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BULETINUL INSTITUTULUI POLITEHNIC DIN IAŞI Tomul LVIII (LXII) Fasc. 3 CONSTRUCŢII DE MAŞINI 2012 Editura POLITEHNIUM

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  • BULETINUL INSTITUTULUI POLITEHNIC DIN IAI

    Tomul LVIII (LXII) Fasc. 3

    CONSTRUCII DE MAINI

    2012 Editura POLITEHNIUM

  • BULETINUL INSTITUTULUI POLITEHNIC DIN IAI PUBLISHED BY

    GHEORGHE ASACHI TECHNICAL UNIVERSITY OF IAI Editorial Office: Bd. D. Mangeron 63, 700050, Iai, ROMANIA

    Tel. 40-232-278683; Fax: 40-232-237666; e-mail: [email protected]

    Editorial Board

    President: Prof. dr. eng. Ion Giurma, Member of the Academy of Agricultural Sciences and Forest, Rector of the Gheorghe Asachi Technical University of Iai

    Editor-in-Chief: Prof. dr. eng. Carmen Teodosiu, Vice-Rector of the Gheorghe Asachi Technical University of Iai

    Honorary Editors of the Bulletin: Prof. dr. eng. Alfred Braier, Prof. dr. eng. Hugo Rosman

    Prof. dr. eng. Mihail Voicu, Corresponding Member of the Romanian Academy, President of the Gheorghe Asachi Technical University of Iai

    Editors in Chief of the MACHINE CONSTRUCTIONS Section

    Prof. dr. eng. Radu Ibnescu, Assoc. prof. dr. eng. Aristotel Popescu Honorary Editors: Prof. dr. eng. Gheorghe Nag, Prof. dr. eng. Cezar Oprian

    Associated Editor: Assoc. prof. dr. eng. Eugen Axinte

    Editorial Advisory Board

    Prof.dr.eng. Dorel Leon, Gheorghe Asachi Technical University of Iai

    Prof.dr.eng. Nicuor Amariei, Gheorghe Asachi Technical University of Iai

    Assoc.prof.dr.eng. Aristomenis Antoniadis, Technical University of Crete, Greece

    Prof.dr.eng. James A. Liburdy, Oregon State University, Corvallis, Oregon, SUA

    Prof.dr.eng. Virgil Atanasiu, Gheorghe Asachi Technical University of Iai

    Prof.dr.eng.dr. h.c. Peter Lorenz, Hochschule fr Technik und Wirtschaft, Saarbrcken, Germany

    Prof.dr.eng. Petru Berce, Technical University of Cluj-Napoca Prof.dr.eng. Ion Bostan, Technical University of Chiinu,

    Prof.dr.eng. Noura -Barbu Lupulescu, University Transilvania of Braov

    Prof.dr.eng. Fabio Miani, University of Udine, Italy Republic of Moldova Prof.dr.eng. Walter Calles, Hochschule fr Technik und

    Wirtschaft des Saarlandes, Saarbrcken, Germany

    Prof.dr.eng. Mircea Mihailide, Gheorghe Asachi Technical University of Iai Prof.dr.eng. Sevasti Mitsi, Aristotle University of

    Prof.dr.eng. Doru Clrau, Gheorghe Asachi Technical University of Iai

    Thessaloniki, Salonic, Greece Prof.dr.eng. Vasile Neculiasa, Gheorghe Asachi Technical

    Prof.dr.eng. Francisco Chinesta, cole Centrale de Nantes, France

    Assoc.prof.dr.eng. Conalves Coelho, University Nova of Lisbon, Portugal

    University of Iai Prof.dr.eng. Fernando Jos Neto da Silva, University of Aveiro, Portugal Prof.dr.eng. Dumitru Olaru, Gheorghe Asachi Technical

    Prof.dr.eng. Juan Pablo Contreras Samper, University of Cadiz, Spain

    Assoc.prof.dr.eng. Mircea Cozmnc, Gheorghe Asachi

    University of Iai Prof.dr.eng. Manuel San Juan Blanco, University of Valladolid, Spain

    Technical University of Iai Prof.dr.eng. Spiridon Creu, Gheorghe Asachi Technical

    Prof.dr.eng. Loredana Santo,University Tor Vergata, Rome, Italy

    University of Iai Prof.dr.eng. Gheorghe Dumitracu, Gheorghe Asachi

    Prof.dr.eng. Cristina Siligardi, University of Modena, Italy Prof.dr.eng. Filipe Silva, University of Minho, Portugal

    Technical University of Iai Prof.dr.eng. Ctlin Fetecu, University Dunrea de Jos of

    Prof.dr.eng. Laureniu Sltineanu, Gheorghe Asachi Technical University of Iai

    Galai Prof.dr.eng. Mihai Gafianu, Gheorghe Asachi Technical

    Lecturer dr.eng. Birgit Kjrside Storm, Aalborg Universitet Esbjerg, Denmark

    University of Iai Prof.dr.eng. Radu Gaiginschi, Gheorghe Asachi Technical

    Prof.dr.eng. Ezio Spessa, Politecnico di Torino, Italy Prof.dr.eng.Roberto Teti, University Federico II, Naples, Italy

    University of Iai Prof.dr.eng. Francisco Javier Santos Martin, University of

    Prof.dr.eng. Alexei Toca, Technical University of Chiinu, Republic of Moldova

    Valladolid, Spain Prof. dr. Dirk Lefeber, Vrije Universiteit Brussels, Belgium

    Prof.dr.eng. Hans-Bernhard Woyand, Bergische University Wuppertal, Germany

  • B U L E T I N U L I N S T I T U T U L U I P O L I T E H N I C D I N I A I B U L L E T I N O F T H E P O L Y T E C H N I C I N S T I T U T E O F I A I Tomul LVIII (LXII), Fasc. 3 2012

    CONSTRUCII DE MAINI

    Pag.

    MOUSSA KARAMA (Frana), Comportarea barelor compozite laminate la interfeele dintre straturi (engl., rez. rom.)..................................................

    1 ISAAC NELSON (SUA), CONSTANTIN CIOCNEL (SUA) i HEIDI

    FEIGENBAUM (SUA), Curbele de reorientare pentru un aliaj Ni50Mn28.5Ga21.5 (engl., rez. rom.)...............................................................

    19 CIPRIAN ATNSOAEI, VIOREL GOAN i PAUL DORU

    BRSNESCU, Compozite din cordierit armat cu oxid de zirconiu(engl., rez. rom.).......................................................................................... 31

    RZVAN FLORIN BARZIC, ANDREEA IRINA BARZIC i DANA-ORTANSA DOROHOI, Comportamentul de deformre n condiii de forfecare a unor amestecuri de hidroxipropil celuloz/L-cistin (engl., rez. rom.)..................................................................................................... 41

    IONU DUMITRACU, PAUL-DORU BRSNESCU i BOGDAN LEIOIU, Studiu comparativ privind materialele compozite armatebidirecional cu fibr de carbon, cu matrice termorigid i termoplastic(engl., rez. rom.).......................................................................................... 47

    IONU DUMITRACU, PAUL-DORU BRSNESCU i VIOREL GOAN, Influena matricei asupra proprietilor ale materialelor compozite armate unidirecional cu fibr de carbon i matricetermoplastic (engl., rez. rom.).................................................................... 53

    EDUARD GHEBAN, NORINA FORNA i BOGDAN LEIOIU, Considera-ii asupra preciziei determinrii modulului de forfecare al unui acrilat de uz stomatologic (engl., rez. rom.)................................................................ 59

    EDUARD GHEBAN, NORINA FORNA I BOGDAN LEIOIU, Considera-ii asupra ncercrilor la traciune asupra unui material de uzstomatologic (engl., rez. rom.)..................................................................... 67

    DAN ILINCIOIU i COSMIN MIHAI MIRIOIU, Influena ipotezelor simplificatoare asupra distribuiei tensiunilor la structurile metalice hiperstatice (engl., rez. rom.).....................................................................

    75

    S U M A R

  • DAN ILINCIOIU i COSMIN MIHAI MIRIOIU, O comparaie ntre cteva soft-uri folosite pentru studiul tensiunilor mecanice n structuri metalice (engl., rez. rom.).. 85

    ADRIAN LIVIU PARASCHIV, MARIUS GABRIEL SURU i LEANDRU-GHEORGHE BUJOREANU, Variaia proprietilor, datorit coninu-tului de nichel i a prelucrrii termomecanice, la feroaliajele Fe-Cr-Ni-Siutilizate pentru pregtirea unor aliaje cu memoria formei pe baz de Fe (engl., rez. rom.).. 93

    MARIAN MARE, CRISTINA RACU, LILIANA BUHU i ADRIAN BUHU, Proprieti mecanice ale unor materiale compozitebiodegradabile cu matrice polimeric (engl., rez. rom.).............................. 101

    LEONID TARTAKOVSKY (Israel), VLADIMIR BAIBIKOV (Israel), MARCEL GUTMAN (Israel), DORON POPESCU (Israel), MARC VEINBLAT(Israel) i YORAM ZVIRIN (Israel), Compararea emisiilor poluante de la autobuzele urbane i de la automobilele de pasageri din Israel (engl., rez.rom.)............................................................................................................ 109

    VICTOR BRATU, ALEXANDRU BOROIU i ION TABACU, Cercetri cu privire la mbuntirea i modernizarea sistemului de transport public de persoane n zona preurban din oraul Piteti. (I) Studiul factorilor determinani pentru sistemul public (engl., rez. rom.)................................ 117

    CLAUDIU BUTNARU, Influena recirculrii gazelor de evacuare asupra arderii i emisiilor ntr-un motor HCCI (engl., rez. rom.)........................... 127

    CLAUDIU BUTNARU, Influena turaiei i a consumului de combustibil asupra gazelor de ardere (engl., rez. rom.).................................................. 135

    VASILE CAUNII, Aspecte privind strategiile de control a compresorului aerului condiionat (engl., rez. rom.)........................................................... 141

    COSTIN DRAGOMIR, CONSTANTIN PAN, NICULAE NEGURESCU iALEXANDRU CERNAT, Investigaii teoretice i experimentale ale motorului cu aprindere prin scnteie supraalimentat (engl., rez. rom.)....... 151

    MARIUS ATANASIU, MIHAI MARIUS PRODAN i EMIL JUGUREANU, Analiza comparativ ntre metoda produsului planar i metodageometriei plane pentru modelul matematic al compresorului spiral(engl., rez. rom.).......................................................................................... 159

    MIHAI ADAM, GEORGE OVIDIU RU i GHEORGHE DUMITRACU, Cercetri experimentale privind stocarea energiei termice n materiale cuschimbare de faz: aliaj eutectic Sn-Pb (engl., rez. rom.)...

    167

    MIHAI ADAM, RZVAN FLORIN BARZIC, GEORGE OVIDIU RU iGHEORGHE DUMITRACU, Evaluarea direct a conductivitii termice pentru materiale utilizate n sisteme de stocare a cldurii prin transformri de faz (engl., rez. rom.)......................................................... 173

    GABRIEL ALEXANDRU, GHEORGHE DUMITRACU i FLORIN GABRIEL FLOREAN, Modelarea curgerii ntr-un compresor centrifug transonic. (I) Influena modelrii stratului limit al curgerii (engl., rez.rom.)............................................................................................................ 179

  • GABRIEL ALEXANDRU, GHEORGHE DUMITRACU i FLORIN GABRIEL FLOREAN, Analiza numeric a efectului Coriolis ntr-un compresor centrifugal transsonic (engl., rez. rom.)..................................... 185

    GEORGE OVIDIU RU, MIHAI ADAM, IVANCU IONEL i GHEORGHE DUMITRACU, Instalaie experimental pentru studiul transferului decldur cu schimbare de faz n termosifoane (engl., rez. rom.). 191

    GEORGE OVIDIU RU, MIHAI ADAM i GHEORGHE DUMITRACU, Investigarea experimental a limitelor de fierbere i inundare, pentru tuburi termice termosifon cu diferite diametre (engl., rez. rom.) ............... 197

    DRAGO S. CRUDU i VASILE MERTICARU, Contribuii teoretice la optimizarea dinamic a mecanismului de lucru a ncrctorului frontal(engl., rez. rom.)................... ...................................................................... 205

    DRAGO S. CRUDU i VASILE MERTICARU, Date experimentale de referin pentru proiectarea mecanismului de lucru de la ncrctorulfrontal (engl., rez. rom.) ............................................................................. 219

    CRISTIAN IOSIFESCU i SORINEL TOFAN, Studiul unui turn de rcire umed n contra-curent. (I) Studiul funcionrii (engl., rez. rom.) .............. 233

    SORINEL TOFAN i CRISTIAN IOSIFESCU, Studiul unui turn de rcire umed n contra-curent. (II) Analiza exergetic (engl., rez. rom.)................ 239

    ADRIAN I. SIMEDRU, Comparaia teoretico-experimental la funcionarea cavitaional a turbinelor hidraulice axiale de la hidrocentrala Porile de Fier (engl., rez. rom.)................................................................................... 245

    BOGDAN CCIUL, VIOREL POPA i TNASE PANAIT, Studiu privind temperatura optim a sursei calde care acioneaz un sistem prin adsorbie solar de climatizare (engl., rez. rom.) ......................................... 253

    GEORGIANA BOLAT i DANIEL SUTIMAN, Studiul termodinamic al sistemelor binare formate din toluen+alcani la temperatura de 318.15 K(engl., rez. rom.) ......................................................................................... 259

    FLORIN GABRIEL FLOREAN, IONU PORUMBEL, GABRIEL ALEXANDRU i GHEORGHE DUMITRACU, Simularea numeric i determinri experimentale ntr-un jet turbulent de gaze evacuate dintr-o turbin cu gaze (engl., rez. rom.)................................................................. 265

    FLORIN GABRIEL FLOREAN, ALEXANDRU GABRIEL i GHEORGHE DUMITRACU, Determinri experimentale i simulri numerice n curgeri turbulente izotermice (engl., rez. rom.)........................................... 271

    DANIELA TASMA, TNASE PANAIT, KRISZTINA UZUNEANU iCTLIN MOCANU, Evaluarea exergetic a gazeificrii rezidurilor din agricultur (engl., rez. rom.)........................................................................

    277

    DANIELA TASMA, TNASE PANAIT, KRISZTINA UZUNEANU iCTLIN MOCANU, Influena coeficientului de exces de aer asupra gazeificrii biomasei (engl., rez. rom.). ................................................. 285

  • OLIVIA GIUCA i IOAN NICOAR, Utilizarea planurilor de experimente pentru verificarea stabilitii dimensionale a nanocristalelor (engl., rez.rom.)............................................................................................................. 295

    MARIUS CATAN i DANIELA TARNI, Modelul virtual tridimensional al articulaiei genunchiului uman (engl., rez. rom.)..................................... 303

    RALUCA SOFRONIA, ARJANA DAVIDESCU i GEORGE SAVII,Interaciunea os-ferstru n cadrul unui simulator haptic (engl., rez.rom.)............................................................................................................. 309

    MARIAN STANCU, DANIEL DRAGOMIR-STANCIU i CONSTANTINLUCA, Instalaie de cogenerare de mic putere cu gazeificarea lemnului (engl., rez. rom.).......................................................................................... 317

  • B U L E T I N U L I N S T I T U T U L U I P O L I T E H N I C D I N I A I B U L L E T I N O F T H E P O L Y T E C H N I C I N S T I T U T E O F I A I Tomul LVIII (LXII), Fasc. 3 2012

    MACHINE CONSTRUCTION

    Pp.

    MOUSSA KARAMA (France), Behaviour of Laminated Composite Beam at the Interfaces of Layers (English, Romanian summary)............................. 1

    ISAAC NELSON (USA), CONSTANTIN CIOCNEL (USA) and HEIDI FEIGENBAUM (USA), Reorientation Curves for a Ni50Mn28.5Ga21.5Alloy (English, Romanian summary).......................................................... 19

    CIPRIAN ATNSOAEI, VIOREL GOAN and PAUL-DORU BRSNESCU, Particulate Cordierite - Zirconia Composites (English, Romanian summary) ................................................................................... 31

    RZVAN FLORIN BARZIC, ANDREEA IRINA BARZIC and DANA-ORTANSA DOROHOI, Deformation Behavior under Shear Field ofSome Hydroxypropyl Cellulose/L-Cystine Blends (English, Romanian summary) ........................................................................ 41

    IONU DUMITRACU, PAUL-DORU BRSNESCU and BOGDAN LEIOIU, Comparative Study of Cross-ply CFRP with Thermoplastic and Thermoset Matrix (English, Romanian summary)............................... 47

    IONU DUMITRACU, PAUL-DORU BRSNESCU and VIOREL GOAN, Matrix Influence on the Mechanical Properties of Unidirectional CFRTP (English, Romanian summary).............. 53

    EDUARD GHEBAN, NORINA FORNA and BOGDAN LEIOIU, SomeConsiderations on Shear Modulus Precision Determination of a Dentistry Acrylate (English, Romanian summary)..... 59

    EDUARD GHEBAN, NORINA FORNA and BOGDAN LEIOIU,Considerations on Tension Test, when Applied on a Dentistry Material(English, Romanian summary).................................................................... 67

    DAN ILINCIOIU and COSMIN MIHAI MIRIOIU, The Influence ofSimplifying Assumptions Over the Stress Distribution for HyperstaticMetallic Structures (English, Romanian summary)..... 75

    DAN ILINCIOIU and COSMIN MIHAI MIRIOIU, A Comparison Between Some Software Used for Metallic Structures Stress Studies (English, Romanian summary).................................................................................... 85

    ADRIAN LIVIU PARASCHIV, MARIUS GABRIEL SURU andLEANDRU-GHEORGHE BUJOREANU, Properties Variation, Due toNickel Content and Thermo-mechanical Processing, in Fe-Cr-Ni-Si Master Alloys Used for the Preparation of Some Fe-Base Shape Memory Alloys (English, Romanian summary)...........................

    93

    C O N T E N T S

  • MARIAN MARE, CRISTINA RACU, LILIANA BUHU and ADRIANBUHU, Mechanical Properties of Some Biodegradable Polymer MatrixComposite Materials, with Natural Yarn Fabrics Reinforcement(English, Romanian summary)................................................................ 101

    LEONID TARTAKOVSKY (Israel), VLADIMIR BAIBIKOV (Israel), MARCEL GUTMAN (Israel), DORON POPESCU (Israel), MARC VEINBLAT (Israel) and YORAM ZVIRIN (Israel), Comparison of Pollutants Emission by Urban Buses and Passenger Cars in Israel(English, Romanian summary).................................................................... 109

    VICTOR BRATU, ALEXANDRU BOROIU and ION TABACU, Researches Regarding the Improvement and the Modernization of the Public Passengers Transport in the Peripheral Area of Pitesti. (I) Study of Determining Factors for the Public Transport System (English, Romanian summary).................................................................................... 117

    CLAUDIU BUTNARU, Impact of Exhaust Gas Recirculation (EGR) on Combustion and Emissions in a HCCI Engine (English, Romanian summary)..................................................................................................... 127

    CLAUDIU BUTNARU, Influence of Engine Speed and Fuel Consumption on Exhaust Emissions (English, Romanian summary)..................................... 135

    VASILE CAUNII, Aspects Regarding the Control Strategies of Air Conditioning Compressor (English, Romanian summary).......................... 141

    COSTIN DRAGOMIR, CONSTANTIN PANA, NICULAE NEGURESCU and ALEXANDRU CERNAT, Theoretical and Experimental Investigations of the SI Engine Turbo Charging (English, Romanian summary)..................................................................................................... 151

    MARIUS ATANASIU, MIHAI MARIUS PRODAN and EMIL JUGUREANU, Comparative Analysis Between Planar Product Method and Plan Geometry Method for Scroll Compressor Mathematical Model(English, Romanian summary).................................................................... 159

    MIHAI ADAM, GEORGE OVIDIU RU and GHEORGHE DUMITRACU, Experimental Research on Thermal Energy Storage Using Phase Change Material: Eutectic Sn-Pb Alloy (English, Romanian summary). 167

    MIHAI ADAM, RZVAN FLORIN BARZIC, GEORGE OVIDIU RU and GHEORGHE DUMITRACU, Thermal Conductivity Direct Assessment of PCM Used in Heat Storage Systems (English, Romanian summary)..... 173

    GABRIEL ALEXANDRU, GHEORGHE DUMITRACU and FLORIN GABRIEL FLOREAN, Modeling the Flow Through a Transonic Centrifugal Compressor. (I) The Influence of the Wall Treatment Method(English, Romanian summary)........................................................................ 179

    GABRIEL ALEXANDRU, GHEORGHE DUMITRACU and FLORIN GABRIEL FLOREAN, Numerical Analysis of the Coriolis Effect in aTransonic Centrifugal Compressor (Englih, Romanian summary)............. 185

    GEORGE OVIDIU RU, MIHAI ADAM, IVANCU IONEL and GHEORGHE DUMITRACU, Experimental Setup for Testing the Phase Change Heat Transfers in Heat Pipes (English, Romanian summary)..................................................................................................... 191

  • GEORGE OVIDIU RU, MIHAI ADAM and GHEORGHE

    DUMITRACU, Experimental Investigation of Boiling and Flooding Limits, using Two-Phase Closed Thermosyphons with Different Diameters (English, Romanian summary)................................................... 197

    DRAGO S. CRUDU and VASILE MERTICARU, Theoretical Contributions to Dynamic Optimization of the Frontal Loader Working Mechanism (English, Romanian summary)............................................... 205

    DRAGO S. CRUDU and VASILE MERTICARU, Experimental Data Reference to Design Working Mechanism for Frontal Loader (English, Romanian summary).................................................................................... 219

    CRISTIAN IOSIFESCU and SORINEL TOFAN, Study of a Counterflow Wet Cooling Tower. (I) Simulation Model for Performance Analysis(English, Romanian summary).................................................................... 233

    SORINEL TOFAN and CRISTIAN IOSIFESCU, Study of a Counterflow Wet Cooling Tower. (II) Exergy Analysis (English, Romanian summary)........ 239

    ADRIAN I. SIMEDRU, Theoretical and Experimental Comparison of the Axial Hydraulic Turbines Working with Cavitation at Iron Gates I Hydro-Power Plant (English, Romanian summary).................................... 245

    BOGDAN CACIULA, VIOREL POPA, TANASE PANAIT, Study Concerning Optimum Heat Source Temperature for a Solar Adsorption System (English, Romanian summary)....................................................... 253

    GEORGIANA BOLAT and DANIEL SUTIMAN, Thermodinamic Study of Toluene + an Alkane at 318.15 K (English, Romanian summary).............. 259

    FLORIN GABRIEL FLOREAN, IONUT PORUMBEL, GABRIELALEXANDRU and GHEORGHE DUMITRACU, Numerical Simulation and Experimental Measurements in a Gas Turbine Turbulent Exhaust Jet (English, Romanian summary)................................................. 265

    FLORIN GABRIEL FLOREAN, ALEXANDRU GABRIEL and GHEORGHE DUMITRACU, Experimental Measurements and Numerical Simulations in Isothermal Turbulent Flows (English, Romanian summary).................................................................................... 271

    DANIELA TASMA, TNASE PANAIT, KRISZTINA UZUNEANU andCTLIN MOCANU, Exergetic Evaluation of Agricultural Residues Gasification (English, Romanian summary)................................................ 277

    DANIELA TASMA , TNASE PANAIT, KRISZTINA UZUNEANU and CTLIN MOCANU, Influence of Excess Air Ratio on Biomass Gasification (English, Romanian summary)................................................ 285

    OLIVIA GIUCA and IOAN NICOAR, Experimental Plans Used for Verification of Dimensional Stability Nanocrystals (English, Romanian summary)..................................................................................................... 295

    MARIUS CATAN and DANIELA TARNI, The Three-Dimensional Virtual Model of the Human Knee Joint (English, Romanian summary)..................................................................................................... 303

    RALUCA SOFRONIA, ARJANA DAVIDESCU and GEORGE SAVII,Physics-Based Bone Sawing Interaction for a Haptic Simulator (English, Romanian summary)....................................................................................

    309

  • MARIAN STANCU, DANIEL DRAGOMIR-STANCIU and CONSTANTIN

    LUCA, Small Cogeneration System with Wood Gasifier (Englih, Romanian summary)....................................................................................

    317

  • BULETINUL INSTITUTULUI POLITEHNIC DIN IAI Publicat de

    Universitatea Tehnic Gheorghe Asachi din Iai, Tomul LVIII (LXII), Fasc. 3, 2012

    Secia CONSTRUCII DE MAINI

    BEHAVIOUR OF LAMINATED COMPOSITE BEAM AT THE INTERFACES OF LAYERS

    BY

    MOUSSA KARAMA

    Universit de Toulouse, France

    Received: April 2012 Accepted for publication: June 2012

    Abstract. One of the current problems connected with multiplayer

    composite structures concerns the analysis of the distribution of the stresses around peculiarities (free edge and loaded edge) and at the interfaces of each layer. This work presents a new shear stress function in the form of the exponential function, to predict the mechanical behaviour of multi-layered laminated composite structures. As a case study, the mechanical behaviour of laminated composite beam (90/0/0/90) is examined. The results are compared with the model Sinus and 2D finite element method studied. Results show that this new model is more precise than older ones as compared to the results by the finite element analysis (Abaqus). To introduce continuity on the interfaces of each layer, the kinematics defined by Ossadzow is used with new exponential model. The equilibrium equations and natural boundary conditions are derived by the principle of virtual power.

    Key words: composite materials, shear function, laminated structure, interface, refined model, finite element.

    1. Introduction

    One of the major challenges in computational structural mechanics is the development of the advanced models and numerical techniques in order to provide efficient tools exhibiting good interior and edge solutions. In this paper we are introducing an exponential function as a shear stress function; the

    e-mail: [email protected]

  • 2 Moussa Karama

    exponential functions are found to be very much richer than trigonometric sine and cosine functions in their development series. According to the definition of the transverse shear stress function, the existing laminated composite beam is divided into two broad categories; firstly, the global approximation models and secondly the discrete layer approximation models. The equivalent single-layer laminate theories are those in which a heterogeneous laminated plate is treated as a statically equivalent, single layer having a complex constitutive behaviour, reducing the 3-D continuum problem to 2-D problem.

    The equivalent single layer models are:

    i) the Kirchoff (1850) Love (1934) theory (or classical theory) in which deformation due to transverse shear is neglected, implies that the normal to the mid plane remains straight and normal at mid-surface after deformation. This theory can be used for thin beams.

    ii) the Reissner (1945)-Mindlin (1951) theory (or first order theory). That the first order deformation theory extends the kinematics of the classical laminated plate theory by including a gross transverse shear deformation in its kinematic assumption, the transverse shear strain remain constant with respect to the thickness coordinate, implies that the normal to the mid plane remains straight but not normal to mid-surface after deformation due to shear effect. The first order theory requires shear correction factors, which are difficult to determine for arbitrary laminated composite plate.

    iii) and the higher order models are based on the hypothesis of non-linear stress variation through thickness (Reddy, 1984), (Touratier, 1991). These models are able to represent the section warping in the deformed configuration.

    These theories do not satisfy the continuity conditions of transverse shear

    stress at layer interfaces. Although the discrete layer approximation theories are accurate, but they are rather complex in solving problems because the order of their governing equations depends on the number of layers.

    Di Sciuva (1987, 1998) and then Touratier (1991, 1992) proposed simplified discrete layer model with only five variational unknowns (two membrane displacements, a transverse displacement and two rotations), allowing the section to be represented wrapping in the deformed configuration for the Touratier (1992) model. Nevertheless, in these two cases the compatibility conditions, both layer interfaces and the boundaries, cannot be satisfied. From Touratiers work, Beakou (1991) and Idlbi (1995) proposed, respectively, shell and plate models which satisfy both the stress continuity at interfaces and the zero stress conditions at the boundaries.

    Finally, He (1994) introduced the Heaviside step function which enables automatic satisfaction of the displacement continuity at interfaces between different layers. The new discrete layer model comes from the work of Di Sciuva (1993), He (1994) and Ossadzow et al. (1995), the displacement field is

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 3

    (1)

    01 1 3 1 1 3 ,1 1 1 3 1 1

    2

    3 1 1

    ( , , ) ( , ) ( , ) ( ) ( , ),0,

    ( , ) ( , ),

    U x x t u x t x w x t h x x tU

    U x t w x t

    = + = = with transverse shear function

    1

    ( ) ( ) ( )3 31 3 3 1 3 3 3 3

    1

    ( )( ) ( ) ( ) ( )2 2

    Nm m

    m

    x f xh x g x x x H x x

    =

    m = + + + ,

    where, H(x3 x3(m)), the Heaviside Step function is defined as:

    ( )3 3( )

    3 3 ( )3 3

    1 for ,( )

    0 for ,

    mm

    m

    x xH x x

    x x

    = >

    where is the diameter of the and the closed domain && is set such that { }edge /2/ .z h= = = && From the beginning our objective was so clear, to find out a transverse shear stress function f(z), which gives the mechanical behaviour of the composite laminated structures as much close as possible to the exact 3D solution (Pagano, 1970) or finite element analysis in 2D (stress, strain plane), and better representation of the transverse shear stress in the thickness of the laminated structure. Since different higher order polynomial and trigonometric function already has been tried which are as follow:

  • 4 Moussa Karama

    Ambartsumain (1958), where

    2 2

    ( ) ,2 4 3z h zf z =

    Kaczkowski & Panc (1975) and Reissner (1975) where

    2

    25 4( ) 1 ,4 3

    zf z zh

    =

    Levinson (1980), Muthy (1981) and Reddy (1984) where

    2

    24( ) 1 ,3

    zf z zh

    =

    and finally Touratier (1991), where

    ( ) sin ,h zf z h

    =

    So, we took a start with an exponential function, because an exponential function has all even and odd power in its expansion unlike Sine function, which have only odd power. So an exponential function is much richer than a Sine function. If we take a look on the expansions of different transverse shear stress functions as

    Reddy (1984), where

    2 3

    2 24( ) 1 1.33 ,3

    z zf z z zh h

    = = (3)

    Touratier (1991), where

    3 5 7

    2 4 6( ) sin 1.645 0.812 0.191 0.0261h z z z zf z z

    h h h h= = + +9

    8zh

    , (4)

    Present model

    2

    3 5 72( / )

    2 4 6( ) 2 2 1.333 0.666 .z h z z z zf z ze z

    h h h h= = + +

    9

    8 (5)

    As it is clear from expansions of the transverse shear stress functions, that the coefficient of successive terms in Sine functions are decreasing more rapidly than present exponential function which are the main responsible to gives different mechanical behaviour of laminated structures. For the transverse shear stress behaviour, it is very important that the first derivative of the transverse shear stress function must give a parabolic response in the thickness direction of the laminate and satisfy the boundary conditions.

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 5

    2. Governing Equations

    From the virtual power principle, the equations of motion and the natural boundary conditions can be obtained. The calculations are made in small perturbations. According to the principle of virtual power

    (6) * * *( ) ( ) ( ) .a i eP P P= +

    But the virtual power of the acceleration quantities is

    * *( ) d ;T

    aP U U

    = && (7)

    we suppose

    (8)

    /2 /2

    3 ' 3/2 /2

    /2 /22

    ' 3 3 1 3 3/2 /2

    /2 /221 3 3 ' 3 1 3 3

    /2 /2

    d , d ,

    d , ( )d ,

    ( )d , ( )d .

    h h

    w uwh h

    h h

    w uh h

    h h

    wh h

    I x I x x

    I x x I h x x

    I h x x I x h x x

    = =

    = =

    = =

    3

    So, the Eq. (6) becomes (see Appendix A for the mathematical detail)

    ( )* ( ) * ( ) * ( ) * ( )( ) 1 1 10

    dL

    u o w waP u w x

    = + + + *w , (9) with

    ( )1 ' ,1 1

    ( )' 1,1 ' ,11 ' 1,1

    ( )1 ' ,1 1

    ( )' 1 ' ,1 ' 1

    ,,

    ,

    .

    u ow uw u

    w ouw w w w

    ou w

    w ouw w w

    I u I w II u I w I w I

    I u I w I

    I u I w I

    = + + = + = + + = + +

    &&&& &&&&&& && &&

    &&&& &&&&&& &&

    Now the virtual power of internal work is

    *

    *( ) : d ,

    T

    iP D

    = (10) but

    11 12 13 11 12 13

    21 22 23 21 22 23

    31 32 33 31 32 33

    , ,D D D

    D D D D D D D

    = =

  • 6 Moussa Karama

    so, in two dimension 11 11 13 13: 2D D D = + .

    *.

    (11) Resulting stresses N , M and P are defined as

    (12)

    /2 /2

    11 11 3 11 3 11 3/2 /2

    /2 /2

    11 1 3 11 3 13 1,3 3 13 3/2 /2

    d , d ,

    ( ) d , ( ) d ,

    h h

    h h

    h h

    h h

    N x M x x

    P h x x P h x x

    = =

    = =

    so Eq. (10) becomes (see Appendix B for the mathematical detail), * * * * * * *

    ( ) 11,1 1 11,11 11,1 13 1 1 11 1 11,1 11 ,1 11 10

    ( ( ) )dL

    o oiP N u M w P P x N u M w M w P = + + + (13)

    Now the virtual power of external loading is

    (14) * * *( )

    dT TeP U f U F

    = + d

    2

    but 1 1

    * * *1 3 2

    3 3

    0 , , ,Tf F

    U U U f f F Ff F

    = = =

    with * * * *1 1 3 ,1 1 3 1*2

    * *3

    ( ) ,

    0,

    .

    oU u x w h x

    U

    U w

    = +==

    We define

    /2 /2

    33/2 /2

    /2 /2

    3 3 3 3/2 /2

    /2 /2

    1 3 3 1 3 3/2 /2

    d ,d ,

    d , d ,

    ( ) d , ( ) d ,

    h h

    i i iih h

    h h

    ii ih h

    h h

    ii iih h

    F xn f x N

    m x f x M x F xi

    p h x f x P h x F x

    = =

    = =

    = =

    (15)

    so Eq. (14) becomes (see Appendix C for the mathematical detail),

    * * * * * * *1 11 3 1,1 1 3 1( ) 1 1 1 1 ,1 11

    0

    ( ( ) )d ( )L

    o oeP n u n m w p x N u N m w M w P

    * = + + + + + (16)

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 7

    Now, by the Eqs. (5), (8), (13) and (16), governing equations and natural boundary conditions for , *1

    **1 ,, wuo

    ( )111,1

    ( )3 1,111,11

    ( )11,1 13 1

    ,

    ( )

    .

    u

    w

    N n

    M n m

    P P p

    = + = + + = +

    , (17)

    And natural boundary conditions for: : *1,*1

    **o1 w,,w,u

    111( )

    3 111,1

    111

    111

    0 ,

    ( )

    0 ,

    0 .

    w

    N N

    ,M N m

    P P

    M M

    = + = + = +=

    (18)

    The three-dimensional orthotropic constitutive law is

    (19)

    11 12 1311 11

    12 22 2322 22

    13 23 3333 33

    4423 23

    5513 13

    6612 12

    0 0 00 0 00 0 0

    .0 0 0 0 0 20 0 0 0 0 20 0 0 0 0 2

    C C C C C C C C C

    C C

    C

    =

    The dimension x2 is supposed unitary, and the effects of the 33 are neglected, so orthotropic law (19), becomes

    , (20) '

    11 1111

    13 1355

    020

    C C

    = with

    *

    11 1,1 1,1 3 ,11 1 1,1

    31 1,3 12

    ' 11 33 1311

    33

    ,

    2 ,

    .

    oU u x w h

    h

    C C CCC

    = = +=

    =

    Now, the generalized constitutive law

  • 8 Moussa Karama

    *11 1,111 11

    11 ,1111 11

    11 1,1

    13 1

    00 .0

    0 0 0

    oN uA B KM wB D TP K T SP Y

    =

    %%%% %

    %

    (21)

    So, the governing Eqs. (17) become

    ( ) *111 1,11 11 ,111 1,11

    ( ) *3 1,111 1,111 11 ,1111 1,111

    ( ) *1,11 ,111 1,11 1 1

    ,

    ,

    .

    u o

    w o

    o

    A u B w K n

    B u D w T n m

    Ku Tw S Y p

    = + + = + + + = + +

    %%

    %% % % (22)

    And the natural boundary conditions (18) become

    *11 1,1 11 ,11 1,1 1

    ( ) *11 1,11 11 ,111 1,11 3 1

    *11,1 ,11 1,1

    *11 1,1 11 ,11 1,1 1

    0 ,

    ,

    0 ,

    0 .

    o

    w o

    o

    o

    A u B w K N

    B u D w T N m

    Ku Tw S P

    B u D w T M

    = + = + + = + += +

    %

    %

    %% %

    %

    (23)

    Continuity coefficients : To find out the value of the continuity coefficients, the conditions of the

    continuity of the transverse shear stress between each interfaces of the layers were used (Fig. 1)

    . (24) ( ) ( ) ( 1) ( )13 3 3 13 3 3( ) (m m m x x x x+= = = )m

    1)

    Interface of layer (1) and layer (2)

    (1) (1) (2) (13 3 3 13 3 3( ) ( ) x x x x= = =

    (1)1 (1) (1) ( 2 ) (3) 355 1 3 1 1 1

    (1)2 (1) (1) ( 2 ) (3) (1)355 1 3 1 1 1 1

    '( )1( ) '( ) ( )2 2

    '( )1( ) '( ) ( ) .2 2

    f xQ x g x

    f xQ x g x

    + + + + = = + + + +

    +

    .

    (25)

    Interface of layer (2) and layer (3)

    (2) (2) (3) (2)13 3 3 13 3 3( ) ( ) x x x x= = =

    Since, Q55 of the second and third layer are equal (Fig. 1), so,

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 9

    ( 2 )2 ( 2 ) (1) ( 2 ) (3) (1)355 1 3 1 1 1 1

    ( 2 )3 ( 2 ) (1) ( 2 ) (3) (1)355 1 3 1 1 1 1 1

    '( )1( ) '( ) ( )2 2

    '( )1( ) '( ) ( ) .2 2

    f xQ x g x

    f xQ x g x

    + + + + + = = + + + + +

    ( 2 )+

    (26)

    Now by Eqs. (25) and (26),

    (27) (1) (1) (2)1 1 1

    (2)1

    ,

    0.

    = +=

    This shows that if the mechanical characteristics of the two consecutive layers are the same (Fig. 1), the coefficient of the continuity will be zero ((2) = 0). Interface of layer (3) and layer (4)

    , (3) (3) (4) (3)13 3 3 13 3 3( ) ( ) x x x x= = =

    (3)3 (3) (1) (2 ) (3) (1) ( 2)355 1 3 1 1 1 1 1

    (3)4 (3) (1) ( 2) (3) (1) (2 ) (3)355 1 3 1 1 1 1 1 1

    '( )1( ) '( ) ( )2 2

    '( )1( ) '( ) ( ) ,2 2

    f xQ x g x

    f xQ x g x

    + + + + + + = = + + + + + + +

    (28)

    we have,

    (1) (3)3 3

    (1) (3)3 3

    '( / 4) '( / 4),

    '( / 4) '( / 4).

    f x h f x h

    g x h g x h

    = = == = =

    So, by Eqs (26), (27) and (28), gives

    (3)

    1 (3 ) (1) ( 2 ) (3 ) 355 1 3 1 1 1

    (3)4 (3 ) (1) ( 2 ) (3 ) (1) (3 )355 1 3 1 1 1 1 1

    '( )1( ) '( ) ( )2 2

    '( )1( ) '( ) ( ) ,2 2

    f xQ x g x

    f xQ x g x

    + + + + = = + + + + +

    +

    (29) (1) (3)

    1 1

    (1) (3)1 1

    0

    = +=

    So, by Eq (27) and (29), Eq (25) becomes

  • 10 Moussa Karama

    (30) 1 (1) 2 (1) (1)55 3 55 3 1( '( )) ( '( ) ),Q g x Q g x = +

    1 2 (1) 2 1 (1)

    (1) (3)55 55 3 55 55 31 12 2

    55 55

    ( ) '( ) ( ) '( and .Q Q g x Q Q g x Q Q

    = = ) (31)

    3. Finite Element Analysis

    Since no exact 3D solution exists for the considered case study, so ABAQUS (finite element analysis software) is used to show the efficiency of the present model. In this paper finite element results are taken as a reference for the comparison of different models of laminated composite structures, done by Abou Harb (1998). The 3D approximation of the behaviour is carried out by element type CPS8 (quadrilateral element of eight nodes, 16 dof per element). To validate the finite element results, firstly it is necessary to find out the convergence of laminate meshing. So, for the given problem, in static and dynamic, the convergence found to be at 1680 elements included 24 element in thickness.

    4. Some Evaluations of the Present Model

    The static bending analysis is studied, so the virtual power of acceleration quantities is cancelled. Three different bending analyses have been developed for three different specific boundary conditions. For the simply supported conditions, the unknown variables are deduced directly by the equation of motions. For clamped conditions, kinematical boundary conditions are used and, finally, in a free edge case, natural boundary conditions are employed. The beam studied has a length of L = 6.35 m, a unitary width, and a thickness h = =2.794 m in the thick case and h = 0.2794 m in the thin case. The beam possesses four layers of the same thickness at 90/0/0/90. The material used for the four layers is boron epoxy. The mechanical properties of the 0 layer are as follows (Pagano, 1970): E11 = 241.5 GPa, E22 = E33 = 18.89 GPa, G23 = 3.45 GPa,

    G12 = G13 = 5.18 GPa, 23 = 0.25, 12 = 13 = 0.24, and the density, = 2015 kg/m3. The continuity coefficients from the Eqs. (27), (29) and (31)

    1(1) = - 1(3) = 0.2210501411, 1(2) = 0.

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 11

    Fig. 1 Description of the beam.

    Problem 1: bending of a simply supported beam under distributed

    sinusoidal load.

    The surface and volume force components are cancelled except

    13 3 3

    0

    d sin . h

    oxn f x q qL

    = = = For the simply supported boundary conditions, the Levy solution is used, define as

    1 11 1cos , sin , coso

    o o ox x xu u w wL L

    = = = 1

    L. (32)

    Now the governing Eqs (22), with P(a)* = 0 , becomes

    *11 1,11 11 ,111 1,11

    * 111 1,111 11 ,1111 1,111

    *1,11 ,111 1,11 1

    0 ,

    0 s

    0 .

    o

    oo

    o

    A u B w KxB u D w T qL

    Ku Tw S Y

    = + = + +

    = +

    %

    %

    %% % %

    in , (33)

    Now, by the Levy solution, the governing equations become:

    2 3 211 1 11 1 1

    3 4 311 1 11 1 1 1

    2 3 21 1 1 1

    0 cos cos cos ,

    0 sin sin sin ,

    0 cos cos cos cos with,

    o o

    o o o o

    o o o o

    A u x B w x K x

    B u x D w x T x q xK u x T w x S x Y x L

    = + = + += + =

    %%

    %% % %

    and then in matrix form

  • 12 Moussa Karama

    = (34) 2 3 2

    11 113 4 3

    11 112 3 2

    0,

    0

    o

    o o

    o

    A B K u B D T w q

    K T S Y

    %%

    %% % %

    and also, the displacement (1), becomes

    ( )1 1 3 3 1 3 1

    2

    3 1

    ( , ) ( ) cos( ),

    0,

    sin( ),

    o o o

    o

    U x x u x w h x x

    U

    U w x

    = +==

    (35)

    and now by Eq. (20), stresses expression

    (36) '11 1 3 11 3 1 1( , ) ( )sin( ),o o o x x C u x w h x= +

    and,

    13 1 3 55 1,3 1( , ) cos( ),o x x C h x= (37)

    and integration of the equilibrium equation 13,1 33,3 0 + = , enables us to calculate the analytical value of 33

    33 55 1 3 1( ) sin( ).oC h x x = (38)

    The numerical results obtained (qo = -106 Pa) using the present model are compared with those obtained by the finite element analysis7 and the Sine7 model by Touratier (Table 1).

    Table 1 Bending of the simply supported thick beam under distributed sinusoidal load

    Model U3 (L/2)

    m

    U1 (0, h/2)

    m

    13 (L/4, 0) (Interface)

    Pa

    11 (L/2, -h/4+) (Interface)

    Pa

    33 (L/2, h/2)

    Pa Present -6.370110-4 2.119610-4 -940098.0 8112840.0 -1039990.0

    Error (%) 4.4 8.3 6.6 3.5 3.9 Sine7 -6.279410-4 2.018010-4 -896865.0 8158932.0 -1047274.0

    Error (%) 2.9 12.7 10.8 4.1 4.6 Abaqus7 -6.100610-4 2.312510-4 -1006000.0 7835200.0 -1000900.0

    For this problem, the present model present a better mechanical

    behaviour better than Sine model compared to the finite element analysis results except the transverse deflection (U3). Percentage error reduction is more significant in case of transverse shear stress (13) at interfaces of layers. The efficiency of this model is shown for (Figs. 2, 3 and 4), different stresses and

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 13

    displacement plotted according to the length and thickness of the beam, showing that the present model at every point on the beam, is closer to the finite element results then to those of the Sine model. Here we can see also the continuity of displacement and transverse shear stress between layer interfaces of the present model.

    Fig. 2 Variation of the stress 11 along the direction x1 for x3 = -h/2 for

    Problem 1: Present (-*-), Sine7(-), Abaqus7(- - -).

    Fig. 3 Variation of the transverse shear 13 through the thickness for x3 = 0 (Interface).

    for Problem 1, Present (-*-), Sine7(-), Abaqus7(- - -).

    Fig. 4 - Variation of the displacement U1 through the thickness for x1 = L/4 for

    Problem 1, Present (-*-), Sine7(-), Abaqus7(- - -).

  • 14 Moussa Karama

    *

    d

    5. Conclusions

    1. Shear stress continuity of displacement and transverse shear stresses at interfaces of the layers and the boundary conditions for a laminated composite are exactly satisfied by this present new multi-layered structure exponential with the help of the Heaviside step function (Figs. 2-10). 2. For the new proposed model the results are compared with the existing model (like Sine (1998)) model by Touratier (1991) and by the finite element method by Abaqus (1998). Results show that the new proposed exponential model present a better approximation than the Sine (1998) model as compared to the finite element analysis, except for some results, (Table 1), especially results are very much favourable on interface of the layers. 3. The new model is also simple in so far as any correction factor is used in opposition to the higher order models. In the case of static analysis, (Figs. 2-4) presents the numerical results for the bending deformation under different types of loading and boundary conditions on a thick beam, showing that the present model is always trying to approaches to the finite element analysis by Abaqus (1998). As a whole we can conclude the present exponential model is more accurate than other existing analytical models for multi-layered structures compared to finite element analysis.

    Appendix A

    (Virtual Power of the Acceleration Quantities) We have,

    1 1 3 ,1 1 1 3

    * * * * *1 1 3 ,1 1 1 3

    , ,and

    , .

    o

    o

    U u x w h U w

    U u x w h U w

    = + =

    = + =

    && &&&& && &&

    So Eq. (6) becomes, * * *

    ( ) 1 1 3 3( )aP U U U U

    = + && && . By the integration by parts

    * * * * *( ) 1 1 3 3 1,1 1 3 1 1 3 1( ) ( ) d

    oaP u u u x u w h x u x w u

    = + + + && && && && && d

    and, now

    ( ) ( )( ) ( )

    * *( ) 1 3 ,1 1 3 1 1 3 1,1 3 ,11 1 3 1,1

    * *1 3 1 3 ,1 1 3 1 1 3 1 3 ,1 1 3 1

    ( ) ( ( ) )

    ( ) ( ) d ( ) d ,

    o o oa

    o o

    P u x w h x u w x u x w h x w

    h x u x w h x x u x w h x w

    = + + + ++ + +

    && && && && &&

    && && && &&

    * +

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 15

    /2 /2 /2* *

    ( ) 3 1 3 3 ,1 1 3 3 1 10 /2 /2 /2

    /2 /2 /2 /22 *

    3 3 1,1 3 3 ,11 3 1 3 3 1,1/2 /2 /2 /2

    /

    / 2

    d ) ( d ) ( ( )d )

    d ) ( ) ( d ) ( ( )d )

    (

    L h h ho o

    ah h h

    h h h ho

    h h h h

    h

    h

    P x u x x w h x x u

    x w dx u x x w x h x x w

    = + + + + + +

    +

    && &&

    && && &&

    2 /2 /22 *

    1 3 3 1 3 1 3 3 ,1 1 3 3 1 1/2 /2

    /2 /2 /22 *

    3 3 1 3 3 ,1 3 1 3 3 1/2 /2 /2

    ( )d ) ( ( )d ) ( ( )d ) d

    ( d ) ( d ) ( ( )d )

    h ho

    h h

    h h ho

    h h h

    h x x u x h x x w h x x

    x x u x x w x h x x w

    + + + + +

    && &&

    && &&

    +

    +

    and now by relations (7),

    ( )* ( ) * ( ) * ( ) * ( )( ) 1 1 10

    dL

    u o w waP u w x

    = + + + *w

    Appendix B

    (Virtual Power of the Internal Work)

    By relation (11), virtual power of the internal work (10) become

    ( )( )

    * * * * *( ) 1,1 3 ,11 1 3 1,1 11 1,3 3 1 13

    * * * * *( ) 11 1,1 3 ,11 11 1 3 11 1,1 13 1,3 3 1

    1( ) 2 ( ) d ,2

    ( ) ( ) d .

    oi

    oi

    P u x w h x h x

    P u x w h x h x

    = + + = + +

    Now, by integrating each term by parts:

    * * * * *( ) 11,1 1 3 11,11 1 3 11,1 1 1,3 3 13 1

    * * * *11 1 3 11 ,1 3 11,1 1 3 11 1

    ( ) ( ) d

    ( ) d ,

    oi

    o

    P u x w h x h x

    u x w x w h x

    = + + +

    *

    /2 /2 /2* * *

    ( ) 11,1 3 1 3 11,11 3 1 3 11,1 3 10 /2 /2 /2

    /2 /2 /2* *

    1,3 3 13 3 1 1 11 3 1 3 11/2 /2 /2

    d d ( ) d

    ( ) d d - d d

    L h h ho

    ih h h

    h h ho

    h h h

    P x u x x w h x x

    h x x x x u x x

    = + + + +

    *3 ,1/2 /2

    * *3 11,1 3 1 3 11 3 1

    /2 /2

    d ( ) d .h h

    h h

    w

    x x w h x x

  • 16 Moussa Karama

    *.

    Now by relations (12),

    * * * * * * *( ) 11,1 1 11,11 11,1 13 1 1 11 1 11,1 11 ,1 11 1

    0

    ( ( ) )dL

    o oiP N u M w P P x N u M w M w P = + + +

    Appendix C

    (Virtual power of the External Loading) By relations (15), virtual power of external loading (14), becomes:

    1 1* * * * *

    ( ) 1 3 2 1 3 2

    3 3

    0 d 0e

    f FP U U f U U F

    f F d

    = +

    * ,

    ,

    * * * * *

    ( ) 1 1 3 3 1 1 3 3

    * * * * *( ) 1 1 1 3 ,1 1 3 1 1 3

    * * * *1 1 1 3 ,1 1 3 1 1 3

    / 2 / 2 /2* *

    ( ) 1 3 1 3 3 3 1,1 3/ 2 / 2 /2

    ( )d ( )d ,

    ( ( ) )d

    ( ( ) )d ,

    d d

    e

    oe

    o

    h h ho

    eh h h

    P f U f U F U F U

    P f u f x w h x f f w

    F u F x w h x F F w

    P f x u f dx x f x

    = + + +

    = + + +

    + + +

    = + +

    / 2* *1 3 1 3 1 10 /2

    /2 /2 / 2 / 2 / 2* * *

    1 3 1 3 3 3 1 3 1 3 1 3 1 3 1 3 ,1/2 /2 / 2 / 2 / 2

    ( ) d

    d d d ( ) d d

    L h

    h

    h h h h ho

    h h h h h

    w h x f dx x

    F x u F x x f x w h x F x x F x w

    + + + + +

    and now by relation (15),

    * * * * * * *1 11 3 1,1 1 3 1( ) 1 1 1 1 ,1 11

    0

    ( ( ) )d ( )L

    o oeP n u n m w p x N u N m w M w P

    * = + + + + + .

    REFERENCES

    Ambartsumian S.A., On Theory of Bending Plates. Izv. Otd. Tech. Nauk., AN SSSR., 5, 69-77 (1958).

    Beakou A., Homognisation et modlisation des coques composites multicouches. Thesis ENSAM, Paris, 1991.

    Di Sciuva M., A General Quadrilateral Multi-layered Plate Element with Continuous Inter-laminar Stresses. Computers and Structures, 47(1), 91-105 (1993).

    Di Sciuva, M., An Improved Shear Deformation Theory for Moderately Thick Multi-layered Anisotropic Shells and Plates. J. Appl. Mech., ASME, 54, 589-596 (1987).

    Gachon H., Sur le flambage des plaques: modle de calcul, modles exprimentaux. Construction Mtallique, 4, 23-52 (1980).

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 17 He L.H., A Linear Theory of Laminated Shells Accounting for Continuity of

    Displacements and Transverse Shear Stresses at Layer Interface. Int. J. Solids Structures, 31(5), 613-627 (1994).

    Idlbi A., Comparaison de thories de plaque et estimation de la qualit des solution dans la zone bord. Thesis, ENSAM, Paris, 1995.

    Kaczkowski Z., Plates. Statistical Calculations. Arkady, Warsaw, 1968. Karama M., Abou H. et al., Bending, Buckling and Free Vibration of Laminated

    Composite with Transverse Shear Stress Continuity Model. Composite Part B, 29B, 223-234 (1998).

    Karama M., Touratier M. et al., An Evaluation of the Edge Solution for a Higher-order Laminated Plate Theory. Composite Structures, 25, 495-502 (1993).

    Kirchhoff G.J., Uber das Gleichgewicht und die Bewegung einer elastischen Schreitbe. Reine Angew. Math, 40, 51-58 (1850).

    Levinson M., An Accurate Simple Theory of the Statics and Dynamics of Elastic Plates. Mech. Res. Common., 7, 343-350 (1980).

    Love A.E.H., A Treatise on the Mathematical Theory of Elasticity. 4th Ed., Cambridge University Press, 1934.

    Mindlin R.D., Influence of Rotary Inertia and Shear on Flexural Motions of Isotropic Elastic Plates. J. Appl. Mech., ASME, 18, 31-38 (1951).

    Murthy M.V.V., An Improved Transverse Shear Deformation Theory for Laminated Anisotropic Plates. NASA Technical Paper, 1981.

    Ossadzow C., Muller P. et al., Une thorie gnrale des coques composites multi-couches. 2ime Colloque National en Calcul des Structures, 1, Hermes, 1995.

    Pagano N. J., Exact Solution for Rectangular Bi-directional Composites and Sandwich Plates. J. Composite Materials, 4, 20-34 (1970).

    Palardy R.F., Palazotto A.N., Buckling and Vibration of the Composite Plates Using the Levy Method. Composite Structures, 14, 61-85 (1990).

    Panc V., Theories of Elastic Plates. Academia, Prague, 1975. Reddy J.N., A Simple High-order Theory of Laminated Composite Plate. J. App. Mech.,

    51, 745-752 (1984). Reissner E., Reflection on the Theory of Elastic Plates. J. Appl. Mech., 38, 1453-1464

    (1945). Reissner E., On Transverse Bending of Plates, Including the effects of Transverse Shear

    Deformation. Int. J. Solid Structure, 25, 495-502 (1975). Touratier M., An Efficient Standard Plate Theory. Int. J. Eng. Sci., 29(8), 901-916

    (1991). Touratier M., A Generalization of Shear Deformation Theories for Axisymmetric Multi-

    layered Shells. Int. J. Solids Structures, 29(11), 1379-139 (1992). Widera G.E.O., Logan D.L., Refined Theories for Non-homogeneous Aniso-tropic

    Cylindrical Shells. J. Eng. Mech. Division, EM6, 1053-1090 (1980).

    COMPORTAREA BARELOR COMPOZITE LAMINATE LA INTERFEELE DINTRE STRATURI

    (Rezumat)

    Una din problemele actuale legate de structurile compozite multi-strat se refer la analiza distribuiei tensiunilor n zonele cu particulariti geometrice i la interfeele

  • 18 Moussa Karama

    dintre straturi. Pentru a prognoza comportamentul structurilor compozite multistrat, n cadrul acestei lucrri am introdus o funcie exponenial determinat n raport cu tensiunea de forfecare, avnd o acuratee mai mare fa de funciile trigonometrice sinus i cosinus, relativ la dezvoltarea n serii. Ca studiu de caz se prezint comportamentul mecanic al barei compozite laminate (900/00/00/900). Rezultatele sunt comparate cu modelul Sinus i analiza bidimensional cu elemente finite. Datele arat c noul model propus n cadrul acestei lucrri furnizeaz rezultate mai bune dect cele anterioare. De asemenea, pentru definirea strii de tensiuni n compozitele multistrat, noul model propus este mai simplu i mai precis dect vechile modele existente.

  • BULETINUL INSTITUTULUI POLITEHNIC DIN IAI Publicat de

    Universitatea Tehnic Gheorghe Asachi din Iai, Tomul LVIII (LXII), Fasc. 3, 2012

    Secia CONSTRUCII DE MAINI

    REORIENTATION CURVES FOR A Ni50Mn28.5Ga21.5 ALLOY

    BY

    ISAAC NELSON, CONSTANTIN CIOCNEL and HEIDI FEIGENBAUM

    Northern Arizona University, Department of Mechanical Engineering

    Received: April 2012 Accepted for publication: June 2012

    Abstract. This paper presents experimental results for variant reorientation curves specific to a Ni50Mn28.5Ga21.5 alloy. Reorientation curves show the stress and magnetic field values when reorientation begins and ends for various load conditions. The curves in this work have been generated based on material response under three loading conditions: constant stress variable field, constant field variable stress, and variable stress variable field. Reorientation curves can give insight into the material behaviour and are key features of phenomenological models for MSMAs. Previously, variant reorientation curves have been generated only for the constant field variable stress loading case, and models have been limited to predicting either constant field - variable stress or constant stress variable field conditions, but not both. Thus, to this point, it has not been clear if it is possible to develop one model that can predict the magneto-mechanical behaviour of MSMAs subject to any possible stress field loading conditions. The experimental results in this work suggest that a set of reorientation curves covering the whole 2D magneto-mechanical loading spectrum is achievable, which implies that the magneto-mechanical behaviour of MSMAs can indeed be captured with a single model. Accordingly, the results of this work will be useful in developing such a model.

    Key words: NiMnGa alloy, variant reorientation, reorientation curves.

    1. Introduction

    NiMnGa is a relatively new magnetic shape memory alloy that exhibits the shape memory effect in the presence of a magnetic field. The shape memory effect is facilitated by the microstructure of the material that consists of three

    Corresponding author: e-mail: [email protected]

  • 20 Issac Nelson, Constantin Ciocnel and Heidi Feigenbaum

    martensite variants, as shown in Fig. 1. The tetragonal martensite variants are characterized by a magnetic easy axis that is aligned with the short side (side c in Fig. 1) of the unit cell.

    Upon the application of a magnetic field, the variants magnetization easy axis tends to align in the direction of the applied field, causingup to 10% macroscopic reorientation strain (Marioni et al., 2003). The magnitude of thereorientation strain is contingentupon the chemistry of the alloy, the materials training, the applied magnetic field and the compressive stress that is experienced by the material; a compressive stress as small as 5MPa (Karaca et al., 2005) can prevent variant reorientation under any magnitude magnetic field.

    From an applications point of view, this material is suitable for actuation, sensing and power harvesting applications, at a minimum. In all of these applications the stress is compressive and applied axially, while the magnetic field is applied perpendicular to the stress, in the transverse direction. For actuation applications, a MSMA element should be subject to a constant axial compressive stress and a variable transverse magnetic field. During this type of loading, the variants will reorient to align with the magnetic field, thus elongating the MSMA element and beginning the actuation process. The limiting factor for actuation applications is the blocking stress specific to the material. For sensing and power harvesting applications, a MSMA element should be subject to constant transverse magnetic field and variable axial compressive stress. During this type of loading, the variants will reorient to align with the compressive stress, and as they do so the direction of the internal magnetization changes, which can be sensed or harvested using a pick-up coil.

    Fig 1. The three martensitic variants with magnetic easy axis parallel to the short axis (adopted from Kiefer and Lagoudas, 2005).

    2

    1

    2

    1

    For a robust design of a MSMA based device, one has to be able to predict the magneto-mechanical response of the material to various loading conditions. Furthermore, new applications of MSMAs may be discovered through a better understanding and more comprehensive modelling of the magneto-mechanical behaviour of MSMAs.

    Reorientation curves are one way to get a better understanding of the magneto-mechanical behaviour of MSMAs, and reorientation functions are key features of phenomenological models of MSMAs.

    To illustrate what the reorientation curves are, consider the material response to a constant field-variable load condition, as shown in Fig. 2. In this case, at the beginning of the test, ideallythe materialis allin variant 2 (the

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 21

    magnitude of the field causes all variants to reorient such that the easy axes align with the external field, forcing variants 1 and 3 into variant 2). Upon the application of the compressive stress, after some period of pure elastic deformation, some material in variant 2 will start to reorient into a stress preferred orientation, i.e. into variant 1. This point is called start 2 to 1 and is identified as S(2,1) in Fig. 2. Reorientation then continues until all material is in variant 1, i.e. the finish 2 to 1 point, identified as F(2,1) in Fig. 2. Once full reorientation from variant 2 to variant 1 is completed, further increase of the compressive load causes the material to deform only elastically. Should the compressive stress then be decreased, the material will initially deform only elastically, however, at some point the removal of the stress and the presence of the magnetic field will cause some material in martensite variant 1 to begin reorientation back into variant 2, this is called start 1 to 2 and is identified as S(1,2) in Fig. 2. Finally, the point where reorientation from variant 1 to 2 ends is called finish 1 to 2 and is identified as F(1,2) in the same figure. Reorientation curves show these start and finish points for various magnitudes of load and load paths on a stress vs. field graph.

    Fig. 2 Variant reorientation points identified on the magneto-mechanical response of the material experiencing a variable compressive stress under a constant magnetic field.

    Prior to this work, Couch et al. (2007) performed constant stress variable field and constant field variable stress tests; data from the later was used to generate reorientation curves. Both types of tests were performed on a2mm x 3mm x 16mm specimens provided by Adaptamat Ltd., same manufacturer that supplied the specimens used in this study. In all of their experiments, the stress was compressive and applied axially, while the magnetic field was applied perpendicular to the stress in the transverse direction. To determine the reorientation curves, the stresses at which variant reorientation

  • 22 Issac Nelson, Constantin Ciocnel and Heidi Feigenbaum

    occurred from the field preferred to the stress preferred orientation and back, from the stress preferred to the field preferred orientation were recorded for various constant field values. The reorientation curves from Couch et al. show that the start and finish values of stress vary in a nonlinear way with applied magnetic field. Such curves can be used for model development and calibration when simple constant field variable stress loading conditions are being simulated. However, to date no researchers have determined reorientation curves for other loading conditions, such as constant stress variable load or variable field variable load. As a result, the objective of work is to determine these curves.

    These types of reorientation curves will be used in future work to help

    derive a model that captures the behaviour of MSMAs subject to general loading conditions. Similar to yield functions in plasticity theory, phenomenological models of MSMAs, such as those by Kiefer and Lagoudas (2005, 2009) and Waldauer et al. (2011), rely on reorientation functions to determine whether or not reorientation is occurring. Once the material reaches a stress field state for reorientation to begin, the material must harden for reorientation to continue until the finished point is reached. Accordingly, reorientation functions play a vital role in the modelling of MSMAs and the experimental work reported here can be used to motivate future models.

    Moreover, robust and general constitutive model should be calibrated on

    one set of data, and with that unique calibration the model to be able to predict the magneto-mechanical response predictions under any loading condition. However, as Waldauer et al. (2011) showed, current material models for MSMAs, such as those by Kiefer and Lagoudas (2005, 2009) and Waldauer et al. (2011), can only be used for loading similar to which the model was calibrated. For example, to simulate variable field-constant stress loading, the model must be calibrated with variable field constant stress experimental data. Furthermore, Waldauer et al. demonstrated that the material parameters found will be quite different if calibrated with variable field-constant stress data than they will be if calibrated with variable stress- constant field data. So at this point it is unclear if a single model that captures the magneto-mechanical behaviour of MSMAs under any load is even feasible.

    Accordingly, the goal of this paper is to establish experimentally a set of

    reorientation curves that can be used to verify whether a single model for all load cases is possible. And if so, the experimentally found reorientation curves in this work can help researchers formulate a constitutive model that can predict material response under any loading conditions. The following sections describe the experimental setup and the experimental data analysis procedure used to acquire and develop the variant reorientation curves.

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 23

    2. Experimental Setup and Procedure 2.1. Experimental Setup

    The experimental setup consisted of a bi-axial 8874 Instron hydraulic test rig equipped with a 3470 GMW 45mm dipole electromagnet (Fig. 3). The magnetic field generated by the electromagnet was applied normal to the direction of the applied compressive stress and was monitored using an AC/DC 5170 Gaussmeter with a transverse Hall probe.The tested specimen wasa single crystal NiMnGa specimen with dimensions 3mm 3mm 20mm, provided by AdaptaMat Ltd.

    Electromagnet

    MSMA specimen

    Magnetic field probe

    Fig. 3 Experimental setup.

    a b Fig. 4 a Load profile as applied using the 8874 test rig and a constant load

    device; b Constant load device as installed on the Instron 8874 frame.

    A power supply controls the current passing through the electromagnet coils and allows for both, constant and variable magnetic fields to be applied on

  • 24 Issac Nelson, Constantin Ciocnel and Heidi Feigenbaum

    the specimen. The compressive load is applied directly by the machine, in the case of variable stress-constant field and variable stress-variable field experiments, or using a device that applies a constant load on the specimen, for the constant stress-variable field case. The need for the constant load device comes from the fact that the stiffness of the specimen changes significantly during tests and the 8874 system cannot keep the load truly constant on the specimen, as it continuously tries to accommodate the change in stiffness. As a result, the applied load from the test rig can vary significantly from the desired constant load,as shown in Fig. 4 a. However, when the constant load device is used there is almost no change in the applied load, as shown in Fig. 4 a.

    2.2. Experimental Procedure

    The constant loaddevice, shown in Fig. 4 b, is made of acetyl-butyl styrene copolymer (ABS) and on one side it has a push rod similar to the aluminium push rods used to perform the tests, while on the other side it has a cylindrical bearing that facilitates the sliding up and down, along a guiding rod, of the device as the specimen expands or compresses upon the application of the magnetic field. The sliding occurs with minimal friction. The constant load device was designed such that it allows the addition of various size weights on it to simulate different stress levels on the tested specimen. As an example, Fig. 4.b shows the constant load device with its own mass of 199 grams, and on top of it another mass of 434 grams, simulating approximately 0.7MPa of stress on the specimen. Additional weights have been manufactured to allow application of stress in increments of 0.25MPa, between 0.25 and 1.75MPa.

    Experiments have been performed in three loading modes: a) constant field variable load, b) constant load variable field, and c) variable load- variable field. In cases a) and c), the tests started with the specimen in variant 2 (fully elongated), while in case b), the tests started with the specimen in variant 1 (fully compressed). Also, in cases a) and b), the load and field have been varied between zero and a maximum value, respectively. In case c), the field was varied between a maximum value and a minimum value equal to 0.25 the magnitude of the maximum value, while the load was varied between zero and a desired maximum value. In all cases, the direction of the loading remained the same as shown in Fig. 3.

    3. Results

    Fig. 5 illustrates the magneto-mechanical response of the material for each loading case considered. The constant field tests were performed at fields ranging between 0.6T and 0.95T in increments of 0.05T and with the compressive stress varying between zero and a maximum of 6.67MPa. The constant stress tests were performed under constant stresses applied in increments of 0.25MPa, between 0.25MPa and 1.75MPa, and magnetic field

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 25

    varying between 0 and 1T. The complex loading tests were performed with the stress and field varying linearly between 0 and 2.5MPa, and between maximum values for magnetic field of 0.65T, 0.75T, 0.85T, 0.95T and a quarter of this magnitude, respectively. These tests started with the specimen fully elongated.

    The data recorded during these tests has been used to determine the start and finish reorientation stress-field values. It is important to note that for low stress levels (between 0.25MPa and approximately 0.4MPa) in the constant stress tests and field magnitudes above 0.75T only reorientation from variant 1 to 2 can be observed experimentally. This can be explained as follows. In the constant stress case, the test is started with the specimen fully in variant 1 from the constant stress applied. As the magnetic field is increased, the variants reorient into variant 2. Then, as the magnetic field is removed, the stress is too weak to be able to induce reorientation back to variant 1. Accordingly, from these tests, only the first two start and finish reorientation stress-field pairs may be obtained.

    In order to produce reorientation curves, a clear criteria for selecting the start and finish reorientation points is needed and previous work has not yet established such criteria. In an effort to be consistent in the selection of the stress and field reorientation values, the authors used a 0.05 strain offset from the elastic region of the reorientation curve, as illustrated in Fig. 5. The start and finish reorientation values have been collected from material response plots that exhibited full reorientation, similar to those shown in Fig. 5. For the constant field variable load case, Fig. 5 a, the material is initially in variant 2 and upon the application of the increasing stress, the variants reorient into variant 1. Therefore, the red line intersects the material response at the points of start reorientation 2 to 1 (S(2,1)) and at finish reorientation 1 to 2 (F(1,2)). The green line intersects the material response at the points of finish reorientation 2 to 1 (F(2,1)) and at start reorientation 1 to 2 (S(1,2)). For the constant stress variable field case, the material is initially in variant 1 and upon application of the increasing magnetic field, it reorients into variant 2. Fig. 5 b shows the selection of the start and finish points for reorientation for this type of loading using the same criteria of 0.05 strain offset from the elastic region.

    For these two cases, where either field or stress is constant, the selection of the stress-field values for the beginning and end reorientation points is fairly straightforward once the off-set strain is defined. However, for the variable stress variable field case, the approach in determining the start and finish reorientation points is a little more involved. One could follow the same procedure as done for the cases where one load is constant, however, now there will be both field strain curves as well as stress strain curves to from which key points may be gathered. If the off-set strain is used for both the field strain plots as well as the stress strain plots there is the potential to select field and stress values that are not happening simultaneously.

  • 26 Issac Nelson, Constantin Ciocnel and Heidi Feigenbaum

    Specifically, it could be seen that the strain value is different if the key point is identified on the strain field curve as compared to if the key point is identified on the stress strain curve. Thus, the following procedure is proposed to identify the stress-field reorientation values with complex loads. First, one picks the start-finish reorientation values for the stress at the 0.05 strain offset, from the stress-strain plot (Fig. 5 c) and then, for that specific strain value reads the corresponding magnetic field value for reorientation from the raw experimental data file.

    Using this procedure start and finish points for reorientation were found for various magnitudes of load for constant stress variable field, constant field variable stress and variable field variable stress loading. A summary of all the results is shown in Fig. 6.

    It must be noted that the experimental data plotted in Fig. 6 shows an unexpectedly large scattering of the data. This may be due to the fact that the specimen developed several cracks between the time the constant field tests

    a b

    F(2,1)

    c d

    Fig. 5 a Constant field variable stress; b Constant stress variable field; c & d Variable stress variable field. The dotted line is plotted parallel to the elastic region during the loading unloading sequence, while the red and green continuous lines are drawn parallel to the dotted line with an offset of 0.05strain.

    S(2,1)

    F(1,2)

    S(1,2)

    F(1,2) S(1,2)

    S(2,1)

    F(2,1)

    0.05

    S(2,1)F(2,1)

    F(2,1) F(1,2)S(2,1)

    S(1,2) S(1,2)

    F(1,2)

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 27

    were performed and the time the other tests were performed (Fig. 7). These cracks developed in the specimen during several tests performed in a dynamic regime to assess the material suitability for power harvesting. As no other specimen was available at the time of data collection, the cracked/chipped specimen was used to perform the remaining tests necessary for this study. The authors expect that once a new fully intact specimen is available it will be used to gather similar type of data, and the scatter should be significantly reduced.

    In addition, the method used for the magnetic field measurement may have contributed to the scattering of the data. Specifically, the field was measured using a Hall probe whose position along the specimen may have not been the same when measurements were made for the various tests performed. While the field distribution between the magnetic poles, along the specimen height, is uniform in the absence of the MSMA specimen, as the variant reorientation occurs within the MSMA there is a change in the direction of internal magnetization, which can affect the external magnetic field. So if there are variations along the length of the specimen of the variant volume fraction, reading the field at slightly different locations along the specimen may lead to slightly different measured field values at key points. This would lead to scatter in the reorientation curves as seen in Fig. 6.

    F(2,1)

    S(2,1)

    S(1,2)

    F(1,2)

    Fig. 6 Variant reorientation data for a Ni50Mn28.5Ga21.5alloy.

  • 28 Issac Nelson, Constantin Ciocnel and Heidi Feigenbaum

    To improve the reorientation plots shown in Fig. 6, additional experiments need to be performed to provide data particularly in the regions below 2MPa stress or 0.6T field. Data points in these regions are the most difficult to acquire because when a low constant stress is combined with a medium to low field, reorientation will occur only in one direction, from variant 1 to 2, as the stress will not be able to overcome the field to reorient the variants back to variant 1. And similarly should for a low constant field with medium to low compressive stress value.

    chip

    Fig. 7 Tested specimen exhibiting cracks and chips after being loaded dynamically.

    crack

    4. Conclusions

    1. The results shown in Fig. 6 demonstrate that a single model for when reorientation begins and ends which can capture all the three loading conditions used in this work (variable stress constant field, variable field constant stress, and variable field variable stress) is possible.

    2. Lines have been drawn in Fig. 6 to show the approximate reorientation curves given by the data. Despite the large scatter of the data, these lines show that a single curve can capture relatively well each of the key reorientation points (the start 1 to 2, start 2 to 1, finish 1 to 2 and finish 2 to 1) no matter which type of loading the material was subject to (constant stress variable field, constant field variable stress or variable stress variable field).

    3. While this only shows that a single model to capture the three load cases used here could be developed, these load cases are diverse enough to suggest that a single model that can simulate any 2D load case is possible.

    4. Reorientation functions that mimic the curves seen in Fig. 6 will be important features of a phenomenological model that can capture any loading case with a single calibration.

    Acknowledgements. This material is based upon work supported by the

    National Science Foundation under Grant No. 0923517 and Grant No. 1101108. The authors would also like to thank AdaptaMat Ltd. for providing the MSMA samples.

  • Bul. Inst. Polit. Iai, t. LVIII (LXII), f. 3, 2012 29

    REFERENCES

    Couch R.N., Sirohi J., Chopra I., Development of a Quasi-static Model of NiMnGa Magnetic Shape Memory Alloy. Journal of Intelligent Material Systems and Structures, 18, 611-622 (2007).

    Karaca H.E., Karaman I., Basaran B., Chumlyakov Y.I., Maier H.J., Magnetic Field and Stress Induced Martensite Reorientation in NiMnGa Ferromagnetic Shape Memory Alloy Single Crystals. Acta Materialia, 54, 233245 (2006).

    Kiefer B., Lagoudas D., Magnetic Field-induced Martensitic Variant Reorienta-tion in Magnetic Shape Memory Alloys. Philosophical Magazine, 85, 42894329 (2005).

    Kiefer B., Lagoudas D., Modeling the Coupled Strain and Magnetization Response of Magnetic Shape Memory Alloys under Magnetomechanical Loading. Journal of Intelligent Material Systems and Structures, 20, 143-170 (2009).

    Marioni M., Bono D., Banful A., del Rosario M., Rodrigue E., Peterson B., Allen S., OHandley R., Pulsed Field Actuation of Ni-Mn-Ga Ferromagnetic Shape Memory Alloy Single Crystal. Phys. IV France, 112, 10011004 (2003).

    Waldauer A.B., Feigenbaum H.P., Ciocanel C.,, Improvements to the Kiefer and Lagoudas Model for Prediction of the Magneto-Mechanical Behavior of Magnetic Shape Memory Alloys. ASME 2011 Conference on Smart Materials, Adaptive Structures and Intelligent Systems (SMASIS 2011), Scottsdale, AZ, 2011.

    CURBE DE REORIENTARE PENTRU UN ALIAJ Ni50Mn28.5Ga21.5

    (Rezumat) Lucrarea prezint curbele de reorientare obinute experimental pentru un aliaj

    magnetic cu memoria formei. Aceste curbe de reorientare caracterizeaz rspunsul materialului la diferite tipuri de ncrcri i sunt necesare pentru simularea rspunsului materialului cu modele de material fenomenologice. Rezultatele susin posibilitatea crerii unui model fenomenologic care s foloseasc un singur set de curbe de reorientare pentru obinerea parametrilor modelului, parametri cu care modelul poate simula toate tipurile de ncrcri la care poate fi supus materialul.

  • BULETINUL INSTITUTULUI POLITEHNIC DIN IAI Publicat de

    Universitatea Tehnic Gheorghe Asachi din Iai, Tomul LVIII (LXII), Fasc. 3, 2012

    Secia CONSTRUCII DE MAINI

    PARTICULATE CORDIERITE - ZIRCONIA COMPOSITES

    BY

    CIPRIAN ATNSOAEI, VIOREL GOAN and PAUL DORU BRSNESCU

    Gheorghe Asachi Technical University of Iasi, Department of Mechanical Engineering, Mechatronics and Robotics

    Received: May 2012 Accepted for publication: June 2012

    Abstract. The literature proposes many studies on improving the

    mechanical properties of zirconia (ZrO2) reinforced cordierite. Strengthening mechanisms operating in the system cordierite - zirconia are based on large difference between thermal expansion of the two components and transformation of zirconia from tetragonal to monoclinic state (transformation toughening). The best results were obtained especially when transformation of zirconia in zircon was avoided by using Yttria Stabilized Zirconia (YSZ) combined with a high heating rate or Rate-Controlled-Sintering (RCS).

    Key words: cordierita, zirconia, zircon, composite materials.

    1. Introduction

    Cordierite is a ceramic with a very low thermal expansion (2 10-6/C), good dielectric properties (~4 at 1 MHz), high chemical stability and a relatively low cost price. These qualities are often valued in the manufacture of structural ceramic components for use in aggressive environments (catalytic converters, multilayer circuit boards, kiln furniture, thermal insulation parts, diesel particulate filters, etc.). However, the poor mechanical properties limit the usefulness of this material. It is widely accepted that the best way to improve the mechanical properties of cordierite ceramics is to use fibers or

    Corresponding author: e-mail: [email protected]

  • 32 Ciprian Atnsoaei et al.

    particulate reinforcements. The range of reinforcement materials used is quite large: diamond (Hasselman et al., 1994), mullite (Ebadzadeh & Lee, 1998), SiC (Wadsworth & Stevens, 1991), ZrO2 (Wadsworth et al., 1990), Si3N4 (Zamir et al., 2010) etc. A quality composite requires careful control of each stage of processing. This is even more important in the case of cordierite because its sintering temperature range is very narrow (about 50C). In addition, zirconia reinforced cordierite is prone to a particular problem: the tendency of zirconia to react with the cordierite matrix, resulting in zircon - a compound with poor mechanical properties.

    The scientific literature gave pretty much attention to reinforcement of cordierite with zirconia particles proposing several variants of technological routes, each having results more or less significant. This paper aims at highlighting the technological details that lead to obtain substantial improvements of mechanical properties of zirconia toughened cordierite.

    2. Toughening Mechanisms in Zirconia-Cordierite Composites 2.1. Transformation Toughening

    In terms of crystalline structure, zirconia shows three states: monoclinic (m zirconia), tetragonal (t zirconia) and cubic (c zirconia) (Xia & Langdon, 1994). The monoclinic structure can be kept up to 950C. The temperatures between 9502370C correspond to tetragonal structure and beyond 2370C usually we can find only the cubic structure. Regarding the transformation toughening mechanism, the most important fact is zirconia transition from tetragonal to monoclinic structure (t-m transformation), because it implies a volume increase of about 4%. If zirconia is dispersed in a (ceramic) matrix with a similar thermal expansion, t-m transformation will significantly change the stress field within the ceramic body. Therefore, transformation toughening alters the normal propagation of macrocracks by creating stress concentrators into the ceramic body.

    In the case of zirconia toughened cordierite, transformation toughening is not always a very important mechanism influencing the composite performance because the thermal expansion of cordierite is much lower than that of zirconia, This allows reinforcing particle to have a volume increase greater than that induced by the t-m transformation (Wadsworth et. al., 1990). Besides this, the increase in volume due to t-m transformation is similar to volume shrinkage after sintering, and thus the two phenomena are partially or totally cancelling their effects. On the other hand, the combination of several factors (the use of additives, particle size, homogeneity, etc.) can inhibit the t-m transformation.

    As one can see, when we are talking about zirconia toughened cordierite, the contribution of transformation toughening to mechanical performance is hard to predict. In practice, the presence of the transformation toughening mechanism can be evaluated by X-ray diffraction (XRD), comparing the values

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    measured for m-zirconia, before and after polishing the surface studied (Jang, 1995).

    2.2. Microcracking

    The trajectory of a macrocrack can be deflected if it encounters areas with different mechanical properties (obstacles, different stress fields, etc.). The mechanism of microcracking involves the appearance of cracks in the ceramic body. These microcracks occur in areas with high tensile stresses which attract the microcrack and divert its trajectory (Fig. 1).

    Fig. 1 Macrocrack deflected by Fig. 2 A crack front pinned by particles microcracks (Xia & Langdon, 1994). (Xia & Langdon, 1994).

    Increasing the length of macrocrack path can reduce its energy below the

    limit at which propagation is possible. In the zirconia-cordierite system, microcracks are induced by the large

    difference of thermal expansion of the constituents. Of course, despite the fact that it is not always very efficient, t-m transformation can be another microcracks source.

    2.3. Crack Pinning

    Crack pinning mechanism consists in stopping the propagation of a macrocrack when it meets a particle or a fiber which has the tensile strength greater than the macrocrack tip stress (Fig. 2). In the zirconia-cordierite system, the big difference between the mechanical properties of the constituents makes the crack pinning mechanism to be very effective. However, the efficiency of this mechanism is closely related to the quality of cohesion between matrix and reinforcement material.

  • 34 Ciprian Atnsoaei et al.

    3. Effect of Starting Powders Preparation 3.1. Particle Size Effect (Milling and Mixing Effect)

    Both theoretical and practical (Jang, 1995), is well known that densification of powders can be significantly improved by reducing the size of the starting powders. This is also true in zirconia-cordierite system, where milling up to 24h or more can reduce the optimal sintering temperature below 1300C. The mechanical properties, especially fracture toughness, hardness and f