Course Syllabus - الرئيسيةpharmacy.uobasrah.edu.iq/images/acadimic_desc... · Major intra and extra cellular electrolytes. 2 Preparation and standardization of 1N 1NaOH (known

College of PharmacyDepartment:Pharm.Chem.5thStage:

Ministry of HigherEducationAnd Scientific ResearchUniversity of Basrah

CourseSyllabus

Name of the First Teacher of the Course:Dr.HatmAhmd

Academic Rank: Prof

Degree : PhD

Email:

Name of the Second Teacher of the Course:Dr.MaanAbdulrazaq

Academic Rank: Lecturer

Degree:PhD

Email:

Name of the Third Teacher of the Course:Dr.Kowlahabdulrasol

Academic Rank: Assist prof

Degree:PhD

Email:

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Advanced Pharmaceutical AnalysesCourse Title

SemesterAcademic System

: To study spectrometric methods used for identification andObjectivescharacterization of organic compounds, including UV, IR, MASS and NMRspectroscopy; it enables students to understand the applications of these techniquesfor qualitative and quantitative analysis of organic compounds.Course Objective

v

v

vTextbooks

.Spectrometric Identification of Organic Compounds bySilverstein, Bassler and Morrill; 2. Applications of absorptionspectroscopy of organic compounds by Dyer JR. 3. OrganicChemistry by McMurry; 5thed; Thomason learning CA, USA 2000.

Reference Books

End SemesterExaminationProjectQuizzesLaboratory

Work

TheoreticalContent

ExamCourse

Assessment forSemester System

(100%) 50551525

FinalExamination

LabWork

SecondTerm

MidtermExamFirst TermCourse

Assessment forAnnual System

(100%)

AdditionalInformation

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Weekly Schedule

NotesLaboratory WorkTheoretical ContentWeekIntroduction &demonstration tovisible spectrophotometry.

UV / visiblespectroscopy; Samplehandling andinstrumentation;

Characteristicabsorption of organiccompounds; Rules forcalculation of lambdamax and application;Application ofUV/visible;spectroscopy; Problemsand solutions.

1

Absorption spectra of knowncolored solution.


Characteristicabsorption of organiccompounds; Rules forcalculation of lambdamax and application;

Application ofUV/visible;

spectroscopy; Problemsand solutions

2

Absorption spectra of unknowncolored solution.


Characteristicabsorption of organiccompounds; Rules forcalculation of lambdamax and application;

Application ofUV/visible;

spectroscopy; Problemsand solutions

3

Beer's law plot of knownsolution.

Infra Red spectroscopy(theory and H-bonding

effect; Samplingtechniques and

interpretation ofspectra; Characteristicgroup frequencies of

4

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organic compounds;Application of IR

spectroscopy; Problemsand solutions.

Beer's law plot of unknownsolution.



interpretation ofspectra; Characteristicgroup frequencies oforganic compounds;

Application of IRspectroscopy; Problems

and solutions

5

Colorimetric assay oftetracycline (FeCl3), knownsample.



interpretation ofspectra; Characteristicgroup frequencies oforganic compounds;

Application of IRspectroscopy; Problems

and solutions

6

Colorimetric assay oftetracycline (FeCl3), unknownsample

H1 –NucleomagneticResonance (NMR) and C13-

NMR spectroscopy;Introduction, the nature ofNMR absorption, chemicalshifts and factors affecting

them, information obtainedfrom NMR spectra, more

complex spin-spin splittingpatterns, application of H1-

NMR spectroscopy;C13-NMR spectroscopy:

introduction andcharacteristics, DEPT C13-

NMR spectroscopy.

7

Colorimetric assay oftetracycline (acid), knownsample.




8

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NMR spectroscopy.

Colorimetric assay oftetracycline (acid), unknownsample.







NMR spectroscopy.

9

Colorimetric assay ofstreptomycin (maltol, knownsample).







NMR spectroscopy.

10

Colorimetric assay ofstreptomycin (maltol, unknownsample).

Mass spectroscopy:Introduction and

interpreting Mass spectra;interpreting Mass spectrafragmentation patterns,Mass behavior of some

common functional groups.

11

Colorimetric assay ofstreptomycin (oxidized, known

Mass spectroscopy:Introduction and12

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sample).interpreting Mass spectra;interpreting Mass spectrafragmentation patterns,Mass behavior of some

common functional groups.

Colorimetric assay ofstreptomycin (oxidized,unknownsample).

elemental microanalysisCHNSO13

Colorimetric assay oftetracycline (basic, knownsample).


Colorimetric assay oftetracycline (basic unknownsample).


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College of PharmacyDepartment:Pharm.Chem.1stStage:


CourseSyllabus

Name of the First Teacher of the Course : Dr.husenhasenhusen

Academic Rank: prof

Degree : PhD

Email:

Name of the Second Teacher of the Course:Dr. kowlaabdalrasol

Academic Rank: Assist Prof

Degree:PhD

Email:

Name of the Third Teacher of the Course: Dr. husennaser

Academic Rank: lecturer

Degree : PhD

Email:

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Analytical ChemistryCourse Title


To provide students with a sound theoretical back ground inchemical principles that is essential to practice chemical analysis.It enables students to understand the importance of judging theaccuracy and precision of experimental data and techniques ofquantitative analysis, and also to show that theory frequentlyserves as a useful guide to the solution of analytical problems.

Course Objective

vFundamentals of Analytical Chemistry by Stook and WestTextbooks

v

vFundamentals of Analytical Chemistry by Stook and West.

v

Reference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule

NotesLaboratory WorkTheoretical ContentWeekDemonstration of some

laboratory equipments.

Review of elementaryconcept important to

analytical chemistry: Strongand weak electrolytes;important weight and

concentration units.

1

Separation and identification of

group 1 cations (individual test).

The evaluation of analyticaldata: Definition of terms.2

Analysis of group 1 cataionsmixture.

An introduction togravimetric analysis:

Statistical analysis of data;rejection of data;

precipitation methods;gravimetric factor.

3

Preparation and standardizationof an acid.

Buffer solutions: Theory ofneutralization titrations of

simple system.4

Determination of thepercentage of acetic acid.

Theory of neutralizationtitrations of complexsystem; Precipitation

titrations.

5

Analysis of sodium carbonateand sodium hydroxide mixture.

Calculation of pH incomplex system; Volumetricmethods based on complex

system.

6

Determination of chloride by theMohr method.

Equilibria in oxidation-reduction system; theory of

oxidation-reductiontitrations.

7

Determination of chloride by theVolhard method.

Spectrophotometricanalysis: An introduction tooptical methods of analysis;

Methods based onabsorption of radiation.

8

Preparation and standardizationof 0.1N KMnO4.

The scope ofapplications of

gravimetric analysis:Inorganic

precipitating agents;organic precipitating

agents

9

Determination of ferrousform of iron in Mohr's salt

An introduction tovolumetric methods

of analysis:10

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Volumetriccalculations; acid-base equilibria and

pH calculations.Determination of total hardness

in tab water.complex system11

Gravimetric determination ofNickel.

complex system12Gravimetric determination

of Nickel.complex system13

Gravimetric determinationof Mg.

complex system14Gravimetric determination

of Ca.complex system15

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College of PharmacyDepartment:3thStage:

Ministry of Higher EducationAnd Scientific ResearchUniversity of Basrah

CourseSyllabus

Name of the First Teacher of the Course: Dr. retasabah


Degree: PhD

Email:

Name of the Second Teacher of the Course: mazennadem


Degree : MSc

Email:

Name of the Third Teacher of the Course: Dr. raheemjamail


Degree: PhD

Email:

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Inorganic Pharmaceutical ChemistryCourse Title


To present a review of the principles of inorganic chemistry thatapplied to medicinal and /or pharmaceutical chemistry. It includesunderstanding atomic and molecular structures, and explanation ofatomic structures and the relationship with binding forces andcomplexation. It also describes inorganic products used aspharmaceutical preparations or diagnostic tools.

Course Objective

Wilson and Gisvold; Textbook of Organic medicinal and

Pharmaceutical chemistry; Delgado JN, Remers WA

vTextbooks

v

Inorganic Medicinal and Pharmaceutical Chemistry by Block,

Roche Soine and Wilson, Latest edition

v

Reference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule

NotesLaboratory WorkTheoretical ContentWeek

Preparation and standardization of 1NHCl (known sample).

Atomic and molecularstructure/Complexation.1

Preparation and standardization of 1NHCl (quiz and unknown).

Major intra and extracellular electrolytes.2

Preparation and standardization of 1N1NaOH (known sample).

Major physiologicalions.3

Preparation and standardization of 1NNaOH (quiz and unknown).

Dentals product4

Assay of NaOH solution (knownsample).

Electrolytes used inacid- base balance.5

Assay of NaOH solution (unknownsample).

Physiological acid- basebalance.6

Assay of sodium benzoate (knownsample).

Essential and trace ions:Iron, copper, sulfur,iodine.

7

Assay of sodium benzoate (quiz andunknown).

Non essential ions:Fluoride, bromide,lithium, gold, silver andmercury.

8

Assay of Borax (explanation of basicconcepts).

Gastrointestinal agents.9

Assay of Borax (quiz and unknown).Acidifying agents.10

Assay of citric acid (known sample).Antacids.12

Assay of citric acid (unknown sample).Protective adsorbents.13

Assay of magnesium hydroxide (knownsample).

Radiopharmaceuticalpreparations.14

Assay of magnesium hydroxide (quizand unknown).

Radio opaque andcontrast media.15

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College of PharmacyDepartment:Pharm.Chem.2ndStage:


CourseSyllabus

Name of the First Teacher of the Course: Dr. shaker abdalsalumnamaa

Academic Rank: prof

Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. husamhamza

Academic Rank: Assist. prof

Degree : PhD

Email:

Name of the Third Teacher of the Course: Dr.Huda Salah


Degree: PhD

Email:

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Organic Chemistry IICourse Title


To enable students to understand the chemistry of carbon, andthe classification, properties and reactions of organic compounds.It includes understanding the basic structure and properties oforganic halides, carboxylic acids, aldehydes, ketones and amines,in addition to the principles and application of stereochemistry onthese compounds.

Course Objective

1- Organic Chemistry by Robert T. Morrison and Robert N. Boyd.(Latest edition).

2- Organic Chemistry by Mc Murry; Thomason learning; CA, USA; (LatesTextbooks

1- Organic Chemistry by Robert T. Morrison and Robert N. Boyd.(Latest edition).

v2- Organic Chemistry by Mc Murry; Thomason learning; CA, USA; (LatestReference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Determination of meltingpoint (Known sample).

Aromatic Hydrocarbons(includes benzene,electrophilic aromaticsubstitution, arenas andtheir derivatives).

1

Determination of meltingpoint (quiz and unknown).

Carboxylic acids:properties andreactions.

2

Determination of boilingpoint (known sample).

Functional derivativesof carboxylic acids.3

Determination of boilingpoint (quiz and unknown).4

Elemental analysis(explanation of basicconcepts).

Amines I and II.5

Elemental analysis (knownquantity and qualitysample).

Aldehydes and ketones(include also aldol andClaisen condensation);Classification, reactionsand properties.

6

Solution and filtrationtechniques (explanation ofbasic concepts).

Phenols.7

Re-crystallization (knownsample).


8

Re-crystallization (quiz andunknown sample).

Carboxylic acids:properties andreactions.

9

Extraction technique(known sample).

Functional derivativesof carboxylic acids.10

Extraction technique (quizand unknown).11

Distillation techniques(known samples).

Amines I and II.12

Distillation techniques (quizand unknown).

Aldehydes and ketones(include also aldol and13

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Claisen condensation);Classification, reactionsand properties.

Sublimation technique(known sample).

Phenols.14

Sublimation technique (quizand unknown).


15

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College of PharmacyDepartment:Pharm.Chem.5thStage:


CourseSyllabus

Name of the First Teacher of the Course: Dr.raheemjameel


Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. leaqaaabdulratha


Degree: PhD

Email:

Name of the Third Teacher of the Course: Dr. mazanNadm

Academic Rank: Lecturer

Degree: MSc

Email:

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Organic Pharmaceutical Chemistry IVCourse Title


Course Objective


Pharmaceutical chemistry; Delgado JN, Remers WATextbooks

vWilson and Gisvold; Textbook of Organic medicinal and

Pharmaceutical chemistry; Delgado JN, Remers WA

v

v

v

v

Reference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Basic concept of prodrugs;Covalent bonds (cleavable);Prodrugs of functional groups;Types of prodrugs.

1

Types of prodrugs.2Types of prodrugs.3Project.4Chemical delivery systems;Polymeric prodrugs; Types andstructure of polymers; Cross-linking reagents

5

Types of prodrugs.6

Types of prodrugs.7

Drug targeting8

Drug delivery system9



Combinatorial chemistry;Peptides and other linearstructures; Drug like molecules;Support and linker; Solution-phase combinatorial chemistry.

12

Solid support13

Detection, purification andanalgesics; Encodingcombinatorial libraries; High-throughput screening; Virtualscreening; Chemical diversityand library design.

14

Solid support15

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College of PharmacyDepartment:Pharm.Chem4ThStage:


CourseSyllabus

Name of the First Teacher of the Course: Dr. Leaqaaabdurathraheem


Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. raheemjameel


Degree: PhD

Email:

Name of the Third Teacher of the Course: Mazannadeam


Degree: MSc

Email:

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organic Pharmaceutical Chemistry IICourse Title


The course is devoted to the discovery and development of newagents for treating diseases, and enables translating the drugstructural formula into therapeutic effect. Additionally, it focuses onthe methods of preparation for some pharmaceutical agents

Course Objective




Pharmaceutical chemistry; Delgado JN, Remers WAReference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Preparation of salicylic acid.Cholinergic agonists;1

Re-crystallization of salicylicacid.

Cholinergic agonists;stereochemistry and structure-activity relationships (SAR);products; cholinesterase inhibitors.

2

Synthesis of aspirin.Cholinergic blocking agent;structure-activity relationships(SAR); Solanaceous alkaloid andanalogues; synthetic cholinergicblocking agents and products;ganglionicblocking agents(neuromuscular blocking agents).

3

Re-crystallization of aspirin.Analgesic agents (SAR of morphine,SAR of meperidine type molecules;SAR of methadone type compounds;N-methylbezomorphans, antagonisttype analgesics in benzomorphans).

4

Assay of aspirin (knownsample).

Cholinergic blocking agent;structure-activity relationships(SAR); Solanaceous alkaloid andanalogues; synthetic cholinergicblocking agents and products;ganglionicblocking agents(neuromuscular blocking agents

5

Assay of aspirin (unknownsample).

Analgesic agents (SAR of morphine,SAR of meperidine type molecules;SAR of methadone type compounds;N-methylbezomorphans, antagonisttype analgesics in benzomorphans

6

Preparation ofnitrobenzene.

Analgesic receptors, endogenousopioids; Products; Antitusive agents;Anti-inflammatory analgesics.

7

Preparation of aniline.8

Preparation of acetanilide.9

Re-crystallization ofacetanilide.

Adrenergic agents (Adrenergicneurotransmitters); Adrenergic10

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receptors; Drugs affectingAdrenergic neurotransmission;Sympathomimetic agents;Adrenergic receptor antagonists.

Chlorosulfonation ofacetanilide.11

Amination of p-chlorobenzene sulfonylchloride.

CNS depressant; Benzodiazepinesand related compounds;Barbiturates; CNS depressant withskeletal muscle relaxant properties;Antipsycotics; Anticonvulsants.

12

Hydrolysis of p-chlorobenzene sulfonylchloride to sulfanilamide.

CNS depressant; Benzodiazepinesand related compounds;Barbiturates; CNS depressant withskeletal muscle relaxant properties;Antipsycotics; Anticonvulsants.

13

Assay of sulfa drugs (knownsample).

Steroid hormones14

Assay of sulfa drugs(unknown sample).

Steroid hormones15

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College of PharmacyDepartment:Pharma.Chem.Stage: 4th


CourseSyllabus

Name of the First Teacher of the Course: Dr. Raheem Jameel


Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. retasabah


Degree: PhD

Email:

Name of the Third Teacher of the Course: Dr. Leaqaaabduratha


Degree: PhD

Email:

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Organic Pharmaceutical Chemistry IIICourse Title


To enable understanding mechanisms of drug action, including antibacterial,antifungal and antiviral agents, at molecular level, and the role of medicinalchemistry in the discovery and development of synthetic therapeutic agents.It also enables students to understand the concept of structure-activityrelationship and its application in design and synthesis of newchemotherapeutic agents and hormone derivatives with potential biologicalactivity.

Course Objective






Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Cannizaro reaction (part I).β-Lactam antibiotics (Penicillins); β-Lactamase inhibitors; Cephalosporinsand Monobactams.

1

Cannizaro reaction (part II).Aminoglycosides andChloramphenicol; Tetracylines;Macrolides; Lincomycins andPolypeptides; Antiviral agents(properties of viruses, viralclassification, products).

2

Re-crystallization of benzoicacid.

Sulfonamides (chemistry,nomenclature, mechanism of action,resistance, toxicity, side effects,metabolism, protein binding,distribution and SAR); products;Sulfones.

3

Assay of ascorbic acid(known sample).

Anti-neoplastic agents: Alkylatingagents; Antimetabolites; Antibiotics;Plant products; Miscellaneouscompounds.

4

Assay of ascorbic acid(unknown sample).

Hormones and related compounds;Future anti-neoplastic agents;Monoclonal antibodies; Gene therapyof cancer.

5

Synthesis of Phenol.β-Lactam antibiotics (Penicillins); β-Lactamase inhibitors; Cephalosporinsand Monobactams.

6

Assay of phenol (knownsample).

Aminoglycosides andChloramphenicol; Tetracylines;Macrolides; Lincomycins andPolypeptides; Antiviral agents(properties of viruses, viralclassification, products).

7

Assay of phenol (unknownsample).


8

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Synthesis of chlorbutanol.Anti-neoplastic agents: Alkylatingagents; Antimetabolites; Antibiotics;Plant products; Miscellaneouscompounds.

9

Synthesis of paracetamol.Hormones and related compounds;Future anti-neoplastic agents;Monoclonal antibodies; Gene therapyof cancer.

10

Cannizaro reaction (part I).β-Lactam antibiotics (Penicillins); β-Lactamase inhibitors; Cephalosporinsand Monobactams.

11

Cannizaro reaction (part II).Aminoglycosides andChloramphenicol; Tetracylines;Macrolides; Lincomycins andPolypeptides; Antiviral agents(properties of viruses, viralclassification, products).

12

Re-crystallization of benzoicacid.


13

Assay of ascorbic acid(known sample).

Anti-neoplastic agents: Alkylatingagents; Antimetabolites; Antibiotics;Plant products; Miscellaneouscompounds.

14

Assay of ascorbic acid(unknown sample).

Hormones and related compounds;Future anti-neoplastic agents;Monoclonal antibodies; Gene therapyof cancer.

15

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College of PharmacyDepartment:Pharm.Chem 1stStage:


CourseSyllabus

Name of the First Teacher of the Course: Dr. MontherAbduljalel


Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. HusamHmzah

Academic Rank: Assist. Prof

Degree: PhD

Email:

Name of the Third Teacher of the Course: Dr. Huda Salah


Degree: PhD

Email:

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Organic Chemistry ICourse Title


To enable students to understand the chemistry of carbon, andthe classification, properties and reactions of organic compounds.It includes understanding the basic structure and properties ofalkanes, alkenes and alkynes, in addition to the principles ofstereochemistry and features of aromatic compounds.

Course Objective

Textbooks

Organic Chemistry by Robert T. Morrison and Robert N. Boyd .

Organic Chemistry by McCurry; 5th ed. Thomason learning;

CA,USA; 2000.

Reference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Determination of meltingpoint (Known sample).

Introduction.1

Determination of meltingpoint (quiz and unknown).

Alkanes and methane.2

Determination of boilingpoint (known sample).

Alkenes I and II3

Determination of boilingpoint (quiz and unknown).

Alkynes and dienes.4

Elemental analysis(explanation of basicconcepts).

Stereochemistry I & II5

Elemental analysis (knownquantity and qualitysample).

Alcohols and ethers.6

Solution and filtrationtechniques (explanation ofbasic concepts).

Alkyl halides.7

Re-crystallization (knownsample).

Cycloalkanes.8

Re-crystallization (quiz andunknown sample).

Introduction.9

Extraction technique(known sample).

Alkanes and methane.10

Extraction technique (quizand unknown).

Alkenes I and II11

Distillation techniques(known samples).

Alkynes and dienes.12

Distillation techniques (quizand unknown).

Stereochemistry I & II13

Sublimation technique(known sample).

Alcohols and ethers.14

Alkyl halides.15

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College of PharmacyDepartment:Pharm.Chem2ndStage:


CourseSyllabus

Name of the First Teacher of the Course: Dr. Shaker Abdulsalm

Academic Rank: Prof

Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. husamhamza


Degree: PhD

Email:

Name of the Third Teacher of the Course: Dr. montherabduljalel


Degree:PhD

Email:

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Organic Chemistry IIICourse Title


To teach students the principles of heterocyclic chemistryincluding the fundamental principles and the features, classes andreactions of heterocyclic compounds; it enable students to applythese principles in complicated reactions that involveheteroatoms.

Course Objective

Textbooks

Reference Books


Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Determination of solubilityclass (known sample).

Heterocyclic system:Classes of heterocyclicsystems; generalstructures; properties;Occurrence in natureand in medicinalproducts.

1

Determination of solubilityclass (quiz and unknown).

Five-membered ringheterocycliccompounds: pyrrole;furan and thiophen.

2

Identification of alcohols(known sample, quiz andunknown).

Source of pyrrole, furanand thiophen.3

Identification of phenols(known samples).

Electrophilicsubstitution in pyrrole,furan and thiophen:Reactivity andorientation.

4

Identification of phenols(quiz and unknown).

Six-membered ringheterocycliccompounds: Structure& reactions of pyridine.

5

Identification of aldehydesand ketons (explanation ofconcepts andquiz).

Saturated five-membered heterocycliccompounds.6

Identification of aldehydesand ketons (known sample).

Heterocyclic of five &six member rings withtwo & threeheteroatoms.

7

Identification of aldehydesand ketons (quiz andunknown).


8

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Identification of carboxylicacid (explanation ofconcepts).

Five-membered ringheterocycliccompounds: pyrrole;furan and thiophen.

9

Identification of carboxylicacid (known sample).

Source of pyrrole, furanand thiophen.10

Identification of carboxylicacid (quiz and unknown).

Electrophilicsubstitution in pyrrole,furan and thiophen:Reactivity andorientation.

11

Salts of carboxylic acids(known sample).

Six-membered ringheterocycliccompounds: Structure& reactions of pyridine.

12

Salts of carboxylic acids(quiz and unknown).

Saturated five-membered heterocycliccompounds.

13

Classification of reactions ofamines (known sample).

Heterocyclic of five &six member rings withtwo & threeheteroatoms.

14

Classification of reactions ofamines (quiz and unknown).


15

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College of PharmacyDepartment:Pharm.Chem 3rdStage:


CourseSyllabus

Name of the First Teacher of the Course: Dr. Reta Sabah


Degree: PhD

Email:

Name of the Second Teacher of the Course: Dr. Raheem Jameel


Degree: PhD

Email:

Name of the Third Teacher of the Course: MazenNAdam


Degree: MSc

Email:

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organic Pharmaceutical Chemistry ICourse Title


To enable understanding mechanisms of drug action at molecularlevel, and the role of medicinal chemistry in the discovery anddevelopment of synthetic therapeutic agents. It also enablesstudents to understand the concept of structure-activityrelationship and its application in design and synthesis of newcompounds or derivatives.

Course Objective






Work

TheoreticalContent

ExamCourse


(100%) 50551525

FinalExamination

LabWork

SecondTerm



(100%)


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Weekly Schedule


Preparation and standardization of0.1N KMnO4 (known sample).

Drug distribution.1

Preparation and standardization of0.1N KMno4 (quiz and unknown).

Acid- base properties.2

Assay of hydrogen peroxidesolution (known sample).

Statistical prediction ofpharmacological activity.3

Assay of hydrogen peroxidesolution (quiz and unknownsample).

QSAR models.4

Assay of ferrous sulfate (knownsample).

Molecular modeling(Computer aided drug design).5

Assay of ferrous sulfate (unknownsample).

Drug receptor interaction:force involved.6

Preparation and standardization of0.1Na2S2O4 solution (knownsample).

Steric features of drugs.7

Preparation and standardization of0.1Na2S2O4 solution (quiz andunknown sample).

Optical isomerism andbiological activity.8

Assay of copper sulfate (knownsample).

Calculated conformation.9

Assay of copper sulfate (unknownsample).

Three- dimensionalquantitative structure activityrelationships anddatabases.

10

Assay of Chlorinated Lime (knownsample).

Isosterism.11

Assay of Chlorinated Lime (quizand unknown).

Drug-receptor interactionand subsequent events.12

Preparation and assay of Lugol'sSolution (known sample).

General pathways of drugmetabolism: Sites of drugbiotransformation;Role of cytochrome P450mono-oxygenases in oxidativebiotransformation; Oxidativereactions; Reductivereactions; Hydrolyticreactions; Phase II reactions.

13

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Preparation and assay of Lugol'sSolution (quiz and unknown).

Factors affecting drugmetabolism.14

Assay of Alum (unknown sample). Drug distribution.15

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Documents

Course Syllabus - الرئيسيةpharmacy.uobasrah.edu.iq/images/acadimic_desc... · Major intra and extra cellular electrolytes. 2 Preparation and standardization of 1N 1NaOH (known