Edition, released July 2006 Ninth Edition, released January 2007 NL

DisclaimerTechnical Information contained in this publication is for reference purposes only and is subject to change without notice. Every effort has been made to supply complete and accurate information; however, Thermo Fisher Scientific assumes no responsibility and will not be liable for any errors, omissions, damage, or loss that might result from any use of this manual or the information contained therein (even if this information is properly followed and problems still arise).

This publication is not part of the Agreement of Sale between Thermo Fisher Scientific and the purchaser of a FlashEA® 1112 system. In the event of any conflict between the provisions of this document and those contained in Thermo Fisher Scientific’s Terms and Conditions, the provisions of the Terms and Conditions shall govern.

Reference to System Configurations and Specifications supercede all previous information and are subject to change without notice.

Trademarks

FlashEA® 1112 and Eager® 300 are trademarks of Thermo Fisher Scientific. Other brand and product names may be trademarks or registered trademarks of their respective companies.

Contents
Chapter 1CHN Determination............................................................................................................................ 6
Chapter 2CHN/O Determination ........................................................................................................................ 8

Chapter 3CHNS Determination ......................................................................................................................... 12

Chapter 4CHNS/O Determination...................................................................................................................... 14

Chapter 5S Determination ................................................................................................................................. 18

Chapter 6O Determination................................................................................................................................. 20

Chapter 7N Determination ................................................................................................................................. 22

Chapter 8N Lubricant Determination................................................................................................................ 24

Chapter 9NC Determination .............................................................................................................................. 26

Chapter 10NCS Determination ............................................................................................................................ 28

Chapter 11NC-Soils, NC-Sediments, NC-Filters Determinations..................................................................... 30

Chapter 12N/Protein, N-Brew Determinations ................................................................................................... 32

Chapter 13FlashEA IRMS EFCt (NC Determination) ......................................................................................... 34

Chapter 14FlashEA HT (O/H and NC Determinations) ...................................................................................... 36

Consumables and Spare Parts Catalog iii

Contents

Chapter 15Kits of Consumables and Spare Parts .............................................................................................40

Chapter 16Reactors, Absorption Filters, GC Columns and Fittings................................................................46

Chapter 17Reagents and Chemicals...................................................................................................................52

Chapter 18Analytical Standards and Reference Materials ...............................................................................58

Chapter 19Adsorber for Fluorine Compounds ..................................................................................................60

Chapter 20Kits for FlashEA 1112.........................................................................................................................62

Chapter 21Sample Containers.............................................................................................................................64

Chapter 22Sample Preparation Accessories .....................................................................................................68

Chapter 23MAS200 R Autosampler for Solid Samples .....................................................................................70

Chapter 24NoBlank Sampling Device .................................................................................................................74

Chapter 25CM2 Manual Sampler .........................................................................................................................76

Chapter 26AI/AS 3000 Autosampler for Liquids ................................................................................................78

Chapter 27AS 2000 Autosampler for Liquid Samples .......................................................................................80

Chapter 28Accessories for Injection of Liquid and Gas Samples ...................................................................81

iv Consumables and Spare Parts Catalog

Contents

Chapter 29Resting Foot Kit ................................................................................................................................. 82

Chapter 30Recommended Spare Parts .............................................................................................................. 83

Chapter 31FlashEA 1112 FPD Option ................................................................................................................. 84

Chapter 32Cables ................................................................................................................................................. 88

Chapter 33Electronic Flow Controller Modules ................................................................................................ 89

Chapter 34Flash EA 1112 Electronics ................................................................................................................ 90

Chapter 35Eager 300 Ethernet A/D ..................................................................................................................... 92

Chapter 36Single to Double Furnace Upgrade Kit ............................................................................................ 94

Chapter 37Furnaces Transformation Kits.......................................................................................................... 96

Chapter 38MAS 200 R Driver............................................................................................................................... 106

Chapter 39Flash EA 1112 Validation................................................................................................................... 108

Appendix ACustomer Communication................................................................................................................ 111

How To Contact Us................................................................................................................ 111

Consumables and Spare Parts Catalog v

1

6

CHN Determination

Table 1-1. Consumables and Spare Parts for CHN DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Chromium Oxide 25g 338 229 003 High Quality Copper 50g 338 353 124 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 00R Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70-- Quartz Crucible 1 252 045 10

CC Multiseparation Column (PTFE; 2 m; 6x5 mm) 1 260 082 20

-- Tin Containers 100 240 064 00-- Forceps 1 205 005 00-- Spatula 1 205 006 00

-- Cyclohexanone STD 1g 338 224 00-- Atropine STD 2g 338 244 00-- Imidazole STD 1g 338 354 30-- Acetanilide STD 2g 338 367 00-- Urea STD 2g 338 400 01-- Nicotinamide STD 2g 338 400 19

Consumables and Spare Parts Catalog

Chapter 1CHN Determination

WARNING! If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to eliminate the Quartz Wool between Chromium Oxide and High Quality Copper and between the High Quality Copper and the Cobaltous-Cobaltic Oxide.

AS. Autosampler R. ReactorCC. Chromatographic Column TCD. Thermal Conductivity Detector

Consumables and Spare Parts Catalog 7

2

8

CHN/O Determination

Table 2-1. Consumables and Spare Parts for CHN/O Determination Refer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Chromium Oxide 25g 338 229 003 High Quality Copper 50g 338 353 124 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 005 Nickel Plated Carbon 5g 338 238 006 Quartz Turning 50g 338 223 007 Soda Lime 100g 338 352 358 Magnesium Perchlorate (Anhydrone) 100g 338 219 00-- Nickel Wool 2g 338 250 00

R1/R2 Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70-- Quartz Crucible 1 252 045 10F Empty Adsorption Filter Tube (Small Size) without Fast

Connectors1 281 131 04

CC1 Multiseparation Column (PTFE; 2 m; 6x5 mm) 1 260 082 20CC2 Oxygen Separation Column (SS; 1 m; 6x5 mm) 1 260 079 00

-- Tin Containers 100 240 064 00-- Silver Containers for Oxygen Determination 100 240 054 00-- Forceps 1 205 005 00-- Spatula 1 205 006 00

-- Cyclohexanone STD 1g 338 224 00-- Atropine STD 2g 338 244 00-- Benzoic Acid STD 2g 338 225 00-- Imidazole STD 1g 338 354 30


Chapter 2CHN/O Determination

-- Acetanilide STD 2g 338 367 00-- Urea STD 2g 338 400 01-- Nicotinamide STD 2g 338 400 19

AS. Autosampler R1-R2. ReactorsF. Adsorption Filter CC1-CC2. Chromatographic ColumnsTCD. Thermal Conductivity Detector

Table 2-1. Consumables and Spare Parts for CHN/O Determination (Continued)



WARNING! CHN Determination

If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to eliminate the Quartz Wool between Chromium Oxide and High Quality Copper and between the High Quality Copper and the Cobaltous-Cobaltic Oxide.

WARNING! Oxygen Determination

If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the reactor of pyrolysis. In this case it is necessary to reduce from 30 mm to 20 mm the Quartz Wool in the lower section of the reactor.

10 Consumables and Spare Parts Catalog



3

12

CHNS Determination

Table 3-1. Consumables and Spare Parts for CHNS Determination Refer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Copper Oxide 50g 338 217 103 Electrolytic Copper 70g 338 353 13-- Vanadium Pentoxide 1g 338 375 10R Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70R Prepacked Quartz Reactor for CHNS/NCS/S 1 468 020 15-- Quartz Crucible 1 252 045 10

CC Packed Column CHNS/NCS (PTFE; 2 m; 6x5 mm) 1 260 082 15


-- BBOT STD 2g 338 352 10-- Sulphanilamide STD 2g 338 251 00-- L-Cystine STD 2g 338 400 18


Chapter 3CHNS Determination

WARNING! If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to reduce the Quartz Wool between Copper Oxide and Electrolytic Copper up to obtain a thin layer and to reduce the Copper Oxide proportionally as shown in the figure above.

AS. Autosampler R. ReactorCC. Chromatographic Column TCD. Thermal Conductivity Detector


4

14

CHNS/O Determination

Table 4-1. Consumables and Spare Parts for CHNS/O Determination Refer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Copper Oxide 50g 338 217 103 Electrolytic Copper 70g 338 353 134 Nickel Plated Carbon 5g 338 238 005 Quartz Turnings 50g 338 223 006 Soda Lime 100g 338 352 357 Magnesium Perchlorate (Anhydrone) 100g 338 219 00-- Nickel Wool 2g 338 250 00-- Vanadium Pentoxide 1g 338 375 10

R1/R2 Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70R1 Pre-packed Quartz Reactor for CHNS/NCS/S 1 468 020 15-- Quartz Crucible 1 252 045 10F Empty Adsorption Filter Tube (Small Size) without Fast


CC1 CHNS/NCS Separation Column (PTFE; 2 m; 6x5 mm) 1 260 082 15CC2 Oxygen Separation Column (SS; 1m; 6x5 mm) 1 260 079 00

-- Tin Containers 100 240 064 00-- Silver Containers for Oxygen Determination 100 240 054 00-- Forceps 1 205 005 00-- Spatula 1 205 006 00

-- Atropine STD 2g 338 244 00-- Benzoic Acid STD 2g 338 225 00-- Sulphanilamide STD 2g 338 251 00


Chapter 4CHNS/O Determination

-- BBOT STD 2g 338 352 10-- Acetanilide STD 2g 338 367 00-- Urea STD 2g 338 400 01-- L-Cystine STD 2g 338 400 18-- Nicotinamide STD 2g 338 400 19

AS. Autosampler R1-R2. ReactorsF. Adsorption Filter CC1-CC2. Chromatographic ColumnsTCD. Thermal Conductivity Detector

Table 4-1. Consumables and Spare Parts for CHNS/O Determination (Continued)



WARNING! CHNS Determination

If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the oxidation/reduction reactor. In this case it is necessary to reduce the Quartz Wool between Copper Oxide and Electrolytic Copper up to obtain a thin layer and to reduce the Copper Oxide proportionally as shown in the figure above.

WARNING! Oxygen Determination

If the sample to be analyzed presents particular characteristics (high presence of inorganic material) we suggest to insert the quartz crucible into the reactor of pyrolysis. In this case it is necessary to reduce from 30 mm to 20 mm the Quartz Wool in the lower section of the reactor




5

18

S Determination

Table 5-1. Consumables and Spare Parts for S DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Copper Oxide 50g 338 217 103 Electrolytic Copper 70g 338 353 134 Magnesium Perchlorate (Anhydrone) 100g 338 219 00-- Vanadium Pentoxide 1g 338 375 10R Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70R Prepacked Quartz Reactor for CHNS/NCS/S 1 468 020 15-- Quartz Crucible 1 252 045 10F Empty Adsorption Filter Tube (Small Size) without Fast


CC Sulphur Separation Column (PTFE; 0.8 m; 6x4 mm) 1 260 078 00




Chapter 5S Determination


AS. Autosampler R. ReactorF. Adsorption Filter CC. Chromatographic ColumnTCD. Thermal Conductivity Detector


6

20

O Determination

Table 6-1. Consumables and Spare Parts for O DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Nickel Plated Carbon 5g 338 238 003 Quartz Turnings 50g 338 223 004 Soda Lime 100g 338 352 355 Magnesium Perchlorate (Anhydrone) 100g 338 219 00-- Nickel Wool 2g 338 250 00R Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70-- Quartz Crucible 1 252 045 10F Empty Adsorption Filter Tube (Small Size) without Fast


CC Oxygen Separation Column (SS; 1m; 6x5mm) 1 260 079 00

-- Silver Containers for Oxygen Determination 100 240 054 00-- Forceps 1 205 005 00-- Spatula 1 205 006 00

-- Cyclohexanone STD 1g 338 224 00-- Benzoic Acid STD 2g 338 225 00-- Sulphanilamide STD 2g 338 251 00-- BBOT STD 2g 338 352 10-- Acetanilide STD 2g 338 367 00-- Urea STD 2g 338 400 01-- L-Cystine STD 2g 338 400 18-- Nicotinamide STD 2g 338 400 19


Chapter 6O Determination

WARNING! If the sample to be analyzed presents particular characteristics (high presence of inorganic material)we suggest to insert the quartz crucible into the reactor of pyrolysis. In this case it is necessary to reduce from 30 mm to 20 mm the Quartz Wool in the lower section of the reactor.



7

22

N Determination

Table 7-1. Consumables and Spare Parts for N DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Copper Oxide 50g 338 217 103 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 004 High Quality Copper 50g 338 353 125 Soda Lime 100g 338 352 356 Molecular Sieve 3 Å 100g 338 018 017 Silica Gel plus indicator 100g 338 400 35 -- Chromosorb® WAW 25g 338 375 30

R1/R2 Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70-- Quartz Crucible 1 252 045 10

F1/F2 Empty Adsorption Filter Tube (Large Size) without Fast Connectors

2 281 130 64

CC Nitrogen Separation Column (PTFE; 0.5m; 8x6 mm) 1 260 078 20


-- Nicotinamide STD 2g 338 400 19-- Aspartic Acid STD 2g 338 400 22-- Atropine STD 2g 338 244 00


Chapter 7N Determination

AS. Autosampler R1-R2. ReactorsF1-F2. Adsorption Filters CC. Chromatographic ColumnTCD. Thermal Conductivity Detector


8

24

N Lubricant Determination

Table 8-1. Consumables and Spare Parts for N Lubricant DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 25 mm HPAR (Set of 5) 1 290 206 49-- Top O-Ring for 25 mm HPAR (Set of 5) 1 290 206 821 Quartz Wool 5g 338 222 002 Oxidation Catalyst 40g 338 400 003 High Quality Copper 50g 338 353 124 Soda Lime 100g 338 352 355 Silica Gel plus indicator 100g 338 400 35 6 Molecular Sieve 3 Å 100g 338 018 01

R1 Prepacked HPAR Reactor; 25 mm OD 1 468 020 08CR HPAR Crucible 1 252 050 11

R1/R2 Empty HPAR Reactor; 25 mm OD 1 468 200 75F1/F2 Empty Adsorption Filter Tube (Large Size) without Fast


CC Nitrogen Separation (N-Brew) Column (PTFE; 1 m; 8x6 mm) 1 260 700 04

-- Tin Containers 100 252 080 00-- Tin Disk 30 mm diameter 100 252 080 15-- Forceps 1 205 005 00-- Spatula 1 205 006 20

-- Atropine 2g 338 244 00-- Lubricant Reference Material 2g 338 352 40


Chapter 8N Lubricant Determination

AS. Autosampler R1-R2. ReactorsF1-F2. Adsorption Filters CC. Chromatographic ColumnTCD. Thermal Conductivity Detector CR. HPAR Crucible


9

26

NC Determination

Table 9-1. Consumables and Spare Parts for NC DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Copper Oxide 50g 338 217 103 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 004 High Quality Copper 50g 338 353 125 Magnesium Perchlorate (Anhydrone) 100g 338 219 00

R1/R2 Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70-- Quartz Crucible 1 252 045 10F Empty Adsorption Filter Tube (Small Size) without Fast


CC Multiseparation Column (SS; 2m; 6x5 mm) 1 260 079 20


-- Nicotinamide STD 2g 338 400 19-- Aspartic Acid STD 2g 338 400 22

Atropine STD 2g 338 244 00


Chapter 9NC Determination

AS. Autosampler R1-R2. ReactorsF. Adsorption Filter CC.Chromatographic ColumnTCD. Thermal Conductivity Detector


10

28

NCS Determination

Table 10-1. Consumables and Spare Parts for NCS DeterminationRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Copper Oxide 50g 338 217 103 Electrolytic Copper 70g 338 353 134 Magnesium Perchlorate (Anhydrone) 100g 338 219 00-- Vanadium Pentoxide 1g 338 375 10R Empty Quartz Reactor Tube 18 mm OD (Set of 2) 1 468 200 70-- Pre-packed Quartz Reactor for CHNS/NCS/S 1 468 020 15-- Quartz Crucible 1 252 045 10F Empty Adsorption Filter Tube (Small Size) without Fast


CC CHNS/NCS Separation Column (PTFE 2 m; 6x5 mm) 1 260 082 15




Chapter 10NCS Determination




11

30

NC-Soils, NC-Sediments, NC-Filters Determinations

Table 11-1. Consumables and Spare Parts for NC-Soils, NC-Sediments, NC-Filters DeterminationsRefer To: Description Qty PN

-- Bottom O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 206 40-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 10-- Bottom O-Ring for 25 mm OD HPAR (Set of 5) 1 290 206 49-- Top O-Ring for 25 mm OD HPAR (Set of 5) 1 290 206 821 Quartz Wool 5g 338 222 002 Oxidation Catalyst 40g 338 400 003 High Quality Copper 50g 338 353 124 Magnesium Perchlorate (Anhydrone) 100g 338 219 00

R1 Prepacked HPAR Reactor 1 468 020 08-- Empty HPAR 25 mm OD 1 468 200 75

CR HPAR Crucible 1 252 050 11R2 Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 70F Empty Adsorption Filter Tube (Small Size) without Fast


CC Multiseparation Column (SS; 2m; 6x5 mm) 1 260 079 20

-- Tin Containers 100 252 080 00-- Tin Disk 30 mm diameter 100 252 080 15-- Tin Disk 35 mm diameter 100 252 080 18-- Forceps 1 205 005 00-- Spatula 1 205 006 20

-- Aspartic Acid STD 2g 338 400 22-- Soil NC Reference Material 5g 338 400 25


Chapter 11NC-Soils, NC-Sediments, NC-Filters Determinations

AS. Autosampler R1-R2. ReactorsF. Adsorption Filter CC. Chromatographic ColumnTCD. Thermal Conductivity Detector CR. HPAR Crucible


12

32

N/Protein, N-Brew Determinations

Table 12-1. Consumables and Spare Parts for N/Protein, N-Brew DeterminationsRefer To: Description Qty PN

-- Bottom O-Ring for 25 mm HPAR (Set of 5) 1 290 206 49-- Top O-Ring for 25 mm HPAR (Set of 5) 1 290 206 821 Quartz Wool 5g 338 222 002 Oxidation Catalyst 40g 338 400 003 High Quality Copper 50g 338 353 124 Soda Lime 100g 338 352 355 Silica Gel plus indicator 100g 338 400 35 6 Molecular Sieve 3 Å 100g 338 018 01-- Chromosorb® WAW 25g 338 375 30

R1 Prepacked HPAR Reactor; 25 mm OD 1 468 020 08CR HPAR Crucible 1 252 050 11

R1/R2 Empty HPAR Reactor; 25 mm OD 1 468 200 75F1/F2 Empty Adsorption Filter Tube (Large Size) without Fast


CC Nitrogen Separation Column (PTFE; 0.5 m; 8x6 mm) 1 260 078 20CC Nitrogen Separation (N-Brew) Column (PTFE; 1 m; 8x6 mm) 1 260 700 04

-- Tin Containers 100 252 080 00-- Tin Disk 30 mm diameter 100 252 080 15-- Tin Disk 35 mm diameter 100 252 080 18-- Forceps 1 205 005 00-- Spatula 1 205 006 20

-- Urea STD 10g 338 400 02-- Aspartic Acid STD 10g 338 400 23-- Pasta Reference Material 10g 338 400 24


Chapter 12N/Protein, N-Brew Determinations

AS. Autosampler R1-R2. ReactorsF1-F2. Adsorption Filters CC. Chromatographic ColumnTCD. Thermal Conductivity Detector CR. HPAR Crucible


13

34

FlashEA IRMS EFCt (NC Determination)

Table 13-1. Consumables and Spare Parts for FlashEA IRMS EFCt - NC DeterminationsRefer To: Description Qty PN

-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Chromium Oxide 25g 338 229 003 Silvered Cobaltous- Cobaltic Oxide 25g 338 245 004 Reduced Copper 100g 338 353 00 5 Magnesium Perchlorate 100g 338 219 00

R1/R2 Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 70F Adsorption Filter 1 281 131 00

CC IRMS Separation Column (SS; 3m; 6x5 mm) 260 082 05

-- Tin Containers (Set of 100) 1 240 064 00-- Forceps 1 205 005 00-- Spatula 1 205 006 00

-- Cyclohexanone STD 1g 338 224 00-- Atropine STD 2g 338 244 00-- Nicotinamide STD 2g 338 400 19-- Acetanilide STD 2g 338 367 00


Chapter 13FlashEA IRMS EFCt (NC Determination)

AS. Autosampler R1 - R2. ReactorsF1 - F2. Adsorption Filters CC1 - CC2. Chromatographic ColumnsTCD. Thermal Conductivity Detector CFI. Continuous Flow InterfaceIRMS. Isotopic Ratio Mass Spectrometer


14

36

FlashEA HT(O/H and NC Determinations)

IMPORTANT The HT Pyrolysis chemicals for O/H determination constituted to ceramic reactor, glassy carbon reactor, graphite tube, graphite crucible, glassy carbon granulate, silver wool, etc., can be ordered directly to Thermo Fisher Scientific GmbH Bremen, Germany.

O/H Determination

NC Determination

Table 14-1. HT FurnaceRefer To: Description Qty PN

-- O/H Separation column (SS; 1 m; 6x5 mm) 1 260 079 00

Table 14-2. Consumables and Spare Parts for FlashEA HT- NC DeterminationsRefer To: Description Qty PN

-- Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229 101 Quartz Wool 5g 338 222 002 Chromium Oxide 25g 338 229 003 Silvered Cobaltous- Cobaltic Oxide 25g 338 245 004 Reduced Copper 100g 338 353 00 5 Magnesium Perchlorate 100g 338 219 00-- Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 70-- Adsorption Filter 1 281 131 00-- IRMS Separation Column (SS; 3m; 6x5 mm) 1 260 082 05

-- Tin Containers (Set of 100) 1 240 064 00-- Forceps 1 205 005 00-- Spatula 1 205 006 00


Chapter 14FlashEA HT (O/H and NC Determinations)

-- Cyclohexanone STD 1g 338 224 00-- Atropine STD 2g 338 244 00-- Nicotinamide STD 2g 338 400 19-- Acetanilide STD 2g 338 367 00

Table 14-2. Consumables and Spare Parts for FlashEA HT- NC Determinations (Continued)



AS. Autosampler R2. ReactorsF2. Adsorption Filter CC2. Chromatographic ColumnTCD. Thermal Conductivity Detector CFI Continuous Flow InterfaceIRMS. Isotopic Ratio Mass Spectrometer




15

40

Kits of Consumables and Spare Parts

Kit for 1000 Analyses for FlashEA 1112No Description Qty PN

CHN Determination 1 190 024 101 Tin Containers (Set of 100) 20 240 064 002 Quartz Wool (5g) 1 338 222 003 Chromium Oxide (25g) 1 338 229 004 Silvered Cobaltous-Cobaltic Oxide (25g) 1 338 245 005 High Quality Copper (50g) 4 338 353 126 Empty Quartz Reactor Tube (Set of 2) 1 468 200 70

No Description Qty PN CHNS / NCS / S Determination with Empty Quartz Reactor 1 190 024 11

1 Tin Containers (Set of 100) 20 240 064 002 Copper Oxide (50g) 2 338 217 103 Magnesium Perchlorate [Anhydrone] (100g)

Only for NCS and S determinations1 338 219 00

4 Quartz Wool (5g) 1 338 222 005 Electrolytic Copper 4 338 353 136 Vanadium Pentoxide (1g) 1 338 375 107 Empty Quartz Reactor Tube (Set of 2) 2 468 200 70


Chapter 15Kits of Consumables and Spare Parts

No Description Qty PNCHNS / NCS / S Determination with Prepacked Quartz Reactor 1 190 024 12

1 Tin Containers (Set of 100) 20 240 064 002 Magnesium Perchlorate [Anhydrone] (100g)

Only for NCS and S determinations1 338 219 00

3 Quartz Wool (5g) 1 338 222 004 Vanadium Pentoxide (1g) 1 338 375 105 Prepacked Reactor for CHNS, NCS and S determinations 4 468 020 15

No Description Qty PNOxygen Determination 1 190 024 16

1 Silver Containers (Set of 100) 10 240 054 002 Magnesium Perchlorate [Anhydrone] (100g) 1 338 219 003 Quartz Wool (5g) 2 338 222 004 Quartz Turnings (50g) 1 338 223 005 Nickel Plated Carbon (5g) 8 338 238 006 Nickel Wool (2g) 1 338 250 007 Soda Lime (100g) 1 338 352 358 Empty Quartz Reactor (Set of 2) 1 468 200 70

No Description Qty PNN Organic Determination 1 190 024 13

1 Tin Containers (Set of 100) 20 240 064 002 Molecular Sieve 3Å (100g) 1 338 018 013 Copper Oxide (50g) 2 338 217 104 Quartz Wool (5g) 1 338 222 005 Silvered Cobaltous-Cobaltic Oxide (25g) 2 338 245 006 Soda Lime (200g) 2 338 352 307 High Quality Copper (50g) 8 338 353 128 Chromosorb® WAW (25g) 1 338 375 309 Silica Gel plus indicator (100g) 1 338 400 35

10 Empty Quartz Reactor Tube (Set of 2) 2 468 200 70



No Description Qty PNN Lubricant Determination 1 190 024 30

1 Tin Containers (Set of 100) 20 240 064 002 Top O-Ring for HPAR Reactor (Set of 5) 1 290 206 823 Molecular Sieve 3Å (100g) 1 338 018 014 Quartz Wool (5g) 2 338 222 005 Atropine STD (2g) 1 338 244 006 Soda Lime (200g) 5 338 352 307 Lubricant Reference Material; N% = 0.58 (2g) 1 338 352 408 High Quality Copper (50g) 12 338 353 129 Oxidation Catalyst (40g) 2 338 400 00

10 Silica Gel with Indicator (100g) 1 338 400 35

No Description Qty PN NC Determination 1 190 024 14

1 Tin Containers (Set of 100) 20 240 064 002 Copper Oxide (50g) 2 338 217 103 Magnesium Perchlorate [Anhydrone] (100g) 1 338 219 004 Quartz Wool (5g) 1 338 222 005 Silvered Cobaltous-Cobaltic Oxide (25g) 2 338 245 006 High Quality Copper (50g) 8 338 353 127 Empty Quartz Reactor Tube (Set of 2) 2 468 200 70

No Description Qty PNNC-Soils, NC-Sediments, NC-Filters Determination 1 190 024 15

1 Tin Disk 30 mm OD (Set of 100) 20 252 080 152 Magnesium Perchlorate [Anhydrone] (100g) 1 338 219 003 Quartz Wool (5g) 1 338 222 004 High Quality Copper (50g) 4 338 353 125 Prepacked HPAR Reactor 1 468 020 086 Empty Quartz Reactor Tube (Set of 2) 1 468 200 70



Kit for N/Protein AnalysesTable 15-1. Package A for Solid Samples

No Description Qty PNPackage A of Consumables for Solid Sample 1 190 042 20

1 HPAR Crucible 1 252 050 112 Tin Disk 30 mm diameter (Set of 100) 20 252 080 153 Bottom O-Ring for HPAR Reactor (Set of 5) 1 290 206 494 Top O-Ring for HPAR Reactor (Set of 5) 1 290 206 825 Molecular Sieve 3Å (100g) 1 338 018 016 Quartz Wool (5g) 2 338 222 007 Soda Lime (200g) 5 338 352 308 High Quality Copper (50g) 12 338 353 129 Oxidation Catalyst (40g) 2 338 400 00

10 Aspartic Acid STD (10g) 1 338 400 2311 Pasta Reference Material (10g) 1 338 400 2412 Silica Gel plus indicator (100g) 1 338 400 35

Table 15-2. Package B for Solid SamplesNo Description Qty PN

Package B of Consumables for Solid Sample 1 190 042 251 HPAR Crucible 2 252 050 112 Tin Disk 30 mm diameter (Set of 100) 100 252 080 153 Bottom O-Ring for HPAR Reactor (Set of 5) 1 290 206 494 Top O-Ring for HPAR Reactor (Set of 5) 1 290 206 825 Molecular Sieve 3Å (100g) 6 338 018 016 Quartz Wool (5g) 8 338 222 007 Soda Lime (200g) 25 338 352 308 High Quality Copper (50g) 60 338 353 129 Oxidation Catalyst (40g) 6 338 400 00

10 Aspartic Acid STD (10g) 2 338 400 23



11 Pasta Reference Material (10g) 2 338 400 2412 Silica Gel (100g) 4 338 400 35

Table 15-3. Package A for Liquid SamplesNo Description Qty PN

Package A of Consumables for Liquid Sample (AI/AS 3000) 1 190 042 291 Complete Vials 2 SVW Package (Set of 100) 10 240 140 192 Vial Solvent 4 mL ST 4-SVQ (Set of 5) 1 240 140 323 Bottom O-Ring for HPAR Reactor (Set of 5) 1 290 206 494 Top O-Ring for HPAR Reactor (Set of 5) 1 290 206 825 Septa for Waste Bottle (Set of 5) 1 313 032 186 Septa for FlashEA Injector (Set of 50) 1 313 032 307 Molecular Sieve (100g) 1 338 018 018 Quartz Wool (5g) 1 338 222 009 Soda Lime (200g) 3 338 352 30

10 High Quality Copper (50g) 8 338 353 1211 Oxidation Catalyst (40g) 2 338 400 0012 Silica Gel plus indicator (100g) 2 338 400 3513 Screw Caps 8-SC (Set of 5) 10 386 060 85

Table 15-4. Package A for Liquid SamplesNo Description Qty PN

Package A of Consumables for Liquid Sample (AS 2000) 1 190 042 281 Vials 10 CV (Set of 5) 1 240 300 002 Vials 2 SV (Set of 100) 10 240 740 413 Bottom O-Ring for HPAR Reactor (Set of 5) 1 290 206 494 Top O-Ring for HPAR Reactor (Set of 5) 1 290 206 825 Seal 8 mm Teflon (Set of 100) 10 313 032 176 BTO Septa (Set of 50) 1 313 032 307 Silica Gel plus indicator (100g) 2 338 400 35

Table 15-2. Package B for Solid Samples (Continued)



8 Quartz Wool (5g) 1 338 222 009 Soda Lime (200g) 3 338 352 30

10 High Quality Copper (50g) 8 338 353 1211 Caps 20 x 7 mm for Vials 10 CV (Set of 100) 1 386 060 3512 Plastic Screw Caps for Vials 2 SV (Set of 100) 1 386 060 74

Kit for 1000 Analyses for FlashEA for IRMS and FlashEA HT (NC Determination)

Table 15-5. Kit for 1000 Analyses for FlashEA for IRMS and FlashEA HT (NC Determination)No Description Qty PN

NC Determinations FlashEA IRMS 1 190 024 181 Tin container (set of 100) 10 240 064 002 Sealing O-Ring for adsorption filter (PN 281 13100) 2 290 136 033 Top O-ring for 18 mm OD quartz reactor (set of 5) 2 290 229 104 Magnesium Perchlorate (110g) 1 338 219 005 Quartz wool (5g) 1 338 222 006 Cyclohexanone STD (1g) 1 338 224 007 Chromium Oxide (25g) 4 338 229 008 Silvered Cobaltous Cobaltic Oxide (25g) 4 338 245 009 Reduced Copper (100g) n.4 4 338 353 00

10 Empty Quartz Reactor 18 mm OD (set of 2) n.2 2 468 200 70

Table 15-4. Package A for Liquid Samples (Continued)


16

46

Reactors, Absorption Filters, GC Columns and Fittings

ReactorsTable 16-1. Reactor Tubes

No Description Qty PN1 Empty Quartz Reactor 18 mm OD (Set of 2) 1 468 200 702 Top O-Ring for 18 mm OD Quartz Reactor (Set of 5) 1 290 229103 Bottom O-Ring 18 mm OD Quartz Reactor (Set of 5) 1 290 206404 Empty Quartz Reactor 18 mm OD CYL (Set of 2) [for IRMS/HT] 1 468 200 60

5 Empty HPAR Reactor 25 mm OD 1 468 200 756 Top O-Ring for HPAR (Set of 5) 1 290 206 827 Bottom O-Ring for HPAR (Set of 5) 1 290 206 49

8 Prepacked Quartz Reactor for CHNS/NCS/S Determinations 1 468 020 159 Prepacked HPAR Reactor for N/Protein/NC-Soils Determinations 1 468 020 08

10 HPAR Crucible 1 252 050 1111 Quartz Crucible (13 mm OD) 1 252 045 10

12 HPAR Reactor Extractor (see A) 1 205 006 2613 Crucible Extractor (see B) 1 205 006 2714 Cleaning Device for HPAR Reactor (see C) 1 205 006 2515 Cleaning Device for Quartz Reactor and SS Crucible (see D) 1 276 060 10

A B

C D


Chapter 16Reactors, Absorption Filters, GC Columns and Fittings

Adsorption FiltersTable 16-2. Adsorption Filters

Table 16-3. Adsorption Filters (Old Types)*

* The Absorption Filters (Old Types) have been mounted on FlashEA™ 1112 Elemental Analyzer till Serial Number 20005214

No Description Qty PN1 Adsorption Filter FC (Small Size) without Fast Connectors 1 281 131 042 Adsorption Filter FC (Large Size) without Fast Connectors 1 281 130 64

3 Fast Connectors Couple (Male plus Female) - See Figure 1 190 502 084 Fast Connector Couples plus Fast Connectors Adapters - See Figure

consisting of:- Fast Connectors (male + female), Set of 2- Fast Connector Adapters, Set of 2

1 190 502 09

1. FC Male 2. FC Female 1. FC Male 2. FC Female 3. FC AdapterFigure 16-1. Fast Connectors Couple Figure 16-2. Fast Connector Couples plus Fast

Connectors Adapters

5 Sealing O-Ring for Adsorption Filter FC [PN 281 131 04] (Set of 2) 1 290 036 356 Sealing O-Ring for Adsorption Filter FC [PN 281 130 64] (Set of 2) 1 290 100 82

No Description Qty PN1 Adsorption Filter (Small Size) 1 281 131 002 Sealing O-Ring for Adsorption Filter [PN 281 131 00] (Set of 2) 1 290 136 03

3 Adsorption Filter (Large Size) 1 281 130 604 Sealing O-Ring for Adsorption Filter [PN 281 130 60] (Set of 2) 1 290 100 82

1 2 1 2 3



Table 16-4. Adsorption Traps (Pyrex Type)**

** It substitutes the Absorption Filter (Large Size) with Fast Connectors PN 281 130 65 in N/Protein and NC-Soil Configurations when the sample contains very high humidity percentage and when several daily analyses are required.

Table 16-5. Adsorption Traps for IRMS and HT Versions

No Description Qty PN1 Large Adsorption Trap (Pyrex Type) without Fast Connectors 1 281 131 062 Sealing O-Ring for Pyrex Type Large Adsorption Filter (Set of 2) 1 290 036 35

No Description Qty PN1 Adsorption Filter (Small Size) 1 281 131 002 Sealing O-Ring for Adsorption Filter [PN 281 131 00] (Set of 2) 1 290 136 03



Gas Chromatographic ColumnsTable 16-6. Gas Chromatographic Columns

No Description Qty PN1 Multiseparation Column (PTFE; 2m; 6x5 mm) 1 260 082 202 Multiseparation Column (SS; 2 m; 6x5 mm) 1 260 079 203 CHNS/NCS Separation Column (PTFE; 2 m; 6x5 mm) 1 260 082 154 Oxygen Separation Column (PTFE; 1 m; 6x5 mm) 1 260 079 005 Sulphur Separation Column (PTFE; 0.8 m; 6x4 mm) 1 260 078 006 Sulphur Separation Column for OEA / FPD (PTFE; 0.15 m; 6x4 mm) 1 260 078 017 Nitrogen Separation Column (PTFE; 0.5 m; 8x6 mm) 1 260 078 208 Nitrogen Separation (N-Brew) Column (PTFE; 1 m; 8x6 mm) 1 260 700 049 IRMS Separation Column (SS; 3 m; 6x5 mm) 1 260 082 05

reattori

Characteristics Analytical Determination

Material Length(cm)

OD (mm)

ID (mm) CH

NS

CHN

NCS

S (T

CD)

S (F

PD)

O N

N/Pr

otein

N-Br

ew

NC

NC-S

oil

NC-S

edim

ents

NC-F

ilter

s

IRMS

(NC)

HT (N

C)

HT (O

/H)

Colu

mns

Steel 100 6 5 ✔ ✔

200 6 5 ✔ ✔ ✔ ✔

300 6 5 ✔ ✔

PTFE 15 6 4 ✔

50 8 6 ✔ ✔

80 6 4 ✔

100 8 6 ✔

200 6 5 ✔ ✔ ✔



FittingsTable 16-7. Fittings & Tubes

No Description Qty PN1 O-ring for 6 mm OD tube (set of 10) 1 290 305 672 Aluminium Ferrule, 2 mm (set of 10) 1 290 340 453 Aluminium Ferrule, 4 mm (set of 10) 290 340 514 Knurled nut for Polyethylene Tube PN 420 100 00 1 350 021 245 Push Fit Connector Tube 5 350 341 086 SS Tubing Nut; 2mm (Set of 10) 1 350 404 037 Male hose adapter for Polyethylene Tube PN 420 100 00 (set of 10) 1 350 441 378 6 MB Brass Blanking Nut (Set of 10) 1 350 451 009 SS Tube; 2x1 mm 3 m 391 025 00

10 Polyethylene Tube, Blue Color; 5x3 mm 5 m 420 100 0011 PTFE Tube; 2x1 mm 1 m 420 015 0012 PTFE Tube; 2x1mm 5 m 420 015 0113 PTFE Tube; 4x2 mm 1 m 420 016 0014 PTFE Tube; 6x4 mm 1 m 420 017 00




17

52

Reagents and Chemicals

CHN DeterminationTable 17-1. Reagents and Chemicals for CHN Determination

CHN-O DeterminationTable 17-2. Reagents and Chemicals for CHN-O Determination

No Description Qty PN1 Quartz Wool 5g 338 222 002 Chromium Oxide 25g 338 229 003 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 004 High Quality Copper 50g 338 353 12

No Description Qty PN1 Magnesium Perchlorate (Anhydrone) 100g 338 219 002 Quartz Wool 5g 338 222 003 Quartz Turnings 50g 338 223 004 Chromium Oxide 25g 338 229 005 Nickel Plated Carbon 5g 338 238 006 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 007 Nickel Wool 2g 338 250 008 Soda Lime 100g 338 352 359 High Quality Copper 50g 338 353 12


Chapter 17Reagents and Chemicals

CHNS DeterminationTable 17-3. Reagents and Chemicals for CHNS Determination

CHNS-O DeterminationTable 17-4. Reagents and Chemicals for CHNS-O Determination

S DeterminationTable 17-5. Reagents and Chemicals for S Determination

No Description Qty PN1 Copper Oxide 50g 338 217 102 Quartz Wool 5g 338 222 003 Electrolytic Copper 70g 338 353 134 Vanadium Pentoxide 1g 338 375 10

No Description Qty PN1 Copper Oxide 50g 338 217 102 Magnesium Perchlorate (Anhydrone) 100g 338 219 003 Quartz Wool 5g 338 222 004 Quartz Turnings 50g 338 223 005 Nickel Plated Carbon 5g 338 238 006 Nickel Wool 2g 338 250 007 Soda Lime 100g 338 352 358 Electrolytic Copper 70g 338 353 139 Vanadium Pentoxide 1g 338 375 10

No Description Qty PN1 Copper Oxide 50g 338 217 102 Magnesium Perchlorate (Anhydrone) 100g 338 219 003 Quartz Wool 5g 338 222 004 Electrolytic Copper 70g 338 353 135 Vanadium Pentoxide 1g 338 375 10



O DeterminationTable 17-6. Reagents an Chemicals for O Determination

N DeterminationTable 17-7. Reagents and Chemicals for N Determination

N Lubricant DeterminationTable 17-8. Reagents and Chemicals for N Lubricant Determination

No Description Qty PN1 Magnesium Perchlorate (Anhydrone) 100g 338 219 002 Quartz Wool 5g 338 222 003 Quartz Turnings 50g 338 223 004 Nickel Plated Carbon 5g 338 238 005 Nickel Wool 2g 338 250 006 Soda Lime 100g 338 352 35

No Description Qty PN1 Molecular Sieve 3 Å 100g 338 018 012 Copper Oxide 50g 338 217 103 Quartz Wool 5g 338 222 004 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 005 Soda Lime 200g 338 352 306 High Quality Copper 50g 338 353 127 Chromosorb® WAW 25g 338 375 308 Silica Gel plus indicator 100g 338 400 35

No Description Qty PN1 Molecular Sieve 3 Å 100g 338 018 012 Quartz Wool 5g 338 222 003 Soda Lime 200g 338 352 304 High Quality Copper 50g 338 353 126 Oxidation Catalyst 40g 338 400 00



NC DeterminationTable 17-9. Reagents and Chemicals for NC Determination

NCS DeterminationTable 17-10. Reagents and Chemicals for NCS Determination

NC-Soils, NC-Sediments, NC-Filters DeterminationTable 17-11. Reagents and Chemicals for NC-Soils, NC-Sediments, NC-Filters Determination

No Description Qty PN1 Copper Oxide 50g 338 217 102 Magnesium Perchlorate (Anhydrone) 100g 338 219 003 Quartz Wool 5g 338 222 004 Silvered Cobaltous-Cobaltic Oxide 25g 338 245 005 High Quality Copper 50g 338 353 12

No Description Qty PN1 Copper Oxide 50g 338 217 102 Magnesium Perchlorate (Anhydrone) 100g 338 219 003 Quartz Wool 5g 338 222 004 Electrolytic Copper 70g 338 353 135 Vanadium Pentoxide 1g 338 375 10

No Description Qty PN1 Magnesium Perchlorate (Anhydrone) 100g 338 219 002 Quartz Wool 5g 338 222 003 High Quality Copper 50g 338 353 124 Oxidation Catalyst 40g 338 400 00


56


N/Protein, N-Brew DeterminationTabella 17-12. Reagents and Chemicals for N/Protein, N-Brew Determination

IRMS and HT NC Determination

No Description Qty PN1 Molecular Sieve 3 Å 100g 338 018 012 Quartz Wool 5g 338 222 003 Soda Lime 200g 338 352 304 High Quality Copper 50g 338 353 125 Chromosorb ® WAW 25g 338 375 306 Oxidation Catalyst 40g 338 400 007 Silica Gel plus indicator 100g 338 400 35

Table 17-13. Consumables and Spare Parts for FlashEA IRMS and HT NC DeterminationsNo Description Qty PN1 Magnesium Perchlorate 100g 338 219 002 Quartz Wool 5g 338 222 003 Chromium Oxide 25g 338 229 004 Silvered Cobaltous- Cobaltic Oxide 25g 338 245 005 Reduced Copper 100g 338 353 00




18

58

Analytical Standards and Reference Materials

Table 18-1. Analytical Standards

* 2,5 bis (5-ter-butyl-benzoxazol-2-yl) thiophene ** Cyclohexanone 2,4-dinitrophenylhydrazone

Table 18-2. Reference Materials

No Description Qty PN1 Acetanilide 2g 338 367 002 Aspartic Acid 2g 338 400 223 Aspartic Acid 10g 338 400 234 Atropine 2g 338 244 005 BBOT* 2g 338 352 106 Benzoic Acid 2g 338 225 007 Cyclohexanone 2,4 DNPH ** 1g 338 224 008 dl-Methionine 25g 338 352 209 Imidazole 1g 338 354 30

10 L-Cystine 2g 338 400 1811 Nicotinamide 2g 338 400 1912 Sulphanilamide 2g 338 251 0013 Urea 2g 338 400 0114 Urea 10g 338 400 02

No Description Qty PN1 Lubricant Reference Material 2g 338 352 402 Pasta Reference Material 10g 338 400 243 Pasta Reference Material for S determination (OEA / FPD) 2g 338 400 274 Soil NC Reference Material 5g 338 400 255 Soil NCS Reference Material for NCS determination and S

determination (OEA/FPD)2g 338 400 26

6 OEA/FPD Reference Solutions Kit constituted by 4 flasks (2 mL each) containing 10, 50, 100 and 500 ppm for Sulphur

1 338 190 40


Chapter 18Analytical Standards and Reference Materials

IMPORTANT! All the standards and the references material are accompanied with a quality certificate including the storage condition and the lifetime of the products.

Standard N% C% H% S% O%Acetanilide 10.36 71.09 6.71 11.84Aspartic Acid 10.52 36.09 5.30 48.08Atropine 4.84 70.56 8.01 16.59BBOT 6.51 72.53 6.09 7.44 7.43Benzoic Acid 68.85 4.95 26.20Cyclohexanone 2-4 DNPH 20.14 51.79 5.07 23.00dl-Methionine 9.39 40.25 7.43 21.49 21.45Imidazole 41.15 52.93 5.92L-Cystine 11.66 29.99 5.03 26.69 26.63Nicotinamide 22.94 59.01 4.95 13.10Sulphanilamide 16.27 41.84 4.68 18.62 18.58Urea 46.65 20.00 6.71 26.64

Reference Material N% C% H% S%Lubricant (batch n° O12A) 0.58 76.44 12.00 2.40Pasta (batch n° H13A) 1.89Pasta for OEA/FPD (batch n° N12A) 0.134Soil NC (batch n° N12A) 0.20 2.01Soil NCS (batch n° N12A) 0.20 2.01 0.032

OEA/FPD Reference Solutions Kit 10 ppm of Sulphur (2 mL flask)50 ppm of Sulphur (2 mL flask)100 ppm of Sulphur (2 mL flask)500 ppm of Sulphur (2 mL flask)


19

60

Adsorber for Fluorine Compounds

Table 19-1. Adsorber for Fluorine CompoundsNo Description Qty PN1 FluoAdso

Specific adsorber for Fluorine compounds CHN, NC and N Determinations

15g 338 400 30

100 mm

50 mm

30 mm

20 mm

30 mm

10 mm

Reactor: Quartz TubeTemperature: 950 C

TCD

Temperature: 75 C

Quartz Wool

Adsorber

Chromium Oxide

Copper

Silvered Cobaltous-Cobaltic Oxide

Quartz Wool

FlashEA 1112-CHN Configuration for �Fluorine-containing Compounds


Chapter 19Adsorber for Fluorine Compounds


20

62

Kits for FlashEA 1112

Kit for Total Organic Carbon (TOC) in Solid Sample PN 190 041 28

Total Organic Carbon is a very important parameter for soil or for other organic matrix.The kit for TOC allows to eliminate all inorganic carbon as Carbon Dioxide by effect of the acidification and heating of the sample in special containers.

The kit includes the following material:

Part Number Description Quantity240 054 05 Silver sample container for solid (set of 100) 1334 130 36 Sample holder plate 1 354 600 17 Electric heater 1365 005 30 Syringe 1750 LT 500 μL 1

Sample Holder Plate and Electric Heater


Chapter 20Kits for FlashEA 1112

Oxygen Line Purge Kit PN 190 042 60

WARNING! Suggested for FlashEA 1112 models with serial number S/N up to 20034906The Oxygen Line Purge kit permits to eliminate the diffused air present in the pneumatic circuit of the oxygen line decreasing, at this way, the blank value and optimizing the OEA analysis.

The presence of the diffused air in the oxygen line may be due to the following reasons:

• damaged or worn out cylinder pressure regulator

• the length of the oxygen pneumatic line

The kit contains all the materials required to install the Oxygen Line Purge Kit on your FlashEA 1112:

Part Number Description Quantity290 040 45 Aluminium ferrules 10347 081 03 Tee connection 1350 004 03 6MB retaining nuts 7391 024 00 2x1 mm SS tubing 30 cm405 107 00 Needle valve 1


21

64

Sample Containers

Figure 21-1. Tin and Silver Containers

1. “Soft” containers are obtained by pressing light metal foil.2. “Hard” tin containers are heavier than the “Soft” ones and allow hermetic sealing. For this reason the “Hard” tin containers

are obtained by moulding ultrapure tin sheets.

NOTE You will find here an optimized guide for the best choice of containers tailored to your specific analytical needs, through a detailed specification both for tin and silver containers to be used according to the different applications. To avoid deformation problems and to guarantee a complete use of all the sample containers, these are conveniently supplied and protected in adequate plastic boxes in package of 50 and 100.

Tin ContainersTable 21-1. Tin Containers (See Figure 21-1)

Refer To: Description Qty PNA Universal “Soft” Tin Containers 100 240 064 00B Small “Soft” for Solid Sample 100 240 053 00C Tin Containers for N/Protein and N-Brew Analysis 100 252 080 00D “Hard” Tin Containers 100 240 088 10E “Hard” Tin Container 100 240 088 20F “Hard” Tin Container 50 240 072 00G “Hard” Tin Capillary 50 240 070 00H Tin Disks 30 mm diameter 100 252 080 15I Tin Disk 35 mm diameter 100 252 080 18

“Soft” (pressed tin/silver container)1 “Hard” (flat smooth bottom tin/silver container)2

A B C L M D E F G N


Chapter 21Sample Containers

Silver Containers

Tin Container Type UseA Recommended for solid samples (organics, soils, sediments, food, plastic, coal, etc.) or

liquid samples adsorbed on inert solid material Chromosorb® WAW (PN 338 375 30). See Figure 21-2.

B Recommended for solid samples.C Recommended for N/Protein and N-Brew Determinations.D Recommended for the analysis of any viscous sample. See Figure 21-2.E Recommended for the analysis of any liquids; for volatile liquids we recommended the use

of liquid sealing device (PN 205 030 02). F Suggested for analysis of trace elements (N, C, S) in liquids such as water, wine, beer,

milk, urine, etc.G Suggested for the analysis of liquid samples when the material is available in very small

amounts. Useful for volatile samples. Use of Sealing Device (PN 205 030 02) is highly recommended. For more details on Sealing Device please see Chapter Sample Preparation Accessories

H Use Sealing Device (PN 252 090 10)I Use Sealing Device (PN 252 090 10)

Table 21-2. Silver Containers (See Figure 21-1)Refer To: Description Qty PN

L Universal “Soft” Silver Containers 100 240 054 00M “Soft” Silvers Containers 100 240 054 05N “Hard” Silver Containers 50 240 051 00

Silver Container Type UseL Recommended for Oxygen determination for solid samples.M Recommended for Total Organic Carbon (TOC) determination according to the Thermo

Fisher Scientific method (patent n. 90110186.5). See Figure 21-3.See Kit for Total Organic Carbon (TOC) in Solid Sample PN 190 041 28 in Chapter 20.

N Recommended for Oxygen analysis of liquid samples (e.g. gasoline). The Sealing Device (PN 205 030 02), is highly suggested for these liquid samples.



Figure 21-2. Sampling Technique

Figure 21-3. T.O.C. Determination

Add Chromosorb 1 spatula

Weighing

Liquid Sampling Technique

TM

Add the liquid sample

on the Chromosorb surface

TM

Seal and Weigh

Viscous Sampling

Technique

Ag Capsules Add 5 - 20 mg of sample

WEIGHING

Add 1 drop of HCl 1:1

80 C

Leave at 80 C until dry

ANALYSING

1 2 3

4 5 6

Sampling Technique for T.O.C. Determination




22

68

Sample Preparation Accessories

Table 22-1. Sample Preparation AccessoriesRefer To: Description Qty PN

A Sealing Device for Solid Containers 1 205 003 10B Sealing Device for Large Tin Containers 1 252 090 10C Sealing Device for Liquid Containers 1 205 030 02D Pocket Sample Holder for Small Containers 1 240 100 24E Cleaning Device for Quartz Reactor and Crucible 1 276 060 10F Cleaning Device for HPAR Reactor 1 205 006 25-- Forceps 1 205 005 00-- Crucible Extractor 1 205 006 27-- HPAR Extractor 1 205 006 26-- Small Spatula for Container Filling 1 205 006 00-- Large Spatula for Container Filling 1 205 006 20-- Microsyringe 710 SNR 100 μl 1 365 002 04-- Microsyringe 10 μl 1 365 020 01

Ref. CommentsA Available on request.B Inserted in N/Protein, N-Brew, NC-Soils, NC-Sediments and NC Filters Standard Outfit.C Liquid device for liquid containers (available on request), allows the analysis of

hygroscopic solid compounds and volatile liquid substances without variation of weight. The samples are introduced in the container using a spatula, syringes or generic needles. We suggest the use of liquid tin containers or capillaries according to the viscosity of the liquid sample. The container is then placed in the sealing device slide. The container is to be purged with a flow of Oxygen or Helium before closing. The container is tightly closed and the constancy of weight is monitored by an electronic balance. For liquids with high vapor pressure use tin capillaries: the treatment with inert gas in not necessary because the vapor pressure generated by the liquid sample is sufficient to flush the atmospheric gases from the container.


Chapter 22Sample Preparation Accessories

D This device, available on request, is used to carry up to 52 weighed and sealed containers from the balance to the autosampler mounted on the instrument.

E Available in all FlashEA 1112 Standard Outfit Configurations. Recommended tools to clean the reactor when replacing the catalyst.

F Inserted in N/Protein, N-Brew, NC-Soils, NC-Sediments and NC Filters Standard Outfit.

Ref. Comments

A

C D

E F

B


23

70

MAS200 R Autosampler for Solid Samples

Spare PartsTable 23-1. MAS200 R Autosampler for Solid Samples-Spare Parts

No Description Qty PN1 Loading Spring 1 315 052 112 Positioning Spring 1 315 052 123 Gear Plate 1 358 006 264 MAS200 R Geared Motor 1 318 076 285 MAS200 R Plastic Front Cover 1 241 055 35

6 MAS200 R Complete Shaft 1 343 015 12

7 MAS200 R Drum No 1 (0 - 32 Position) 1 240 101 35


Chapter 23MAS200 R Autosampler for Solid Samples

Knurled Screws Kit

8 Additional MAS200 R Drum No 2 (33 - 63 Position) 1 240 101 369 Additional MAS200 R Drum No 3 (64 - 94 Position) 1 240 101 37

10 Additional MAS200 R Drum No 4 (95 - 125 Position) 1 240 101 3811 Window O-ring (Set of 10) 1 290 300 1412 MAS200 R Internal O-ring (Set of 10) 1 290 300 1713 MAS200 R Plastic Cover 1 241 044 7714 MAS200 R Assembly Motor 1 318 076 2415 MAS200 R Plastic Window 1 301 080 20

Table 23-2. MAS200 R Autosampler for Solid Samples-Knurled Screws KitNo Description Qty PN

Knurled Screws Kit (Set of 3) 1 190 042 57

This kit allows to further simplify the shaft cleaning procedure. By replacing with the practical finger-tightening knurled screws, the access to the shaft in the MAS 200 R autosampler for maintenance, can be performed in a jiffy. This kit is applicable on all MAS 200 models.

Table 23-1. MAS200 R Autosampler for Solid Samples-Spare Parts (Continued)



Switching BoxTable 23-3. MAS200 R Autosampler for Solid Samples-Switching Box

No Description Qty PNSwitching Box 1 432 101 52

When the analyzer is equipped with two MAS 200 R autosamplers, it is possible to switch from a channel to the other by using the dedicated Switching Box as schematically shown in the figure below.

21

43

MAS200 R"A"

MAS200 R"B"

Autosampler

SWITCHINGBOX

A B

A B




24

74

NoBlank Sampling Device

NoBlank sampler option is a special device, applied to OEA/IRMS and OEA instrument, which are the primary function to reduce the Nitrogen Blank Peak to a very low value. Reducing the Nitrogen Blank Peak Area means to increase the accuracy and precision power of the IRMS analyzer.The NoBlank sampler option can be installed on:

• FlashEA 1112 models, especially on IRMS and HT configurations

• TC/EA instruments and all previous Thermo OEA models as EA1110, EA 1108, NA 2500, etc.

For Ugrading FlashEA SystemTable 24-1. No Blank Sampling Device for Updating FlashEA Systems

No Description Qty PN1 No Blank Sampler Option

It is constituted to:

• NoBlank system

• Standard outfit

• Instruction manual

1 432 102 30


Chapter 24NoBlank Sampling Device

For Upgrading TC/EA and Previous OEA ModelsTable 24-2. No Blank Sampling Device for Upgrading TC/EA and Previous OEA Models

No Description PN1 No Blank Sampler Option 432 102 302 MAS 200 R with a 32 position drum 432 174 003 MAS Driver (for servo air automation to electric signal) 432 101 50

NoBlank Spare PartsTable 24-3. No Blank Spare Parts

No Description PN1 NoBlank rulon cone complete 281 135 202 NoBlank rulon cone o-ring 290 003 563 O-ring NoBlank bottom (set of 5) 290 003 17


25

76

CM2 Manual Sampler

NOTE CM2 Manual Sampler can be installed on 18 mm OD Quartz Reactor and 25 mm OD HPAR Reactor. The CM2 Standard Outfit contains both connections. The CM2 Standard Outfit also includes parts used for the FlashEA 1112 using 18 mm OD reactors, for the EA 1110 Elemental Analyzer, and other parts only for any FlashEA 1112 Configurations using the 25 mm OD oxidation reactor. Refer to the following table.

(*) All the configurations except N/Protein and NC-Soils

Table 25-1. CM2 Manual SamplerNo Description Qty PN1 CM2 Manual Sampler 1 251 026 50

PN Part Description Instrument Configuration350 084 17 Adapter for 18 mm OD reactors EA 1110 - FlashEA 1112 All the configurations (*)350 014 27 Nut 304 EA 1110 - FlashEA 1112 All the configurations (*)290 009 17 O-Ring 2068 EA 1110 - FlashEA 1112 All the configurations (*)350 084 18 Adapter for 25 mm OD reactors FlashEA 1112 N/Protein - NC-Soils350 014 65 Nut 1”1/4 FlashEA 1112 N/Protein - NC-Soils


Chapter 25CM2 Manual Sampler


26

78

AI/AS 3000 Autosampler for Liquids

AI 3000 AS 3000

Table 26-1. AI/AS 3000 Autosampler for Liquid Samples

No Description Qty PN1 AI 3000 Auto Injector for liquids 1 251 174 802 AS 3000 Auto Sampler for liquids 1 251 174 903 Upgrade option AI to AS 3000 190 502 30

4 10 μl syringe 1 365 005 255 50 μl syringe 1 365 040 40


Chapter 26AI/AS 3000 Autosampler for Liquids

6 100 μl syringe 1 365 040 417 250 μl syringe 1 365 040 42

8 8-position tray with label 1 240 101 409 105-position tray for AS 3000 1 240 101 45

10 Waste bottle complete with 5 septa and caps 1 240 124 1611 Complete Vials 2 SVW Package (Set of 100)

[Require screw top cap with septa PN 386 060 85]10 240 140 19

12 Vial Solvent 4 mL S T4-SVQ (Set of 5) [Require screw top cap with septa PN 386 060 85]

1 240 140 32

13 Septa for waste bottle (Set of 100) 1 313 032 1714 BTO Septa for FlashEA injector (Set of 50) 1 313 032 3015 Screw Caps for waste bottle (Set of 100) 1 386 060 7416 Screw Caps 8-SC (Set of 5) 10 386 060 85

Table 26-2. AI/AS 3000 Spare Parts

No Description Qty PN1 AI/AS 3000 M/S printing circuit board assy 1 152 200 602 Complete Base assy 1 221 071 003 Complete Top cover assy 1 241 055 704 Slide stepper motor 1 318 029 175 Front door AI/AS 3000 1 333 309 456 AI/AS 3000 bracket for FlashEA 1 368 127 427 Complete Tower assy 1 370 014 35

Table 26-3. AI/AS 3000 Cables

No Description Qty PN1 Power Cable 10A/250V 1 230 330 002 Power Cable 10A/125V 1 230 330 353 RS232 cable 1 230 434 534 Flat Cable Flex 26F/16F 1 230 436 10

Table 26-1. AI/AS 3000 Autosampler for Liquid Samples (Continued)


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AS 2000 Autosampler for Liquid Samples

Consumables and Spare PartsTable 27-1. Consumables and Spare Parts for AS 2000 Autosampler

No Description Qty PN1 Microsyringe 10 μl 1 365 005 252 Microsyringe 710 SNR 100 μl 1 365 002 043 Syringe 500 μl 1 365 005 30

4 Kit Washing Vials • Washing Vials 10 CV (Set of 5) PN 240 300 00 • Cap for Washing Vials PN 386 060 35

1 190 146 47

5 2 mL Vials (Set of 100) 1 240 740 416 Seal 8 mm Teflon-faced (Set of 100) 1 313 032 177 BTO Septa (Set of 50) 1 313 032 288 Plastic Spacers (Set of 100) 1 350 015 019 Plastic Screw Caps (Set of 100) 1 386 060 74

10 Plastic “Snap” Caps for 10 μl Vials (Set of 10) 1 386 100 15

11 Fuse, slow-blow, 800 mA, 5x20 mm (set of 2) 1 282 150 1112 Fuse, slow-blow, 1.6 A, 5x20 mm (set of 2) 1 282 140 18


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Accessories for Injection of Liquid and Gas Samples

Table 28-1. Accessories for Injection of Liquid SamplesNo Description Qty PN1 Manual Injection Device for Liquid or Gas Sampling 1 190 041 38

The Kit includes:• Injector body for OEA

• Coupling joint for liquid/gas

• Injection connection

• Different septum holders for every FlashEA 1112 and previous OEA models

• Syringes

— 10 μL

— 100 μL

— 500 μL

• Septa (set of 50)

Manual

Injection

Device


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Resting Foot Kit

In our continued instrumental design modification based on customer request to cover different lab table types we are now introduced the Resting Foot kit.The foot are robust, aluminum legs painted in the same FlashEA color.

The function of the kit is to lift the FlashEA chassis off the table top some additional millimeter (height: 25 mm) allowing more room for access the oven and opening of the traps compartment.

The Resting Foot Kit is an option and it can be order separately.

Table 29-1. Resting Foot Kit

No Description Qty PN1 Resting Foot Kit (Set of 4) 1 190 042 58


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Recommended Spare Parts

Table 30-1. Recommended Spare PartsNo Description Qty PN1 Complete Furnace (18 mm furnace adapter) 1 354 600 212 Complete Furnace (25 mm furnace adapter) 1 354 600 223 Complete HT Furnace

(18 mm furnace adapter, max temperature 1450 °C) 1 354 600 35

4 HWD 430 Detector 1 419 075 105 Heater for Oven 1 354 215 106 Temperature Sensor Pt 100 for Oven 1 403 110 957 Thermocouple Pt/Pt-Rh 1 403 200 058 HT Thermocouple Pt/Pt-Rh for FlashEA HT 1 403 200 069 Furnace Transformer for all FlashEA versions except HT 1 413 250 7510 Furnace Transformer for FlashEA HT 1 413 250 76

11 3.6 V Battery 1 219 015 0512 Fan V2S 1 406 003 00

13 Fuse, slow-blow, 1.6 A, 5x20 mm for AS 2000 1 282 040 1814 Fuse, slow-blow, 800 mA, 5x20 mm for AS 2000 1 282 050 11


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FlashEA 1112 FPD Option PN 432 101 45

The OEA / FPD option increases the sensitivity in Sulphur determination by using a highly selective and sensitive Flame Photometric Detector (FPD) coupled with the FlashEA 1112 Elemental Analyzer.This FPD option can be applied to any FlashEA configuration and it allows the determination of trace Sulphur (low limit: 10 ppm) in both liquid and solid compounds.

The OEA / FPD option comprises of:

• FPD 1112 detector module that includes the FPD detector and the pneumatic circuit to control the detector gases flows.

• FPD control module to control the detector parameters.

• FPD standard outfit.


Chapter 31FlashEA 1112 FPD Option

FPD Performance Specifications

OEA / FPD Reference Material

Table 31-1. FPD Performance SpecificationsLow Limit 0.001% (10 ppm) SulphurMax Limit 0.5% (5000 ppm) Sulphur

(for more info refer to FlashEA 1112 Technical Specifications)Gas Requirements Helium Chromatographic-grade purity

Air 99.995%Hydrogen 99.995%

Power Requirements 120/230 Vac; 50/60 HzHost Hardware Requirements Pentium Processor-operating system Windows® 2000 or XPHost Software Requirements Eager 300Dimension Gas Control box: 177 x 235 x 287 mm (l x h x d)

FPD Control Module: 180 x 85 x 485 mm (l x h x d)Mass Gas Control box: 5 kg

FPD Control Module: 6 kg

Table 31-2. OEA/FPD Reference MaterialDescription Qty PN

Pasta Reference Material for Sulphur Determination (OEA/FPD) 2g 338 400 27Soil Reference Material 2g 338 400 26Reference Solutions Kit constituted by 4 flasks (2 mL each) containing 10, 50, 100 and 500 ppm of Sulphur

1 338 190 40



OEA / FPD Detector Spare PartsRefer to the following figure:

Table 31-3. Flame Photometric Detector Spare PartsRef. Description Qty. P/N

1 Mirror plug 350 053 502A

Maintenance kit for FPD

Graphite seal 2

190 045 892B Heat shield 22C VitonTM O-ring 3106 12D VitonTM O-ring 3175 12E VitonTM O-ring 75 SH 13 Detector body 1 190 501 114 Heater/sensor/coil cable (1.5 m) 1 230 435 875 Aluminium O-ring 1 290 032 306 FPD jet 1 404 045 118 Flange and relevant VitonTM O-ring 1 368 142 359 Interferential filter for sulphur 1 281 070 0010 Photomultiplier 1 286 004 5011 FPD fixing tool 1 205 021 50

Silcosteel tubing 1 m; 0.4 mm OD x 0.25 mm ID 1 391 100 25Graphite ferrule ID 0.45 for silcosteel tubing (set of 2) 1 290 134 87Nut for or silcosteel tubing (set of 5) 1 350 324 23




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Cables

Table 32-1. CablesNo Description Qty PN1 Power Cable (Part of the FlashEA 1112 Standard Outfit) 1 230 330 002 RS 232 Cable (Part of the FlashEA 1112 Standard Outfit) 1 230 434 85


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Electronic Flow Controller Modules

Table 33-1. EFCt ModuleNo Description Qty PN1 EFCt Module (complete) for FlashEA 1112 models with serial

number S/N upper than 200349061 425 091 50

2 Flow Sensor 13 2-way Valve (Normally Open) 14 2-way Valve (Normally Closed) 15 Proportional Valve 16 3-way Valve 1

Table 33-2. EFC ModuleNo Description Qty PN1 EFC Module (complete) for FlashEA 1112 models with serial

number S/N up to 200349061 425 090 95

2 Flow Sensor 13 2-way Valve (Normally Open) 14 2-way Valve (Normally Closed) 15 Proportional Valve 16 3-way Valve 1


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Flash EA 1112 Electronics

Printed Circuit BoardTable 34-1. Printed Circuit Board

No Description Qty PN1 TRF1112 Transformer Board 1 236 484 452 MB1112 Mother Board 1 236 484 503 AC1112 Alternative Current Board 1 236 484 554 TRC1112 Thermo Control Board 1 236 484 605 HWD1112 TCD Control Board 1 236 484 656 CPU1112 Central Processing Board 1 236 484 707 PWR1112 Power Supply Card 1 236 484 808 DPFC1112 Electronic Flow Control Board 1 236 484 90

9 LTA-1 Thermo Coupled Linearizer Box 1 209 017 0010 LTA-1 HT 1 209 017 0310 EV Control Box 1 333 209 6011 Icon Panel (Complete) 1 333 105 45


Chapter 34Flash EA 1112 Electronics


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Eager 300 Ethernet A/D

Ethernet Box USB Version PN 432 331 36This Kit allows to upgrade all Eager 200 to Eager 300.

The Eager 300 Ethernet key comprises of:

• Ethernet adapter box

• Sentinel Key (USB version)

• Eager 300 Program (CD-Rom)

• Eager 300 Operating Manual

• Connecting cables for FlashEA 1112 and previous OEA modules.

Examples:

Ethernet Box for 2nd Channel (or 3rd Channel) PN 432 100 96Add-on channel(s) required for the connection of additional OEA instrument(s) to the same host PC. The Ethernet 2nd (and 3rd) channel comprises of all the above mentioned parts of the Eager 300 Ethernet A/D (PN 432 331 36) except for the Eager 300 software and the sentinel key.

Examples:

EA 1110 / Eager 200 EA 1110 / Eager 300 (with a PC with the minimum requeriments listed below)

FlashEA (TCD) + Eager 300 FlashEA (TCD+FPD) + Eager 300 and additional channel

N°1 EA 1110 with Eager 300 + N°1 PC N°2 EA 1110 with Eager 300 and USB box 2nd channel + N°1 PC.


Chapter 35Eager 300 Ethernet A/D

Eager 300 Upgrade Kit without A/D Converter PN 190 042 30The kit allows to upgrade Eager 200 equipped with Chromatography Card (PC with ISA slot) to Eager 300 (same PC with ISA slot).

The Eager 300 upgrade kit without A/D converter comprises of:

• Eager 300 software CD-Rom

• Sentinel key (parallel version)

• Instruction Manual

Examples:

Eager 300 Hardware Minimum Requirements

EA 1110 / Eager 200 (PC with ISA slot) EA 1110 / Eager 300 (PC with ISA slot)

Table 35-1. Hardware Minimum RequirementsComponent Description

Computer Any PC can be used, including laptop computerOperating System: Windows™ 2000 / XPPentium Processor minimum 256 MHzHard drive with at least 1 GB freeOne free COM port for instrument controlOne free COM port for balance, if requiredOne free COM port for AI/AS 3000 autosampler, if requiredCD driver

Monitor Color 102 4x 768 or betterPrinter Any printer accepted by the operating system


36

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Single to Double Furnace Upgrade Kit

The kit allows to trasform the configuration of your analyzer, e.g CHN or CHNS, equipped with a single furnace, in a configuration having two furnaces, e.g CHN-O or CHNS-O.

The kit is suitable for every FlashEA models.

Table 36-1. No Description Qty PN1 Single to Double Furnace Upgrade Kit

It is constituted to:

• Furnace

• Plate

• Connections

• Fittings

• Accessories

1 190 042 77


Chapter 36Single to Double Furnace Upgrade Kit


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Furnaces Transformation Kits

FlashEA Configuration

1. O/N Determination 2. NC Determination

Furnace L Bottom Conn. L Furnace R Bottom Conn. R

CHN, CHNS, NCS, O yes (18 mm) 2x1 mm no no

CHN/O or CHNS/O yes (18 mm) 2x1 mm yes (18 mm) 2x1 mm

N Org yes (18 mm) 4x2 mm yes (18 mm) 4x2 mm

N Lubricant yes (25 mm) 6x4 mm yes (25 mm) 6x4 mm

NC org yes (18 mm) 4x2 mm yes (18 mm) 4x2 mm

NC Soils yes (25 mm) 4x2 mm yes (18 mm) 4x2 mm

N / Protein yes (25 mm) 6x4 mm yes (25 mm) 6x4 mm

FlashEA IRMS yes (18 mm) 2x1 mm yes (18 mm) 2x1 mm

FlashEA HT yes (18 mm)1 2x1 mm yes (18 mm)2 2x1 mm


Chapter 37Furnaces Transformation Kits

Transformation Kits AvailableIMPORTANT! The transformation kits do not include the furnace but the adapters, connectors,

plate assembly, etc.

According to the option reported in Table A and Table B, four different kits are available: 1 Transformation furnace kit (from 25 to 18 mm, bottom connector 2x1 mm) 190 042 512 Transformation furnace kit (from 25 to 18 mm, bottom connector 4x2 mm) 190 042 523 Transformation furnace kit (from 18 to 25 mm, bottom connector 6x4 mm) 190 042 714 Transformation furnace kit (from 18 to 25 mm, bottom connector 4x2 mm) 190 042 72

Example: from CHNS/O to NC Soils modelCHNS/O: 2 furnaces 18 mm; both bottom connections 2x1 mm

NC Soils: 2 furnaces (25 mm, 18 mm); bottom connection 4x2 mm

For this modification needs:

• Transformation kit (from 18 to 25 mm, bottom Conn. 4x2) n.1

• Bottom Connection (18 mm, 4x2 mm) n.1

• 4 x 2 SS tubing and relative joints



If the user want to add a new furnace (and upgrade the instrument configuration)

Transformation Furnace Kits ListThe items inserted in the transformation kits are here listed:

In this case the user needs need a complete furnace and a transformation furnace kit.A furnace will be chosen according to the application (18 or 25 mm type) while the kit will be used for find all the top level FlashEA reactor connection (on the top level of the instrument) and for the bottom connection according to the analysis requested:

• 18 mm, bottom connection 2x1 mm




Example: CHN (single furnace) CHN/O (double furnaces)For this modification needs:

• Complete furnace (18 mm diam) p/n 354 600 21

• Transformation kit (18 mm, bottom Conn. 2x1 mm) p/n 190 042 51

• 2 x 1 SS tubing and relative joints



No Description Qty PNTransformation Furnace Kit from 18 to 25 mm bottom connection 6x4 mm

1 190 042 71

1 Furnace Adapter 12 Bottom O-ring (Set of 5) 13 Top O-ring (Set of 5) 14 Seal for Furnace Adapter; 25 mm 15 Aluminium Ferrule; 2 mm diam. 66 Plate assembly (circular) 17 6MB nut (set of 10) 18 Fixing Cup 19 Cup (5x3 mm) 4

10 Tube connector for PTFE; 5x3 mm 411 Top Connector (25 mm) 112 Screw (4x20 mm) 213 Polyethylene Tube; 5x3 mm; 1 m 114 Clip (Filter fixing) 415 Pressure Equilibration Cylinder 116 Clip (Pressure equil. Cylinder fixing) 117 Teflon Tube; 2x1 mm; 1 m 118 Bottom Connection (25 mm diam; 6x4 mm) 119 PTFE Tube; 6x4 mm; 1 m 1 20 OR/OV Viton 121 Nut, M 12x1 mm 122 Plate Assembly (rectangular) 123 Screws for plate assembly (circular) 3




1 190 042 72

1 Furnace Adapter 12 Bottom O-ring (Set of 5) 13 Top O-ring (Set of 5) 14 Seal for Furnace Adapter 25 mm 15 Aluminium Ferrule 2 mm diam. 66 Plate assembly (circular) 17 6MB nut (set of 10) 18 Fixing Cup 19 Top Connector (25 mm) 1

10 Screw (4x20 mm) 211 Clip (Filter fixing) 412 Teflon Tube; 2x1 mm; 1m 113 Bottom Connection (25 mm diam; 4x2 mm) 114 PTFE Tube; 4x2 mm; 1 m 1 15 4 mm OD Ferrule (Set of 10) 116 Nut, M1; 2x1 mm 117 Plate Assembly (rectangular) 118 Screws for plate assembly (circular) 3




1 190 042 51

1 Furnace Adapter 12 Bottom O-ring for 18 mm OD Quartz Reactor (Set of 5) 13 Top O-ring for 18 mm OD Quartz Reactor (Set of 5) 14 Seal for Furnace Adapter 18 mm 15 Plate assembly (circular) 18 mm diam. 16 6MB nut (set of 10) 17 Fixing Cup; 18 mm 18 Top Connector (18 mm) 19 Screw for Filter Clip 2

10 Filter Clip 211 Teflon Tube; 2x1 mm; 1 m 112 Bottom Connection; 18 mm diam; 2x1 mm 113 PTFE Tube; 2x1 mm; 1.5 m 114 Ferrule (Set of 10) 115 Plate Assembly (rectangular) 18 mm diam. 116 Screws for plate assembly (circular) 3




1 190 042 52

1 Furnace Adapter 12 Bottom O-ring for 18 mm OD Quartz Reactor (Set of 5) 13 Top O-ring for 18 mm OD Quartz Reactor (Set of 5) 14 Seal for Furnace Adapter;18 mm 15 Plate assembly (circular) 18 mm diam. 16 6MB nut (set of 10) 17 SS Tube; 2x1 mm 3 m8 Top Connector 18 mm 19 Screw for Filter Clip 2

10 Filter Clip 211 Fixing Cup; 18 mm 1 m12 Bottom Connection; 18 mm diam; 4x2 mm 113 PTFE Tube (4x2 mm) 1.5 m 14 Ferrule (Set of 10) 115 Fixing Nut 116 Ferrule 2x1 mm (Set of 10) 117 PTFE Tube; 2x1 mm; 1.5 m 118 Plate assembly (rectangular); 18 mm diam. 119 Screws for plate assembly (circular) 3



Transformation Furnace Kit: Explanations on Some Items

Plate AssembliesThe rectangular (18 and 25 mm) plate has been mounted on FlashEA 1112 till fall 2003 (serial n.20034136) and then it has been substituted by the circular (18 and 25 mm) plate. Both Plate Assemblies (rectangular & circular) are inserted in the Transformation Kits.

Top Connections

Rectangular Circular

No Description PN1 Plate Assembly (Rectangular) 18 mm 334 012 292 Plate Assembly (Rectangular) 25 mm 334 012 303 Plate Assembly (Circular) 18 mm 350 084 604 Plate Assembly (Circular) 25 mm 350 084 65

No Description PN1 Top Connector 18 mm 350 084 212 Top Connector 25 mm 350 084 23



Furnace AdaptersThe washer adapter (18 or 25 mm) is placed on the top of the furnaceUnder the washer is placed the suitable seal.

Bottom Connections

No Description PN1 Furnace Adapter 18 mm 267 027 222 Furnace Adapter 25 mm 267 027 213 Seal for Furnace Adapter 18 mm 290 036 324 Seal for Furnace Adapter 25 mm 290 036 33

18 mm diameter 25 mm diameter

No Description PN1 Bottom connection (18 mm diameter; 2x1) 350 084 332 Bottom connection (18 mm diameter; 4x2) 350 084 323 Bottom connection (25 mm diameter.; 6x4) 350 084 264 Bottom connection (25 mm diameter; 4x2) 350 084 31



Bottom Connections for FlashEA IRMS and HT (O/H and NC Determinations)

The FlashEA 1112 bottom connection for IRMS and for HT is different from other OEA configurations. The bottom connection is constituted by the following parts:

IMPORTANT! According to the FlashEA configurations, if necessary to have a complete system the following parts should be ordered:

• Bottom Connection (if requested)

• Reactors (quartz or special stainless steel)

• Crucible (quartz or special stainless steel)

• Filter (small or large)

• Separation column

• Catalysts

• Adsorber

No Description PN1 Nut 350 114 102 Metal Ring 356 032 103 Washer 290 029 104 Reactor Coupling Union 350 084 27


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MAS 200 R Driver

The MAS200 R Driver is a device which allows to the older OEA models (EA 1110, NA 2100, EA 1108 etc.) equipped with the pneumatically actuated AS 128 or AS 200 autosamplers to be up-graded to the new electrically actuated MAS 200 R.

The MAS200 R Driver is easy to install and it will be provided with a detailed installation guide.

AS 128 / AS200Pneumatic actuated autosamplers for EA1110, EA 1108 and TC/EA, NA2500, NA1500 etc.Utilities: Servo Air + Helium / Oxygen

The AS 128 and AS 200 on previous OEA models can be replaced by this system: MAS200 R (PN 251 17400) + MAS200 R Driver (PN 432 10150) Utilities: Helium / Oxygen

MAS 200 R Driver

AC Adapter


Chapter 38MAS 200 R Driver

No Description Qty PN1 MAS200 R Driver 1 432 101 50

The MAS200 R Driver includes:MAS200 R Driver base unitAC adapter / power modulePower cordCable providedCable for IRMS

Dimensions & weight:Dimensions (w x d x h): 80 x 146 x 45 mmMass (MAS Driver base unit): 200 gMass (MAS Driver complete including power module, cables etc.): 900 g


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Flash EA 1112 Validation

Validation is a process to evaluate and certify the performances of the instrument.Validation is a process of signing, dating and executing a set of qualifications which can be stored in the Thermo Validation folder.FlashEA 1112 equipment and the relative Eager 300 software is validated for the installation (Installation Qualifications IQ), operation (Operation Qualification OQ) and performance (Performance Qualification PQ). The procedure requires typically two (2) days of “on-site” testing including executing, dating, and signing a set of qualifications which are stored in the Thermo Validation Folder.

No Description Qty PN1 FlashEA 1112 Validation Package Folder 1 199 100 302 AI/AS 3000 for OEA Validation Package 1 199 100 05


Chapter 39Flash EA 1112 Validation

For the FlashEA validation are requested:

• The FlashEA Validation Package folder (PN 199 100 30)

• One (or more) validation kit according to the configuration which consists of consumables, standards, filters and GC separation column (all components required for the validation procedure).

Chart of Validation Kits

WARNING! The FlashEA Validation can be done with Thermo OEA consumables esclusively.

The FlashEA Validation can be carried out only by trained Thermo OEA specialist.

No Description Qty PN1 CHN Validation Kit 1 190 042 802 CHNS Validation Kit 190 042 853 O Validation Kit 190 042 904 N Org Validation Kit 190 042 955 NC Org Validation Kit 190 043 006 NCS Validation Kit 190 043 057 NC-Soil Validation Kit 190 043 108 N/Protein Validation Kit 190 043 159 N-Brew Validation Kit 190 043 20

10 AI/AS 3000 Validation Kit 190 043 25


Chapter 39Flash EA 1112 Validation



A
Customer Communication
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How To Contact UsThis appendix contains contact information for Thermo Fisher Scientific S.p.A office. To contact your local Thermo Fisher Scientific office or affiliate, please refer to:

Thermo Fisher ScientificVoltaweg 222627 BC Delft, the Netherlands

Tel: +31 15 257 13 14Fax: +31 15 257 22 97

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Documents

Elemental Analyzer Consumables and Spare Parts Catalog · 6 Consumables and Spare Parts Catalog 1 CHN Determination Table 1-1. Consumables and Spare Parts for CHN Determination Refer