E & E INC - EXPANDED SITE INSPECTION REPORT - VOL 3 OF 4 - … · 2020-02-20 · expanded site inspection report for h.o.d. landfill antioch, illinois u.s. epa id: ild980605836 ss

EXPANDED SITE INSPECTION REPORTFOR

H.O.D. LANDFILLANTIOCH, ILLINOIS

U.S. EPA ID: ILD980605836SS ID: IL2F

TDD: F05-8702-124PAN: FIL0141XB

VOLUME 3 OF 4

Field Investigation Team Zone II

EPA39

HAZARDOUSSITEEVALUATIONDIVISION

CONTRACT NO.68-01-7347

EXPANDED SITE INSPECTION REPORTFOR

H.O.D. LANDFILLANTIOCH, ILLINOIS

U.S. EPA ID: ILD980605836SS ID: IL2F

TDD: F05-8702-124PAN: FIL01A1XB

VOLUME 3 OF 4

SEPTEMBER 22, 1989

ecology and environment, inc,111 WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL 312-663-9415

International Specialists in the Environment

recycled paper

TABLE OF CONTENTSVOLUME 3

Appendix • Page

G LABORATORY ANALYTICAL DATA OF FIT-COLLECTED SUBSURFACESOIL SAMPLES.............................................. G-l

11

APPENDIX G

LABORATORY ANALYTICAL DATAOF

FIT-COLLECTED SUBSURFACE SOIL SAMPLES

G-l

ROUTINE ANALYTICAL SERVICES

CONTRACT REQUIRED DETECTION AHD QUAHTITATION LIMITS

Contract Laboratory ProgramTarget Analyte Ujt

Inorganic Quantitation Limits

COKFOUND

Aluminum. Ant loony

ArsenicBarltmBerylliumCadalumCalciumChromiumCobaltCopperIronLeadKagnesiumKanganeseKercuryKickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

PROCEDURE

ICPFurnacefurnace1C?ICPICPICPICPICPICPIcpFurnaceICPICPCold VaporICPICPFurnaceICPICPFurnaceICPICP

SOILVATER

200 ug/L601020055

50001050251005

5000150.240

5000510

5000105020

SEOIHEKTSLUDGE

*0 ag/Kg2.424011

10002105201

100030.0088

100012

10002104

Cyanide Color 10

Contract Laboratory ProgramTarget Compound List

Pesticide and PCS Quantitation Limits

COMPOUND

alpha-BBCbeta-BBCdelta-BBCgamioa-BflC (Lindane)BeptachfcoCAldriaBeptachlor epoxldeEndosulfan IOieldrln4.4MXTCEndrioEndosulfan H4,4'-000Endostufan sol fate4t4'-ODTHethoxychlor (Maria te)End r in ketooealpha-Chlordinefault— chlordaneToxapheneAROOJO&-1016AROCLOR-1221AROCLOR-1232AROCLOR-1242AROCLO&-1248AROOO&-1254AROCLOR-1260

CAS ff

319-84-6319-85-7319-86-858-89-976-44-e

309-00-21024-57-3959-98-860-57-172-55-972-20-8

33213-65-972-54-8

1031-07-850-29-372-O-5

53494^70-55103-71-95103-74-28001-35-2

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

WATER

0.05 tig/L0.050.050.050.050.050.050.050.100.100.100.100.100.100.100.50.100.50.51.00.50.50.50.50.51.01.0

SOILSEOIKEKT

SLUDGE

8 «g/X«8888888

1616161616161680168080

1608080808080

160160


Seaivolatlles QuantiUtIon L

COMPOUND

Pluorene4-Nltroaqillne4 , 6-Olnl tro-2*«e thylphenolH-nitrosodlphenylaalne4-Bronophenyl~phenyletberBexachlorobenzeneFen tachlorophenolPhenan threatAnthraceneDi-o-butylphthalateFluoranthenePyreneButylbenzylpbthalate3f3'-0ichlorobentldlneBe&zo(a)*nthraceneChryceneb 1 a (2-E tbylhexyl) ph thala t eDi-n-octylphthalateBenzo(b) floortn thcaeBenzo(k)noorantheneBenxo(a)pyreneXndeao(lv2t3-«d)pyreneDlbenz(afh)antAraceneBenzo(g(ht l)perylene

CAS 1

86-73-7100-01-6534-52-186-30-6

101-55-3118-74-187-86-385-01-8

120-12-784-74-2

206-44-0129-00-085-68-791-94-156-55-3

218-01-9117-81-7117-84-0205-99-2207-08-950-32-8

193-39-553-70-3

191-24-2

VATER

10 ug/L5050101010501010101010102010101010101010101010

SOILSLUDGE

SEDIMENT

330 ug/Kg16001600330330330

1600330330330330330330660330330330330330330330330330 -330


Se»lvol«tll«s Quantitatloa Limits

COMPOUND

Phenolbis(2-Chloro«thyl) ether2 -Oilo ro phenol1 f 3-Oichlorobenzene1 f 4-OlchlorobenzeneBenzyl Alcohol1 , 2-Oichlorobenzen«2-Hethylphenolbls(2-Chlocolsopropyl) ether4-HethylphenolN-Nitroso-dl-a-dipropylaalneBexachloroe thaneNitrobenzeneIsophorone i2-Nitrophenol2,4-OiBethylphenolBenzole Acidbls(2-Chloroethoxy) Methane2 , 4-Oichloropbenol1,2,4-TrlcalorobenzeiieNaphthalene4-ChloroanillaeBexachloroba tad iene4-Chloro-3-*ethylphenol2-He thylnaph thalen«Bexachlorocyclopentadlene2 , 4 , 6-Trlchloropbenol2 « 4 1 5-Trlcbloro phenol7— TMi>rfwiiphT*'*l Tvt2-MitroanllineOinethylphthalateAcenaphthylene2 , 6-Olnl t rotoloene3-NitroanilineAcenaphthene2 , 4-Olni trophenol4-NltrophenolDlbenzoCuran2,4-DlnltrotolueneDlethylphthalate4-Chlorophenyl-phenyl ether

CAS 1

108-95-2111-44-49S-57-8541-73-1106-46-7100r51-695-50-195-48-7108-60-1106-44-5621-64-767-72-1 .98-95-378-59-188-75-5105-67-965-85-0

Ul-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-4M-Sft-7^w— •88-74-4131-11-3208-96-8606-20-299-09-283-32-951-28-5100-02-7132-64-9121-14-284-66-2

7005-72-3

VATER

10 ug/L10101010101010101010101010101050101010101010101010105010501010105010505010101010

SOILSEDIMENTSLUDGE

330 ug/T330330330330330330330330330330330330330330330160033033033033033030033033033033016003301600330330330160033016001600330330330330

Contract Laboratory ProgramTarget Coapound ListQuantltatlon Ll«its

COMPOUND

Chloroae thaneBcooooe thaneVinyl chlorideChloroe thaneKethyltn* chlorideAcetoneCarbon disulfide1 1 1-dichlocoetheneltl-dlchloroe thane1,2-dichloroethene (total)Chloroform1,2-dichloroe thane2-butanone (HEX)1,1, 1-trichloroethaneCarbon tetrachlorldeVinyl acetateBrooodichlorooe thane1,2-dlchloropropanecls-lf3-dlchloropropeneTrichloroetheoeDibroftocblor o*e thane1 1 l«2-trlchloroe thaneBenzeneTrans-1 ,3,-dichloroBtopeneBrooofon4-Kethyl-2-pentanoae2-BexftnoneTe t rachloroe theneTolene1 , 1 , 2 , 2-tetrachloroe thaneChlorobenzeneEthyl benzeneStyreneXylenes (total)

CAS I

7A-87-374-83-975-01-A75-00-375-09-267-64-175-15-075-35-A75-34-3

S40-S9-067-66-3

107-06-278-93-371-55-656-23-5

108-05-475-27-478-87-5

10061-01-579-01-6

124-48-179-00-571-43-2

10061-02-675-25-2 -

108-10-1591-78-6127-18-4108-88-379-34-5

108-90-7100-41-4100-42-51330-20-7

VATER

10 ug/L1010105

10555555

1055

10555555555

10105555555

SOILSEDIMENT

SLUDGE

10 ug/K«10101055555555

1055

10555555555

1010 -5555555

ecology and environment, incr111 WEST JACKSON BLVD.. CHICAGO. ILLINOIS 60604, TEL. 312-663-9415


FTDate Received for ReviewTO: ^VnFrom: Zena Gold-KaufmSubject: HOO

PAN:

Date Review Completed

Case

Sample Description______Organics (VOA, ABN, Pest/PCB

Kb Low SoiLow WaterDrinking WaterOther

Inorganics (Metals, Cyanide)

Low SoilLow WaterDrinking WaterOther

•Project Data Status Completed!

Incomplete, awaiting:

FIT Data Review Findings:Samples

Voft 51/UJm fLSb? o>>'

Cci nrnOA jlttirQjrd p /LO lfe .

Compounds were detected in sample(s); see enclosed Chemical• Evaluation Form.

Book No. Page No. sk

/if

: T/t/17

UNITED STATES ENVIRONMENTAL PROTECTION AGENCYREGION V

LJM It. i f f y u f .—•

/•^

SUBJECT: Review of Region V CLP Data..Received for Review on

FROM: Curtis Ross, Director (5SCRL)Central Regional Laboratory

TO: Data User: pi T

We have reviewed the data for the following case(s).

SITE NAME:__ttoT) ZÂfSFfC*-__________SMO case No.No. of D.U. /Activity

ERA Data Set No .spy* tr/SF*to<.9 Samples: /& Numbers

CRL No.

SMO Traffic No. g7 Mrs. Required

CLP Laboratory: ^/V/I//ÔDVAJ*£' for Review:

Following are our findings:

^-^^ P&sr/c,/z>e/'p<L8'5 ,#7- /*7&>sur> êTi/^'c FOR v&ur/ces . .i, OTM€# AMfityscs uje*.g fir

( ) Data are acceptable for use.(**) Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory(z<) Data are unacceptable. *& e<_*67 p&r

cc: Duane Geuder, Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas

EPA FORM 1320-6 (Rev. 5/87)

//

DATA QUALIFIERS

CfCase TV

Below is a summary of the out of control audits and the possible effecton the data for this case:

X

<?/r ,$•> fc- rve

/5

V

Reviewed by:

Phone:

Date:

//

DATA QUALIFIERS

Contractor:Case 735-v

. . - . - . . . - .Below Is Vsummary of the out of control audits and the possible effecton the data for this case: rf\

AT

AT

TO

Reviewed by:

Phone:

Date:

I

CASE*

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDS7357 - - - CONTRACTOR £

W/#y7&Av?»7- 5-?**--*

DATE/TIME:

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Oisulfide1,1-Dichloroethane1,1-Dichloroethene>ans-l,2-Dichloroethene

^vhloroform2-Butanone1,2-Dichloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1,2-DichloropropaneTrans-l.3-D1chloropropeneTrichloroetheneDi bromoch 1 oromethane1,1,2-Tri ChloroethaneBenzeneci s-1 ,3-Di chl oropropene2-Chl oroethyl vi nyletherBromofonn'-Methyl -2-Pentanone

-]2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorobenzeneEthylbenzeneStyrenem-Xvleneo/p-Xylene

AFFECTEDSAMPLES:

nit. Cal.C-3-S7

F

•

IRSD *

€Tor-€J-;aJttjr4-«j4-7et-*etf3ffCSJ-tf^Jl)

Cont. Cal.*->J7/'*:VX

RF %0

591 3

3/2

3.J.Or/.A

37. A

*

J

J

JJ

3"

«JI*T" erwie<- ui- cuts*

Cont. Cal .\-^.f? /607

RF to3/3

*

J

fcCa^TyHJ

Cont. Cal.•y-rr /tt:*3

RF ID

*

*

€cas-?/*fS5

Cont, Cal. '*\

RF *D *

vo

These flags should be applied to the analytes on the sample data sheets.

1/87

//

UNITED STATES

CASE* 7W/ '

/#&—£**** €*>T ***$•-/DATE/TIME:

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMethylene ChlorideAcetoneCarbon Pisulfide1,1-Dicnloroethane1,1-DichloroetheneTrans-l,2-DichloroetheneChloroform2-Butanone1,2-Di chl oroethane1 , 1 ,1-Tri chl oroethaneCarbon TetrachlorideVinyl AcetateBromodi ch 1 oromethane1 , 2-Di chl oropropaneTrans-l,3-DichloropropeneTrichloroetheneDibromochl oromethane1 ,1 ,2-Tri chl oroethaneBenzeneci s-1 ,3-Di chl oropropene2-ChloroethylvinyletherBromoform4-Methyl-Z-Pentanone2-KexanoneTetrachloroethene1,1,2 ,2-Tet rachl oroethaneTolueneChlorobenzeneEthylbenzeneStyrenem-Xyleneo/p-Xylene

AFFECTEDSAMPLES:

EWIRONMENTAL PROTECTION AGENCY REGION V. CALIBRATION OUTLIERS -VOLATILE HSL COMPOUNDS _ '£

" * CONTRACTOR &twtoSb>*J£ \e

nit. Cal.&-S~-€7

F

•

XRSD3f

*

O"

&JU.9- fLJLC*

..

Cont. Cal.£•//•>? /C-lfRF %D

— •

*,0"

*r^S(io

--T^— — -—— ' -

Cont. Cal.-'/ *7//?.'/e

RF XD

s*>

*

J

J-

zt-s&i-etA^-s

Cont. Cal.•/A-f7A:a*

RF ID

vy

3<*

'

*

J3*

, -

et?4^-frX364

Cont. Cal.

RF •-o

-

*

• • . . -.; j t

\^^

1

V3

tP


CASE*

UNITED STATES EHVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDSCONTRACTOR

-DATE/TIM£:ChloromethaneJromometnaneVinyl ChlorideChloroethaneMetnylene ChlorideAcetoneCarbon Oisulfide1,1-Dichloroethane1,1-DichloroetheneTrans-1 ,2-DichloroetheneChloroform2-Butanone1,2-Dicnloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1,2-DichloropropaneTrans-1 ,3-Di chl oropropeneTrichloroetheneDi bromochl oromethane1,1,2-Tri ChloroethaneBenzeneci s-1 ,3-Di chl oropropene2-Chl oroethyl vi nyl etherBromoform4-Methyl-Z-Pentanone2-HexanoneTetrachloroethene1,1,2 ,2-Tet rachl oroethaneTolueneChlorobenzeneEthyl benzeneStyrenem-Xyleneo/p-Xylene

AFFECTEDSAMPLES:

nit. Cal.£-AT- ? 7

F

-

•

tRSO

7^6>9

•- -

*

•To

&J3CS)«6»t7-««

i=<J47/ aO

;ont. Cal .•vd'-/7//'-''*IF %D

?<6

JJ*31

48

37

*

J"J

J0"

0*

J*

^ca<i7<=£-*& 7#SffC?67>H5&

Cont. Cal.lCont. Cal .

RF ID * RF-

ID

-

*

-

Cont. Cal.

RF %D *

k\

* These flags should be applied to.the analytes on the sample data sheets,

1/87

CASE*

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION .OUTLIERS

SEMIVOLATILE HSL COMPOUNDS. .. j. :.: JPage 1)

"• •-• : ' • - - ' - - ; - CONTRACTOR

• / **y4b*>ifMT s~??<~DATE/TIME:

Phenolbis(-Z-Chloroetnyl JEther2-ChloPOphenoll,3-0ichlopobenzene1 ,4-Di chl orobenzeneBenzyl Alcohol1,2-01 chl orobenzeneZ-Methylphenolbis(2-chlopoisoorooyl JEther4-Methyl phenolN-NitPOSO-Di-n-? ropy 1 ami neHexachlopoethaneNitrobenzeneIsoohoponeZ-Nitrophenol2, 4-01 methyl phenolBenzole Addbis(2-Chlopoethoxy)Methane2 ,4-DI cnl opophenol1 ,2 ,4-Tpi chl orooenzeneNaphthalene4-Chloroan111neHexachlopobutadiene4-ChloPO-3-Methyl phenol2-Methyl naphthaleneHexachl opocyclooentadi ene2,4 ,6-Tpi chl opoohenol2,4,5-TplchloPophenol2-Chloponaohthalene2-NitPoanil1neDimethyl PhthalateAcenaohthylene3-NitPoanilineAcenaphthene2,4-DinitPOPhenol4-NitrophenolOlbenzofuran

AFFECTEDSAMPLES:

Enit. Cal.^-/?-Jf7RF XRSD *

•

^.y&>?.£>

?Tf

j

JO*

«=j-/as~€JWW>»S<£JV< r>»*&T/-7C.

:ont. Cal. Cont. Cal.

RF *D

••-.

*

--

"- - -

RF -0 *

;ont. Cal.lCont. Cal.

RF

.

•

%D * RF %0

-

*

* These flags should be applied to the analytes on the.samole data sheets,

CASE*


SEMIVOLATILE HSL COMPOUNDSPage 2CONTRACTOR

•xv/#STKtv»etoT $"?f&.

DATE/TIME:

2,4-D1nitrotoluene2,6-OinitrotolueneDiethylpmnalate4-Chloroohenyl-phenyletnerFluorene4-N1troaniline4,6-D1nitro-2-MethylphenolN-Ni trosodi pheny 1 ami ne4-3romoohenyl-phenyletnepHexachl orobenzenePentachl orophenolPhenanthreneAnthraceneDi -n-Buty } phtnal ateFluoranthenePyreneButyl benzyl phthal ateBenzo( a) Anthracenebis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyt PhthalateBenzo( b )F1 uorantheneBenzo(k)FluorantheneBenzo(a)PyreneIndeno(l,2.3-cd)PyreneOibenz(a,h)AnthraceneBenzo(g,h,1 ) Perylene

[nit, Cal.£•/» - 9 7RF 1RSU

SQg

*

CT

Cont, Cal.

RF %U

-

*

Cont. Cal.lCont. Cal.

RF I ID * RF

•

ID *

Cont. CiV.*£«

RF M * • t

SEE PAGE 1 FOR AFFECTED SAMPLES.


1/87

CASE?


SEMIVOLATILE HSL COMPOUNDS(Page 1)

CONTRACTOR \/W57*c4/>7fA/r $-rr&DATE/TIME:

Phenolbis(-2-Chloroethyl )Ether2-Chloroohenol1 ,3-Oi chl orobenzene1,4-01 en 1 orobenzeneBenzvl Alcohol1 ,2-5 i chl orobenzene2-Mernylohenolbisi2-chloroisoorooyl JEther4-Metnyl phenolN-Nitroso-Di-n-? ropy 1 ami neHexachloroethaneNitrobenzeneIsoohorone2-Nitrophenol2, 4-Qi methyl phenolBenzoic Acidbi s ( 2-Ch 1 oroethoxy )Methane2,4-Oichlorophenol1,2,4-TrichlorooenzeneNaonthalene4-ChloroanilineHexachlorobutadiene4-Chloro-3-Methyl phenol2-Methyl naphthaleneHexachl opocyclooentadi ene2,4t6-Trichloroohenol2,4,5-Trichlorophenol2-ChloronaPhthalene2-Nitroanil1neDimethyl PhthalateAcenaohthylene3-NitroanilineAcenaohthene2,4-D1nitroohenol4-iNitroohenolDibenzofuran

AFFECTEDSAMPLES:

Init, Cal.C'tj-g-r

RF XRSD *

I1

•

<&&3L.S-

Cont. Cal. Cont. Cal. Cont. Cal. Cont. Calic^

RF %D

O"3"

er/37^rag

€-<-?j<-ffd*47

-

* RF %0 *

1

i

iRF ID » RF %D *

•

1 1

i

* These flags should be applied to the analytes gn,the.sample data sheets

1/87

CASEI 73^7


SEMIVOLATILE HSL COMPOUNDSPage 2 __

CONTRACTOR

'ATE/TIME:

2,4-Dinitrotoluene2,6-DinitrotolueneDietnylohthalate4-Chloroohenvl-phenvletnerFluorene4-Nitroaniline4, 6-Qinitro-2-Methy] phenolN-Ni t rosodi pheny 1 ami ne4-3 romoohenyl-phenyl etherHexachlorobenzenePentachlorophenolPhenanthreneAnthraceneDi-n-ButylphthalateFluoranthenePyreneButyl benzyl pnthal ateBenzol a JAnthracenebis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyl PhthalateBenzo(b)FluorantheneBenzo(k)FluorantheneBenzo(a)PyreneIndeno(l,2.3-cd)PyreneOibenzt a, n) AnthraceneBenzo(g,h,1) Perylene

Init6-/3

RF

. Ca-97%RSD

&$,3

. I

*

3"

Cont

RK

. Ca

%0

•

* 11

Cont

kh

. Ca

*D1

11

1

.1

*11

Cont

kh

. Ca

%D

.1

*

Cont

kH

. Ca

ID

-^*


* These flags should be applied to the analytes on the sample data sheets.

1/87

//f //ENVIRODYNEENGINEERS

June 25, 19871990-07351

Ms. Carol ShaefferSample Management Office300 North Lee Street, Suite 200Alexandria, Virginia 22314

Dear Ms. Shaeffer:

Enclosed are'the results of analysis of sixteen samples from Case 7351 forvolatiles, semivolatiles, and pesticides/PCB's performed under Contract68-01-7087. This report covers eight soil samples, EJ 125 through EJ 128and EL 256 through EL 259, received by Envirodyne on May 27, 1987, andeight soil samples, EL 260 through EL 267, received on June 4, 1987. Onematrix spike and matrix spike duplicate for low level is included withthese samples.

All samples were screened and extracted by the low level method for BNA'sand pesticides/PCB1s. One volatile sample, EL 267, was outside the lowlevel range in several compounds, so was analyzed by the medium level soilmethod. The limits of detection for the HSL's given on the data sheets formedium level VGA's in this package represent a dilution of 125 from the lowlevel method, because 0.04 grams of soil was purged as compared to thenormal 5 grams aliquot. A matrix spike and matrix spike duplicate were alsoprepared from sample EL 267 for volatile analysis.

If you have any questions about this report, please contact me.

Sincerely,

Margaret C. WinterProject Manager

MCW/sgcEnclosures

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY ^REGION V *X

^DATE ?-V-f 7 <&

SUBJECT: >P<ec./<3^^c. £e5ûAjSt? To CCS /=^/> ^/o^-^ -7^5-, ^0

X7 .. , . . — .. *X ~ « _FROM:

TO:

7 /s «ejec.7f-o ffcc^sc /r

2>/o

EPA FORM 132&4 (REV. 3-7C)

~

Caa« No.Low ——

Contract Laboratory HLOJWk)6 Contract No. Vft-CM-Medium

VOLATILE SEMI-VOLATILE

U.tflC•0.

Ui-uf l

i.i oi(tHtlif -04 •CNllNC-OI

111- (HI

• 14

nt-un II*- Mil lll'iltl lt*-llt|

• lltltfi**

4174

It, UMnq 113

EL2 (oU HL, (oM

It_S-X.

Hi 4,-? 33-

II SO 6(0yos -U 50 57•si 55-

Ubno 36,

102. 53lo I 94 53 q i

±* VALUES ARE OUTSIDE OF CONTRACT REQUIRED QC LIMITS

**AftulCnov LIMITS ONLY

VolstilesiSsml-Ptstlcidtl!

O out of kO outsids Of OC limit Ioutside of OC limitsoutildt of QC limit!

M- 4o

7/65

FORM II

Caaa He1 ow „

!•»•'(£•0.

fafc* IH- 1 *\l •*!e L- (*\A I

£t- at! MS£t, 31,1 <W>

,

* VALUES1 *ADVISOR1

Coffvnwi

. M'iSl r.

M«r1bvn I/

on tract Lat

r

inrAlnry fc rWUlRODWAJ^ ST <*nnlr»*l Mn L.X-OI-7f lX7

Ut-ltfl

I DOJl SI ft'ft

> ^'l

•*•lf*-IIU

iGftM>^^

Ml

I.I •>C«tO*0-

>mq^^5

• CHlfNt-lt

111- lift

k)fr

^

-

l-riwcMO*

AlAz^

^t—4^

.

•<*iu-un

A^fl^^ I

1xU

ARE OUTSIDE Of CONTRACT REQUIRED OC LIMITS Voliti

f LIMITS ONLY Sami~Ptstic

•^

CMI-VOLATlL

IK-llM

Affl-

.. /-,.^^

Iftll 0 . OUt «f , I 3-- |

X/nUHUat ^f $f |

IH.«t Mil Of J

Ill-itti

XJ/)^^

•^\S

'»N|HX

1 It- till

^''tJA11

\y /

-PCSTICtOC--

**

Y/

\^

outsidt of QC limit! 7/85outsidt Of QC limit!wtild* of QC limit!

.

FORM II

cL(

4-OIL _.VTL...

•M No, 13 .1 ———————— C

>w lovoL, ^ - *

FRACTION

VOASMO

SAMPLE NO.

B/NSMO

SAMPLE NO.

ACIDSMO

SAMPLE NO.

PESTSMO

SAMPLE NO.

COMPOUND

1.1-0ldtok>rtthtntTrichlorotlhcntChlorobtnitntTolutntBfnnnt1 ,2.4'Trichlorobtntin«Actn«phihtnt2.4 DiniiroiolutntPVrtntN Niiroiodl-n-Propvltmtnt1 ,4-DichlorobtniintPcnucMoro phtnolPhtnol2-CMorophtnol4-Chloro-3-MetHylphtnol4-NitrophtnollindintHtpuchlorAldrinOiiWrlnEndrin4.4'-DDT

SI ..."

rontraol

lotflum

CONC. SPIKEADDED lug/Kg}

toL /S

*tt\fTG

i r

i i/>^c>o

vl/(n.510Sla 3"

1

I

0$-

P^

1 1*0.

' '.....TH... SP. ...; U .1

ar ^K)V/ IR.OOV^^'

Ltvi 1

SAMPLERESULT

AAD

i

5

,

O

^ /

O

CONC.MS

SK5*/^. 55£. )-^•/.3SO. 5H5M650? Gl^ri^QHl O

1417^3^V^t>A<fa_An loCTTiOOc"^

ftMolOSoo

M(0I* (a

*^^-

3-OU/07<Zo

REC

PV1>P59?$*<?-5(j(o3-15*^loO404*f53(/ 16nUMTDloi

1 Cl"7<0GK«r

C F T ",O<

Contract No.

CONC.M5D

(/?._5S/.-556-. 59."5Si\^t*

•j,T)

f,q<jft>1i oRlVoOTl^/sSSVfiTtffLol 36bmtoi)1^-^60IUl'60

64W7SS

^09SMU•r\ aa

RECInff1/0>-*)7^?lw t

^1 «Q

U»Ov*xfl O

144

m*fc3-

V-irO (0

S31*1 o

130|^5f\5I*lU^K

RPD

/ 9/^f

JOlOo\IU1*3T3^10a*743*3S3T•'T

80*n

0, X•73*•XQ*

IV

or I»MIT«*RPD22242121212319473638274735SO3350503143384550

RtCOVCRY50.17262-13760-13359-13966-14238-10731-13728-8935-14241.12628-10417-109269025-10226-10311.11446.12735.13034.13231-13442-13923-134

'ASTERISKED VALUES ARE OUTSIDE oc LIMITS.RPD: vOAi_Q_om of

B/N — Q TT out ofACID—L. out ofPCCT ^* V* V * ^H.

Cofflflwrts; - _ou,

outiWt QC llmlitoutildt QC llmliioutiidt OC II ml 11oulild* OC llmlii

RECOVERY: VOAiJLôut of /° *B/N — Q_out ofACID -C_ outPEST _2Loul of J r;

outtW* OC limit*outiidt QC llmiiiounldt OC llmliioutiidt QC llmiti

FORM III7/85

JOI. JA1....C S CB.~ATL... S1...E l..'LK. CO RY

Contract No.

LOW LtVtl Uadlum L«««l

FRACTION

VOASMO

SAMPLE NO.

tLÛ"?

B/NSMO

SAMPLE NO.

JOA

ACIDSMO

SAMPLE NO.JO*

PESTSMO

SAMPLE NO.

•k>A

COMPOUND

1,1-OlcholortthfnfTrichlorofthtntOlorob«nifntTolutntBfnitnt1 ,2.4-TrichlorobentfntActniphthfne7,4 DinitroiolufntPvrtntN-Nitrowdl-n-PropyUmin*1 ,4-Oichlorobtntf mPcntichlorophtnolPhtnol2-ChloropHtnol4.Chloro-3-Mfihylphtnol4-NitrophtnolLindtniHtpttchlofAldnoOitkJrinEndrin4.4'-OOT /

CONC. SPIKEADDED fug/Kgl

C?^ foo

^

_,/

//

/

SAMPLERESULT

L>OfOD

aôWhut>

* •.

^S"

s

CONC.MS

4010M-tt^b

J5*- 30|l ^6bOTK>

_,s^

/

•

%REC

bt*ao1§i4â

>^X"

CONC.MSD

SlSlNMlpSOIP Odt>41^0umo

. ^"1^

%REC

5i**U~J^3lo IS

W 9

S

^

RPO

ri\0SC

~fr-

or i IMITS •RPO

7?242121212319473638274735503350SO31433845SO

RECOVERY50-17262-13760-13359-13966-142 ,38-10731-13728-8935-14241.12628-10417-109269025-10726-10311-11446-12735-13034.13231 13442-13973-134

ÂSTERISKED VALUES ARE OUTSIDE OC LIMITS.

RPO: VOAi—Q_out of 5 i• ' ; ; B/N«V ACIDlv PESTCofflflwntt!..

out of.out ofout of

outildt QC llmltioutildt OC llmtiioutiidt OC llmliiouiild« OC llmili

RECOVERY: VOAiJL-outofJO.;B/N ———— out of——.;ACID —— out of——.;PEST,__.out of __;

owtiMt OC llmltioutikta QC llmliiouttldt OC llmliioultldt OC llmlti

FORM IM7/85

SOIL MATRIX SPI. ,/MATRIX SPIKE DUPLICA._ RECOVERY•' 1 2 f t f

I ^S ^^ I J — b\ • J AXV 7 * —- ^ A ACat* No. _c=i-LL_________. Contractor g/iki/TQgy/rt;_____. Contract No.

low L«v*l. Medium

FRACTION

VOASMO

SAMPLE NO.

B/NSMO

SAMPLE NO.

ACIDSMO

SAMPLE NO.BL JO?

PESTSMO

SAMPLE NO.

COMPOUND

1,1-Oicnolorethene

TrichloroethcneChlorobenieneTolueneBcn*cn«1 ,2,4-Tr tchlorobenitneAcenaphihent2.4 Dmiiro toluenePyreneN-Nitrotodi-n-Propylamint1 ,4-0ichlorob*nftnePentachlorophtnolPhenol2-Chlorophtnol4.Chloro-3-Mfthvlph«nol4-NiirophtnolLindantHeptachlorAldrinDitldrinEndrin4.4'.DDT

CONC. SPIKEADDED lug/Kg)

too .OOOiI11

V^?/y).ADO

\o?/y)0j

V

.5000

N/

SAMPLERESULT

0

\ /o

*\<" I)/-

\ '

CONC.MS

tf£300//VOOO3 5. OO/J6»COO/01000t\./l\f\J \t/

*^ *^ *^^^Vl

Jtu*yÔLiX5fX>oj?/ 9^007*>L/(Y)O~^C'u' tJ

\fa7(tiJf.%%1

ut2 0

110 A/-><>/*

REC

/03/t^5/O?-^/i/i/ ^yjk5t i t yMl XJ/V 5fi «j*- / y\fr *% J^ Sf

Vs<2(AX-tlfap?J/-)f

^7S ^«

CONC.MSD

Sf/ yiOo}/<focc4*7popllfdob*?V7X?5?^j06/A/.VW)/QtloCQD^/XO^D7pfX>/3ir^£)< (p6O/ rH^n9>^3f?S& /i7a t't/y)

REC

q d/3d6;/ v -jfM/ttil-*?3OG'X/IrT

/0J

fys

JOOf55 ifyos/079i

RPD

ifLf

/O

t£^/>-30//)J l5/ I

t/f> y55 ^?V2>•5 L/

v^V

X v

I1U_ _0p MMITS*HPD

22242121212319473638274735503350503143384550

RECOVERY59-17202-13760-13359-139W-14238-10731-13728-8935-14241-12628-10417-10928-9025-10726-10311-11446-12735-13034.13231-13442.13923-134

*ASTCRISKEO VALUES ARE OUTSIDE OC LIMITS.

RPO; VOAi_——out ofa/N . 0— out ofArm 0 -... OfPEST -oi—. out of

outiidt OC Mmlliouitidt QC Ifmiisoutiide OC llmiiioutiidt OC llmlll

RECOVERY: ôut ofB/N J out ofAC 10. 7 out of/iL;PESTM_out of

outikH QC Mmltioutlkt* QC llmitioutiide QC llmitioutiide QC llmiti

FORM III7 /85

METHOD BLANK SUMMA,.f4

K> V > Con,,.,., Ng

0.1*

^s«n$ cr*l^v^-

£S3aS

£s*>qa--

.ViSST.(o-lUT?

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s&*„<£*

FORM IV 3-1 7/85

€•»• No. 1351 Cortrte,

OAK OfAMACTI4 MAtMW SBfe M»t.« COUrOUHB IH»l.,TlC OK UHMtKMNI CMC. UmTI cut*.

10

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Comment*:

JjQ»0 -7 ID mfi.,~0^

FORMtV Poj ^cr|3 7/C

$' W' SjvCase No. n»qinn ~5L Contraclor Contract No.,(f % "P '

to 04ICOT r li ACTION en COMPOUND (HSL.fIC ON UNKNOWN) CONC.

-JLUuÛmu^

1O063

BWA smo

5003"

QilC.

Comments:

FORM IV 7/85

Organics Analysii Data Shttt(Pig, i) :—————— ——— ————-———.

t Samplt Nnmbtr: EJ 123

Laboratory Namt: ENVIRODYNELab Samplt ID No: 17002399Samplt Matrti: SOILData Rtloait Aathoriitd By: .

!Cast No: }5QC Rtport No:Contract No: .Datt Samplt Rtctivtd:

Voli11 It Compoondf

Conctntrat ion: LOWDatt Eitracttd/Prtparad:Datt Analysed: (-3-17Cone/Oil Factor: 1Ptrctnt Moiitort (not dtcanttd): 11.24

CiS Nt: •Of CaS It: •1*1

74-17-174-IJ-fTs-ii-475-ll-JH-lf-2(7-44-173-13-173-35-473-14-3134-41-347-U-3117-14-17M3-371-33-4«-23-slll-IS-473-27-4

CklirtBttiaat 1IriBtBttkaatfiijl CkltridtCkltrittkaitHttkrltit Ckl t r idtieittitCarkai Dif iKidi i1,1-DlckUrtitkmI,l-Diekl*rittk»ttriM-l.Z-OUklttottatftiCkltrtftral.Z-Dltiltrtttkut2-litutul.M-TritklireitkiMCarkti Tttriekltrtltfiifl icitattIrtttdlekltrtittkait i

I 9: v2 02 VS*

VI1V0011

2 t11

12 f1 I

71-17-31II41-II-479-IM124-41-171-11-371-43-2lllil-IM111-73-173-J3-2141-11-1J91-7I-4117-11-479-34-Slll-ll-tlll-fl-7111-41-4111-42-3

1.2-DitkIiritritiattraaf-l,3-DickIititrtt»tTrleklirittkiBtBikmi£kltrnttk»t1,1,2-TriaitrtttkaBtItlltBI

cif-1.3-OUklirttrtt»*2-aitrtitkrlTiiflttktrIrmftn (4-RltkfI-2-IIBtlBtBt1-1*1 11 II*TttutklirtttkiBtI.l,2.2-TttraaitrtttkaBtTtlltBICkllttktBftltItkflktBIIBISljriBtTttal XrltBM

0V0VfVV

12 1V

22

0V

Data Ititttiaf Biallfitrf

YUUI:If tkt milt ii a raltt friattr tkti tr tfial tt tki dtttetitiliiit, rt|trt tkt tain.I:Itdieattt eti|tn< vai aialrstl fir kit att 4tttctt4. Itttrt tkt•iiim Itttetiti liiit ftr tkt tamflt vitk tkt 0 (tf.im kaitd•• itetfiarr ctietit.Uilitlti aetita. (Tkii is ait itetssarll|tkt iutrntat ftttttlti liiit.) Tit ftttattt fkttll rial: V-CtiftiU wi utl;n4 ftr kit itt dtttcttd. T*i inktr li tki•iii ••• attiliaklt Ottctlti I it it fir tki iuilt.J:Iiiicttii ai tftliati4 ft In Till fla| ft Hit titktr vkti»tfutli| a ciietatratiii ftr ttatattttlf idtitifitd etmptndfvktrt a 1:1 rtfltiiit Ii .ajfmt* tr «k» tki un ifietral 4ataii<ieatt< tkt trtstict if a cutm* tkat mti tkt UtitifUatUacriticla kit tkt ruilt It Itfi tkai tki iitcifitt Itttetiti liiitirtattr tk» itrt (if. HJ). If liiit if ditietiti it If t|I aid aetieiitratiti if 3 ifl ii ealetUttd, ttftrt « U.

C:Tkis fla| at|Iitf tt yMtieidt tarautin vktrt tkt idntif ie i -tfti mi etifirmtd ly Kin. Siiflt enptatit M>tUiri«iJ.ll•f/il U tkt (inl Mtcaet iktild kt cnfintd IT CC/HSI:Tkif Utf it utd via aaalfti U ttnt IB klaak ti mil •» alatfli. tt iBdieatti |tiilkli/frikiklt klaak ciituiaatiti udmm tki data Mir tt takt affrttriatt acttti.onn:Otktr flaft aad ftttBittt BIT ti rtfiirtd ti irtftilf itfintkt rtiiltf. If ntd, tktf Mil kt fillr 'tieriktd aid sickdifcriftiti attaektd ti tkt data fvaurr rittrt.

kit

Laboratory Na*e:Case No: 7351

ENVIRQDYNE Sample Number——————————————— -<&- —— i

Organics Analysis Data Sheet(Page 2)

Seaivolatile Compounds

Concent ra t ionDate E x t r a c t *Date Ana lyzedC o n e / O i l FactParctnt Hoist

CASNK

106-45-2Hl-44-495-57-6541-73-1106-46-7WWW95-50-195-W-739638-32-9106-44-5621-64-747-72-19B-95-37WH6B-75-5105-67-965-85-0111-91-112W3-2120-BM91-20-3106-47-887-66-3W-56-791-57-677-47-486-06-295-95-491-5B-7BB-74-4131-11-3•*M «J *OJO TOTJ

9W9-2

: LOWd /P repa red : 6-1-87: -6 ID 0? <o-l3-*"Tor: 1ure (decan ted ) : 18

Phenolbii-(2-aiiraethyl)vthcr2-ttlcrcphenoll,3-Dichl(ratMZB»l,4HhchlerabeizeneBenzyl Alatel1,2-OichlDrabenzent2-ftethylphenalbis-(2-Oilcroi«iprofiyl)ethcr4-fethylptaalH-nitrou-Oi-a^ropylatiMHecachliraethmKtntaamIsgpharm2-ttitrophBwl2,4-toMthylphBBlBsnzoic Acidbis- (Dilaraethay) Nethane2,4-Didilirophenol1 ,2, 4-Trichlarofa«i2B»Niphtlulew4-QilaroaniUnaHn art Icr abut jdieot4-Oil(ro-3-«thylphmol2-HKhylMphthilewHeiachlonrycl opmtadim2^4,fr-TndiIarc?h8nal2,4,5-Trichlonphml2-Chlaronaphtlulnt2-NitroaniliniDiiethyl pbthalatiAcviapthylm3-ttitrMnilini

.2

uokg

810 U810 U810 UB10UBtOUB10U810 U810 U810 U810 U810 U810 U810 U810 U610 U810 U3900 U810 U810 U810 U810 U810 U810 U610 U810 U810 U610 U3900 U810 U39000810 U810 U3900 U

GPC C leanup i YESSep. Funne l E x t r a c t i o n : YES 'Cont in . Liq.-Liq. Ext. : YES (

CASNo:

8>32-951-2H10H2-7132-64-9121-14-2406-20-284-66-27005-72-386-73-7100-OW534-5M86-30-6101-55-3118-74-187-96-5B5-OH120-12-764-74-2206-44-0129-00-085-68-791-94-156-B-3117-B1-7216-01-9117-64-0205-99-2207-OS-930-32-6193-39-553-70-3191-24-2

Acnapfathene2,4-Oiratn9tmi4-*trop6molDitazohran2,4HKiutrotDluB»2,6HhnitnitQliM>Ktthyl phttulitf4-QUtnphtnyl-phBtvl etherFllKTCOlA-fctnaraline4,4-frioitro-HrthYtphmolM-ui U lauUphenylaiim (1)4-flronptanyl-flb0yl etherItaachlarobenzeMrntadtloraptmlf^m 11I imnmnlt mmARthracneDi-fi-butyl phthalatfFluor «tbe»ryrewButyl-tauyl-pMItilatt3f 3' -Dichlontezidin*BBuo(a)aathraawbis-(2-Ethylhsiyl)phthaliteQryseneDi-irxtyl phthiltttBnzo(b)fluara0thmBnotUflunnthntBmodJpyrenfIndenot 1 , 2,3-cd)pyreneKbetnoii,h)aBtlracw»Bvuolûlperylm

j^*\GLQ) ( c i r c l e one)ô) ( c i r c l e one)

<**

610 U3900 U3900 U810 U810 U810 U810 U610 U810 U3900 U3900 U810 U810 U610 U3900 U610 U810 U610 U810 U810 U610 U1600 U610 U

fy*610 U810 U810 U810 U810 U610 U810 U610 U

(D-Cannot be separated froa diphenylaaine

FORM 1

Laboratory

NoSample Number

Concentration

Organics Analysis Data Sh*«t(Page 3)

Pesticide/PC Bs

Medium (Circle One) GPC Cleanup^Tes DNo

75

Date Extracted'Prepaced _____Q

Date Analyzed: _____6~tt>'l~l

Cone/Od Factor:

Percent Moisture (decanted)

CASNumber

Separatory Funnel Extraction QYes

Continuous Liquid * Liquid Extraction OYes

ugv*Cg^(Circle OneT

319-84-6319-85-7319-86.858-89-976-44-8309-00-21024-57.3959-99-960-57-172-55-972-20-833213-65-972-S4-81031-07-850-29-372-43-553494-70-557-74-98001*35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha -BHCBeta-BHCDelta -BHCGam ma -BHC (LmdanelHepiacftlorAldrmHeptacWor £poxid«Endosutfan 1DfeWrin4. 4--DOEEndrmEndosutfan II4. 4--DODEMosutfan SuHate4. 4--OOTMetttoxychlofEndrin KcioneChlordancToxaphcntAroclor-1016AfocIor-1221Aroclot-1232Aroclor-1242Atocl<X-1248Aroclof-1254

Aroclor-1260

/6U|t> UIk U.)b aIt uit «_ft [4U U32-W-32. (L72. (A?ZLt?ZU_52 UZl W.(do U31 U.Ifeo U52<?16Ifeo 1^li U,)b9 U

Ifrff U.1t«7 U

32J> W.5Z.n u.

V- * Volume oC extract injected (u(|

V ' Volume of water extracted (ml)

W£ * Weight of sample extracted (g|

V * Volume of total extract (ul)

orW. 3o . 600

Form 1 7/85

•oratory Name , _£-Ml) \\L

• No _____

GASNumber

Organics Analyses Data Sheet(Page 4)

Tanlativftly Identified Compounds

'-.

3..

0-.

Compound

- Pucanong A', KHd rD

i

cm

TUiJi/xa^f

Fraction

"7'ftrL_L

10.(I. 1

IS- 5IS . 1

IV S. I

3-l-U. -7

3-S.-I

(ug/f

i10-0 S

morn

For<m 1. Pan B ? es

O r g a n i c * A n a l y s i s D a t a Shut( P a g i 1) !--

5a*pl« Namber: EJ

Laboratory Nami: ENVIHODYNELib SaapU ID No: 87002400SiapU M i t r i i : SOILData Rilttsa Anthociitd 87: .

Caff NoQC Rtport No:Contract Mo: (fQ-6l-Dttt Savpli Rictiftd

V o l a t i I t Compound!

C o n c t n t r a t i o n : LOWD a t a E i t r a c t i d / P r t p a r t d :D a t t A n a l y n d : 4-3-17C o n c / D i l F a c t o r : 1Ptrcint M o i f t o r t (not d t can tad ) 15.43

CIS Ki: CU *•:

74-17-174-ll-f7S-I1-475-11-1TS-lf-247-44-171-tS-l75-15-475-14-1154-41-347-44-3117-14-1M-fl-171-55-434-11-3in-15-475-27-4

Cklirmtkail 1

IriatattkABi 1Tiiyl CklltKi tCklirittkait IRitkrlui CklirUticttiitCirfcti Oii i t lUi1.1-DUkHrtltktil

1,1-DiekIiriitkanttaaf*l,2-DiekI»iutkiitCkliriftra1,2-Bleklirtitkuil-iitu»tl.l.l-TriefclirittkaiiCarbia Titfuhltfiitf l iyt leitatiIrnitflcklicnitkui

2 B2 D2 02 B121110B011

2 V11

12 11 I

11

7I-I7-S11141-12-47»-ll-4124-41-171-11-5Jl-41-211141-11-5111-75-175-2S-2lll-ll-lSH-71-4127-11-479-14-5lll-ll-llll-fl-71IM1-41II-42-S

1,1-OiekUripnpiii 4tiaas-l,l-Ditklit«praptM 4Ttlckltmtktu 4lilriaieklittaitkaii i1.1.2-TriekIiriitkaai 4Bill IB! tclf-l,l-DiekIiripriiiii i2-UIiriitkyltiBylitkir 1Briaifm 44-HitkyI-2-tHtaam2-ItiaataiTitraeklitittkiii1.1,2.2-TitraekliriitkaBiTiliiitQlitiktastiiItkylktiiittItfttaiTital Zyliais

BVBBBBB

2B

22

Data lt|«itlif Qialif i ttf

C:TUDE:If Ui iftilt if a vain frutir tkii »r tiiil t« tkt <*t*eti»liait. iipfrt tk* riln8:

ctBftntf vas aialyii< ftr kit ait Jttiettc'. lipitt tkiJi tKtif i l imit (tr tki umpti vitk tki B (if, 110) laittf

» uctfiarr ctictat. / l i l i t it i actin. (Tiis it Ml i iciff iri lytkt luttntat Ittietlta I l t i t . ) Til (ittuti iioU ctal: V-C»B|i»< wi ualyit4 ftt kit itt 4tt*ct«4. Tki infeir it tkiBitira attt i iafclt littetiii lUlt dr tki tuilt.J:talieatti u tftiutt< Tain. Tkii (Uf li aft< titkir «fc»tftliatiii a ciitaitratiii Ur ttitttirtly ia»t i f i i< CHf»*dtvkiti a 1:1 nittisi li atsntl 11 «k» tkt un f^tctral litaii4ieatatf tki iriiiiet •( a CMtintf tkit uitf tkt UtitUttatltier i t i r ia kit tki milt It Itfi tkai tki iMCifiit Itttetin liait litfriatir tkai itri ( i f , 1IJ). If Halt »f tfitietiia It II t|I u< ituciittatiii if 1 i|I it etleiUtU, rtpirt at JJ.

nil f laf atf l f i f ti f i f t i e i t t Miuittrt vkni tki i l t a t i f i e i -titi nt c»flrai4 ky K/Itt. Siiili e»i*mt itsticUis)*!!ai/il ii tkt fiaal tittaet ikiiU ki eufirai* ky CC/K5I:Hit fla| it till vku tiaiyti ti fml la klaik at nil ai alaafli. It lafieatts |iiiiklt/trikakli klaik ctitiiiiitiii ai<vtrn tki <ata ttir ti Ukt aiyriyriati ictin.OTtU:Otktt (Uff aa4 (tttaitit aiy ki riiiirid ti rr*M^T <*<>•*tkt rti i l tt . If ui4. tkty ant ki f i l l y 4iierikitf aid lickfistriitin atUcki4 ti tki lata tnaary

Laboratory Na>e:Case No: 7351

E N V I R O D Y N E Saaple Nuaber: EJ 12a

Organic* A n a l y s i s Data Sheet(Page 2)

5e*ivolat i le Compounds

Concentrat ion: LOWDateDateC o n c / D i lPercent

xtr ac ted /Prepared: 6-1-87nalyzed: 6-13-87il Factor: 1t Moisture (decanted) : 15.4

CASta

108-95-2 Ptwnol111-44-4 bii-{2-QU<TQBtbyl)ether95-57-fi 2-Ol(rophBiQl541-73-1 l,3-QichlcniwuB)i106-46-7 J,44icfal(rQbnzB*100-51-6 Bmzyl Uotel95-50-1 l,2-Didilx(taizB«95-46-7 2-*thylphral39638-32-9 bii-(2-Q>l(roisopropyl)ether106-44-5 4êthylphnol621-64-7 H-aitrnHh-ft-propylakne67-72-1 taadtlorathn98^5-3 tttnteum78-59-1 IfflphtrmBB-75-5 2-Nitropnnol105-67-9 2,4-fce*hylphe»l45-65-0 Bwuoietad111-91-1 bii-(Chlxaethmy)nvtham120-0-2 2,4-ttchlxcplwnoli2Hfc™i li2i4~Triciu7D8CW91-20-3 taptithalm106-47-6 4-Qax«niUneB7-6B-3 IfaactilorofefUdiBw59-50-7 4K3u(TQ-3-erthylpnflttl91-57-6 2-fMhyln^hthalew77-47-4 faachla-KyclcvBitadiBitao~vo~2 244)6-Tnoil(n ilMDl95-95-4 2t4,5-Trichlxq)nwol91-58-7 2-OavcnaphtlultneBB-74-4 2-ttitnaniUnB131-11-3 KeKhyl phthalite208-96-€ Aonapthylm99-09-2 3-tfitroanilitt

Sep. Funnel Extract ion : YESQ.

*M

780 U780 U780 U780 U780 U780 U780 U78011780 U780 It790 U780 U780 U780 U780 U780 U3800 U780 U780 U780 U780 U780 U780 U780U780 U790 U780 It3800 U780 U3800 U780 U780 U3900 U

Contin.

Gttfe

B3-32-951-28-5100-02-7132-64-912M4-2606-20-28H6-2

Liq.-Liq. Ext. : YES(

AuMpbtbm2,4-Dira tn hnl4-ttitropb«)lDibenzoftran2,*-tKiitn)tolutt»2,6-DinitratolumDifthyl phtlulitt

7005-72-3 4*{hlaraphe<iyl' )tienyl etherB6-73-7100-01-6534-52-116-30-6Wl-55-3tffl-74-1C-Kr5e-oi-e120-12-781-74-2206-44-0129-00-0B-tt-791-94-156-55-3117-81-7218-01-9117-84-4205-99-22D7-OB-95D-32-8193-39-5SHO-3191-24-2

fluarnt4-fctnurahne416-Oiutro-2-fHhrlphtnolM-nitnaiiiphmylanne (1)4-firoK9tarl-pb«rl etheritaadu nrobenznrBudil oropnBuPtienaitthreniiRttracneDi-n-fautyl phthalateFlurmtliatryrtmBtttyl-bwiyi-pfctJuliti3f3 ' -Dichlmbcaidi neBeno(a)anthracmbis-(2-EthylhByl )phthal«tiQTYIMDi-n-octyl phthalateBeno(h)fliaravtiteMBn»(kmurvth«8mDi4}pyrneInd«i(l,2,3-aI)EnTw»DibeBO U,h) arthr acevBenzo( u)pryle«

i_Nm^ ( c i r c l e one)NQy ci rcl e one)

»- — s

upkg

780 U3800 U3800 U780 U780 U790 U780 U780 U780 U3800 U3800 U780 U780 U780 U3900 U780 U780 U11007VU790 U790 U1600 U780 UWi Sf US -tFTV ^* *^ C^Trf

780 U790 U790 U790 U780 U780 U780 U780 U

(1 ) -Canno t be separated f ro* d i p h e n y l a e , i n e

FORM 1

Laboratory Name

case NO _':._Sample Number

Concentration f°™J Medium\^^-Date Extracted 'Prepared ____b_:

Date Analyzed ______o "" fo"~

Cone/Oil Factor: ___________L_

Organlcs Analysis Data Sheet(Page 3) t

Pesticide/PC Bs

(Circle One) GPC Cleanup^Yes DNo

_____ Separatorv Funnel Extraction DYes

————— Continuous Liquid - Liquid Extraction DYes

of\


CAS ug/lorug^KgNumber (CircU Onet319-84-6319 85-7319-86-858-89-976-44-8309-00-21024-57-3959-96-860-57-172-55-972-20-833213-65-972-54-81031-O7-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha -BHCBeia-BHCOelli-BHCGammj-BHC (Undane)HeptachlorAldrm

HeotacMor EpoxideEndosutfan 1Oieldnn4. 4--OOEEndrinEndosuKan U4. 4--OOOEndosutfan Sutfate4. 4--ODTMettwxvchlorEndrin KetoneChkxdaneToxapneneAroclor-1016AfockK-1221Arocloi-1232Aroc lor- 1242Aiocior-1248Aroclor-1254Aroclor-1260

/ f cUIt U;t \JLIfo i.L\'0 LiIt «Ifc UIt U32- U.3itLTi (A7iU.7zcc52 U-31 1(_Ifco U7^ U.tfe» U52? U.

»f?9 f.d

Uj U')b? iXitr ix\k& U

3^ tc52.1 fx

V- » Volume of extract injected |u()

Vs * Volume of water extracted (ml)

Ws * Wetght of sample extracted (g)

Vt « Volume of tola! extract (uO

orW. 30* lo, ooo

Form 1 7/85

Organic* Analysis Data Sheet(Page 4)

Tentatively Identified Compounds

CAS

(««g/t D

n-o

ift.lU-2,

m CjOu f

IS.i 5563

. 6 5^03

4-1.

3*65tJiikftI I . -_ !„ .

*JL* -

? 85

Otginici Xnilytis Dttt Shift(Pigt 1)

1 Simpl t Nambt r tJ 127I——— ——— _- —— —— „ —— _.

L i b o t t t o r y Nimt: ENVIRODYNELib Staplt ID No: 87002401SimpU M i t t i i : SOILD4t» Rilttit A o t h o r i n d By:

C4.. No: ^QC Rtport No: /.1 UContrtct NoD i t t S*mplt R t c t i t t d :

VoUt i l* Compoandf

Conctntrttion: LOWD4t* EitrtcttdfPrtptrid:D4tt Anilytid: 4-3-87Cont/DiI Fictor : 3Ptrcint Koiiturt (not dtctnttd) 15.98

om

OC/5

-O

CO.

CIS Hi: CU Mr

74-17-174-13-175-11-473-11-175-11-147-44-175-15-173-13-473-14-3134-41-347-44-3117-14-1tl-H-l71-53-*54-11-31H-IS-473-17-4

ChlttimtthiitIttmtmttkmTiiyl Ckltti4tUlitittktatE« tljl.it Chltrilt•Cttlll

Cuioi Di i i lUftl . l-DUhlittithtii1,1-Ditkllt i itkutti 4M-1, l-DiekltrtttktitCklittfinI.l-Dithlmtti4*t1-titutiti.l.MilemUitftlmutCttbti Tttutkltti4tTiiyl IttUUItf»t4ltkliinttkiii

41 D41 I41 8il 1fr*l

11 131 131 IIIII11ilII3141II

1) 1

71-17-3llltl-ll-4

71-43*1llltl-ll-3UI-75-173-X3-:lll-ll'l

U7-1I-47t-»-5lll-ll-llll-fl-7111-41-4

TrickltrtttktiiBibimeklttiMtktitI,l,l-Tttek[itittk4iiItutu

Itntdr*

Tili4tklir»»tkntl,l,l.l-Ttti4ckUttitkiitttlitfti

ItkflbtmiimiityituTtt4i tyltiii

31 131 Q31 V3i aII III U31ilII414131II31IIIIIIII

B«U lifirtiif (hil if itn

4itieU»iHUT:U tkt milt ii t vtlit fiittti tkit ti t*nl ttlimit, ttfirt tkt »»ln1

ctmfttmd «•• 4m4lyn4 (tt bit mtt 4ittcti4. li»trt tki4itieti» limit (n tht iimfli with tki 0 drllQ) bi*i4

tm itcifitty et iet i t .Miltt i tm ttliti. (Tk.ii ii tit mtcni4tllytkt iuttatit 4tticti» l i m i t . ) TV« (ttttitt ikt«I4 tti4: B-Cimf«n< vu U4lyit4 (it kit tit ittttt«4. Tki inkit it thtmikima ittunHt 4it»ctl» l imit (it tki iim»ltJ:Imiie4tti 4m tttimati4 ttlit Thli (Uf ii tft4 titbit wbiitittAititf 4 t»etiti4titi tti ttmtittfily 14iiti(it4 ctmyindi•ktti 4 1:1 tt*M"i ii timtl tt wktt tkt min iitetnl i*Uitiitttti tkt itiittci il t cimttnl tk»t a»ti tki Uittidcitltieritiru kit tht ttult ti lilt th4m tht i|ict(lt4 4tttctiim limitlittttr th4t itit (t|, 1IJ). II limit tf 4tttctin ii II <l' *>d itvictitrititi •( 1 ill li c4lc«Utt4, tttttt 4« 3J.

fU| iMliii ti |itticl4i îiuitin vktti tkttit* HI etitlrmi* by CCfHS Siiili eii»omt ri«tlei4t<)«ilM'li t« tki (iul ntnet ikitU bt etifirmtl by CCfKSI:Tkii (U| i> "*4 •••» ttiiyti it (ti«4 i» bluk u vtil n 4IU|U. It ii4iutti |tiiibli/|tibiblt bluk e««tuii4tin 4m4«4tu tki 44ti tut ti ttki i f l t tff l ttt t fc t i i t .OTHH:otkti (U|i u< (iitntM MT i« mi'ti* tt in^ t r iT ttiiittki tnilti. II tit4, thif milt bi ( i l ly 4ucitbt4 it4 tick4tictifti«i 4tt4ckt4 ti tht 4tti tomuif t t f i i t .

bit

Laoaratory Naae:Case No: 7351

ENVIRODYNE Sa*ple Nuntier: EJ 12//

Organic* Analysis Data SheetiPage 2)

Setivolatile Conpounas

Concentration: LOWDateDateConc/Di1Percent

x t rac tenalyzef l

a /P repa red : 6-1-87: 6-13-87

Sep. Funnel E x t r a c t i o n : YES \Contin. Liq.-Liq. Ex t . : YES (

J^y ( c i r c le o n e )NQJ ic i rc le one*

il Factor: 1 ^-^t Moisture ( d e c a n t e d ) i 16

CAStta:

108-45-2111-44-495-57-8541-73-1106-46-7100-51*695-50-195-46-73%3fr-S2-9106-44-5621-64-747-72-198-95-378-59-1BB-75-5105-67-965-65-0111-91-1120-63-2120-82-191-20-3106-47-8B7-6B-359-50-791-57-677-47-4BB-06-295-95-491-5B-788-74-4131-11-3208-46-899-09-2

Phenoltu G - (2-QU orathy 1 ) rtrv2-Oilcrop6«ol1,3-Oichlcnteirent1,4-ftchlrobenzentBvayl Alotall,2HhctilcrobmzBW2-HKhylpteulbii-(2-Chloroiscpropyl)ether4-*thylfr*iolIrHl bTOCQ*vl " t~OrQOVl 4B W

F^Bt dOU VQ^CThdftt

tttrcboiatInnhcrtn2-tttnyheiol2,4-OiMthylphmoltaucric Acidbis-IIM£nKthaiy)nBth«2,4-ttdilQrophenol1 ,2, 4-TrichlxobeJueneMjhthilmt4-Qil crovuliniHBadilorobutadicne4-Oiltro-3-wthylphmol2-VthyluphthalencHexachl crocyd cventadi en*2,4,6-ThcfalDrQphcnol2,4,5-Trichlcnptanol2-ChlGrDMphtfealerw2-MitroanilintKvthyl ptithalattAorupthyleit3-tbtnunilint

^

790U790 U7%U790U790U790 U790 U790U790U790U790 U790U790 U7WU790U790 U3BOOU790 U7901179011790 U790U790 U790U790 U7%U790U3800 U790 U3800U790U790U3BOOU

CKfe:

83-32-951-28-5100-$2-7132-M-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-9120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-91-721MI-9117-64-0205-99-2207-06-450-32-8193-39-553-70-3191-24-2

tanaphth«2,Hhnitntfwral4-tttrcpbnolDibvzotirn2,4-Dinitrotolum2tHKnitrotalmDirthyl phtbalatc4-Oilanvteiyl-phenyl ethrFluorne4-tttnunihne4,6-Oi ni tro-2-Hetfayt ptwwlIHutnBotiiphenylMitt (1)4~firoiDpoBiyl' nBtyl etfavta«±Icnt«uwtatadiloroptwnolPtwunthmAntlrKnrOi-n-fautyl phthalati \FliarMtbBWPyrweButyl-totzYl-pbth&lite3,3 ' -OieW crrteu idiwBeuDialanthracBttbi f - 12-Ethyl tey 1 i phthal auQrrsemDi-rrxtyl phthalatiBmiDtblflixrxthinfBmzoOclfluranUcniBBUotal rm!ndena(l,2,3-ol)pyrmDilwizo (*, hi nttar acswBmzofgtulperylm

*,*>7901)38001)3800 U790U790U7?OU790U790U790U3800 U3800 U79011790U790U3BOOU790U

_790U ._ _ _ ^ J \

79o u79411790U1WO U7VOU510 *T VJ'f.Tt790U790U790U790U7WU790U790U790U

(l)-Cannot be separated irom diphenylaaine

FORM 1

Laboratory Name gto \Mft-OPH >^C


Tentatively Idontifiod Compounds

Smm&le Number

E3- 1-3-"?

CASCompound NMTM Conc«n(r>t*on

(ug/1

) V ' ™ 1 JLfi.Amir*

ID. 110 ^

13.

14.

15.

16.

17.

IB.

19-

20._

21..

22. _

24..

25..26..27..28..

29..30..

luÂr-iv a.rbgv^

VOX)

form 1. P»*1 8 7 85

Organic! Ana Iyiis Data Sheet(Paga 1) I--

Laboratory Name: ENVIHODYNELab Sample ID No: 17002402Sample Hat rii: SOILData Ralaaia Authorised By: .

Ca.. Ho:QC R t p o r t No:C o n t r a c t N o :Data Sample Received

Velat ila Compound!

Concentration: LOWData Citracttd/Piaptrid:D a t a A n a l y s t d : 4-3-17Cenc/Dil factor: 5Parcant Moiitan (not decanted); 14.74

CIS Ma: CIS Ka: aarg

74-17-374-II-f7S-H-475-11-1TS-lf-I47-44-175-15-173-15-475-H-JISt-il-S47-44-1117-li-l71-fl-l71-55-4S4-2I-Illl-IS-475-17-4

Cklarnatkaae 12 9IretaMtkaae It Vfiiyl Ci lar i4a 12 1Cklinataua tl 1Hatkj laaa Ckliti l i 54 1Icataaa &J 1Cirkaa Dtn l f i i tt , l-Dlekltrattkiia1,1-OttkIatMlkaait r>ai- l ,2-DieklateatkaaaUlarafara1,2-Dicklaraatkaaat-htaiau1,1,1-TrieklinathaaaCarlaa Tattiaiarllaftijl leatati 1Z 1lr«aa'taiarnatk«aa * >

71-17-5 l ,:-OickUttBMBaaa 4 U11141-12-4 ttm-l.l-DiekUtiaiatiaa 4 V7f-IU4 Tricalamtktai 4 V124-41-1 liiiiuekUiaMtkaii 4 ffn-lf-S l. l .I-Trieklariatkiaa 4 V71-41-2 laaiata 4 0lllil-ll-S e i i - l , l -Diekl«t«acaftaa 4 9tll-75-l 1-aiartatkTl'iarlitkar 12 I73-25-2 Iraudra 4 0111-11- 4-HatkTl-2-itiUaaaa 12 V3H-7I- 2-liiaam 12 I127-11- TatricklaraatkataT1-J4-S |.l.2.2-Tatnaiaraatka»111-11- Talaaialll-tl- QIar*k»iaia111-41- Elkfliaaiaia1M-42-5 Stfraia

TaUI IT I tin

Data liatrtiaf Qaalidan

III til:If tka raailt if a ralta a,ieater tkaa ar taail ta tka e'etattiealint, raaart tka talae.I:Ia4ieate« eeiaewad MI aulyiaf far kat aat 4atacle4. leant tka•iaiia* aatacttai Iliit (ar tka laaala vitk tka V (af.HQ) iifat*ta aaeasiary caicaat . /J l lat i i i tctiaa. (Tkli (a iat tacanarilytka iaitrtmaat itttctiti H a l t . ) Tka faataati ikaaU raa4: V-Camaaaatf vai aulfta4 (ar kat aat 4it«etia. Tka tamkar !• tka•iaira attaiaakla atttetiti ttiit (ar tka iam|Ia.J:Ii4icita« aa aft imata4 talaa. Tlii (Ia| ii an I" aitier "»*atittutlif a ctteaatrattai (ar ttitatltalf 14aati(ia4 caiaendflvfcara a 1:1 ra«aaaia ti aima4 ar vkaa tka un iitctnl 4ataIi41uta4 tka arenaee at a cnptn< tkat atiti tka t4t i t i f icat ie icriteria kit tka Taialt it laaa tkaa tka faec i f ia4 lataetlaa Itiitl iaatar tkai lara ( i f , 1 IJ ) . If Halt if it tic tin ii II ifl aa4 acaiceatratiai t( I aal ii c«lcitata4, rtptrt " *J

C:fU| aaBliaa ta ya f t i c i l i Baruntiri vkaia tka i t f aa t i t i e i -

tita via caafinaa' if CC/IB. S ia f l a caiaaaaat i * i t i e i l * i ) « l laf/tl ii tka fi ial aitiut <kaal i ba cnlirati IT CC/RSI:Tkii f lat ii "<< vk" aitlfta ti fatal la kliar ai wal l ti ai up It It iilieitti aaf i ikla/ iraaakla blaak eaatuiaitl ia ia4Mru tka iata aiar ta Ula affrafrlata aet iaa .OTUI:Otkar f laft aia* faataatai iaf »a raâirai ta i t»Mt'T 'afliatka rtniti K ntl, tkaf Hit ka ( a l l y <aicriba4 aatf tack4aicriatiaa itUtkt* ta tka data IOMI; r iaert .

kat

Laboritory Na«e:Case No; 7351 ENVIRODYNE

Samp le Nugfaer j EJ

Organic! Analysi, Data Sheet2)

128

Concentration: LOWDate Extracted/Prepared: 6-1-87Date Analyzed: 6-13-87Conc/Dil Factor: 1Percent Moisture (decanted)

Se«ivolati1e Compounds

14.6

CASttx

111-44-495-57-fl541-73-1106-46-7100-51-695-50-195H8-739638-32-9106-44-5621-64-767-72-198-95-378-5H»-75-5105-67-965-B5-0111-91-1120-63-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-788-74-4131-11-3

Bvevl Alcohol1,2-OidilarobauiMZ thylphml61 s- (2-flil croi sopf opyl ) rthr

*hii troso-ft -fr-pr opyl an MHBachliroeUuni

Inphonn

tosoicbii-<QUatcthuy)fethm

1 ,2, 4-TrichlorcteaentIbphthalm4-Chl<nianilin*teacblorriutadim*

2- thylnaphthalent

2,4,6-Trichlcroptewl2,4,5-Trichl(raphBwI2-Chl(rmapt)thalcM

fcmapthylnW-W-2 Wtromliot

770 U770U7TOU770 U770 U770U770 U770 U770 U770 U770 U770U770 U770U770 U770 U3BOOU770U770U770U770 U770U770U770 U770 U770U770U3BOOU770 U3800 U770 U770U3900 U

6PC Cleanup : yesSep. Funnel ExtractionContin. Liq.-Liq. Ext.

83-32-951-2M100-02-7132-64-912-14-2606-20-284-66-27005-72-386-7^7

534-52-1B6-3N101-55-3118-74-187-86-5B5-01-8120-12-784-74-2206-44-0129-00-085-69-791-W-l56-55-3117-B1-7

117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2

2,4-Ouutr^hmol

2,4-ffiritrotoliant

Fluornt

4,6-«Bitro-2-(W)ylphwol(1)

ette-

W-tHxrtyl phthalat*

( c i r c l e0~)<c i rcU

one ône)

K-n-octyl phtiulati

770 U3800 (J3BOOU770 U770U770U770U770U770 U3800 U3800 U770U770U770U3BOOU770U

770 U770U77001500 U770U560 »770 U770 U770U770U770 U770 U770 U770 U

We.

___ —— _--i» = = as»*»»M*«««*z = «»»»«»**»»«s:ss*»»a

(U-Cannot be lepabated fro* diphenylaaine

.. - _r-- . FORH 1

Laboratory Name

Case No

Organics Analysts Data Sheet(Page 3)

S«mpt« Numb«r

-nz-.

Concentration

Date Extracted'Prepared

Date Analyzed ______

Medium

-1-17

Pesticide/PC Bs '

(Circle One] GPC Oeanup^Yes ONo

___ Separator^ Funnel Extraction QYes

——— Continuous Liquid - Liquid Extraction DYes

Cone/Oil Factor


CAS ug/loruguKgNumber (Circto One)

319-84-6319 85-7319-86-858-89-976-44-83O9-00-21024-57-3959-98-860-57-172-55-972-20-633213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha-BHCSeta-BHCDefta-BHCGamma-BHC (UndanelMeptachlorAldnnHepiacnior CpoxideEndosuKan 1Dietdnn4. 4--OOEEndrinEndosutfan U4. 4--000Endosutfan Surfate4. 4--DDTMetnoxychkxEndrin KttoneChlordancToxaphen«Aroclor-1016Ar odor-1221Aroctor-1232Aroclor-1242

Arockx-1248Aroclof-1254Aroclor-1260

/6UIf U

/fc U.it au u.Ib KIt UIb U32- U-31 \L7i (AJ2-U.72. LC3l U3i U.Ibo U3i u.Ifco U32916

tfco (XUa UJt5 U

l&(? U-»fe? U310 K.

5Z.o fX.

Vj * Volume of extract infected (ul)

V » Vofume of water extracted (ml)

Wt * Weight of sample extracted (g)

V( * Volume of total extract (ul)

3o<\ _ v IO.AOO

7/85

No

Organic^ Analysis Data Sheet(Page 4)


CASCompound N

(ug/l

10..11..

13..

17..

18..

21.

22.

24

26..27..

29..

30..

V » / n V

M\JULA (d roGCLr be n

bo n

- 1

10.uu13

ISM

35.

3 6 - 1

l lGTJÂ

Ifc-oo 3

5503

60 3

-o

Form 7 65

Organics Analysis Data Shut(Pigi 1)

5a»plt Nomb«r: El

,-v

"£&Laboratory N*«i: ENVIROOYNELab 3a»pJi ID No: 17002*03Simpli Hatrii: SOILData Rtlcaic Anthoriitd By:

C... N,: ' } TJ6>QC R*port No:Contract No: _Dati Sampli Rtctitod

V o l a t i l t Coaponndt

Conctntrat ion: LOWDatt Eitracttd/Prtpartd:Datt Analyttd: 4-3-87Conc/Dil Factor: 1Ptrctnt Moiftort (not dicantid): 14.74

CIS Nt: •1*1 CIS Rt: 1919

74-17-174-13-t73-11-473-H-I73-l»-l47-44-173-13-173-13-475-14-1134-41-3(7-44-1117-14-171-fl-l71-33-434-11-3111-13-473-17-4

CkliiiMtkat* 1]IrUHltktll 1f i ty l Ckl i r td i 1Cklenitkati 1RitkylHi Cil i r idiIcitii* ^Carkit D i n l f i d tl.l-Blckliriitkiti1,1-Diaiiriitkatitraii-l.l-DickliriitkitiCklirifinI.l-Dickliriitkati1-lltUltl1,1,1-TrickIirntkuiCarkit TitraekliridtTiifl Icitati 1Imidiekliriutkiti 4

9t 91

( 917#>

t >I1

1 11

7I-I7-J1M41-I1-47M1-4H4-4I-17MI-J71-O-111141-11-31II-7J-I75-15-1lll-ll-l3fl-7l-4117.11-4Tf-14-3lll-ll-lIII-fl-7111-41-41II-4M

1,1-DichUrttretiittrati-t,l"0ickIir«pr»M"TricklirntkitiBikrmcklir nit k*uI.I.S-TiieklirttUmlimiteii-1.3-DiekliriiriM | f

l-CkUriitkfltii?Iitk«rIrmfirm4-Kitkfi-i-Mttiioti1 -IliumTitrickliriitkni1.1,1,1-TitraUUnitkatiTiliitiCklinkitiiiiitkfikiiiiiiStymiTital If 1 iiti

0UVI00V

1 10

tl Vtl

BV

DiU Diallfiiri

C:

. B-tki

THIrt:If tki milt i« i "In fti ittf tk«i tr MI«! U tkil iv i t , t t f« r t tki rail*.B:Ittieittf ciu^tH vai tialrt*' («r kit ««t ddietiT liytrt tkilimn ditietiit l i i i t fir tki luplt vitk tki V ( i f . I l l f ) kauri•• sieiisarr client . / i i l i t i i i attiii. (Tkit ii tittki listrtmiit 4iticti» l i i i t . ) Tki t»tnti ikiild rtiiCeiM"' «* ualyiil fir kit tit 4it iet itf . Tl* tnkir iilima itt i i i tklt ittictin i i i i t fir tli ia*»Ii.J:Iiriieitif at ittiMtii* rtlii. Tkii (U| if tsid iltkir•itiiatltf a CHCiitratlii fie t i i ta t i f i l r i< i i t i f l i 4trkiri * 1:1 riifiiii ii limit ir wkn tki uis tyittril 4at«ItriicatH tki fri»Mci if a ciifinri tktt Miti tki Kitt i f lcat l i ter i t i r ia kit tki null Ii I»n tkit tki tfttiliti l itietlit Hut kittr iat ir tkat lit* ( i f , 1 I J ) . If l imi t if l i t ict itt ii II ifl aid aeiieiitntiii if 1 ifl if calctlati4. nftrt at IJ

i i i t ie i t f i yaruitits tfkiri tki i d i t t i f t e i -If CC/I1S. Siifli eimfotiit ft* t icHn)«llutraet f hoi 1 4 ki eitfiiaid IT

Tki* f l a t *Mli«tilt vai citfirmidM/iI Ii tki f i t a lI:nil f l i f ii tiH wkit i it lfti if (»n< t> bl t tk is *•!! tf afufli. It liditatii ^ i f i ik l i /pr ikakl i kUtk ciitaiintitt aidvarti tki data mr ti taki a|fti|riiti ac t i i t .OTttl:Otktr (li|f attf f i i tutM lay Ii ii|iiriri ti y r o f i r l f i i f lutk« r i i t l t i . If ifid. tkif uit ki f i l l f Oiciikid aid iitk

t attackiri ti tki data

Laboratory Na«e:Case No: 7351

ENVIRQDYNE Sample Nunber


SentvolatiIs Compounds

Con c an tr at i on : LOWDate Extracted/Prepared: 6-1-87Date A n a l y z e d : 6-13-B7C o n c / D i l Fac to r : 1Percen t M o i s t u r e ( d e c a n t e d ) : 14 .

CAS NK

108 5-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-3W106-44-5621-64-767-72-198 95 378-59-i8B-7W105-67-965-65-0111-91-1120*5-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-45-491-58-783-7M131-11-3*** HI •ffJO TO Q

99-09-2

Phenolbi5-(2-QU(raethyl)rthr2-Odaraqhenol1 ,3-DioMflnteunl,4-fcchIxQbB«B»Bwuvl WcoSol1,2-ftchl.irotanzB*2-fethylphaulbif- (2-Otl oroi foprafryl ) rttw4-fethylphrolH-ni tr oso-ft -tt-prniyl m wteachlomthantKtrobBttmIiophorm2HtttropheioI2,4-Di«thylphBioiBenzoic Acidbii-ttMaroethoxy)Nethane2,4HKdilirqitm)L1 ,2, 4-TrichlflntenzBnIbptithalm4-OJtroinihntttaadUcrdbutkim4-Qaoro-3-^trylph0X)l2-fethylnaphthalmHnachl tncydopentadi me2,4,6-TridilcrophBiol2, 4,5-Tri dd orophexil2-Dil oronaphthilwf2-HitroaniliniBivtbyl phthalatiAcnapttiylne3-tttrtwuliw

B

uqtq

770 U770 U770 U770U770 U770 U770 U770 U770 U770 U770 U770U770 U770U770U770U3800 U770U770U770 U770 U770U770 J770U770 U770U770U3800 J770U3BOOU77011770U3800 U

6PC Cleanup : YESSep. Funnel Extraction : YES CC o n t i n . L i q . - L i q . E x t . : YE5 (

CAS to:

83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27006-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-OH120-12-7B4-74-2206-44-0129-00-085-68-7tl-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2

kenapfethm2,4-Oinitrflptwnol4-tftn3pheaolDibenzottran2,4-OiutrotoluiM2r6-0initrotoliantDitthYl phtlulatc4-QiIorflDhBiyl-phenyi ethe*RUOTB*4-tbtroaiilin*4,6H)initro-2^VthYlphB)olH-nitrnodiphEnylaiini (1)4-Bro^«nyl-phmyt etherteadilonteiZHifrBitacfaloroyhcMiFtvunUv ••AntbricM ,Di-trbutyl phtiuiit* /FlmrvthmPyrentButyl -b«yl-j*thtlite3,3 '-Oi chltrobenzi dimBouodJirthracentbif-(2-EthylteKYl)phUulatcOryffMDi-n-octyl phthalatcB*UD(b)fluoranthcntBBaotklfluranthiniBfrao(i)pyrB»Indni(ll2T3-oi)pyrnR bwzo ta.h) wthraontBenzolghilprYlvii

^1 (circle one)v N Q / ( c i r c l e one >

oqlq

770 U3800 U3800 (J770U770 U770U770 U770 U7701)3800 U3BOOU770 U770U770 U3800 U770U

r-Jauu— 22LLJ77&~T

770 U770U1500 U770U490 » MJ- fJ-^_770 U770 U770 U770U770 U770 U770 U770 U

11)-Cannot be separated fro* diphenyla-nine

.FORM 1

Laboratorv Name

Case No ___'Sample Numb«r

Concentration £o*t/ Medium

Date Extracted'Prepared ____P_

Dat« Analyzed _______LllkliZ

Cone/Oil Factor ________L^


Pesticide/PCBs ^>

(Circle One) GPC Cleanup^Yes QNo

- * '_______ Separatory Funnel Extraction QYes

———————__ Conltnuous Liquid - Liquid Extraction OYes


CAS ug/Iofug^KoNumber {Circle One|

319-84-6319-85-7319-86-868-89-976-44-8309-00-21024-57-39S9-98-860 57-172-55-972-2O-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469 21-912672-29-611097-69-111096-82-5

Alpha -BHCBeu-BHCD«lu-SHCGamma-BHC (Undane)

HepuchlorAWnn

HcptxcMor Epox»d«EndosuHan 1Oietdnn4. 4'-OOEEndnnEndosuHan U4. 4'-DODEndosuHan Sutfate4. 4--OOTMeirxKvchlorEndnn KetoneChk>rdan«ToxjpêneAroclor-1016AroclOf-1221AroclOf-1232Aroclof-1242Arocior-1248Arodcx-1254

Aroclor-1260

lt> U

(b U

/t UH, ILIt U)b KIt UIfc U.37- tA32. OC71 tA7iU.?2 U_3^ u1 U.

(bo U3* U.)feo Lt320 Itit-o 1Ûa U)ba Urtc- It\bc U3~o M.5Z.o (A

orW.

V( « Volume of e«tra« wheeled (ul)

V * Volume of waief extraaed (ml]

W$ s Weight of sample ertracted (g)

v( * Volume of total emraa (ul)

3o^ _ „ IO.AOO

Form 1 7/85

EL-Organic* Analysis Data Sheet

(Page 4)


GAS

7

10..11-

is..16..

17..

18..

50

23

23—

24—ZS._

2G._

27..28._

29._

Compound

u-f jf\ rpp /L r hx5T^Li AAV_ n fru/v .

Fraction

JL_L

IQ • 0

is. \

. L,

\

S6.0

956\-StTb 3

M**o-\

VO

%

? es

O r g a n i c * A n a l y i i i D a t a S h t t t(Pagt 1) I

Laboratory Mam*: ENVIRODYNELab Samplt ID No: 17002*04Samplt Katriz: SOILData Rtltife A u t h o r i i t d BT <V\CXU

S a m p l i N a m b t t„„ —— .-.

EL

Can No: * "QC R e p o r t No:C o n t r a c t No: _______Dat i SaapIt Rtct iv td:

Voiat i1* Compound•

Concentration: LOWDttt Eitracttd/Priparid:Datt A n a l f l t d : 4-3-87Cone/Di1 Factor. 1Ptrctnt Moiftnrt <not dicantid) 14. i

US Mi: Ci! Me •Ik?

74-17-374.-I3-?73-11-475-M-I73-11-2•7-44-173-13-173-33-473-34-3134-41-347-44-3117-14-271-11-171-33-434-J3-!111-13-4T3-J7-4

CklirtMtkanIrtMHtkanTlif l CkltridiCiItiDttkaitRttkfltit Ckltti itiCltlll |

CarkH Dii i l l idt1,1-Diekltttttktit1.1-DiekUtittkaattraii-1.2-DUkltmtkiiiCkltrtftn1,2-Dtaitrtttkui2 -H taitia1,1.1-TrttiUrittkkitCarkti TttiackltrldtTiayl lettattIrntdiekltrmtkut

122217i

i121 1

BVVV

0 i

-I

71-17-3llltl-12-iTt-ll-4124-41-17J-II-S71-43-2UI41-I1-3lll-TJ-l73-23-2lll-ll-l3»l-7l-<1Z7-U-47f-14-3lll-ll-llll-fl-7HI-41-4111-42-3

1,2-Ditkliritrttaattra*i-li3-DickItrBir«|titTricklartitktiiliktntckltrtittkaii1.1,2-TrickltrtttkaitIttitittif-l,3-DltkIiritr«ttii1-CiliriitkjliliYlitktrIcMidnf.-Hitkrl-2-rtitaitit2-Itiaitll

Tttraekltrtitktit1.1.1.2-TitratkIirtitkaitTtllHtCklttlhlltllfl

lUTlkusiiittrrtuTftil IfltKII

IV

12 11 D12 912 I

1fI1VI1

Dttt

fKBI;tl tht ruilt ti i Tilti irittn tin tr 1411! ti tkil imit , rt|trt tkl »*i««

OitlHltrs

Tkii Maf aiiliis tt f t i t i c idt laraatttri witit tkititi vai etafiritd IT CC/fB. Sliflt etBftatitit/il ii tkt dial t itrtet iktild 11 etidntd kf CC/NS

Iilicttti c«f«n< •*• tulyttri (•! kit ut <itict*4. lifirt tktBtiimo ItttetUi liiit dc tkt inpli vitk tki V (M.IIO) ktfidti itttiittf t i ietit . /IUitit i ictttt . (Tkts U i»l itctiitrilftkt lutrntit (ttittiii l i m i t - ) Tkt ftit ittt iktil« ml: V-Cnftnd vtt «»IytH fit kit itt I t t tetH. Tkt inker li tkt•inia tttiinbli littcti» l i» i t (ti tkt tuplt.J:Iitfieittt u tittutid ftlit. Tkii fli| ti nti titktt vktitittmitiii • ctieiittititt ftt t t i t t t i t t l f irititi l it l etifonlivktit a 1:1 rtflfotflt ii aiint^ K wk» tki tan i f iet tal dataI i f le i t i4 tkt ittftiet K a cn|«n' tkat uiti tkt td t i t l f icttitictittrit kit tkt i t i t l t li l i ft tkai tkt i^tiliti < i l tc t i* i lliit kitIttattr tkas itrt (t|, 1IJ) . II I i » i t •( t f t t tet l t i Is II tfl ud acnciittattii t( ! i|l ii ealetlttti, tiptt ai )J.

Tki i flaf It nt< wkii aialfti It ftiid Ii klaik at vill ai a•aa|lt. It lidicatti |tii iklt/ |rtkaklt klaik eiituiittiii uivacii tkt data ifit U takt «||titrtatt actit i .

Otktt f l t f f aid (ittiftti uy W ttftirti tt i t t f ir ly lifiittkt rmlti. If md, tktf ntt kt f i l l f di ici ikid aid sickiitcriititi attaektd tt tkt data tatary nptrt.

Laboratory Naue:Case No: 7351

ENVIRODYNE S a m p l e N u m b e r : EL 2


'

Concentration: LOWDate Extracted/Prepared: 6-1-B7Date Analyzed: 6-13-87Conc/Dil Factor: 1Percent Moisture (decanted)

Seiivolatile Compounds

6PC Cleanup : YES

14.6

CASJto: uqkq

108-95-2111-44H95-57-fl541-73-1106-46-7100-51-695-50-195-48-73963B-32-9106-44-5621-64-767-72-19H5-378-59-1BB-75-5105-67-465-85-0111-91-1120-B3-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47SBB-06-295-95-491-58-788-74-4131-11-3208-96-*99-09-2

Phenolbii-12-ailxoBthyUtthjr2-Qilorcphenal1,3-Dichlardwruerw1,4-DidilxofaenzeneBeruyl Wcrfcl1,2-OichlxDbenzene2-fethylphaulbis- (2-Cblxoisopropyl ) ether4-fethylphenalIhii tr oso-Di -tt-pr op y 1 ati nfHexachlxoethaniNitntenzewiBQphxmeT-tttrophenol2,4Hhwthyl phenolBnzoic Acidbis-{EMxorthmv)nithane2,4-Oichl tropoennl1,2,4-TridUxobenzH*Ibphthalene4-QUxoanilinetoachlxcbutadiene4-Qaxo-3-fethylphenol2-HethyIuphthalBiiteachl xttydcpentadiew2^4,6-Tridilxaphenol2,4,5-TridilxQphenol2-Otlxonaphthalene2-totro*iihf»Diwthyl phthalateAcBiapthylene3-tttroaoilint

770 U770 U770 U770 U770 U770U770 U770 U770 U770 U770 U770 U770 U770U770 U770U3700 U770U770 U770 U7701)770 U770 U770U770 U770 U770 U3700 U770 U3700 U770 U770 U3700 U

), F u n n e l E x t r a c t i o n : YES \i t i n . L i q . - L i q . E x t . : YES (

CASfet

83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-5MB6-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44H)129-00-085-68-791-94-156-55-3117-81-7BB-01-9117-84-0205^9-2207-08-950-32-8193-39-553-70-3191-24-2

Acenaphthene2,4-Oinitrophanl4-tttrophenolDibenzofiran2,4-ttnitnjtolutne2,6-DirutrotolueneDiethyl pbthaliti4-Qilxopnenyl-pnenyl etharFluor ent4-tttroaniline4 , 6-Oi ni tro-2-ttethyl phenolH-nitrosodipnflnylatdne (1)4^roaaphertyl-phenyl etherHexadvlantotteMPentadilxophmlPhenanthreneAnthraceneDi-n-fautyl phthalatenucrnthcnePyreneButyl -benzyl -phthal ate3,3'-DichlxobHi2iilineBenzo (i) anthracenebis-l2-€lhylhoyl)phthaUt«OirysentOitroctyl phthalateBnzo(b)fluoranttwne&nzo(k)fluorantheneBnzo(a)pyreMlndero(l,2,3-cd)pyrtneDi beozo (a f h ) antiracmeBeraoighilperylant

H&iV ( c i r c l e o n e )^JlJO) ( c i r c l e o n e )

770 U3700 U3700 U770 U770 U770 U770 U770 U770 U3700 U3700 U770 U770U770 U3700 U770 U770 tk.

^9wi)770 U770U770 U1500 U770 USWWWj-p^770 U770 U770 U770U770 U770 U770 U770 U

(l)-Cannot be separated fro« diphenyl*«ine

FORM 1

Laboratory Name

Case No ' ' "7Numb«f

Concentration fey/ Medium

Date Extracted'Prepared ____2J

Date Analyzed ._______^

Conc/Dil Factor \


Pesticide/PCBs


______ Separatory Funnel Extraction OYes

_____ Continuous Liquid - Liquid Extraction QYes ^p


CAS ug/loru^KoNumb«r (Circta Onef

319-84-6319-85-7

319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-2111O4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha-BHCBeia-BHCDelta -BHCGamma-BHC (Liodane)HeptachlorAldrin

Heptachlor EpoxideEndosulfan 1Dieldrin4. 4--DDEEndnnEndosuttan It4. 4'-000Endosulfan Sufaie4. 4*-ODTMeihoxyctiforEndrin KetoneChlordaneToxapheneAroclor-1016Aroclof-1221Aroctor-1232Aroclor-1242Arociof-1248AroclOf-1254

Aroclof-1260

/fc UIt U

1h U.It Uli UIb l(It (4Ifc U

32- IA

3iU-71 UJiU.?ZtL52 U?!. IXfto U31. U.) fco U5zoU.'to LlU.3 U

t feo \iI'j? IX\fccr U"JZO L<.

5Z.o U

orW.

V( * Volume of extract injected (ul)

V = Volume of water extracted (ml]

W = Weight of camp(« extracted (Q)

(ul)

0, 600

V. - Volume of total extract (ul)

'Form 1 7/85


Tenlativoly Identified Compounds

CASCompound

~7.0

t613 3

I Q - 6 940It. 1

J3,

rflQO. rb^. J^J.10.

i*.is.16.

17.

18.

20.

21.22.

23.

25.2€.27.28.

^

Uj

ttn I. ? as

Organ i ci Ant I yi i i Data Shctt(Pigt 1)

Samp It Number: EL

Laboratory Naat: ENVIRQDYNELib Samplt ID No: 87002405Simplt Matrii: SOILData Rtltut Authorised By:

50Cast No: :*'QC Rtport No:Contract No: _f/.?_-_Qj;Datt Saaplt Rtciivid

Volat iIt Compoundi

Conctntrit Ion: LOWDttt Eitrtettd/Prtptttd:Dttt Antlyxtd: A-3-87Cone/Oil Factor: 1Ptrcant Moiitnrt (not dtctnttd) 1 8 . 7 1

CIS Mo CIS Ml

74-17-374-13-?73-11-473-11-373-lf-247-44-173-13-173-33-473-34-J134-41-3•7-44-3117-14-27I-71-3Tl-33-434-21-3111-13-473-27-4

Cklt iomttkta t 1IrtmomttkiatTiByl Ckl tc id t 1CklenitkiBiHttkyltat Ck l t t i d tIctttatCttboi D i f i l f i l t1,1-DlcalortttktatI , l-Dtekltrt t tk»ttr iBB-l r2-Dicki t tot tktatC k l t c e f t r m1,2-Oickltrtttkut2-littatatl.l.l-TtieklttottkutCitkti Tt t r t tkl t i idtVlayl icittliIrntdiekltrtmatktaB

2 U1 U2 D1 0^0'10909QV8

2 0V0

U VI 0

TI-17-5IHH-ll-i7»-ll-i124-41-1Tf-M-S71-43-2lllU-ll-511I-7S-I73-23-2lll-ll-t5T1-7I-*127-11-47»-I4-3lll-ll-Jlll-fl-7ltl-41-4111-42-3

1,2-OickItttptiptitttiaf-l,3-DieBlo[apropintTilekltrittktaiBibromtckiaroattktatl,l,!-TriciIeri.U*BiItattat (cif-l,l-DiekI«roprBptat i2-Ckltt*ttkylTiaylitktrItmftrm i4-IIttkTl-2-ptattafiBt2-BtitaeatTttrtekltttttktat1,1.2,2-TttitekliitttktatTil nitCkltrtktaitatttkflitaitatStyrtatTtttI Ifliati

U0U00DU2 DD2 U2 V000000D

Diti I tptr t iaf Qulif i tcs

ULUE:If tkt titolt is i ftltt fritttr tk» ir tt.«il tt tkt dtttctitalimit, rtptit tkt ?»ln.B:ladiettts oaf end vaf tatlyiid (it lit itt dtttettd. Itptrt tkta in an dtttetita lint (or tkt ftmplt witk tkt U (19,110) ktstdta atctiftry ctaetat./dilitita ttti». (Tlii ii act accifinilftat iaitrntat 4tttcti» liait.J Tkt ftttattt ikoiU rud: 0-

vis utlyti< f*r tit att 4ttteti4. Tkt anbir it tktittsiaiklt <ttteti«a limit ftr tkt iu|Ii.

J:laîcitti ta tftimattl rUit. Tkif flif if aittf titktr vktatftimitiaf t etaetatntita tit ttaUtiftlf idtati(it< c*m»otadf•atrt » 1:1 ttiM"* t« »samt< tr vfcta tkt un ittctrtl fittiat*iettt< tkt irtsiiei If « etmtatal tktt mtttt tkt ttftatifltitieae r i t t r i i lit tkt ttiiit it litr ta*a tkt ificifit* ttttctita limitftiitir tkia itrt (t|, 1IJ). K limit t( Itttctita ii II ifl tad tcvactatiitita t( 1 i|l If eileiUUrf. rttttt » JJ.

C:Tki« fltf itplitf t« ftiticidt iitutttri vktri tkttioa vii etafirmtd If CC/KS. Stiflt cemtoBtit iistitidtil-llaffil ia tkt (iul utrict iktild it etafintd by CC/K5I:Tait fUq it tit! wata utlrtt if lond ia il»k n vtl l *f iftmilt. It iadieittt t t i i i k l t / i f t k tk l t tlial c iatuiatt i ta tadmrif tkt d*ti »tr tt tttt itpriiri itt i c t i o i .OTRU:Otkti (Ii(f tad (tttattti may •• itt.iiitd t« ttotnir difiattkt ttfilti. If ictd, tktf mift It f i l l f dtieiibid tid fickdtfcriptioa itttektd tt tkt dttt saury tipart.

lit

Laboratory Naae:Case No: 7351

ENVIRQDYNE Sample Nuaber: EL 258

Orqanics Analysis Data Sheet(Page 2)

Concentration: LOWDateDateConc/DilPercent


GPC Cleanup : YESx t r a c t e d / P r e p a r e d : 6-1-87n a l v z e d : 6-13-87i l F a c t o r : 1t M o i s t u r e ( d e c a n t e d ) : 18.

CftSto:

108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-W-73963S-32-9106-44-5421-44-747-72-198-95-378-59-1BB-75-5105-47-965-85-0111-91-1120-83-2120-82-191-20-3106-47-8B7-4B-359-50-791-57-677-47-4B8-06-295-95-491-5B-78B-74-4131-11-3200 % Q99-09-2

Phenolbi*-(2-0)laraethyl)etiw2-Oilorophenoll,3-0ichlareben2ene1,4-OitMorabenzeneBenzyl Alcttal1,2-Oicblarobenzene2-fethylphenalbis-(2-ChlQroi50propyl)ether4-nethylpnenalIhri trow-to -n-propylainetaachlaroethaneNitrobenzeneliophorane2-Mttropheral2,4-fli*thylphenalBvtzoic Acidbis-IOilirwthoy) tethane2,4-Oidilorophenol1,2,4-TrichlGrobenzenebpfattulene4-OilxoanilineHetachlorobutadiene4-QU aro-3-trthylphewl2-ltthyl naphthaleneteachl crocyd opentjdi ene2^ 4 ,6-Tri ch 1 or ophenol2,4,5-Trichlarapnenal2-Qilaronapt)thalen(2-ttitroaniUneDiwthyl phthalatiAcenapUrylene3-)*itrwnilint

7

uqkg

810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 I)810 U810 U810 U3900 U810 U810 U810 U810 U810 U810 U810 U810 U810 U810 U3900 U810 U390QU810 U810 U3900U

Sep. F u n n e l E x t r a c t i o n : YES <C o n t i n . L i q . - L i q . E x t . : Y E S

CASfc:

B3-32-451-2B-5100-02-7132-44-9121-14-2606-20-284-44-27005-72-386-73-7100-01-4534-52-186-30-4101-55-3118-74-187-B6-585-01-8120-12-784-74-2206-44-0129-00-0B5-48-791-94-156-55-3117-81-721B-OH117-84H)205-99-2207-0&-950-32-8193-39-553-70-3191-24-2

Acenaphthene2,4-DiiutrDpnGnol4HbtrcpheralDifaenztrfiran2,4-OinitrotolueDe2,6-OinitrotoluneHietbyl phthalatf4-QUtn?ihenyl-pinnyI etherFluorine4-Hitroanilinc4 , 6-Di ni tro-2-*Wryl phtoolH-nitrTBodiphenylanni (1)4-fircaophenyl'pt)cnyl ithertaachlorobercemtatachlorophenolPhcnanthremAnthracentOi-nHwtyl phthalatfFluorantteMPyraieButvl-toUYl-phthalate3,3 ' -Oichl tnteui rfi ntfienzotiJ anthracenebii- (2-EthylhexyI ) phthal ateQryseneDi-n-octyl phthalatcBenzotbmuoranthentBcnzo(k)fluranthentBenzolaJpyrentIndeno ( 1 , 2 , 3-cd) jrvreneBibenzo(a,h)antbracene8enzo(ghi)perylene

^£& (ciQjOjjici

oqtq

810 U3900U3900U810 U810 U810 U810 U810 U610 U3900U3900U810 U810 U810 U3900 U810 UJ1QJJ

^JTOOîfmr

810 U810 U1600 U810U320 CBIO U810 UB 1 0 U810 U810 U810 UB10U810 U

(circle one)circle one)

(l)-Cannot be separated iron diphenyla»in« : ._

FORK 1

Latxxaiory Name

Case No ___ .Sample Number

Concentration


Date Analysed .

Cone/Oil Facior

Medium

i'J-

t» - /4 "

Organics Analysis Data Sheet(Page 3) *

Pesticide/PCBs(Circle One) GPC Cleanup,QYes DNo

L_________ Separator^ Funnel Extraction DYes

__________ Continuous Liquid - Liquid Extraction DYes

-2.

-\\0

Percent Moisture (decanted) / *^ /

CAS ug/loru^K^Numt>«r (CircU Or**)

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha-BHC

Beta-BHCDeita-BHCGamm»-BHC (Linda netHepiachlorAldrm

Heptachlor EpoxideEndosutfan IOieldrin

4. 4--ODEEndnnEndosuHan II

4. 4--ODOEndosulfan SuHate4. 4'-ODT

McthorvchlorEndrin Keton*ChlordaneToxaph«f>eAroclor-1O16Afoclof-122lArOClor-1232

Aroclor-1242

Aroclo'-1248Aroclor-1254

Aroclor-T260

/& U

|t> U

\k Ltib aIt UIb ViIt IXIb U.3z- u-31 U,7L tA12. U.?ZtL52 U-31 U.fbo U31* U.Ifcfl U-_?isa_ifeo 11Uo U)b3 \1lfr<? (^\£«? U32-0 K3in LC

V( = Volume of e*lr»ct injected (ul|

V$ = Volume ot waief ettracied (ml)

W$ = Weight of sample extracted (g)

V( s Volume ol total extract (ul)

of W.

Form 1 7/85

fc -JHO

• too Orgaoics Analysis Data Sheet(Page 4)

[ b L

T«n(a(ivoly Id«ntifi«d Compounds

CAS

(wg/l

il/Y\\f

ib.oii.

So -3IS. I

5..

Oo- Icm

3-M.3

tl

O r g a n i c s A n a l y s i s D a t a Shtt t( P a g t 1) :--•

L a b o r a t o r y N a m t : C N V I R O D Y N EL a b S a m p l * I D N o : 1 7 0 0 2 4 0 *Saap la M a t r i i : S O I LD a t a R i l i a c t A u t h o r i s e d B y :

Cast No: 1^QC Rtport NoContract No:Datt 3a»plt Rictivid:

Saaplt N u n b t r : EL

"is"/""""""""

fig-QI-"?D9"7

V o l a t i I t Compounds

C o n c t n t r a t i o n : LOVD a t t E i t r a c t t d / P r t p a r i d :D a t t A n a l y i t d : 6-3-87Conc/Dll Fac to r : 1P t r c t n t M o i s t u r e ( n o t d t c a n t t d )

CU Mt: CIS It:

74-17-374-13-t73-11-473-11-}73-11-247-44-t73-13-173-33-473-34-3134-41-347-44-3117-14-271-73-171-35-434-21-31H-I3-473-27-4

Ckltr tmttkait 1Iromemttkait 1Tiiyi CiltrUt 1Cklort t tkai tftt tkyltit CkUtit tietttit 1Carkti Di t i i fKt1,1-DlekItrtttktitl . t-Ditkltrtttkaitt rau-l ,2-DickIt t t t tkt i iC k l t r t f t r m1.2-DitkItrtttkaitMttmti1,1.1-TrtckItrtitkaitCarkti Tttrackltri i tTiiyi icttattIrtmtti tkltrtmttkaai

2 92 92 92 9

•?£JO9D99V9

2 999

11 9I 9

71-17-3 1 ,2-Dicklertprtptai1M41-I2-4 l t »« - l , I -D i c i I i r o i rop i i iTf-ll-4 Tritkltrtttktit1X4-41-1 Bllrtmtchltrtmttktit71-11-3 1.1,2-Trlckltrtttkait71-41-2 Itiitit11141-11-5 eis-l,3-8iaitrttreptittll-73-l 2^kltrtttkylrii;lttkir73-23-2 liMtftrmlll-ll-l 4-Xttkyl-X-ptitaititSfl-71-4 2-Itiaitit1X7-11-4 Tttrackltrtttkait7T-14-3 1,1.1.2-TttraekItrtttkaattll-ll-1 TtlitMlll-fl-7 Ckltrtfctittit111-41-4 Itkylktmstmt111-42-3 StyriM

TtUI Xyltus

4 Q4 U4 94 V4 94 94 912 I4 912 911 9

Data Itptrtiii Qtalifitrt

.'ILDt:If tkt rmlt ti a ralit f r t i t i r tkii ar it.it 1 tt tkt itttctltil im i t , rattrt tfct Tain.J:Iilicattf CHioni vai aiaiytt< ftr kit lit ItUctid. Itttrt tkt• niin ttttctiti limit dr tkt samslt witk tit 9 (if,110) kastlit itttssary etietit./i'ilitii* actlti. (Tkis ti itt itcisiaiilftki intrant itttctlti limit.) Tki ftttaitt skull rta<: 9-Ctmptiatf wai atalyiiri lor kit itt <«tictt< Tkt inktr If tktmiiimn tttiinklt Itttctiti l i m i t ftr tkt iimftt.4:Ii4ieatts ti tftimattl ralit. Tkii ftif ti ntd titkir vktititimatlif i ctietitratioi ftr tt i t a t i r t l y Htitifitd ctm|ends«ktrt a 1:1 rtxttist tt animtd tf vkti tkt miif tttetril fataIaiicatt4 tkt prtitict if a tntoiad tkat mtttt tkt UtttificatUicrittria bit tkt null If list tkai tki ifteifitt littctlti l i m i t kitirtattr tk«a itrt (t|. 1IJ). If limit tf <ittcU» li II i|I aid atoictitrititi tf 3 i|l is calcilattd, rtfvrt ai JJ.

Tkii flag ifftiif tt ititlcilt taramtttrs vkirt tkt i d t i t i f i c i -tl» «ai etafirmtri ky CC/KS. Siiflt cnptitit lift icidn)«llt|/il li tkt (ital titnct ikttU kt etifirmt* ky CC/HSI:Tkii (Uf is istd wfcti amalytt is ftntf la klui as vt!I as ifUflt . U litfieitti |« is iktt / trt i ikl t klttk e tatamiat t t t i ail•arts tkt lata istr tt takt ai irtprlatt act loa .

Otktr flags aitf ftttittts may I* rtfiirtl tt trtM^T 'tfiattkt rtsilts. If ntl, tkty mtit kt filly ttierikttf »4 nekitieriitioi attaektl U tki Uti stmmacr ti i o t t .

Labor ator v Nane:Case No: 7351

E N V I R Q D Y N E SaiolB Nueber: EL 2S&

Qrqanics Analysis Data Sheet(Page 2)

S e a i v o l a t i l e Co*pound§

Concentration: LOWDate Extracted/Prepared: 6-1-87Date Analyzed: 6-13-87Conc/Di1 Factor; 1Percent Moisture (decanted) 19.2

OSfc: uqkg

108-W-2111-44-495-57-fl541-73-1106-46-7100-51-695-50-195-48-739638-32-106-44-5621-64-767-72-193-95-378-59-1BB-75-5105-67-965-S5-0111-91-1120-B3-2120-82-191-20-3106-47-8B7-t8-359-50-791-57-677-47-488-06-295-95-491-58-780-74-4131-11-3200 96^99-09-2

Phenolbis-(2-Qiltrnethyl)ether2-Qilorophenol1,3-Dichlorobenzenel,4-DichIaraben2eneBenzyl Alcohol!,HKchlcrobenzme2-fethylphenalbi s- (2-Qi 1 or oi sopropyl ) ether4-tethylphenolH-ni tr oso-Di -rrpr opyl ui neIteachl methaneNitrobenzeneIsapharon2-tttrophenol2,4-th KthylphmalBmzoic Acidbis-(Dilimethmy)tetha«2«4-DichlcrQph«K)l1 ,2,4-Trichlorcbenzenetaphthalene4-Qilaroanilir«teachlorobutwiiene4-QUaro-3-«thyl phenol2-*thyl naphthaleneHex achl trocydopaitadi ene2,4,6-Trichlxcphenol2,4,5-Trichlcrophenol2-Oilxowph thai ene2-MitroanilineDiKthyl ptithiliteAtenapthylent3-Mitroaniline

820 U820 U820 U820 U820 U820 U82008200820 U820 U820 U820 U820 U820 U8201)820 U40000820 U820 U820082008200820 U820 U820 U820 U820 U4000 U820 U4000 U820 U820 U4000 U

Sep. F u n n e l E x t r a c t i o n : YES (

C o n t i n . L i q . - L i q . E x t . : YES C

CA5MK

83-32-951-28-5100-02-7132-64121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-5BWH120-12-784-74-2206-44-0129-00-085-6B-791-94-156-55-3117-81-7218-01-9117-94-0205-99-2207-06-950-32-8193-39-553-70-3191-24-2

Acenaahtbent2,4-QinitrQphenal4Hbtrap6enalDi benzol iran2,4-OipitrotoIueM2,6-OirutrotfllueniDietbyl phthaliti4-ChlornphenYl-phenyl etherFluor en*4-fbtroaniline4,6-ftni tro-2-fWiyl phenolLI - 1 i' i i • it *«™fUu uMJLUyJ HIT llfW ll/

4-aroK9h0tyt-phtByl itlwrteachlu (ixsuenePntadilaroêoolntenanuimntnracEntfii-n-ûtyl phthalateFluor aothen*PyrweButyl -fcenzvl-phthalit*3,3'Hhchlarabenziihne6enzD(i)vithracHWbis-(2-ethylheiyl)phthalateChrvuneDi-n-octyl phthalateBetuo(b)flutrwthewBmzDlkHlua-arrtJw*BwiodJpyTBwlndeno(l,2,3-cd)pyreneOi bemo U, h) anthr at eneBenzo(ghi)perylmt

Si^tci^NGjici

820 U4000 U4000 U820 U820 U820 U8200B20U82004000 U4000 U820 U820 U820040000820 UR2CJl^

L41Qj^820 U820U820 U1600 U8200370 ST82008200820 U820 U8201)820 U820 U8200

(circle one)i c i r c l e one)

(U-Cannot be separated fro* diphenylaaine

FORM 1

Orgaoics Analysis Data Sheet(Page 4}


.3*

-f It

VOrt

-0-nn-n-nam-o

90,3-

7 8S


Saaple Nu»ber: EL

Laboratory Naae: ENVIRODYNELab Saaple ID No: 87002776Sa*ple Matrix; SOILData Release Authorized By:

Case No: 7351QC Report No: ./30___.Contract No: ..IfiXr.Qj.Date SaBple Received:

Volatile Compounds

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted) 10.2

<fe

CAS to: CASto: uqkq

74-S7-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278 3-371-55-656-23-5108-05-475-27-4

ChlorotethawBromethancVinyl ChlorideQtloroethsnefrthylene ChloridefcfitmeCarbon BisulfideItHHchhraethcneM-Dithloroethanetrans-1 ,2-tochloroeUwneQtlaroftn1,2-QichloraRthane2-ftitanone1,1,1-ThdUtroethnCarbon TetracbloridiVinyl AcetateBr otodi chl arowthanc

111111 U \11 U l11 U958

• ^'£43W6 U6 U6 U6 U6 U& U11 U6 U6 U11 U6 U

78-67-510061-02-67M1-6124-48-179-40-5

^ 71-43-210061-01-5110-75-875-25-2ioa-io-1591-7B-61Z7-1B-479-34-5lOft-ffl-3106 0-7100-41-4100-42-5

1,2-OichliriroKtrans-1 ,3-OichloniprQ(w»TridUoroetheneDi bronchloraethane1,1,2-TrichloroethaneBenzenecis-1 ,3-OichloroprDpem2H>1 or cethyl vi nyl etherBroKrfori4-ftrthyl-2-penUnone2-tinUKniTetrachl onxthvc1 , 1 , 2, 2-Tetr acil or oethaneTolueneOUorobenzeneEthylbenzeneStyrcntTotal lylenes

6 U6 U6 U6 U6 U6 U6 U11 U6 U11 UU U6116 U6 Ud U6 U6 U

f UM I • mul t (• * *•!»• ^vvtv

trltvl* hwt Ov r»»Mlt !• ! lrt *B««C*IM UiKt •••»


ENVIRQDYNE Number: EL 260


Sen! volatile Compounds

C o n c e n t r a t i o n : L O WDate E x t r a c t e d / P r e p a r e d : 6-10-87D a t e A n a l y z e d : 6-13-87Conc /Di l Factor: 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 10

CASMo:

108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-32-9106-44-5421-64-747-72-198 75-378-59-1BB-7W105-67-945-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-477-47-48B-06-295-95-491-58-78B-74-413H1-3

, 208-96-fl99-09-2

Phenolbii-l2-QilxaEthyneth*r2-Oilo- thcnoli,3-0ichlxobenzan«l,4-ffichlxabejiz»tBenzyl Alcohol1,2-frchlxctanzent2-fcthylphenalbis-(2-QilQroisoprapyl)ether4^tethylphenolH-ni troso-Oi-n-pr cpyl aii HteachlxostharaNitrobenzeneItoptaront2"mtrQphtnol2,4-&i«*hylphenolBenzoic Acidbis-tfMcnxthtsylfethane2,4HHchloraphenol1 ,2 , 4-Tri chl xobenzen*Naphthalene4-QiloroanilintHexichlxcteitadient4-Odxo-3-«thylphHcl2-tethylNphthaleneHB achl xocycl nwtadi ene2,4,irTnthlcrDphenoi2,4 ,5-Tri chlxophwol2-QilcroniptithiImf2-MitnuniliniDiMttwL phUulateAcB^thyler*3-Mtroaniliw

.2

^

730 U730 U730U730 U730 LI730 U

- 7 3 0 U730Q730U73011730 U730 U730 U730 U730 U730 U3600 U

. 730U730U730U730U730U730U730 U730U730 U730U3600 U730 U3600 U730 U730U3600 U

BPC C l e a n u p : YESSep. F u n n e l E x t r a c t i o n : YES \C o n t i n . L i q . - L i q . E x t . : YE5 '

CASNo:

83-32-951-28-5100-02-7132HM-9121-14-2406-20-284-66-27005-72-386-73-7100-01-4534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-OChO85-68-791-94-156-55-3117-81-7218-01-9117-84-0205- 2207-08^50-32-8193-3M53-70-3Wl-24-2

AcBnaphthenc2,4-Oinitnvtad4-tetrcphenolDibeuofiran2^4-OiiiitrotDiicnt2,6-Oinib-DtaliM«Di ethyl ptithalate4-Chl(rmhoiyl-phBTyl etherRutrent4-*tnHnili«4, 6-Oinitro-2-hethy 1 phenolKidtrasadiphenylatini (1)4HkroKph«Tyl-phiRYl ttiwrto achl Tries a*hntachlxophenolPheunthrenetathrxmDi-trbutyl phthalateRuxarthenePyrowButylHtenzyl-phthalati3 ,3 ' -Oi chl tntenz i di mBruoii) anthracenettii- (2-Cthvlteyl ) phthalateChryumDi-trtttyl phthalateBnuo(b)flnr»theM8Bao(k}flurantheniBn20(a)pyraielrdcr«(l,2,3-cri)pYremDibaao(4.h)«thracntBBUt>(ghi)perYleni

r^)(ci<^J(Cl

w730U3600U3600 U730 U730U73011730U730U730U3600 U3600 U730U730U730U3600 U730Urau^<c^s>

^T30U730U7301)1500 U730 U_

/ 1300 8ÔlT

730U730U730U730U

KOU730U730U

ci rcl e one)

(t)-C*nnot be separated froa diphenylaaine

FORM 1

Concentration


Date Analyzed

Conc'Dil Factor

Percent Moisiure (decanted)


Pesticide/PCBs

(Circle One) GPC Cleanup^QYes DNo

Separatory Funnel Extraction OYes

Continuous Liquid - Liquid Extraction

Alpha-SHC

Beta-BHCDclta-BHC_______Gamma-BHC (LindanelHepiacMtxAldnnNeptachtorEndosulfan IDieldrin4. 4--DDEEndnnEndosuWan II4. 4'-OOD

Sutfate4. 4'-Dpf~MelhoKycMofEndnn

Chlordane

Aroclof-IOTSAjoctoT-1221Afoclor-1232AroclQf-124?

DYes

or W.

V -* Volume of extract m|ected (oil

V - Volume of water extracted (m()

W = Weigh! of sample ertracied (gl

V * Volume of total extract Ml

3o lo:

Form 17/85

Afo: 73 5"/ Organic* Analysis Oata Sheet(Page 4)

Tentatively Identified

Concentration

~B*)A ' /•ft

3-M6

<S< t MbOtT

1±M5C.3

3 -3 . 1

drocoL

A* A r^co jf bo

s.

? 85

Organic; Analysis Data Sheet(Page 1)

Saaple Nuaber: EL 261

Laboratory Naae: ENVIRQDVNELab Sample ID No: 87002777Si.pl* Hatrix: SOILData Release Authorized By:

Case No: 7351DC Report No: _£3_Q_Contract No: __ip_3__QiDate Saaple Received:

Volatile Compounds

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted)

Ximn03<:mo

GOrn

CO

COCO—J

14.2

CASto: uqkg OB to:

74-67-374-83-975-01-475-00-375-09-247-64-175-15-075-35-475-34-3156-60-547-66-3107-06-278-93-371-55-454-23-5108-05-475-27-4

OiloroiethaReBroBMetnaneVinyl Oil or id*QtloroeUunefethylww Oil TideAcetoneCarbon Disulfide1,1-DichIoroetter*1,1-Dichlxoethanetrans-l,2H)ichlxaeth«Olxofxi1,2-Didiloroethan*2-ftrtanone1,1,1-TrichloroethaneCarbon TetradilxideVinyl tartateBrondi cftlxo«thane

12 U12 U12 U12017*43"14* <*3-

4U **61)4 U4 U4U6U12 U4 U4 U12 U4 U

7B-&7-510041-02-479-01-4124-48-179-00-571-43-2

c 10061-01-5110-75-875-25-2108-10-1591-78-4127-18-479-34-5108-98-3108-40-7100-41-4100-42-5

1 .2-0i dil or opr opinetrans-1 ,3-DichIxapropmTridilxoethewDi bnnadtl xaetharcl,ltMridilxorthaneBenzenecii-1 , 3-Oichl xopropew2-Qil oroethy 1 vi ny 1 etnerBrocrfon4-tMhyl-2-pottanoneHteanowTetrachloraetheiel,l,2,2-Tetrachlarccth«wTaltBieOilorobeuBwEthvlbauawStyrawToUl Ivlenes

6U4116 U4 U6 U4 U6U12 U4 U12012 U4U4114 U6 U6 U4 U6 U

U <*«,

«M ll««t.> TH*

•*/«! In tM* «l*Mi

t ct «B»X>1 0

M fully

but th» rMMlt !• !••• thwi Uw tatvctlvi llMt bwt

L a b o r a t o r y Naae:Case No: 7351

ENVIRQDYNE 5a«ple Number: EL 261 f\o


Concentration: LOWDate Extracted/Prepared: 6-10-67Date Analyied: 6-13-87Conc/Dil Factor: 1Percent Moisture (decanted)

Seaivolatile COMpounds

GPC Cleanup : YES

14.2

CftS to:

106 5-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9104-44-5621-64-767-72-19*45-378-59-189-75-5105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-46B-06-295-95-491-5B-788-74-4131-11-3'Vfi-Oi—H£M 70 U

99-09-2

Pbenolbi s- 12-Qtl tnethyl 1 eUw2-Oiltropbenoll,3-OidiIord)euBtt1,4-Oidila-DbwieneBenzyl WortilI12-&ichlcriteaene2-fethylptenolbi s-(2-Chl oroisopropyl ) ether4-ftthylphmolH-ni trcwHh-inr opyl MI ottoachlEroethaMNitrobenzmiInpnortiM2-tttrophBtol2,4-ttHthylphmlBenzoic Acidbi s- (Qu(rarthmy ) Methane2,4-Oidiloropheool1 ,2,4-TrichlcrDbsttentIbphUula*4-Chltroaralinetoachlorciwtsdimt4-Oilcrcr3-«thylpnenal2-fethYlnaptithalattteadU trocycl opoitadi aw^4,6-Trichlorophaul2 , 4 ,5-Trichlxcpnenol2-Chlar(naphthalent2HtitnunilintDiKthvl phthalateAcEnapthvlB*3-Hitroanilirv

- 770 U770 U770 U770 U770 U770 U

. 7 7 0 U770 U770 U770 U770 U770U770 U770U770 U770U3700 U770 U770 U770 U770 U770U770 U770 U770 U77011770 U3700 U770 U3700 U770 U770 113700 U

-o

) . F u n n e l E x t r a c t i o n : Y E S 'i t i n . L i q . - L i q . E x t . : YES <

83-32-951-2B-5100-02-7132-64-9m-14-2606-20-2B4-64-27005-72-386-73-7100-01-4534-52-184-30-4101-55-3119-74-187-84-505-01-6120-12-784-74-2204-44-0129-00-0B5-6B-791-94-156-55-3117-91-721B-OH117-94-0205-99-2207-OM50-32-fi193-39-553-70-3191-24-2

AceupbthB*

4-tttraphenolDibaaofxan2,4-Oiaitrotoliane2,6-Dinitrotolunfcrthyl phthalate4-Qutrpphenyl-phBiYl etherFltureM4-tttrwniline4t6-0i oi tro-2-fWiylphwolIhutnHDdiphsrylimnt (1)4-firacphenyl-pbenyl ithrwtauuxobenznPntadilcrQphenalnwanthrenttathracmeDi-rrbutyl phthalateRuoranttontPyrnButyHwzyl-pbthilate3,3'-DichI(rttetziiiiniBRnzD(i)antlratentbit- (2-Ethyltevl ) phthal ateOryfentOi-ff-octyl phthalateBenzolblfluorantheneBmzotkHlutrxrthnB«nzo(i)pynneIndm ( 1 , 2,3-d) pyrmDibetzota^hlaDthracneBBtza(Ai)prYlene

UigjiciÔJ(ci

770 U3700 U3700 U770 U770 U770U770 U770 U770 U3700 U3700 U770U770 U770U3700 U770 U770 U

^"-fflni770U770 U1500 U770 U300*"770 U770 U77011770 U770U770U770 U770U

(circle one)e one)

(l)-Cannat be separated froi diphenylaaine

FORM 1

Laboratory Name

Cas€ No -7TS7Sample Numb«r

Concentration f-°y^ Medium

Date Extracted'Prepared fe -10-

Date Analyzed ______^>" ^ b"T7

Conc/Dil Factor ______!_______


Pesticide/PCBs


_____ Separately Funnel Extraction DYes

_____ Continuous Liquid - Liquid Extractron DYes

On

Percent Woisture (decanted}

CASNumber

ug/lor(CircU One)

319-84-6319-85-7319-86-858- 89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha -BHCBeia-BHCDelta -BHCGamma-flHC {LirvJanelHeptachlorAfdnn

Heptachlof EpoxtdeEndosulfan 1Dieldrin

4, 4'-DDEEndrmEndosutfan N4. 4'-DDDEr*dosulfan Sutfate4, 4'-ODTMethorycMorEodrrn KeioneChlordaneToupheneAroclor-lO16A/oclor-1221Afoclor-1232Aroclor-1242AroclcK-1248Aroclor-1254Aroclor-1260

It UIt U

Ih U.It, UL

ft U.it UIt UIt U3z-u~3i 1C7i IA7i U.?z u.^2 U?2 U./ f e o UJ? U.Ifco U-Jzâ*ô ll\lv Uibo a1'sc U-\bc U?ZV U.52.0 fx

CDCO

V( a Volume of ectraci m|ected (ul)

V - Volume of water extracted (ml]

W - Weight of sample extracted (gj

V. * Volume of total extract (ul)

orW.

Form 1 7/85

K yr^-w.**- -r rv*


CAS

T_.

I..

U *

ti

Tantativoly Idantifiod Compounds

v^b cm

in

_iS_L

11-1

- /- °l

lioo(wg/l oc

iiSCTD 3320 3

500-3

morn

o<sn".

cc

P»«l 0 7 85

Grganics Analysis Data Sheet(Page 1)

Simple Nunber: EL 262

Laboratory Na*e: ENVIRODYNELab Saiiple ID No: 87002776Sample Matrix: SOILData Release Authorized By:

Case No: 7351QC Report No: /3.Q.Contract No: _I__lp_iDate Sample Received:

Volatile Compounds

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-11-87Conc/Dil Factor: 1Percent Moisture (not decanted)i 14.5

X)mom-<mocr>m-o

CJO00

CASto: uqkg CAStot

74-87-374-63-975-01-475-00-375-09-247-64-175-15-075-35-475-34-3lSr*0-547-66-3107HJ6-2Tfl- 371-55-656-23-5108-05-475-27-4

Chlor MethaneBraoKthancVinyl ChlorideChl oroethaneHethylene ChlorideAcetoneCarbon Bisulfide1,1-Oichloroethenel,HKchlaroethanetrans-1 ,2-DichloroetheneChlxofori1,2-Di chl (methane2-Butanone1,1,1-TridtloraethaneCarbon TrtradilorideVinyl AcetateBr Modi chl oroiethane

12 U12 U12 U12 U46 B

• 190 B61)6 U6 U6 U6 U6 U12 U6U61)12 U6U

78-87-510061-02-67W1-4124-48-179-00-571-O-210061-01-5110-75-fl75-25-2108-1H571-7B-*127-18-479-34-5108-flB-3106-90-7100-41-4100-42-5

1,2-Dichlaraprapanftrars-1 ,3-Oichlaraprop**TrichlorottheneDifaroachl araethane1,1,2-TrichtoroethaneBnzncii-l,3-0ichlaropro(«w2-Oil oroethyl vi nyl etherBroiofari4-Hetiryl-2-pentanane2- xanamTrtrachloraithmla^^TetracUxDFthmToluemDilarabenzeneEthylbBQBwStyrewTaUl Ivlen«

b U6 U6 UA U6 U6 U6 U12 U6 U12 U12 U6 U6 U6U4 U6 U6U6 U

••*• ttavartlnt

U IB^.

t«»i ltMt.> tit*

«a«wttw HMt «w **• MB*!*.

*•

OWi— • «!•«• •*« «•*•!»*

. 14 tMMM, th

t* prvtvly tf^ltw

»• fully

Labor at or y Name:Case No: 7351

ENVIRQDVNE Saiole Number: EL 2b2


;OO

1

Concentration: LOWDate Extracted/Prepared: 6-10-87Date Analyzed: 6-13-B7Conc/Dil Factor: 1Percent Moisture (decanted)

Sen volatile Compounds

6PC Cleanup : YES

M.

CftSto: uotg

106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-32-9106-44-562-64-767-72-196- 5-378-59-188-TH105-67-965-85-0111-91-1120-63-2120-8H91-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-58-78B-74-4131-11-3*v*a fti nfJQ TO 0

99-09-2

Phenolbi5-(2-(Jairoethynett«r2-Oilornphenoll,3-OichJ(rttouenB1 , 4-Oi dil orobenzentBmzyl Alcohol1,2-Uichlorcterupw2HtothyIpheralbi s- (2-Chlaroi sflprapyl ) ether4-ftothylphanl(Hiitroso-ft-n-propyluinfteadUaraethaMNitrabenzeneInphorone2-Utrophenol2,4-DiMthylphenalBnzoic Acidbi s- (OU roethaty) Methane2,4-Oidilorophenol1 , 2 , 4-Tri chl ontenz meMitfithalene4-OtlxoanilineHBtachlorobutadiene4-QtI oro-3-«thy 1 phmol2-HetiiylrufhthaleneHex achl (rood op&itadiene2*4t6~TrichIxojrftfnol2,4,5-Tridilorqinenol2-Chloronaptithalenf2HtitnunilineDiwthyl ph thai ateAcmapthylene3-Mitroafliline

770 U770U770 U770 U770U770 U

.770U770U770 U770 U770 U770U770 U770U770 U770 U3700 U770 U770 U770 U770 U770U770 U770 U770 U770U770 U3700 U770 U3700 U770 U770 U3700 U

i. Funnel Ex t rac t i on : YES iitin. Liq.-Liq. Ex t . : YES (

CM KB

83-32-951-28-5100-02-7132-64 J?121-14-2606-20-2B4-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7210-OH117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2

Acmaphthene2,4-Dinitrq)henal4-tttroptauIDibenzofxai2,4-ttnitrotoluaw2,6-DifutrataluBwKetiiyl phthalate4-QUxopnenyl-phenyl etfwFluor CM4Htitn«fuhne4,6-ft ni tnr2-fcthyl phenolIHutnscdiphotylaum (1)4-firMQpbBiyl-jihenyl ethertfaadilonteizenePntjdtlarcphaolnMNntlvEntAnttracen*Di-n-butyl phthalat* (RuoraatbcncPyrentButyl-bmiyl-phthalatt3,3'-DidUcntoizidi(«BenzofaJaotbricentbis-12-EthylteyI)phthalatiChryieuDi-n-xtvl phthalateBBizo(b)fluorintheneteuotkHluxanttaiBBzo(a)pyreuIndm(l,2.3-ol)pvrBWDibnzD£a,h)anthracB»Bauo(Qhi)pryle«

3JfiJ(circle one)NO )( c i r c l e one t

ugkg

770 U3700 U3700 U770 U770 U770 U770 U770 U770 U3700 U3700 U770 U770U770U3700 U77011

' l O o o N^-flfr-tt^

770 U770 U1500 U770 Uao-w u^ p^^770 U770 U770 U770U770 U770 U770 U770 U

<1)-Cannot be separated froa diphenyla«ine

FORM 1

Laboratory Name

Cas« NoSample Number

Concentration f*°y/ Medium

Date Extracted "Prepared P*"i'

Date Analyzed ____I—f o ~W

Conc/Dil Factor ____1_______


Pesticide/PCBs(Circle One) GPC CleanupJQfes QNo

j_7_______ Separatory Funnel Extraction QYes

_________ Continuous Liquid - Liquid Extraction OYes


CAS ug/lorug^KgNumb«r (Circle One)

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494.70-557-74.98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5

Alpha-BHCBeta-BHCDelia -BHCGamma-BHC (LindanelHepiachlor

Aldrm

Heptachlor EpoxideEndosutfan tDtekJnn4. 4^DOEEndnn

EndosuHan It

4. 4'-DOD

EndosuHan SuHate4. 4*-ODT

MethorycnlofEndrin Ketone

ChlordaoeToxaphen«Aroclor-1016AroclOf-1221

Aroclor-1232

Aroclor-1242

Arocior-1248

Aroclor-1254

AfOClor-1260

/6 Ut& U

/fc U

fb aU U,fb K_

It UIfc U31- U-31 a7i (A?2. U.?2- U_32 U-3"! (X.Ibo U31 U.Ito U?2*? It

*fco alie? U.)ba ylIbC1 (X\t*j U32-1? K.

52_o LC

V( * Volume of extract injected (ul)

V$ = Volume of watef extracied (ml)

W = Weight of sample extracted (0)


or W. 30

morn-cmaCOm-o

CO

, 600

Form 1 7/85

NO

Organics Analysis Data Sheet(Page 4}

T«n(aiiv«ly Identified Compounds

70

0..

3.:

drsga.rbon

jdyt>on.rhoo* h «» _ * j -_mda

n.o

r*. I.&>>?-

. -7^3-6

Camc+ntrt t too

7 85

Qrganics Analysis Data Sheet(Page 1) ! —

Sample Number: EL 263 rT\|

Laboratory Nane: ENVIRQDYNELab Sa-ple ID No: 8700277?Saaplt Matrix: SOILData Release Authorized By:

Case No: 7351OC Report No:Contract No: ___U. _-_01;_"lp_ .Date Saaple Received: J^^.^-^.

Volatile Compounds


CAS to: WSta

74-87-374-fiH75-01-475-00-375-09-247-64-175-15-075-35-475-34-3156-60-547-66-3107-06-278-43-371-S-656-Z3-5108-05-475-27-4

CM or MethaneBrtmethaneVinyl ChlorideChloroethanenpthylen* ttlxideAcetmeCarbon Disulfide1,1-DichlxQethene1,1-Oi chloroethanetrans-l,2-DidilxaetheneOil or W or i1,2-OichlxDethane2-flutancw1,1,1-TrichlorocthaneCarbon TetracMorideVinyl AcetateBr nod i chl oroiethane

111t

6i&6i61iiI6

2 U2 U2 U2 U18 9 t/3*77 f U3-

6U ?"UUuuu

2 UUU

2 UU

78-87-510061-02-A79-01-6124-48-179-00-571-4>2

**" 10061-01-5110-75-875-25-210&-10-1591-7B-6127-18-479-34-5106-88-3108-90-7100-41-4100-42-5

l,2-Did)laraprop*wtram-1 ,3-Oichl(raprQpeneTndilxoetheneDi bronchi onaethane1,1,2-TrichlxoethaMBenzeneci s-1 , 3-fii chlxopr opent2-Chl xoethyl vinyl etherBrovrfxi (HWiyl-2-penUxre2-HexanawTetracKIaraethene i1,1,2,2-Tetradaxatthwe (Toluene iChlorobnzene <Ethylbenzene tStyrm tToUl lylns i

UUUUUUU

2 UU

.2 U2 U

U» U> U

UUUU

w HMt f«r U f««,

fully

ill !• !••• UMN t

. 1OJ). t* Ilirtt

•**!•• HMt

1O 1*1 an«

Labor at ory Name:Case No: 7351

ENVIRODYNE Sa«nle Nunber: EL 263

Organics Analysis Data SheetiPaoe 2) or-

Concentration: LOWDate Extracted/Prepared: 6-10-B7Date Analyzed: 6-14-87Conc/Dil Factor: 1Percent Moisture (decanted) 15

CAS

Seat volatile Compounds

GPC Cleanup : YES,cc.

uqkq

106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-3M106-44-5621-64-767-72-19B-95-378-59-18B-7H105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-5U-791-57-677-47-488-06-295-95-491-5B-788-74^131-11-3£K TU tJ99-09-2

Phenolfais-(2-Qilxaethyl)ethB-2-0)1 trapheool1,3-Oichltnbenzene1,4-OidilaroberuentBenzyl Alcoholl,2-&idil(TDb«nien*2-fethylphcnolbis-(2-ChlormscprQpyl}ether4-HethylphenoiK-ni troso-Oi -fr-prnpyl ati neHetachltraethamNitrobenzeneIsophcront2-ntropMnol2 * 4Hh tethy 1 phenolBenzene Acidbi 5- (Oil troethray ) frthane2,4-DidUcropnenol1,2,4-TricnlorobenzEneNaphthalene4-QUtroanihr«teach iTobutadiene4-QUxo-3-tethylphenol2-Hrthylnaphthalencteachl orocycl opentadi ene2,4,6-Trichlxaphenol2,4,5-Tridilorophend2-Chl xarupnthal ene2-WtroanilineDiecthvi phthalateAtvupthylene3-Hib-Qiniline

790 U780U790 U780 U780 U780 U

- 780 U790 U780 U790 U790 U790 U790 U790 U790 U790 U3900 U780 U790 U790 U7BOU780 U790 U780 U790 U790 U7801)3800 U790 U3800 U780 U790 U3BOOU

j. Funnel Ex t rac t i on : YES (itin. Liq.-Liq. Ex t . : YES 7

CASfc:

B3-32-951-28-5100-02-7132-6W121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-311B-74-187-86-5B5-OH120-12-784-74-2206-44-0129HXH)B5-6B-791- -156-5-3117-81-7218-01-9117-64-0205-99-2207-48^50-32-6193-39-553-70-3191-24-2

Acenaphthene2,4-Dinitra?nenal4-tttrophenoiDibenzofiran2,4-Oinitrotoluen*2,HhnitrotolueneDi ethyl phthalatf4-Qilxqpnenyl-phenyl etherFluorenf4-)titroanUint4,6-Dinitro-2-fctJ>yl phenolN-nitroaxtipheiylMir* (1)4-BroBflpbenyI-ptanyl etherteadilorobenzenePtotacfalxopnenolRienanthreneAnthraceneDi-ft-butyl phthalaUFluoranthenePyrentfiutyl-twcyl-ptititalite3,3 ' -Di chl tntonidineBenzo (a) anthracenebi i- (2-EthyI hayl ) phthal ateChryseMDi-n-xtyl phthalateDBUOtu/filfirjPuW

DBHZD ' KJ T lU iVIUW

Benzol a) pyreneIndeno(l,2,3-crf)pyraKfiibenzo (a,h) anthraceneBBnzotghilpa-ylme

NO")ICI

itflkq

7BOU3800 U3BOOU780 U7BOU790 U790 U790 U780 U3800 U3800 U790 U780 U790 U3900 U790 U

r S/ 650J 'U7anrj790 U790 U1600 U790 U240 W780U790 U790 U790 U780 U780U790 U780 U

one)one i

( l ) -Cannot be separated irom diphenylai ine

FORM 1

Laboratory Name

Case NoSample Number

-2

Concentration


Date Analyzed ______

Conc/Dil Factor ____


Pesticide/PCBsMedium (Circle One) GPC Cleanup^Yes DNo

D " JO""T7_________ Separator Funnel Extraction DYes

' "' o ° >___________ Continuous Liquid - Liquid Extraction DYes

o

oc/>m


CAS wg/( or U<K KgNumber (CtrcU Olrvef

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-O7-850-29-372-43-553494-70-557-74-98001-35-212674-11-2111O4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha-BHCBeta-BHCOelia-BHCGamma-BHC (UndarwJHepiachiorAldnn

Heptachior EpoxideEndosulfan 1

Dieldrin

4. 4--DDEEndrmEndosuHan II

4.4<-DOOEndosulfan Sutfate4. 4--DDT

MethoKyChlor

Endrin KetoneChterdaneTo*apn«neAroclor-1016

Aroclof-1221

A/oclot-1232

Aroclor-1242

Aroclor-1248Aroclor-1254

Aroclor-1260

/6U

Ifr U

\i- U.Ifo U-It U.fb K.It UIt U32- U-31. (L72. (A7iU,

3-ZU.32 U.

• 3z U.Ifco U7^ U.Ifea UJzo U,

' fco \LUj U.Ibs U':•? U»ix7 U

32.0 u.52.0 u

orW.

V( = Volume of extract injected (ul|

V = Volume of water extracted (ml)

W - Weight of sample extracted (g)


_ v -ZO, 400

COCO

Form 1 7/85

00

•J

33

^b

^

[Ao

rp^

0>

?u:

t?

tr

OPO

tro

3

x

V

"

p-

c? o

1O

o

3

\

£.-0

3fa

(P*NLJ>I

a-r>-a-3

oMb

r

!«m

0

-

I *

3

R'>

cU


Staple Number: EL 264

Laboratory Naae: ENVIRQDVNELab Saiple ID No: 87002780Saaple Matrix: SOILData Release Authorized By: Jfl_CU)_

Case No: 7351QC Report No:Contract No:Date Sa»ple Received:

CftSMK

Volatile Compounds

Concentration; LOWDate Extracted/Prepared:Date Analyzed: 6-12-87Conc/Dil Factor: 1Percent Moisture (not decanted)

CflS

15.3

74-87-374-5S-975-01-475HJO-375-09-267-64-175-15-075-35-475-34-3154-60-567-66-3107-06-27B-93-371-55-656-23-5108-05-475-27-4

DU or MethanefrmethancVinyl Oil TideQUoncthanefethyleM QilxidtfcitiMCarbon Bisulfidel.Hhchlaraethene1,1-Oidiloroethanetrans-1 ,2-DichlcroEthawQUarofaril,2Hhchlarcethane2-fiutanone1,1,1-TrichIirDethjneCarbon TetradilohdtVinyl fceUttBrModidil or Methane

12 U12 U12 U12 U17 B57*4

' 6U61)6 U6116 U6 U12 U6 U6 U12 U611

78-57-510061-02-679-01-6124-48-179-00-5

0- 71-43-2KT*- 10061-01-5

110-75-875-25-2108-10-1591-78-6127-18-*79-34-510HB-3108-90-710MH100-42-5

l,2H)idilirqn|H»trani-1 ,3-DirfdtnpropeneTridtloroethneDi bronchi oroKthane1,1,2-Tridil methaneBnzncis- 1 ,3-fc ddtrqropwe2-ChloTjethylvinyletMrBrovfori4-ftrthyl-2-penUa»2-HBaKMTvtrachlu uethcv1,1,2, 2-Tetrxfal iroRhantToiuemCblorobenzBieEtfaylbeue»StyreneTotal Xyloe

6 UUUUUUU

12U61112U12 U6116 U6 U6 U6 U6 U611

orn<moCOm

CO

COoo

tvi Holt f«r tlwt

t». t* MBri,

Ui* r>.ult

L a b o r a t o r y Naee:Case Noi 7351

ENVIRODYNE

3A

Saeo 1 e Number : EL 2


VX3

Seaivolat i le Coepounds

Concentrat ion: LOWDate Ex t rac ted /P repa red : 6-10-87Date A n a l y z e d : 6-14-87C o n c / D i 1 Factor : 1Percent Moisture (decan ted) 15.8

CAS to uqkg

108-45-2111-44-495-57-fl541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5421-64-747-72-198 95" 37B-59-189-75-5105 7-945-fl5-0111-91-1120-83-2120-BH91-20-3106-47-flB7-68-359-50-791-57-677-47-4ae-06-295-95-491-58-7BB-7M131-11-3tffi m n43JQ TffTl

99-09-2

Phetolbifi* i2*lJxIorTEuiYl J ffuvr2*ut 1 or opncooi1,3-DichlirtbenzBnt1,4-th til (Tobmz meBnzyl Alcdfill,2-0ichlxab*ramt2-fVthylptodb i s- (2-£hl xw sopr cpyl ) rther4-ttethylphenolH-ni tr oio-Oi-ft-propyl ui rwHecachlcrathantMtrobcozntIfophorm2-tttraphaol2,4-ftMthylptaralBvzoic Aciibii- WW (TtKthaty) fcthant^4-Dichlaroiitwnol1,2,4-TrichltrtteumiIbphthalm4-Oilfroanilini(fexachlorooutadiBtt4-Ovloro-3-«ethyl phaiol2-fMhvluphthaleMteadilcrcydcxHitadiene2, 4,6-Tr i cbl wcohewl2,4,5-Tndaarchenal2-Qil xonaphthalene2-*traaniliniDivtbyl phthalatttawpthylon3-Mitroanilint

790 U780 U790 U780 U790 U790 U

. 790 U790 U780 U780 U790 U780 U790 U780 U790 U780 U3BOOU790 U790 U780 U780 U780U7BOU780 U780 U790 U780 U3800 U790 U3800 U780 U7BOU3800 U

i. Funnel E x t r a c t i o n i YES Citin. Liq.-Liq. E x t . : YES

CASte

83-32-951-29-5100-02-7132-64-9121-14-2406-20-284-66-27005-72-386-73-7100-01-6534-52-184-30-6101-55-3118-74-1E7-66-S85-01-6120- 12-784-74-2206-44-0129-00-0B5-68-791-94-156-55-3

218-01-9117-84-0205-99-2207-08-950-32-6193-39-553-70-3191-24-2

fcnapiittwnt2,4-Qinitraphcnol4-ttitrophnolDibmofuran2,4-Dinitrotnlueni2t6-0initn)toljentDirtfayl pbthalatf4-CilxcphHiyl-phBTyl eti*rFluormt4-ttitnianiIint4, 4-fc nitnr2HWiy 1 pboolN-iutnaodiptKTtylaiinf (1)« *----- i —— i ,L, . 1 -11--BroapMnyi -poea y i KMrnBâcVu GrtD0&Enir^Btt ACnl QTCDItenOl

PtananthrnfcrthracHJtDi-n-butyl phthalatfFluor an tbmPyrmBKtyl-bnzyl-ptttbalate3,3 ' -ffi chl or [tec idineBHUO (a) anthracene

OrysawDi-fr-ortyl phthalatcBeuo(tt)fluDranthcntBnofkHlurvithnBnzo(a)pyre)iInderoU,2,3-td)pYrH»K beoz D (a> ) anthr acawhrao(ctii)OTlent

. N _ 0 2 < c i r c l e one)&\j ^ c i r c l e one j

uqtg

790 U3300 U3800 U790 U790 U780 U780 U790 U790 U3800 U3BOOU790 U790 U790 U3800 U790 U780 U2400790 U780 U780 U1600 U780 U

780U790 U7»U790 U790 U780 U790 U790 U

(1)-Cannot be separated Iron diphenylaaine

: --- FORM 1

Namt

Case No -73*7


Sample Numt>«r

Concentration <tow? Medium

Date Extracted'Prepared *r~ T

Date Analyzed ._______ll^

Conc/Dil Factor ________

Pesticide/PCBs

(Circle One) GPC Cleanup^Yes DNof~i2_i________ Separatory Funnel Extraction QYes


\Percent Moisture (decanted)

CAS ug/1 or ugQ'KgNumber (Orel* Oo«]

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5

Atpha-BHCBeia-BHCDeita-BHCGamma-BHC (Lmdanel

HeptachtorAldnn

Heptachkw EpoxtdeEndosulfan 1Die'dnn4. 4--ODEEndrmEndosutfan 114. 4'-ODDErvdosulfan SuHate4. 4'-DDTMethOKychltxEndrm KeioneChlordaneToxapheneA/oclor-1016Aroclor-1221Aroclor-1232

Aroclor-1242

Arociof-1248AroCtor-1254

AroctOr-1260

ft UIfc Uft aifc ait u.>b ULIt UIb U

32- V~31 a7i tA7i U.^z u.52 U-?Z (X.ibo aJ7 U.IfeB U-

?zo U,^9 f,Ct f i j U.1fe3 U

It? IXIfetf u310 u.

52.0 U

orW.

V( = Volume of enraci injected (ul)

V = Volume of water enracied (ml)

W = Weight of tample enraaed (g)


_ v 1 &, 6 0

Form 1 7/85

OrganJcs Analysis Data Sheet(Page 4)


CAS

^Lfi. .3B.

iL3.

Moo 3

,S..

18.,

>«

23. _

? as


Simple Nuaber: EL 263\

Laboratory Na«e: ENVIRODYNELab Sample ID No: 67002781Sa.plt Matrix: SOILData Release Authorized By: ]V\£Uj_

Case No: 7351QC Report No:Contract No: __b^rCU_-JDCL*i_"^____,_..^1^2.Date Saaple Received: _U_-_4rXrL

Volatile Coapoundt

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-12-B7Conc/Dil Factor: 1Percent Moisture (not decanted): 14.B

CM tew CKfe

74-B7-374-C-975-01-475-00-375-09-267-M-l75-15-075-35-475-34-3156-60-567-66-3107-06-27B-93-37I-B-656-23-5tOB-05-475-27-4

aioroiethaMBrathawVinyl ChlorideEMoropthjneNethYlcnt ChlcrideACBtETCCartaon Wsulfidt1,1-DidUxoethene1,1-Oichlcroethanttran5-l,2-0ichlcmethenettitrcrfxi1,2-Oichliraethani'2-fiut.ncTCl,l,Mrichlcneth.mCarbon TetradiloridtVinyl AdtatiBroealichl oroeethaw

12 U12 U12 U12 U2 9 &190

UElUUUU

[2Uk U> u12U> U

78-87-510061-02-679-01-6124-W-l79-00-571-43-210061-01-5110-75-675-25-2108-10-1571-78-6127-18-479-34-5108-9-3108-W-7100-41-4100-42-5

1,2-Didilcropropanttrans-1 ,3-DidilarapropsitTrichlaroetbencDi braeadU onwthane1,1,2-TricUoraethaneBenzBiedi-l,3-&ichltrDprapBW2H3d(raethyl vinyl etherBraeofort4-fcthyl-2-pent*«ne2-4tsanaMTetrachltroethene1,1,2,2-Tetr .riil methaneTolueneQtlorobeniBWEUiYlbmzmStyrswTotal lylnn

6 U6 U6 U6 U6 U6 U6 U12 U6 U12 U12 U6U6 U1«

61)6U6116 U

•> TM* «!•« •**!!•• t»

••/•I

1M* «!•« 1*

». It K

riiBaltB. 1< «••*. tMnr «Mt

•rlMtM MtacM^ t» tJM M*i

(••). 1**]. If Halt

L a b o r a t o r y Na«e:Case No: 7351


Nuiber: E&265^——— _ „ _ , - , _ _ _ _ _

Seaivo la t i le Compounds

Concentration: IONDate Extracted/Prepared: 6-10-87Date Analyzed: 6-14-87Conc/Di1 Factor: 1Percent Moisture (decanted): 14.8

CAS No: uqkq

100-95-2 Phenol111-44-4 bit-(2-QilaT»thyl)ether95-57-8 2-aiorophenol541-73-1 1,3-OidiloTiefuw106-46-7 1.4Hhchlorob«uen«100-51-4 Bvcyl Alcoxl95-50-1 l,MHdJloro6Bnzew95-48-7 2-tethylphenol39438-32-9 bis-(2-Oil£roi5a?ropyl)rth«r106-44-5 4-tethylphenol421-64-7 lhiitro5oH)i-iri)rapyIiiiM47-7M faachlororthane98-95-3 Mitrcbenzem78-59-1 Ifflphoront88-75-5 2-tob-cpMrwl105-47-9 2,4-DiMthylphBul45-85-0 Benzdc Acitl111-91-1 bi«-«Mtrt»ttey)hrth«12CKffi-2 2,4-Oidilarcphenol120-82-1 1,2,4-Trichlorobmzefle91-20-3 Miphthilne10M7-8 4-OU(roanilint87-68-3 tetdilarofettadirnt59-50-7 4-Qatrcr3- hylphenol91-57-4 2-fethylMpfiUuient77-47-4 HBachlcrocydopentadienc88-06-2 2,4,6-Trichlflrophenol95-95-4 2,4,5-Tridil(rn>nenDl91-58-7 2-ChloraaphthalewBB-74-4 2-tttroanilint131-11-3 Kiethyl pbthalatc208-96-8 Aonapthylem99-09-2 3-tetroaoilin»

770 U770 U770 U770U770U770 U

. 770 U770 U770 U770 U770 U770 U770 U770 U770U770 U3BOOU770U770 U770 U770 U770 U770U770 U770 U770 U770 U3BOOU770 U3800 U770 U770U3800 U

6PC Cleanup : YESSep. Funnel Ext ract ion : YESContin.

Ofi to:

83-32-951-28-5100-02-7132-44-9121-14-2406-20-284-64-27005-72-386-73-7100-01-4534-52-186-30-4101-55-3HB-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-48-791-94-154-55-3117-81-7216-01-9117-84-0205-99-2207-08-950-32-8193-39-553-70-3191-24-2

Liq.-Liq. Ext. : VES

Acmapttthnt2,4-thrutnphenQl4HfttroptolDitwzohran2,4-ftnitnjtoluent2,6-ferutrotaluBWferthyl ptttaUtt4-Oil(roptayl-ptwnYl fttarFluareM4-ltitniaiulini4,6-0iwtTD-2-ni*hylphiriolK-nitrondiphBnylaiiv U)4- roBpfcarl-ptartyi ethrteach! trotes emPtttadtlorqteiolPhaunthrnAntbracnDi-rHwtvl ptthalatcFluor aithmPyrmBotrt-beKyi-pdthalat*3, 3 '-ft chl oniBniiiintBno(i)aatfracBWbii-<2-Ettiyltevl)phthalat*OrysHwDi-n-actyl phttttlat*BenzolblfluaraithenehnzQfttflurvttnewBBno(alpyrn»IndenoU,2,3-cri)pyrer*K iMnzo (a,h) anthr actntBcnzolaMJpa-ylvN

G3D<cir(^Qicir

«rfl

770 UTBVI IIJWJ U

3800 U770 U770 U770U770 U770U770 U3BOOU380CU770U770 U770U3800 U770U

îooj^

770 U770 U1500 U770 U320-£</J-770 U770 U770 U770U770 U770U770 U770 U

one*

= = SSS = S=SZSK=S»3BEX = S 3 X X X = «>

(l)-Cannot be separated fro« dipnenylaaine

FORM i :.rrf"

Latxnaiory Name

Case No ' -*


Sample Number

Concentration £°w.) Medium

Date Extracted'Prepared b "ll

b i , vw».,...._.,*— ________"'o 8

Cone/Oil Factor: ______I_____

\Pesticide /PCBs


1LZ________ Separatory Funnel Extraction DYes

_________ Continuous Uquid - Liquid Extraction DYes


CAS ug/loruovKgNumber (Circta One)

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111096-82-5

Alpha -BHCBeta -BHCDelia -BHCGamma-BHC (LindanelHeptachiorAidnnHeptachlor EpoxideEndosutfan 1Otetdnn4. 4'-ODEEndnnEndosuffan II4.4'-DDDEndosutfan Sutfate4. 4'-DDTMethoxyctilorErtdrin KetooeChlordaneToxapneneAroclor-1016

Aroclof-t221

Aroclor-1232

Aroctor-1242

AroclOf-1248Arocfor-1254

ArocIor-1260

/fa Uh U!h U.ife ait U.'b (XIt, (4u u3z- u-32.0.7i UJiU.?2. U.32 LL71 U.tbo U7z u.|{-D \J_3zv\L1fc0 |,L

Uo UIfe? U'iC1 IX\te UT2-0 l^-52.n (^

orW,

V( s Volume of extract injected (u)|

V s Volume of water extracted (ml)

W = Wetjjht of sample extracted (g)

V( * Volume of total extract (ul)

3o<\ v lo.aoo

form 1 7/85

No* Organics; Analysis Data Sheet(Page 4)

Tentatively Identified Compounds '%CAS

Cooc •*!< f • t

3B2.

3..

S..

7..6..

10..

14..

15..

16..

17..

18..

19..

21..

3i$- "S303J3

27..

28..

3O..

form 1 Pan 8 ? 8S

Organic* Analysis Data(Page 1)

Sheet

1 S aaple Nuaber: EL

Laboratory Naie: ENVIRQDYNELab Saaple ID No: 67002782Saaple Matrix: SOILData Release Authorized By:

/3Case No: 735LQC Report No:Contract No:Date Saiple Received: __U_-_.y_-_V7

Volatile Compounds

Concentration: LDUDate Extracted/Prepared:Date Analyzed: 6-12-87Conc/Di1 Factor: 5Percent Moisture (not decanted) 15.4

A

CASNo; uqkg

74-B7-374-85-175-01-475-00-375-09-267-64-175-15-*75-35-475-34-315WO-567-66-3107-06-27W3-371-95-656-23-5IOBHJ5-4T5-27-*

QltrarthanfbmwthaniVinyl QilorideQiloroethwfMfaylm GhlxideAcetateCarbon ftiuHidc1,1-Oidil trothe*l,Hhthloroethanetrans-1 ,2-Oichl(roethBiettlffoftril.HndUxMthw2-ftitancml,l,Hrichloroeth»Carbm TrtradtLiridtVinyl ftotatflBrnodi chl or owtiunc

39 U59U59 U591)

1708. TOB

30 U30 U30 U30 U30 U30 U59 U30 USOU59 U30 U

7W7-5100il-02-i79-01-*124-W-l79-00-571-43-210041-01-5110-75-875-25-2106-10-1591-78-61Z7-1M79-34-5ioe-w-3108- 71«HH10M2-5

1,2-DichIcn^rDpanetrans-1 ,3-Di chl cropropeneTridilaroetheMDibraBchlarnethnl,l,HridilB-MthaneBmiffccif-1 T3-Oidil orqrDpene2-OJ oroethyl nnyl etherBronfcrt4-Mhyl-2-pmtaroic2-te«r»Tftradtlorathml,lA2-Tttr«tl(rMttwToljsieQvlorobenincEthvlbnznStyrwiToUl lylmes

301)30 U30 U30 U30 U30U30 U59U30 U59U59 U30 U30 J30 U301)30 U30 U30U

rwultk. t* MM, th»v •—« M fully

Laboratory Nane:Case No: 7351

ENVIRDDYNE Satple Nuaher: EL 2oc

Organic* Analysis Data Sheetipage 2)


Concentration: LOWDateDateConc/Di1Percent

x t r a c t e d / P r e p a r e d : 6-10-87n a l y z e d : 6-U-B7il Factor: 1t H o i s t u r e ( d e c a n t e d ) : 15. A

06 to:

108-95-2 Phenol111-44-4 bii-lHSilorwUwl) ether95-57-fl 2-Qil(rDpheoQl541-73-1 l,3-0idd(rtteuene106-46-7 1,4-fcdilircfcnzenf100-51-6 Benzyl Motel95-50-1 l,2-&id>larobenze«95-AB-7 2-ttthylphwol39638-32-9 bis-(2-ChIoroiscorDfiyl>ether106-44-5 4-tethylpt*cl621-64-7 IKitroaHh-ftTr^latiM

98-95-3 totrabwzene78 5r 1 . liophoroncBB-75-5 2-fttropherwl105-67-9 2,4-ttwthylptaal65-85-0 Benzoic Acid111-91-1 bii-tDiltrathiMyUkthm120-fl3-2 2,4Hhthlarcctenal120-82-1 1 ,2,4-Trid\l(rabenzB«91-20-3 tephtbilene106-47H3 4-{Morowilinf87-68-3 teachlircbutadiene59-50-7 4-tWcrtr3-«thyl phenol91-57-6 2-ftethYlMphthalene77-47-4 tearfUcnrydnsntaihent88-06-2 2,4,6-Trichlorcptwnol95 75-4 2,4,5-TridUtro()hi«il91 -5B-7 2-aicrcr*hUnlMBfi-74-4 2-fctro*iilir»131-11-3 Diwthyl phthalate208 96 '8 AceMpthyleni99-09-2 HbtruniliM

uqkq

7801)7BOU780 U7801)790 U780 U780 U790 U780U780U790 U^ 11Tot) U780 U780 U780 U780113BOOU7801)790 U790 U7901)780 U780 U780U780 U780 U780U3800 U780 U38001)780 U780 U3800 U

Sep. F u n nC o n t i n . L

OS to:

83-32-51-28-5100-0 7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6

. 534-52-1

101-55-3118-7HE7-66-585-01-8120-12-764-74-2206-44H)129H30-0B5-6B-791-94-156-55-3117-W-721B-OH117-W-O205-99-2207-08-950-32-8193-39-553-70-3191-24-2

el E x t r a c t i o n : YES(î q . - L i q . E x t . : YES (

Acauptithcne2,4-Oinitn^nenol4-fctrcDMnoiDibcnzofuran2,4-ftnitrotoluent2,6-OinitrDtalumDiethvl phtkaltte4-Qaorophenyl-phwyl etherRuoreM4-ttltnHnilinc4,6-fcnitnr2-ftthTlphenol

4* flro*Dpwjyi"pnwyl tuwHexhltnbenzemPent ich 1 on^MnolPticnxithrEniftothraceMto-n-butyl phthalat*Fluor mtheoePyrentBtttyl-tazvl -ptithal ate3,3'-OictJarabenzidineBenzoUlcthrKRiebis- Mhyl heiy 1 ) phthal iteDryswtDi-n-ortyl phthalatiBenzolbHluorvttteMBenzotkJfluranthencBenz o ( ii pyrernItvfro ( 1 1 2) j"Qi ) pyrweHi bfnzo U^) anthr xer»Bnzolghiiperylent

NAjlciSOci

qk,

780 U3800 U3800 U78011780 U790 U780U780 U790 U3800 U3800 U780 U790 U790 U3800 U79011ffiftu

£7470 J790 U790 U790U1600 U790 U650 Bf780 U790 U7BOU790 U780 U780U7BOU7BOU

(l)-Cannot be separated tram diphenylaaine

FORM 1

T\

ft03.one Ione )

Latx>raiory Name

Case No "


Sarnpla Numt>«r

^V-

<£>Concentration f°^ Medium

Date Exacted'Prepared k "

Date Analyzed _____K> ~i t^

Conc/Dil Factor: _______/

Pesticide/PCBsi

(Circle On«) GPC Cleanup^Yes DNo

'-SI______ Separator^ Funnel Extraction QYes

—————————— Continuous Liquid - Liquid Extraction DYes

Percent Moisture (decanted) is.CA5 ug/l of ugl/ KgNumber (CirefcOn*)

319-84-6319-85-7319-86-858-89-976-44-8309-OO-21024-57-3959-98-860-57-172-55-972-2O-833213-65-972-54-8

1031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-21HQ4.28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Alpha-BHCBeta-BHCDelu-BHCGamma-BHC (L<r\danetHepiacniorAldrin

Hepiachlor EpoxideEndosu'fan 1Dteldrm

4. 4--DDEEodrinEndosuMan If4.4'-DDOEndosuKan SuWate4. 4'-OOTMethoiychlorEndrin Ketone

ChlordaneToKjphen*Aroclor-1016

Aroctor-1221

Aroclor-1232Aroclor-1242

Aroc(0'-1248AroclOf-1254

Aroclor-1260

Ib UIt UIb U.?fo au utb KIt \4U UZz- w-32. LL7i (A7i U.^Z U.52 U31 U.f f c o UJ2 U.K:2 U

3l» \LU?5 l,t

lij U)t? a'i? IX\b<3 U

1^ U.

^2.o K

V( = Volume of ertraci injected (ul|

V * Volume of water extracted (ml)

Ws = Weight of sample ertracted (g)

V » VoJume of total extract (ul)

or W.

Form 1 7/85

E LOrganic! Analysis Data Sheet

(Page 4)

Tantativaly td«ntifi«d Compounds

CASN Number

(ug/(

I "PnspOLncuc, OQxi

12..13..

15..

17..

18..

19..

24..

27..

28..

30.,

1.01.06

I S - '

Ii •

^m.

to"

I. Pan B ? 8S

Laboratory Name:Case No: 7351

ENVIRODYNE Sane I e Nuaber : EL 2 6 7

J'-a•O

Organic* Analysis Data SheetiPage 2)

See ivo l a t i l e C o m p o u n d s

Concentration: LOWDate Extracted/Preparea: 6-10-87Date Analyzed: 6-14-87Conc/Dil Factor: 1Percent Moisture (decanted) 15.4

CASto: uctq

108-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-73963B-3W106-44-5621-64-767-72-198-95-378-59-18B-75-5105-67-965-85-0111-91-1120-83-2120-flM91-20-3106-47-887-68-359-50-791-57-677-47-4BB-06-295-95-491-58-788-74-4131-11-3208-96-899-09-2

Phenolbis-(2-Qacroethyl}etherHMcrocfwnoll,3-0ichlcni)enzeneU4-Oichl7d>enzB»Benzyl Mortal1,2-DichlGrobenzene2-flEthylphenolbis- (2-Qiloroi scprcpyl ) ether4-MhylphenolH-ni troso-Oi -trpr npy 1 m neHeKacMtroethaMNitrctouentla^hcrtm2-thtri h«ool2,4-OieethylpheralBenzene Acidbi s- (Oil tmethm y ) Hethane2,4-Dichlarophenol1,2,4-TrichlardwueneHaphttulene4-QUtroaniUnetteactil or abut aril ene4-Q\l aro-S-B-thyl phenol2-Hethylnaphthalenetoachl trocyd opentadi ene2,4,6-Trichlorophenol2,4,5-Trichltrophenol2-Qtl nronapnthal ene2-ttitroanilineDiwthyl pttthalateAcenapthylET*3-Mitroaniline

7BOU790 U790 U790 U780 U780 U

- 780 U790 U780 U790 U790 U790 U790 U790 U780 U790 U3800 U790 U790 U790 U780 U790 U7BOU730 U790 U780 U780 U3900 y780 U3BOOU780 U780113800 U

) . F u n n e li t i n . L i e

CA£ to:

83-32-951-2B-5100-02-7132-6M121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-48-791-94-156-55-3117-81-7218-01-9117-94-0205-99-2207H36-950-32-8193-39-553-70-3191-24-2

Ex t r ac t ion : YES <I . - L i q . E x t . : YES C

keniphthew2,4-tonitrophenol4-MitrcphenolDibsuriiran2,4-DUitrotoluene2,6-OirutrotoluBieDiethyl phthilate4-Chlxapnenyl-phenyl etherFlunrmt4-*traaniIine4,6-Oinitro-2-fcthylphwolH-mtnBotiphenylaiint (114* u'UKpMnyl-pnenyl etherItaxachl orcfaenz eniPentadilcrflptanolPhenanthrentfetiracawDi-n-fautyl phthalateFlvranthenePyrmButyl-benzYl-phtNalate3,3 ' -Di chl cntett i di neBenzo (a) anthracewbiK-(2-ethYlhoyl)phthalat»OryseneDi-n-octyl phthalaUBenzo<b)flutraothfncBeruolUflutr anthemBentotaJpyrewIntBtt(l,2,3-cd)pyrH»Dibenzod.h) anthraceneBenzo (ghi)perylene

^NOJ^c i r

7BOU3BOOU3800 U790 U790 U780 U790 U790 U790 U3800 LJ3SOOU790 U780U7BOU3800 D780U7BQJJ

[_7M i f/it IT*

-780UTfiOU1600 U780 Ueoor i7BOU790 U780U790 U790 U790 U790 U7BOU

(l)-Cannot be separated fro* diphenylaame

FORM 1

e one)s one)

Laboratory Name

Case No _ ——Numb«r

26-7-

Concentration f ^ Medium

Date Exiracted 'Prepared

Date Analyred ______ b-f

Conc/Dil Factor _____ !

Organics Analysis Data Sheet(Page 3) "o

Pesticide/PCBs -


2________ Separator^ Funnel Extraction QYes



CAS ug/lorug^K^Numb«r (CJrcV* Of>«)

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860 S7-172-55-972-20-833213-65-972-S4-8

1031-07-850 29-372-43-553494.70-557-74-98001-35-212674.11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Afpha-BHCBeia-BHCOUa-BHCGammj-BHC (UndJnelHejjiachlorAJdrm

Hemactiior EpoxKteEndosutfan 1DiekJnn

4. 4--DDEEndrmEndosulfan tl4. 4'-DDDEndosuMan Surtate4. 4'-ODTMethox>chlorEndnn Keion«ChiordaneToKjQt^neA/odtx-1O16Aroctof-1221

A/ociof-1232Aroclor-1242Aroc1(X-1248Aroctof-1254

Aroclor-1260

Ik U\b U

1h U.It, iJLit U.Ib U(It Uifc U.3Z-IA^2.L672. CA.71 U.^z u.52 U71 U./bo UJ^ U.Ifeo U-7ô U

»t?o \L\io U.lie? U

its' a^fco U3in K52. L<.

\

orW.

V- = Volume of extract in|*cted (ul|

V = Vofurne of water eitracted (ml)

W « Weight of umpte e«tr»aed (gt


Form 1 7/85

K/O-. Organios Analysis Oata Sheet(Page 4)

Tentatively Identified Cocnpouods

CAS

Ui n - on.

3.

3 - 2 Sac 3

ArpCart^n8. i-s-o

TV-opQAmV ac^J ;2-ii._

? es

ecology and environment, inc.111 WEST JACKSON BLVD., CHICAGO. ILLINOIS 60604, TEL. 312-663-9415


Date Received for Review _TO: -fcim Paehc ic^From: Zena Gold-KaufmanSubject: HOD

PAN: XUOI4

Sample Description ______Organics (VOA, ABN, Pest/PCB)

LowLow WaterDrinking Water

Other


Case t ?3bll



Project Data Status


Completed!

FIT Data Review Findings:

CAC&Smol

fcf,0

errcr

____\s Compounds were detected in sample(s); see enclosed ChemicalEvaluation Form.

Book No- ^ Page No.

t.1

V0A"

\

s

),

~~$6Q Ludf'f, . ' 'COMPOUND J

cMororicthanebromomclhsnev i n y l chloridechloroethanemethylene chlor ideacetonecarbon dlaulflde1,1-dlchloroethene1, 1-dichloroethan*trans-1,2,-dlchloroethenechloroform1,2-dlchloroethana2 -but a none1,1,1-trJchloroe thanecarbon te t rachlor ldevinyl acetatebrotnodlchloromethene1,1,2,2-tetrechloroethene1,2-dlchloropropanetrane-1, 3-dichloropropcnetrichloroethenedibromochlorome thane1,1, 2-tr lchloroethanebenzenecle-1,3-dlchloropropena2-chloroethylvlnylelherbromororn2-êxanone4-melhyl-2-pentenonetetrechloroethenetoluenecMorobenreneethylbenzeneatyrenetotal xyleneiH-nllrosodlBiethylemlnephenolanilineble(2-chloroethyl)ether2-chlorophenol1 ,3-<Jlchlorobenzene1 ,4-dichlorobenzervebenzyl alcohol1,2-dlcMorobenzene2-««thylphenolbla(2-chlorol8opropyl)ether4 -me thy 1 phenolN-nitroBO-di-n-propylsmlnenexacMoroethanenitrobenzeneJeophrona2-nitrophenol2,4-dlftethylphenolbenzole acidbla(2-chloroethoxy)me thane2,4-dlchlorophenol1,2,4-trlchlorobenzeneoapthalene4-chloroanllInehexachlorobutedlene<-chloro-3-methyIphenol2-methylnaplhBlenehe*act)lorocyclopentadlcne2,4,6-tr lchlorophcnol2,4, 5-trlchlorophenol•> -ti , .„„„„... k . - . i , _ w

UJ

n

ul

'

Dir.. _*~

<*.

obo

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—— ±/-

9^^

2

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p(sfl

HGO. m$\COPOUNO

dlMlhyl phthalsts•cenapt hyleno

3-oitroenilln8•cenaphthene

7,4-dinltrophenol4-Mt rophenoldib^n; of*iranJ,<-dlnltroLoluen« '3,$-dlnitrotoluenedlcthylphthsUto4-chlorophenyl-phenyletherr 1 no r ann4-ol t rosni line*,£-dinitro-2-methylphenol

N-n 1 1 r osod I pheny 1 BJD I ne4-broaxiphenyl-phenylether

herach]oroben?epa

pentechlorophenolphenanthreneanthracenedi-n-txjtylphthelBtefluor«nthenebenildlnepyten«

butylbeniylphthelata3, 3'-dJchlorobenzldineben7o(a)8nttir8cenebi»(2-ethylhflxyl)phth8tatf l

chryeenadi-n-octylphthalatubenlo(Wl<}fluor8nthenebervio(«)pyreneindano(1,2,3-cd)pyrenedlbenxo(*,h) anthracenebenio(q,h, i)peryler>«• lpht~6HCbeta-6HCdelta^HCgaena~€HC(llndan0)

hept«chlor•IdrlnheptacMor epoxldaerxJosulftn Idleldrln*,*'-OOCerxJrinerxJosul fan II4,4'-«JO•ndrin aldehydaerxJoaulfan sulTate4,«'-OOT•»«thoxychlorendrln k«tonoctitordtruitoxapherteAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Artx:lor-1254Aroclor-1260

/•

Lu

5i/>P£T;A////r

ij

t^

n&—bocn

O/n^fcM'

^?SCVT

^ /O

T<T^~5b-2TS'T

C?5J

k?J^^4^T

UTCr5J

OCyabf

WT

*bz

*,M6

S,Cilob^

60 T

<ôJ

770t^J

S3 J

573 X

*

9cC:obb

j t o o

<£C/jSbyo'

i^cn

Hoc uiof /COHPOU1JO

ch 1 or Q"1clhen ebromon-.cthanevinyl chloride

Drr.

chloroethanemelhylene chlorideacetonecarbon dlsul fide1,1-dlcMorocthene1,1-dlchloroelhanat rang-1 t2,-dtchloroethenechlorofor1,2-<JlcMo roe thane2 -bu IB none1,1jJ-t rich1o roe t hanecarbon te t rachlor ldevinyl acetatebroroodichloromethane1, 1 ,2 ,2- te t rechloroe thene

Jjj-dlchloropTopanetrana-1, 3-dlchloropropcnet r lchloroethenedlbromochlorome thane1 ,1 ( 2- t r l ch lo roe thanebenzenecie-1 , 3-dlch]oropropen«2^chloroethylvinylether^broflioform2-hexenone^-ffiethyl-2-pentenonatetrachloroethen*toluenechlorobenzeneethylbenzena•tyrenetotal xylenesN-nitrosodl me thy laminaphenol^•nlllnabia(2-chloroethyl)ether2-cMorophenol1, J-dichlorobenzene1,4-dichlorobenzenebenzyl alcohol1, 2-dicMorobenzene

j HMtttiy 1 phe no 1biBj2-ch]oroi9opropyljether4-»ethylphenolN-nitro8o-di-n-propyla«inehexacMoroethanenitrobenzeneJeophrone2-ni t ropnenpl2,^-dInethylphenolbenzole acidble(2-chloroethoxy)methane2,4-dicMorophenol1,2,4-trlchlorobcnzen*napthalene4-chloro*nllin«heicachlorobutadlene4-chloro-3-<nelhyl phenol2HnethylnapthalenehexBctt lorocyclopentadlcr te2, ^,6-tricMorophenol^2, fl, 5-t r ich3o£c>pji^nol_

Ir

£/

T*

ff5T

Po0

COMPOUNDdimethyl p h t h a l e t eacennpthyleneJ-ni t roeni l lneecenephthene?,4-dlnitrophenol4-nllrophenoldibiruof-inn?,4-dinltrotoluen« '?,4-dinitrotoluen«diethyJphthalsU4-chlorophcnyl-phenyletherf l u o r a n *fl-nitroBnUina4,6-dInltro-2-fnethy]phcnolN-nit roeodlpheny lamina4-bromopNenyl -pîenylctherhex8chlorobtn?epepent ecMorophenolphenanthreneanthracenadi-n-butylphthalaterjuoranthenebenzldlnepyrenebuty lbenzy jph tha la te>,3'-dlchloroben7ldinebenzo(a)anthr8ceneb l« (2 -e th> lh ' )xynph thBla t f lchryeenadi-n-octylphthalatf lbenzo(b4k ) fluor anthenabenzo(t)pyrenelrxJ*rx>(1,2,3-cd)pyrenadlbenzo(i,h) anthracenabenzo(q,h,l)perylen«tlpna-BHCbct«-6HCdelta-BHCgamna -8HC ( 1 1 ndane )heptichlor•Idrlnheptachlor epoxideervdoeuir«n Idlaldrln«.4'-ooeendrlnerxJosulTtn II«,4'-000endrln aldehydeendoaulfan sulfate4.4'-OOT•lethoxychlorendrln ketonachlordanwtoxaphenaAroclor-1016Aroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-12^4Aroclor-1260

/

i*j-i$W

"

for,/ - I H i T

tA

§A

^ •25Cft .

*s«

t

- ————

_ X T E :


•J3JECT: Rev iew of Region V CLP DatRece ived for Rev iew on

PROM: Curtis Ross. Director (55CRL) <f££î j?- d/~^ /tCentral Regional Laboratory / '

TO: Data User:r-Pj^T

We have reviewed the data for the fol lowing case (s ) .

SITE NAME: //O O £-C\f\\^£\H SMO case No.T ~~T No. of D.U. /Activity

EPA Data Set No. F^l J-±> Samples: // Numbers 79oS"/Cl.7M/o O

CRL No

SMO Tra f f i c No.Mrs. Requi red

CLP Laboratory: £rt V* Q^yne ______________ for Review:— ~~ ~* ~~ ™* —i-- - - - . . . - — •

Fol lowing are our f indings:

( ) Data are acceptable for use. /~) .- ft InI(/-'( \f Data are acceptable for use with qual i f icat ions noted above. f<f (7 . / / // \( \ D a t a are preliminary - pending ver i f icat ion by Contractor Laboratory. '( ) Data are unacceptable.

cc: Duane Geuder, Quality Assurance Of f i ce r , EPA Suppo.rt Serv icesJames Petty, Chief Qual i ty Assu rance Research , EMSL, Las Vegas

EPA FORM 1320-6 (Rev. 5 /87 }

70

DATA QUALIFIERS

Contractor

Below 1s a summary of the out of control audits and the possible effecto n t h e data f o r this case: " . . . . V

C

bJ I J~h«— V> TKe 7 ?

we Theo//t

f- e

S*

C/5

Reviewed by:

Phone:

Date:

3DATA QUALIFIERS f-

Contrctor:Case

1s a summary of the out of control audits ;*nd the possible effect _.on the data for this case: " .... - ._ .. ,,v.

(C^^^"

n

f?- ^ L />r/f 7-^

Piet- b o /ut I kc-

1 IP MC- I iv-/r M6-

• Z. /_.{tG-/t&

/'/-f

Reviewed by:

Phone:

Date:

DATA QUALIFIERS

Contrctor:Case 73

Below Is a summary of the out of control audits and the possible effecton the data for this case:

5ffyvfy@ n

s: M s / in $ b ffL cA/t/./t/r J

e,/

\/o/) c f 6T

j \

14

Reviewed by:

Phone:

Date:

DATA QUALIFIERS

nrm- ...a '*•

Contractor:Cise 71 r/

fBelow 1s a summary of the out of control audits and the possible effecton the data for this case: . .

CDCO

1(1 1 nflPSTlct'de

At i.î

/>J

Reviewed by:

Phone:

Date:

CASE*


VOLATILE HSL COMPOUNDS- - CONTRACTOR

7'vr

'AQ

/fco7«c*-f £W .s-f W- /DATE/TIME:

ChloromethaneBromomethaneVinvl ChlorideChloroethaneMethylene Chloride

Imt. Cal . Cont. Cal. lCont. Cal. Cont. Cal.£-/i"-f7 \£r*r- <•?/•¥»RF I5RSD * RF

Acetone )Carbon Oisu l f ide1 ,1-01 en 1 oroetnane1,1-Di chloroetheneTrans-1 ,2-Oi chloroetheneChloroform

•70£,?

j-J

50

^0?/33

^,-3utanone I1,2-Dichloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi Chloromethane1 ,2-Oi chl oroorooaneTrans-l,3-DichloroorooeneTri chloroetheneDi bromochloromethane1,1,2-Tri ChloroethaneBenzenecis-1 ,3-Oichloroorooene2-Chl oroethyl vi ny let herBromoform4-Methy 1 -2-Pentanone

'?-Hexanone.'etrachloroethene1,1,2,2-TetracnloroethaneTolueneChlorobenzeneEthvlbenzeneStvrenem-Xvleneo/o-Xv lene

AFFECTEDSAMPLES:

1

*

j*J

RF 50 *'

\J

_ _ _RF |5D

. 1

*

1

f 1

/V?*? ^6 * 3c= -*f f ST ff>» f S*

Cont. Cal/. . -•*-•*_-•.'• J;:.-

RF 50 i*

1

__ ^^ n i _, _..^__^ _

I1t

1 11 I1

*v1 '

•

* These flags 'should be applied to the analytes on the sample data sheets.

1/87

/i-U N I T E D STATES E N V I R O N M E N T A L P R O T E C T I O N AGENCY R E 3 I O N V

C A L I B R A T I O N O U T L I E R SVOLATILE HSL COMPOUNDS

CASE.it 73.5V '_____ - - CONTRACTOR

/A&TtwetiT £~r*5--A.DATE/TIME:

ChloromethaneBromomethaneVinyl ChlorideChloroethaneMetnvlene ChlorideAcetoneCaroon Disul f ide1,1-Oicnioroethane1,1-QicnloroetheneTrans-l,2-QichloroetheneChloroform2-3utanone1,2-Dichloroethane1,1 , 1 -Tri chl or oe thaneCarDon TetrachlorideVinyl AcetateBromodicnloromethane1,2-OichlorooroDaneTrans-l,3-DichloroDrooeneTrichloroetheneDibromochloromethane1,1,2-Tri ChloroethaneBenzeneci s-1 ,3-Oi chl oroprooene2-Chloroethyl vinyl etherBromoform4-Methvl-2-Pentanone2-HexanoneTetrachloroethene1,1,2,2-TetrachloroethaneTolueneChlorooenzeneEthvlbenzeneStyrenem-Xylene0/o-Xvlene

AFFECTEDSAMPLES:

Inlt. Ca .t5-/jf-^TRF *RSO <r

1

Y</./ ,T

1

•

/^«*.'

Cont. Cal .i-73-*?/;rao(RF iO *

3^-9 J

Cont^ Cal .1-2V-P7/VJIRF XD 1*

*.

Cent. -Cal.;•.- '

R= liD

1V3.7 JIsr.v J

/wn*/

,

1t

^

1

1

*

Cont.' Cal . ;-' ,— '-.:--!••-*. •

RF %0 1* *

1

/"*-•?A/s*2. Ie"tî^-*s"t-a7o «^sr¥

«.36i- ti2?O fntfr.'-tf *ffj-qft->r/-e-i*jry6/V/J-6- F/Mf^S

_ . . . .

ff>»W<i-ff ,•«$•)?1

—— T

1

.

a£

* These f lags should be applied to the analytes on the sample data sheets.

1/87

CASE?

I


VOLATILE HSL COMPOUNDS73ft _ -• ' CONTRACTOR

Init. Cal. iCont. Cal.lCont. CaU iCorrt.. Cal. iCont. CalD A T E / 1 *..*,:

IRF ]«SOChlororretnaneBromcmetnaneVinv i CnlorideChloôe'haneMetnvte-.e CnlonaeAcetoneCarc:n Dlsul f ide

-: C"; oroetnane- 1 cnoroeinene

Trars-1,2-01chloroethene

RF

'hlc-oform

1,2-Cic .11 o roethane1,1,--i rlchloroethaneCarcsn (etracniondeVinv i AcetateBromodlcnloromethanel^-jlcnlorooropaneTrar.s-l,3"DichioropropeneTricnloroetheneOibrcrrcchlorome thane1.1t2-~rich1oroethaneBenzene

\

cis-l,5-DlchiorooroDene2-Chloroethylvinyli etherBromoform4-Me-hvl-2-Pentanone?-HexanoneTetracnloroethene

,1,2,2-TetrachlgroethaneTolueneChlc-o-enzeneEthv;benzeneStvrenem-XvieâO/D-<V": ene

AFFECTEDSAMPLES:

RF RF |%0 I- RF |%Oc^r


1/87

CASE* 73 f/



CONTRACTOR

•t#3rA.u/tftr*jT s-+?<*DATE/TIME:

Phenolbisi-Z-Chloroethyl )Ether2-Chloroohenol1 ,3-Oi chl orobenzene1 ,4-Oi en 1 orobenieneBenzvl Alconol1,2-Di cnlorobenzene2-Metnvl phenolbisi2-cnloroisoorooyl )Ether4-Me^nvlphenolN-N -itroso-Oi-n-? ropy! ami neHexacnloroethaneNitrooenzeneIsoonorone2-Nitroohenol2 ,4-Oi methyl phenolBenzole Acidbi s ( 2-Chl opoethoxy )Methane2,4-Oichlopoohenol1,2,4-irichlorooenzeneNaontnalene4-CMoroanil1neHexacn ioroDutadiene4-Chloro-3-Methvl phenol2-Metnvl naphthaleneHexacn lorocyclooentadiene

_j 2,4,6-TpichloPOohenol2,4,5-Trichloroohtfnoi2-CnlcronaDhthalene2-N-,troanilineDimetP.vl PhthalateAcenasnthylene3-NitPoanil1neAcenacntheneZ,4.Qin1tPOOhenol4-NitroohenolDicanzofupan

_. _ - -AFFECTED-—-SAMPLES:

[nit. Cal.y-/-f7

RF

Wi

1RSD *

•

?f-r?33. f

%

>T^*

€•636?<£La70

Zrtss-f -<r/v?A"a.

Cont. Cal.

RF M *

Cont.-Cal.lCont. Cal.lCont. Cal.*

RF M * RF

i•

ID *

-

RF %D |*

t

Cofr-t-

V7

tcCO•v

* These flags should be applied to the analytes on.the.sample data sheets,

CASE*


SEHIVOLATILE HSL COMPOUNDSPage 2

735*; CONTRACTOR Om/yVST*t,/*ftTA-T £ff t

DATE/TIME:

2,4-Oinitrotoluene2,6-OinitrotolueneDletnylontnalate4-Cnlorooneny l-oneny letnerFluopene4-Nitroaniline4,6-QinitPO-Z-MetnvlpnenolN-NitPOSodipnenylamine4-3 pomoonenyl-oneny letnepHexachloroDenzenePentachlopoohenolPhenanthreneAntnraceneDi -n-Buty 1 ohthal ateFluorantfienePypeneButyl benzyl phthal ateBenzo(a)Antnpacenebis(2-Ethylhexvl)PhthalateChryseneDi-n-Qctvl PhttialateBenzo(b)FluopantheneBenzo(k)FluorantheneBenzo(alPyreneInaeno(l,2,3-cd)PypeneDi benz(a,h)AnthPaceneBenzo(g,h,1 ) Pepvlene

[nit. Cal.f-t'^7

RF

&;£

"1RSD

•36*1

»

/?

Cont. Cal.-tCont. Cvl.lCont. CaV.

RF ZU

...

* RF

-

ID

-

* RF

•

%U

-

*

- -

Conr» earnO

RF

- - •

-.u -*s.-f•(

ff

n

1



1/87

UNITED STATES E N V I R O N M E N T A L PROTECTION AGENCY R E G I O N VC A L I B R A T I O N OUTLIERS

SEMIVOLATILE HSL COMPOUNDS

CASE? IS^t(Page 1)

CONTRACTOR € */l//£C2>VX;€

/*/srm,*9**JT s-?»^ Unit. Cal. ICont. CaUCoat, Cal.lCont, Cal . tCont.- Cal .DATE/ TIME: '7-J-77

IRF %RSO w

Phenol 1

\RF %0 1* RF %3 I" RF 110 1* |RF 10 "

bis(-2-Chloroetnyl )Ethep 1 12-ChloPOonenol 11 ,3-Oicnlorooenzene I

1 1 11

1 11 1

1,4-Oicnlorooenzene • — i —— |— I IBenzvi Alconoi 11,2-Oicnlorooenzene 12-Me*nvlonenoi 1bis t2-ch ioro isooroov l JEtner 14-MetnylDhenol 1 1N-N i t POS o-01 -n-? POO v laminaHexacnlopoetnaneNitPooenzeneIsoonorone2-Nitroohenol2,4-OimethylohenolBenzole Acidbi s ( 2-Chl oroethoxv )Methane2,4-Dichloroohenol1 ,2 ,4-Tri cnl orooenzeneNaonthalene 14-Chloroaniline 1HexacnloroDutadiene 14-ChlopQ-3-Methvlohenol 12-Methylnaonthalene 1Hexacnlorocvclooentadiene 12,4,6-Trichlopoohenol2.4,5-Tpichlopoohenol

3/.3

2-C'nloronaonthalene 1 1-2-iNitroanilineDimethvl PhthalateAcenaontnylene • 1 -3-N1 troani line l irlAcenaohtnene 1

3*

1

-

\1

1%

2.4-Oinitroonenot 1 1

1

1 - 11 11 1

1

11 I1 1

11

11 I I I I I1 1 1

I I 11 - 1i i ii I

1 1- 1 11 1 1 1

4—Nltpoonenoi \ys.8 t.T 1 1Dicenzofuran ly^.a l o - 1 1 1 1 1 1

AFFECTED" * SAMPLES:

i l l

€*flT9 MS \ 1 1 1• ^f v 1 1 i 1

1 1 \ ' '\ ' ~ -

1 1 1 1

1 1 1 1

1 1 1 1

t i l l

1 1 1 1

1 1 1 1

1 - 1 1 I .

mnn<-•=maCOrn•o

01

* These flags should be applied to the analytes p n < t h e . s a m p l e data sheets

1/87

c

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY RESIGN VCALIBRATION OUTLIERS - - ' ' , . . _

SEMIVOUTILE HSL COMPOUNDSPage 2

ASEI "73 <T/ CONTRACTOR £*JWAOWH&

/ASlT&vSirMT flit.

DATE/TIME:

2,4—2initrotoluene2.5-Cinitrotoluene

[mt. Ca• * - -

. ICont. Ca * Cont. Ca7-a-y*F 1WSO

D*e*^vlon-naiate•i-Cr * orocrenvl-onenvietrierF'tucreneA-';- -roam "i ine .*&•i,5— Di ni tro-2-Metnv lonenolN— v: troscaionenvlamined-Sramoonenvl-onenvletner

« 'H

1

. - - .. _ _. Cont. Ca . ICont. Ca

•* IRF 110 1* IRF

1 1 II 11 t

JO

1

*

- • r(!

.RF 'iD "

1 - 1-

C 1

hexccnlorooenzene ' 1PentachloroohenolPher.antnreneAntnraceneDi -n-Butvl ontha! ateFluoranthenePyraneBu*vl benzvl phthal ateBer.zot a lAntnraceneois'v2-Ethvlhexvl ) Phthal ateC'nrvseneQi-n-Oczvi f*htha ateBenzo{b)FluopantheneBenzo(k)F1uopantheneBer-,zo(a)PyreneIr.ceno(l,2,3-cd)PyreneDi Denzta,h)Anthracene

1

1

1

Be".zo(a,h,i ) Pervlene 1 1

'.i'1i

t I111111111 .11I

1

\

11

onnTlSrmaenm-ow

o


* These flags should be applied to the analytss on the SIT.;".a data sheets.

1/87


SEMIVQLATILE HSL COMPOUNDS(Page 1)

CASE.? 736~} . CONTRACTOR eAJt//*oT>y*e

/jj$rKv*i&*fT S'lff-z, llnit. CalO A - i / i IME: 1-7-2- f 7

IRFPhenolbTSt-2-Chloroetnyl )Echer2--nioroohenol1 , 3—3 1 chl orooenzene1 ,--3: cnlorooenzeneBe-Z ' / t Alconol1 ,2-0 i en 1 orooenzane2-'-1e~nvlDnenolbis i 2-chloroisooroovl }Ether4-Me~rivlDhenolN-Nitroso-Di-n-?PODvlamineHexacn loroethaneN-.zrcoenzeneIsoor.orone2-Nitroohenol2. 4-0 i methyl phenolBenzcic Acidbist2-Chloroethoxy JMethane2,4-Dichloroonenol1,2,4-Trichlorooenzene

. ICont1

XRSD «

. Cal .ICont:. -Cal . ICont.- Cal .ICont. Cal.1

RF *Q

1 11

11 1

NsDnzhalene 14-Ch'ioroani line 1 lj .7Hexacn 1 orooutadi ene4-Ch'iopo-3-Methvlonenol

3"1

2-Me'hvlnaohthalene 1Hexacn1! orocyclooentaoi ene2,4,6-Tpichloroohenol2,4,5-Tpichloroohenol2-Cn loronaontnalene2-Ni troani lineC:me-nvl PhtnalataAceraontnvlene3-?4izPoani line lv^.7 J

11

RF

1

11111

-

Acaranhthene t2.*i— Dinitroonenol lva-3 T--N". trooneno 1 I3/.V U

13 - |RF %0

1I1111

1

111

11 I1 1

C'-enzofuran I

AFFECTEDSAMPLES: "

1

1

•

* IRF

1

1

»0 w

--

1I

1 1 !i 1 1

tf^Z&f \ 1 1t^gtt \ 1 1

_p i t t

— I | - 1 - -

1 11 1 11 1 11 1 11 1 11 1 1t I I

RECEIVED SEP 1 5 1387

* These f lags should be app l ied to the analytes on . the.sample data sheets,

1/87

/sr

CASE.?


SEMIVOLVTILE HSL COMPOUNDS• ' Page 273 yv • CONTRACTOR

•ropn

/MfTfi^Mf^rDATE/TIME:

*- ?~

2,4-Qlnitrotoluene2,6-Olnltrotoluene01 etnvlomna ate«i-Cn loroonenvl-onenv leanerFiucrenei-Nitroanlline

Lnit. Cal.r-t-~t7RF iRSU *

Cont. Cal. Cant. Ca . Cont. Cal.lCont. Cal.1

RF %0

1 -1

1 1\.0it

4,6-01nitro-2-MethvlohenolN-Ni trosodi onenvl ami ne4-3rcmoonenv 1-onenvletnerHexacnlorooenzenePentachloroohenolPhenantnreneAnthraceneDi-n-Butylohthalate .FluoranthenePyreneButvl benzyl phthal ateBenzot a) Anthraceneb1s(2-Ethvlhexvl IPhthalateChrvseneDi-n-Octvl Phtha ate

- Benzo(b)FluorantheneBenzo(k)FluorantheneBenzo(a)PyreneInceno(l,2.3-cd)PyreneDi &enz( a, h) Anthracene 1Benzo(Q,h,1 ) Perv ene 1

C. 1

i

* Rh

1

"U « RF |%0

1

1

* RF ID

-4 —— 1.

1

*

1 1

c


* These flags should be applied to the analytas on the sample data sheets.

1/S7

ENVIRODYNEENGINEERS

July 10, 1987

Ms . Carol Shaef f erSample Management Office .209 Madison Street, Suite 200Alexandria, Virginia 22314

Dear Ms. Shaeffer;

Enclosed are partial results of analysis of Case 7351 for Volatiles, BN'As ,ar.d Pesticide/PCBs performed by Envirodyne under Contract No. 68-01-7067.Eleven soil samples, EL268 through EL270, and EM851 through EM858, werereceived on June 12, 1987. The samples were screened for semi volatilelevels by GC; EL268 and EM853 were run as medium level samples based onscreening results. All low level semivolatile extracts were cleaned upon GPC. -

A matrix spike and matrix spike duplicate, the second for this case, wererun for both levels of semivolatiles . Volatile QC to cover the second setof twenty samples on the case will be submitted with the samples receiveden June 19, 1987.

Three volatile samples, EM856, EM857, and EM858, showed solvents (methylenechloride and acetone) above the calibration range. These samples werererun with smaller aliquots on July 7. The dilutions also showed themethylene chloride above the calibration range, and concentrations of thecompound were much higher than those on the 5 gram aliquot. The sampleshad a very muddy consistency, and we feel that the surface area of soilexposed during purging is a factor in determining purge efficiency ofr.ethylene chloride. Another explanation for these results could be thatthe solvents were a contamination from the sample bottles; if this werethe case, different locations of the sample in the bottle could yielddifferent solvent concentrations. We are submitting both the "undilutedand diluted sample results, but have no results below the calibrationrange. Toluene-do was higher than the control limits for two of thethree undiluted samples, but in control on one of the diluted samples.


Sincerely,

m

COm-o

_oo


XCW/jagEnclosure

METHOD BLANK SUMMARY

No. Region Contractor Contract No.

or VltMlI CONC.Ltvfl C*S COMPOUND (HSL.flC ON UNMNOVMI CONC. CHOL

n-n-S7ii nms

in-ii-7 IMA l3.Ji..4fu^ KM J *) 330u^n t ncru/x,

UM IcV Htru,

\JOA ! e r\e

U-3M-17 u;13 f 0

Comments:

FORM IV 17/85

METHCT BLANK SUMMARY

Ca9« No. .Region Contractor g/V.yM*o ^ Contract No.

rue >o 0*tt Or UttHll COMC INS MO c*s COMPOUND (MSL.tIC O" UH*MOVNt CONC. UHlfl

JT5

UML W\ flfi^. line. CM rru. els^M 10

id10*1 --v -

L 1110

L,-*

-5

Commenls;

FORM IV

CMC No.Low

SOIL SURROG. E PERCENT RECOVERY SI 'MARYv.._^^

__ Coolracl Laboralory £KJ V I E-Q CW/U 6________ Conlracl No.Medium

- - V O L A T I L t --- --- - - - - . - - . - - - - - - . - - . - - - - SCMI-VOLAUU

ta.viM-0*

in-tin Ut-ltll

-01

III- Itll HI'1141 111- till

**

III-till

_ _ _ . - - >fc t OX* fv\ecias..loo

H C

J_L

0 •SOS *

U>0il A 0.3 *

OU1n £Lon I53-*

5T

asMO

In sotQ 3-

3 /

i _._i«J 3-7

lol

* VALUES ARE OUTSIDE Of CONTRACT REQUIRED OC LIMITS**ADVISORY LIMITS ONLY

Volatiles:Semi-Vola tilts:Pisticidas:

out oTout ofout of

I outiidi of OC limitst outiidt of OC limit iI outiidt of QC limit! ;•''.

7/85

FORM IIHT^V3

C*se No,Low ——

. JRC-..T I...JCK _.IY _ Mht....Y**

Contract Lob^tocy GM.Ui R.CJ>/M6- _______ __ Contract No. Of" "?OYMedium _yi

i*t*rtc•o.

&L~ A.(t> Btw "jS!x\IVHV 1tLOlAfrt)kuSl^rrv-jC

Ill-Mil

'\

> •'*, (It-ilM

\

^X^>^ ^

1

1

t 1 OiCHiO*0

«•• tto

^'/•'

-\

^^

•CMKMf -»»

III- 1141

"2 3*3 I-i

u ^>n 11

t-'iuOMft-

lit- Mil

O *i

^STU*&9^2>

*

Dl*

^5*<J4

. 1V,q^*S5

_.

t

* VALUES ARE OUTSIDE OP CONTRACT REQUIRED QC LIMITS voiaiiÂDVISORY LIMITS ONLY S"m'"~

Psatic

•

111- Mil

SI"? 1IpUî o1 1

l*«! O OUt Of Q t

r\ *%. f~)X/nlafilA*^ , ,. mil of nJ x j

idest —— i — out of —— b , t

Ill-llll

101^Sn t7*1Ss

iii-nii

Mo*13(a*!SoSo

-

11

,

•PESTICIDE--

^log\ \ a-1^5"^ci'5'*

outsidi of OC limits 7/B5outaidt of OC limitsoutiids of OC limits

Comm«nU:

FORM II

IOC.V

SOIL MATRIX SPIKT MATRIX SPIKE DUPLICATE ^COVERY

CM« No. Contractor Contrtot Mo.

Low L«v«l KUdlum

FRACTION

VOASMO

SAMPLE NO.

8/NSMO

SAMPLE NO.

ku^'BACIDSMO

SAMPLE NO.ku atA

PESTSMO

SAMPLE NO.

EL 9^<g

COMPOUND

1.1-OictX)lortlh«ncTfichlorotthf n«Ch>OfOb*nicntToluentBfnitn** ,?.4-Tiichtorob*nitntAccniphlhtnc7.4 Dmi|roiolutf>tPyuritN-Nitrowdi-n-Propylcmint1 ,4-Dichlorob«nicn«Penuchlo'ophtnotPhtnol

2-Chlorophcnol4-Chloro-3-Mt|hylphtnol4-NilrophtnolLtndtntH«puchtofAldrmDitidrinEndrm

4.4'-DDT

CONC. SPIKEADDED (uq/K9|

100,

>

poo

/ÔO. CjOCt

\ s

Ootô

^ sr

Fi OOO

SAMPLERESULT

Oi

\

. _•_•

, >

\~

/

*c,Ktn-=t

CONC.MS

^^sôIIÔoo*1s3o&la^CColU'looc•Ûl/OO^1-2 OCO3D 'Son,Ons DOC;>riO6o|»>Moco

MOCb

MO"H/MifaiIMM-J-110'1 _-v ^\l.

%REC

1ft

Jjft-^?A| i»>01^1V I I*\oûv\o>T1

ioi*3lM»^Ml*IM$>fSM*i-\ i

CONC.MSD

•memilÔOqÔTT)1HHTL

^V'lot^fsr^friti^^riro1*34 m/HTrl

2or?cin1*\^ ArtftosoKKMÔMZ-bOTA5^4-1

%REC

fij>111qt|K1 ( 4°»15^5^ri-1;v»loaIO4<run103»OT>

15S*lo;s»01ft i

RPO

1O4to1^133010ItS(iW5*6-5*M33'|3(,•a^

or i IMITS *RPD

72242121212319473638274735503350503143384550

RECOVERY59-17202-13760-13359 1396614238 10731.13778-6935-1424102628-10417-109289025-10276-1031 1-11446-12735-13034.1323M3442-13923-134 ,

'ASTERISKED VALUES ARE OUTSIDE oc LIMITS.RPO: outiidi OC limit i

OUltidi QC limiuoutiidt QC limiuouliidt OC limiu

RECOVERY: VOAi__out ol.__;B/N £• - out o» .12s;ACIO-U——OUt 0» \Q: J

PEST _U,out of 12;;

outiUf OC HmlnoutiW* OC Hnwliourtld* OC Hmfliouliidt OC Mmilt

FORM III7/65

C«M NO. 135SOIL MATRIX S P i ; /MATRIX SPIKE OUPLICAT RECOVERY

Contractor &KJ1/IE MDVMfc Contract No.

Low L«v«l Mtdlum Lovtl

FRACTION

VOASMO

SAMPLE NO.

B/NSMO

SAMPLE NO.

ACIDSMO

SAMPLE NO.G.M <&£>**

PESTSMO

SAMPLE NO.

COMPOUND

1.1-Oictxitorfthtnt

TrichlorOfflhcncCNoro ben lent

Totu«ntBrnren*l,?.4-Ttichlofob*nr«nfAc*n«phthenc7.4 Dmiirololuff*PyreneN-Nilrotodi-fl-Propvlimin*1 ,4-DichlorobcnttntPeniichlorophtnolPhtnol2-Chlorophenol4.CMoro-3-M«1hvlphinol4-NilrophtnolLindmt

HflpuchlofAid* mDittdrinCndrm4.4--ODT

CONC. SPIKEADDED <uq/K9|

LuT O

_/\*\ 3OO

v

M

/)

^0<«G

150ISO|-i/»

SAMPLERESULT

^

\

i

^

V

<CR-Pt-

CONC.MS

•^TIOF\n.ôIflH "iC>H'TS I r»SH IDCM-iuriSTÔlaptroI WtlU DOT)

^V't)l frO•» i3.T

61HO°\^•-III

REC

5"Un*i!\o\ttnsi5°1414

M1)^0(01<rt3IS") A135*

v IT

"1*1

TiUB11 M

CONC.MSD

UloÔ/S' lO

5tw*o53s'OLmo3^Crti'^290JitcrOi id ti

1 0 T OO

^ IÔbL?*1M976

ISOJQ.Ou <y

REC

HIM^T

_5JDfL

i)X

n^^^>DMA/^X*lb-5^115"*Ka111linSoI.e.

RPD

^ IS3*ni*•i.

5 rg

/3c50*M^c^^f,<jt

ri i*^SL

OC IIMITS*RPD

722421212123194736382747355033505031433B4550

RECOVERY50-1726213760-13359-13966-14233 to;31-137288935 14741-17678-10417-109769025-10276-10311-11446-17735-13034-13231-13442-13973-134

*ASTERISKEO VALUES ARE OUTSIDE OC LIMITS.

RPO:

Convn

VOAI ___ out of ___ :B/N —— 1 — out ol ..'fl, ;ACID g- out of — -;PEST —^ — out of — Lz — ;

outiidt OC limliiouiiidt QC liminouliidi OC limit!ouliid« OC llmiii

RECOVERY: VOAi __ out of __ IB/N —— L,. out ofJ-i;

PEST _I_ out ol JA;

owttUt OC Mmltiovlild* OC llmliounldt OC Hmlliouiiidt QC llmiti

.....

1

FORM Ml7/85

S d3S


Sample Number: EL 26B

Laboratory Mane: ENVIRODYNELab Sample ID No: 87003034Saaple Matrix: SOILData Release Authorized By:

Case Not 7351DC Report No:Contract No:Date Sample Received:

Volatile Compounds


mom

aCO

enu503

12.8

US to: ugkg WSto:

74-87-374-83-975-01-475-00-375-09-267-44-175-15-075-35-475-34-3156-60-567-66-3107HJ6-278-93-371-55-456-23-510&-05-475-27-4

* .1- BT.

• v*lu*.

* lloMt far '

EM«t./«11Wtll

M*CtlB« 11-

Oil or MethaneBroKMethaneVinyl ChlTid*Oilxoettunetethylew QilxideAcEtcneCarbon Disulfidc1,1-ftchkraettael,l-IHchlxoeth«netrans-1 ,2-ftchlxoethmeDilarofxi1 ,2-Oichlxoethane2-ftitancne1,1,1-TridtloraBthaneCarbon TetrachlorideVinyl AcetateBroBoii chl or Methane

B~. l

MV tM. -• ——— »1 t. t». *^-t,

. *- *«. «k «-W-. «- t

•n artlBn. 11MB ta n*t nv^>*avl

It.) 1TW «BM*W«B *—— U« TBBtfl U-

57 U57 U57 U57U

1100 B290

29U29U291129U29U29 U57U29 U29 U571)29U

Ci

•n till*

>«/<a

•M TklB

IV ——— 1

^•••l

78-97-510061-02-679-01-6124-48-179-40-571-43-210061-01-5110-75-fl75-25-2108-10-1S1-7&-6'127-1W79-34-5108-9-3108-90-7100-4H100-42-5

i

flBB BPpllMB «• •••<

__ r— «.™- »y .e/

*lB« t* *m+4 ahBP an

V, It IntflCBtM PBVM

> tMB «*t« UBV t* *•

l,2-&idUoraprDiMnftrans- L, 3-Oi chl ornpr opecTridilxoethenDi bro-ochlaraBfthane1,1,2-TrichIcroethan*Bnzeneci i-l , 3-Oi chl oropropew2-DU xnethyl vi ny 1 ethe-tartari4-hBthyI-2-pHitanDnt2-fteiwn*Tetrachloroetha*l,i,2,MitradilorDtthiwTduBWDdxobcnzeiMEthvlbenzBvStyrmeTotal Iyler.5

1C1«. BM-«^» ————— • «*. 1

•». Mn.1. .... .1 MM1.1

•lyta IB *•*>« !• klM r BB i

l.l w^MI. .!« —— n—— -

** apa»-B»rl«tB Bctl«n.

29U29U29U29U29U29U29U57U29U57U57U29U

_29UrQ? J29 U29U29U29U

..M1M..-

LB*»>-10

•Ml BB B

taiUwi an*

B« wmllM. T>llB »!•• I

multB. 1* uaart. UMPIT wvC •• *ullv •Mcrttow* MX


ENV1RQDYNE Sample Nunder: EL 269


Seaivalatile Compounds .CO

Concentration: MEDIUMDate Extracted/Prepared: 6-26-67Date Analyzed: 7-2-87Conc/Dil Factor: 1Percent Moisture (decanted): 12.8

CASto: uqtq

106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-B87-68-359-5&-?91-57-677-47-486-06-295-95-491-58-786-74-4131-11-3206-96-899-v9-2

Phenolbis-(2-OUm*thyliether2-Qil or c^teral1,3-Oichltnbeniene1,4-DidilorctenzeneBmryl Alcohol1,2-Oichlcrobeizene2-HBthylpnsnlfcis-IHhloroisoprDpyl lether4-ftBthylphaxilH-nitroKHh-n-propyliiiiwHaachlaroethaneHitrobenzoteIsophorane2-tttrophmot2,4-OiMthylphenolBenzol c Acidbi s- tDiltroeUtt y ) Hethane2,4-frichiorophenol1 ,2,4-TridilorcbenzEneNapftthalene4-QilxtuniHneteachlorobutaiieoe4-akro-3-«thy 1 pnerral2-MhvlnaprithaleneHoachlorocyLlcpBitadierie2,4,6- Trichl or ophenol2,4,5-Tridilarcphenol2-Qil7aiaphthalene2-*troarilineDiwthyl ptithiliteftcen*pthvlff>e3-fetroaniline

23000 U23000 U230COU23000U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U110000 U23000 U23000 U

. 23000 U23000 U23000 U23000 LJ23000U23000U23000 U23000 U110000 U23000 U110000 U23000 U23000 U110000 U

Sep. FunneContin, Li

CASfc:

83-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-386-73-7100-01-6554-52-186-30-6 '101-55-3118-74-187-86-585-01-812H2-784-74-2206-44-0129-00-085- 8-791-94-156-55-3117-81-7218-01-9117-64-0205-99-2207-08^50-52-8193-39-553-70-3191-24-2

1 Extract ion : YES 'q.-Liq. E x t . : YES ,

AteMOhttww2,4-ihrutrn*wol4-*tn$benolDibenzofiiran2,4-DUitrotfllaBit2,6-DinitrotQlifl*fttthyl pfcUuiitt4-Qilarnjhenyl-pnenyl etherHucrenf4-HitroamIine4,6-fonitrD-2-Metrtylp6enolM-mtrwodiphsiylaiint (1)4* Brotaphflnyi -phwyl cthirteachlarEbenzer*FwtactilorophenolFtcnanthnreAnthraceneDi-rHwtyl phthalateFl or anther*ryranButyl-benzyl -phthaUUw»j wiuuU LucnziQincBBiioiiJ itfiLnriccntbis-(2-Ethvlr«vl)phtKalatBDryMfieDi-rroctyl pnthalateBBttoibHlucrttttieneBBUOtk)flucrantheneBBuouipyrentiKtrod^^-dlpyrvieDibemou.hiarttwacerwBenzotgruiperylene

<NO) (cir(J^)(cir

ugkg

23000U110000 U110000 U23000 U23000 U23000 U23000U23000 U23000U110000 U110000 U23000 U230W U23000 U110000023000 U23000U23000 U23000U23000UZ3000LJ45000Uaooou_

(2400 J^2050123000U23000UZ3000U23000 U23000U23000 U2300UU

(l)-Cannot be separated from diphenylamne

FORM 1

Laboratcxr Name

Case No

Organics Analysis Data Sho«t(Page 3)

Numb«r

Concentration Low

Date Extracted 'Prepared1

Date Analyzed —————

Posticide/PCBs

(Circte Ooe) GPC Cleanup CD Yes QNo

Separatory Funnel Extraction QYes '"• *'

Continuous Liquid - Liquid Extraction QYes

X)mo

oConc/Dil Factor


CAS ug/1 oK^gyKg.Number (CircU On*)

319. 84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553169-21-912672-29-6H097-69-111096-82-5

Alpha- BHC

B«ta-BHC

Oetta-BHCGammj-BHC (L«rxJanelHeptactilorAWnn

Heptacnio*- EpoxwleEndosulf an 1Ontldfin

4. 4--OOEEndrinEnbosuHan II4.4'-DODEndosuKan Sulfate4.4'ÔDT

M*thorvchIO«'

Endrm KeioneCWordan*

Touphene

Arod(X-1016

Aroclof-1221Afoc1o»-1232Afoctof-12-:2Aroc(o»-1248A/OClOf-1254

Afoc(0f-1260

IZO, 0 01/PO, <5 K.120, O IL}lG U:rt-c • u[7-c tL_JA^.O U730,0 U

-Z-Vo -USffO.O U..We U

*JWQ.O aXVO.Q U*</o.o U*y-n U.

~I3LOQ,0 U2<JQ<0 11

IZOO,0 U

MQO.O a/2oo.£ IJLMOO.O U

1300,0 UW«=o,o Ujsoo.o Ufftfoo.O Uytjc&.Q Ui

V( = Volume o< ertraci inj«cied (u()

V = Vo<um« of water enracted (ml)

W « Wetght of Mimple e«tr»cted (g)

V * Volume of iota) extract (utj

orW.

Form 1 7/85

urqanics Data SheetiPaqv 1)

Si-pie Nue-ber: EL269

Laboratory Naae: ENVIRQOYNELab Staple ID No: 87003035Saiplt Matrix: SOILData Release Authorized By: _Q?£lU__

Catff No: 7351QC Report No: ~/S /Contract No; _(cA__QjDate SaaplB Received:

Volatili Coipoundi

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-87Conc/Dil Factor: 5Percent Moisture (not decanted) 13,0

CAStte CK to

74-«7-374- 3-975-OH75-00-37W9-267-64-17V15-075-35-475-34-3!&-6iH67-66-3107-06-27^3-371-55-656-23-5108-05-475-27-4

EMoroKthantBroKMethaneVinyl ChlxideOtlortEttuninpthylne ChlcridtAutmCarbon Dlsulfide1,1-IhcKlraetherw1,1-Oirtla-oKhawtr«-l ,2-Oichl croethemOil or of xil,2-Dichl(rtiftha{v2-Butancne1,1,1-TrichlororthaneCjrlKii TrtrachlorideVinyl AcEUtfBrondichlorotetluni

57U57U57115711730300

29U2 9 U291129U29U2 9 U57U29U29U57U2 9 U

7B-B7-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-B75-25-210B-10-'l591-79-61Z7-1B-479-34-5ioiHfi-3106-90-7100-41-4100-42-5

i^cftlT^tjan.tr ans-f, 3-Di chl on^rtpwtTrichlxoetheM&i broeochl (methane1,1,2-TridilcraethawBenzeneaj-l,3-ftdilcrcprcvM2-OU ornethyl vi nyl etherBroeafxi4-fethyl-2-pent2xn2-HnmaneTetracMraetha*1,1,2,2-TetradilcroethaneTolueneDUtrobenzmEUrrltureewStyreneToUl him

2?U2 9 U29U29U» U2 9 U2 9 U57U2 9 U57U57U2 9 U29 U

»52 9 U2 9 U2911

•«/M! IN

t^H«l«lCI

tlB1«B»»10

lw IkMt far

l -ill ill

U (•«,

*v kwt not 4M*t*M. Ifia m^kv !• tM

1T M^tn*


ENVIRQDYNE Saagle Number: EL269

Qrganics A n a l y s i s Data Sheet(Pag* 2)

o

Concentration: LOWDateDateCone/Di1Percent

Seiivolatile Compound*

GPC Cleanup i YES: x t r a c t e d / P r e p a r e d : 6-19-07malyzed : 7-1-87i 1 Factor : 1t hoisture (decanted): 13

CASto:

108-95-2111-44-495-57-8541-73-1106-44-7100-51-695-50-195-48-739638-32-9106-44-5421-64-767-72-1on fie TW-TJ-J78-59-188-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295-95-491-5B-788-74-4131-11-3208-96-899-09-2

Phenolbis-(2-QUcmethyl}«ther2-Qilorophtnoll,3-Dichl(rubenzene1,4-DichlorobenzeniBenzyl Uriell,2-0ichlorobai:ene2-fethylphmalbis-l2-OilaraisojirQpyl)ftt«r4-fethylphenol(Hii tnwHH -n-pr apy 1 ui ntHesachl methaneIK L — *- —— ——ntrooenzene

2-tktroplwwl2,4-fc«thylphenalBenzine Acidbis-iQilxaethnylnWvane2,4-Oictiltropbenol1,2,4-TrichltrobenzewNaphthalene4-Q\ltrojniHneHeiachlorDbutuliene4-Oil iro-3-tethyl phenol2-fHhyluphthileneHex achl arxvd Gpait idi ere2,4,6-TrichIorophenol2,4,5-Tnchlartphenol2-Qilirauphthalenc2-NitroanihneDivthyl phthaUteAcenapthylene3-ttitr owi lint

ugkg

740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U74011740 U740 U3700 U740 U740 U740 U740 U740 U740 U740 U740 U740 U740 U3700 I)740 U3700 Q740 U740 U3700 U

Sep. Funnel E x t r a c t i o n : YE5 'Contin, Liq.-Liq. E x t . : YES

CAS to:

83-32-951-28-5100-02-7132-44121-14-2404-20-284-64-27005-72-3Bfr-73-7IKHH-6534-52-1-86-30-6101-55-3118-74-187-84-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7218-01-9117-84-0205-99-2207-08-950-32-fl ~193-39-553-70-3191-24-2

Aanaphthene2,4-Oinitn?nenol4HtitroQh8wlDibenzofu-an2,4-fcnitrotoluoc2,4HhnitrotolueneKethyl pttthalati4-QUQn^hBiyl-phenvl etherFluor ene4-tttroanihnc4,4-Oinitro-2-h>thylph«olM-nitnsodipnenylauni (1)4- DroiDphenvl-phenYl etherHaadYlontenzenePent icn 1 x opnenolRtenantn ••fcithracK*Di-n-butvl fnttulateFlutrwtheofPyrmeButyl-bwzyl-phthilate3,3'-&ichlini«zidif«Benioiil anthracenebii-(2-Ethylhnyl)phthaiat«ChrysewIh-n-octyl pnthilateBenzotbtnurantheneBenzodclfluranthene

'Bemo(i)pyreneIndBnd^ -oiipyrBCIKbenio(a,h)aflthracencBenzolghilperylene

bjrt (c i rc l e one)(tify ( c i r c le onei

*to

760 U3700 U3700 U740 U740 U740 U760 U760 U760 U3706 U3700 U74011760 U740 U3700 U760 U740 U710 J740 U740 U760 U1500 U7 4 0 U ,

r-<srr"/THTTj760 U760 U760 U760 U - —— -740 U740 U740 U

(D-Cannot be separated 4roe diphenylaaine

FQRtt 1

Cat* No

Concentration: tow Medium

Date Extracted'Prepared:

Date Analyted

Conc/Oti Factor

Organic* Analysis Data Sfxwst(Page 3)

Pestictde/PCBs(GrcfeOne) GPCCleanup CSYes QNo

Separatory Punnef Extraction OYes

7""/~*£*7 r<wiiif

r* {fi*r*mi«1] ) S x =>

CASNumb*r

319-84-6

3)9-85-7319-86-8

58-89-976-44-6309-00-21024-57-3959-98-*60-57-172-55-972-20-833213-S5-972-S4-81031-07-fl50-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-S53469-21-912672-29-611O97-69-1

11O96-82-5

Alpfu-BHC

8eta-BHCO«Ua-8HCGamnu-BHC {(.tndane)

HeptachiorAldnn

««ptacnkx Epo»«ieEndoiurtan 1Dtetdrin

4. 4*-ODE

Endrin

EndosuMan U

4. 4--ODD

EndosuHan Svtf ate4. 4'-ODT ^

Mett>OK>chlor

Endrin (CeioneChlordaneTo«Jptxn«

Arocfor-1016

A/octor-1221Aroclor-1232Aroclof-1242A/ odor. 1248AfOC tor -1254

Afoctof-1260

luous Liquid - LJ

s — \ug/lorf»9/Ko,

(CirefirOnel

/4. 0 UL1^.0 tlIL.O «.

-- /Aô WJ-fc,o a?to a.

/4-O «

/4-<3 t<.^^^ W.j 3,O U.

rz*o a' ^3^3 «

Jp,O t(ja-o t<

" £2-0 U' ILO.£> U.

33.0 U

f(r£>.O U.

33G.& H

]t>O.C> Ullo.a Kf£6~Q U/u>.& u/&6.O U.j^d.^ a32&.O U.

-o

orW.

= Volume o( extraa (u()


t = We*ghl at (gl

V. * Volume o4 total extract (ull

3..0-JL

7/85

flrqanics Analysis Data Sheet(Page 1) !--

Saaole Nuiber: EL

Laboratory Na,»e:Lab Saaple ID No:Si-pie flatrixi

ENVIRQDYNE87003036SOIL

Data Release Authorized B y : _ ( y _

Case No: 7351QC Report No:Contract No:Date Saaple Received: __^L"i>.i*

Volatile Compounds

Concentration; LOWDate Extracted/Prepared:Date Analyzed: i-24-87Conc/Dil Factor: 5Percent Moisture (not decanted 14.0

-o

OS to: CASfc: ugkg

74-97-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5106-05-475-27-4

• .ali« ar-

Oil (methaneBrmethaneVinyl ChlorideQtloroethaneHethylene QtlorideAcetateCarbon Dial fide1,1-Didtloraetbene1,1-DichlDroethanetrara-U2-Dichl QroetheneQUcrotori1,2-OichIcrorth.fle2-Butanone1,1,1-Trichlcraeth.r*Carbon TetradilxideVinyl AcetateBrotodi ch 1 or Methane

•at* «

•at.- tH— ar •«M| t. tta *

SBU5BUSBUSBU940.170 6

29U29U29U29U29U29USBU29U27USBU29 U

•

Ci

MKttan Tdla Maa apal

71H7-510061-02-679-OK124-48-179-00-571-43-210061-01-5110-75-875-25-2108-10-1591-78-6-IZ7-1M79-34-5lOB-eB-3108-90-710CH1-4100-42-5

11 a. t« .Mtt

l,2-DidilarDpra(wn»trans-1 ,3-DichlmjpnB«TrithloriethentDibmachlanaeth.Y»l,l,2-Trichloroeth»eBeweneci s-1 , 3-&i chl tropropene2-Chl xoethy! vi nyl etherBrnotor*4-tethyl-2-pentanone2-HeivnncTftrachloroethme1,1,2,2-Tetr.dilxotth.MTolueneDilarobenzmEthvlbenznStyreneToUl lylenes

.1*. âra»t*-« rtwa U- 1—— rt

29U29U29U29U29 U2?U29U5BU29U5BLJSB U29U79 LitTT29U29U29U29U

me.-

*«/ttl In

anAly*** 1m- but

^ UMt *«r Uw ••••IB ^t* W*W U (•v.

T "MUrMur •cxlan. «TtH« !• «•»

^•cttan UXt.> TIM *••*•••• •Maul* r»a*t V-

nvrt f«r (kwt "•* MMa tM. Tfw «!»••• !• Uv

THta «laaj !• i ari aitfiar

41 •• !•

1*. It l««l

tit* «•*•

tn«tcatart Ww pi ••anea *f * BVBPHV^ Uwt •••*• Uw loanctf t«««lan

art tar I a kwt UM r««»it IB !•«• tlun t>» •aaclfl«« aMartlan Halt

t»an «ar* (•«. IB4) . 14 lta*t •< Mt*«lan »• 10 layl MM

Laboratory Naie:Case No: 7351

ENVIRQDYNE Saaole Number: EL


Concentration: LQNDateDateConc/DilPercent

Senivolatile Compounds

GPC Cleanup : YE5x t r a c t e d /P repa red : 6-19-B7n a l y z e d : 7-1-87il Factor : 1t Moisture (decanted): 14

CAS to:

106- 2111-44-495-57-6541-73-1106-46-7100-51-695-SM95-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-186-75-5105-67-965-85-0111-91-1120-63-2120-32-191-20-3106-47-887-68-359-50-791-57-677-47-4BB-Ob-295-95-491-58-788-74-4131-11-3208 •% fl99-09-2

uqkg

Phenolbis-{2-Chlxaethynether2-Chloraphenat1,3-Dichlxabenzml,4-Did)lxobenzen*tenzyl AlatolIf2-0ichlarab«nzcne2-tethyl phenolbis-(2-Qilaroiwpropyl)pther4-ttthylphenalH-ni trosiH>i -n-prqiy 1 au ncHnachlxcethanenitrobenzenelupnxone2-*trophenol2,4-DiwthylphrolBvuoic Acidbi s- (Oil xoethcB ytttethane2,4-Oichlorcphenol1,2,4-Trichlarabenzenttaphthilene4-QilanuniIineHRachlorabutuJiene4-Qilxcr3-«thvl phenol2-teUiyl naphthaleneHexachlxacyclcpentadiene2,4,6-Trichlorophenol2,4,5-Trictilcrnphenol2-Chlxanaphthalene2-Nitroanihne&i«ethyl phthalateAcHuothylene3-th troaru line

770770770770770770770770770770770770770770770770

UUUUUUUUUUUUUUUU

3700 U770770770770770770770770770770

UUUUUUUUUU

3700 U770 U3700 U770770

UU

Sep. Funnel E x t r a c t i o n : YESC^Mc iContin. Liq.-Liq. Ex t . : YEa QNQJ(c i

CAS to:

83-32-951-28-5100-02-7132-64^121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-L-86-30-6101-55-3118-74-187-86-585-01-fi120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-91-7218-OH117-84-0205-99-2207-W-950-32-8193-39-553-70-3191-24-2

Acenaphthene2,4-ttnitrcpnenQl4-tttraptanolDibenzottran2,4-Oinitrotoluene2,6-Oinitrotoluenefo ethyl phthalaie4-Oiloraphenyl-phenyl etherRucren*4-tatroafulint4,6-Wnitro-HlrthylptawlK-nitraodipnenylaune (1)4-Brcnophenyl-?henyl rtherffaachloTQbenzenePentidilrophmolPhBunthrenetetbraceneDi-rrbutyl phthalateFluor anthenePyreneButyl -beicyl-phthaUte3,3'-DichlxcBfn2idineBen:o(i)»thrKem [bi»-(2-Ethylâ¥l)phthalateChryseneDi-n-octyl phthaliteBeuotblfluirartfwoeBenza(k)flicrantheneBwzoUJpyrmf •Indenotl,2.3-ol)pyrweDiberuo(t,h)inthruen«Benzo(qtu)perylene

ugkg

770 U3700 U3700 U770 U770 U770 U770 U770 U770 U3700 U3700U770 U770 U770U3700 U770 U770 U

UflOuJD J "

WJUJ1500 U.~ —— -^juH550 «•

_770_y.[tfl'j^sT)[69 J_PQ(J"62Jl1 65 J_l

770 U3700 U

( c i r c l e one)e one;

(l)-Cannot be separated from d i p h e n y l A m i n e

FORM 1

No

Organic* Anarysis Data Sheet3)

Concentration: (j-&**) Medium

Date Extracted 'Prepared: ____x2

Date Analyzed: ______/"'

P«st*c*de/PCBs

(Circle One|

X)moGPC Cleanup BYes ONo

Separatory Funnel Extraction O res ~' ^S•—*

Continuous Uqukt * Liquid Extraction Oresco

Cone/Oil Factor:


CASNu«nt>«r

orW.

V = Volume o/ ertract infected (u<)

V - Volume o( wate« extracted (ml)

W = Weigh! of cample extracted (Q|

V( * Volume of total ««*raa <ul|

3C'«

CO

319-84-6319-85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-t72-S5-91

72-20-833213-65-972-54-81031-07-8SO-29-372-43-5534 94-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

11096-82-5

Alptu-8HC

Be»-BHCDelia-BHCG*fT»ma-BHC (LmdanelHep(act>lorAWr-o

HeptactUor Epox*deEndosutfan (D4efdrin4. 4--OOECnoVtnEnoosutfan 04. 4'-OOOEndosutfan Sutfat«4.4'-ODT v

Metttocychlor

Endfin Keton*ChlordaneTouptteneAroctof-1016Aroctof-1221Ar octof- 1232ArodOf-1242

A/oc*<x-1248A/octor-1254

Arocto*-1260

!(*.& W/t.o nit.o a

., l*>*o utt'O a.lk,o U.

it»o utL.O K-S^'tt.33.0 tt

~3t>& UL* .-3QO «

'SJ.O K33*O t.£> U_

ji.O Utl*&O U330.0 U.1t>6.0 Utto.O UKr&.Q U

ILQ.O U/&6.O «.320.Q U3*O.O U.

7/85

Qrganics Analysis Data Sheet(Page 1) ! —

Saaple Nuaber: EH

Laboratory Naie:Lab Saaple ID No:Saiple Matrix:


Data Release Authorized By:

Case No: 7351QC Report No:Contract No:Date Saaple Received: ._U-'_J_' _-_

O

Volati1e Compounds

Concentration: LOUDate Extracted/Prepared:Date Analyzed: 6-24-B7Conc/Dil Factor: 1Percent Moisture (not decanted 12.9

c/im-o

CASte: iqkg uqkq

74-87-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-315WO-567-66-3107-06-27S-93-371-55-f.56-23-510fr05-475-27-4

Oiler Diet hamfirowtluniVinyl QilcrideDilxoethancNtthylnw QiloridtAcEtoneCarbon Disulfide1,1-Diddaroetheie1,1-Dichlarorttunetrans-l,2-0ichlxoethawChlorafori1,2-Oidilaraethdne2-fiutanoncI,l,l-Trichlirt3eth«Carton TitradiliridiVinyl AceUteBrtModichltroiethaM

11 U11 U11 U11 U

f73&OJ

6 U6 U6 U6 U6 U6 U11 U6 U6 U11 U6 U

7B-87-510061-02-679-01-6124-48-179-00-5

^ 71-43-210061-01-5110-75-875-25-2106-10-15W-7H,127-1W79-34-510MB-3106-90-7100-41-410CH2-5

_ _

l,Hidil(rarcfinetr»s-I,3-Oichl(n$rcpeneTridilorpithwto bronchi oro«thani1,1,2-Tnchliroethan*BBUBCds-l,3-0idilarnropew2-Oilaroethyl vinyl etherBroMrfori4-fethyl-2-pntanam24fR«naneTetradUcraetheie1,1,2,2-TetrjeMflraethintTalumQilcrabenzawEthylbenznStyrm*Total lylra

6 U6 U6 U6 U6 U6U6 U11 U6 U11 U11 U6116 U6 U6 U6 U6 U6 U

Ci

Tftt

lly

minimi- »ttAl(u*l« ••••cttvt Halt *«r tiw t* m*~rlr «Wi'

Thla *!•« 1* IM«« Mtmr

t*» •-mat I* !••• UMH UM BpacKlM *M*ctlvi llBtt tort

Labo ra to ry Naae:Case No: 7351

ENVIRODYNE Staple Nu«ber: En 851

Qrganics Analysis Data Sheet(Page 2)

70nn

mo

S**ivolatiIB Compounds

Concentration: LOWDate Extracted/Prepared: 6-19-87Date Analyzed: 7-1-87Cone/Di 1 Factor: 1Percent Moisture (decanted)

CftSto:

12.9

uqkg

lOfr-95-2111-44-495-57-8541-73-1106-46-7100-5H95-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-39-186-75-5105-67-965-85-0111-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-48B-06-295-95-491-5B-7BB-74-4131-11-3208-96-a99-09-2

Phenolbis- 12-Qil cn-ethy 1 ) eUw2-Qilcraphenoll,3-Dichl(roberuenett4-Didilxoben2eneBsuyl Alatall -Oichlontenzene2-tethylphenolbi5-(2-Qilcroi5Cpro()yl)ether4-Heti.ylphmalIHH troso-Di -n-propyl aaincte^hlmiethwtbtrobeniBttIs hxcne2-Wtrophenol2,4-OiKthylpnmlBenzine Acidbis-taitroethcByltethtf*2,4-Di-nitrDp.wnol1,2, 4-Tr i dU cnteu meH thilene4-0.1 Toani lineHexadtlorcbutadiene4-Qil aro-3-iethYl phenol2-ftothylnaphtlulenehaxMTxyclqcntadiene2,4,Hrichlorophenol2,4,Hhdiltnphenol2-Oil croup fit hilew2~(titroa(ulineDivthyl (rtittulateAcaupthylene3-totroanihne

760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760U760 U760 U760 U760 U760 U760 U760 U3700 U

- 760 U3700 U760 U760 U3700 U

i. Funnel E x t r a c t i o n : YES (itin. Liq.-Liq. Ext. : YES <

CASfc:

83-32-951-.B-5100-02-7132-64-9121-14-2606-20-2B4H6-27005-72-386-73-7100-01-6534-52-186-30-6101-55-3118-74-187-46-585-01-8120-12-784-74-2206-44-0129-00-0BtB-791-94-156-55-3117-81-7218-01-9117-64-0205-99-2207-OM50-32-8193-39-55J-70-3191-24-2

Acenapbtbene2,4-Oi[\itn$h6nol4-NitrqtenolDibenottran2,4-OiiitrotDluen*2,6-OinitratoliMneDl ethyl phtbalate4-O.lQnvhaiyI-pnB.yl etha-Fluorene4-tetnaniline4,fr-Oi.itro-2-*thylph«nolH-rutnsodiphBiylaBine (1)4-8roiQphenyl-pnBiyI ethertaachlcr*wuff»rwtaoUoroqhwolrheiUllUff H*

AnthraoneW-n-twtyl phttolrti (FluorMthentPyreneButyl-benzyl-phthalate^S'-DidUT-benzidineBenioiAJ anthracenebi«-(2-€thyltwyl)phthalaUQvyvneDi-n-xtyl phthalateBvzolbHluorwttieReBenzotb luoranthflwSBiioiaJjryrme _ _ _ _ _Ind_.no(l,2l3-alJpyrer.e_Kbe«2o.a,h)..flttYacene8enzQ.ghi)pe-ylent

J§ (ciJ5> (ci

760 U3700 U3700 U760 U760 U760 U760 U760 U7601}3700 U3700 U760 U760 U760 U3700 U760 U

^ZKU"O

^-âou760 U760 U1500 U760 U3706*760 U760 U760 U760 U760 U760 U760 U760 U

-o

(circle one-)-1

PTC

ID-Cannot he separated fro« diphenylaaine

FORM 1

U«txxaiofy

No

Concentration: ( Low) Medium

Date Extracted 'Prepared:Date Analyzed: ______

Organics Analysis Data Shoot(Page 3)

Postic»de/PC8s(Circle One) GPC Cleanup

___ SeparatofY Funnel Extraction QYes

___ Continuous Liquid - Liquid Extraction QYcs

Cone/Oil Factor:

Perceni Mo*store (decanted), 12-?CAS ug/l O'W'K^Numbar m CCircffTTrwl

319-84-6319-85-7

319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-55-972-54-81031-07-850-29-372-43-553494-70-557-74-98O01-35-212674-11-211104.28-211141-16-553*69-21-912672-29-611097-69-111096-82-5

Aipha-BHCB«tJ-BHCDelta -8HCGamm*-BHC (Li<xJanel

HcptachlorAldr.n

Heo»crWor £pox«JeEndosulfan IOieldrin4. 4--OOE£n&inEndosuHan tt

4. 4--OOOEndosutfao Surfate4. 4'-ODT

Mettx>KVCMor

Gndfin KcioneChtcxTJar**ToupheneArockK-1O16A/oct<x-l22lA/octof-1232ArocI<X-1242

A/ockK-1248Aroc(<X-l2S4

Aroc*o*-l26O

if+.o a./t . 0 tttC.O (L

- .16.0 W/4,» Uf fcxO U.

/t>.o u/£>.£>• K

,l2.J> U.33.0 «.^z-c? a.

' .^&-o *iVP.O «^3^3 «

" î-<? «f- /<-<>.£> U.

J .O «/(^X^J W

JU .«O U)l>0.& Ult£>.0 U£6.6 UIWjQ U/6AO U.3.3<>,0 ^3 . 5 6C

orW.

V^ = Vofum« of extract infecred (ul|

V = Vo4um« o< watef extracted (ml)

W = Weight of t*onp<« extracted (gl

V( * Vofume o< total ear»a (uf|

7/8S


Saiple Number: EM 852

Laboratory Nane: ENVIRODYNELab Saaple ID No: 87003038Saaple Matrix: SOILData Release Authorized By: _{Y\

Case No: 7351OC Report NoiContract No: __la 3.-Date Sample Received

Volatile Compounds

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-87Conc/Dil Factor: 1Percent Moisture (not decanted 12.8

CftSlta CflSMo: uqkg

74-67-374-63-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-S-656-23-5108-05-475-27-4

Oil or MethaneBraoeethaneVinyl ChloribtChloraethantHrthylene ChloridefcEtontCarbon DisuHide1,1-Didiloroethenel,HKchlcroethinetrans-1 ,2-ihchlorDethweCbloroforil,2-Didu(roethanB2-Gutamm1,1,1-TridUxoethaneCartxii TetrachlxidcVinyl AcetattBro«odidil or Methane

11 U11 U11 U11 U56 B45 940

6 U6 U6 U6 U6 U6 U11 U6116 U11 U6 U

78-67-510061-02-67W1-6124-48-179-00-5

r 71-43-210061-01-5110-75-fl75-25-2106-10-1591-78-61Z7-1B-4'79-34-51C6-9B-310*40-7100-41-4100-42-5

1,2-Mcraprcw*trans-1 ,3-ttchlcraprapmeTrichlaroetherwvibrtMQchl trapthanel,l,Mncfiloro«hir*Bnzcnedi-l,3-DidilorD9rafiBir2-Qiloroethylnnyletherft-oiDtori4-ftethyl-2-p«tjnonE2-teanmTetrachluoettenel,l,2,HrtradilxwthiMTolueneQilorobenzentEthylbeuowStyrmeTotal lylenes

6 U6 U6 U6 U6 U6U6 U11 U6 U11 U11 U6 U6 U6U6 U6 U6 U6 U

If Ut*

llatt. •tn«lB

n«/ul in ttw ftn«] H tract

ltvrl* kvt UM rnult !• !••• Utwi th» ••vclft** **t«tl«n ttMt

!•*. IOJ1. If lt«4t •« rivfcaMlan !• 1O u»l

Laboratory Name:Case N=: 7351

ENVIRQDYNE Simple Number: EM 852


Concentrat ion: LOWDateDateConc/DilPercen t

Seaivolati le Compounds

BPC Cleanup : YESx t rac ted / Prepared: 6- 19-87naly ied: 7-1-B7il Factor: 1t M o i s t u r e ( d e c a n t e d ) : 12.

CftS to:

106-95-2111-44-495-57-fl541-73-1106-44-7100-5K95-50-195SB-739638-32-910M4-5621-64-767-72-198 75-378-59-1BB-75-5105-67-965-85-0111-91-1120-93-2120-fl2-l91-20-3106-47-8B7-6B-359-50-791-57-677-47-488-06-295-95-491-58-78B-74-4131-11-3208 96 699-09-2

Phenolbii-{2-Oilxoethyl) ether2-Qiltrcohenol1,3-OichlcrabenzH*1,4-DichlorQbenzB*Bmzyl Ma*nl1,2-OichloroBenzene2-fethylphenolbis-(2-£hlxoisaprapyUether4-tethylphenolM-nitrosD-ft-n-propylaiiwHex*hlxTKth«nitrobenzeneIscphcnne2-tttmohenol2,4-foMthylphenolBemoic Acidbi s- (Olcroethcay) teth«2,4-OichlxDphenol1,2,4-TrichlorcteueneNaphthalene4-QilxoanilineHnachlxobutadiene4-CW xo-3-«thy 1 phenol2-Hethylniphthaiewteachl crocycl opentadi me2,4,6-TnchlcrDphenDl2,4,5-Trichlxcphenol2-Qilorauphthiiene2-*btraanilineDiwthyl phtKiJiteAcmapthylene3-Hitrwfiiline

! = = = = = = = = = :

,6

uqkg

760 U760 U760 U760 tl760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U3700 U760 U760 U3700 U

Sep. Funnel E x t r a c t i o n : Y E S <Cont in . Liq.- l iq. E x t . : YES

CKto

83-3251-28-5100-02-7132-M ?121-14-2606-20-284-66-27005-72-386-73-7100-01-6534-52-186-30-6 ,101-55-3118-74-1B7-&-5GE-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-721H»H117-84205-99-2207-08-950-32-8193-39-553-70-3191-24-2

Acenaptithene2,4HhnitropMral4-tttrcpherolDibcnzotran2,4-ttnitrotoliete2l6HhnitrotniuBKDiethyl pbthalate4-OilcTQp6enyl-phenyl etherFluor ene4-*btnuniUne4,6-Oinitro-2HWhyl[>henolN-nitrtHoiipnenYlaiine (1)4-BroMpNenyl-phenyl ttherteach IxotwupwPentachl xtjjhenclPhBunthnneAnthraceneOi-ft-butyl phthalatiFlutranthene"PyrsieButyl -benzyl -phthil ate3 ,3 ' -to chl onaenz i dinefenio(i}»thrttenebi5-(2-Elhylhoyl)phth4ljti!ChryuneDi-n-octyl pnthalittBenzotblflucrartheneBenzotkJUurantheneBenioiupyrtnelndBXi(l,2,3-ai)pyrneIKbenzDU^h) anthraceneBaizQtghiipe^lenc

^NQj)<ci

uqkq

760 U3700 U3700 U7601)760 U7UU760 U760 U760 U3700113700 U760 U760 U760 u37001)760 Uliflu

dS^760 U760 U760 U1500 U760 U410 «760 U760 U760 U7601)760 U760 U760 U760 U

one)

( l ) - C a n n o t be separated iron d iphenylas ine

FORM 1

C»s< No

Concentration: tow Medium

Date Extracted 'Prepared:

Date Analyzed: ______

Organtes Analysis Data Sheet(Page 3)

Peiticid«/PCBs

(Crete One) GPC Cleanup Ores QNo

___ Separatory Funnel extraction

___ Continuous Liquid - Liquid Extraction QYes

nG-"2.

Cone /Oil Factor: 1Percent Moisture (decanted) II-

GAS ug/forfcjg/K^.Number „ (CJrcMTUne)

319-84-6319-85-7319-86-858-89-976-44^309-00-21024-57-3959-98-860- 57- 172-55-972-20-833213-65-972-54-81031-07-S50-29-372-43-553494-70-557-74-98O01-3S-212674-11-211104-26-211141-16-553469-21-912672-29-611O97-69-111096-82-5

Alph*-8HCBeia-BHCO«fu-BHCGamma-BHC (Lindarvel

HeptachiofAkJnn

Hep»c*kx Epox*deEndosutfan IOteWrin4. 4--OOEEndrinEndosutfan fl4. 4'-OOO

Endosotfan SuHate4. 4--DDT ^

Mettioxvchlor

Endrin KetooeChtortfaneTos*pf»eoeAroc(or-1016

A/ocVx-1221Aroctof-1232A/oclof-1242

A/oc*or-1248

AroCior-1254

Aroc*o»-1260

/6. o a/ f r .O fi

K.O a.- ytô «

/Ax(7 afÔlt

/4.0 «

/i. ) a.ry^t»~u.x>.o U.32x0- a

' .j33^> t^>p.o U.XXO «

r ^2,c? «- /<-£>.£> U.

JAO «

/CA^> yJUd. > U)t>O.O UI6.0.O UK6.6 UILC.O UIL6.0 U.320.0 a3*0.0 &

orW.

V. = Volume at extract infected (u(|

V = Volume o( wJter extracted (mt)

W - We*gt« ot c«mp4e extracted (g(

V * Volume at total extract <vt|

30

7/85

Qrganics Analysis Data Sheet(Page 1)

Staple Number: En 953

Laboratory Na«e: ENVIRQDYNELab Saaple ID No: B7003039Saaple Matrix: SOILData Release Authorized By:

Case No: 7351QC Report No:Contract No:Date Sample Received

Volatile Compounds


ofr^fTcon

13.7

CASHo: unkg CAS to: uofcg

74-S7-374-83-975-OH75-00-375-09-267-AH75-15-075-35H75-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5106-05-475-27-4

ChlorotethaneBroeoiethaneVinyl ChlorideOilonvthtfcHethylen* ChlorideAcetoneCarbon Bisulfide1,1-Qichloroethene1,1-Dichlxcethanetrans-t ,2-DichloroetheneChlxofori1,2-OichlorotthaneHut-none1,1,1-TrictilcrorthaneCarbon TetrachlcnbeVinyl fcttatiBroKXJichlxDKthane

•

12 U12 U12 U12 U

_ *T

6 U6 U6 U6 U6 U6U12 U6 U6 U12 U6 U

7M7-510061-02-679-OK124-4&-179-00-5

** 71-43-210061-01-5110-75-875-25-2108-10-1591-7W127-1B-4'79-34-51QB-B-3108-90-710MHKXM2-5

1, Hhdil or opr opinetrans-1 ,3-OichlxGprapeneTrichlxoetheneDibronctil oravUune1,1,2-TrichloroethaneBenzenecis-1 ,3-ftchloropropene2-Chl orcethyl vi nyl etherBroiotxi4-Hrthyl-2-pwtanane2-teirtneTetrachloraetnavl,l,2,Hetr*ddorDeth*ntTaltaneDilarabeiKtneOhylbaueneStyrewToUl lylenes

6 U6 U6 U6 U6 Utu6 U12 U6 U12 U12 U6116 U6 U6 U6U6 U6 U

•V/ul in th* MM! ••wact

CM* LMts-wit *j*«BettM( ll*4t.) TH* Imatna*.

Mf»l*>a *tt«lM^l* **«*c«i*>i tt«*t f*r Ut*

it

lB*tCB*«* •> *BtlMt*« VKlu^ TK1* <!•« t*

•rtt*r-i* but t*- r• ault i* 1*** tkwi tit* *v*ct41** *vt*e«lwt n*it kwt

•r-^rtv t»t«t !•>-• (•*. 1OJ). K UMt •* **t*ctl*n i* 1O u*J *n* •

i*n«*mrati pi. •« i •*,! i* ckic*a«tB*. i *'t •• U.

«. tt In«t

tit* *at« taar t*

Laboratory Na•e:Case No: 7351

ENVIRQDYNE ! Saaple Nuaber: EM 853


Seal volatile Compounds

Ornmarn

C o n c e n t r a t i o n : M E D I U MD a t e E x t r a c t e d / P r e p a r e d : 6-26-87Date A n a l y z e d : 7-2-87C o n c / D i l Fac tor : 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 13.7

OS to:

106-95-2111-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-67-965-85H)Ul-91-1120-83-2120-82-191-20-3106-47-887-68-359-50-791-57-677-47-488-06-295 75-491-58-7BB-74-4131-11-3208-96-899-09-2

Phenolbis-(2-Qil(rtBthyl>tther2-Chlorophenol1,3-OidiltrdMizHie1,4-ftchlirQbenztneBenzyl Motel1,2-Oichlorobenzenf2-fethylphenoll>is-(2-Qilaraisopro()yl)ether4-fethylpneralIhii tr oso-Di -n-propy lua MteaoMtraethaneNitrobenzeneI9?harone2-fctrophenol2,4-Die*thylphenalBenzole AcidbiHOUoroethatylhethane2,4-DichlTophenol1,2,4-TnchlirobenzeneNaphthalene4-(WoraaniliiwHniachl orcbutuf i cne4-Q>ltro-3-e«thyiphHwl2-Hethyl naphthaleneto achl trocycl cpentadi me2,4,6-Trichlxophenol2,4,5-Trichlo-n)Nenol2-ChloriiJaphthilin*2-MitnunilineDivthvl phthilateAcaupthyleê3-MitrDaniliiw

SPC C l e a n u p : NO -^Sep. F u n n e l E x t r a c t i o n : Y E S C j S t c i rC o n t i n . L i q . - L i q . E x t . : YES (W\ i c i r

-

23000 U2300. U23000 U23000 U23000 U23000 U23000 J23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U23000 U110000 U23000 LJ23000U23000 U23000 U23000 U23000 U23000 U23000 U23000 UZ3000LJ110000 U23000 U110000 U23000 U23000 U110000 U

CASfe:

B3-32-951-28-5100-02-7132-64-9121-14-2606-20-284-66-27005-72-3B6-73-7100-01-6534-52-1 ~86-30-t101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-69-791*94-156-55-3117-81-721S-01-9117-84-0205-99-2207-06-950-32-8 -193-39-553-70-3191-24-2

Actnaptithene2,4-OinitrqitaQl4-ntrop&enolDibenztrfifao2,4-OinitrDtoluene2,6-OinitrotolueneDivUiyl pfcthilite4-Chl(rq>nflnyl-pnenyl etherFluortM4-fctnunihne4,6-{hnitrD-2-fkthyIphenolIhiitrosodiphenylatine (1)4 Droiophenyl-phenyl rtherHkachlxcbenzenePwtathlorophtnolrnenanthmAnthraceneIh-rrbutyl phthilat*RucraRtheMPyreneftttyl-faeftzyl-phthalite3 ,3 ' -Oi chl ontetz idineBenzofalanthricencbii-(2-Ethyl hexyl) phthal ateQtryseneDi-n-ortyl phthal at*Berno (b H 1 uor utheneBcnzoOclflnranthflntBBuo(a)pyreMInderad ,2,3-dt)pyreneHi benzo(a,h) anthraceneBenzatîilperylene

•akg

23000 U110000 U110000 U23000 U23000U23000 U23COOU23000U23000U110000 Unoooou23000 LJ23000 U23000 U110000 U23000 LJ23000 U23000 U23000 U23000U23000U46000U23000U23000U23000U23000023000 U23000U23000 U23000 LJ23000U23000 U

circle one)

(U-Cannot be separated froi diphenyl aaine

FORM 1

Laboratory Name £rtt/>rv»

Case No

Concentration Low

Date Extracted 'Prepared-

Date Analyred —————— 7--7-T7


Pesticide/PCBs

(Circle One) GPC Oeanup QYes

_ Separatory Funnel Eirtraction QYes

_ Continuous Uqutd - Liquid Extraction QYes

QN

Cone /Oil Factor-

Percent Moisiure (decanted)

CASNumber

319-84-6319-85-7319-86-8

58-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-9U672-29-611O97-69-111O96-82-5

Alpha- BHC

Beia-BHCOelta-BHCGamma-BHC (Lrodane)HeptactilorAkJrm

Hepiachlor EpoxtdeEtvtoiuHan 10»e*drin4. 4--OOEErxlrmEodosuHan 114. 4'-DOOEndosulfan Sulfate

4.4--DDT

M*thoryctitof

Endrtn tCetone

ChlordaneToKjpheneArocJo<--1016

Aroclof-1221

Aroclof-1232Afoclor-1242

AfOC(eH-V248

Aroclof-1254

Arocloc-126O

iz&, o ajzo. o aIZQ,O \LIK> Wno • uv<? iL_}*O.Q UiI2A.O. U

W0 U.mo.o a.*ye a

*Jiqo.Q Uwo.o uaqo.Q (1-24n U

'13.00,0 U3<JO,0 U

IZoo.O QMGOtO (1

/P<X>,^ tJLIAOO.O U\300tO UI3GO.O U\200.0 Uaqoo.O U.j?V^>-O R

orW.

V. * Volume of extract (ut)


W = Weight oA sample extracted (gl

V * Volume of total extract (ut)

Form 1 7/85


Sample Nu«ber: EM 354

Laboratory Na»e:Lab Saiple ID No:Saaple Matrix:


Data Release Authorized By:

Case No: 7351QC Report No: JContract No:Date S*«ple Received: .Jfl-

Volatile Compounds

Concentration: LQWDate Extracted/Prepared:Date Analyzed: 6-24-B7Conc/Dil Factor: 1Percent Hoisture (not decanted) 13.6

CASMo:

74-87-374-S3-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5106-05-475-Z7-4

Oil or methaneBronAhaneVinyl Oil videDUtroethanehVthylene Oil TideAcetoneCarbon Disulfidel,HKchl(Toethenel,HHchlxoethafletrarn-1 ,2-OichlxoetheneQilorofori1,2-Dichl methane2-But2none1,1,1-TrichlxoethantCarbon TrtrachlxideVinyl AcetateBr OKXJ i di 1 or owthanc

- -

"9*9

12 U12 U12U12 U31BHT60 B ur

6 U P T C

6 Uf c U6 U6 U6 U12 U6 U61112 Ui U

CASNo:

78-B7-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-fl75-25-2108-10-1591-78-6'127-19-479-34-5109-8B-3108 0-7100-41-4100-42-5

1,2-Dichloropropanetr aw - 1 , 3-Oi chl oropr openeThchlofoetnewDi brtBDchl xtarthane1,1,2-TndilxDrthanefimzowcii-l,3-DidiloropropBie2-Qil xorthyl vi nyl etherBroBfxi4-ftethy 1 ~2~pHitanone

TetradUxoethene1,1^2-TetradilxDethaneTO!UB«ChlxotwnzBwEthylbenzemStyreneTotal lylenes

uqiq

6 U6 U6 U6 U6 U6 U6 U12 U6 U12 U iotl6 U6 U4 U6 U6 U6 U6 U

yivtf «w tart no*

Tkl« *!•« •**!(•• t*

Uwi ••• cw*«lr«« kv K/W. Mn«l

BtMr

Laboratory Na«e:Case No: 7351

ENVIRQDYNE Saaple Nunber; EN 854 •£Organic* Analysis Data Sheet-

(Page 2)

Se»ivolatile Compounds

Concentration: LOWDate Extracted/Prepared: 6-19-B7Date Analyzed: 7-2-87Conc/Di 1 Factor: 1Dercent Moisture (decanted) 13. a

CASto:

106 5-2111-44-495-57-fi541-73-1106-46-7100-51-695-50-195-48-73963B-32-*106-44-5621-64-747-72-198 5-378-59-iBB-75-5105-67-965-65-0111-91-1120-83-2120-82-191-20-3106-47-fl87-68-359-50-791-57-677-47-4BB-06-295-95-491-5B-7BB-74-4131-11-3208 96 699-09-2

Phenolhii-(2-ChlrQethyl}etha-2-aioroph«nol1,3-DichltrcbenzHw1,4-OichlarQbenzeneBmzyl Alcatel1,2-Oidilarctenzene2-hethylpnmilbis-(2-Qilxoisoprcpyl)pther4-ftpthYlpnendK-ni tr oso-fli -n-propyl ui neHecachlcrarthaneUtrriwniHWIsophcniv2Hktr (phenol2,4-DivthylphaulBenzoic Acidbi i- ( Qi 1 (Ttethm y ) Hethane2,4Hhchlxcpfiefiol1 , 2, 4-Tri chl mtem entNaphtha! etw4-ChlaroanilineHBachlorobututiene4-CM tnrS-nthvl phewl2-ftet h y 1 naphth il en BHD ach 1 orocycl opsi t ad i ene2,4,6-TrichIorophenol2,4,5-Tnchlxophenol2-ChloronaphtbaleRe2-fatrwnihneDivthyl phthalateAcenapthylene3-Witrtwiilin*

766 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 UPOOU

" 760 UPOOU760 U760 UPOOU

. F u n n e l E x t r a c t i o n : YES CjiO) < c i r c 1 e o n e )t i n . L i q . - L i q . E x t . : Y E S ( R u ) ( c i r c l e o n e )

CAS No: uqkg

83-32-951-29-5100-02-7132-64-9UH4-2606-20-2B4-66-27005-72-386-73-7100-01-6534-52-1 -86-30-6101-55-3118-74-187-86-585-01-8120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-7218-01-*117-84-0205-49-2207-08-450-32-8193-39-553-70-3191-24-2

Acenaphthene 760 U2,4-Oirutrqjrienol POO U4-tbtrophinol POO UDibenzoriran 760 U2,4-OinitrBtolune 760 U2,6-{hnitrotfllua» 1*& t'iKethyl phthalate f» J4-OUoTcpnoiyl-jwnYl etna- 760 URurene 760 U4-tttroaniliM 3700 U4,6-Oiaitrcr2-tkthylphBiol 3700 UIHutroMtiptarylaiing U) 760 U4-flroMptwnyl-piwyl ether 760 U

Pwtachlorcphwol POO U

Anthracene 760 UKirbutyl phthalatB OSr*Fluoranthew 64 Jfy«ne 69 JftrtyHwnzvl-phtlnlitf T5"'j313'-DichlcrabeniidiK 1500 UBer:oii)intfiracm* 760 Ubis-(2-€lhylhnvlifihtnaliti 390 >&" MX pj eDrysew 760 UDi-n-actyl ohthilaU 760 UBenzoibHluorantJww 57 J IBmzo(kmucrantra« 760 UBenzodlpyrene 760 Ulntara(l,2,3-alJpyrem 760 UK6enzo(a,h)anthrKm 760 U

( 1)-Cannot be separated fran diphenvlanine

FORM 1

No

Organic* Analysis Data Shoot(Page 3)

Pesticido/PCBs

Concentration: ^^X Medium

fete Extracted 'Prepared:

Date Analyzed:

(Circle One) GPC Cleanup Bv'es DNo



Cone/Oil Factor:


CAS wg/lofLNumb«r . (OfCfi

319-84-6319-85-7319-86-858-89-976-44 -63O9-OO-21024-57-3959-93-860-57-172-55-972-20-833213-65-972-54-81031-07-8SO-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-21H41-16-S53469-21-912672-29-6U097-69-111096-82-5

Alpha -BHCBew-BHCrXia-BHCGammj-BHC (Lindane)HepwchlorAldnnHepcacWor Epox*deEndosutfan 1O*e<drin4. 4--OOEEndrinEndosutfan fl4. 4'-OOOEndosuWan Suftate4. 4--ODT ^MethoKychtorEndrin (Celcx>eChkxdarveToupn«r*

Aroctef-1016A/oclof-1221Aroctw-1232Afoclof-1242

A,oc*x-1248Arockx-1254Aroc(or-126O

rg/Ko,-Cn^J

H~.0 UL/t.r>IL.O

/A«,

.- Ib'O U\b.v aib-o u.

lt>*O Uil.O. u(.

_ ?l*0 U.33.0 «.3i-0 a

* *33-0 «33.0 14J3WD tc.

r ~Zl,o U' / LO.£> u.

ji.o UILAO U

JU4.& U1&>O.O uI(.£>.O U

fc&.Q U/tA.Q UK.6.O U.32 0,6

3*O.Ouu.

orW.

V = Volume of eKtraci (ul)

V = Volume of waie* CKiracied (ml)

W * We«ght of camp4« exacted (g)

V. * VoftMTve o< tot*l CKiract MlI

I Offtt I 7/85

drganics Analysis Data Sheet(Page 1)

Saaple Nufiber: Eh 855

Laboratory Nane: ENVIRQDYNELab Saaple ID No: 870030415a«ple Matrix: SOILData Release Authorized By: _

Cast No: 7351QC Report Moi _/i[_Contract No: __jfii-Date Sample Received

Volatile Compounds

Concentration: LQHDate Extracted/Prepared:Date Analyzed: 6-25-87Conc/Dil Factor; 1Percent Moisture (not decanted)

-nnm<ma~V)m-Q

en

12.7

CASta: CASto:

74-67-374-83-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-27B-93-371-55-656-23-5108-05-475-27-4

ChloroiethaneBrcmethaneVinyl ChlorideChloroethaneto bylaw ChlorideAcetoneCarbon Bisulfide1,1-Oichl oroethene1,1-Dichloroethinetrans-1 , 2-Di chl oroetheneQilcrofori1,2-Dichloroethane2-Manane1,1,1-TricMaroethaneCarbon TetradilorideVinyl Acetatefir otodithl or Methane

-

11 U11 U111)11 U21 B*J82 B *•*",:

6 U6 U6 U6 U6 U611n u6 U6 U11 U6 t )

7B-87-510061-02-679-01-6124-48-179-00-5

r<. 7H3-210061-01-5110-75-875-25-2108-10-1591-7&-6,127-18-479-34-5108-8B-3108-9&-7100-41-4100-42-5

1,2-Oichi or opr opinetrans- 1 , 3-Oi chlxopropeneTrichloFoetheneDi broBchl oroKthane1,1,2-TrichloroethaneBenzeneci%-l,3-Dvchlarapropene2-Chl oraethyl vi ny letherBronfcri4-»tethyl-2-pentanoneHteacrv*Tetrachlaroethene1,1,2, 2-TftracMaroethafteTolueneDilorobenzemEthyl benzeneStyreneTotal Xylenes

6 U6 U4 U6 U6 U6 U6 U11 U61111 U11 U6116 U6 U6 U6 U6 U6 U

t* »J*» rwvwlt tl •WttftB

tlCl«BB>*ia

••Mr* • HI

tnttli

vltwl* kwt t*m

y**i*r uwn trt

c^«cwitr«tlBi •*

(•«, 1OJ1. 1< l lMt

nil !• calculate*

•« ••>.»' li»> !• 1O u«l


ENVIRODYNE Saaple Number


Concentration: LOWDate Extracted/Prepared: 6-19-97Date Analyzed: 7-2-87Conc/Dil Factor: 1Percent Moisture (decanted)

Seaivolatiie Compounds

6PC Cleanup : YES

12.7

CASto; uqkg

ioe-95-2lU-44-495-57-8541-73-1106-46-7100-51-695-50-195-48-739638-32-106-44-5621-64-747-72-198-95-37B-59-18B-75-5105-67-965-85-0HI-91-1120-33-2120-B2-191-20-3106-47-B87-68-359-50-791-57-677-47-488-06-295-95-491-5B-7 .flB-74-4131-11-3•VIQ 01 a4W Tfl O

99-09-2

Phenolbis-a-QUtroethyUeUwr2-Qtlorophenoll,3-ttchl(rcbenzenel,4-ttthlcro&enzmeBenzyl Alcdwl1,2-DicMorobenzene2-tethylptanalbi s- (2-Cht or oi sopr opy 1 ) et her4-ftthylphenolIKii trtwHh irpr opy 1 au MHBadilcroethaneNitrabmzentIsophormMbtroptenol2,4-OiKthylphe«lBwitnc Acidbis-CQvlorarUuiy)frthm2,4-Didilcropbawll,2,4-Trichlxti«n2mekwnthiler*4-tJll(TTHfUlir«

facichlorobutadiene4-QU tr u-3-«tlivl phmol2-tethYlnapnthilmeHex adtl xxytl opeitadi ene2,4,6-Trichloropheool2,4,5-TrichlaraphenoI2-Oilaranaphtltalene2-KitriunilineDiKthyl phthiliteAcEMpthylste3-HitroaniUne

760 U76011760 U760 U760 U760 U760 U76011760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U

__760 U3700 U760 U760 U3700 U

i . Funne l E x t r a c t i o n : YESi t i n . L i q . - L i q . E x t . : YES '

CftSta

E3-32-951-2B-5100-02-7132-64-9121-14-2606-20-294-66-27005-72-3B6-73-7100-01-6534-52-186-30-6'101-55-3118-74-1B7-96-585-01-fl120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3117-81-721B-OH117-84-0205-99-2207-06-950-32-9193-39-553-70-3191-24-2

Acenaphther*2,4-Oirutnshenol4-HitrophenoiDiberaofcran2,4-Oinitrotflluene2,6-frnitratalueneDi ethyl phthilate4-aUa-Qpfwyl-phfnyl etherFlucreoe4HhtrDiniline4 , 6-to D i trtr2-tethyl phenolH-nitroaitiphenylatitw (1)4-firotflphenyl-phenyl etherHExadilorcbcnzBiePntadilxaphcnolFteunUrentAnthraceneth-n-butyl phthalateFlucraathencPyreneButyl-beniyl-phthilate3 , 3 ' -Oi oM omwu i di neBenzo(a) anthracenebis- (2-Elhvi heryl ) phthal ateOiryseneDi-froctyl phthalateBeruoib)fluoranthencBenzo(k)nuratither«Benzoi upyreneIndeno ( 1 ,2,3-cd) pvreneOibenzouJU anthracBwBeruoiainw^lw

t o J t c i r c l e o n e )t s N p J t c i r c l e one )

760 U3700 U5700 U760 U760 U760 U760 U766 U760 U3700 U3700 U760 U760 U760 U3700 U760 U7&U

c^notTN^TRHJ

760 U760 U1500 U760 U650.W *T e^760 U760 U760 U760 U760 U760 U76£> U760 U

( l ) -Canno t be separa ted f r on d ipheny laa ine

FORM 1

Njirne

Case No

Organics Analysis Data Sh««t(Page 3)

Coocentrjtion; tow Medium

Date Extracted Prepared:

Date Analyzed:

Cone /Oil Factor:

(Grcle One)

Peslicide/PCBs

GPC Cleanup QYes ONo



-»•.;?

Percent Moisture (decanted]

CAS «g/lofbg/KjiNumber . <CircHTJne|

319-84-6319-85-7

319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-650-29-372-43-553494-70-557-74-96001-35-212674-11-211104-28-2nut. 16-553469-21-9

12672-29-611097-69-111096-82-S

Alpha -8HCBeta-BHC

D*lia-BHCGammj-BHC (Lioda ne}

HcptachiofAkJrtn

HepucMof Epo*KJeEndosulfan 1Oteldrin

4, 4' JOEEndrinEndosuHan U

4. 4'-DODEndosulfan Sutfatc4. 4 '-DOT

MethosvcWofEndrin Ketoo*CMordaneTotaphene

Aroclor-1016

A/ockK-1221A/oclo(-1232Aroclof-1242

Aroc«x-1248

AroC(<X- 1 254

Arocl<x-126O

Kr.0 Ui

/L.o nK..O U

" .'t.p Utis<? alb,C U.

/t>.o uIL.O.U^~&-Q U-.-w.o U.r?i-<? a

1 03-^ t^tfP.O £/J3^3 «

r VW «h /ta^> u

J3.& U

tL.6.0 U

J30.0 U]t>O.O UIt'0,0 U

KA.Q Wiu>.o u/ÂO U320.6 U3ZO.O It

V^ = Volume of cMrjct injected <ul|

V = Volume of waier enrj<ied <rrt<|

W = Weiflhi o< cample extracted (fll

V x Volume o< total extract (ul)

<XW.

7/85

DECEIVED SEP 1 5 1287,

uc1LJ

.12

L-*J01

.crn

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aUl — «

.^^

>• CP

i a.c --*•X

Uluc

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b "§ £ S S S - ; | ~ £ a ! S S *

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f i f i S S 1 i S « R " R>^ O -*i -t^ Ja T^ i C b 11 3 * -*» >- ifC *- < -V* Qi k. •— • •— * W *^ f*4 <+* ^^* b. c O

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i « M p i n j sUi J - £ * i j . ^ 2 ' t iE r P * I 2 _ - » vk ! - • • • • • • f • T

1 . . i K k f i i S f 1

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• l * * r t r I I L

• 1 5 i t * j • * t I t * £- s I - I c< • 1 I 1 2 1I w W * > ' C l i t * > •

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1 " a f c * | c ; : i ; r If : = 5 l l f £ d i ^ £ t f 2 t k

Organic? Analysis Data SheetiPage 1) !--

Laboratory Naae: ENVIRODVNELab Sanple ID No: B7003042Sample Matrix: SOIL .Data Release Authorized By: JlVÛl-

! S a c a l e Nusiber: Eh 8SoDL;

Case No: 7351QC Report No:Contract No: _.U.-_OJ.-.lClDate Sample Received: fc - \J2. - "&— -— - ___

Volatile Compounds

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 7-7-87Conc/Dil Factor: 3Percent Moisture (not decanted;

CASHo: uqkq CftSNo:

74-57-374-63^?75-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-Z7W3-371-55-656-23-5108-05-475-17-4

CMxoaethaneBroKaethaneVinyl ChlxideChlxoethaneMethyl ene ChlorideAcetoneCarbcn lisulhdet.Hichloroethene1,1-Dichixoethanetrans-l,2-DidilxDetheneChlxofxi1,2-Dichltroethane2-Butanone1,1,1-TrichlxocthaneCarbon TetrachlxideVinyl AcetateBroiodichlxDwthane

3 4 U34U34U34U

1600 B300B

17 U17 U17 U17 LJ17 U17 U34 U17 U17 U3 4 U17 U

7B-87-510061-02-679-01-6124-48-1

' 79-00-57H3-210061-01-5110-75-875-25-2105-10-1591-78-6127-18-479-34-5ioe-ffl-3106-90-7100-41-4100-42-5

1,2-Dichloraoropanetrans-l,3HhcnlxopropeneTrichlxoettwneDibro-Dchlxaae thanel,l,Mrichloroeth»neBenzenea j- 1 , 3-Oi chl xccropene2-ChloraethYivinvlstnerBrotcrfori4-flethyl-2-pentanone2-Hei:anoneTetrachlxorjiene1,1,2,2-Tetr.cnlxQethaneTolueneChlxobenieneEthvl benzeneStyreneTotal Xvlenes

17 U17 U17 U17 It17 U17 U17 U34017 U3 4 U3 4 U17 U17 U4 6 J

17 U17 U17 U17 U

Data Aa~«rtlnf

trw V*|UB.

B*tlMttn« • c

^••r* • 111 ri

ln«lc*tBB UHI

crltBi-l* hvt *

. Tbi« «!•« !•

itt !• !••• than tk« BB

, 1OJ>. H l l M t o< •

l !• r a lCuI* l<M. i-BBi

Tfilm *!•« t» !!••< tfw

•«•!•. It ln«tc*t«

lM •vt*ctt*n llatt >ut

lox )• 1O u«l •«• •

klanh cant Mil n*t I mr>

L a b o r a t o r y N a m e :Case No: 7351

ENVIRQDVNE Sample Number: EM


S e n i v a l a t i l e Compounds

x t r a c t e d / P r e p a r e d : 6-19-67na l y red : 7-2-67il F a c t o r : 1

Sep. Funnel E x t r a c t i o n : YESCont in. L iq.-Liq. E x t . : ¥ E 5

Olg,( (ciCÔ) *ci

t M o i s t u r e ( d e c a n t e d ) : 12

CAS No:

106-95-2111-44-495-57-6541-73-1106-46-7100-51-695-50-195-48-739636-32-9106-44-5621-64-747-72-198-95-378-59-188-75-5105-67-965-65-0111-9I-1120-B3-2I20-E-!91-20-3106-47-667-66-359-50-791-57-677-47-438-06-295-95-491-58-7 -88-74-4131-11-3206-96-699-V9-2

Phenolbis-(2-Oilxoethvl)ether2-Chloraphenol1,3-Dichlarabenzene1,4-tochlorobenzeneBenzyl Al canal1,2-Oichlorobenrene2-Methyl phenolbis- t2-ChloroisopropyU ether4-flethylpnenolU-ni tr Dso-Di -n-propyl ail neteadiloroethaneNitrobenzeneIsaphorone2-fetrophenol2, 4-Oiiethyl phenolBen; OK Acidbis-(QUoraethaxyiNetMne2,4-Oichloropnenol1,2,4-TnchlorooenzeneNaphthalene*-Gil oraam lineHBichlorobutauiene4-Oii arQ-3-*ethyl phenol2-tethvlnaphtnileneHer adil arocyc 1 apentad; sne2,4,trTrichlorQphenc:2.4,j-TnchlxDphenol

-2-Diloronapnthalene2-fctroinihne&iKtnvl phthalateAcenapthvime3-Nitroinihne

uqkq

750 U750U750U756U750U750 U750U750U750U750 U750U750U750U750U750U750U3600 U750U750U750U750U750U750 U750 U750 U750 U750 U3600 U750U3600U750U750 U3600U

CAS fe:

83-32-51-2B-5100-02-7132-64-9121-14-2606-20-284-*6-27005-72-386-73-7100-01 -b534-52-1,86-30-6101-55-3118-74-187-86-585-01-6120-12-784-74-220e-44-0.129-00-085-66-791-94-156-55-3117-81-7216-01-9117-84-0205-99-2207-06-950-32-6193-39-553-7<>3191-24-2

Acenaphthene2,4-Oirutrophenol4-tbtroghenolDibenzoturan2,4-Oinitrotoluene2,HHnitrotolueneDi ethyl phthilite4-Oilorophwvl-phenyl etherFlLDTHie

4-Nitroaniline4, 6-Oi ni tro*2-ftthy 1 phenolK-nitrosodipnenvlatine (1)4-froiDphenyl-phenyl rtherHexachlTobenzenerWtachlorophenolPhenanthreneAnthraceneDi-rHwtyl phttelateFluor ant henePvreneButyl -ben:yl-phthal ate3, 3 ' -Oi chi or obenz i m neBenzou) anthracenebis-(2-Ethvif«rvliphtnali:eChryseneDi-n-octyl phtnalateBefi:o(b)fluorantheneBenzolkHlutrandiene&cn;o(UpyrenelnoencU,2,3-cfl)DvreneDibenzota.h) anthraceneBer,;cigni)pff\'iene

uqkq

750U3600 03600U750 U750U750U750U750U750U3600U3600U750 U750U75&U3600U750U750 U .

< lfaC^/Sull750U750 U1500 U750U250 «f750U75u U750U750 U750 U75C' U750 U750 U

(1^-Cannct be separated from a i p h e n v l a m i n e

FORM 1

M

Case No *

AC-- -

Organics Analysis Data Shoot(Page 3)

S*mpf« tyurn b*f

<£Concentration: ( low.) Medium

Date Extracted'Prepared;

Date Analysed: ______

Pasticide/PCBsS* • ' " ^"~S

(Circle One) GPC Cleanup OJres ONo ,,.,*'

____ Separatory Funnel Extraction QYes

___ Continuous Uqu*d - Liquid Extraction QYes

Cooc/Dif Factor:


CAS uq/lofJL/g/Kg,Numb*f . (GrcfiTJoe)

319-04.6319-85-7319-86-858-89-976-44 -a309-00-21024-57-3959-98-860-57-172-55-91

72-20-833213-55-972-54-81031-07-850-29-372-43-553494.70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6

11097-69-111O96-82-S

Alpha -8HC

Beu-BHC

Oefta-BHCGamma-BHC (Li«xJan«|HeptJChlOr

AkJrtn

McpiacWor £po«»dcEndosulfan 1

Oieldrin

4. 4*-ODEEndrinEndosutfan (14. 4*-ODOEftdosuifan SuHaie4. 4 '-DOTM«thOKVCtilorErtdnn <eiooeO(ordan«Toupheo*Arocfor-1016

A/oclOf-1221A/oclor-1232ArocIor-1242

AfOchx-1248Aroc(0f-1254

AroC«X-126Q

/4.0 W/ f c .O MIt.O iL

-•• ll*c Uh.c (J./Lt U.

tt>,0 Url.O ^Q-d u-.sa.o M.fisC a

' *3a.o «^ _A?.O ^.32,0 W

3:. «^tO,£> U

-?.?.o «/fcAO W

JU .<5 U

/&£>.£> W/^^.^ i/&A.6 U/U>.& U

/ .<? Uj.a0.0 ^/3^^.^> W

orW.

V. £ Volume of einraa (o(J

V = Volume of waier CKlraoed (mlj

o<

V. * Volume of total extract (ul|

(gl

Form 1 7/85

Qrganics Analysis Data SheetiPage. 1 >

Sample Nuaber: EM B57

Laboratory Naae: ENVIRQDYNELab Simple ID No: 87003043Saaple Matrix: SOILData Release Authorized By:

Case No: 7351QC Report No:Contract No: __kS-rDate Staple Received

Volatile Coapounds

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 6-24-67Conc/Dil Factor: 1Percent Moisture (not decanted): 12.7

CA5 uqkg CflSNo:

74-67-374-33-475-OH75-00-375-0 -267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-27B-93-371-55-Q56-23-5106-05-475-27-4

Chl or MethaneBroKMethaneVinyl ChlorideOil a- oe thaneHethylene ChlorideAcetoneCarbon Disulfidc1,1-Cichlaroethenel,l-0i:hloroetnanetrans-l,2-fcchloroetheneChlorotxil,2-&ichloroethane2-Butanone1,1,1-Trichltraethan*Carbon TetrachlorideVinyl AcetateBrotod i ch I or oiethane

11 U11 U11 U11 U350 B200 B

6 U6 U6 U6 U6 U6Un u6 Ut u11 U6 U

7B-67-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-75-975-25-2106-10-1591-78-6-127-18-479-34-5106-88-3106-90-710CM1-4100-42-5

l,Hhd)l(ri*n,»etrans-1 ,3-Di chi DropropeneTridilorDetlw*DibroBochl oroiethane1.1,2-TridilarorthaneBenzenecis-l,3-i)ichlorapropene2-Oil or aethy 1 vi nv 1 etherBnwrfori4-hWiyl-2-pent*wne2-Hei anoneTetrachloraettiBifi1,1,2,2-TetrathlToethineTolueneChlorobenzeneEthylberaeneStyreneTotal Xvlenes

6 U6 U6 U6U6 Uc L Jo U11 Uo 'J11 uIt U& Uf*-

LJJ.6 U

6 Uo U6 U

I* ttt* r««ttJt l« a vaku* arMtvr than

llatt. r>B«rt Uw valta*.

U laf.

lwt UMt . )

Halt for tit*

«. It

tit* *

tMIMr *!•••

UM r»mlt».

I ank a* ••! 1 a* a

lwi t» IO u«l

Organics Analysis Data Sheet(Page U :-

Number: EM 857DL

Laboratory Na«e: ENVIRQDVNELab Sanple ID No: 87003043Saaple Matrix: SOILData Release Authorized By: JVJ

Case No: 73S1DC Report No:Contract No:Date Saaple Received: _jL?_-_

JL3J

Volatile Conpounds


cs

CASHo: UOkQ CASNo: ugkg

74-87-374-S3-975-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-27-4

ChloroKthaneBrojKwethaneVinyl ChlxideQilxoethaneMettiyleoe ChlorideftcetoneCarbon Bisulfide1,1-Oichloroetlwnel,H)khloroethinetrafts-l,2-DidilcroetheneOil or of or i1,2-Oichloroethane2-Butanone1,1,1-TrichlaraethaneCarbon TptnchlorideVinyl AcetateBroaodichl or Methane

57U57 U57U57 U

1600 B340 B

29U29U29U29U29U29U57U29U29U57 U29U

- -

7B-87-510061-02-679-01-6124-48-179-00-571-43-210061-01-5110-TH75-5-2106-10-1591-78-4.127-18-479-34-5108-ffi-3108-90-7100-41-410CM2-5

1,2-Oichloroorooanttran5-l ,3-DidiloropropeneTnchloroetheneDi bronchi Dnvthane1,1,2-TnctiloroethaiieBenienecis-li3Hhchlxopropene2-Di 1 or otthy 1 vi ny 1 etherBrcwfori4-rtethyl-2-oentanone2-HKafloneTetrachloroethene1,1,2,2-TttriCtiloroettianeTolueneChlTD6en:en«Ethyl benieneStvreneTotal Xylenes

29U29U29U29U29U29U29U57 LJ29U57 U57U29U29LJ7 f t

29U29U2 9 U29U

VMJJKl

I* tlk« »••-• tlw l««"tltltl

tictaw>-tci

»<!<•••« hv K/r«

In klMik •• veil M •

«« ••* •*

Laboratory N a m e :Case No: 7351

ENVIRODYNE Sample N u m b e r : EM 657 Up

O r g a n i c s A n a l y s i s Data Sheet(Page 2)

C o n c e n t r a t e on: LOWDateDateC o n e / D i 1Percent

S e m i v o l a t i l a Compounds

GPC Cleanup : YESx t r a c t e d / P r e p a r e d : a-19-67n a l v z e d : 7-2-87il Fac to r : 1t Moisture ^decan ted ) : 12

CASNo:

lCfr -2111-44-495-57-8541-73-1106-46-7100-51-495-50-195-48-73963B-32-910d-44-5621-o4-767-72-198-95-378-59-186-75-5105-67-965-85-0111-91-1120-B3-2120-82-191-20-3106-47-887-66-3S-50-791-57-077-47-4BB-Oo-295-95-491-58-788-74-4131-11-3208-?o-699-09-1

Phenolbia-(2-Chlxoethvliether2-ailorophenol1,3-Dichlarawnzen*l,4-Dichlxoben:eneBvzvl Mcoholl,2-0ichlxoben;ene2-«ethylphBwlbis-(2-ChloroisopropyU ether4-Hethyl phenolH-ni troso-Oi -n-pr opyl an netetachlxoethaneNitrobenzeneIsopnarone2-Nitrophenol2, 4-DiKthyl PhenolBen: 01 c Acidbis-itJlxoethtttvlMethane2,4-DicMorophenoll,2,4-Trichlxoben:eneNaphthalene4-OilxoanihneHeiictilcrobutadiene4-Chlxa-3-*ethti crenel2-fletnylniotith4ierEHex achl xocycl opentadi ene2,4,6-TnchixD()hefiol2,4,5-Trichlxophenol2-OilorDn4ohthilene "2-+*itrtianiIineDiKthvl ph-.r.iUtEAcenapthylene3-Nitroamhne

. 7

+9

760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U760 U3700 U760 U760 U760 U760 U760 U760 U760 U760 U766 U760 U3700 U

- 760 U3700 U760 U760 U3700 b

Sep. Funnel E x t r a c t i o n : VE5Contin. Liq.-Liq. Ext. : >EB

CAB to:

83-32-951-28-5100-02-7132-64-9121-14-2406-20-284-66-27005-72-386-73-7100-01 -ft534-52-1,86-30-6101-55-3118-74-187-86-585-01-8120-12-7B4-74-2206-44-0129-OOHJ85-bB-791-94-156-55-31 17-81-721B-01-9117-84-0205-99-2207-06-5

- -50-32-8193-39-553-70-"191-24-2

Ateruphthene2,4-Oinitropnenol4-fttroehenolDibenzoturan2,4-Oinitrotoluene2,6-OinitrotDlueneDi ethyl phthalate4-Oiltrnphenyl-phenyl etherFluor ene4-Nitroanihr*4,6-Ihnitrcr2-flEthylphenolM-nitrosodiphenylaiane (1)4-firoiOQhenyl-phenvl etherHexactilorobenzenePentidilcrophenolPtcntfithreneflnthraceneDi-fHxitvl phthalate (Fluor an thenePyrsneButvl -benzyl -phthilate3,3'-thchlaroDeruiiline.BenzDU) anthracenebis-(2-€thvlhwYl 'phthalateChryseneDi-ft-octvl phthalateBenzot b)Uuoran:heneBemoik; fluoranthene

- - &en:oi*)pyren*-Indeooil,2,3-cdjpvreneEribeniDii.hj anthraceneBenzcighi'ijervlene

MO (c i rNO (cir

^0

76011POOU3700 U760 U760 U760 U760 U766 U760 U3700 U3700 U760 U760 U760 U3700 U760 U

^\^ 2300 J• THHT

760 U760 U1500 U760 U370 J 57oO U760 U7&OL760 li760 U7tt; U760 U760 U

(It-Cannot be separated f r o m d i p h e n v l a m i n e

FORM 1

Ljoof jtorv

No

4 AC-* -

Concentration. ( LowJ Medium

Date Ejaracied'Prepared: ____^6~f

Oate Analyzed ______i /_•"/" T7

Organtcs Analysis Data Shoat<Page 3)

Pesticide/PCBs

(Circle OneJ GPC Cleanup GJYes ONo

___ Separatory Funnel Extraction

___ Continuous Liquid - Liquid Extraction OYes -oCone/Oil Faaor:

Percent Moisture (decanted) 12,7

CAS og/l o<f*g/K^Numt>«r . (CirtrfclJn*]

319-84-6319-85-7319-86-858-89-976^4-6309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-850-29-372-43-553494-70557-74-9

8001-35-212674-U-2111CW-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

A(oha-BHC

8eu-8HC

Delia- 8 HCGarnmj-BHC (LtndjrteJ

H«trtachlorAkJr.n

Heptacnicx Epox*deEndosuffan 1

0»eMrin

4. 4--OOE

EndrinEnbosuHan fl

4. 4--DDOEndosw^fan SuHaie

4. 4 '-DOTM«rhoK>chloc

Endftn Keion*ChtortUne

ToKapher>eX^rockx-1016A/oclo^-1221A/ock>f-1232Aroclcx-1242

A/odcK-1248Aroc(cx-125'»Aroc(tx-126O

^.£> 6t/t.rt /i/t.o tc

-- ALc a.It*: a

\h,» «./t.o «._/i,^)-K.Ji,» U-33.0 U

. -c* a* ^s^-o n

33.0 143S-0 t<

5t-.-c K' IL0.0 U

J3.0 U

It, 6.0 UXJO.& U

}&>0. 0 UIL&.O U&6.G Uiu>.o u/&6.O U330.6 a3*0. 0 IL

V^ = Volume of eruaa mj«ne<J (ulj

V = Volume of water eKiracird (ml)

W - Weight of t*m0<e enracied (gt

V( * Volume of t«*( ectract (ul|

7/85

Grganics Analysis Data SheetiPage 1)

Saftple Number: EM 356

Laboratory Na«e: ENVIRQDYNELab Sample ID No: B7003044Saaple Matrix: SOILData Release Authorized By: _

Case No: 7351QC Report No:Contract No: .I]aSr_PJ-.nZ>_i.l.Date Sample Received: __Le.~-.

-TV-nrn

Volatile Conpounds

Concentratlon: LOWDate Extracted/Prepared:Date Analyzed: 6-24-37Conc/Dil Factor: 1Percent Moisture (not decanted 1 1 , c

COm-o

CAB ft: ugrg CftSto:

74-67-374-83^?75-01-475-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-278-93-371-55-656-23-5108-05-475-Z7-4

CM or MethaneBroKMetnaneVinyl ChlxideChlxoethaniItethylene ChlorideftcetoneCarbon Bisulfide1,1-OidilxoBthenel,Hhchlxoettijnetrans-l,2-DichlxoethcneChlxofxi1,2-tochlxoethane2-Butanone1,1,1-TrichlxoethaneCarbon TetrathlorideVinyl AcetateBr Modi chlor Methane

11 U11 U11 U11 U300 B190 B

6 U6 U6 U6 U6 U6 U11 U6 U6 U11 U6 U

- -

78-67-510061-02-679-01-6124-48-179-00-571-4J-210061-01-5110-75-G75-25-2108-10-1591-78-6-127-18-479-34-5ioe-ffl-3ioe-w-7100-41-4100-42-5

1,2-Oichloropropanetrans-1 ,3-&ichlxopropeneTrichlocoethen*Dibronchlxoa«thane1,1^2-TrichlxoethaneBenzenecis-t ,3-Dichlxopropene2-QUon»UiylYinvletherBTCWOITI4-hBthyl-2-oaitanone24triACfi(Tetrachlxorthenei,l,2,2-TrtrachloroethaniTolueneChlxobenzeneEthvloenzeneStyreneTotal Xylenes

6 U6 U6 U6 U6 U6 U6U11 U6 U11 U11 U6 UULLLi

6 U6116 U

If tn* r*mult im • VK!UB ^rm»tmr tttvi v mmitml t* t»w »«t»cliwi TDIB «!•« a**!!** (• t** p>r>aMBr* Mar* tx*

tn tN* final •« tract •M«iU

«n*ir»»* fv kut n«t Mtactv*. ^Mi

MfiOka ••^•cttvn Uut far !*• aaa«l« -ttti ttt* U tva.lOU)

•n naw:a<iar^ nncvnt. /«» lutlan art. 1 an.

Ui« ln«tru«ant ••tactlon Matt.) Th» *

OeaapOkn* na* an*lvia^ far but

•tniaHB attMna*t* MKKttv* Halt far til*

Jl

Tut* «l«a I

aaawla. It

awn* tit* a

an^lyt* 1* ««M In klwik M n*l I

Mriar «!««• an* fa*tra«*« a«v •• r»«uirMI (• arawly «

th» raaulta. If i.iaaa . tNav auat a* fully •••cftfca* an*

eomttratlan

ttarl* »vt tha> ravult la )•«• tHan tn*

a*tar Cn«n lava !«a, IOJ). If HMt •«

tnv l«antlflc*tl«n

a* *a«actlan Halt kwt

lof I* 1O t^l and •

Grganics Analysis Data Sheet(Page 1) !--

Sanple Number: EM BSBDL

Laboratory Mane: ENVIRQDYNELab Saiple ID No: 87003044Saaple Matrix: SOILData Release Authorized By: _IYlC.Ui

Case No: 7351QC Report Nor _i3.JContract Not __(^?_rDate Saaple Received: __ia-.

Volatile Compounds

Concentration: LOWDate Extracted/Prepared:Date Analysed; 7-7-87Conc/Dil Factor: 5Percent Moisture (not decanted):

i

11.6

CASNo: ugfcg CASNo:

74-07-374-83-975-OH75-00-375-09-267-64-175-15-075-35-475-34-3156-60-567-66-3107-06-276-93-371-55-656-23-5108-05-*75-27-4

ChloroKthaneBroraettaneVinyl DilorideOil xoe thaneHethvlwe ChlorideAcetoneCarbon Bisulfide1,1-Oichlorocthene1,1-Dichloroethanetrans-1 ,2-DichlaroetheneChlorofori1,2-Oichlaroethjne2-ButanoneM.HridilxaethaMCarbcn Tetr .chlorideVinyl fcetite&-D4wn:Mcr at* thine

571157 U57U57U

1100 B150 &

28 U23 U26 U2 8 U28 U2 S U57U2 8 U28U57U2 8 U

78-67-510061-02-479-01-6124-48-179-00-571-43-210061-01-5110-75-875-25-2108-10-1591-78-0127-18-4 -79-34-5108-88-3108-90-7100-41-4100-42-5

1,2-Oicnloropropwetrans-l,3-DidiIir[j)rcp€neTridiloroethewDibroiDchloroaethane1,1,2-TridilGTorthaneBenzenecis-l,3-OichlorDprop«ie2-Chl xoethyl « nyl etherErurixi4-flethyl -2-pentanonB2-HKjnoneTetrachlxoethene1,1,2,2-TetradUoroethaneToluswChlorobenzeneEthyltHTceneStyrweTotal Wires

28 U28 U28 LJ29 U28U28 L)26 U5 7 U2 6 U5 7 U57U23 U2 8 U8 W

2 8 U28U28 U28 U

If tM

HMt,

••/ul in th» final •• tract

fla« I* iiMtf •!»•« «««ly<« IB «•»»»• In »lw>k •• ••! 1 4*

>•. It trMICBt** •*••.!>l»/^-••••la blank cwtMiMtlan

aa> «n B*tlMit«« -ralu*. Thl» flM '» u**^ Hthar iri««ft

t.tan »»r- tantatlrvly I«w>tl4laa1 caawaun**

•fur* • 111 •'•••ana^ 1m Hi n i« V ultan tit* aaaa apaMtral ««t.a

IntflCBt** IX* pi iia.K.» *f • i IBM mi I Wv*« •••*• tfw l*ontlflc«tl«n

crltarla but t*» raw.)* t* !«•>• than ttw BavclflM avtactlvn llMt but

tr*a.tar tNar. iar-« laaj, lOJi. If Hut *f «rt.actlBn la 1O ka|l am a

cwteantratlBH a* 3 ual I* caleulvtM, rvwart » W.

OUt«r flat* MM «••*(•*«•• *w •• f*aulr*« t* *r«a«rly

th* r«*Kt)t*. I* waaM, tfvy au»t »• fully •••tribal an

•*«:rl»tl«B attachari tv tlv* «at* MaMMry raawt.

Labor atory Name:Case No: 735 1

ENVIRQDYNE Sanp 1 e Number EM 956 rrt


S e f i i v o l a t i l e Com pounds

C o n c e n t r a t i o n : L O WDate E x t r a c t e d / P r e p a r e d : b-19-87D a t e A n a l y z e d : 7-2-6"C o n c / D i l Fac tor : 1P e r c e n t M o i s t u r e ( d e c a n t e d ; : 11

CASNo:

108-95-211 1-44-495-57-8541-73-1106-46-7100-51-095-50-195-48-739638-32-9106-44-5621-64-767-72-198-95-378-59-188-75-5105-07-9o5-65H>111-91-1120-83-2120-32-191-20-3100-47-887-66-359-50-791-57 -B77-47-486-Oc-295-95-4

— —91-56-7 -88-74-4131-11-320S-96-B99-09-2

Phenolbis-(2-Qiloroethyl)ether2-Dilorophenoll,3-0ichlxafaen:ene1.4-Dictiloroben;eneBenzyl Alcohol1,2-Dictilorabenzent2-tethyl phenolbis-(2-ailoroisoprDpyl)ether4-ttethvlphenolH-ni trreo-Di -n-pr apylui tieHeachloraethane(btrobenreneIsophorone2-Hitrophenol2,4-OitethyiphenclBen: OK Acidbis-Oiltrwthosyihethane2,4-Dichlorcphenoll,2,4-Tridiloraben;eneKapnthalene4-GUoroanilinEHeiacMorooutadiene4-Chl oro-3-iet.hvl phenol2-ttethvl naphthaleneHexacMorocycloDentadiene2,4,6-Trichlorophenol2,4,5-Tnchlcropnenol

-2-Qiloronaphthalene -2-KitroafiihneDiKthyl phtnalateftcenjpthylene3-Nitroanihne

.6

^

750U750U750U750U750U750U750U750U750U750U750U750LJ750U750U750U750U3600U750U750 U750U750U

. 750U750U75-) U750U750 U750U3600U

_ 750U3600U750U750U3600U

6PC C l e a n u p : YE5Sep. F u n n e l E x t r a c t i o n : Y E 5 {C o n t i n . L i q . - L i q . E x t . : Y E S

CASfc:

83-32 ?51-2B-5100-02-7132-64-9121-14-2606-20-264-66-27005-72-386-73-7100-01-6534-52-1fc-30-o'101-55-3118-74-187-66-585-01-3120-12-784-74-2206-44-0129-OCH;85-6B-791-94-i56-55-3117-81-7216-01-9117-fl4-.j205-99-2207-«'*-T50-32-8193-39-553-70-3191-24-2

Acenaphthene2,4-&initrophenol4-totrophenolDibenzoturan2,4-OinitrDtoluene2,6-OinitrotolueneDiethyl phttalate4-Oiloropnenyl-pnenyl etherRuorene4-*btroanihne4,6-fonitro-2-ftetnylphenolH-nitrosodiphenvlaune (1)4-&roiophenvi-phenyl etherfatachlarabenzenePentachlorophenolPteianthreneAnthraceneDi-n-butyl ohtnaliteFluor jnthenePyreneflutyl-fcnzvl-phthilitf "3,3 -OiduxoberuidineBenzoia) anthracenebii-{2-ElhvlhovlionthilateQiryseneIri-n-ortyi phtnalatetei:o(bJfiuorantheneBeniotkjiluorsrtneneBenzotatpvreneInoern U , 2 , 3-cdi pyreneDibenzDia.hlanthraceneBenzoiortiiDerYiene

\f

N£ ( c i r c l e o n e ;\»^ (C i re 1 e one i

unkq

750U3600U3600U75011750 U750U750 I)750U750 U360u U3600 U750U750U750U3600U750 U750 UIfo750 u750 U750U1500 U750 U4% W U3" pj^750 u750 LJ750 U75u U750 U750U750U750 U

(li-Cannot be s e p a r a t e d rrom d i p n e n y l a m i n e

FORM 1

Name S*mp4« tyurntxai

rM Try

Concentration; ( LowJ Mediumi

Date Extracted'Prepared:

Date Analyzed: _____

Conc/Oil Factor: _____


Pesticide/PCBs(Circle One| GPC Cleanup fSres ONo

___ Separatory Funnel Extraction

___ Continuous Liquid - Liquid Extraction QYes


CAS «g/l<Kt»g/K^Number . (CircKTjnel

319-84-6319-85-7319-86-858-69-976-44-6309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-54-81031-07-650-29-372-43-553494-70-S57-74-96001-35-212674.11-211104-26-211141.16-553469-21-912672-29-611097-69-1l 1096-82-5

Alpha -8HCB«ta-BHCDelia-BHCGamma-BHC (LindanelHe0**chl<x

AkJrm

Heptachfor £pOK*deEocJosulfan |

Otefdrtn

4.4'-OOEEnoVinEndosuMan (I4. 4'-DOOEndosuifan SwHaie4. 4'-ODT *

M«ttxiKvchI<xEndrin (CeioncChkxtlarx

Tocaphen«Aroc(<x-1016

A/oc(of-1221Arocloc-1232Aroclor-1242

A/odcx-1246

Aroc«x-1254

AfocKx-1260

!<*.0 U.1(>.O ILIC..O U

- H,& a16<o a.1^0 W-tL*O Uit,.O K_Q-fi'-U.33.0 U3z,o a

' »J3^ U>P.O l<

Jp^ t<"%-^C3 M/to.;? Ujyj.^? «11,0.0 UJ30.& U

;6<3.<5 UIt-0.0 U&6.0 Ul&c.o uM6.O Ujji>.o a310.O VL

r>m. -• o

oom-o

V( = Volume of enracr injected (u<|

V - Volume of water extracted (m(|

W - Weight o* «mp*e extracted (gj

V * Volume ot total extract (ul)

Focm 1 7/85

Contractor: (TtJ Vl fit)~

TENTATIVELY I D E N T I F I E D COMPOUNDS tgMATCH ASSESSMENT

enNOTi: Reviewer should note directly on Organic Analysis Data Sheet (QACS) —

those matches that 1n his op in ion (based on contract cri teria) are counreasonable .

CP.ITE31A

(1) Relative intensities of major Ions (>10-) reference spectrumshould be present 1n the sample spectrum.

(2) Relative intensities of major ions In sample spectrum shouldagree to within +_ 201 of reference spectrum întensities.

(3) Molecular ions present in reference spectrum should be present1n sample spectrum.

(4) Ions present in sample spectrum, but not in reference spectrumshould be reviewed for possible background contamination orpresence of coeluting interferences.

(5) Ions present in reference spectrum, but not in the samplespectrum should be reviewed for possible subtraction from thesample spectrum because of background contamination or coelut-ing interferences.

(5) If, in the reviewer's opinion, no valid identification canbe made the compound should be labelled as "unknown" and theinitials and date of the reviewer placed on the OAOS.

Analysis Data Sheet(Page 4)

Tantativoly Idontifiod Cofnpounds•A)&O

CAS

2.

3.

S.

7.

e>.t.

2...

17.

J8.

iO

-o

? 8S

No



CASCompound

"feu/v~T(/0 3

6.

7.

9.

10.

11.

12.13.

14.

15.

16.

17.

18.

20.

~ V

510.3

U U O3^0-3

GarbOO (-7-63603

•Lud-roQXLrb&n3-1

£±LA5_Z :nox

1*

MM

27.

28.

30.

? 8S

No: ^ \

£ K) VJ 1 Analysis Data Sheet(Page 4)

Tentatively ldonttf*«d Compounds

I EL

- %CAS

Compoond F» action Concentration(wg/l

,2-io-c 5

i:: 35C5403

no9. I'M

MUCLTII.

13.. lud rocar hxc

17.

18. tore dGL r b c o

0 l l 35.2 Moo1/64

I. P»n 6 7 8S

No-

Organic* Analyns Data Sheet(Page 4)


CASCompound N*m«

(wg/l

-FuAOLnetrvg t d'llL^dm-•*^ I ft A *

. 2.. 3

I7

10.

11.

13.1*.

17.

r8-Its.20.

(21.

23.24.25.

26.

27.

26.

29.

IS. 3 USO 3

IS- 2.id vr) o a. r t>6-uû

UW d rri (i/i rhvrv .

rbc xi 3-1- -7

a*1-7 (TOT

IMCTD

XxIA j

f o«n I.P»n B 7 85

No:

£N 01 £6t>V IsJG- Organic* Analysis Data Sheet(Page 4)

Tentatively td«ntifi«d CompoundsXJmommac/>m•o

f <xm 1. P*n 6 ? 8S

VrtM

GASNumb**'

*

13.

1*.

15.

16.

19-

, I

27..

29..

30..

P-OD V^J£Pr9anics Analysis Data Sheet(Page 4)


•Compound Fraction

A/M.

RTocScwiConcentration

(vg/lor wg/kg|

X)•Tlom

aCf>

CO"

1. Pan 6 7 85

•*e No:


T«nCativ«ly ld«ntifi«d Compounds s«=*«

1.2.

3.

BtoA -7.S.0

not)3^03

IS-S

7..

. e.,

! 9--

111..il2..

13..

15..

16..

8..

in.b

0>(03\lCro

5903-CA

1'

fbrm H 3303

^^ JIM

27.,

26..

3O..

fcxm \ 85

Organics Analysis Oata Sheet(Page 4)

Tenlativoly Identified Compounds

-umo

oCO

en

30

FO*«» 1. Pan 6 7 8S

:-sc NO:

Organlcs Analysis Data Sheet(Page 4)


Cocnpouod

t 3t-i> 3

H.S M 5C 3'5.2. t ^MC

.r btrw

1O.,

II..12..

S-I.-1CCLrbfv.

. 1

16.

17.

20.

21.

7.4.

zs.26.

Z7.

28.

1^03rt

rhr*

ûdt Sc-2 SHCJ

form I. Pan B 8S

DECEIVED SEP > 5

o£w«w«o ^

~£>c3

ctt0)

\r,cT|r5 o« Z\ *\i

• '

W^

i.1*•**eo•3>s«c«K

,.ISJ « s

IIu* 5 "0 ?

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Sc*

«N

wm

b«f

C

.!Sii

fZ

CA

SN

umbe

r

•£Ci

C

<:<^CA

Cic

•

*^

• t1 r•» ir tjri f» tD 0r. <3 »- f

-

-J 1

•»k****

t *

,<f.

t VJf) M

*

j r* 0a r 1 *• r4 r

ii

t «J V ut r a CI Q

ari

No


Tentatively Identified Compounds on}

1CASNomb*< Cofnpoond Nam*

, - ^MVCI 2.———————

i::

,26..» 27..

IB..

I!3

If . vWEatemnoic lacu

n

L ocxd ,^3'-Ud^bis-^

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HOC 3

n.i MMC1- 2.

I. Pan 6 ? 85

S9

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'62

•81

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'SI•9)

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Organic* Analysts Data Sheet(Page 4)

CAS

*

9.1O.

1.,12...

13..

IS..

"6..

18..

:O..

/3.24.

26.

T7.

:e.

Ito.


rr.r-n

rbev*cv-

6

Fraction NwmtMf

ILi

(1.0

so.So -335.2

Ct(«m*t*d

iIE.? 6

^700 T

-noCI

7 8S

S8

•V '

"Of

"6!

::::i'SZ

'c:

'Oc

'61

'81

;:i•5

1 L

'O

svo

I1

ecology and environment, inc.111 WEST JACKSON BLVD., CHICAGO. ILLINOIS 60604, TEL. 312-663-9415


Date Received for Review

From: Zena Gold-KaulxanSubject: MOD

PAHtltO/*//


Case # IISample Description _____

Organics (VOA, ABN, Pest/PCB)

Low SoilO*Low WaterDrinking WaterOther



•Project Data Status Completed!



- beiûr C£DL

Book No-

Compounds were detected in sample(s); see enclosed ChemicalEvaluation Form.

Page No.

K ecology and environment, inc.CHICAGO, ILLINOIS

CHEMICAL EVALUATION FORM

DATE:

CASE

TOX/PERS

735") UNITS' REVIEWER:

COMPOUND CRDL 3-SxCRDLE/M

10Chfusenfe 530

5 •CTss

Oi-n-cc&j' 330

DATE:

SUBJECT

FROM:

TO:


/<

Review of Region V CLP DataReceived for Review on

Curtis Ross, Director (5SCRL)Central Regional Laboratory

Data User: P ^ T/

<<\

Vo

tP

We have reviewed the data for the following case (s ) .

SITE NAME: /-Pn£.£"%H

EPA Data Set No.

CRL No.

No. ofSamples: Q

SMO case No.TLU. /ActivityNumbers

SMO Traff ic No.

CLP Laboratory: '' ôk^/ôeHrs. Requiredfor Review: 6

Following are our findingsfT^

Data are acceptable for use.( ) Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory{ ) Data are unacceptable.

... — -cc: Du'ane Geuder, "Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas

EPA FORM 1320-6 (Rev. 5/87)

CASE I

\UNITED STATES ENVIRONMENTAL PROTECTION AGENCY REGION V

CALIBRATION OUTLIERSVOLATILE HSL COMPOUNDS

' ' - - CONTRACTOR

DATE/TIME:

Chl oromethaneBromomethaneVinyl ChlorideChloroethaneMethyl ene ChlorideAcetoneCarbon Dlsulfide1,1-Dichloroethane1,1-DichloroetheneTrans-1, 2-Oi chl oroethenerhloroform,-Butanone1,2-Di Chloroethane1,1,1-Tri ChloroethaneCarbon TetrachlorideVinyl AcetateBromodi chl oromethane1,2-DichloropropaneTrans-1 ,3-DichloropropeneTrichloroetheneDi bromoch 1 oromethane1,1,2-Tri ChloroethaneBenzenecis-l,3-0ichloropropene2-Chloroethyl vinyl etherBromoform4-Methy 1 -2-Pentanone2-Hexanoneetrachloroethene

1,1,2,2-Tetrachloroethane'tolueneChlorobenzeneEthylbenzeneStyrenem-Xyleneo/p-Xylene

AFFECTEDSAMPLES:

nit. Cal.-/^"-Jf7F

•

1RSD

70(o%

*

JJ"

&L lAtotLe*

*ont • Cal .£ Sf'£7 /?:V5*

*F *0

yo313?

*

J3-J-

££M&<a&

<£M%d

Cont. Cal .-J6-ST /7:7«

RF to

¥/¥o

*

crJ

e^fî-f^ttLf

Cont. Cal.-jt-/7 //t:rr

RF ID

5^

/oi"/

^?^

^7?

*

CT

JJ

T

J

€>f8"66

Cont. OLlj.(<\

RF *D *ô ^— V 5\ *

— - c<

"âc°.

These flags should beTppHed to the analytes orTthe sample data'sheets.""1----;

1/87

CASE? 7 3 57



CONTRACTOR

••.DATE/TIME:

Phenolbisl-Z-ChloPoetnyl )Ether2-ChloPOohenol1 ,3-Oi chl orobenzene1 ,4-01 en 1 orobenzeneBenzyl Alcohol1,2-01 chl orobenzene2-Metnylphenolbis(2-chloro1sooropyl }Ether4-MethylphenolN-Nitroso-Di-n-?POpylamineHexachloroethaneNitrobenzeneIsoohorone2-Nitroohenol2,4-OimethylphenolBenzole Acidbi s( 2-Chl opoethoxy )Methane2,4-OlcttloPOphenol1 ,2 ,4-Tri chl orooenzeneNaphthalene4-Chloroanil1neHexach 1 opobutadi ene4-Cn 1 OPO-3-Methyl phenol2-Methyl naphthaleneHexacnlopocyclooentadiene2 ,4,6-Tri chl opoohenol2,4,5-Tpichloroohenol2-Chloronaohthalene2-Nitroan1l1neDimethyl PhthalateAcenaonthylene3-Nitroanil1neAcenaohthene2,4-OinitPOphenol4-NitrophenolDibenzofupan

. AFFECTEDSAMPLES:

_ . . . . _ - - . ._ . . . . . . _

[nit. Cal.f'3-Sr*F %RSO »

,0V?

M-V

•

S&.0

3?.J

J

^

J

tfv*rf^-e%vJ65*

II MI r. Cal . I'X'JiT. Cal .

*F %D *7- 6-8 7 \RF

I

*D * tt

I II I I

%o *

I

7-/tf-S"7RF |%D *

I I

I

II I I

II

3*,7

VrP-7

V0.3

J"

f

J~

*?/wrS-9

I

.

*

• .

.«7

3(9.6

33.3

T

%

J

&H9<a4>

9

^

* These flags should be applied to the analytes on.the-.sample data sheets.— -

CASE*


SEMIVOLATILE HSL COMPOUNDSPage 2 _

CONTRACTOR

DATE/TIME:

2,4-Qinitrotoluene2,6-OinitrotolueneOietnylpnthalate4-ChloPOonenvl-phenvleinerFluorene4-Nitroaniline4, 6-DinitPO-Z-Methyl phenolN-Nitrosodiphenylamine4-Bromoohenyl-ohenyl etherHexachlorobenzenePentachl orophenolPhenanthpeneAnthracene01 -n-Butyl phthal ateFluoranthenePypeneButyl benzyl phthal ateBenzo( a) Anthracenebis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyl. Phthal ateBenzo(b)FluopantheneBenzo(k)FluopantheneBenzo(a)PypeneIndeno(l,2.3-cd)Pyrene01 benz( a ,h ) AnthraceneBenzo(q,h,1) Perylene

Init. Cal.7-a-?7RF

.Oil

-RSD *

^

iTwiT. Cal *

RF 10

I

ii

*

' .llwrt-.. Ca*y.j7-6- S- 7 1

RF M 1*1

RF 1%0 1*

•

.en ft

*• cRF

- •--

.«a^1

to » "

•

/^



1/87

ENVIRODYNEENGINEERS

12161 Lackland Road.St Louis, Missouri 63146(314)434-6060

July 17, 1987

Ms. Carol SchaefferSample Management Office290 Madison Street, Suite 200Alexandria, Virginia 22314 - • ' ' ' '

Dear Ms. Schaeffer:

Enclosed are partial results of analysis of Case 7351 for Vola tiles, BNA'sand Pesticide/PCB's performed by Ehvirodyne under contract no. 68-01-7087.Soil samples, EMS59 through EM866 were received on June 19, 1987.

The samples were screened for Semi-Volatile levels by GC and they were allshown to be low level samples. All samples were cleaned up on GPC forPesticide analyses.

A matrix spike and matrix spike duplicate, the second for this case, were runfor volatile organic analysis only. Semi-Volatiles and Pesticide/PCB QualityControl Samples were submitted with previous samples on July 10, 1987*

In general, all quality control criteria were met, except sample EM866 had tobe re-extracted and analyzed for SNA due to low recovery of one surrogate.

In second column confirmation of pesticides, we observed higher than allowedpercent difference for the compounds of interest. However, the samples hadbeen analyzed in between the calibration check standards. The analyses wereterminated for corrective action for samples following the last calibrationstandard.

If you have any questions, please call Dr. Margaret Winter at 314/434-6960.

Sincerely,

Shaaban Ben-PooratLaboratory Operations Manager

SBP/smb:198Enclosures

f? fi? *L-JUL 201937

U S CPA, CEN lfcAL MtGlONAL j>B.536 S. CLARK STREET

CHICAGO. ILLINOIS 60OA

CAM Ho.Low.——

SOIL SI DOGATE PERCENT RECOV tY SUMMARY——— Contrtot Laboratory E-rrVt. f~6 **f*&-*_________ Contract No.

MediumVOLATILE SEMI-VOLATILE •PESTICIDE-

• HO**rr•a.

tOLUCNC-H iri 1.1 AiCHLMft*CTM4MC-»«

If «- 11 II

MiTflO- 1-fLUMO-•I'MIMTL

rtft'NtMIL• 14

(14- M»)

t'fVUOMOPMtNCK.

lt»*tllt III- III)

•numNLMCNt

110- 1*0)

**

lUL2tfL &£

tOL HB_ &&

W/Of 'it K>A *

mia5_ j£&- m±_

1: * VALUES ARE OUTSIDE OF CONTRACT REQUIRED- QC LIMITS: **ADVISORY LIMITS ONLY

VoUtllasiS«ml-VolitlU8t

CJ ft"* ofJ— out of

O

t outild* of QC llffllttI outildt of OC llmltiI outild* of QC

C

7/66

SOIL MATRIX 'IKE/MATRIX SPIKE DUPLir TE RECOVERY

Low L«v«l

Contractor

Medium L«v»l

FRACTION

VOASMO

SAMPLE NO.

8/N iSMO

SAMPLE NO.

ACIDSMO

SAMPLE NO.JO/I

PESTSMO

SAMPLE NO.

DA

COMPOUND

1.1-Dichok>rtlhtn«Trichlorotlhen«1&rt W*Tolutrf*

CA/*t>fc*ft««41,7,4-Tfichlorobtnicn*Aciniphihtni2,4 DmiuotQlutn*PvrtntN-Niiroiodl-n-Propytimint1 ,4-DichlorobtnnniPenuchlorophtnolPhtnol2-Chlorophcnol4-Chloro-3-Mtlhvlph«nol4.Ni|rophtnolLind*niHtptachlorAldnnOitWfinEndrin4.4'-DDT

CONC.ADDED

SPIKElug/Kg)

tf3f3$sH*$

*Jfl1

fljft

=1=

SAMPLERESULT

A)DA->T>A)P1.0Pt>

>l

*\J/

CONC.MS

•6(0S/rt(ofi^ft

T*M 1 A

X /AJ/^*\1/

XREC

97*fjtltfY1T?3)('

\

A

/MI

CONC.MSD

6,3.445V56goJuA

/JL>/i

\

RECf&f7U>

j

V.

/I

\

ft

•••^

>•

RPO

/3L34-

C2aJ>l

aL)f\

\X

1 1 UA.//I

OC LIMITS*RPD

2224 /j

C2lr217123194738382747356033506031433845SO

RECOVERY

59-17262-13760-13369-139M-14238-10731-13728-8935-14241-12878-10417-10978-9075.10778-10311 11448-17735-13034-13231-1344213923-134

ÂSTERISKED VALUES ARE OUTSIDE OC LIMITS.

RPD: VOAi—L_out «• £ ;B/N——£_<>« ol A ;ACID Q.. om of Jp ;PEST ——2L out ol

OC llmltiouiiide OC llmiuouliidt OC llmitlouttidt OC llmiu

RECOVERY: outtkt* OC MmlnoutiM* QC llmitloutlidf QC llmiuOuttidt OC Mmili

FORM III7/85

98/1 AthUOJ

•

/"vwwns

AI

•&-/(£OS

XNvia ao

Orginics Analyiii Data Shctt(Pagi 1)

Saaplt Nuaber: EMB59

Laboratory Naae: ENVIRODYNELab Siaple ID No: 87003138Saaple Mitrii: SOILData Release Authorised By:

Gift No: 7351QC Riport No:Contract No: .Datt Samplt Rcctiftd

VoIitiU Co»ponndf

Concent rat ion: LOWDate E x t r a c t e d / P r e p a r e d :D a t e A n a l y x e d : 4-25-87Conc/Dil F a c t o r : 1Percent Moiitore (not decanted): 13.73

CIS Ho: iqtf CIS Mi igkg

74-17-174-13-?73-11-473-fl«-373-l»-247-44-173-13-173-35-473-14-313(-ll-347-44-3117-14-17M3-171-33-434-11-3UI-B3-475-17-4

CklatOBitkait [ItBBBBitkaaiTiByl CklBt id i 1CklBiBitkaaiHitkylm CklnidikCltBBI

Cirboi D i f iK id il . t -OicklBioi tkiniLl-Dicklir t i tkaiittaii-U2-Dickl«r«itkiiiCklindn1,2-DieklitiitkaBt2-litaiiB«t.l.l-TrickIt[»itkniCaibfi Titruklirii iVti|l ke i ta t iItOBBdiehiitflEitkaii

i7~li o J

2 12 021 1If 11V9tVi

2 V11

11 01 1

71-17-3lltil-12-t7f-l t-41H-U-17T-II-S71-43-2lMU-ll-3ltl-73-l73-13-1ltl-10-13fUTI-4127-11-477-34-31II-II-3lll-fl-7111-41-4111-42-3

1,2-DtckI iTBpt tpant r iBf- l ,3-OlekUiBft r f i i t i*TricklotoitkniDlbr»*ekItr»Bitkiii1,1,1-TticklBiiitkaBilinitie i f - l , 3 - D i c k I i r B B t B p t n <1 - C k l O t B l t k f I f i B T l l t k B I

Ir»ifin4-IUtkrI-2-p«ttiiiti2-RltttBBITitrickliriitkiBi1,1,1.2-TitKcklariitkaiiTo I • tilCklmkiBiiitItkflbtlllBtStfr tnTttll tfllltl

0QD9U0D

12 BQ

11 0L2 1

VV00ff0n

Oatt ItpirtiBo, Qialifiiri

if • vilu jriatir tin ir iivil ti tki ditictiiBthi

C:WLK:If thi ttivltlilit, tlBBlt

I:Ii4ictl»i tiBfflnl MI tulfi** I«t lit »t 4ttteti4 Itftit Ui•iiiau dittcti*! liiit ftt tht itmfli «ttk tki 0 Ufl . l lQ)» itctititT CBtetit. / l i lttiBi aetifli. (T&ii U ntIht iutmBSt 4tt*ttiBt l i l i t . ) Tki f*»ti*ti ikoiU rial: I-Ciiptid vu tit lf itd fti »«t ait 4itBCti4. Tkt ink it ii tkiBiaiin at tainkl* It t tct lat lUit fit tk* lupU-J:iBdicitii *i titiMtai* tain, nil fltf if lit* iltkti wkiiHtiiatUf i ctittitrttiBt, (tt tiitiliiili iiiitifiil ctEfoodi - „•hut a 1:1 rtiaoiiB if iftn*d ir «t» tka man iiictril iatt --":•--ii41catH tkt ptistiei •( i ciatoiad tkat Miti tfci iititllicatloierittiia kit tki tifilt ii lin tkai tki ii«cidH dttictin lii.it kitftttiir tkn uta (if, tlJ). If lilit if dittctioi ii II i|I aid t

nil flat iiplin (• iBfticidi Mi"<titi vkttB tkitiii was etilirmtf IT CC/KS. Siiqli cnpBint itittcidtsl'll•l/il ii tki final iitttct (koiU •• tBifiiktd kf CC/HSI" - • - -nil f la f if tfil vk» atatyti Ii fond ti kl»k u «<ll ai alill!i It iiduitii piiiibU/irikibli klank cBitutiatitn andmm tki data nit tt taki afpupt i i t i tct ioi .OTHE1:Otk*t fliii aid foattotn may 11 riqurid ti |iB|irlT difintki rifilti. It isid, tiif Hit ki (tllr disciibid aid tickdncrittiii attickid t« tki dtt* nutty

Laboratory Nt»«Cist No: 7351

ENVIRODYNE S i m p i t N u » b « r

Organic* Analysis Data Sbttt(P«gfl 2)

Scaitolttilt Compounds

C o n c e n t r a t i o n ; LOVDiUt E t t r a c t e d / P r e p a r e d : 4 - 2 4 - 8 7

t A n a l y s e d ; 7 -2 -87c / D i l F a c t o r ; 1cent M o i s t u r e ( d e c a n t e d ) ; 1 3 . 7 3

CIS K>:

lll-fS-2 FkiBol111-44-4 k l s - ( 2 - C B l t C M t k f l ) t t k t i13-37-1 2-CkUroBktBaI341-73-1 1,3-DickUrilti itBt114-44-7 l ,4-DickUr*bmeit111-31-4 Itttyl lletktlf3-3l-l 1,2-OickUttbtutiifS-41-7 2-IUtkTltkiBtl3f43l -32-f b i i - ( 2 -Ck lorB i f e i i o»r I ) i tk« i114-44-3 4-Kttk7l|ktB«I421-44-7 l-iitrti»-Di-t-Brtpfla»iBt47-71-1 ImckUttttkaufl- f3-3 litrikmiBt7l-3f-l Istektrtit11-73-3 2-Ntt iopkiBil10S-47-* 2,4-DiaitkylihiBtl43-13-1 Iwttie Icii111-fl-l ii«-(CkIei«tktiT>H«tkaBt121-13-2 2,1-DUkUratkiBtl121-12-1 l ,2 .4-Tritklu«i<BimM-10-3 RiBktkalm114-47-1 4-CkIitoiiilin17-41-3 luaekUrtkit adieu37-10-7 4-Ckl«n-J-mttkjlik*aelf l -37-4 l -Hatkf lBafktkal»i77-47-4 liiickItriCTcltp»ta«i*Bi11-14-2 2 , 4 , 4 -T i t tkUrDBkiBt lT3-f3-4 2,4,3-TiickliitpkiBtlf 1-51-7 2-CkliriBipktktliBi11-74-4 l-litr»tBilifte131-11-1 Oi i t tkyl iktkilitilll-fi-l IctBiptkrliuff.|f-2 3-Nitr iaBi l i ie

( l>-C»nnot bt

S e p .Cont

Mk,

310 0311 V111 Q110 V111 0no o310 0311 V311 0311 U311 Q311 V111 V311 I311 V310 1tfll 0310 «311 B301 1311 Q111 V311 0310 Q311 0310 V111 DItll D311 1Ifll 0311 0111 1If l l U

t tparat td

Funne l E x t nin . L i q . -L i q

CIS No:

13-31-f31-21-3111-02-7132-44-f121-11-2414-21-214-44-27013-71-314-73-7111-01-4334-32-114-31-4111-33-1111-74-117-14-313-11-1120-11-714-74-22H-44-Illf-OI-l13-41-7fl-M-134-33-1117-11-7211-ll-t111-14-1H3-tf-2217-ll-f

_ 31-32-1lfl-3f-333-71-3ltl-24-2

f rom di phtny 1

i c t i on : YES C J W U i r c I e. Eit . : YES (tity ( c i r c l e

ICtBlpktktBI

1 , 4 -DUi t i tpk i i o I4-Xit lD |k lBQl

DiktBiof i r iB2 , 4 - D i a i t r > U l i t f t «2 , 4 - O i B i t t i t B l i t B iDi i tky l iktUUti4-CkUropki iTl-pki iy l t tk trFliotut4 -N i t re«B i l i i f f4 ,4 -Di i i t ro-2-Ki tkr lphiBolM-iitraii4i |k*Bf limin <1)4-ltek«ikiirl-ik«iTl ttktrItiickUititini*Ftitackltrtiknolfktiaitkrti*iitkraeiBiOl-t-bitTl pktkiUt ifli irtBtkiicFfllBI

I l t T l - k C B t f l - I B t k l l l t l

3,3' -DickIttebiBtidiBtIcBttdl iBtkrattBtUl - ( 2 -CtkT lk t iT l ) | k tk iUt iCktTintgt-1-tttfl iktkalatiI t B I B t k H l l O K B t k l B t

ltBi«(k)tlten»tkiBiItBItdltTtBB*

Iiiii»(t,l,l-t4)|fii«Dikt t i i<a ,k )a i tk [ i c tB iliBi«(|ki)ttryltit

amint

one )one )

i^kq

310 QI f l l 0mo o311 U310 D311 D311 Q310 QJ l f l 0Itl l UI f l l V311 U311 D310 6mo Q311 U310 0410 1311 D310 3311 D771 U310 Q710 131 BX

QjJL^310 U310 0310 Q310 Q311 D311 D

FORM 1

Laboratory

Case No __

Organic* Analy*1"5 Data Shoot(Page 3)

Pesticide/PCBsConcentration: ( Low) Medium

i _Date Extracted'Prepared:

Date Analyred: ____L£L

Cone/Oil Factor: ____

(Grcle GPC Cleanup Bês ONo


Continuous Liquid - Liquid Extraction OVes


CAS ufl/lo^fc*9/Ko,Numb*r . (GrcleT7n«l

319-64-6319-85-7319-86-858-89-976-44 -fl

309-00-21024-57-3959-98-860-57-172-55-972-20-833213-65-972-M-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6UO97-69-1M 096-82 -5

Alpha-BHC

Seia-BHCOUa-BHCGammj-BHC (Lindine)

HeptJch'Of

AWnn

HeptacMor EpoxtdeEodosulfan 10*e(drin4. 4' JOE£ndftnEndosutfan d4. 4--OOOEndosuffan Sutfate•4. 4--DDT ^MemovycMorEndf in KeiooeChlordaneTo«Jpn«f>«

Arodof-1016A/octor-1221A/ockx-1232Aroclof-1242A/odo<-1248Afoc(or-1254

Arocfo<-1260

«.. a/ t .<0 flIL.O U

- /6.0 «

/6.0 «./A-0 «./t.o uH.O K _33.0.VL.-53.0 U

JS,<? a*33^J «jrp.o uJ30 «J3JJ U

1 (*&.£> U.

Jl.0 UH~AO U

Jwo. ) Uite.o ulL£>.Q U£6.O Uiu>.o ul(,t>,0 UJ20.0 U

320.O IL

V- * Volume of e*iraci infected (u<|


Wfi * Weight of cample extracted (gj

V( * Vofume of total ectrao fuQ

orW.

7/85

Envirodyne Engineers

D»ta SheetOrparwcs

T*oUtrvfl1y Identified Compound*

Organic! Ana l y s i s Data Shttt(Page 1)

St>pIt Nu«b*r

Laboratory Naat: CNVIRODYNCLab Samplt ID No: 17003140Simplt M i t r i i : SOILData Rtltast Aathoriitd By:

Case No: 7351QC Riport No: _Contract No: _____Date Saaplt Received

Vo 1 at iIt Compoandf

Conctntrat ion: LOWDate E i t r a c t e d / P r e p a r e d :Datt Analysed: 4-25-87Conc/Dil Factor: 1Percent Moisture (not decanted) M.I

CIS No: •fkf CIS Ko

74-17-374-13-179-11-473-M-37S-II-1•7-44-175-15-175-35-475-34-S151-il-Si?-ii-l117-li-l7I-I3-!71-35-iSi-11-3lll-IS-473-17-4

Ckltrei t tkait 1lioieittkait 1TtiTl Ckltridt 1CklottttkaitKit If I tit Ckl t r id tictttitCarkoi D i n l f i d t1,1-Dickloittthtit1,1-Dicklerit tkaitttais-l,l-0ickltrectkntC k l t r t f e r i1,2-Oickltitttiait1-littieii1,1.1-TriekltrottkaitCailti Tt t taekl t t ldtTiifl ictt i t iIt iitdiekl tint t kut

2 D1 02 D2 DVI 194 1

V00s11

2 6V1

1 V1

71-17-3llltl-12-i7f-lt-t124-u-iTI-H.S71-43-1lllil-ll-311I-7S-I73-13-1lll-ll-ISJ1-7M117-11-47T-34-Stll-ll-Jlll-M-7111-41-1111-42-5

1,1-DiekUitprtputt t i i s - l ,3-Di tkI0reptDi in tTricklervttkiKl i fcl lBOCklBtt l t tkal l

l , l , l -Ti ichlet«i tki i iItiititc i i - l , 3 -Dick Io ia f topcnil-CkltrottkyUiiyittfcKIrate fo ra4-Httkfi-i-ptiUioitI -It I ail II

Tttrackltrtt tktit1,1,2,2-TttratkIirutkiitTtlititCklttiktiiiititkf ikciitiiStyrtiiTttil Iflnti

0DVBDQ0

11 D0

1 IJ[2 V

I1

2 IJVVD0

DtU Itptrttif Qitl ifUri

If tkt molt If i f i l i t f inti i tkti ti MCI! t« titl i i i t , r tyo i t tkt f t l i t .

Utftcitt i eiKptntf v» atilfiH dr lit lit tftttetii*. I t f t t i tkt•iiiia ttttetlti l i i it fit tkt fuplt v i tk Ui Q ( i f . l I D ) Iift4•i itetfsitf et i t t i t . / l i l i t l i i ictltt. (Tkii if itt nciiutilytkt intiaiit tkttctiti l i m i t . ) Ht (ictioti ikeild ttit: V-

•«> «iil|iH (ir bit lit Ittictit . Tki laku is tktitt intkU tftttctUi l int fit tki itmplt.

J:Itf lcit if u t*timitt< ?«Iit. Tkit f ltf i f l f l< *itktt vktiii lima til) * eiittitnttii (tr tnUtlfilf iditil i i i

a 1:1 r»M*<* tf «•«•*' •' •*«« tki Uitkt friinei tf a e»find tk*t uit> tkt i l t i t i f i c t t io i

e r i t t r i a kit tkt rit i tt ii 1m tkai tkt *t*titi*i ( t ttct it i l i i i tir t i t tr tkn itrt (t|, 1IJ) . If lint if ritttcti i i ii U til aid a

C:Tkii tlif i p p l i i f ti ytitiei't Miuittrs vhiic tki i<tati(ict-titi vif ciifiiatd kf CC/HS, Slitlt cetpoint piittcidn)»II•f/il ti tkt liial ntriet ikailri bt e»»(ir»i< hr "^

Tkii flii is in* viti aialftt Is ftii< ii kUik is wtil as a•ABpIt. It iiiititti ttssiklt/srtkiklt H*it coituintiia tndmm tkt lati is*t tt till apsttpriatt «ctiti.OTHE1:Olktr (Ufi »< f t i t i t t ts UT I* tiîittd ti i r sp tr ly <t(iittkt rmlti If titi, tit; «i>t kt f i l l r d t i e r ikcd aid sickftseuptit i itttckttf tt tkt data imatf

lit

L a b o r a t o r y NaaeCase No: 7351

ENVIRODYNE Nuabtr

Otganici Ana Iyf i § Data Sheet(Page 2)


e E i t r a c t e d / P r e p a r e d : 4 - 2 4 - 8 7e A n a l y z e d : 7 - 2 - 8 7c / D i l F a c t o r : 1cent M o i s t u r e ( d e c a n t e d ) : 1 4 . 7 8

CIS Mi:

111-93-1 fkinel111-44-4 k i i - ( l - C k l o t » i t k f I ) t t k i r93-37-1 1 -Ckloropkt io I341-71-1 l ,3 -0 iekl*t*kt i t t»lli-44-7 1,4-DicklflroktBitBi111-31-4 Inifl i lcoktl93-31-t 1,1-Dickltieknttit93-41-7 2 -Ki tk f lpkt io l39431-32-f k i i - {2 -CkI«ro i f*pro i r l ) i tk t r114-44-5 4-HitkjIpktiol411-44-7 M-itttoft-Di- i -propylui i t47-71-1 ImcklitMtkait98-f3-l Mitrtkiai t ie71-39-1 I i tpkoiDBi11-73-3 2-Nittipkttot113-47-f 2 ,4 -DtMtk i t fkne l45-15-1 leetoic JLciit l l - f l - 1 k i i - <CkIo t f l i t k f l i y )H i tkaM121-13-2 2 , 4 -D i ckIoropk iw l111-12-1 l , l , 4 -Tr i ck l i r»k<Bi i i e91-20-3 Napktkalin114-47-1 4-Ckloruii l iBi17-41-3 BiiackUr*kitadi»t39-31-7 4-CkIir i - l -MtkrIpkeBol91-37-4 2-Hitkyl iapktkaI iBi77-47-4 I i iackI«r*tTcl tpeBta<iue11-14-2 1,1,4-TrickUrepkift i l93-93-4 1.4.3-TiiekIit ipki i«l91-31-7 2-CkIir»apktkaUBtH-74-4 2 -Ki t r0a i f l iB t131-11-1 D in tky l fktkal i t iIl l -f4-l le iBaptkyli i i99-19-1 3 -Ni t r0aBtI ia t

SepCent

tfltq

Ifl V3fO QIfl 9191 9391 9191 9191 9Ifl 9Ifl 9Ifl 9Ifl 9391 9191 9Ifl V191 9191 9If l l 9191 9191 9Ifl 9Ifl 9191 9191 9191 9Ifl 0Ifl 9Ifl 91911 DIfl 9Ifll 0Ifl 9Ifl 91911 0

F u n n e l E i tin . L i q . -Li

CIS No:

11-12-951-11-5111-12-7132-44-9111-14-24K-2I-214-44-17115-71-314-73-7111-11-4334-32-114-11-4111-53-1111-74-117-14-3IS-l l- l111-11-714-74-2214-44-1119-11-113-41-791-94-134-33-1117-11-7111-11-9117-14-13 IS - f f - 2117-11-9SI-11-1191-19-351-71-1191-14-2

r a c t i o n : YES [N&<; < c i r c l eq. Eit . : YES Q K p f c i r c l e

Ituapktkuil , 4 - D i B i t t o e k i B « I4-Kitr»tk»«lOiktaitf iraa2.4-Dtiitittaliiae1 ,4 -DiHi tr i toUi i tSl i tky l pktkalaU4-CkUrepkiif I -pkcny l i tk i tFlierm4-Mit toaBiI i i i4,4-OiBitr0- l -Ritk rI ik»0II-aiti«i0i'itkiiy!amiit (1)4-lr0Bopk»yI-0kityl etket••iackl»r0ktaitatPeatackUrtpkitelfkiititkriiiUtkraciB*Dl-a-kityl pktki lat iriiitiitiiitFyriBil i t r l -k0Bt r l -pktkiUtel , r -DickI0t ik iBi i r i i t iIiiiadtiitkricmki i - (2 - t tkr [knr l ) ek tk<Ut<CkryctitDi-i- ietT l p h l k i l t t il i i f id l f l i t iaBtkiBil»it(k)f [tirutkutltni(«)iyriit *Ii<0ae(l l l l]-c4)|yr0i0DikiBi«(a .k)aBtkia»Biic i t tCfki lptr i l in

one )one )

igk;

3ft 9mi v1911 93ft 91ft 9Ifl 9191 93fl 8391 VI f l l 0I f l l 9391 9Ifl 93ft 9I f l l 9Ifl 0391 91411 1Ifl 03fl 03ft 9771 93ft 0451 13fl 03H 03ft 03fl 9391 0191 9191 93ft 9

(l)-Cannot bt itpirtttd (torn diphtnyIi,min«

FORM 1 ~ ,

Laboratory Narpe

Gate No "~

Organtes Analysis Data Shoot(Page 3)

Posticid«/PCB$

Concentration ( LowJ Medium (Circle One)/ ._ 9</ -

Date Extracted'Prepared ____o *\~1

Date Analyzed: ____ (~~ * ' • _

Cone/Oil Factor: _________f

GPC Cleanup SYe* ONo


Continuous Liquid - Liquid Extraction OYes

mom<cmo


CAS

319-84-63I9-8S-7319-86-858-89-976-44 -6

309-00-21024-57-3953-98-860-57-172-55-972-20-633213-6S-972-S4-81031-07-650-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611O97-69-111O96-82-5

Alph»-8HC

Beia-BHC

Defta-BHCGamma-BHC(UxJ*oelHeotachforAkJrm

NepiacWor EpoxideEndosulfan 10*eldrin4. 4--QOEEndrin

Endosurfan 04. 4'-OOOEndosuffan Svtfate4. 4-.ODT ^

M«tfK>«Y«hl<X

£ndrin KetooeChtordaneToup<t«rt«

Arocfor-1O16Aroctof-1221ArocIor-1232

AroclOf-1242

A/oclor-1248

ArocKH-1254

Aroc«x-l260

H*.o uIL.O tiIt.O tt

.- !(,.& U/£•£> UM.O «./4.O y/*»<0 *t

JTJt-O «..-0,0 a^3-<3 tt

1 *3?0 Uj-p,o UJ3-O K

r ^3^3 «/<.£>.£> U

JJ. «/tA^ U

JUo,£> U)tfO,o uite>.o uKA& u./£&& UI16.O U330.^ i/326.O Ut

oo

extract iojeacd (ut|

V = Volume of water enracted (ml)

W *• Weifftit of cample extracted (gl

V( * Vofume o< tocaf

orW.

7/8S


Analysis O*tB Sheet(Page 4)

Identified Compounds

Orginics Anilfsif Diti Shit t(Pigt 1)

SiapIt Number: E

Libontory NIBC ENVIRODYNELib Sinplt ID No: 87973141StmpI* Hitrii: SOILDiti Rclcif• Aathoiind By:

Cis t No : 7351QC R t p o r t No: __C o n t r a c t No: __!____D » t t Siapl t R t c i i v e d :

V o l a t i 11 C o m p o u n d !

C o n c i n t r a t i o n : L O WD i t t E i t r i c t t d / P r t p i r c d :D i t c A n a l y n d : i -U-67C o n c / D i 1 F a c t o r : 1P t r c i n t K o i s t u r t ( n o t d t c a n t t d ) 1 5 . 2 ?

CIS Ho: ift?

74-17-374-13-973-I1-473-10-373-17-147-44-173-13-175-33-473-34-313(-il-347-44-3117-li-l71-73-371-33-431-13-3111-83-473-17-4

Ckl t iOMtkt i i 1Iratoiitktitf i i f i Ck l t r id i 1Chloret tk in iHitkTlm C k l t r i d tUeteiiCirkoi D i i i l f i d i1,1-Dicklarai tht ic1 ,1 -Dickl ir i t tktEitr»i- l . l -DiekltrottkiitCkUrtfirm1.2-Ditklirutkiit1- lit 11 lit1.1,1-TrickltriitkinCirkft Tituekliridif i i f i Icit ittIr »o< i ck 1 ir »t t ktit

2 02 0i a1 V21 1U 10u009V

2 fVV

12 0( 0

CIS Ki:••••••mi

71-17-3

igkq

79-11-4124-41-177-11-371-43-2

111-73-173-13-2111-11-371-71-127-11-7Y-34-3111-11-in-»i-1IC-41-111-42-

1,1-Dieklutf i tpi t tt ra i f - l ,3 -DickTuefcUi.ttktii

1,1.1-TrickleteitktiiItitin

Iroieform

1-IisiioitTitrickUrittktitl , l . l ,2-Tit t«ckl»i t t tk»iTilttn

Tittl

4 U4 V4 04 0i U4 04 V11 U4 D12 011 I

0I

V0t0

DiU leportitf

C:ttlUI:If tki rtin It is t filit iriittr tkia «r Mitt ti tkt l ittetitiI t i i t . nptrt tkt flUt.B:Iidtettei cMfttid vit »tlfit< (tr kit itt dtttet id. l iftrt tki•inin Jt t i c t i t i lint (it tki (U|U v i tk tki V (19,110) kiitd•• itciftitj t i itnt. / l l l it i i i ittiii . (Tkif is itt ucMiiri lftkt iutrntit dittetlti l i m i t . ) Ti. (tttieti ikeiU mi 0-Ciueii< vis »4lfs«< fir kit lit dt t ic t id . Tkt mktr if tki•iiiin t t t i i iakl i dt t tct ioi liiit fir tki iiafli.J:Ulictttf » t it imittd f«Ui. Tkis fU( if •<•< t i tk ir vkii•ftiutiif « ciictvtntiii fir t i i t i t iT iI f i ln t l f i t l citêndivkiri t 1:1 rifptii! is tssntd ir vkii tki uts siietril dittt idieit id tki iritiici if a e»iond tkt t Btiti tki td i i t t f i e i t i o ie i i t ir i* kit tki rtf i l t is Iifi tUi tki f p t c i f i i d di t tct i t i liiit kitf i c i t tr tkn nci ( i f , 1 I J ) . If l int if d i t i c t i e t is II igi »d i

Tkis (Uf tpptits ti f t s t i e id t ftruttirf wktrt tbt i d t i t i f i E i -till vtt cttfimd If CUK5, Si ig l i ctipeint i t i t i c idts ) - ! !M/il U tki f inl utricl ikt i ld ki eitftmd k? CC/KSI:nil f l« | if isttf wkit mlftt Is ftnd ti klt ik is Mil is i•u|li It i idicitis p i f s i k l i / p r i i t k l t kUit eiituiittiii indvain tki d«ti iitr ti till i tpretri it i ict i t t .OTHE1:Otktr f l i q f nd f i it i it i i uj kt riff.iirtd ti prop t r l r dif i i itkt rts i i ts . If istd. tkty list it ( i l l y d i t cr ik id nd lickdner ip t io i i t t icktd ti tki diti SVBBIIT r i p e r t .

L a b o r a t o r y NameCase No: 7 351

ENVIRODYNE Sa»ple Nanber

Organics Ant Iff is Data Sheet(Page 2)

Sealvolatile CoBpoands

e Ei t r a c t e d / P t t p a r e d : 4 - 2 4 - 8 ? S e p . Funne l E i t r a c t i o n : YES Qâ c i r c 1 e o n e )e A n a l y i e d : 7 - 2 - 8 7 C o n t i n . L i q . - L i q . E i t . : YES Q^) t c i r c 1 e o n e )c / D i l F a c t o r : 1cen t M o i s t u r e ( d e c a n t e d ) : 1 5 . 2 9

CIS Ni:

111-93-1111-44-495-37-1541-73-1104-44-1lll-Sl-(93-30-193-41-739131-31-910(-44-3(ll-(4-7(7-72-191-93-371-39-111-75-31IJ-47-9(3-15-1111-91-1121-13-1lll-ll-l91-28-3lli-47-l17-11-339-51-791-37-477-47-411-04-295-93-491-51-714-74-4131-11-120l-9(-l99-19-2

PhtBOl

bt i - ( 2 -a i e rB i tkr l ) i tk i r2 -Ck lBrBBkea t l1 ,3-DUfcUrtttBiiBt1,4-OicMfrBktBieBtItiifl lleokel1 , 1 -D i eh l e rabBBiBB il - N i t k y [ p h > B B lb i s - ( 2 - C k I e t e t f 0 p r 6 i f l ) t t k i [4-Ktthf lpktBtlK-BitrBie-Di-B-prop- luiBBI i i ickUrtttkiBilitrobeiiiieI l B p k B C B B C1-XitropkiBol2 ,4-Di i i tkYlpk«BlItBteic Ac idbi i - (Ckl troBtke iY>Retkaae2,4-Oicb.{*ropk*Bol1,1,4-Tt ithUribmiiiMapktba l tBe4-CkUrBaBiI iBeiBiaeklBrobetadi iBi4 -CklBrt -3 -Mtk T lpkBBi l2-K*tkf lBipktkaItBtItfacklBrecfcUBflBtai ' ieBe2 ,4 .4 -TrUkl*rf lBktBel2 , i ,3-Trickl«tBpbiBi lI-CklcroiMitkiUit2-Rl troaBi l iBeDiBt thy l pitkalat iIc tBapthr l iBB3-Ni troa i i l iBe

•4kg

391 D391 V391 0391 V391 V398 9390 0190 U190 D198 1190 5191 1190 V198 1398 tf198 11910 V198 1398 D398 V398 0391 V190 U198 B390 0191 8390 V1988 D398 U1908 D190 V391 01900 V

CIS KB:

13-31-931-11-3188-82-7131-14-9121-14-2401-20-214-11-27803-72-311-71-7180-01-4334*32-114-38-4101-55-3110-74-117-04-313-81-1120-12-704-74-1184-44-8129-08-813-18-791-94-154-33-3117-11-7211-11-9117-14-0285-99-2287-01-958-12-1193-39-553-71-1191-24-1

IctBapktkBB*2 , 4 - D l B i t i « p k i B o l4-Kitrtpfc iB»lDibtt iof i t i i2 , 4 - O i B i t r c t i l B i a e2 , 4 -D lB l t r t tB l t iBeD i i t h f l p b t k t l a t B4 -CklBrBpkcBf l -pk tBf 1 B t k i rrinriBe4-Ri t iBaBiUBi4 .4-DiBitr»-2- fUtkTlpkeB*II-BitrBieiipktBjluiBt (1)4-lrtMpkiBfI-pkiBf 1 etkstIiitcbliribtiKBiPiBtiekl i tefkiBiIPkiBaBtkriBiiBtkrtCIBt

ni-B-kityl p k t k t l a t eTI ior tBth iBtPfitifll a t T l - b i B i T l - p k t k a l a t B3 ,3 ' -D i :kUrob in i idn«l i i iadl iBtktictt ib i s - a - C t k T l k i i r l l p k t k i l i t iCkrfitBiDl-B-tctf l p k t k a l a t el e B i B ( k ) ( I i i r l iBt«(t)f InrutktBtleBiB(a)efi*BtlB<tBt( l , l ,3 -Cf Ippttt

01ktB iB(a ,k )aBtkracBBtl iBiB(gkUp»r;IeBe

•in391 D1911 U1910 U3TI UIfl 0390 13fl 03U U391 01911 01910 V191 0390 V3(1 V1908 03*1 0191 ?211 BJ3ft 0311 U311 U711 9311 tf311 I311 D111 03TI 0311 D310 0311 D310 U318 9

<l)-Cannot be separated from diphenylamina

FORM 1

Laboratory

No

Organtes Analysis Data Sheet(Page 3]

Cooccntration: tow Medium


Date Analyzed: ?7" ^

Cooc/Dil Factor: _____1

Pasticide/PCBs(Grcle One) GPC Cleanup GTYes ONo

(/ ^7f!"*/>_____ Separatory Funnel Extraction \

Continuous Liquid - Liquid Extraction OYes *^


CAS ug/l<xf»g/K£Numb«r . (CircleTJKe)319-84-6319-85-7319-86-856 89-976-44-8309-00-21024-57-3959-98-86O-S7-172-55.9*72-20-833213-65-972-54-81031-O7-850-29-372-43-553434-70-557-74-98001-35-212674-11-21UO4-28-211141-16-553469-21 -91 2672-29-6U097-69-1110S6-82-S

Alpha -BHCBetJ-BHCD*Ua-BHCGamma-BHC (Ltodar*)HeotacfiUxAldrtnNeptacntor EpoxideEndosulfan 1Dtetdrin4. 4' )OEEndrinEndosuKan 04. 4--OOOEndosutfan Sutfaie4. 4'-ODT ^MethORVCtUor

Endrin KeioneChlordan«ToxapheneAroc«<x-10l6Arocio*-1221A/octef-1232Arodof-1242A/ocl<x-1248Aroci<x-1254Afoct<x-l26O

Ho.O UtL.<y ILtC.O tL

.- /fc.O «i(,.o ait,.o u./t,.o utl>,C> U.

xf.o U-.• .o U3i.e> u.

1 i3tPO «JJ-o UJ3-0 Hja^3 «

/CA£> U.J3-& «/tAO «

JLJO. > U

Hrt.G UlLo.0 UKAA UIM£> U116.0 U.320.6 U33&.O U.

V- * Volume of exlrad «nf«cied (uf|

V * Volume at water extracted (m)|

W^ « Weight of camp(e extracted <g|

V. * Volume o4 total extract (ufj

orW.

7/es

Envirodyne Engineers^

O«y»mcx Analysis O*t» Sheet'(\

Tentatively W«ntif»«<J Compounds

CAS•C<m»e*«nlM«m«

4&kJu

TT

IT10,

cris.16.17.

I'

£-7. Of)

21..

Z3..24...

2*

7LVOA

Organics Analysif Data Sheet<Pagt 1)

Samp It Number EM842 j>

Lab o r a t o r y Name: ENVIRODYNELab Sample ID No: 87003142Samp 1e Ka t r ii: SOILData Reltast Authoriitd By:

Cast No: 7351QC R e p o r t No:C o n t r a c t No: . • 70Date Sample Received

V o l a t i l e Compound!

Concent rat ion: LOVDate Eitracttd/Prtpartd:Date Analyied: 4-24-87Conc/Dil Factor: 1Percent Moisture (not decanted): 15.63

CIS No. CIS Mi: igtg

74-17-374-U-t73-11-473-IB-l7S-lf-247-14-173-13-173-33-473-34-313<-il-3i7-i*-3117-li-l7i-n-i71-33-434-21-S111-19-473-27-4

Caloroit thii t 1Itomomitkaairiifi ckiotidi iCkleioitkaiiHitkyUBi Ckl i t id ilettiaiCtriea O i i i l f i d il,l-Bickl»rBitkni1,1-DieklBriitkatit tatf- l ,2-DickUmtkniCklindrm1.2-Ditklitiitkaat2 -lit ami1,1,1-TiickliriitkaieCaibn Tit tacklocidiTiiyl leitatiItHodteklatimitkaii

2 51 02 Q2 011 141 1000VIff

2 91V

12 01 D

7I-I7-S 1 ,1 -Dick l i tap ioptn11141-ll-i t ra i i - l , 3 -DickIeroFton i i7t-ll-t Tiiekloititkin124-41-1 Dib iomocklotomithai t7T-II-5 1 ,1 ,2 -Tt ick loto i tkan71-43-1 IHIIBI1IK1-I1-S c i i - l , 3 - I>UkI i top toptn i

001V0V0

111-73-1 : -CiUro.t iT [ f i iT ! . thtr 12 Q75-IS-l ItiBifirm i V111-11-5tl-TI-127-11-7*-34-3111-11-l l l - f l*111-41-141-41-

4-HitkTl-l-piitai«n 11 02-Iiiaini 12 ITitiacklirntkiii i V1.1 ,2 ,2-TitracklMBitkan < 1Til mi / i jjCklltlbllllll < 0ItkilkniHi * VStytni i VTital I f l i iM i 0

Data Itpittiig Qialifitrt

TlUt:If tki milt ii a «!•• iriatti tkai it intl ti tkil im i t , ttpit tkt ralBi.0:tidicati* citfoiid war ualfsil fir lit lit ditittttf. Iipirt tkimien tf i t ict i i i l imi t ftr tki famil* vitk tki 0 ( i f , 110) landIB iieeiiatf eiiciit./iltitiii actlei. (Tkii is lit ittmaiilftki intrant ditietiu l i m i t . ) Tki ftetnti ikoili i\\i. 0-Ciii«i»4 wai aialysid (it kit lit dititt*4. Tki inkir ii tki•into t t ta i i ak l i ditictii i I t i i t ftr tki laapii.J:Udicatif 11 iitimatii f i ln Tkii (laf Is tiitf l i tkit vkitifttmatiif i ci ictittatioi (»r tiititivilf Uutifii< ciap«nif _ "vkin a 1:1 iiitoin if aisaid it vfeii tki Ban iMttiil latitii'icatii' tki iriinei if > ciifend tkit Miti tki 14itti[itttiait r i l i rU kit tki nsilt it Ini tkai tki i f t e i l i t i <iticti» l im i t•r t i t tr tin ins ( f i . 1 I J ) . IE l im i t •! i iUctioi ti II i|I aid a

C:Tkii fla| afiliu ti inticidi iiruitiri vktn tki idnt i f ica-tin vai eitftrmid kf CC/KS. S i i f l i cempenit r c i t i e i d i i l ' l li|/il ii tki l i t i l uttact iknld hi cnfirmid kf &C/HSI:Tkii fla« ii tsid vkii aialfti If find ia link if mil *• afaajli. It liditatit ufiikli/iiibtvli klail ctatuiiatin tndvatii tki data tut ti tafci i|ttitriati actiei.OTHEI:Otkir fla|f aid (ntiitif w| >i riqund ti M o M f ' T <i ( t»tki f i i i l t t . It ind, tkif nit ki t i l l r d iscr ib id aid tickdi ic i t i t in attackid to tki data inmaif r i i o t t .

kit

laborat or y NtmeCist No 7351

ENVIRODYNE Saiplt Number

Organici Analyiii Data Sheet(Page 2)

S«ni TO I a t i I • Compounds

e E x t r a c t e d / P r e p a r e d : . - 2 4 - 8 7e A n a l y i e d : 7-2-87c / D i l F a c t o r : tcen t M o i s t u r e ( d e c a n t e d ) : 1 3 . 4 3

CIS N>:

101-73-1111-44-475-57-1341-73-1104-44-7100-31-473-30-173-41-737431-32-7114-44-3411-44-747-72-1TO-13-371-Jt-l11-73-3105-47-74S-I3-I111-71-1121-13-1110-01-111-24-3114-47-017-41-337-30-711-37-477-47-401-04-173-73-471-31-700-74-4131-11-3101-74-177-07-2

Fhiflolk i<- ( l -C . l» [» iUf I )» tk*r1-CkloropkiBoIl ,3-. iekI«rabiBiuil ,4 -DichIorobt i ie_ iImyl ll tokel1,2-DichIatcbiBien2 - K i t h y l f l k t i o Ik i i - ( 2 - C U o r f l i f t f t r e i y Hi the r4-Hitkylpkt iBlK-iitr»sa-Dl-B-ptBpylaiiiileiickliiottkui•ItribeisiBiIsiakacBBcl-Klttopkmll ,<-Di«t-y!pktioIliBsoic Acidb i s - (Ckluo i tkBiy>Ht tkau2 ,4 -Dlcb . lB iBpki io l1 ,1,4-TrUkUrt.iiitnMipbUlltn4-CkUrttiiIii*Hincklotebat idi iBi4-C_lor»-3-«tkylpk«ol2-Kitkylupkt. i l ineIt i iekloracTcUpttUditf t t2 ,4 ,4 -Tr iekIe iopk iBs l1, ' ,3-TricBliropkcBoll-CkletB.ipktkiliBff2- l i t rBaai l iBiD i M t h y l pktki l t teIciBiptkylm3-KittBti i l i ie

S*p F u n n e l E i t r a c t i o n : YES (N£/< c i r c 1 e o n e )C o n t i n . L i q . - L i q . E i t . : Y E S QNJX ( c i r c l e o n e )

•9H

371 0310 V310 037C Q370 0310 0310 9310 0370 U371 V371 V310 V370 0370 I370 9370 91700 9310 1310 9310 9370 9374 9371 9370 9310 9310 9371 01700 0170 91701 9370 9370 91104 9

CIS No:

13-31-131-21-3100-02-7131-44-7121-14-2404-10-114-44-27005-72-314-73-7100-01-4314-32-114-30-4101-35-3111-74-117-14-315-01-0110-12-7H-74-1104-44-4111-40-0IS-44-7fl-74-154-33-3117-11-7111-01-1117-44-0243-77-1207-04-730-32-4173-31-533-70-3171-24-1

ICtBlpktklBI

1 ,4 -DiBi t r epk i io l4-Xi t r tpht i t lDi i t i i t f i r tB1 , 4 - O i i i t r o t t l B f B i2 ,4 -Di i i t r e tB l i t t iD i i t k y l pk tk i l t t t4 - C k I o r « p k c i f 1-pkcByI i th t rriieciii4-Mitr**BiIii i<,4 -OtBi t r e -2 -Hi tky lpk»o lM-iitrtfli4ipkurlaiitc (1)4-lroB*phetyl-phiiyl i tktr

. IciacklfltBbflBiiBtFittickUitpkciaiPkentitkriie-itkraeiBBDi-B-bi ty l p k t k a l a t iriioititktBify t iB*I t ty l -k i i iy l -pktk tUte3 ,3 ' -Dick l t tBb«Bi i l iB it i i t t<«)ti tkncti tb i f - ( 2 - C l k T [ B « i y U p k t k t i i ( *CkryteieOi-i-«ctyl p h t k t U t il - i t i tbXliirai tkiBiIl*It(t)f I l t fUtkt l t

liBiedlpytiiilBdiM(l , l ,3-cOpfrntoibitt*u,k)ii tk[iciBti t n« (gk i )p i iy t iBC

< q k g

310 911B4 0HOD U311 U310 9370 9374 9370 9374 D1701 91744 V374 Q374 9314 9

__U40 9/ soTI

1TTTT134 BJ370 9314 D310 9710 9310 9410 1374 D370 9314 9370 9314 9314 9370 9314 9

{1)-Cannot bt fiparattd Iro» diphcnylamin*

FORM 1

Case Mo

Organic; Anafyiis Data Shoot(Page 3)

Pesticide/PCBs

Concentration: (Low^ Medium (Circle One) GPC (— L - 74 "?-yOil* Fjrtracf*d/Pr*riar*rt U • * { -&/_ ^-^r

O*tf Anrntyrrd l^^-\/. r/wifi

f!ftnc/Dil Far-Tor- /

pfrr^ni Moicrurp (ri<*fjini*rf) _ /->.»

CASNumtw

319-84-6319 85-7319-86-858-89-976-44-8309-00-21024-57-3959-98-860-57-172-55-9*72-20-S33213-65-972-54-fl1031-07-8[SO- 29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21 -912672-29-611097-69-111096-82-S

Aloha -BMC

8eia-8HC0«iia-6HCGamma -8HC (L'ndanet

HeptachlorAldfin

Kepiachhx EpoirieEndosutfan 1Oteldrin

4.4--OOEEndrtnEndosoHan fl4. 4--OOOEndosutfan SuH*ie4.4--ODT - *MethOKychlor

Eodrin KetoneChlordaneToiapfeeneArocfor-1016

A/octof-1221Arocioc-1232Afocio^-1242Afocio*-12-»8AroCl<K-1254

A<oc(o*-1260

êanup CSYes C

a fory Funnel Ex-

luous Liquid - L

ug/lor£ig/Ka,(CircfiTjnc]

((P.O M./t . 0 fl

/^.O tL- /6.0 «

/6.O Uff,.0 «,/t.o «/l.O K

JW-O U..- .o «.JEa.d «.*33^J U3$>0 UJ3^5 tt.

•33-<& tl1 1 d. I/.

JJ. > «

/tA^> U

330.& W

/ .O tt

/ d. > «

^d,-0 «/ 5u5 UM6.O «.J3d, tt3^3. 0 U.

V

V- % Volume of ectraci injected (u(J


W( * Wfrigtn of cample extracted (g)

Vc « Volume «4 total extracs Ml

orW. . C 1 -Xl--'

• Of III 1 7/8S


Ai\*tr£t£ Oat* Sheet

«~vUN~mb«


CAS

CT

z 7-7^-C.

7..

2/t«*

10.n.

S3HM16..

19. 3CLs:

2*.

27.,

in

n

r *

Ocganics Analysis Data Sheet(Page 1) !--

Sample Number: EK863

J4bLabor at ory Name:Lib Sample ID NoSamp 1 • Mat r ii :

ENVIRODYNE87003143SOIL

Datt Release Authorised By

Cast No: 7 3 5 1QC R e p o r t No:C o n t r a c t No: {&j?"*D a t t S a m p l e R e c e i v e d

~ 70

Volat iIt Compounds

Concent rit i on: LOWDatt E x t r a c t e d / P r e p a r e d :Datt Analysed: 4-26-87Conc/Di1 Fact or: 1Ptrctnt Moi s t u r e (not decanted) 1 7 . 3 4

CIS Me:

74-17-374-13-t75-11-475-10-375-H-247-44-175-13-175-35-473-34-3ISi-il-S(7-ii-I1I7-U-271-tJ-J71-5S-431-23-5111-03-473-27-4

Ckliromitkaii 1IteieittkiniViiTl Cklnidi 1CklereetkaaeKetkTliti CkierideIceteteCatkoi Difilfide1,1-DickioreitkiBcl.l-Dickletietkaietrais-l,2'DickIiiiitkiiiCklirefera1,2-Oieklereetkaie2-letaiite1.1.1-TcieklereetkaiiCatket TitrackleiideTiifl Acetatelt»edlckleie»etkaia

2 V2 02 V1 V31 144 15QBVI12 0V1

12 VI V

CIS He:

71-17-5l l l f l - l l -<71-11-4124-41-171-ll-S71-43-2lllil-ll-5111-75-173-23-1lll-ll-lSfl-71-4117-11-47J-I4-S1II-II-3lll-M-7111-41-4111-42-5

•fl

l ,2-DickI«r t i i ip i i ittaii-l.i-OickleiiiioH"TriekleriitkiuDikriioekliieutkaii1,1.1-TrickIereetkaiileitiiieii-1 , J -DtckUroi topt t t2 -CkIen i tk r ln iy I i tk i tli*mefera4-Hitkyl-2-piitami2-biaieiiTitraeklireitkiie1,1,1.1-TitracklereetkaiiTel • HICklirikett*iittkyikeisiieStfteieTetal Ifltin

H

VVVVu0a

i iV

12 1\ 11IDI9Ua

Dili lipittiif Q i a l i f l e t f

VaLUI:If tki itMlt ii a tain friatu tkii it «<nl ti tki <ttieti»liiit, fipott tfci tain.I:f i i ic i t t f eaii on 4 was aialf"' («r lit lit 4eticti4. Itpttt tkt•inin «it*etl» l int (ii tit lampli witk tki I df . l lU) lisidei iteifsatr c»c»t./41Ittiit actlti . (Tlii if let iictfianlftkt i«ttn«it i t t ie l iM lint ) Tkt dotiiti ikoi i i rud 0-C»Mpiii< was aialTi*4 (tr kit nt i i t ic l td. Tie tnkti ti tkaBitiin a t ta i iak l i r f i t ie t io i lint fir tki taapli.

Iiiicitu ii nHutid filn nit f l a g is •••* i l tk i t whettitiiatiti a eeteiitratiet Iir tettiUulf i € i t t i ( U 4vkiie a 1:1 iistotse is aisaed et wket tki iaii iiicttal lataitUeita* tke irintci ef a ciiteiid tk i t leitf tki i l e i t i f i ea t l o tc t i t i r ia kit tki unit Is Im tkai tke > M c i f i i 4 let ict i i t l intI t iat ir tkai mi ( i f , 1 IJ ) . If l in t ef 4it iet i» ii II til aid t

C:Tkit flaf apilin te p e s t i c i d e inuttdi wken tki idntifiei-tlei was cotfirud k| CC/RS. Sitale cimpaiett i*ftfcides)»!!tf/il it tke fital uttact ikield ke citfirted kf CC/KSI: -Tkis flaf ii tied wkit atalfti Ii fend it klitk at will it amill It itdicates piiitkli/icikikli klail ciitaiiittiii udwarn tki data eiic ti taki a p p t i p r i i t e ictiai.OTHH:Otket flaff aid (eettitit ma; ke teqtited te proiitly difititke tesiitfl. If end, tkiy »it ke I i i l f deictiktd aid tickdeieiiptiet attacked ti tke data traitT upott.

kit

Labor& t ory Nine:Cast No: 7351

ENVIRODYNE Simple Number: EM84

Organic* Analysis Data Shttt(Ptgt 2)

Seftivolitil* Compound!

t E i t r a c t e d / P r e p a r e d : 4 -24 -87t A n a l y x e d : 7 - 2 - 6 ?: / D i I F a c t o r : 1c e n t M o i s t u r e ( d e c a n t e d ) : 1 7 . 3 4

CIS N»:

101-95-Z111-44-493-37-1541-71-1114-44-7110-Sl-i95-50-19S-4I-73f43l-3Z-9114-14-3•21-44-747-72-191-95-371-39-111-75-5115-47-945-13-1111-M-liii-n-i120-12-191-Z8-3104-47-117-41-339-51-791-37-477-47-4ll-Oi-Z93-93-4Jl-31-711-71-1131-11-3ZII-94-199-19-2

fhlBOlki i - (2-CUomtk?n«t fc t t2-Ckloropketol1,3-DickIarobeiti ie1,1-Qieklflrokentenileityl Ucokai1.2-DiekIerobeBitBe2 - K i t k y l f k e i o Ib i i - ( Z - C k I o r « i i c p r o p f I ) e t k i r4-Hitkj l iki i i IM-iitr«o-Di-i-irotyIi«iieItittaliMttkiBiRitr«b«BiiBtIitikoioii2-KitropieMl1,1-OimttkylphiBolItncic lci<k i i - (Ck lo io« tk» i j ) l f» tk4«Z,1-DickUropkeieII , l ,4 -Tr ick l i r»b«i i«a»Kipktfc i l tn1-Cklore»iliieKeiaekler ibst idi i ie1-CkIore-l- i t tkyIpkii t lZ-Rt tky l i ipb tk i l en iEtiachlir iCTcIapCBUfl ' i tBiZ,1 ,4-Tr ieklor«fhtBiI2,4.3-TriekIiropkiBOl2-CkloroiapklhaliBi -2-Mi t re iBi l iBtDimethyl y k t k a l a t eIciBiptkyliBi3-Mittitiiltii

Sep .C e n t

•III

401 9111 9110 9101 9400 9100 Q111 9401 9401 9411 9111 9401 9111 9400 9401 9401 91901 9411 9401 9400 9400 9410 1411 9400 9400 9401 9411 91910 9400 01900 9401 9401 91901 9

F u n n e l E i t r a c t i o n : YES (JiG^ c i r c Iin. L i q . - L i q . E i t . : YES ( N O j ( c i r c ]

US Me:

13-32-951-ZI-3111-12-713Z-44-9111-14-1414-10-114-44-27015-72-314-73-7111-11-4534-32-1U-30-4101-53-1HI-74-1I7-I4-S15-11-1111-11-711-74-2104-44-01Z9-II-013-41-791-94-154-55-3117-11-7211-11-9117-14-0ZI5-f9-ZZI7-OI-93I-JI-I193-39-333-71-1191-14-2

-

IcciapktkiBiZ . I -Qi i i tMfk t io l4-Nitropbti«IOibiiiedraiZ,4-DiiitriteIteii1,4-DiBit r i t i InuD i i t k y l pk tk i l a te4 - C k I e r a p k t t f l - p k n y l i tk t rFlttllBt

4-litreaBiIiii1,4-OiBitre-Z-RetkyIpkiBtIR-iitr»iidi|hiif luiBe (1>l-lromepkeiyl-fkii;! etket•iiackliMbmit*FtiticklirtiknelPkiiiitkniiUtkraeeBeBi-i-bityl p k t k a l a t iFlitnitktiiPyriBiI t t r l - b i B t f l - f k t k a U t f fl ,3 ' -DltkU(«biat idi ieleise(4}aitfcracitel i i - (Z-E tky lke iy t ) ik tk iUt iCkryieBiOi-i-ictyl i k t k a l a t elllll(lt(ll(Tll thillIiBtefktf IiirutkutleBit(a)fyriieIi4»«(t,l.l-cd>pT"ieBikiiiid.klaitkiictiiItiii{|ki)ptrytiii

e one )I e one >

t f l t j

111 9I f l l 9I f l l 9111 Q401 9111 9111 9111 Q111 91911 DIfll D111 9110 9111 9I f lO 9

OH)401 9141 BJIII 9lie 9401 DIII 0111 9til 1ni y >

1 11 A J111 9111 0111 9410 9401 0111 0

<I)-Cannot b« tepartted fiom diphtnylamin*

FORM I

No

Organic* Analysts Data Shoot(Page 3)

Pcsticide/PCBs

Concentration. ( LowJ Medium

Date Extracted'Prepared ____£_T

Date Analyzed: ____/""•("" V/.

Cone/Oil Factor: I_______

(Grde OneJ GPC Cleanup C3ês ONo

Separatory Funnel Extraction OYes


-nr>(SI


CAS

319-84-6319-85-7

319-86-858-89-976-44-8309-00-21024-57-3959-98-660-57-172-55-972-20-833213-65-972-54-fi1031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-S53469-21 -912672-29-611097-69-111096-82-5

Alpha -BMCBeia-BHC

Oeita-BMCGamma-BHC (LtndjnelHeptachtorAJdnnHeptacnlor £po«id«Endosutfan 1Oieldrin4. 4--OOEEndrinEndosuHjn 0

4. 4'-DDOEndosutfan Sutfate4. 4'-DOT *MetfwxvctUorEndrin KetoneChlordaneTotapneneA/octor-1016

A/octor-1221Aroctor-1232A/odor-1242

A/ockx-1248

A/ockK-1254Arod<x-I260

ft,.0 U./L.O MIL.O H

., /t,,o atC-O Uit,.o u./(nO U.tL.Q t*.

J3-0 U-.-o.o ajjj.d U.

' *33^> M.XP,o 14.32-0 «

" ja^> «!(.£>.£> U

JS.O «iu>,o Ujad. ult&,& ull£>.£> U

&£.& U/£O.& UIL6.O UJ2d. U3ZO.O tjL

V( * Volume of extract infected (uf|

V * Volume o* water eAracied (ml)

W( * Weight o* campfe extracted (gl

V( * Volume of lot*! extract (ut)

7/85


Orpamcx An*fy*J£ O*t» Sheet(P»9e4)

T*nutreaty Id*oti5od Compounds

0ann-o•3

Orginici Analysis Data Shift(Page 1)

Laboratory Name: ENVIRODYNELab Si up It ID No: B7003H4Simple M a t r i i : SOILData Reltast Aathociitd By:

Case No: 7351QC Repor t No:Contract No: _____Datt Sample Rece ifed

Volatile Compounds

Concent rat i on: LOWDate E i t r a c t e d / P r t p a r e d :Date Analyzed: 4-24-87Cenc/DU Factor: 1Percent M o i s t u r e (not decanted) 22 ?3

-no

Simplf Numbtr: EM864:rn:OJ COm-o

oo

CIS No: •fkf CIS Mo tgkq

74-17-374-13-f73-11-475-00-373-lf-I»7-«4-l73-13-073-33-473-34-315t-iO-5i7~ii-l117-01-27M3-371-33-*34*13-3111-13-473-M-4

Ckliromitk»e 1Irotomttktni 1Tiiyl Ckl i r id i 1Cklonitkaai 1Rithyl i ie C k l i r i d iicitoaeCarboa D t s i l f i d el, l-Dickloriitli»i1,1-Dicklirietktiitr»f-l,2-DickliroitkiiiC k l i r i f i r m1,1-Dieklirietkiii2-lit»«ie1.1,1-TrickliroetkaiiCarbon Tetuckloi ideTiiyl acetateI r imodickUi imi tk in

3 U3 D3 V] V41 104 I000aV•

3 D09

13 V1 0

7I-I7-SUOil-02-i7»-01-4114-40-17f-00-S71-43-:lflOil-01-Siie-73-i73-I3-Illl-tl-t3M-73-4117-11-471-34-3tll-ll-1110-10-7111-41-4111-42-5

1,1-DickIiieprepiietnn-l ,3-Bickloroprop«niTr i tk lo r i i tk tBiBibtomockloroutkiBe1,1,1-TrickIorntkiatIIBIIIIc i f f - l , 3 - D i e k l o r i p r o p » el -Ck lo t i i t ky l i i i f l i t k i rI romofon4-Hitkyl-l-putaaeii1-IeiaieiiTitraeklirutkiii1,1,2.2-Titrackliroitkii tTiluniCkleriktiimEtkf IktticnStfrneTlllI I f l lB t f

V00uV00

13 UU

11 93 1

nVD90V0

Dati Itportitq Qitlifitii

flLtrt:If tki resilt ii a ralie frutir tk» «r MDI! ti tki ditictittliiit, report tki Title.9:Iidicatis ttmpaiid vtf aBalyted (ir bit lit <ettcUd. leport tke•itiin dttictiii limit fir tke sample witk tki I (i|,UU) lased•i iicisstry eeiceit./diliti»i utioi. (Tkii it let ieci«f«iilrthe iutrncit ditictiia l i m i t . ) Hi feitnti ikiild rud: V-CoKfiHd vti itilftid fir kit lit dttictid. Tki aabir ii tke•ililts ittttiibl* delicti!! limit fir tki iimple.J:Indicate! » iitimi.tid valie. Tkit flaf ii lied iltker vkiieitimatiif i ceBctitratioi fir tutatirily i d i i t i f i i d cotiondivmiri i 1:1 retpoiie if aimed n "kti tke mait spictrtl ditalidleited tki presiBce if a etmpond tkat mutt tki idiitifieatioieritirti kit tki reult Ii lesi tk» tki ipieifiid ditictioi limit

C:Tki i (I»j ippliis ti |i>ticidi paruitirt wkcn tki i d e n t i f i e rtin vii ciifirmid by CC/KS. Siifli componit p i f t i c t d i i ) « l l•t/il ii tke fiaal eitrtet ikitld be ciitirmid by CC/KSI : . - . . - . . -.:_.Thii (Uf If tied vk» aiilyte it find ti bluk 11 well as aitipli. It tidteites ifistkli/irobtble blaik ciituiiitiiB ind•atBi tki ditt iser ti tike ipproitiite ictiiB.OTHU:Otker (lags ltd feotiotii miy be riîirid ti p i e p e r l y didiitki r e f i l l * . If icid, tkiy net bi f i l l y dner tb td iid tickdeicr ipt io i i t t ickid ti tke data inmiry r ip i t t .

bit

-n

L*bon t ory N«atCast N o : 7 3 5 1

ENVIRODYNE SiBplt Number: EM664

Organic* Ana Iyiif Dat a Shttt(Figt 2)

Stmi»o1 at iIt Compounds

e E i t n c t e d / P r e p a t e d : 6 - 2 4 - 8 7• A n a l y z e d : 7 - 2 - 87c / D i l F a c t o r : 1ctnt M o i s t u r e ( d e c a n t e d ) : 2 2

US Me:

101-93-1111-44-495-37-1341-73-1114-44-7111-31-493-31-193-41-739131-31-9114-44-3411-44-747-71-1H-93-171-Sf-t11-73-3119-47-945-15-1111-91-1111-13-1UI-II-1tl-20-3114-47-117-41-359-5B-791-37-477-47-411-14-293-93-191-31-711-74-4131-11-31BI-94-I99-*t-l

Fhuili i f -a-aionttkyhttkirl-Ckloropkei«l1 ,3-Dickl ir i f t i i t i i il ,4-DickIit»biit»Blinyl l lcaki ll ,Z-DickloE«biniu1-Ritkf Ipk iBo lk i f l - (Z -CkIe i o i i i p ropy I ) i t k i r4-HitkrlpkiialN-iitr«ii-Di-i-propTluinleiicklinetktiflIttl lklBSIM

IfitketuiZ-Kitttpk»«Il,4-OiHtky[yk*»lliBisie UHk iB - (CkIoro i tk i iT>Hc tk i»1 ,4 -D ickIaropk iBo l1,1,4-Ttickli i ibBitBitItpkthtllBI

4-Cklor i iBi l i t el incklartiBtidiiBi4-Cklirt-l-MtkTlpkinl1-ItitkTli ipktkiIi i iIii ickltricyclgpiitidiiii1.4 ,4-Trtekl irvpkei i l2 .4 ,3 -Tr ickI iMpkiBi l2-CkUr»ipktkiI»e2-l lttmilUiBiictkjl BktkiUtiactBiptkyli i i3 -Ki t ro iB i l iB t

S e p .Cont

. ? 3

«•>.431 V431 1431 B431 V43B B43B V43B V43ft B431 B431 043B B41B B111 V111 113B 0431 B1111 V431 B131 9431 B411 043B B431 B431 B43B 0431 V431 Bmi o

: _ 431 V -1111 V431 V431 B1111 B

F u n n e l E i t r a c t i o n : Y E S f m / t c i r c Ii n . L i q . - L i q . E i t . : YES7^ ) ( c i r c I

US Mo:

13-31-f31-1B-31IB-B1-713Z-44-9111-14-14B4-1I-114-44-17IIS-71-1B4-73-71IB-I1-4334-31-1B4-3I-4111-33-3111-74-117-14-3I3-B1-I111-11-7B4-74-11B4-44 -B129-IB-fl15-41-791-94-134-33-1117-11-7111-11-9117-14-11B5-T9-Z1I7-BI-I31-11-1193-39-333-71-1191-Z4-Z

IctBipktkcii1 ,4-Di i i tnpkiBoll-XitripkiioIBibtuofirii1 ,4 -D i i i t r i t o I i iB i1 ,4-Dl i i t i i toI i iuB i i t k y l pk tk i l i t i4-CkI»rcphiByI -pktsyI i t h e rFluriiB4-Kit i«t i l I i i t4 .*-Dit i t i t - I -Httkylpki i« ll - i i t iosidlfkBirluiBB t t )4-liBB»pkti.yl-pk»yl itknIiiieklitBbiiiiiiFtitickloteibiBolFkiiiatkriiBiitkrietuBi-i-bityl pk th i l i t iFllOraatktlt

FT milityl-tiBiTl-pktkilitt3 , 3 ' -D i tk l i i i b tB i i d iB iItiiidliitkuciiil i s - ( l -E tk j l k« i ynpk th iUdCkrfi iBtDi-i-tcly! pk tk i l i t il iB i i (k ) f l i i r i i tk ia il iB i i (k) l l t i r lit kmliin(i)pfriitI idi t«( l , l 13-ci '} iTriBiBikmid.kl i i tkrict i il i i i i (ok i )p irr l i i i

e one )e one )

iqi;

431 U1111 Ut i l l 0431 B431 B430 1411 Bue Q431 1mi Bmi B431 B411 f411 Bn i i B/nn

^3lT111 8J431 B411 B431 8Id B431 Bt!i 3J431 B431 B411 B411 B411 a431 B431 B411 B

(l)-Cannot be ttparattd from diphtnylamint

.-:" -T ":"-" -"-'FORH 1

Laboratory

Cate No

Ac..


Concentration: (Low^) Medium (Crete One)

Date Extracted''Prepared: ____*L

Date Analyzed: '^~ -f \Z

Factor:

Pesticide/PCS s

GPC Oeanup QYes ONo

Separato/Y Funnel Extraction OYes


(-0


CAS uo./lorkg/Kg.Numb** . (CircfiTUne)

319-84-6319-8S-7

319-86-858-89-976-44-8309-00-21024-57-3959-98460-S7-t72-SS-91

72-20-S33213-65-972-54-81031-07-$50-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-S53*69-21-912672-29-611097-69-111096-82-5

Alpha -BMC

Be»-BHCD«lta-8HCGamma-BHC (LtrxJjoelHcpt»ch»orAWftn

Keoiactikx EpoxideEndotulfan IOtddrin4. 4--ODEEndfirt

EndosuKan fl4. 4'-ODOEndocuffan SuHaie4. 4--OOT *Metttoxyctilor

Endrm KeioneChkKdarwToxjf>t>er>eArocfcx-1016A/ockx-1221Aroc«of-1232AfodOf-1242

Arcx^<X-1248

Aroc*oc-12S4

Ar odor -1260

Kr.O 0.

rL.f> ti1L.O IL

.- /6.0 U

&.o atf,.0 U./t-o «__/t.o KJ*.0 «.^5.0 U.

â-o a' *aao «.

^P-o ttJ3^3 t<

f ja^) u/to.^> itJ-7-0 «

KrAO U

330.& U; >. u1^0.0 U&A.O UItAJ> UI16.O U.330.Q a320.O U.

V- * Volume of extract injected (ul|


W « We«otn of cample extracted (gl

V( * Volume of total extract full

orW.

Form 1 7/8S

Envirodyne Engineers^

Sheet(Page 4)

ld«ntir«d

r>T

C/3m-o

1

L a b o r a t o r y N a a t : E N V I R O D Y N EL a b S a m p l t I D N o : 8 7 0 0 3 1 4 3Saap 11 Mat r ii: SOILD a t a R t l c a i e A a t h o r i s t d B y :

Organic* Analfsis Data Shctt<Pagc 1) :--

N u B b t r : E M 0 6 5t -

Cai* No: 7351QC Report No:Cont ract No: _Datt Saaplt Rictivid:

Vo1 at iIt Compound!

Conctntration: LOWDatt E i t r a c t i d / P r t p a r t d :Datt Analyzed: 4-16-87Conc/Di1 Factor: 1Ptrctnt Moisturt (not decanttd) 1 1 8 6

CIS No: CiS No:

74-17-374-13-173-11-4T3-BI-373-lf-Z47-H-l73-tS-l75-33-473-34-313i-il-3i7-i*-J1I7-K-271-93-371-33-431-13-3101-43-473-27-4

Cklor iMotkaiolr»»otkaioTiiy! CkloridoCklireitkanHitkflii i C k l o r i d oAc it inCukei D i n l f l d i1 ,1-OickIoro i tkcBO1,1-QickIorootkaBOtraif-1.2-Dick1i[oitkiioCktor i forel .Z-Oieklir i i tkato2-litanit1,1,1-TrickIiriitkanCarkoi Ti t raeki i r id iTti f l icotatoIr iBidiekloroMtkaio

3 03 Q3 03 0U 1If 1Q0DIVI

3 0V9

13 QI 0

7I-I7-Slllil-12-i79-ll-i124-41-17f-ll-371-43-2iiiti-u-5iie-73-i75-25-2lll-ll-lSM-71-4127-11-471-34-3lll-ll-llll-M-7111-41-4111-42-3

1 ,2-Dick loroprop in <t r a i f - l , 3 - D i c k I o r i p t o p i n iTrickloriothoio IDikimcki or e« thin1,1 ,1-Tr ickIoiootk iBo 1lOBIOBO 4eii-1, J -Di t l l c r e i r ep in t (2-CkI f i ro i t i fU iBTl i t h i rIroBifon 14-NitkfI-l-piitaiin2-Htia»nTitrackloriotkoio1,1 ,2 ,2-Totracklor iotkaioTolioioCkloroonioiot t k f l k O I I O l OStyronTotal Xjl t i i i

V0VB900

3 09

3 13 09001

1 IJ00

Data I tport i i f Q i a l l f i i r i

ViLfft:If tkt r tin It it a Tilai inatir tkai ir cival t« tki dittctiiiItiit, riport tkt rain.V:Iiditatts cimpiud wn nalfiid Itr kit itt diticttd loport tki• iiiin dotoetioB Iii.it for tki ia»plt nitk tkt Q (of.HD) katid01 ueissarj eiicnt./dilitiii aetiii. (Tkii it itt iieiifarilftht iBitrniBt dotictiii liiit.l Tko ftoticto ikoill toad: 0-

vas iialyitd fat kit »t iitictid. no tabor It tkoitttiiiilc doUctioi limit for tki lutlo.

11 i ittutod talio. Tkli fU| if ind oi tki t vkii• coicntratioi fit Ui tat l fo l f Id t i t i f i i t eoifondf

wkno a 1:1 iiiioBio ii iiiaod or wfcti tko uis ipoctral dataitdlc<tt< tko ironic* of t coipoiid tkat Hiitt tko Id i i t i f ieat lo ic r i t i r i a kit tki milt ii Itn tkai tko t p i c i f i i d dotict i i i liiit

C:Tkif fltf ippUof to p i i t i e i d i paraiottri vkitc tko t d i n t i f i c i -tin "ii eiifirud if CC/HS. Siifli eoipeioit t t f t i c i d c i ) « l l•f/tl it tki fiial oitraet «k»ld ki cnfirnd kf CC/KSI: . _Tkif flag if ifid vfcot aialfto it find ii kltnt at mil n a•a>pli. It iidicatii lofiikli/priiibli klaik eiituiaatliB ndvarif tko data nor to taki a p p r i p r i a t i actin.OTHU:Otkir tla«f aid teitietii mty It tiqiittd to fitftilj difintki roiiltf. If n*4, tkif Kift ki f i l l y d o t e r i b o d aid ncfcdncriptlii attackid ti tki data inmair ripott.

lit

Labor at ory NamtCast No: 7351

ENVIRODYNE Saaplt Namb«r: EMB65

Organic* Analysis Data Shut(Fagt 2)

i1* Co»poandi

t E i t r a c t e d / P r t p i r e d : 6 - 2 4 - 8 7t A n a l y s e d : 7 -2 -87: / D i l F a c t o r : 1cent M o i s t u r e ( d e c a n t e d ) : 2 1 . 8 6

CIS No:

iii-ts-:111-44-4T3-37-I341-71-1114-44-Tuo-51-475-31-173-41-73f(3l -32-t104-44-3ill-44'747-71-1M-73-371-Sf-l11-75-5113-47-f43-13-1l l t - f l -1121-13-2UI-12-1fl -20-3114-47-117-41-33I-SO-771-57-477-47-411-14-2?3-f3-4tl-31-711-74-4Ul-11-32II-U-IM-l?-2

Fktiell i i - ( 2 -CkI« [« i t ky t ) i t k i r2-CkIiropkiiall , 3 -0 iek l«r»bt i i f l i tl ,4 -DickI0tot iBi t»l i i t ft l lcobol1,2-DitkUrobtfiiiat1 -Ht tky lpkt iv lk i i - ( l -CkIoro i i »pr0py l ) i tk i r4-Kitkf lpki iQlM-iitraii-Di-i-proiyluUeIttiekUtMtkiatXitrtbiiitu(i«pkar««i2-Kitnpkiiil1,4-DiBitkylpkti i lBencic icilk i f l -<CkI t to i tk« iy )Ht tkn il ,4 -DiekIor«ph»oI1,2,4-Ti iekliiibtutitMapklkaUie4-CkIoteaai l i i eEtiichUrabittdiini4-Ckleri-3'UtkyIpkiaol2-H*tky[iapktkil«atItnckltitcycUptitaliiBi1,4.4-TricklaropkeitI2,4 ,3-Ti ickUrBphnol2-CkUt«itpktktIiit2-Kittmili i iDiMtky l pktka la teIcnaptkyUit3 -Ni t t»a i i l i i i

S e p . F u n n e l E i t r a c t i o n : YES AjnJ( c i r c I e o n e )C o n t i n . L i q . - L i q . E i t . : YES p^P < c i r c 1 e on* )

•111

421 Q410 1411 V411 I421 0421 V410 V410 U411 V411 I420 9411 I411 U420 1410 V410 11000 0410 1421 Q421 1421 0420 Q421 U420 0421 V42fl V120 02000 D410 02100 Q421 9421 92111 D

CIS No:

13-31-f31-11-3101-11-7131-44-f111-14-1484-11-214-44-17013-71-314-71-7110-01-1334-32-1I4-3M101-33-3111-74-117-14-313-OUI110-11-704-74-1104-44-1llf-00-913-41-7M-14-134-35-1117-11-7l l l - l l - f117-14-02I3-M-11I7-M-?30-11-1H3-1I-333-71.3171-14-1

actaipktkiu1 ,4 -D i i i t t tpk t t o l4-Nitropkti i lDibet iof i i t i1 ,4-Di i i tr i t i I i ia il , i -0 i i i tr»t i l i« i«Dlitkyl iktkilati4-Ckloropki iy 1-pkaayl otkctFluriai4-Nltroaii l i i i4, i -Di i i tr i -2-f letkylpki i«IH-i itroi*tf ipkiaylaBiae (1)4-Braiepkttf I-pknyl i tkicItitckl»tob«iit»PiitacklortpkiialfkiaaitkriitUtkraeiieDi -a -b i ty l p k t k i l t t iriittiitkiBtPfrml i tT l -b ia ty l - ik tka l i t eJ ,r-DiekUr6l inni i i iItiioUUitknctilb i s -d -E tky lk i i rDpktk tUt tCkryitaiOi-a-oetyl pktktlitiIt i i t lblUiaraatktaiB»i«(k) f l i« t» tk i icB»i*{a}pytt»lit'iiid.l.J-ci'lpTrtaeDibei i«(a ,k) i t tkiaciailt i i»(fi i}pit |Itat

MM

410 9llll U2111 Q411 Q421 9411 9411 0411 9411 9llll 92111 9411 9411 9411 9llll 9411 U411 9Ul BJ411 0411 9111 U111 9411 Q411 BJ411 Q/jHD* <iiV411 9410 9411 0421 9111 9

(1)-Cannot b* ftparattd from diphtnyiamint

FORK 1

Laboratory Ac.-

Organics Analysis Data Sheot(Page 3)

Concentration: fiLow/ Medium

Date Extracted'Prepared: ____*LL

Date Analyzed: ____'j.

(Crete OneJPosticide/PCBs

GPC Cleanup Q'v'e* QNo

Separatory Funnel Extraction


X)mom<:mo

COm

Cone/Oil Factor:


CAS

319-84-6319 85-7319-86-858-89-9

76-44-8309-00-21024.57-3959-98-860-57-172-55-972-2O-S33213-65-972-54-81031-07-850-29-372-43-553494-70-557-74-98001-35-212674-11-211104-28-211141-16-553469-21-912672-29-6

11097-69-111096-82-5

Alpha-BHC0*ta-8HCD*lia-BHCGammj-BHC(L«odar»ei

HeptacWorAldrtn

Hepiachtor Epo»deEndosulfan 1DteWfin

4.4--O06EndrinEndoswHan fl4, 4--OOOEndosuffan Sutfaie4, 4--ODT ^Mettx>crchlorErtdrin KetooeCritordaneTocapOeneA/octor-1016A/ockH-1221Aroctot-1232Aroclor-1242A/octo^-1248Aroc tor- 1254

Aroctor-1260

iL.o a/ t .O /AIt.O tL

.- t(,.e> ai<>.o atf,.O U.tl,.O Uti.O Af.

J3.0 U..-53.0 U.

Ss.o U.' *33-O U

JP'O W520 «.

" J3.0 «/tO.£> U.

31. & U

IL6.0 UJtJd. > U]ô.o u/£.£>.& U£6.6 U/U>4> U/60.O U.330.6 ^3^.O fct

V- * Volume of extract infected (ul|


Ws « Weight of cample extracted (g|

V( « Volume of total extract (ul)

orW.

7/85

Erwirodyne Eng ineers

antes Analysis Oat* Sheet

T«ntfttivatY M*otifi*d Compounds

:0Organic* Analysis Data Shtkt

/o . -. i^ >._(P*gt 1Nuabcr: EK8&6

L»bor»tory Niai ENVIRODYNELab Saapli ID No: 17003146Simplt Matrii SOILData Rtltast Authorized By:

Cast No: 7351QC Rtport No: __Contract No: <£ &•Datt Samp It Rtctivtd

Vo I at i11 Compounds

Concent rat ion: LOWDatt E i t r t c t t d / P r i p a r i d :Datt Analysed: 6-26-87Conc/DiI Factor: 1Pi rcent Mo is tur t (not dtcanttd)

&// ff? 7

13.48

US No CIS le:

74-17-374-13-173-11-4.73-IB-J75-lf-l17-44-173-13-B73-13-473-14-3134-il-*47-44-3117-14-271-fl-S71-33-434-13-3tll-«3-473-17-4

CkleieiitkiitItoiiittkaitTiiyi Cki i t td tCklototthiniHitkylni Ckl t i id tIcitlBI

Catben D i i i l f i d tl . l -Dieklot t t tkt i t1,1-DiekIiititkintrats-l,l-Di£kItriitk»tCklit«(«rmt,2-0icklir»tkait2-litaiui1,1,1-TriekltctttkiitCitbn TttiaekUildtTiiyl iciUttliindickl HIM I kail

11 BU 013 B11 B111 14f 1

7 B7 87 B7 B7 B7 B13 V7 87 B11 B7 B

7I-I7-S11*41-11-47t-ll-4114-41-177-11-371-43-111141-11-3111-75-175-23-1lll-ll-lW-71-4127-11-471-14-3lll-ll-liu-ri-7111-41-4111-43-3

1,1-DickUrtpropantrati- i . l -DicbloropropiniTttcklonitkmHifcriaiekloriittkaii1,1.1-TriikIouiUanilimitc i i - l . l -DUkloro frap iB i1 - C k I i t o i t k y I f i B y I i t k i iIroiaioral-Hltkyl-l-piitlBOii2-BliaintTitraekltrtttkiit1.1 ,2 .2-TtUatkIir i i tktnTtlititCkliribiBttiiItkTlkiiitiiStyrmT«UI If lilts •

7 B7 B7 07 87 B7 B7 B13 U7 B11 V11 I7 B7 B

1 IJT 07 B7 B7 B

Oitt liputiif Q i a l i t i i r i

T1WI:If tkt riinH ii a ftU» |tiatit tku it iqnl t* tki Itttctiialitit, tijott tki Ttlii.

«ti tiilriid fti kit ut iitietttf. Itpitt tktItttctiu l imi t ftr tkt ftk|lfl vitk tkt 0 <t« ,UO) kistd

•• itctfitry c»ct i t . /4t l i t i« i tetivi. (Tkis li itt itcitittiETtki iutttatit l i ttct ita l i m i t . ) Tkt (tfttiitt ikuld rtid: U-Cii|ind vn utlfi id fit kit ut dittct id. Tkt mbit ii tkt•iiim tttaiiaklt dtttctioi lliit (ir tkt fuplt.J:tidieaUf u •itimttU filn. Tin (U| ii uid k i tkt t wfeti•it ii4 tli| * ciiciitntiii for tut i t i f i l f Unt i f i id eei|endivktri i 1:1 riipoui ii tuned tt vku tkt usi ipictttl dtUfidicittd tki yristict if i t»poHd tkit »itti tkt tdtitlfleitiiBer i t t r i i kit tki rtult it Im tku tkt t p i c i f i t d dttittiii l im i t

Tkis fli| ippl i t i tt fisticidi fituittri vbtti tki i d i s t i f i e i -tlet vti etiHtiid by CC/HS. Siigti eo»p«itat p«tiei4«s>«llil/il ii tkt fiial utriet iiuld kt ctifiiaid by CC/K5I: --- _Tkif Iltf ii utd vkti »4tytt ii ftiid ii bl iak if mil if :•upU. It i idicitt i y i i f ik t i /yn l ib l i blank coituiutiii andwit u tki data ifti tt Ukt ipprsprUt i i c t io i ,OTHEI:Otktr fltqi ltd (titiitti Uf ki itqiind ti ftoptily dtfiittki tiiiltt It uid, tkty mt bi I i l l i ditcribid aid lickdiicii|ti» attackid tt tki dita ifmiaiy riport.

lit

L a b o r a t o r y N a m e : E N V 1 R O D Y N ECas t N o : 7351

Or g a n i cs

.

I S a m p l e N u m b e r : E M B 4 6

A n a l y s i f( P t g e 2

Semi v o l a t i l e

C o n c e n t r a t i o n : L O WD a t e E x t r a c t e d / P r e p a r e d : 7 -4 -87D a t e A n a l y z e d : 7 -9 -87C o n c / D i 1 F a c t o r : 1P e r c e n t M o i s t u r e ( d t c a n t t d ) : 2 3 . 4 8

CIS MB :

lll-fS-2 FkeBol111-44-4 b i i - ( 2 - C k l « T B i t k y l ) « t k i [73-57-1 I -CkUropkinol341-73-1 1,3-DitkIiniiiiBie114-44-7 1,4-OUkIorBteBitiitll-St-4 Iiityl UcBkBl•3-31-1 1.2-DiehlerBkeaiiBi•5-41-7 2 - K B t k f l p k B B B l3f43l-32-f k i i - (2 -CkIemiop t f l iy I ) i tke r114-44-5 4-lUtbyliktBBl421-44-7 M-aitroio-01-B-irBiylaftiie47-72-1 IntchUciitkiiBfl-13-3 litiokiitiBi71-St-l IiBpkBtBte11-73-3 1-Hitrtiktitl113-47-V 2 ,4-Di ie tkyI ik tBBl43-13-1 iBiSBie lei 4111-11-1 k i i - ( C k l B r B B t k B i T > K t t k a i e121-11-2 2 , 4 - D i c k l B f B p k t B B l121-12-1 1,2,4-TricklBrBkBiiBiBM-21-3 Kapktki lBae114-47-1 4-CalBrB»iI i ie17-41-3 •iiacBlorikitiiiiit31-51-7 -CklBte-3-ietkyIpkBiBlf 1-3 7-4 -HelbylupktkiltBe77-47-4 a iack l f r tcyc lBi tBta i ' iBa i11-04-2 ,4,4-Triekl tr«pkeaBlH-tS-4 ,4.3-TiickIitBikciolfl-SI-7 -Ckloraiipitkilt i t11-71-4 -litriaiiliie131-11-3 Bimetal ihtkiUte2II-T4-I IcHiptkyliiif f - l t -2 3-Nitroai i l iu

GPCS e p .C o n t

• gko

431 0431 1431 0431 0431 0431 0431 0431 0431 0431 9431 0431 9431 9431 9431 9431 92111 9 »431 9431 0431 9431 0431 9431 0431 9431 9431 9431 02111 0431 02111 0431 0431 02111 0

D a t a Shee t

*

C o m p o u n d f

C l e a n u p : NO s* —— VF u n n e l E x t r a c t i o n : YES f HZj( c i r c 1 e

V. jf~r£i n . L i q . - L i q

CIS MB:

13-32-f31-21-5111-12-7132-44-f121-14-2414-21-214-44-27«3-72-314-73-7ltl-ll-4334-32-114-31-4111-33-3111-74-117-14-3IS-ll-l121-12-714-74-2214-44-1m-n-i13-41-7M-f4-l34-33-3117-11-7211-ll-f117-14-12l3-?t-2117-ll-f31-32-1113-37-333-71-3l«l-24-2

Eit . : YES ( N D ^ M c i r c I t

Iciiapktkne2,4-Dii i t rBpki i f l l4-Nitr»iiBiilBibiatBfirti2,4-Diii tr i t i I icie2 ,4-DlBi t r i te I ie i iD i i t k y l iktUUte4 - C k l B f B p k i B y l - i k B i y ! e tkcrfliereBB4-MitrBtBil l i t4,4-Oiaitri-2-llitk;lpk»el1-BitreiBdiikBByIuiti (1)4-9rH*pkeiyI-pkiBf I etkBtliitcklitibttiiiiPuticklBrepbiialFkiiiitkctitaitkracBiBBi-i-fcBtyl p k t k t l t t iriitrntbtiiFyriBel i t r l -btBiyl-Bktki l i t i3,3 '-DiekIirBb»iidii ilean(i)tBtkr«ciBeb i i - ( 2 - E t k T l k t i y I } B b t f c t U t BCkiyieBiDl-i-BCtyl Bk tk iUt itut a (b) f l ie r tit butI t l f t t t l f I lBfUtkBBIItiioUliyriat .ti<»tU,l,3-c<)Bfrntt lb«IIt(t ,b)«BtkttCllf

9 e B i B < f k i ) p B i y l B H

30T1

ft?<

COm

LO

tooo" J

one )one )

•qtq

431 92111 02111 0411 0411 0411 0431 0411 0411 02111 02111 0411 0411 0431 02111 0431 0411 0341 BJ411 0411 0411 0Id 0411 0If l BJ431 0131 0411 0410 0411 0411 0411 0411 0

( l ) - C a n n o t b t f « p « r » t t d f r o m d i p h t n y l * » i n «

FORM I

Laboratory

NOOrganics Analysis Data Sheat

(Page 3)

Concentration: ( Low) Medium*—~-^Date Extracted 'Prepared

Date Analyzed; ____^2.

Pesticide/PCBs

(Circle One) GPC Cleanup GlYes QNo

Separator? Funnel Eirtradion QYes


Conc/Dil Factor: I


CAS og/l<Kfjg/KgNutnb«f . (GrcioTJo*)

319 84-6319-85-7319-86-858-89-976-44 -fl309-00-21024-57-3959-98-860-57-172-55-972-20-833213^5-972-54-81031-07-850-29-372-43-S53494-70-557-74.98001-35-212674-11-211104-28-211141-16-S53469-21-912672-29-611097-69-111096-82-5

Alph»-8HCBeta-BHCDelia- BHCG*mma-BHC (LindanelHeotacWorAJdr.n

Hepuenior EpoxKJeEndosu'fan 1Otetdrin

4. 4--OOEEnd/in

EndosuHan D4. 4--DOO

Endosuffan Sutfate4. 4'-DDT ^

Mettwicychlo*£ndrm KeioneChlordaneTOKJO*^*"*Aroctor-1016

A/oc(of-1221A/ocloe-1232Aroclcx-1242

A/odCK-1248AroClCK-1254

Arocttx-1260

/<..£> 6t/ t - o /I/t.O «_

- /6.0 W

/c.o alt,.0 U./4-0 «/i.O H

33-0 U..-w.o «.J3,o a<3JO «^P.o KJ3^3 t<

^J^» M/*.£>.£> U.

J .O «/t,AO U

330. £> U/£<9.<9 U/t.0.0 U.

&Q.O U]U>.£> UIL6.O Ujao.6 £/3ZO.O U.

a

V * Volume of extract *nfecied (ul|

V * Volume of wJier extracted (ml|

W * Weight of umpfe enracted (g|

V * Volume of total enract (ufl

7/85

Erwirodyne Engineers

Orp antes Analysis Data Sheet om

ld*ntifi*d Compounds o

0=

ecology and environment, inc.Ill WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415


Date Received for ReviewTO:From: Zena Gold-KaufmanSubject:

PAN:


Case I -?35/

Sample Description______Organics (VOA, ABN, Pest/PCB) Inorganics (Metals, Cyanide)

Low Soil *Low WaterDrinking WaterOther


froject Data Status


Completed


CI?DLdetected in

enclosed sheet-

Book No.

Compounds were detected in sampTe(s); see enclosed Chemical• Evaluation Form.(p__ Page No.

736"/

^

£/

/rV

p£6T

P6-5

COMPOUNDdimethyl phthaleteacenepthylena3-nltroanllinaacenaphthena2,4-dinltrophenol4-nitrophcnolaibiniof'ittn2,4-dlnitrotoluene '2,6-dlnltrotoluenedlethylphthalata4-chlorophenyl-phenyletherf lnorarm4-nltroanllina4,6-dJnitro-2-fltethy]phcnolN-nltrosodlphenylsmlne4-bromophenyl -phenyletherhexschlorobenzenapentachlorophenolphenanthrene•nthracenedl-n-butylphthalatefluoranthennbenzldin*pyrenebutylbenzylphthelata}, V-dlcMorobenridineben2o(a)anthraceneblt(2-«th)lhnxyl)pNthalat4chryaenedi-t-octylphthalat*ben2o(bik)rjuoranthen« 'benzo(a)pyrcn«Indano(1t2,3-cd)pyrenadlbenzo(aih)anthracenebanzo(q,h,l)pery]ane.lpha-6HCbett-8HCd«lta-6HCqafma-8HC(llndsne)heptachloraldrlnheptachlor epoxldeendosulfan Idlaldrin4.4'-M)eendrlnendosulfan II4, 4 '-000andrln aldehydeendoaulfan sulfate4,4'-OOTatethoxychlorendrln Ice tonecMordanotoxaphen*Aroclor-lOUAroclor-1221Aroclor-1232Aroclor-1242Aroclor-1248Aroclor-1254Aroclor-1260

r

Ul-J

5l/>

*

ter,f-lHiT

— t

IA

Sfc<?

S»/S£-— . ——— *•

•

»76

W^

^Ll \

tf\

)"

t

•• —————————

-

;

V0An

^,

,

HQO <Mio£L,s •COMPOUND t _ J

chlorowethanebrocwx&e thanevinyl chloridechloroelhanewelhylene chlorideecetonacarbon dlsulflde1, 1-<fichloroethene1,1-dJchloroeth«netranf-1i2,-dichloroelhenechloroform1,2-dlchloroethane2-butanona1,1,1-trlchloroe thanecarbon tetrachlorldevJnyl acetateb r o»od 1 ch 1 o r omet h ane1, 1,2,2-letrachloroethane1,2-dlchloropropanetran«-1»3-dlchloropropenetrlchloroethenedJbronochlorome thane1,1,2-lrJchloroethBnebenzenecle-1,3-dichloropropene2-chloroethylvlnyletherbrowoform2~hexanone4-tiethyl-2-pentBnonetetrachloroethenetoluen*chlorobenzen*•thylbenzenaatyran*total xyleneaN-nitroaodlaiethylsnlnephenol•nil In*bia(2-cMoroethyl)ether2-chlorophenol1,3-dlchlorobeniene1 ,4-dlcMorobenzenebenzyl alcohol1 , 2-dlcMorobenzena2 -«ethyl phenolbJi(2-cMorolsopropyl)ether4 -Methyl phenolH-nltroao-dl-n-propylamlnahexachloroethanenitrobenzeneJeophron*2-nitrophenol2, 4 -dlaethyl phenolbenzole acidbla(2-ch]oroethoxy}methane2.4-dichlorophenol1,2,4-trlcMorobenzenenapthalena4-chloro*nllin«hexachlorobutadlena4-chloro-3-«ethylphenol2-«ethylnapthalene 'hexacMorocyclopentadlene2.4, 6-tr Ichlorophenol2,4.5-trlchlorophenol2-chloronaphthalen* i?_n)t rr.«ni 1 1 ne

LJ

a.itfi

1

DfT.. . —hMtl

,

<*..

•

rnSfoQ

13"*

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\

fUNITED STATES ENVIRONMENTAL PROTECTION AGENCY / 4

REGION V

-, - Q\~L\~ Ql

DVTE : 4SUBJECT: Review of Region V CLP Data

Received for Review on___

F30M: Curtis Ross , Director (5SCRICentral Regional Laboratory

c i -rTO: Data User: F I T

We have reviewed the data for the fol lowing c a s e ( s ) .

SITE NAME : H Q D LANDF ILL ________SMO case No.____________~ ~~~—————No. of r D . U . / A c t i v i t y _ ,

EPA Data Set No. ^ 4l3b Samples: D Numbers 79Q5/C~JZJOQ

C R L No.________&1FP\\S1S ^ , - :

SMO'Traffic N6Vr—"~"r

.:_ :--Hrs. Required;— «'• V -for Review:- ^^

Following "are "our findings:'

Data are acceptable for use.{ v) Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory( ) Data are unacceptable.

cc: Duane Geuder, Quality Assurance Off icer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas

EPA FORM 1320-6 (Rev. 5/87)

DATA QUALIFIERS

Contractor; f —1 •"» *»•Case 7 A A

Below Is a summary of the out of control audits and the possible effecton the data for this case:

oo

/C v. / g / 0 \i U'l ..", A

,{-•'* 'l-t,-^'."

., a

Reviewed by:

Phone: __

Date: slain

UNITED STATES

CASE*

ENVIRONMENTAL PROTECTIONCALIBRATION OUTLIERS

VOLATILE HSL COMPOUNDS

R E G I O N V

CONTRACTOR

,QATE/Ti.w.E:

-Chloroir.eina.neBrorr.ometnaneVinvl ChlorideChloroethaney.etnvlene ChlorideAcetoneCarbon Disulf ide1,1-Oic.nloroethane1,1-DichlorostheneTraris-l,2-DichlorcetheneChloroform2-Sutancne1,2-Qichloroethane -= —1,1,'1-TrlcMoroethane .... •Carbon Tetrachlor.ide :Vinyl Acstate . - ^ r f T_ -BromocSichloromethane ~s- •-.-1,2-DichloroorooaneTrans-l,3-DichloroorooeneTrichloroetheneDibrcnochloromethane1,1,2-TrichloroethaneBenzeneci s-1 ,3-Di chl oroorooene2-Chloroethyl vinyl etherBrotnofonn4-Methyl-2-Pentanone2-HexanoneTetrachloroethene1 , 1 ,2,2-Tetrachl oroethanaTolueneChlorobenzeneEthylber.zeneStyrenem-Xyleneo/p-Xylene

AFFECTEDSAMPLES:-

H

I nilb

RF

- ..

&&,^r

if

fr

:i Carl(ffl'^RSO

,^sc

-

— _ .

•

f^ rj

1

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11RF'

<îe.

<c1

.. C* . - ^

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^tf

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V\JS/V>^

Bl.

(*

...

-

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:>——~

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n?om


CASE? 7357

STATiS ENVP.OWENTAL PP.OTEITIDN AGENCY REGION VC.-LIBP.ATIO'i CUTLIE'3

'MI'.'iM A T T I ~ PC; r^vr"i:';f;<;*, **. i 4 9 \* t», I 1 U ta 1* ., h_ \ # W i - . v ^ » I W * J

(Pace 1} ,,_______ COH73ACTOR . ' > ,; tlye?d L|

nit, Cal. ICont. C;:.ICc-.z. Cal Cont. Cal.tCon:.DA11/

IRF 10 * .0 -Pr.enolbisi-2-Chicrce:hvl;E-ner2-Cnlcrocheno1 .S-Oicnlcrcoenze-.s.-i cruorocerue".*

Eer.rvl Alccr.c.*! i c rcenze- .=

t is {2-cn1oro1 scare:-/ i )£:r.er

K-Nitrcsc—Ji-n-PrtrKexcchicroe'haneNizrccenzsneIscchorone2-Nlrrocneno'2»4-D.imeth"vToh6nol

2,4-Oicr.loroonenoi I -

4'Chlcrccr.i lineHexachlorobutadier.e4-Chloro-3-Me*nvi:.re.r:ol2-MsthylHexacniorocvciooenteciiene2,4,6-TrichloroohenoT2,4,5-Trichloroohe-.ol2-ChloronaDhthaler.e2-NitroanilineDimethyl PhthalateAcenaDhthvlene3 - N i t r o a n i l i n eAcenaohthene2,4-Dinitrocnencl4-NitroDhenolDibenzofuran t I I

AFFECTED•SAMPLES:

I


1 /Q7

CASES

UNITE-0 STATES ENVIRONMENTAL PROTECTION AGENCY REGION VCALIBRATION OUTLIERS

SEMIVOLAT1LE HSL COMPOUNDS- / ' Page 2 x' - {

I CONTRACTOR T v p yt pi'AvnoIS

DATE/TIME:

2,4-DinitPotoluene2,6— DinitPotolueneDierriylpntnalateA-Criloroohenvl-phenyl etherFlucrene - „. _4-Nitroani line4, 5-Qirhtro-Z-Methyl phenolN-Nitrosodiohenvlanine4-SrontCDhenvl-onenyletherHexachlorobenzenePentachlorophenolPhenanthreneAnthracene

- Di -n-Buty 1 phthal ate - — — — -Fluoranthene _ ... ^^-^~~~,-

-Pyrene-,- --— — r,~^;- ~- ~:-r-r-Butyl benzvl phthal ate-^ -;-.-? •.-Benzo( a JAnthracene -.?. -T- "=.._:---bis(2-Ethylhexyl)PhthalateChryseneDi-n-Octyl PhthalateBenzo(b)FluopantheneBenzo(k)FluorantheneBenzo(a)PyreneIndeno(l,2.3-cd)PyreneDi benz ( a , h ) ArthraceneBenzo(g,h,i) Perylene

Initt Cal.7/.r/* '/RF

*e«iSj.

'- .. .a-'-

~-^~~ ""^~

WSO

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— - .'.. " "— ,~\--'..-.„"-

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RF

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1/87

STATES ENVI5CWE:i7AL F307E:7;0:; AGE"CV RE-SICK V

SEMIVCLA7ILE HSL C'jX?:u:;DS(Pacs 1)

Cr.Si? i f .' \

. . •OAi i / i i t f t : . |

Phenolbis'.-2-Cnlcros:nyl jEiner2-Cnlcr3cneiol1.3-DicnlcrcDer.2e-;£1.4-D*cnlcroênze".=

-E-£-".zvl Alc^noll.Z-Dic.nicrcênze^s2-Me^nvl3r.enol&isl2-chloroi score:-/ 1 Jcir.er<i-V.cC?.v"iDher.olN-:iitrcsc-Ci-n-?r;;vlam .-=HsxacnloroetnaneMi trccenzeneIscsrtcrcne -— --- -.

•-Z-Nirroshanol'Tr.^--— •-- .- ••. 2.Z.4-01 methv-1 ohenol. "iV' r^ ;;- Ee^zcric~Acia_ ..-•^rf^^^^-r"-'1

bist2-Ch-loroethoxv JMeihana-2,4-D1cr'.loroonenoi- -1 ,2,4-TricnlorcbenzeneKarr.chclene4-Chlcrcc.r.ilineKexccnloro&utadler.e4-Cnloro-3-Mg-jivlGre.no]2-Methvlnashzhale^sHaxacnlorocvclooentadiene2,4,6-Trichloroohenol2,4,5-Trichlorophenol2-Chloronaohthalene2-NitroanilineDiinethvl PhthalateAcenanhthylene3-Nitroani lineAcena^hthene2,4-Dinitrocher.ol4-Ni troonenolDlbenzofuran

- AFFECTED•SAMPLES:

V

4 ,

loi:?//£/'lr

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,

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* These flags should be applied to the analytes on the sample data sheets,

CASE*


SEMIVOLATILE HSL COMPOUNDSPace 2 X

CONTRACTOR ^t U

DATE/TIME: .

2,4-Dinitrotoluene2,6-OinitrotolueneDietnylpntnalate4-Cr.lcroonenyl-phenyl etherFluorene4-NizPoani line4, 6-Dinitro-2-Me:hvl phenolN-N1 irosodi phenvl ami ne4-3 rofTiGcnerwl-pnenvl etherHexachlorcoenzenePentachlorophenolPhenanthreneAnthracene

-Di-n-Butylohthalate.Jluoranthene— r ; -...- —— —

Pyreneir^— ~=~~^= -—•'-— :. -~.~• Butyl benzvl phthal ateBenzotaJAnchracene -•'* -. -•bis(2-Ethylhexvl)PhthalateChrvseneOi-n-Octyl PnthalateBenzo(b)FluprantheneBenzoCtcJFluorantheneBenzo(a)PyreneIndeno(l,2,3-cd)PyreneDibenz(a«h)AfrthraceneBenzo(g,h,i ) Perylene

I nit7/ytRF '

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? /Cal//•r/iRSD

.

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* These flags should be applied to the anal^tes on the sample data sheets.

1/87

i!

ENVIRODYNEENGINEERS

JUly 24, 1987

Ms . Carol Schacf ferSample Management Office209 Madison Avenue, Suite 200Alexandria, Virginia 22314

Dear Ms. Schaeffer:

Enclosed are the results of analysis of five samples from Case 7351 forvolatiles, semivolatiles, and pesticide PCBs performed under Contract68-01-7087. TCiis report covers five soil samples, EM867 through EM871 ,received by. Ehvirodyne on June 27, 1987. One matrix spike and 'matrix spikeduplicate for low -level. is included: with these samples, -and will- apply to the

the. -case- that was received ~on "

J£s^^seTlteuti^Âcid fraction ^there :are~:tw:

.samples

If you have'any questions about this report, please contact me.

Sincerely, /—\

Shaaban Ben-FooratLaboratory Director

CAJ/smb

Enclosures JUL 27 1987

US .S3C £. CLA^K STREET

CHICAGO. ILU-JG1S 5060*

Case No.

REAGENT BLANK SUMMARY ..AUG 1 8 1987

Contractor contract

FB.C 10 CMC orAMALT9I* FRACTION fBfc Mtr.iO CAI NUUICR COMPOUND (HSL.TlC OH UNMHOVN) CONC. UMtTt CHDL

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FORM IV4/84

RECEWEO * SOIL SURROGATE PERCENT RECOVERY SUMMARY

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SOIL MATRIX SPIKE/MATRIX 3MKt; • . ! • . ! . . '

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COMPOUND

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Organic* A n a l y s i s Data Sheet(Page 1)

S a m p l e Number • EM867

L a b o r a t o r y Nine: ENVIRODYNELab Sample ID No: 670032*1Staple M a t r i x : SOILDat» R e l e a s e A u t h o r i s e d By:

Case No: 7351QC Report No:C o n t r a c t No .Date Sample Rtceiftd

V o l a t i l e Compound!

Concent rat ion: LOVDate Eitiacted/Prepired:Date Analyzed: 07-01-B?Cone/DiI F a c t o r : 1Percent Moisture (not decanted) 15 .4.

CIS No:

74-17-374-13-1

C h l o t O B e t h i t ilioiontbiniVii f l C h l o r i d e

. ChUrotlbinr ,73-lf-l

"47-44-r

75-34-3134-4B-S47-44-31I7-B.-2

71-55-434-23-3111-13-473-17-4

icttoue

1,1-DiekUretthia*t r iB i - I , 2 -Dick lo ra i tk iB iC f c l e r o f o ul , l -Dtchlor«i thaa il - l l t lBOBI1,1,1-TrithloroitkaBeCarkei T i t i a c k U t i d eTiiyl UitateiMBodi th lor iBt tha i t

12 U12 U12 0

: 11 U_ 124 I

5U002 V0V

U V4 a

CAS No:

71-17-5t B O f l - l l - 477-11-4124-41-1-7?-ll-371-43-2 -HI4i'-lt-3111-73-175-25-1

5»l-7l-4127-11-471-34-3tll-ll-3tlt-M-7tl«-41-4lflt-41-S

igtg

1 . 1 - D i c k U r o p r o p i n il i i s s - I , 3 - D U h U r o p r B p t n iTt ick lere t t i t i tD i l r i i i c b l o r B M t h a n t --

cis-Jl.j-Ditklptcproptie

1-ItsinoBtTitriCBlorettBini1,1,1.1-TituekloieithiniTltBBBC

CtBf lb lBSIBB

StyriBtTtttl I

Diti Q u l i f i t M

TILUE:II tkt r isul t is i Tilat g r t i t i t tkiB eit i i it . ti»«tt tki

to tk i i » t « c t t o B

SidniUdnitis cimpevBd vis iBi l jud for knt BOt d i t i e t t d I tpv i t tbi

nifioi lBt tc t i«> l i i i t (or tkt s»pli *ltk tki D ( t g . t f l O ) »n*4•B itTuitri tuc tB t .Mi l i t i oB itt iot . <nif is Bot BBces s i i i l ytbi ikjhttBiit OUetieB l i i i t . ) Tki fiotsolt ikoBld tt id 0-

a i t l f i td (ot bit tot d o t i c t i d . Tki inbcr it tfciiKblt dotoEtioB lint (or tko saiplt

Iiiicttcs^ est i t i t id uU« Tail (Uq is «s«d t i t k c t VBBBest i f t t t i>t^ .ef lBtiBtr i t ioB (or t f l n t t t i i t l f i d i i t i l u d cotpotodivhire i l:^g«»poii( is iss»td «: vktB Ike B*JI s p t c t i a l 4 t t4i B d i t k t t d tta prosiBd o( » CBipeoBd tkit »tts thi id in t if ic i t lonc i i t i t i i bit t t i run It is lesc tkia tkt i p t e i f i i d e t t t c t ioa Hutfti t t ir tku ier» (if , 10J). K liiit »( Cittttiot it 10 iql tad icoici i t t i t i iB of 3 iql is c i l e i U t o d , r i pe r t as 3J.

This (Ug i p p l i i f l i p i s t i c i d * i t tmt t t i warn tki i d t a t i f i c itioB vis confuted ky CC'KS. Singlt eopoaint put i c idn) -U

ii tkB ( i ta l u t r i c t i k e a l d I t eoBt incd by CC/KS

Tkis (lag is «id wkti mltti ii foind it kliak n ««11 if iiiipli It iidicatti pemfcli/irebibli blioi centinmt IPB todwarns Iki data isir to l»l* appropriate actios.OTHE8:Qtker (U|s aid (aotittti aay it nqaitid to p i o t t r l f d t t i B itki r i i B l t i . H B i i d , tk*i Hit bi l i l l y duc i i e td isd cichd i f c r i p t i B B a t t ack id t t tko da ta SBBBIIT r i p o t t .

•ot

Liberate:?.NineCist No: 7351

ENVIRODYNE S i m p l e Number EM867

Otginics Ant 1ys i f Di t a Sheet(Page 2)

Stmivolatilt Compoundi

Concentration: LOWDate E x t t a c t e d / P r t p t r t d : 07-02-87Dat t Analyzed : 07-1 1-B7Cone /Di I F a c t o r : 1P e r c e n t Moisture (decanted): 15.4

GPC Cltanup : NOSep Funnel Ext r a c t i o nC o n t i n . L i q - L i q E x t .

i r c l e o n e )0 ] ( c i rc le o n e )

CIS Mi. CIS No iql?

— - - _ _— -

rC-r--"-- -

" - - • _

^SJ

SO

CO

<cQUJ

UJo

101-15-2111-44-495-57-1541-73-1114-44-7 »-.-.lOf l -S I -4 v.~95-51-195-41-739131-32-9101-44-5421-44-717-71-191-95-3II-JM11-75-5105-47-943-15-0111-91-1111-13-1110-02-191-21-3101-47-017-41-359-51-791-S7-477-47-411-04-295-95-4fl-51-701-74-4131-11-3iii-n-i99-19-2

F b t B f l lb i i - ( 2 - C h U i B i t b j l ) i t k « i1-Chlo ioph tno l1,3-Di tb lBiobia i iBi , ^^^1 ,4 -Dich I f l i f l b«nua i~ ~:l iBiy i^ l Icf lkf l l — —--_• ------i ;2-DickUrol«niiBe ;;7l - n t t b y l p h « B B l ~- -.b i i - ( l - C a i o r o i « o p t B p y l ) t t B i r4-tltthf I p h e a s lM - i i t r o i B - D i - B - p r o p j l u u a iKtmkUrf l t t a i aeK i t T B b l B l l B I

InphOIOBt

2-KittBpbiBOl2 , 4 - D i i « t k y l p k i B 6 litoioic A c i dbi i - (Ci l« [ ai t keif )Hi tk«ai2 . 4 - O i c h l f t r o p h i B 6 l1 . 2 , 4 - T t i c h l B t B b l B t B B CN l p b t b l l t B B

4-CkUtsiBiliBtH e i i c b l o t B b t i t i d i i B C4-CkUrB- l - t t t kT lphcsB l2-Ht tk f i B l p h t b l l C B B

K c n c b l o r a c T c I o p e B t i d i f B i2 , 4 , f - T r i c b [ B i B p h c B o l2 , 4 , 5 - T l l C B l B t B p b l B B l

2-CklBIBBlpbtklI lB*

1 - K i t l B l B i l i B I

D i m i t h i l p h t b i l i t tletBipthf ItBt3 - K i t r o t n i l i n t

( l ) - C a n n o t

390 V390 Q390 0

_---.»• "-_ 39J 0. 390 V .; "391 «

390 939« 0390 V390 D390 0390 V390 1391 t390 11900 0390 0390 V390 9390 V390 9390 V390 0390 0390 V390 If1901 D390 01901 0391 0390 «1910 0

be i t p a r a t c d I

13-32-951-10-5100-02-7131-14:9lli-14-240t :20-3:

"-- l«7fcT-l70J5-71-3 ~

""01-73-7 _f100-ll-iS34-32-1Oi-31-i111-55-3111-74-117-1*-!15-01-0120-12-704-74-2201-M-O119-10-0IS-il-791-94-1Si-SS-3117-11-7lt l-l l-9117-14-0205-99-1207-01-950-32-0193-19-353-70-3191-24-1

r OBI d i p h e n y 1

ic i i iphthtni1 , 4 - D i f l i t r B p b i D o l4 - I i t t o p b t B B lDiii t iefnt i2,4-DiBitt«UivtBi2 , 4 - D i a i t r « U l B t f l «D i i t k f l i k t k i U t i4 > C k l l I 6 p k f B f i - B k t B } l i tk i r

Flionai4 - K i t r o t B i l i a i ~ ~ '4 , 1 - D i B i t r B - l - K i t k T l p b c B o lM-BitroiediphdiUai i i U)4-lroiophiBf I - tk iayl i th t iItltCllttttlBIIBt

FtBtickl0t«pb(BelFktBtBtkClf l t

latktietBtDi-a -bo ty t B b t h i U t iFli trnt l iktFyraatl l t f l -k tBIf l - p b ( k l l t t «U'-DicaUiBbiBtidiBil l B I B d l l B t k r t C t B Ii i s - ( 2 - C t k y l a c i | l ) p b t k i ] t t iC k r f f i a iD i - B - B c t y l p b t B i l i t il t t l e ( k ) f l B O K B t k t B «

l lBIoUHl t l l lB tkCBI

l iBiedlifiiBil a d i a e ( l , 2 , 3 - c d ) p T [ | i tO i k i B i f l ( t , k ) a a t k t i c t B illBIt(|ki)|tIf ItBt

a m i n t

310 U110B Q1100 031B U390 0390 K "

"~- 390 C390 V390 B190f UHOB 03tl U310 0390 V1900 939B 03JJLU

/""*TTo~)^ —— l»TO

310 0390 0710 0310 D170 BJ110 Q310 t)31D 0310 U390 U390 019B Q390 C

or FORM 1

Case No


Concentration; ( LowJ Medium.*-*

Date Extracted 'Prepared

Date Analyzed

Cone/Oil Factor:

Pesticide/PCBs

(Grcle One) GPC Oeanup QYes ONo

Separatofy Funnel Extractkxi

"7- fo - vy rfwiii

;rf {drenntfd) /^ - T

.._.:- -_ - .'.. -.-

'FT- --—— '--— —

.-.-••_;-_-•- - - . - •

CASNumber

3)9-64-6319-85-7

319-86-858-89-976-44-8

309-00-21024-57-3959-98-860-57-1 --72-5S-91--72-20-633213-65-972-54 -81031-07-850-29-372-43-553494-70-557-74-9

BOOl-35-22674-11-21104-28-21141-16-S

53469-21-92672-29-61097-69-1

1096-82-5

iuous Liquid - L

S —— Nog/lo<Lig/Ka

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Alpha-BHCBcu-BHC

Oelia-BHCGamma-BHC (L>ndjrve)H«pi»ct (o<Atdrtn

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AfQClO'- 1 246

Acocic* • 1 254

Arocl<x-l260

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H»m«: Envirodyne Engineers

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Libsnt czy. NiaeCase No 735 1

ENVIRODYNE Sattp 1 « Numbe r• EMB 6B

Or gin i c s A n a l y s i s Data Sheet(Page 2)

Concentration: LOWDate E x t r a c t e d / P r e p a r e d : 07-02-87Datt A n a l y i e d : 07-14-87Conc/DiI F a c t o r : IPercent M o i s t u r e (decanted)

S e m i v o l t t i l c Compounds

CPC Cle a n u p :U<0Sep. FtCont in.

14

CIS He

10l-f5-2'll 1-44-495-57-1541-73-110(-4i-7 .llfl-Sr-4'5-51-1 _:»S-4I-T' '.3fi3l-32-f111-44-5121-14-717-72-1fl-tS-37l-5f-lII-73-5115-17-fis-is-iIII-* 1-1110-13-2i:i-i:-l91-2B-3lli-47-117-11-351-50-7Tl-57-i77-47-4ll-Oi-2tS-15-4fl-51-711-74-4131-11-32GI-t<-lff-flf-2

P h e n o lb t s - ( 2 - C b U i o c t h T l ) e t b t r2 - C h I o r o p b e n o I1 , 3 - D i c b U t o b t n i e B k

I l ixy l1 , 2 - D i c b l o t o b i n t c i L e "_ . ,2 - K * t b j I p b e n o l , • - "~" Lb i f - ( 2 - C b I o t o i s o p r o p r n c t b e r

M - B i t r o s o - D i - B - p r o p y l n i n iH c i i c h U r o c t b t n tX i t r o b c o i i D iI f i p b o t O B t2 - K i t r o p b e n o l1 , 4 - O i i e t b y l p b i B o l

b i s - ( C i U r o « t b 6 i T ) K t t b « B i1 , 4 - D i c b l o r e p l i C B o l1 , 2 , 4 - T t i c h U r b b i B t c x tN a p h t b U c o i4 - C h I o t o a B i l i B iH e i i c h U r c b o t i d i t B *4-Ch lor o-3-i« thy 1 p h e n o l2 - n c t h y l B t p h t b i I e n t

2 , 4 , 1 - T n c b l o t o p b e n o I2 , 4 , 5 - T i i c b U i o p h i B o I1 - C U a r o a i p h t b i l t B e2 - K i t i e i B i I i B tD i i c t b y l p b t b i l i t eI c i n i p t b y l i a c3 - K i d o i n i l i n «

310 0310 U310 D310 D.310 U^310 U310 0310 U3ID U310 U310 Q310 0310 0310 0310 U310 01100 Q310 V310 D310 V310 U310 U310 D310 D310 Q310 0310 QIfOO U310 ITIfOO U310 U310 U1100 Q

i n e l E x tL i q -L i

CIS Ho.

13-31-t51-21-5100-12-7132-14-f,121-14-2101-20-214-11-27005-72-3li-73-7100-fll-l534-52-1li-30-1101-53-3111-74-117-11-5I5-B1-I120-12-714-74-2201-44-0121-00-015-11-711-14-131-5S-3117-11-7111-01-1117-14-0205-M-2107-OI-f50-32-1113-31-553-70-3111-14-2

r a c t i o n : YES (Kp^( c i rq. Ext . : YES (^(cir

I t t n i p h t h i B *2 . 4 - D i a i t r o p h e n o I4 -Ni t t opb tno i .D i b i B J c f a r a a ,,_-_..2 , 4 - D i a i t r o t a I n e a e _ _2 ,1 -Oia i t ro to i s iBCD i t t b y l phtbi l i t r

,4-Ci Ioropat iy l -pkiBj 1 e t b c rr iBorcie ~n"< :--•••••• '-----:•4 - K i t r o i B i I i a t4, 1-DiBi t r o-2 -H* thy I p h e n o lH - B i t r o t f l d i p b i D y l i i i a e ( 1 )4 - B r o i o p b t B y I - p b e a y l i t b i rR e i a c k l o i i b t B i i a iP i n t i c h U r o p h t D o IP f l t B i B t k t i n tIntknetBiD i - k - b B t y l B b t b i U t cTIiBinti tniP y r i B tI n t y l - l e B i y l - p h t i i U t t3 , 3 ' - D i C B l o i o b c n i t d i B eI t B i B f i U i t h r i t e B fb i f - ( l - t t h y l b e i y l ) p h t h i l i t iCb . iy i f f i (D t - i - o c t y l i h l b i l i t cI t B i o ( b ) f l a o r « B t b i f l el e i i e d i n n o t i n t k i n iI c B i o d t p y i e f i it B d t B o ( l , 2 , 3 - e d } p y i i B iD i b c B i o ( i , B ) a B t h r i c t n eI t B i o f g b i l i e r f E c B t

c 1 e one )nit one )

n g t g

310 Ui i o e u1100 U

- 310 U.- sia o -J

310 0 :..310 D

310 0^3 1 0 01UC U1100 U310 U310 U310 U1100 U310 U

^^Jlfl D

C 1100^^310 U310 U310 D770 U310 U110 BJ310 U310 U310 U310 U310 Q310 Q310 U310 U

1 = i • = :

ouJOi

( l ) - C a n n o t b e s e p a r a t e d f r o n

FORM 1

Case NoS *rnpt« W jj rn b-« f

Concentration ( Low) Medium


Dale Analyzed

Conc/Dtl Factor

Organics Analysis Data Shoet(Page 3)

Pesticide/PCBs

(Circle One) GPC Cleanup

Separafory Funnel Enracaion OYes

•1- \O • V7 rVinfi*

1i-r o •

r (rf*cani<"d} ' * • f

- . - ~~ ' -'-- - • - • • - - -,

CASNumber

319-84-6

319-85-7

319-86-858-89-976-44-8309-00-21024-57-3959-98-860-S7-1-- _72-55-9 — -72-20-6 -"33213-65-972-54-81031-07-850-29-372-43-S53494-70-557-74-9

8001-35-212674-11-211104.28-211141-16-S53469-21-912672-29-6

11O97-69-1

» 1096-82-5

Alpn»-8HCBeia-BHC0*lia-BHCGamma-BHC(Lirw3jr*|

HeptachlofAkJrtn

Hepiachl<x Epo^KJeEndosuifan 1 - .Dteldrin - . ~ ~~4.4*-ODE -"• -

Endrin

EndosoMan n4.4'-OOOErvtcrsutfan Sc/tfate

4.4'-OOTMethorvchtor

Eodfin Kctor>e

Ch'ofdat**ToopherveA/ocl<x-1016A/ociof-1221

A/ockx-1232Afoc'o*"- 1 2*2

AroC*O'- 1248

AfOC"0'-t254

Aroclo*-126O

iuous Lkjuid - L

f — sog/locfcjg/K^,

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V = Volume o' e*uaci injected (uU

V = Volume o( wafer extracted (ml)

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form 1 7/65

1*0 s

Or g *n i cs A n a l y s i s D a t a Sheet(Page 1) !--

Samp Ic N u m b e r : EMB6 9

Laboratory Ntme: ENVIRODYNELab Sample ID No: 67003293S a m p l e K a t r ii : SOILData R e l e a s e A u t h o r i i e d By

Case No: 7351QC R e p o r t No:Cent rict No: _Da t e Samp Ie Rece i red

Vol 11 i It Compounds

Concentration: LOWDate E i t r a c t e d / P r e p a r e d :Date A n a l y t e d : 07-01-B7 ___Cone /DiI F a c t o r : 1Percent M o i s t u r e (not d e c a n t e d ) 13

CIS No

_~ ..

'r. Jl

•- . -'-r-COcn20*"<a"*C

. -^

7*-l7-374-83-»75-01-475-88-375-81-2 :47-44-173-13-075-35-475-34-3151-40-54 7 - 4 4 - 3117-04-27l-»3-371-33-454-23-5101-13-473-27-4

LUOUloc

C k l e r a i e t b a n eI roaa ie tbane?iayl Cbloridc—^: - ...C h l o r o e t k a n e - _ _^ — -H c U y l e B c - C k U r i d e ' — .-icetoae -------- • _ ^ _ L _ _ _C a r b o n D i s n K i d e --- - -1 , 1 - D i c h l o r o i t b e n e —1 t l - D i c b l o r o t t b a i L et r a a s - 1 , 1 - D i c h l a r o e t h i n eC h l o r o f o r m1 , 1 - D i c h I o r o i t h i n e2-latatose1 ,1 ,1 -Tr i ch lo roe tk ineC a r b o B T e t r i c b l o r i d cV i a y l A c e t a t eI r a B e d i c b l o r o m e t b a i c

agrg

12 U12 U

-12 0

_ 4 I31

4 Q4 D4 D4 U4 Ui 012 U4 U4 V11 U4 U

CAS No:i s i t :± :BCX

7I-I7-S10041-12-4U-B1-4. .12.I-U.-1 "-7f-00-3 _71-43-21 0 0 4 1 - 0 1 - 5110-75-175-25-2lOt -10-15f i -78-4127-11-47T-34-5101-10-3lfll-fO-7100-11-4110-42-3

ngtg

1 , 2 - D i c b U r o p i a p i n et r i a s - l , 3 - D i c k I e r o p r o p e n e

J)jbroioj:Ji_UroiethaBe V— -1,1,2-TiicbUtoeUaBe -

: e i s - L 3 - D u k l o r o p r o p e n e ~l - C h l q r p j t f a i J i i n f l e t h e tIreiefori4-Hetbf I - 2 - p c n U n e n el-8(iioontT e t r a c b l o r o c t b e n e1 , 1 , 2 , 2 - T e t r a c b I e r o e t b a i eTolaeneCblorobeBieiet t k i l b e B i e n eS t j r e a eTota l

UU ,0--ff vn

12.04 012 D12 U4 04 0_

4 04 04 0

D a t a l e p o r t i B g Q o i U f i e n

If the resnit is a talne greater thin ot equal to the detectionlint, r e p o r t the Taint.U:Indieites compound was analysed for bat lot detected, teport thiliiiin tfitection liiit (or tbe fatplc wtlb tbc U (15,1011) bendon Bccessarf etactnt./diliticB ictioi. (This is aot ncfffiril|Ut iBstrntat detectian liiit.) Tbc footaetc ikooH riad: V-Coiponnd vas »«lrtid for bat let d t t c c t i d . Tkt aombir ii tbi• iaiira attiiaabU dctiction limit far tbc tuple.J:ladicitu aa estititcd film, Tbic (lag i« iftd litber whenistimitinq a tontnttition far tcatitiTiiy idintificd coipoondiwh*n i 1:1 rtfpoott is asined or when tbe mi i p i c t r i l ditiindicated tke piescnci o( a coBpaand tbit teetf tkc ideatificitiontritirii but tke resalt is less Uin tbc ipecified detcctiaa tinterntir tkaa lire (eg, 1BJ). If liiit of detectioa is 10 ag! a«4 icoacenttitiei of 3 oql is ca l c n t i t c d , report at 3J.

Tiii flio applies to pesticide pirnettrs wheri thi i d e n t i f i c i -tioa vts coafirattd by CC/K5 Siagli toipontot p e s t i c i d e s ) = 1 0ag/al ti tbe final eitrict sbeold be confiracd bf CC/KSI:This (lag is ased vtea aaatyte is foaiid in blinl is well as isample. It iadicitcs possiblt/prebable blank coatiiinition *nd*»irnj tbe data flser to tike a p p r o p r i a t e i c t i o n .OTHER:Otber flags aad foetnatcs Biy be reqaired to profitly definetke r e s a l t s . If ased. tbey init be f i l l ] t e i c r i b e d nd sicbd e i c t i p t i o n a t t a c k e d to tke d « t a snuir; r e p o r t .

bat

L i b o r i t o i y ' N i n eCase No: 7351

ENVIRODYNE Simplc N u m b e r

Organic* Analysis Data Sheet< P a g e 2)

Concentration: LOUD»te E i t r a c t e d / F r epared : 07-02-87Date Ana lyte'dT 07-14-87Conc/Di1 F a c t o r : IPercent Moisture (decanted)

SeaiTo1 at iIe Compounds

GFC Cleanup

13 9

CIS Ka:

S e p . F u n n e l E x T c t i o nCon t in L i q - - L i q . Eit .

CAS No;

_~^-~

— y ——

~ —

-—— "

•"83O~—

: i>•^

aLU>LUOLU

101-15-21H-44-413-57-1 _ _3U-73-1 - •'-.1I4-U-7 —100-31-4 --?3-5o-r ~_J5-4I-73H3I-31-1101-44-3i21-44-747-72-111-15-371-31-111-73-5113-47-1iS-13-0111-11-11ZC-I3-2121-11-1H-20-3lli-47-l17-41-337-30-711-57-477-47-411-04-2JS-15-411-51-7OI-74-4131-11-1211-14-111-Ot-l

Sib™;11111111111 ,3 -Dicb te rob tBi iB i __~~~ __l,4-Ditfi!erob«nitai -" "-ZliTv-,I tB t j I i lcohel ~" ~~- :"~--~. -l ,2 -Dicb . Ie iobent iB» — ~ *_ii2-Hetf l j lpf l iBfl I " • " - ~;_.bis- t 2 - C h l o r o i sop r o p y IJ i tb . t r4-Rttb.f Iph iBolK - B i t r o s o - D i - B - p r o p j l a a i a *Ht i i caUio t th imNitrobeaitfitIsoph*[«Bi2 -Ki t i opBcno l2 , ( -Dia* t i j lph inoIIcBte ic acid• ii-(Cb.Uro«tb.«tf >Htt»iBt2 , 4 - D t c B l o i a p b c B o l1 , 1 , 4 - T r i e b . l f t T o b e B t t B Ct U p b t B l I t & l4 - C U e r o i B i l i a tHtiitBlocobflUdiiBt4 - C U o r o - 3 - i t t B T L p h t B o l2 - H t t h f l B l p b t b l l l B t

HeitchlerocTctoptBtidiiBt2 , 4 , 4 - T i i c B l o t o p b e o e i2 , 4 , 3 - T r i c b I e t o p h c B o l2 - C b l Q t a B i p b t b a I t B C2-Ki U o i B i l i B iOiattbTl phtBi la teI t t n i p t h j I i B t1 - N i t i f t i B i l i B i

310 U310 tl310 Qno u •

"/ ^318 0...JT.SII D -_ _3IO B"_ 310 0

300 Q300 D310 B110 U310 ano B300 fno ot t l f l D310 V310 0310 B310 B300 B110 Bno ono Bno ano B1110 U311 B1700 Uno Bno BHOD B

13-32-1

100-02-7

- 121-14-1

14-44-270*5-72-304-73-7lDO- f l t - 4314-31-10 4 - 3 0 - 4lfll-53-1111-74-117-14-503-01-0120-12-714-74-1201-44-0121-00-005-11-7

S4-I5-!117-11-7111-01-1117-14-0205-17 -2207-00-150-32-1

33-70-1111-14-2

c i r c l e o n e )N O ) < c i r e I e o n e )

n g k g

i c e & i p b t b t B t1 , 4 - D i n i t i o p h c f l o l4 - K i t i « p B C B o rD i f c t B i e f a i i B " " • - - -

D i t t h y ! fb th i l i t iethn

4-HitieaBiliBt4 , 1 - D i B i t i o - l - n i t B T l p b . i n o lM - B i t r o f o d i p h i t f l * a i i e ( I )4-lre«ephtBTl-pkiBfI tthtrHciachla tobtBi ta if cBtac i l e topBiBo lFktBlf t t l t tBt

UtAric iBiDi-B-ivt;[ pbtkil i t iF l O O U B t b l B C

PJI IBI

3 , 3 ' - D i c h t o i a b t B i i d i B ileaiodliBtbrictBi

Carî (BtDi-f l -octyl i b t h i l i t il t a i f l ( b ) ( U c t » a U i B *I tB io tkH I n e r i B t b i B C

DibtBieU.Btiitbiictoi

310 BHOC U1100 B

310 B

no T1*6 Bnet BHOC B310 Bno B310 B1101 B310 U310 B110no o3IC Bno u770 B310 B310 9J310 U310 U310 U310 B310 B310 Uno u310 B

(l)-Cinnot be fepirated from diphenyI mine

FORM 1

Case No

Orgonics Analysis Data Sheet(Page 3]

Concentration: C LowJ Medium

Date Exiracted'Prepared:


Pesticide/PCBs

(DVcte On«J GPC Cleanup QYes'ONo

Separalory Funnel Extraction


Cone/Oil Factor:


oocr>

CASNumber319-84-6

319-85-7319-86-856-89-976-44-8309-00-21024-57-3959-98-860-57-172-S5-972-20-633213-65-972-54-8

1031-07-850-29-372-43-553494-70-557-74-9

8O01-35-212674-11-2M1O4-26-211141-16-5

53469-21-912672-29-6

MO97-69-1

11O96-82-S

Alpha-BHC

Beta-BHC

Detia-BHCGa"\(T»a-BHC (L«odaoelHeptachlofAWr.n

HcpiacWof EpondeEndosullan t

0»eldrin4.4--OOE£r*dnnEndosuKan II

4.4'-DOOEndost/lfan SuHate4. 4'-OOT '

Methorychlor

Erxicin Ketone

ChkxdjnrToRapr«eneAroclor-1016

A/oc«o*-1221

AroclOf-1232

Arocl(x-1247AY oc)O^- 1 248

A'oc(o<* 1 254

Arocio*- 1 260

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L a b o r a t o r y . NineCast No: 7351

ENVIRODYNE Staple Number: EM870

Orginics Analysis Dati Sheet(Page 2)

Stmlvolitili Compounds

CFC Cleanup NOD a t e E i t r a c t e d / P r e p a r e d : 0 7 - 0 2 - 8 7 S ep .D a t e A n a l y s e d : 0 7 - 1 4 - 8 7 Cen tConc /D i 1 F a c t o r : 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 1 5 3

CIS No:

101-73-2111-44-493-57-8 ,

—— — 341-73-1.

fhtaolk i i -O-CBloro t ta j I ) « th i r2-CkIorapataoI .l ,3 -Ditklor*btai ta i -

"~--~ ~ 184-44-7 --l-,~4-Dicflttr«ktnieni - . . - - : r~-X-. — -^88-31-4 . %--. Ji 75-38-l_ . ._ - ; -7. ~ " "73-48-7 ---1 39433-32-7

184-44-5421-44-747-72-178-75-373-37-188-73-3103-47-713-85-0111-91-1UO-03-2128-03-1

rg 71-28-3g> 101-47-030 07-40-3_ 39-38-7,:> 71-37-4

> 77-47-4rn •»-•*•*l7j 93-95-4> 71-38-7UJ 00-74-4O 131-11-3gi 208-94-0

77-09-2

UBIJI i iccioi . „ ...„.._; -:.1,2-DiehlotobiBiiae ; . ._ .2-Httkf rpkiaol, :;-.'.'. "-'•kis-d-CUflroifoptopyPitaet4-IUthf lpbiBolK-a i t rBSQ-Di -B -prop j i i a iB tRi i tca loTBithtBtNittobcottaiInphoroBi2-HitrvpkiaolI,4-DiiitayIpflta«Ileaioic Icidkif-(CkUi«ttboiy)Kttkui2 .4-Dichl«ropatao ll ,2 ,4-7richUr«btBtffatKipathil iBi4 - C k I o r » a a i l i a i•• i icBl«r*bBtidi iBi-Chlor«-3-«tbj I p k i a o l-HithfUipfithilinii i i cb l o r e c f t l op i a t td i iB i,4.4-TtickUropbeBol, 4>5 -Tr i ch l « t opbcao t-CkUrt&apbUaliat- K i t r e i B i l i B *

OlMtbfl BBtk i l l t tICIBlpUyltBI3-Ki troa i i l i a t

•Ikl

390 0390 B390 0».* "

. ...370 0^ ;^*370 8-• r"^ J« B

370 1 . - -390 8 . --"390 V390 0390 Q390 Q370 8370 8370 81700 0390 Q390 Q390 V390 8398 8390 8390 Q390 Q390 8390 81900 8390 U1700 8370 8370 81700 8

Funne l E i t ri n L i q - L i q

CAS No:

03-32-951-10-3100-02-7132-44-7

- ', l2i-(4-2•'lY-S.M

" 8 4 - 4 4 - 2^ - 7005-71-3

•"-' 84-73-7 _"180-01-4534-32-104-30-4101-55-3110-74-137-04-513-01-8118-12-704-74-2204-44-0129-00-005-41-791-74-134-55-3117-01-7211-01-9117-04-0183-99-2207-00-950-32-0193-39-553-78-3191-14-2

a c t i o n : YES (N^X c i r c l e one >Eit . : YES (^Jo)<c i rc l e o n e )

I

IcutpbtatBt1 , 4 - Q i B i t i a p k e a o l4-Hitropb.tBolDiktaicf t i ia~274-DiYit"r«t~6lBiay " ' —2,4- jDi f i i t iaUJBiacBiitkyl |ktkiliti "" •" •• —4-Cklerepb«Bjl-pi iBji ethir * _FlBortae4-Nit ie»iI iai4, 4 -Dia i lr •-!-«• tkj l phenolM - a i t r o f o 4 i p B i B T l u i B i ( 1 )4-8ifl iopkiB|l-phiBjl ttherHiiackliribtaicBfFeatickleropbtaol?k»tatkriifietkneiMDi-i-ifltyl ibtkaLite (f l ie i tatkcBiFjteailBtT>ktaiTl- |btki lattS . J ' - D i c h l f l t o b i D i i d i i il iBiofaUatkt ietaik i i - d - C t k y l k t i j D p h t b i l i t fCkryuniDi -B-oc t j l ik th iUt iliaia(b}(lBor«Btbtflt8 i B t « ( i l ( I i o t i a t B C B i8ffaieU)pfttBBIa4tao{ l , l , 3 -e<}pfr iBCOikiaiB(a,k)tatkrtccBiI tB tB tak i l p i t f l t a t

9^

390 8tw u1900 8394 0390 8iib'T398 8390 *« ;398 8not 81 9 0 0 8391 8390 8390 81900 8390 8

JUSD010M

*T7O390 B39G 5710 8390 8710 8390 839G 839G 8390 8398 8390 8390 8398 8

(l)-Cinnot be separated from dipheny1arnint

FORM 1

Case NOOrganic* Analysis Data Sheet

(Page 3)

Concentration. -Ow Medium

'7 "-

Pesticide /PC Bs(Circle One) GPC Cleanup QiYes'ONo

flail- Annlyr^- , , "7- JO - V7 <-ftni;

rnnr/nif Parlor- I

Pf rr*nt Mnicfiir»(H»rxn^ri) 73. J

""-' _ - - . ^ ~ ^, -^ ^ _ — ^

_ .—•--:, — - -ryr- rr-rirrL'-- ~— : *._ ~- ~ --»-• t"T '- '• J?fr— ."-sf= -i-'

.-•.ST.-TTT=: " :--, •:- .-).--- = - ---

--'::-.-^—— -------- -• ••"—— - " '

•

r*-CO

. - oo.

CASNumber

319-84-6319-85-7

319-86-856-89-976-44-8309-00-21024-57-39S9-98-8 -60-57-1— -72-55-9 -72-20-833213-65-972-54-8031-07-8

50-29-372-43-S53494-70-S57-74-98001-35-22674-11-21104-28-2114I-16-S

53469-21-92672-29-61O97.69-11O96-82-S

A(phj-BHCBeu-BHCO«UJ-8HCG<mma-8HC{Lind>nelHeouchlocAWr.n

HeptacMof Epox*de

Oteldrfn- -*-— • v - -. - -• -4.4*ODE-Erttfrin '• —EndosuKan II4. 4*-OOOEndoso fan SuKate4.4--DDTMethocvchlorEndrin ICetoneOi'ordJne

ToKjpneneA/oclor-1Ol6A/octof-1221A/ocior.1232Aroclor-1 242

A,OC10'-1248

AôCtOf'1 2$4

A.ocKx-1260

luous Liquid.- Liquid Extraction QVes

~~ (CJrctotJneJ

!(*.& U.H.O /A11. 0 VL.

. ]b.(? M

/A'P »A/*.p U

^°-*<'

-2i.^ ^V,O UJ^-i? U

- sJ3^> UJ-P*0 It

33-0 Kr Ti.c) U

/60.*> U.JJ-O «/£,£.£ U

JUd. > U; .<9 Ullt>.o U&£,A U

I&O.O UMAO UJ 3 <?• 5 £(2*>&a O UL,

. __ V. s Volume of exif *CI *n|ecled (ol)

^ V = Volume of water extracted (ml|

"™ W * Weight of cample extracted (gj

LUfy, V * Vofume at total eciraa (ut(

-! —————————— -..i.™. ——— --'.-I- ——-—— --

t---^=â"^^^--^---r:;:--^-- ---" -"fe^T"

r - _ . - ; . - . __ , —— .^ - , . . -

PII —

.- .-

ofW.

7/85


She«t(Page <)

T*ntativfllY ld»ntifi»<J Compounds

Organic* A n a l y s i s Data Shtit(Page 1) !--

Sample Number: EM871

La b o r a t o r y Nime: ENVIRODYNELab Sample ID No: 87003295Simple W a t r i i : SOILDatt Rtltait Authorixed By:

C a s e N o : 7 3 5 1Q C R e p o r t N o :C o n t r a c t N o : _ _ * £ ? 'D a t t S a m p l e R e c e i v e d

V o l a t i l e C o m p o u n d s

C o n c t n t r a t i o n : L O VD a t t E i t ne t t d / P r e p a r t d :D a t t A n a l y z t d : 07-01-87C o n c / D i 1 F a c t o r : 1P e r c e n t M o i s t u r e ( n o t d e c a n t e d ) 23

CIS tat;« « 3 «74-d5?-3

"74rl3-?17511-4

Cklorometkaae 13 B13 .B

CIS No:•CCSCSXI

71-17-3 1 ,2-Diek lorepropaactrau-l,3-DieUTtitkloreetktae

:DiSremetfc_UrflmeSS]Siil-'«^"^^ ;Jek]ereelkrBV

73-14-3

(7-U-3117-14-27I-V3-371-35-4

111-13-473-17-4

-._,.—. 5 s^-__,—-. :«a»»wwre.T»rt«>

I , l - D i c k l « r c i t k a a et r aBi* l , l -DickI f l r»e tkeaeC n l c r o f o i B1,2'DiekIetBttkaail-litai«Be1,1,1-TrichUroithiBiCtrbflB

Ice ta te

BU0B

IS 04 B< 6U B( B

73-15-Jlfll-ll-1Sfl-71-4117-11-47»-3<-3111-11*3111-90-7llfl-41-4llt-42-3

IrnitoiB ,. ; • :

4-RitkTl-:-i iBtaBOBt2-Eiiaa0BtTitraekloroetheael,l.].2-Tetrack!ireetkaaeTelBeie

ttkylfceaieatStficaiTetal Xy l iae«

Data liportiBf Qvalifiari

If tkt molt is a raise oreatet tkaa *i eqaal to tke ittectioatiiit, rcftit tke raise.3:ladicates ctipoiad wai aBtlftetf (or kat aet detected lei«rt tkeaiiiBQB iilictioD liait (er the laiple vitk tki B (*{.1IU> kastdIB leceiiarr eoaeeat./dilatieB actioa. CTkis is a«t aecmarilitat iBitrnint ditectioB limit.) T&e faotneti ikoald tiad: 0-Ceipoaad «as aialyied fer kat aet detected. Tke anbir ii tkiliiiita atttisakle detectiea liait for tke taipli.J:Indicates aa istiiated ralai. Tkii Hag ii ated eitker vseaestitatiaf a c«aeiatratioB for tiatatifilv ideatified toapooDdivkiri a 1:1 KSIQBII is assvied or vkca the »is tpeetral dataiadicated tke iteteace *( a tOBpoand tkat Beets tke idffitifititioncriteria lot tke resalt is less tkaa tfci specified d e t e c t i o n ItaitIteater tkaa ser« (eg, tO J > . If limit *f detictioa is ID aot aad aeoiciatratiaa of 3 a«l is calcvlatid, report at 3J.

Tkis (lag applies te pesticide parameters wfteie the identifica-tion wii eonfiind |y CC/IU. Single coipoBtat pesticidcs}>10

la tke fiaal attract skeaid ke confirmed by CC/K5

Tkis flag is iscd VBIB aaalfti is fo»d ia bliak is xell as asample. It iatfieatas pessikle/prokakle bUnt ceataaisit ion aadwaras tke data asec te lake ap p r o p r i a t e actioa.OTHll:Otkir lligi »Bd f*otaetcs aij ke required to prepeily definetke resalts If ised. tkej mast ke t a l l y d e sciibed aid sackdescription attacked te tke data ssuary r e p o t t .

ka t

L a b o r a t o r y - NameCase No: 7351

ENVIRODYNE Sa*pU Number• EM671

Organic* Analysis Data Sheet(Pagt 2)

Semiioltt ile CODpounds

Concent r » t ion ; LOVDate E i t r a c t e d / F r e p a r e d : 07-02-87Date Analyitd: 07-14-87Conc/Di 1 Factor : 1Percent Moisture <d e c * n t e d > 23

CIS Ho vgtg

CFG Cleanup : NOSep funnel Eitra c t i o nC o n t i n . L i q . - L i q . E i t .

US Ho:

c i r c l e one )N o ( c i r c l e o n e )

•gkg

10l-?3-2I11.44_4__

•*:-^$j&2L^•SZ-itiLffi'^

-:.-;r.--M-SI-l-«i^r

- . t^_''"-'*i.f 3-41-7 --^-^~7 39433-32-f

104-44-3421-44-747-72-110-15-371-Jt-l10-73-3103-*7-»

^ iJ-OJ-03 111-M-l30 120-13-2-*^ 120-03-1

r-r» f l -3f l -3"3 104-47-0Q 17-41-3UJ 31-30-7> '1-37-4UJ 77-47-4

UJ "•"-'0? f3-)S-4

91-31-701-74-4131-11-3200-H-3Jf-01-2

Phenolkii-(2-CUor»ttkTl)etker .

^3îcBj.r.b,.»».:=~a

lti.nl ilclk<^-==^-':^-^^4 .2-DicfcIertftjftsMi .^^':^-3-HttflTlBklBttl~'^'r~"~" -±^~?—

k i i - ( 2 - C k l o i < i i o p r o p f l ) e t k e r4- f Ie tkyIpbiaoIN-Btt roso-Oi-B- i ropyla i iBiHnacklereitkaaiXit robe&t i f ieliflBkeioaeJ-Ki t rophtnoI2 ,4-Dt i i tk | lpkcBBliBBioic Acidh i i - (CkUui tke i j )Kt tkaBi2 .4 -DickUropkiBol1 ,2 ,4 -Tr ickIe rob tBt iBf lKapbtha l t a i4-ChIoMiniIiiiHt i tchlotobol id icB*4-Ckl« ro -3 -MtkyIpk iBo l2-Ht thy lBipb tb i l iBCHeiack lo r scyc I tp iB tad icBi2 , 4 , 4 - T r i c k l o c o p k t B o l2 , 4 , 3 - T r i c b l e r o p k i B o l2-CkIor iBapktki leBe2-Ki t re iBi l iB iDi»tkf l p k t k i l a t eAciaaptkfliBi3-Ni t reaBi l ia i

430 0430 V

-J! -^431 P^-y^-^^S'ct-ipss :U 0 -$S-^-^^z7

«^=._4IIJ -.ste^hTfi-JT~- -' 430 0 ' ' -— -*• ~~ •-- •. -• .""«• 0 '"^"rr^T^'

430 0430 0430 0430 0430 0430 0430 02100 0430 V430 0430 V430 0430 0430 0430 0430 U430 0430 02100 U430 02100 0430 B430 92100 0

13-31-131-20-3

»*•*«££

&MA.M-;fi%i-i7 OB 5-72-314-73-7-100-01-4334-S2-104-30-4101-53-3110-74-117-04-303-01-0120-12-714-74-2204-44-012f-00-003-43-7M-H-134-35-3117-01-7210-01-f117-04-0205- f f -2207-00-V30-32-1lf3-3»-333-70-3ltl-24-2

ittaapbtbiBf2t4-Diaitt«pkiBol .

^^llmys^^^g:^^7^DiiilitTtilIî}-^^Kik;-=*i«lkTl •kikiUte;Iuî:-.i-:--.itI .. 4-CUiTifitByI-pktifl etkir - :----^TllaoteBe .^-^.iLs^-iV-T ' .'l'..7;^;V '-.-.

4-Mitr»4BiU«4.4-Dif l i t ro-2-HetkyIpkiBoI1-aitreiedipkeByUiiii (1)4-IrciepbiBfI-pfcinjI i thtrIlIiCkIlC»blBIIB«

PeatackltroBkeaelPkeButkriaeAatkractieii-B-bitfl yk tk i la teflioraitbiBiPyrcBil i t f l -keas f l - ik tkaUt t3,3'-DickIirebiBiidiail»ie(>)aBtkraciae» i i - ( 2 - C t k f l k t i y l ) p k t k a l a t iCkiyiiBiDi-B-«tt j l p k t k i U t el » B t « ( b ) ( l B O r i B t k « f l C

l i a i « ( k ) f l B i r a B t k c a il*Bi«(a)pyr»«l B < » o ( l t 2 , 3 - e d ) p T r t B eO i k t B s o ( i , k ) a B t k r a e « a iliiitffkilpiryUae

430 0^ 2 1 0 0 V _ . .

m**j>&^1! JW,-ir_«30.B^-^;

>;r.«JD «-—--:. ' "_ 430 0 .-"::'•'••'-

2100 D2100 0430 U430 0430 02100 0430 U430^

/tiT)^Htt-li

430 0430 U040 0430 0110 8J430 U430 U430 0430 U430 D430 0430 0430 0

( l ) - C a n n o t b e s e p a r a t e d f r o m d i p h e n y l a n i n e

FORM 1

Laboratory

Case No _

Ac..

iOrganic* Anatysis Data Sheet

(Page 3)

S *mpl« ,/yu m txo r

Concentration. C LowJ Medium



Pesticide/PCBs

(Circle One) GPC Cleanup QYes ONo

Separator* Funnel Exuacjion OYes

Continuous Liquid - Liquid. Extraction OYes

Cone/Oil Facior:


-^M^»-—---~^;;^^^^?^*-^-^~--

•• r .._- ui. — ;'±;, — -"".-•.-'• r.. ,>."•_ -1_ ' . . " " • - -* '•* —

K8«

«.."Jj

a£a]ou;or

CASNumber

319-64-6

319-85-7319-66-858-69-976-44-8-309-00-2 :1024.57-3-959-98-8 —60-57-1- ---:-72-55-9 .72-20-8 -33213-65-972-54-81031-07-850-29-372-43-553494.70-5S7-74-96001-3S-212674-11-2111O4-28-211141-16-5S3469-21-912672-29-611O97-69-1U096-82-5

Alpha -BHCBeia-BHCDeha-8HCGamma -BHC (LindaneJHeouchlof •- ---^.-r-AWfin , -.—--, ^_

HepiacWof Epoxide ^rtr-—Endosulfan 1 .-.-- -t -^yaiOiefdrin- -.••• " . --•'.*.-.-?=.4.4--OOE —- — ••--Endrin ,

EnoosuHan 114,4'-000Endosuffan Suttat*4.4-.DDTMeinoicvchlorEndrin KeioneChlordaneToKapheneA/octor-1016Ajoclof-1221Aroctof-1232Aroctof-1242A/oc(o**1248Aroci<K.12S4

Aroc«K-1260

**0/lof^q/Kg(GreUUo<

?(,.£> U/ t .O 1LIL.O U

... K'O u"IfÔ^t.

-— 1fe,o-U-*/A;O"«-V--*Î*.O U—"- 3z .» u-33.0 -«.3Z^M

0»^> «^ .o K^3^5 «

r J2.^ U/tO.£> U.

33.0 U

/fcAO «

JL70. > U

l£>0.0 U

tlo.0 UK^.O UILO.O U/&&.O u;330.6 U3*0,O VL

>

• , ; • • . - • ' .-.:'-

-----* ~—i^wfc^.-^^J^^4-^v.«-3S^r.-

^ê^ -TT^g^y^y .-- - - '.* .r- --,—— ——— f ----_ ---'T- - i-" - - 4. . "^ • .ff"-^^.*i*;-£_--- • ,- -

." -"•"-.'. v.t:-v *~ ,:i:-"--:- ' ~ ••- - -

.

wW.

V. x Volume of extract injected (ul)

V * Volume of water extracted (mil

W * Weight of ta'mole extracted (g|

V * Volume of total eciraa (ul)

Form 1 7/85

Znvirodyne Engineers^

Aiwlyias Data Sheet(Page 4}

T«nUtrv«ly IdentiHftd Cocnpotmds

ecology and environment, inc,111 WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415


Date Received for ReviewTo:From: Zena Gold-Kaufman?^Subject: HOD

PAN:

Date Review Completed 9 Q| OT~

Case I

Sample Description______Organics (VOA, ABN, Pest/PCB)

Low Soil (JJILow WaterDrinking WaterOther


Low SoilLow Watert-Drinking Water-Other

Project Data Status Completed!


FIT Data Review Findings:em

/e tec-ted aHf\|| 6I\fl deeded noid/nfeKfv f€,\€cted^ fcrrReviewer flagged

det d

results-far em 8?,for

Book No.


Page No. \^


•JSJECT: Review of Region V CLP Data Q ,^ . Q~7Received for Review on O ~ «^ " O /

SOM: Curtis Ross , Director (5SCRL)Central Regional Laboratory

'0: Data User:


SITE NAME: HOD LANDFILL _______ SMO case No. 73S1- . No. o f T D . U . / A c t i v i t y

EPA Data Set No. or ^t\too Samples: \) Numbers _____________

CRL NO. 8"1FP\\SZ4 - 528____________SMO Traff ic No. EM 8"?2 - Slfe____________________

- — ; M r s . R e q u i r e d ,CLP Laboratory: ENV\RODNM£_____________ for Review: AHQ


r/ ( 5^0

( ) Data are acceptable for use.(y.) Data are acceptable for use with qualifications noted above./**( ) Data are preliminary -pending verification by Contractor Laboratory^(Xj Data are unacceptable*. yo AS fl/V/Ji £K ^M *'x?i efa**Ji fi'Ali"Tt<

cc: Duane Geuder, Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas

EPA FORM 1320-6 (Rev. 5/87)».v

DATA QUALIFIERS

Contractor: 73 J/

Below ts a sumap/ of the out of control audits and the possible e'ffect. on the tfata for this case: .

- C

»7

(r C . ^> -TO VVWV «-Si^

>. /e fcJ**~ VThC

7 1

^* _ju.» -t'j_*-^l c.î b v^-J-i *ui.

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Revle-ed by:

Phone: 3

At ; fc^ T*.trir* f /I ¥/? 7

~G S

DATA Q U A L I F I E R S

Contractor: £"K»>'I v<? c«e73r/Belo* Is a surmarjr of the out of control audits and the possible e'ffect

. on the data for this case:

O\5. C~(;

C*/ 1 -r

JJ/LT" 4£*'

^ n *-

I*

"•••f iA.i

«î f /-t

W-f

Reytexed

Phone:

DATA QUALIFIERS

Contractor: C'se T35Y

Belo* Is a sumnar/ of the out of control audits and the possible effect Û .. on the data for this case: *x\x*o

A 1 /^ l/a/lfct J.

ftISAM

S f ,*»«, \ f.

PL,

57 5** CUlff 1-1 C-4 U/

â^^rAiyg. ire^s i*s(t-i fov **£{ f*9-r*.*».*s£***-f

lK (f) o__^ ^T7

by:

Phone:

DATA QUALIFIERS

Contractor; C.se

Belox Is • summary of the out of control audits and the possible effect. on the data for this case:

5. sc%_-»-j*' •tLf-o.T*

»•»

re, £ At• OK .

. < >*-<Lfc<

»

w * I'•'IT.

RevTe-ed

Phone: O?

DATA QUALIFIERS

Contractor: £****+* <fy* <- Cisec£

"7.

Below ts a jurmap/ of the out of control «udfts and the possible effecton the data for this case:

-fV e, P

*.*•&. 't

S^.*r-ftc*-fl

J. *s+*.

2O Oil T

— -/At.100 /«-SS 4- k.*

30.

LS*

flj-fHO

Reviewed byt

Phone: ra

t c r

CASE?

U N I T E D STATES E N V I R O N M E N T A L PROTECTION AGENCY R E 3 I OC A L I B R A T I O N O U T L I E R S


____________ CONTRACTOR £W?v-o«gy

Imt . C a l . ICont , C a l . J C o n t . C a U I C o n z . C a 4 . I C o n ; . C a l

IRF IRF |% RF |RF i R rPhenol

JEtner2-Ch io rooneno

Alconc1,2*31 entorosenzsne2-Ve'nvionenotbisU-cnloroisoDPoovi4 - M e t n v i D h e n o iN—Nil ros o-DI *n-rroov1 arm neHexacnloroeinaneNitroDenzeneIsoonorone2-NitPOOhenol2,4-Oimethvionenol y\Benzole Acidbisl2-ChloroethoxvjMetnane2,4-Oichioroonenol1,2,4-Trlen t oropenzeneNaonrnaiene4-Chloroaniline P/ICHexacnloroDutaalene4-Chloro-3-Metnvlonenol2-MetnvlnaontnaleneHexacniorocvclooeniadlene

2,4,5-Trlchloroohenol2-Ch loponaon tna i ene2 - N i t r o a n i l i n eDimethyl Phina lateAcenaontnvlene T \3-Nitroaniline 34 rAceraonthene2,4-DinitrQonenot4-NitPoonenoO i D e n z o f u r a n

AFrZCTEDSAMPLES:

* These flags should be applied to the analytes on the sample data sheets

CASE*


SEMIVOLATILE HSL COMPOUNDSPage 2 - - -•• -

CONTRACTOR £**'*•-

'

QATE/TIME:Inlt. Cal.

Rr! 2,4-DirntPOtoluerie

2,6-DinitrotolueneDie'nylontp.alate4-cnlcpocneivl-pnenvletierFiuorene

' 4-Nitroam line4,6-Dinitro-2-MethvlohenolN-Nitrosccioherwlamine4-BPcr,c-r.5nvl-onenylethepHexacnlorooenzenePentachlopoohenolPnenantnrene

i AntnraceneDi-n-Sutvlohthalate

•RSD w

Cont. Cal. lCont. Cal.lCont. Cal .1 1

RF ID * IRF

59 T

Fluorantnene tPyreneButvlbenzvlohthalateBenzol a ) Antnracene 1bis(2-Ethvlhexyl)PhthalateChrvsene

1

i01-n-Octvl Phthalate 1 1Benzo(b)FluopantneneBenzo(k)FluopajitheneBanzota JPvreneIndeno(l,2,3-cd)PyreneDlDenz(a,h)Anthpacene-Benzo(a,h,1 ) Pervlene

11

t

10 1- |RF1

I1 111

1 111

11t

t 11

ID *

Cont. Cal . >

RF

1 11

11 t1 1 '

1

t

10 *

•

1

1

1

1


These flags should be applied to the analytes on the sample data sheets,

1/87

ENVIRODYNE St LOUIS Mssoun i3146(314)434-6960

\

1n

nu11alrndddddd

August 7, 19871990-7351

Ms. Carol Schaeffer ^^ •- ..Sample Management Office 52$ - ",**• -i209 Madison Street, Suite 200 ''"'•••iJj "' * -Alexandria, Virginia 22314 '" ''Ui/y-j

Dear Ms, Schaeffer;

Enclosed are partial results of analysis of Case 7351 for volatiles, BNAsand Pesticide/PCBs performed by Envirodyne under Contract Mo. 68-01-7087,Five soil samples, EM872 through EM876, were received by Envirodyne onJuly 7, 1987.

The semivolatile fractions were screened for concentration levels by GC,and extracted by the low level method. Because surrogates were out ofcontrol on the SNA blanks from the original extraction, the SNA fractionswere re-extracted on July 30, 1987.

A matrix spike and matrix spike duplicate were extracted with all fractionswith these samples.


Sincerely,


MCW/jagEnclosures

PAGE OF

Case: 7?

Contractor:

TENTATIVELY IDENTIFIED COMPOUNDSWATCH ASSESSMENT

NOTE: Reviewer should note directly on Organic Analysis Data Sheet (OADS)those matches that in his opinion (based on contract criteria) areunreasonable.

CRITERIA

(1) Relative Intensities of major Ions (>IQ%) reference spectrumshould be present in the sample spectrum.

(2) Relative intensities of major Ions in sample spectrum should.agree to within +_ 20% of reference spectrum intensities.

(3) Molecular Ions present In reference spectrum should be presentin sample spectrum.

(4) Ions present in sample spectrum, but not in reference spectrum' should be reviewed for possible background contamination or

presence of coeluting interferences.

(5) Ions present in reference spectrum, but not in the samplespectrum should be reviewed for possible subtraction from thesample spectrum because of background contamination or coelutinginterferences.

(6) If, in the reviewer's opinion, no valid Identification can bemade the compound should be labelled as "unknown" and the initialsand date of the reviewer placed on the OAOS.

Reviewer's Initials/Date: ~<$sfcAz* ">*>•• w**l y3//?7

CONTRACT LABORATORY PROGRAMDeputy Project Officer Communication Summary

-I .Date DPO Notified of Issue; ?'t'-f7 DPO Notified By: r">Tr •f^'-~' <*

Subject Laboratory: £A/'.W 3 &.VMeT __________ Case/Sas No: 7^

Contact for Resolution:(Laboratory or PO)

Date of Contact: _______________________ Call or Visit (Circle One)

Summary of Issues & Resolutions:Document the issue(s), resolution(s), and action deadlines, if any.

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UNITED STATES ENVIRONMENTAL PROTECTION AGENCY 3REGION V <

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SUBJECT: ^^c gesPv***- TV &£* 73-SV

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Laboratory Naae: ENVIRO&YNECase No: 7351

Saaplc Nu*oer: EM-37

Organic* Analysis Data Sneet(Page 3i

Pesticides I PCS s

Concentration: LOWDate Extracted/Prepared: 7-23-87Date Analyzed: 7-28-97Conc/Dil Factor: 1Percent Moisture (decanted): 21

CAS Not

6PC Cleanup : YESSep. Funnel ExtractionContin. Uiq.-Liq. Ext.

uqkg

J

I

31H4-6319-85-7JlH!6-fl**•• f-J- ftJD un7 -44-4309-00-21024-57-39SHHW-S7-172-5H72-20-8JC13-6H72-54-81031-07-fl55-29-372-43-55S474-7M57-74-98001-35-212474-11-211104-3-2534&7-2HS34i9-a-912tf2-29-i11097-49-111096-C-5

AlpbHHCBeta-Ktalta-ftCfiMirflt (LiixtaniiHqtaddorAltHnh rtichlcr EptnidfEndosulta IKeldrin414'-UEEndriiEnkBulfan-U4,4'-R»EnkKuliw Sjliiti4,4'-OOTHrttacydilDrbdrii KrtoneDOcrinTou«ttmfrnJx-1016DrKla-1221fcTtlir-1232fc-xIx-1242AnxUar-124a«rodcr-[254frTClor-m

20 U20 U2flU20 y20U20 U2DU20 U411)41 U41 U41 D41 U41041 U200 U41 U200 U41ft U2DQU200 U200 U2UU2MU410 U410 U

A'1 *•*»*.*srrt*****'*rr .-Afc^'TS

30 9

Vi « Voluae o^ extract injected <ul>Us » Weight of caaplc extracted (g)Vt " Volume oi total extract (uli

Vt " 40,000 ul

FORM 1 ^

Vi « 2.0 ul

Laboratory Naae: ENVIRODfNtCase No: 7351

1 5 a « p l e N u « o e r ; En 573

O r g a n i c * A n a l y s i s Sata sneel2i

106-15-2UM4-495-S7-S5*1-73-1104-4o-7100-51-tt95-50-195-«-739435-S-9104-M-5421-64-747-72-196^5-378-59-1B-75-5105-87-945-fi5-0111-fl-l120-83-2120-82-1tl-20-3lflo-47-fl

Rwnol

2-QilorDptiflml'

l«4-OicMcrc6cn:awBnyl Alcohol

2-fetnylphnlfcis-(2~0ilarmi^re?yl)ethir4-flRhylphmlIHri troscHH-tt-prDpy laai MteadUtroeth**tfi trot BIT meIfi narane

2,4-OiHthytphBiolfinoic Acidbii-(0>!xoettitBy)Hethane2,4HHdU(ropn«nol

5"r-50-791-57-877-47-4BB-Oo-2

HBadUxawtidient 'H1U (TQ-3-wthylphHUl2-ntthyInapttthaJm

71-3-7 2-QlatnaphthalBWB&-74-4 2-tetroafuline131-11-3 Kvtfayi20fl-9e-fl Auruptnyli9M9-2


Date cxtracttd/Fr*par*d: 7-30-S7Datt Analyzed; 6-5-B7C o n c / u i l Factor; 1Percent Moisture (decantidi: 19.7

CASHo:

410 U410 U410 U410 U410 U410 U410 U410 U410(1410 U410 U410 U410 U410 U410 U410 U2000 U410 U410 U410 U4101)410 U410 U41011410 U410 U410 U2000U410 U2000 U410 U410 U2000 U

6PC Cleanup : NuSep. Funnel E x t r a c t i o n : YESContin. Liq.-Liq. Ext . : YES

CAStfc

BS-3M31-2&-5

121-14-2406-20-2B4-6&-27005-72-386-73-7100-01-4534-52-1Bb-30-6101-55-3118-74-1B7-84-585-OH120-U-7W-74-2204-44-0129HJO-0B5-4B-7fl-^4-1Si-55-3117-81-7218-OH117-W-O205-W-2207-06-950-32-8W3-3W55-70-3191-24-2

2,4-irinitrcpnBial4-MtrapiiBialDibfraonran214-DiaitrotaluiM

4-NitnBnilin>4,fr-Oiutro-2-flIHutrosxtipcwnylaiiH (It

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pbthalati

Pym

bis-(2-EthylnBylipnth4latiQrysmDi-mctyl phthilitiharo(b}ftooranthmlnB(UHuranthm

Indm 11,2,3-cdJ pyrwwtitauo u,h) anthracint

(U-Cannot fa* separated froa tfipnenylaaine

FORM 1

410 U

20COU410 ij410 U410 U410 U410 U410 y2000 U2000U410 U410 U410 U2000U410 U410 U

410 U410 U410 Uazou410

410 U410 U410 U410 U410 U410 U410 U410 U

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J

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Laboratory Na«e: ENV1RQQYNECase No: 7551

Saaple Number


Pesticides I PCB i

Concentration: LOtaDate Extracted/Prepared: 7~/f-Date Analyzed: 7-21-87Cone /&i I Factor: 1Percent Hoisture (decanted):

7-/f -f^

d): 20

CAS No:

31W4-*31WS-7319-flW•» na a3dTT T

74-44-fl309-00-21024-57-3»• »*> *Ul III U

40-57-172-5W72-20-833213-6H72-54-fl1031 -07-850-2^372H3-55M?4-70-357-7W1001-35-212&74-11-2m04-2B-25S4»-2l-f5S4W-21-9Uo72-2KUOW-4WlIWh-a2-5

6PC Cleanup"- Sep. Funnel

Contin. Liq.

Alpha-filCBeta— tKDriti-BCSâ-BC (UndxieJhpUchlirW*iflWaddv ResideEnksuH»IKrldriB4,4'-90EEheriiEndoailfarrll414'-OTbdoulfan Sulfatt4,4 '-HOTIhUatydilorEvHt KrtaneOtlcrdantlaaphiM•nclor-lOUfrttl a-1221(rrdx-lISZArodcr-1242frodx-1246*roclor-l234ftTTltr-UW

I YES -. ——Extract ion : YES VJlflMcircl e onei-Liq. Ext. : YE&^TSd iTii r cle one iV_X

ugkg

201120 U2DU20020 U20020 U20 U40U400401)40(140040040 g2000460200 U400 U2000200U2001}200 U200 U400 U400U

Us * 30 9

Vi • Voluae of extract injected <ul>Hft * Height of laaple extracted (q)Vt « Volume of total extract (ult

Vt " 40,000 ul

FORM l"

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Ji!i

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CAS

17

11.

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Organic* Analysis OaCa Sheet(Page 4|

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Laboratory Nane:Case No: 7351

ENVlRODYNE Nu«0f: En-674&:urganics Analysis Data Sheet

(F1 a g e Si

Pesticides i PCS s

Concentration: LOWDate Extracted/Prepared:Date Analyzed: 7-21-87Conc/Di 1 Factor; lj | 0 *"Percent Moisture ideânte

6PC Cleanup : YESSep. Funnel Ex t rac t ion : YE5 fNQVici rcl e one)Cont in. Liq.-Liq. Ex t . : YE5 f "Nu j c i r c l e one

CAS No: ugkgia = e=s

Alptu-3(C

[ ^^_ ,

3I7-35-7

•K -Ml H3D OT T

74-44-fiJOHiO-21024-57-3

W-37-i77-SW72-2H

72-54-6KOl-OT-fl

7H3-55H«-70-5S7-7HfiC«l-3S-21247M1-211104-26-2

DfltHtCEuu-fitC dindane)

EpoxidiEndosultan IDitldrin4,4'-OutEndrinEnoosuliw-ll4,V-OWEndoul{» Sulfati4,4 '-WTIMtayctdorEndriilCfftantOilontantToiapfctntAroclcr-lOla

11W7-6M1109o-82-5

Arxlor-1242frodor-1248Aroctor-125*

160 UIBuU

180

18 U18 U

36 U341)liU3iU180 U36 U160 U3WU160 UIfiOU160 U160 U160 U

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*D.|. IMOVt * 40,000 uL

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I*i*4r1

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I 1

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LaboratoryCase No: 7551

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ENVIRQDYNE -----Sanp1e Nuaoer:

**J7 * s e*T(*-Organics Analysis Data sheet;»c<- A •/•*•'"?

.faeatvolatile Compound*

(U-Cannot bt separated fro« diphenylieine

FORM 1

•u,-

1 e ^ i * Ih V ^h I" — . - » . —

L-fS u/tv «•»•*- ^J "AA

C o n c e n t r a t i o n : L O WDate E x t r a c t e d / P r e p a r e d : 7-30-67Date A n a l y z e d : 8-5-87Conc/Di 1 Factor: 1P e r c e n t M o i s t u r e { d e c a n t e d ) : 4

CASfc:

106-45-2111-44-495-57-e541-73-1106-46-7100-51-695-50-195-48-739638-32-9106-44-5421-64-767-72-196-95-378-5H68-75-5105-67-945-85-011H1-1120-33-2120-82-191-20-3106-17-6B7-6B-359-50-791-57-677-47-468-06-295-95-491-58-78B-74-4131-11-320Q 96 fl9W-2

Hanoibis-{2-OJ (methyl Jrther2Oiloroph(nol1,3-OichloratxTOewl,4-fiidiioroben:tnttauyl (UOTdlf2-{Kd)lcrcbn:nff2-ftothylphnlbis- (2-Dil or oi soprc^yl ) rthr4-nethylphcnolM-ni tr oso-Oi it-propyl ui nt(exachlarotthanittttrobnintIsqinoroni2-Mitrophnol2,4-DiiethytphBiolhnimc Andbii-iChlarwthavinrthw2,4-Oichloraphtnal1 , 2, HrioMDnteniBMMftphthalcRf4-Ovlxoanilinitotadilorabutadint4-Chltro-J-Kthylptoal2-fkthylnapiitlttlnffHdKhlxocydipvtîene2,4,6-Trichlirophtnol2, 4 ,5-TrioM inph«ttlKUorortaphthalm2-MitroaruliniDitftiryJ (MbalatfAcoupthylvt3-tttroaniline

uqkg

34011340 U340 U340 U3401)340 U340 U340 U340 U340 U340 U340 U340 U340 U340 U340 U1700 U340 U340 U340 U340 U340 U340U340 U340 U340 U340 LI1700 U340 U1700 U340 U340 U1700 U

BPC C l e a n u p i NOSep. ' Funne l E x t r a c t i o n : YES^Con t i n . L i q . - L i q . E x t . : Y E a ^

ttSfc:

63-32-951-28-5100-02-7132-64-9121-14-2606-20-264-66-27005-72-384-73-7100-01-6534-52-186-30-6101-55-3I1B-74-167-66-56SH)l-6120-12-764-74-2306-44-0129-00-085-68-791-94-156-55-3117-81-721B-OH117-64-0205-99-22D7KI6-950-32-8193-39-553-70-3191-24-2

-

AceiuphthcnB2,4-Dinitnîenal4-tttraptitnnlDibttzofirvi2,4-flinitrotolucnt2,6-Dinitrotaluff*Dirthyl pbthalati4-OiIaropfiinyl-phenyl ethrFluartM4-Kitroaniline4,6-Oi ni tro-2-(tethy 1 ph«wlH-nitrosDdiptunylaiine (1)4-frtnophetyl-phenyl rttwrHn**ltro«uMPentacMorophenolPtwnanUf ••fcithracmtDi-tHwtyl phthalitiFluor mtiewPyrveButyl-tarylfhttuUttStS'-OiohlTtbeaidinihnzoialaBttraciMbis-O-EthylhetyUphthalatiOry«ntDi-n-octyl phthalatiBBtzoiblfluoranthmleraol^nuranthnknxDdlpyrenttrim ( 1 ,2,3-d) pyrv*Kbcnzo (L,h) anttracfntInzoighDprYlBv

/

35; (ci: T J u ) ( c i^ — -x

Mgkg

3*0 U. 1700 U

1700 U340 U340 U340 U340 U340 U340 U1700 U1700 U340 U340 U340 U1700 U340 U340 U15&X340 U340 U340 U490U340 U130 Ui340 U340 U340 U34011340U340 U340 U340 U

Ov. f l r* /

( c i r c l e one)(circle onei

»[•

J %Laboratory tUne: ENVIROGYNECase No: 7351

Organics Analysis Data Sneet

Concentrat ion: LOWDate Ex t rac ted /Prepared : "7-Date Analyzed: 7-21-87Conc/Dil Factor: 1 t lO *Percent Moisture (decan ted ) :

Pesticides -v PCb s

GF-C Cleanup : YESSep. Funnel ExtractionCan tin. Liq.-Liq. Ext.

ici rcl e.(circle

one)one i

CAS No: ugkg

50 g

319-W-iJ19-35-7319-66-8m fift B•U VI T

76-44-fi309-00-2W24-S7-3««» m aWf TO B

W-57-I72-5H72-20-833213-AW72-54-810S1-07-85fr-25-372-43-553494-70-557-74-9BOOt-35-212674-11-211104-23-251489-21-9S34A9-21-912&72-29-411097-49-11109i-e2-5

Mpha-ilCBeti-BKEelta-etCCuu-OC Oindaneih itadilorUdrinItaptactilx Epoiiti*EndasuHanlKridrin4,4'-DflEEndhoBtdosultan-II4,r-MOEndoulfw SulUti4,4 '-DOThetha lxEndria KrtcntChlcrtantTaaptimArodtr-lOUlroclQr-1221flrodo-1232Arodv-1242Arodx-l24Bfc-oclx-125*

170 U y.170 U *170 U *170 U *•170 U Xnyfrr17 U17 U33 U331)33 U33 U33 U33U33U170 U33 U170 U330 U170 U170 U170 U170 U170 U330 U330 U

Vi » Voluae or extract injected (ul)Us » Height of sa«ple extracted (g)Vt - Voluie of total extract (ul)

Vt » 40,000 ulA *0°/O*

FORM I

Vi 2.0 ul

sa

•teLabora tory Nane:Case No: 7351

ENVIRQDiNE Sample Nuaoer: EH

Grganics Analysis Data Sheet

j

j

C o n c e n t r a t i o n : LDHDate E x t r a c t e d / P r e p a r e d : 7-30-B7Date A n a l y z e d : 6-5-67C o n c / D i l Factor: 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 24.8

[AS Ho:

lOft-55-2111-44-495-57-B541-73-1106-44-7100-51-495-50-195-48-7

Phenol

2-Oilcrophenol

teuyl AlcoSol1,2-ttdilcroteBtne

104-44-5621-44-747-72-1

bis~ (2-Chlcr m scpropyl) ether4-fethylpnBiolH-ni tr oso-Oi -n-propy! wineHnachloroethane

Tfi-59-1B&-75-5105-47-945-85-0lli-91-112WS-2120-32-191-20-3104-47-*87-46-359-50-791-57-477-47-4

Inphxm

2,4-DiicthylptaQlBwitric Acidbis-(Oilo*vUffiY>Hethaw

1,2,4-TrichlonteutneMaphthtlmt4-tMtroaniUn*tfacachlorobutadiene

teachl crocyclQxntadm

VS^R-* 2,4,5-Trichlornphmjln-5B-7BB-74-4131-11-3 Diiethyl phthalatff20Q 94 8 KBUputylent99-09-2 3-tttrwniliM

450 U450U450 LJ450 U450 U450 LI4SOU450 U450 U450 U450 U450 U450 U450 U450 U450 U2200 U450 U450 U450 LJ450 U450 Lt450 U450 LJ51 J

450 U2200 U450 U2200 U450 U450 U2200 LJ

e Compounds

'SPC Cleanup t NOSep. Funnel ExtractionContin. Liq.-Liq. Ext.

CKte

B3-3H51-2&-5100-02-7132-44-9121-14-2404-20-2

AcBUphthcne2,4-nnitrQDhenol

Dibnotiran2^4-OinitrotDlufne

phttalztc7005-72-384-73-7100-01-45S4-52-1&HO-4101-55-3na-74-1

Flarwf4-Hitroaniline

IHutrasadiphBiYlaunt Hi

e-oi-a120-12-7B4-74-2204-44-012HO-0

HBChlvoboucnePKtachlorophendFteanthrvte

phthilattFlvantbmFynn

56-S5-3117-81-7

BBQD (a) anthracene

117-W-O265 *9-2

QrYScnefc-n-octylkcolblfluorantJunefcrcoikHlimnttae

50-32-619>39-553-70-3191-24-2

Kbnzola^hlarthracmt

(l)-Cannot bi separattd f roa diphenylaaint

F Q R H 1

(circle(circle

one ione J

uqkg

L a b o r a t o r y Na*e :Case No: 7351

E N V I R Q D Y N E Saflple

Ji Qrganics Analysis Data SheetiPaqe 3>

C o n c e n t r a t i o n : L O WD a t e E x t r a c t e d / P r e p a r e d : 7-Date Analyzed: 7-21-37C o n c / D i l Factor: 1P e r c e n t M o i s t u r e ( d e c a n t e d ) : 27

CAS No:

1

a

H* 30 g

Pesticides k PCS I

GPC Cleanup : YESSep. Funnel ExtractionContin. Liq.-Liq. Ext.

uqfcg

YES one •

319-B4-4.319-85-7

MW6-SBI.BS aJB 07 7

7M4-63W-00-21024-57-3W?'vB Dtf-57-172-55-972-2H3EI3-65-972-54-fl1031-07-fl55-»-372-«-553494-70-557-74-98001-35-212474-11-21U04-29-2SJ4i9-21-953449-21-912672-29-411WHH11096-C-5

Alpha-MBfti*wthltJ-ftC6-w-fiH: (Lindm)HqitadUorAliHaItptidiior Epmide&iteulfan IDieldria4,4'-H£EndriaEncteulf«-II4,4'-OWGndoaiHw Sulfitt4,4'-»T(MtayddirEndria KrtontQdordmTiuphcMfrrxJtr-lOli*roclx-1221frodor-1232*roclor-1242Ardor-124aft-Klor-1254frvclx-12U

22 U22 U22 U22 U22 U22 U22 U221144U44U44 U44 U44U44U -44U .220 U44U220 U440 UZ20U220 U220 U220 U220 U440U440U

Vi * Voluae oi txtract injected (uliMs • Height ai siaple extracted (g)Vt - Voluat of total txtract (uli

Vt » 40,000 ul

FORK I

Vi • 2.0 ul

CAS

3.

«.

7.

IO..

13..

15..

16..

19..

M.

3.

10.

J

£\AOcganlci Analysis Data Shoet

(Page 4)

ld«n(<fie<J Compounds

Compownd N

e vtVJ I 4

Ul

A

U-HdvfrggM

JU rbcn

f

n *

M-3

I t - M

. r12. -5

i±^_in 6

(wg/f or

7/o.J

es

ecology and environment, inc.Ill WEST JACKSON BLVD., CHICAGO, ILLINOIS 60604, TEL. 312-663-9415


Date Received for Review

From: Zena Gold-KaufmanSubject: HdO

PAN: ID-0141 X&


Case

Sample Description______Organics (VGA, ABN, Pest/PCB)




-project Data Status


Completed!


-556Common lob - Qc£kme(di-n~

Book No.


Page No. 200

UNITED S T A T E S ENVIRONMENTAL P R O T E C T I O N A 3 E N C YREGION V

:;TE: f/v/fEJECT: Rev iew of Region V CLP Data Q __ ,-, Q-I ^

Rece ived for Rev iew on _____Q "" 1 / " Q '________ jfy

OM: Curt is R o s s , Di rector (5SCRL) /&K*4. & ofa~&4 -&? ^r,Central Regional Laboratory / <£„

TH: Data User: ______F IT____________________ /^%>

1


SITE NAME: HOD LANDFILL SMO case No. 73S1rr * » « - > No- of A °-u- /Ac t i v i t v

EPA Data Set No. br 4\b3 Samples: 4 Numbers VSQ5/C7ZIQQ

CRL NO.SMO Tra f f ic No. EM &17 " 8&Q

_ ' . Hrs. RequiredCLP laboratory: hNVlRQD^NJE ______________ for Review:


/-

( ) Data are acceptable for use.(><0 Data are acceptable for use with qualifications noted above.( ) Data are preliminary - pending verification by Contractor Laboratory{ ) Data are unacceptable.

cc: Duane Geuder, Quality Assurance Officer, EPA Support ServicesJames Petty, Chief Quality Assurance Research, EMSL, Las Vegas _-

EPA FORM 1320-6 (Rev. 5/87) - ' . . . .

DATA '-JA

C o n t r a c t o r ;

Belt* Is fi suTrr-ar/ of the out of control audits and the possible. on the data for this case:

/,

.2.VcÂt •' 3

•W >•*•• «•«.'* JQ <^V-*C.

4"'* o *>*.

t*>*.*-

>*<f

H

»*oi c ^ 3 •* /A /o£ l S — c 'j dodecy/

R e v i e w e d

Phone:

DATA QUALIFIERS

C o n t r a c t o r ; Case 73 S/

B?1c>* is a sufrr-.jr/ of the out of control audits and the possible ef fect- on the tiata for this case :

•——7u.-H'ie.v-

PK * s r <-« L«- t t

fts : »•<> o uL*4 Iy

77 TO. eg. J_L7n

t £ l

R e v i e w e d by:

Phone: 51

DATA QUALIFIERS•\

Cont rac to r ; Case 735)s

Belorf is a sundry of the out of control audits and the possible e f fec t. on the data for this case: -

** ^f f (0^7,1 f

£faJi>f)r7

_£ 7/23/f?.

Rev iewed by: At .

Phone: 3/ ?-

PAGE 5 OF

Case:

Contractor:

TENTATIVELY IDENTIFIED COMPOUNDSWATCH ASSESSMENT

NOTE: Reviewer should note directly on Organic Analysis Data Sheet (OADS)those matches that in his opinion (based on contract criteria) areunreasonable.

CRITERIA

(1) Relative intensities of major ions (>10%) reference spectrumshould be present in the sample spectrum.

(2) Relative intensities of major ions in sample spectrum shouldagree to within 20% of reference spectrum intensities.

(3) Molecular ions present in reference spectrum should be presentin sample spectrum.

(4) Ions present in sample spectrum, but not in reference spectrumshould be reviewed for possible background contamination orpresence of coeluting interferences.

(5) Ions present in reference spectrum, but not in the samplespectrum should be reviewed for possible subtraction from thesample spectrum because of background contamination or coelutinginterferences.

(6) If, in the reviewer's opinion, no valid identification can bemade the compound should be labelled as "unknown" and the initialsand date of the reviewer placed on the OADS.

Reviewer's Initials/Date:

UV.7ED STA'ES E N V I R O N M E N T A L P R O T E C T I O N A G E N C Y R E G I O N VC A L I B R A T I O N OUTL1E-.S

^ c- r VOLATILE HSL COMPOUNDS _0 5 < CONTRACTOR *

3?

l l m * . Ca'i . Ca1 i . C a U l C o n t . C a U I C o n t .

IRF |V.S:l* iRF RF RF

irvl

M5'.-.v i e"e C". i c1"! ce

I ^ I1 i

-

L ,2-D1 cr.'i1,1,1-Tncr.loroetMane

Tet recn ior iceV i n v l Ace ta te

- c r o n e t n a n e1,2-OicnlcrccrcraneTrar,s-l ,3-Di chloroDroreneTn en i oroetnene

cls-1,3--i

*, e * r\ y\ - 2- ? e n t a n o n e2-Kexanone

1,1 .Z^-oiuene

Stvrenen- X v1e n e

AFFECTEDSAMPLES:

II MB* 1 1 A106M

* These f lags should be appl ied to the analytes on the sample data sheets.

1/S7

CASE?


SEMIVOLATILE HSL COMPOUNDS/ (Page 1)' CONTRACTOR £ * v" r*>*&

Imt. Cal. ICont. Cal.ICont. Ca•• r^*~^^* •• ,• •» ••• i ^-^ i •-"—^^^— Cont. C a i . I C o n t . a i

RF f-RSD RF RFPnenoiDi oroetrwi )tne2-Cn i . 3

TO-

Eeizvi Alconoi1,2-Dicn2—Metr.y tone*____________b is \2 - cn lo ro i soDPOOv l )Etr,er

Hexacnloroe'naneNTtro-enzeneIsocnorone2-Nitrooneno2.4»OimetMvlonenolBenzolc A C T Obi st2-C'nloroethoxv jMethane2,4-DicnTorooneno'1,2,4-TricniorooenzeneN a c n i n a l e n e4-ChloroanilineHexacnlorooutaciene4-Chloro-3-MgtnylDneno12-MetnvlnaonrnaleneHexacn'iorocvclooentaaiene T

2,4,5-Trichloroohenol2-Chioronaontnaiene2—NizroanilineDixe-nvl Phtnalate

3-Nizroam lineAce-aonthene

- i mtroonenoi-Nitroonenol

Oioenzofuran

AFFECTEDSAMPLES: £"A\ X go

These flags should be applied to the analytes on the sample data sheets

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY RE-3 ION VCALIBRATION OUTLIERS

SEMIVOLATILE HSL COMPOUNDS2 . -

CONTRACTOR C Mi/I *-o N,^^^*

1 Init. Cal. ICont. Cal .DATE/TIME: I //£

IRF IWSD2,4-Oinitrotoluene I \2,6-DinitrotolueneDietnvlont'ia ate4-Cnlorocneiyl-pneiv leanerFluorene4-Nitroaru line4, 6-Dinitro-2-Metnvl phenolN-Nitroscciohenylamine •

- IRF Ml

3*5 T

4-3rotnoDnsnyl-onenylether jHexacnlorcoenzenePentachloroohenol 1Phenantnrene }AnthraceneDi-n-ButvlohthalateFluoranthene 1Pyrene 1Butyl benzvl phthal ateBenzoia)Antnracenebisl2-£thvlhexyl )PhthalateChrysene 1Oi-n-Octvl Phthalate

t

It t

Benzo(b)Fluoranthene IBenzo(k)FluorafltheneBenzola jPyreneIndeno(l,2,3-cd)PvreneDiDenz(a,h)Anthracene- |Benzo(a,h,1) Pervlene

*

1

Cont. Cal. ICont. Cff l .^ 1

RF

I 1

1

iD lw |RF1

111

1

t 11 1

tI II 1

1

*0 *

1

n3

Cont. Cav£l-o

RF

111

11

11 -

1

1

»0 *I _,

--«*,

1



1/87

CASE*


SEMIVOLATILE KSL COMPOUNDS

/ < CONTRACTOR

mornJ

Unit. Cal . ICcnt. Cal. Cor.t. Cal. Conz. Ca . Con:. Calrt*DAiE/ i iMt : I ?/tl

IRF SRSOPhenolbi s(-Z-Chloroet,nvl JEtner2-ChiOPConenol1 ,3-OicriloPODenze*.e1.4-Dicn opocer.zeneEe".rvi A conc i1 ,2-Dicnlor03enzer.e2-Metnvlonenol

^îs;2-cn orolsooroovl JEtner4-Me^nvlohenolN-Nizroso-Di-n-Proovlar.ineHexacnlopoetnaneNltPODenzeneIsoonorone2-Nitroohenol2.4-OlmethvlonenolBenzole Acid .bi s ( 2-Ch 1 oroethoxv )Me"hane2 ,4-Di cnl opoonenol1,2,4-TricnlorooenzeneNaontnalene4-ChloroanilineHexacnloroDutaaiene4-ChlOPO-3-Metnylonenol2-Metnvlnaontnalene

^Hexacniorocvclooentadiene2,4,6-TpichloPOonenol2,4,5-TplchloPOohenol2-Chloronaontnalene2-NitPoanilineDimetnvl PhtnalateAcenasntnvlene

» t-I

IF ISO

111

11

,0*3! 3^ K/RI11

11

.0| tf/RI1 1

1111

*

3-iNitroanilineAcanaontnene2,^-DimtPooneno'i4-NitPoonenolDlcenzofupan

* AFFECTEDSAMPLES:

En /"T7

_ • I I V- IRF '• J

1i

1

1

iiiI

iti

i3

IRF

1111

11

•

j w

11

r | Mwi | w |1 "~

1|1111

1

g>— j

1

1 11 11 1I I -1 11 1I I1 11 11 1

11

* These flags should be applied to the analytes on the sample data sheets,

CASE*


SEMIVOLAT1LE HSL COMPOUNDSI Pa9e * ^j_______ CONTRACTOR E K 1/1*0 J-

DATE/TIME:

2,4-01r,itrotoluene2»6-Oinitro':olueneDiecnylorâlate4-Cnlcroonsnvl-pne iv letterFlucre-:e4-N1tPOenilinel^-Dinitro-S-Me'nvlonenol

T^N-N-itPoscciDhenvlamine4-3 roôsneny l-oneny let herHexacn'iorcoenzenePentacnloroohenolPhenar.inreneAntnraceneDi-n-5utylohthalateFluopantnenePypeneButvlbenzvlDhthalateBenzo(a)Antnracenebis(2-Ethvlhexyl JPhthalateChryseneDl-n-Octyl PhthalateBenzol bJFluorantheneBenzo(k)FluopanzheneBenzoiaJPvpene

- Indenot 1 ,2 ,3-cd )PypeneDioenz(a,h)Anthracene-Benzo(o,h,1 ) Pervlene

Init

ftRr

:

I

I

I

I

. Cat(J«SD

I

?r

»- 1

r

i

Cont

RF

II

. Ca

10

11

L

*

i

111

Cont

RF

. (a

10 |i

i

111

1

.11w 1

ii1

1

1

Con*

RF

. Ca

•0

I.I1

* 1

1

Cont

Rf*

-1

. Ca

to

1

i .

*

SEE PAGH 1 FOR AFFECTED SAMPLES.


1/87

J3<\OENVIRODYNE

ENGINEERSAugust 14, 19871990-7351

Ms. Carol Schaeffer 3;. ;. j. ,'\A -•Sample Management Office t _..„,,, '.:..-••—••209 Madison Street, Suite 200Alexandria, Virginia 22314

Dear Ms. Schaeffer;

Enclosed are partial results of analysis of Case 7351 for Volatiles, BNAs,and Pesticides/PCBs performed under Contract Number 68-01-7087. Four soilsamples, EM877 through EM880, were received on July 17, 1987. it is ourunderstanding that the case is completed with the submission of these re-sults.

All semivolatiles were extracted and analyzed according to the low) levelsoil protocol. No Pesticide/PCBs were detected on the first GC quanti-tation runs, so second column confirmation was not required.


Sincerely,


MCW/jagEnclosure

______IVIn Reference to Case No(s)

Contract Laboratory ProgramREGIONAL/LABORATORY COMMUNICATION SYSTEM

Telephone Record Log

Date of Call:

Laboratory Name:Lab Contact:

Region:Regional Contact: ' -|s

Call Initiated By: __ Laboratory ^ Region

In reference to data for the following sample numbeKs):

rT\O

«/

Summary of Questions/Issues Discussed:

i J C

^ .3

Summary of Resolution:

£~ 2T T r-.î 1 j^. /f *- .-^ A •»../- r^. Q

- y

A t ^.,

f

-f

_ . »."r* /

Signature '

Distribution: (1) Lab Copy, (2) Region Copy, (3) SMO Copy

Date

? ?.

SOIL SURROGX.E PERCENT RECOVERY SUMMARYC«MNct*?*»r _

M»i»*ft*.

mfsn lE.mVttfYiB* 2EfY^b

£[wnerfl^n^

•

•

.

•

* VALUES""ADVISOR

CommMi

i ._. .T-Sb" _ CiX * LUrfL.ni

. . ._ -_- . -_ VOLAltLf - - -

1*. *(»<•••&'.."..« 7

ID'4

| \01D*>U 4H5lo^

•'•

io*4VDIloSqi^3-^"1

t !-•*•(•••

i,;,. ,;,/•*^^

^S"c\^^XIOO101

Mlracl Labnr.t-vy fcÛI ÔDVMfc ronlr«r.l Mn b^S '01 - /&* 7

~^ff.l.36>juflW

310,%&

TV 10/- -7/4&UA

^55/^^'+tta

,

*"

<?/^?/JU/JQQffft<&t

• t

ARE OUTSIDE Of CONTRACT REQUIRED OC LIMITS VolitY LIMITS ONLY Simi"

Pt>tl(

EUI-VOIATIL E -.-.-----_.-._--.

»»t«<K-ll

IH- nil

/ i!5ftjj*ff *{-*

it *l *1

*£>'7+3S/

!•*• „ ,*^ . out of /a iVoUtlUit - — &£. out oIdtsi — C — out o

r . L?^ |r <^ I

t-'iWO**-

111*1111

30v53^/•t-3/Ztt)

-/<?•*

.'.*'' •

i.*.t i *•••••*•

HI* till

*j-l

59lUfl

37/.?¥36>

•. . '

., •

/

1

-PCSTlClOC-

.**

/06///

M\/<?&// -3/£Z£U

ouUidi of QC limits 7/86

outildi or QC limits

«•: ———— - ————— - ——— —— ————————————————————————————————————— j^^ ————

' ——————————————————————————————————————————————————— £jj£» »_

VA)

FORM II

'/'i./1

V;*. No. Rdglon


Contraclor Conlracl

otrc or Vilftll CCMC.LtvfL Mir.io C*S COUfOUNO iNSi.riC M UNIMOVHl CONC. IMlfl CNDL

ov ' u 10

E> Sail 5185-i

Commonta:

FORM IV 7/85


C«)« No. .Region Cootriclor u Contract No.

nc to 0»lt Of VtlHIl !Gb IN jr. 10 CAl NUUtCM COU^CUNO (MSI.. TIC ON UHKHQWH! CMC.

SR1S-1 (HA - 360(.0005

3-503

V.I

Commonl>;

FORM IV 7/85

f 9

CX1TULATED INSTRUMENT DETECTION LIMITS

\

VK, 107-02-t •crolein3V) 107-13-1 •crylorutrUe

V) kcnzencV) carbon

I7V) IOt-90-7 chJoroberacnr0V)IV) 71-39-4 IJJ-frichJoroethfcftt

UJv) 7VK-> MîehlofBTthant"*VJ 7VO&.3 l,U-TTiehiorpe^h*f*T

3V)(UV) 7VOC-J*\<V) ) ID-TV I 7-cfJftroetf>yl»inyl

47-44-3 chloreform7V35-*

IM-40-5

O3V) 10041-02-4 »vu- l_J»4ichJor opropem10041-01-05

34V) JOG-* I -* nhy IbcnieneChJartoe

7»-47-3 chloremethanc(UV) 7M3-9

7V2V2 kromoformWomodj chlor omcth&nv

75-4V* tluerotrkMoromethvte7V7l-t

Chlor odibromomtthanr127-14-4 ^BUftChiorovthwe

O4V) I04-U-) «»ltmK07V)(UV) chloride

47

TVfV)7 VIVO

104-10-1100^2.)I04-OV4

»* •! xvl*n«t

inn100

252525

252525

2525505025252525252525255050502525

2525252550

100100

2510010025to

"25"

f -C

U»P) JCVOQ-?OOP) 40-37-1C»1P) 57-?*-*»2P) JO-7J-Smp) 7J-SV*t»*P> 72.)*-tttJP) 1IV2V7(WP) I1J.21-7t»7P) 1031-07-1IMP) 72-JO-t<WP) 7*21- »V*(1DOP) 74-44-1UOIP) I024-37-JU02P) Jl*-l*-4(103P) Jl*-tV7(10tP) >lVW-t(105P) «-l^»CIMP) J>*4»-2l-»(I07P) 11017-^Vl(IMP) 11104-71-2(1WP) lll*l-lt-S(HOP) t2i72'7V4(IMP) 11 OH- 12- 5(11 IP) 12474-H.7 &D010V2

tltfrmtficldnnCMord*ne•(»'-DDT«,*'-DDE»,»'-DDD•C-4ndo»u!l»n_^ -*r>do»uli*n•ndcnuHan luMifr•nsrift«n*i fcJOe^wflthf¥t»ctjorhcp\»ctto< tpeuoc•C-&HC^tf-BMC/ -*HC-r-*HC Umtene)K<VI2*2PC6-12HPC B- 127)PCB-1232PCB-12HPC B- 12*0PCB-lOlttouphrnr

1.51 .512

2.2

1.21.22.11.42.11.82.11.51.51.22.02.01.5

302040

40202040

200

n

CALCULATED INSTRUMENT DETECTION LIMITS

\

23.

1JIijiii

21 A)22A)24 A)

"J1A)>A)^7 A);3iA)15'A)

;4CM(41. A)(43A>

(IB)136)UB)(9fi)02B)(UB)UOB)(33B)Q4B)Q7B)C21B)O5B)(34B)(STB)O9B)(*0fi>I+1B)<42B}(43B)

U-04-239-50-795-37-*

120-S3-2105-47-9U-73-3

JOO-02-731-21-5

53^-32-1t7-lfr-5

10&-9V243-13-095- 1-7

10t- 39-495-95-4tV 32-992-17-5

120-12-1111-74.147-72-1

11 1-* k-*

9l-3t-79V30-1

5* 1-7 VI104-44-791-94-1

121-14-2404-70-2123-44-7204-44-0

700V72-3101-33-J

394 3V 32.9111.91-1

2,4.4- tricMoropSenoIp-chJ or o-m-cr e» 12- ChJorophenol2tfc-dJchJoMphenol2,4-di me thy tpheno 12- nitrophertol•-riitrophenol2,4-4iniiropSenol4 ,4-dinj tr o- 2-mtth y tp Senolpent achlor op Senolphenolbenzoic acid2-methylphenolVmethy Ipnenol2.*,3-trichlorophenoIacenaphthenebenzidine1 *2 , 4- tr ichlorobenzenehexachJorobenzenehezacHloroethAnebii{2-chJof oe thy I fe ther2-chloron*phthalene1 îchlorobenzene1 J-dJchlorobenzene1 ,4-dichtar obenzene).T-tfichloroberaidine2.4-dinitrotoluene2.4-dinitrotolueneU-djp hefty Ihydratifl*tluaranthenet-chloropSenyl phenyl ether4-bromophenyl phenyl etherbn (2-chloretMpropyl) etherbii (3-chioroethoxv) methane

10101010in1020201020102010101010101010101010101010102020101010101010

(32B)O3B)(MB)(53B)t * J*\\^WO|

(4 IB!(42B)(43B)(44B)(47B)<41B><4»B)(7 OB)(7 IB)(726)(73B»(7*6)O36)

t7-4S-377'*?-*7»-39-l91-20-391-15-342-73-9K4-30-4

421-44-7117-11-7B5-41-7S*-74-2

i i7-i*-a•4-44-2

131-11-)54-55*350-32-1

305-99*2207 -OS-9

he xachlor obirtad ieneheiachlofocydopentad.eT*isopnoronerMphihAJenehitrobenzeneN-nitroiod tmethy UmineN-nitr OKMJ ipHeny Um irveN-nitrnodipropyl*minebis C?-«thylheiy!) phth*J»tebenzyl butyl phth*l*iedi-ivôTyl phthalkietfi-n-octyl phthklitetfiethyl phthalaietf methyl phth*Utebenz0(aknthracen«benxoUfeyrenebemoCb Hi uor *ntt»en«benzoOiH luor antNene

10101010

in20101010101010

1010101010

10<74B) 211-01-9 chrrwne 10C77B)C7SB)(79B)UOB)a IB)U2B)(iJB)a»B)

20S-94-S120-12-7191-24-214-73-715-01 -ISV70-3

193-39-3129-00-047.JV3

100-31-4104-47-1132-44-991-57-4U-7»-*99-09-2

100-01-4

acen^hthyleneanthracenebenzo^hilperylenefJuorene»henanthren«tflbenzota lanthr aceneIndenef 1 ,2.3-cdlp yrene•TTVfW

•fulinebenzyl alcohol4-cMeroanUineCbenzolxraf*3-tnethy tnaphthalene2-*utr*arulir*eJ-futraanilii»4-rotfMniline

10101010

" io101010101010

10101010

10

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