City of Newark Municipal Pretreatment Program Annual ... of Newark... · Flo-Form 215 Oakwood Ave. Newark, Ohio 43055 Garrie Hill Insignificant IU Local Limits Tri-annual Last inspection

City of Newark

Municipal Pretreatment Program

Annual Report

November 2014

Prepared by:Employees of theCity of NewarkDivision of Water and Wastewater

TABLE OF CONTENTS

Page

EPA Form 4117 (2/11)...............................................................................................1

Monitoring Equipment Inventory ..............................................................................11

Industrial Pretreatment Sampling and Testing Schedule ...........................................12

Program Evaluation ...................................................................................................14

Appendix 1 – Priority Pollutants and TTOs ..............................................................18

Newark WWTP Priority Pollutants, September 2014........................................19

Anomatic TTO, November 2013........................................................................26

Anomatic TTO, February 2014 ..........................................................................29

Anomatic TTO, June 2014 .................................................................................32

Anomatic TTO, September 2014 .......................................................................35

Owens Corning Priority Pollutants, March 2014 ...............................................38

Pretreatment Program Annual Report (For Approved Pretreatment Programs)

Instructions: Annual reports must be completed each year and submitted no later than the date specified in Part II of thepermittee’s NPDES permit. Please note that the “Pretreatment Priority Pollutant Reporting Form” (EPA 4221) must besubmitted with this form.

Part A: Certification

Approved Program Information

Date: November 6, 2014Sewer Authority Name: City of Newark, Ohio

Period Covered By Report: October 1, 2013 – September 30, 2014

Wastewater Treatment Plant(s) Included In Program: NPDES Permit Number(s):

1. Newark Wastewater Treatment Plant 1. 4PE00001*MD

2. 2.

3. 3.Contact Name and TitleName: Darin Wise Title: Plant Superintendent

Mailing Address: 1003 E. Main Street

City: Newark State: Ohio Zip: 43055-8845

Phone: (740) 349-6768 x 202 Fax: (740) 349-6771 E-mail: [email protected]

Certification (Must be signed by the responsible official)

I certify under penalty of law that I have personally examined and am familiar with the information in this report and allattachments. Based on my inquiry of those persons immediately responsible for obtaining the information contained inthe report, I believe that the information is true, accurate and complete. I am aware that there are significant penaltiesfor submitting false information, including the possibility of fine and imprisonment.

Signature:

Title: Date: / /

Mail completed annual reports to:Ohio EPA, DSW Pretreatment

UnitPO Box 1049

Columbus, OH 43216-1049

EPA 4117 (2/11) Page 1 of 10 Distribution: DSW Files

Pretreatment Program Annual Report

Part B: Pretreatment Performance Summary

POTW Information

POTW: Newark Wastewater Treatment Plant

NPDES Permit Number: 4PE00001*MD

Reporting Period: October 1, 2013 – September 30, 2014

Total Significant Industrial Users (SIUs): 13

Total Number of Categorical Industrial Users: 3

Total Number of Significant Non-Categorical Industrial Users: 10

Compliance Monitoring Program

Number of Effective Control Documents: 13

Number of SIUs Inspected: 13

Number of SIUs Sampled: 13

Significant Noncompliance (SNC) Assessment

Number of SIUs In SNC (Categorical/Non-Categorical): 0/0

Number of SIUs In SNC for Sampling Violations: 0

Number of SIUs In SNC for Reporting Violations: 0

Number of SIUs In SNC for Compliance Schedule Violations: 0

Enforcement Activity

Number of Show-Cause Hearings: 0

Number of Compliance Schedules Issued: 0

Number of Administrative Orders Issued: 0

Number of Civil Suits Filed: 0

Number of Criminal Suits Filed: 0Amount of Penalties Collected (Total dollars/Number of IUs assessed): $0.00/0

Number of Facility Enforcement Activities Published (Attach newspaper list): 0



Part C: Industrial User Inventory and Monitoring Page 3 of 10

POTW Information (Attach additional pages if necessary)

POTW: City of Newark Wastewater Treatment Plant


Facility Name &Address/Contact

Person

LocalClassification

Applicable Standards

POTW IU Monitoring IU Self-Monitoring

Number ofInspections

Numberof Sample

Events

Numberof

SampleEvents

ReportingFrequency

Anomatic Corporation1650 Tamarack Rd.

Newark, OhioSteve O’Toole

Categorical IU433 and

Local Limits1

6/wk312/yr

ContinuouspH

365/yr1/mo

Universal Veneer1776 Tamarack Rd.

Newark, OhioJames Wright/Terry Mellars

Categorical IU429.35 and 429.105existing source, use

Local Limits1

1/wk52/yr

Daily pH5/wk

260/yr1/mo

Tamarack Dairy1701 Tamarack Rd.

Newark, OhioBrian Snodgrass

Categorical IU405.24 and

Local Limits1

6/wk312/yr

ContinuouspH

365/yr1/mo

Holophane214 Oakwood Ave.

Newark, OhioRon Houdeshell

Significant IU Local Limits 1 1/yr n/a n/a

Arboris LLC1780 Tamarack Rd.

Newark, OhioDave Neely

Significant IU Local Limits 16/wk

312/yr

ContinuouspH

365/yrn/a

Owens Corning400 Case Ave.Newark, Ohio

Mark Arnold/Randy Hilleary

Significant IU Local Limits 1Daily365/yr

Daily365/yr

1/mo

Star Wipers1125 E. Main St.

Newark, OhioTodd Wilson

Significant IU Local Limits 11/wk52/yr

1/mo12/yr

1/mo








Person

LocalClassification




Numberof Sample

Events

Numberof

SampleEvents

ReportingFrequency

International Paper1851 Tamarack Rd.

Newark, OhioEd Johnston


n/a n/a

PCA205 S. 21st St.Newark, OhioDave Gawelek


Determinedby PCA

Corporate

As testingoccurs

Buckeye Linen76 Jefferson St.Newark, Ohio

Carl Sipe


n/a n/a

Licking MemorialHospital

1320 W. Main St.Newark, OhioJohn Tolliver


n/a n/a

MPW150 S. 29th St.Newark, Ohio

Brent Hamilton

Significant IU Local Limits 16/wk

312/yrn/a n/a

Tencate23 Sisal St.

Newark, OhioPaul McElhaney

Significant IU Local Limits 1 1/yr n/a n/a

Modern Welding72 Waldo St.

Newark, Ohio 43055Jeff Turner

InsignificantIU

Local Limits

Tri-annualLast inspection

2014, nextinspection 2017

1/yr n/a n/a








Person

LocalClassification




Numberof Sample

Events

Numberof

SampleEvents

ReportingFrequency

The Ohio StateUniversity - Newark

University Dr.Newark, Ohio 43055

Dave Mettler

InsignificantIU

Local Limits



1/yr n/a n/a

Tectum Corporation105 South 6th St.

Newark, Ohio 43055Roger Lewis

InsignificantIU

Local Limits



1/yr n/a n/a

Contour Forming/Flo-Form

215 Oakwood Ave.Newark, Ohio 43055

Garrie Hill

InsignificantIU

Local Limits



1/yr n/a n/a



Part D: Industrial Inventory Modifications Page 6 of 10





Person

Add,Change,Delete

If Deletion,State

Reason forDeletion

If Addition or Significant Change, Complete the Following:

ProcessDescription

LocalClassification

Flow Rate Pollutants ApplicableStandards

No changes

EPA 4117 (2/11) Page 6 of 10 Distribution: DSW File


Part E: General Monitoring Information Page 7 of 10




Industrial User Classification POTW Industrial User Monitoring Industrial User Self-Monitoring

InspectionFrequency

SamplingFrequency

SamplingFrequency

ReportingFrequency

Anomatic CorporationCategorical Industrial User

1/yr 6/wk

Continuous pHmonitoring, report

daily max/min. TTOquarterly, other

parameters weekly

1/mo

Tamarack Farms DairyCategorical Industrial User

1/yr 6/wkContinuous pH

monitoring, reportdaily max/min

1/mo

Universal VeneerCategorical Industrial User

1/yr 1/wk

pH monitoringevery 2 hours,

report dailymax/min

1/mo

Arboris LLCSignificant Industrial User

1/yr 6/wk n/a n/a

Owens CorningSignificant Industrial User

1/yr 1/dayDaily

Phenol quarterly,TTO yearly

1/mo

Star WipersSignificant Industrial User

1/yr 1/wk 1/mo 1/mo

International PaperSignificant Industrial User

1/yr 1/wk n/a n/a








InspectionFrequency

SamplingFrequency

SamplingFrequency

ReportingFrequency

PCASignificant Industrial User

1/yr 1/wkOccasional splitrequired by PCA

Corporate, not CityAs testing occurs

Buckeye LinenSignificant Industrial User

1/yr 1/wk n/a n/a

Licking Memorial HospitalSignificant Industrial User

1/yr 1/wk n/a n/a

MPWSignificant Industrial User

1/yr 1/wk n/a n/a

HolophaneSignificant Industrial User

1/yr 1/yr n/a n/a

TencateSignificant Industrial User

1/yr 1/yr n/a n/a

Modern WeldingInsignificant Industrial User

Tri-annual(once every three

years)1/yr n/a n/a

OSU-NInsignificant Industrial User


years)1/yr n/a n/a








InspectionFrequency

SamplingFrequency

SamplingFrequency

ReportingFrequency

TectumInsignificant Industrial User


years)1/yr n/a n/a

Contour Forming/Flo-FormInsignificant Industrial User


years)1/yr n/a n/a



Part F: Upsets, Interference and Pass-Through Incidents Page 10 of 10




Type of Incident Date Explanation/Reason Corrective Action(s) Taken

No incidents of WWTPupset, interference orpass-through to report

during this period


11

City of Newark Industrial Monitoring Equipment Inventory

• 1 - 2008 Chevrolet Uplander

• 2 - Portable Temperature and D.O. Meter – YSI Models 55 & 550

• 5 - Thermos Ice Chests

• Portable Samplers2 - American Sigma Model 900 SD5 - American Sigma Model 9005 - American Sigma Model 900 MAX

• 2- MSA Orion Multi Gas Detectors

• 1 - KitchenAid Ice Maker; Model #W10136157B

• 2- portable Oakton Waterproof pHTester10

• 1 - True MC Refrigerator; Model T- 49

Autosampler locations:

900 MAXWWTP Final BldgStar WipersUniversal VeneerWWTP

900Buckeye LinenMobile Power Wash (MPW)Licking Memorial Hospital (LMH)Landfill

900 SDArboris

Autosamplers in storage:1 – 900 SD1 – 900 MAX

Industrial Sampling and TestingRevision Date: November 3, 2014

\\\Env. Lab - Industrial Pretreatment Sampling and Testing Schedule

Tier 2 Tier 1

PARAMETER OCF TAMARACK ANOMATIC ARBORISLLC

STARWIPERS

PCA MPW INT’LPAPER

L.C.M.H. UNIV.VENEER

BUCKEYELINEN

Alkalinity

Ammonia NH3-N 7/wk-C 6/wk-C 6/wk-C 6/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C

Bis(2-ethylhexyl) 1/qtr-C 1/qtr-C

CBOD5 1/mo-C 6/wk-C 6/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C 1/wk-C

COD 7/wk-C 1/mo-C 6/wk-C†

Color IWI-7/wk-C

% Transmittance IWI-7/wk-C

Cyanide, Total 2/yr-C

DO

Nitrate NO3-N

Nitrite NO2-N

O & G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G 1/qtr-G

pH IWI-daily-G IWI-daily-G IWI-daily-G IWI-daily-G IWI-1/wk-G 1/wk-G 6/wk-G† 1/wk-G 1/wk-G 1/wk-G 1/wk-G

Phenol note *

Phos-Bray

Phos-Tot 2/yr-C 2/yr-C 1/wk-C 2/yr-C 2/yr-C 1/qtr-C 1/qtr-C 1/qtr-C 1/qtr-C 1/qtr-C 1/qtr-C

Susp. Solids 7/wk-C 6/wk-C 6/wk-C 6/wk-C 1/wk-C 1/wk-C 6/wk-C† 1/wk-C 1/wk-C 1/wk-C 1/wk-C

TKN

Tot. Solids 6/wk-C†

Vol Acid

Vol Solids

Tot. Diss. Solids 1/mo - C 1/mo - C 1/mo - C 1/mo - C 1/mo - C 1/mo - C 6/wk C† 1/mo - C 1/mo - C 1/mo - C 1/mo - C

Ba 1/yr-C

Cd 1/yr-C 1/yr-C 1/wk-C 1/qtr-C 1/mo-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Cr-Hex 1/mo-G

Cr-Tot 1/yr-C 1/yr-C 1/wk-C 1/qtr-C 1/mo-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Cu 1/yr-C 1/yr-C 1/wk-C 1/qtr-C 1/mo-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Pb 1/yr-C 1/yr-C 1/wk-C 1/qtr-C 1/mo-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Hg 1/yr-C 1/yr-C 2/yr-C 2/yr-C

K 1/yr-C 1/yr-C

Ni 1/yr-C 1/yr-C 1/wk-C 1/qtr-C 1/mo-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Ag 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Se 1/yr-C 1/yr-C 1/qtr-C 2/yr-C 2/yr-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

Zn 1/yr-C 1/yr-C 1/wk-C 1/qtr-C 1/mo-C 2/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C 1/yr-C

* OCF Phenol – Run if NH3-N is above 30 mg/l† MPW changed to daily sampling starting 7/26/14IWI = Industrial Waste Inspector dataC = 24 Hour Composite sample, except Bis-2 (3 grabs 30min - 2hrs apart)G = Grab sampleNote: All industries with pretreatment (OC, Tamarack, PCA, Star Wipers, Anomatic, UV) compare influent to effluent to check efficiency of pretreatment, once per year.

12

Industrial Sampling and TestingRevision Date: November 3, 2014

Env. Lab - Industrial Pretreatment Sampling and Testing Schedule

Tier 1 CSO Monitoring

PARAMETER CONTOURFORMING

TECTUM

UP &DOWN

MODERNWELDING

OSU-N

UP &DOWN

TENCATE

UP & DOWN

HOLOPHANE

UP & DOWN

CSOSAMPLES

CSO1008

Alkalinity

Ammonia NH3-N 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Bis(2-ethylhexyl)

CBOD5 1/yr-G 1/yr-G 1/yr-G 1/yr-G

COD 1/yr-G 1/yr-G

Color

Cyanide, Total 1/yr-G

DO

Nitrate NO3-N

Nitrite NO2-N

O & G 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

pH 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Phenol

Phos-Bray

Phos-Tot 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Susp. Solids 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

TKN

Tot. Solids

Vol Acid

Vol Solids

Flow X X

Al 1/yr-G

Ba

Cd 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Cr-Hex

Cr-Tot 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Cu 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Pb 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Hg 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

K

Ni 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Ag 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Se 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

Zn 1/yr-G 1/yr-G 1/yr-G 1/yr-G 1/yr-G

IWI = Industrial Waste Inspector dataC (this page only) = Composite sample made from 3 grabsG = Grab sampleNote: All industries with pretreatment (OCF, Tamarack, PCA, Star Wipers, Anomatic) compare influent to effluent to check efficiency of pretreatment, once per year.

13

14

Pretreatment Program Evaluation 2014

A. Narrative Statement

The approval of Newark’s Industrial Pretreatment Program in March 1985 was thebeginning of what has been a continuously successful program. Cooperation between theCity and its industrial dischargers has been very good. Each industrial discharger whohas a pretreatment system is monitored, as well as those who discharge directly to thePOTW without treatment. Newark is currently in compliance with federal, state andlocal regulations, and Newark’s WWTP is operating in compliance with its currentNPDES permit, 4PE00001*MD.

B. Legal Authority

The authority of the City to issue Industrial User Permits (Administrative Orders)to Newark’s industrial dischargers is contained in the Newark Codified Ordinance,Chapter 1040, Section 25, Part C (Sewer Use Ordinance) and amendments thereto. Theauthority to administer the FOG program is contained in Chapter 1047. The Cityapproved an updated Sewer Use Ordinance in 2013. The current Industrial User Permits(Administrative Orders) were issued that same year.

C. State and Federal Regulation Changes

Newark’s Industrial Pretreatment Program is current with federal and stateregulations. The current Industrial User Permits (Administrative Orders) have aneffective date of April 1, 2013 through March 31, 2017. The laboratory analysis methodsused to regulate the City of Newark’s Industrial Users are in compliance with the latest40 CFR Part 136 update published May 18, 2012. The City of Newark WastewaterTreatment Plant is operating under an NPDES permit with an effective date of August 1,2011 until July 31, 2016.

D. Industrial Pretreatment Operating Procedures

Newark’s categorical and significant IU’s are inspected annually; insignificant IU’sare inspected tri-annually. We maintain continuing surveillance of all our significant andcategorical industrial users. Five (5) significant IU’s submit monthly self-monitoringreports. Data from in-house and self-monitoring analyses are reviewed to ensure that allregulated parameters are within limits. All data is maintained in the Allmax Synexusdatabase. Refer to pages 12 and 13 of this report for a complete listing of the surveillance

15

completed by the City of Newark on the Industrial Users during the October 2013 –September 2014 reporting period.

The WWTP Influent, Effluent and Cake have been analyzed for Priority Pollutants,and two of our industrial dischargers routinely self-monitor Total Toxic Organics. ThePriority Pollutant and TTO data are contained in Appendix 1 of this report.

E. Industrial Pretreatment Program Financing

In 2013, Newark began a “stepped” approach to increasing industrial user fees andwastewater strength surcharges. There is a scheduled increase in July of each year until2016. Strength surcharges are assessed on all industries discharging higher thanbackground concentrations of suspended solids, CBOD and ammonia. This additionalfee helps to recover the City’s increased waste treatment costs associated with higherstrength waste (electricity to run blowers, trucking costs to remove biosolids, etc.).Surveillance charges are assessed on the industries based on the number of scheduledsampling events per week; higher surveillance frequency results in a higher charge. Thischarge is used to recover the cost of collecting samples, testing, and reporting analyticalresults. The 2013 adjustment to the industrial user fees and strength surcharges updatedthe previous rates that were established in 1999.

The WWTP also uses other capital-building measures such as fee-based trucked wastedisposal and selling scrubbed methane to the natural gas utility to meet the demands of itsoperating budget.

F. Program Accomplishments

Anomatic:

Anomatic continues its effort to ensure the Newark WWTP is able to meet the currentNPDES target for the City of Newark’s effluent; a monthly-averaged phosphorus limit of663 kg/day (summer months, May – Oct only). No violations of that monthly-averagedlimit have occurred during this reporting period (Oct 1, 2013 – September 30, 2014). OnMay 1, 2016, the phosphorus limit for the WWTP discharge will drop to a summermonthly-averaged target of 331.5 kg/day per the City’s NPDES permit. Anomatic is thebiggest contributor to the phosphorus loading at the WWTP, so control at this industrialfacility is paramount to Newark achieving its phosphorus reduction goal. Anomatic has,and continues to invest large amounts of capital improvement money to reduce theamount of phosphorus discharged in its industrial wastewater.

16

Several locations on each of the eight factory lines are sampled three times per day in aneffort to detect and locate leaks that could be high in phosphorus or nickel. Anomatic’slab tests phosphorus daily. If high phosphorus is found in Anomatic’s wastewaterdischarge to the City, it is Anomatic’s protocol to locate and stop the source of thephosphorus ASAP.

Over the past three years, all eight factory lines have been re-plumbed to segregateindividual wastestreams based on their chemical constituents. These wastestreams arethen re-mixed in specific ratios to facilitate flocculation and precipitation of phosphorus,reducing the discharge of reactive phosphorus to the sewer. Anomatic has also added analuminum chlorohydrate (ACH) introduction point within its rebuilt pretreatment system.In the event an untreated slug load of high strength phosphorus passes into thepretreatment system, ACH can be added as an emergency measure. ACH acts as abinding agent, rendering phosphorus insoluble and unavailable for biological processessuch as algal growth.

G. Problem Areas of Industrial Pretreatment Program

There were no pass through incidents at the WWTP during this reporting period.

H. Program Modifications

MPW surveillance has increased from once per week to 6 days per week at theindustry’s request. This industry is attempting to reduce its total suspended solidssurcharge through better tracking of day to day fluctuations in their waste stream. TheCity regularly assists Industrial Users in data collection and expanded testing whenquestions or problems arise with their wastewater discharges. Creative problem solvingbetween current industries and the City helps to ensure the Newark WWTP will havecapacity for future industrial dischargers.

I. Local Limits

The most current Local Limits Study was completed in 2011, and was the basis forthe latest Industrial User Permits (Administrative Orders) issued in 2013. An updatedLocal Limits study for background constituents is scheduled for the latter end of 2016when our NPDES Permit expires.

J. Special Considerations

Most of the industries in our pretreatment program take their role in theprevention of pollution very seriously. They are generally receptive to any modificationsto their system that we request. Without their cooperation, Newark’s pretreatmentprogram would be almost impossible to administer. The City of Newark also recognizes

17

Ohio EPA’s ongoing assistance with the effective implementation of this Program.OEPA has been very helpful in creating a stronger Industrial Pretreatment Program forthe protection of both our citizens and the environment.

18

Appendix 1

Priority Pollutants andTotal Toxic Organics Data:

City of Newark WWTPAnomatic

Owens Corning

19

City of Newark WWTP

Priority Pollutants

September 2014

26

Anomatic

Total Toxic Organics (TTO)

November 2013

Parameter Result Units PQL Method of Analysis Prep Date Date of Analysis NotesArsenic, Total <0.005 mg/L 0.005 EPA-200.9 11/14/2013

Molybdenum, Total 0.067 mg/L 0.020 EPA-200.7 11/15/2013

Selenium, Total <0.020 mg/L 0.020 EPA-200.9 11/19/2013 Higher detection level due to sample matrix.

Aldrin <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Alpha-BHC <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Beta-BHC <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Delta-BHC <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Gamma-BHC (Lindane) <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Chlordane <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

4,4'-DDT <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

4,4'-DDE <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

4,4'-DDD <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

Dieldrin <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

Alpha Endosulfan <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Beta Endosulfan <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

Endosulfan Sulfate <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

Endrin <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

Endrin Aldehyde <0.50 ug/L 0.50 EPA-608 11/11/2013 11/12/2013

Heptachlor <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Heptachlor Epoxide <0.25 ug/L 0.25 EPA-608 11/11/2013 11/12/2013

Methoxychlor <2.50 ug/L 2.50 EPA-608 11/11/2013 11/12/2013

PCB-1016 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

PCB-1221 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

PCB-1232 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

PCB-1242 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

PCB-1248 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

PCB-1254 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

PCB-1260 <5.00 ug/L 5.00 EPA-608 11/11/2013 11/12/2013

Toxaphene <12.5 ug/L 12.5 EPA-608 11/11/2013 11/12/2013

(Surrogate) TCMX 72.6 % EPA-608 11/11/2013 11/12/2013 (14.2-117.2)

(Surrogate) DCB 44.9 % EPA-608 11/11/2013 11/12/2013 (D-134.4)

Acenaphthene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Acenaphthylene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Anthracene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Benzo(a)anthracene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Benzidine <100 ug/L 100 EPA-625 11/12/2013 11/13/2013

Benzo(b)fluoranthene (3,4-benzofluoranthene)<20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Benzo(k)fluoranthene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Benzo(g,h,i)perylene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Benzo(a)pyrene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

bis(2-chloroethoxy)Methane <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

bis(2-chloroethyl)Ether <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

bis(2-chloroisopropyl)Ether <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

bis(2-ethylhexyl)Phthalate 29.4 ug/L 10.0 EPA-625 11/12/2013 11/13/2013

4-Bromophenyl phenyl ether <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Butyl benzyl phthalate <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

2-Chloronaphthalene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

4-Chlorophenyl phenyl ether <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Chrysene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Dibenzo(a,h)anthracene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Di-n-butyl phthalate <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

3,3'-Dichlorobenzidine <40.0 ug/L 40.0 EPA-625 11/12/2013 11/13/2013

Diethyl phthalate <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Dimethyl phthalate <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

2,4-Dinitrotoluene <40.0 ug/L 40.0 EPA-625 11/12/2013 11/13/2013

2,6-Dinitrotoluene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Di-n-octyl phthalate <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

1,2-Diphenylhydrazine <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Fluoranthene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Fluorene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Hexachlorobenzene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Hexachlorobutadiene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Hexachlorocyclopentadiene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Hexachloroethane <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Indeno(1,2,3-cd)pyrene <40.0 ug/L 40.0 EPA-625 11/12/2013 11/13/2013

Isophorone <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Parameter Result Units PQL Method of Analysis Prep Date Date of Analysis NotesNaphthalene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Nitrobenzene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

N-Nitrosodimethylamine <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

N-Nitrosodiphenylamine <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

N-Nitrosodi-n-propylamine <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Phenanthrene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

Pyrene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

1,2,4-Trichlorobenzene <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

4-Chloro-3-methylphenol (p-chloro-m-cresol)<100 ug/L 100 EPA-625 11/12/2013 11/13/2013

2-Chlorophenol <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

2,4-Dichlorophenol <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

2,4-Dimethylphenol <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

2,4-Dinitrophenol <100 ug/L 100 EPA-625 11/12/2013 11/13/2013

2-Methyl-4,6-dinitrophenol (4,6-dinitro-o-cresol)<100 ug/L 100 EPA-625 11/12/2013 11/13/2013

2-Nitrophenol <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

4-Nitrophenol <100 ug/L 100 EPA-625 11/12/2013 11/13/2013

Pentachlorophenol <100 ug/L 100 EPA-625 11/12/2013 11/13/2013

Phenol <20.0 ug/L 20.0 EPA-625 11/12/2013 11/13/2013

2,4,6-Trichlorophenol <40.0 ug/L 40.0 EPA-625 11/12/2013 11/13/2013 Reported as an estimate due to 2 or more surrogate recoveries falling outside established limits.

Higher detection levels due to sample matrix.

(Surrogate) 2-Fluorophenol 0.7 % EPA-625 11/12/2013 11/13/2013 (3.2-64.3)

Result is outside established limits.

(Surrogate) Phenol d6 0.2 % EPA-625 11/12/2013 11/13/2013 (D-48.1)

(Surrogate) Nitrobenzene d5 75.2 % EPA-625 11/12/2013 11/13/2013 (18.5-99.2)

(Surrogate) 2-Fluorobiphenyl 64.0 % EPA-625 11/12/2013 11/13/2013 (D-131.4)

(Surrogate) 2,4,6-Tribromophenol 1.6 % EPA-625 11/12/2013 11/13/2013 (6.6-127.4)

Result is outside established limits.

(Surrogate) p-Terphenyl-d14 73.2 % EPA-625 11/12/2013 11/13/2013 (13.7-123.6)

Dioxin Screen * Y/N 625/8270DIOX 11/13/2013 Non Detect

625/8270 Library Search * Y/N 625/8270 TIC 11/13/2013 Attached

Chromium, Hexavalent <0.010 mg/L 0.010 SM-3500-Cr B 11/08/2013

Cyanide, Total 0.01 mg/L 0.01 SM-4500-CN E 11/13/2013

Acrolein <50.0 ug/L 50.0 EPA-624 11/13/2013

Acrylonitrile <50.0 ug/L 50.0 EPA-624 11/13/2013

Benzene <5.0 ug/L 5.0 EPA-624 11/13/2013

Bromodichloromethane (Dichlorobromomethane) 5.9 ug/L 5.0 EPA-624 11/13/2013

Bromoform <5.0 ug/L 5.0 EPA-624 11/13/2013

Carbon Tetrachloride <5.0 ug/L 5.0 EPA-624 11/13/2013

Chlorobenzene <5.0 ug/L 5.0 EPA-624 11/13/2013

Chloroethane <10.0 ug/L 10.0 EPA-624 11/13/2013

2-Chloroethyl Vinyl Ether <10 ug/L 10 EPA-624 11/13/2013

Chloroform 20 ug/L 5.0 EPA-624 11/13/2013

Dibromochloromethane (Chlorodibromomethane)<5.0 ug/L 5.0 EPA-624 11/13/2013

1,2-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 11/13/2013



Dichlorodifluoromethane <10 ug/L 10 EPA-624 11/13/2013

1,1-Dichloroethane <5.0 ug/L 5.0 EPA-624 11/13/2013

1,2-Dichloroethane <5.0 ug/L 5.0 EPA-624 11/13/2013

1,1-Dichloroethene (1,1-dichloroethylene)<5.0 ug/L 5.0 EPA-624 11/13/2013

trans-1,2-Dichloroethene (1,2-dichloroethylene)<5.0 ug/L 5.0 EPA-624 11/13/2013

1,2-Dichloropropane <5.0 ug/L 5.0 EPA-624 11/13/2013

cis-1,3-Dichloropropene (1,3-dichloropropylene)<5.0 ug/L 5.0 EPA-624 11/13/2013

trans-1,3-Dichloropropene (1,3-dichloropropylene)<5.0 ug/L 5.0 EPA-624 11/13/2013

Ethylbenzene <5.0 ug/L 5.0 EPA-624 11/13/2013

Methyl Bromide (Bromomethane) <10.0 ug/L 10.0 EPA-624 11/13/2013

Methyl Chloride (Chloromethane) <10 ug/L 10 EPA-624 11/13/2013

Methylene Chloride <10 ug/L 10 EPA-624 11/13/2013

Tetrachloroethylene <5.0 ug/L 5.0 EPA-624 11/13/2013

1,1,2,2-Tetrachloroethane <5.0 ug/L 5.0 EPA-624 11/13/2013

Toluene <5.0 ug/L 5.0 EPA-624 11/13/2013

1,1,1-Trichloroethane <5.0 ug/L 5.0 EPA-624 11/13/2013

1,1,2-Trichloroethane <5.0 ug/L 5.0 EPA-624 11/13/2013

Trichloroethylene (Trichloroethene) <5.0 ug/L 5.0 EPA-624 11/13/2013

Trichlorofluoromethane <10 ug/L 10 EPA-624 11/13/2013

Vinyl Chloride <10 ug/L 10 EPA-624 11/13/2013

m,p-Xylene <5.0 ug/L 5.0 EPA-624 11/13/2013

o-Xylene <5.0 ug/L 5.0 EPA-624 11/13/2013

(Surrogate) 1,2-Dichloroethane d4 111.1 % EPA-624 11/13/2013 (53.6-137.7)

(Surrogate) Toluene d8 97.1 % EPA-624 11/13/2013 (69.7-120.9)

(Surrogate) 4-Bromofluorobenzene 100.7 % EPA-624 11/13/2013 (31.3-173.6)


29

Anomatic


February 2014

Parameter Result Units PQL Method of Analysis Prep Date Date of Analysis NotesAldrin <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Alpha-BHC <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Beta-BHC <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Delta-BHC <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Gamma-BHC (Lindane) <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Chlordane <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/20144,4'-DDT <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/20144,4'-DDE <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/20144,4'-DDD <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/2014Dieldrin <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/2014Alpha Endosulfan <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Beta Endosulfan <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/2014Endosulfan Sulfate <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/2014Endrin <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/2014Endrin Aldehyde <0.50 ug/L 0.50 EPA-608 02/20/2014 02/20/2014Heptachlor <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Heptachlor Epoxide <0.25 ug/L 0.25 EPA-608 02/20/2014 02/20/2014Methoxychlor <2.50 ug/L 2.50 EPA-608 02/20/2014 02/20/2014PCB-1016 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014PCB-1221 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014PCB-1232 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014PCB-1242 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014PCB-1248 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014PCB-1254 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014PCB-1260 <5.00 ug/L 5.00 EPA-608 02/20/2014 02/20/2014Toxaphene <12.5 ug/L 12.5 EPA-608 02/20/2014 02/20/2014 (Surrogate) TCMX 125.6 % EPA-608 02/20/2014 02/20/2014 (7.8-124.7)

Recovery of surrogate outside limit (bias high). Associated results were not affected.

(Surrogate) DCB 77.9 % EPA-608 02/20/2014 02/20/2014 (1.6-132.9)

Acrolein <50.0 ug/L 50.0 EPA-624 02/17/2014Acrylonitrile <50.0 ug/L 50.0 EPA-624 02/17/2014Benzene <5.0 ug/L 5.0 EPA-624 02/17/2014Bromodichloromethane (Dichlorobromomethane) <5.0 ug/L 5.0 EPA-624 02/17/2014Bromoform <5.0 ug/L 5.0 EPA-624 02/17/2014Carbon Tetrachloride <5.0 ug/L 5.0 EPA-624 02/17/2014Chlorobenzene <5.0 ug/L 5.0 EPA-624 02/17/2014Chloroethane <10.0 ug/L 10.0 EPA-624 02/17/20142-Chloroethyl Vinyl Ether <10 ug/L 10 EPA-624 02/17/2014Chloroform <5.0 ug/L 5.0 EPA-624 02/17/2014Dibromochloromethane (Chlorodibromomethane) <5.0 ug/L 5.0 EPA-624 02/17/20141,2-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 02/17/20141,3-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 02/17/20141,4-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 02/17/2014Dichlorodifluoromethane <10 ug/L 10 EPA-624 02/17/20141,1-Dichloroethane <5.0 ug/L 5.0 EPA-624 02/17/20141,2-Dichloroethane <5.0 ug/L 5.0 EPA-624 02/17/20141,1-Dichloroethene (1,1-dichloroethylene) <5.0 ug/L 5.0 EPA-624 02/17/2014trans-1,2-Dichloroethene (1,2-dichloroethylene) <5.0 ug/L 5.0 EPA-624 02/17/20141,2-Dichloropropane <5.0 ug/L 5.0 EPA-624 02/17/2014cis-1,3-Dichloropropene (1,3-dichloropropylene) <5.0 ug/L 5.0 EPA-624 02/17/2014trans-1,3-Dichloropropene (1,3-dichloropropylene) <5.0 ug/L 5.0 EPA-624 02/17/2014Ethylbenzene <5.0 ug/L 5.0 EPA-624 02/17/2014Methyl Bromide (Bromomethane) <10.0 ug/L 10.0 EPA-624 02/17/2014Methyl Chloride (Chloromethane) <10 ug/L 10 EPA-624 02/17/2014Methylene Chloride <10 ug/L 10 EPA-624 02/17/2014Tetrachloroethylene <5.0 ug/L 5.0 EPA-624 02/17/20141,1,2,2-Tetrachloroethane <5.0 ug/L 5.0 EPA-624 02/17/2014Toluene <5.0 ug/L 5.0 EPA-624 02/17/20141,1,1-Trichloroethane <5.0 ug/L 5.0 EPA-624 02/17/20141,1,2-Trichloroethane <5.0 ug/L 5.0 EPA-624 02/17/2014Trichloroethylene (Trichloroethene) <5.0 ug/L 5.0 EPA-624 02/17/2014Trichlorofluoromethane <10 ug/L 10 EPA-624 02/17/2014Vinyl Chloride <10 ug/L 10 EPA-624 02/17/2014m,p-Xylene <5.0 ug/L 5.0 EPA-624 02/17/2014o-Xylene <5.0 ug/L 5.0 EPA-624 02/17/2014 (Surrogate) 1,2-Dichloroethane d4 98.6 % EPA-624 02/17/2014 (53.6-137.7)


Parameter Result Units PQL Method of Analysis Prep Date Date of Analysis Notes (Surrogate) 4-Bromofluorobenzene 88.8 % EPA-624 02/17/2014 (31.3-173.6)

Acenaphthene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Acenaphthylene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Anthracene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Benzo(a)anthracene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Benzidine <50.0 ug/L 50.0 EPA-625 02/20/2014 02/24/2014Benzo(b)fluoranthene (3,4-benzofluoranthene) <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Benzo(k)fluoranthene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Benzo(g,h,i)perylene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Benzo(a)pyrene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014bis(2-chloroethoxy)Methane <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014bis(2-chloroethyl)Ether <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014bis(2-chloroisopropyl)Ether <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014bis(2-ethylhexyl)Phthalate 24 ug/L 5.0 EPA-625 02/20/2014 02/24/20144-Bromophenyl phenyl ether <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Butyl benzyl phthalate <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20142-Chloronaphthalene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20144-Chlorophenyl phenyl ether <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Chrysene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Dibenzo(a,h)anthracene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Di-n-butyl phthalate <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20143,3'-Dichlorobenzidine <20.0 ug/L 20.0 EPA-625 02/20/2014 02/24/2014Diethyl phthalate <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Dimethyl phthalate <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20142,4-Dinitrotoluene <20.0 ug/L 20.0 EPA-625 02/20/2014 02/24/20142,6-Dinitrotoluene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Di-n-octyl phthalate <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20141,2-Diphenylhydrazine <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Fluoranthene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Fluorene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Hexachlorobenzene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Hexachlorobutadiene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Hexachlorocyclopentadiene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Hexachloroethane <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Indeno(1,2,3-cd)pyrene <20.0 ug/L 20.0 EPA-625 02/20/2014 02/24/2014Isophorone <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Naphthalene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Nitrobenzene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014N-Nitrosodimethylamine <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014N-Nitrosodiphenylamine <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014N-Nitrosodi-n-propylamine <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Phenanthrene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/2014Pyrene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20141,2,4-Trichlorobenzene <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20144-Chloro-3-methylphenol (p-chloro-m-cresol) <50.0 ug/L 50.0 EPA-625 02/20/2014 02/24/20142-Chlorophenol <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20142,4-Dichlorophenol <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20142,4-Dimethylphenol <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20142,4-Dinitrophenol <50.0 ug/L 50.0 EPA-625 02/20/2014 02/24/20142-Methyl-4,6-dinitrophenol (4,6-dinitro-o-cresol) <50.0 ug/L 50.0 EPA-625 02/20/2014 02/24/20142-Nitrophenol <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20144-Nitrophenol <50.0 ug/L 50.0 EPA-625 02/20/2014 02/24/2014Pentachlorophenol <50.0 ug/L 50.0 EPA-625 02/20/2014 02/24/2014Phenol <10.0 ug/L 10.0 EPA-625 02/20/2014 02/24/20142,4,6-Trichlorophenol <20.0 ug/L 20.0 EPA-625 02/20/2014 02/24/2014 Reported as an estimate due to 2 or more surrogate recoveries falling outside established limits.

(Surrogate) 2-Fluorophenol 0.1 % EPA-625 02/20/2014 02/24/2014 (3.2-64.3)Result is outside established limits.

(Surrogate) Phenol d6 0.3 % EPA-625 02/20/2014 02/24/2014 (D-48.1)


(Surrogate) 2-Fluorobiphenyl 39.0 % EPA-625 02/20/2014 02/24/2014 (D-131.4)

(Surrogate) 2,4,6-Tribromophenol 0.4 % EPA-625 02/20/2014 02/24/2014 (6.6-127.4)Result is outside established limits.




624/8260 Library Search * Y/N 624/8260 TIC 02/17/2014 Non Detect

Chromium, Hexavalent <0.100 mg/L 0.100 SM-3500-Cr B 02/14/2014 Higher detection level due to sample matrix.

32

Anomatic


June 2014

Parameter Result Units PQL Method of Analysis Prep Date Date of AnalysisAldrin <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Alpha-BHC <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Beta-BHC <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Delta-BHC <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Gamma-BHC (Lindane) <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Chlordane <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/20144,4'-DDT <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/20144,4'-DDE <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/20144,4'-DDD <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/2014Dieldrin <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/2014Alpha Endosulfan <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Beta Endosulfan <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/2014Endosulfan Sulfate <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/2014Endrin <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/2014Endrin Aldehyde <0.50 ug/L 0.50 EPA-608 06/10/2014 06/12/2014Heptachlor <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Heptachlor Epoxide <0.25 ug/L 0.25 EPA-608 06/10/2014 06/12/2014Methoxychlor <2.50 ug/L 2.50 EPA-608 06/10/2014 06/12/2014PCB-1016 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014PCB-1221 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014PCB-1232 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014PCB-1242 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014PCB-1248 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014PCB-1254 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014PCB-1260 <5.00 ug/L 5.00 EPA-608 06/10/2014 06/12/2014Toxaphene <12.5 ug/L 12.5 EPA-608 06/10/2014 06/12/2014 (Surrogate) TCMX 79.8 % EPA-608 06/10/2014 06/12/2014 (Surrogate) DCB 31.8 % EPA-608 06/10/2014 06/12/2014Acrolein <50.0 ug/L 50.0 EPA-624 06/06/2014Acrylonitrile <50.0 ug/L 50.0 EPA-624 06/06/2014Benzene <5.0 ug/L 5.0 EPA-624 06/06/2014Bromodichloromethane (Dichlorobromomethane) 7.0 ug/L 5.0 EPA-624 06/06/2014Bromoform <5.0 ug/L 5.0 EPA-624 06/06/2014Carbon Tetrachloride <5.0 ug/L 5.0 EPA-624 06/06/2014Chlorobenzene <5.0 ug/L 5.0 EPA-624 06/06/2014Chloroethane <10.0 ug/L 10.0 EPA-624 06/06/20142-Chloroethyl Vinyl Ether <10 ug/L 10 EPA-624 06/06/2014Chloroform 18 ug/L 5.0 EPA-624 06/06/2014Dibromochloromethane (Chlorodibromomethane) <5.0 ug/L 5.0 EPA-624 06/06/20141,2-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 06/06/20141,3-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 06/06/20141,4-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 06/06/2014Dichlorodifluoromethane <10 ug/L 10 EPA-624 06/06/20141,1-Dichloroethane <5.0 ug/L 5.0 EPA-624 06/06/20141,2-Dichloroethane <5.0 ug/L 5.0 EPA-624 06/06/20141,1-Dichloroethene (1,1-dichloroethylene) <5.0 ug/L 5.0 EPA-624 06/06/2014trans-1,2-Dichloroethene (1,2-dichloroethylene) <5.0 ug/L 5.0 EPA-624 06/06/20141,2-Dichloropropane <5.0 ug/L 5.0 EPA-624 06/06/2014cis-1,3-Dichloropropene (1,3-dichloropropylene) <5.0 ug/L 5.0 EPA-624 06/06/2014trans-1,3-Dichloropropene (1,3-dichloropropylene) <5.0 ug/L 5.0 EPA-624 06/06/2014Ethylbenzene <5.0 ug/L 5.0 EPA-624 06/06/2014Methyl Bromide (Bromomethane) <10.0 ug/L 10.0 EPA-624 06/06/2014Methyl Chloride (Chloromethane) <10 ug/L 10 EPA-624 06/06/2014Methylene Chloride <10 ug/L 10 EPA-624 06/06/2014Tetrachloroethylene <5.0 ug/L 5.0 EPA-624 06/06/20141,1,2,2-Tetrachloroethane <5.0 ug/L 5.0 EPA-624 06/06/2014Toluene <5.0 ug/L 5.0 EPA-624 06/06/20141,1,1-Trichloroethane <5.0 ug/L 5.0 EPA-624 06/06/20141,1,2-Trichloroethane <5.0 ug/L 5.0 EPA-624 06/06/2014Trichloroethylene (Trichloroethene) <5.0 ug/L 5.0 EPA-624 06/06/2014Trichlorofluoromethane <10 ug/L 10 EPA-624 06/06/2014Vinyl Chloride <10 ug/L 10 EPA-624 06/06/2014m,p-Xylene <5.0 ug/L 5.0 EPA-624 06/06/2014o-Xylene <5.0 ug/L 5.0 EPA-624 06/06/2014 (Surrogate) 1,2-Dichloroethane d4 104.5 % EPA-624 06/06/2014 (Surrogate) Toluene d8 89.6 % EPA-624 06/06/2014 (Surrogate) 4-Bromofluorobenzene 93.9 % EPA-624 06/06/2014Acenaphthene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Acenaphthylene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014

Parameter Result Units PQL Method of Analysis Prep Date Date of AnalysisAnthracene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Benzo(a)anthracene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Benzidine <50.0 ug/L 50.0 EPA-625 06/10/2014 06/11/2014Benzo(b)fluoranthene (3,4-benzofluoranthene) <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Benzo(k)fluoranthene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Benzo(g,h,i)perylene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Benzo(a)pyrene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014bis(2-chloroethoxy)Methane <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014bis(2-chloroethyl)Ether <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014bis(2-chloroisopropyl)Ether <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014bis(2-ethylhexyl)Phthalate 6.4 ug/L 5.0 EPA-625 06/10/2014 06/11/20144-Bromophenyl phenyl ether <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Butyl benzyl phthalate <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20142-Chloronaphthalene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20144-Chlorophenyl phenyl ether <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Chrysene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Dibenzo(a,h)anthracene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Di-n-butyl phthalate <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20143,3'-Dichlorobenzidine <20.0 ug/L 20.0 EPA-625 06/10/2014 06/11/2014Diethyl phthalate <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Dimethyl phthalate <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20142,4-Dinitrotoluene <20.0 ug/L 20.0 EPA-625 06/10/2014 06/11/20142,6-Dinitrotoluene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Di-n-octyl phthalate <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20141,2-Diphenylhydrazine <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Fluoranthene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Fluorene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Hexachlorobenzene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Hexachlorobutadiene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Hexachlorocyclopentadiene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Hexachloroethane <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Indeno(1,2,3-cd)pyrene <20.0 ug/L 20.0 EPA-625 06/10/2014 06/11/2014Isophorone <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Naphthalene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Nitrobenzene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014N-Nitrosodimethylamine <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014N-Nitrosodiphenylamine <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014N-Nitrosodi-n-propylamine <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Phenanthrene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/2014Pyrene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20141,2,4-Trichlorobenzene <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20144-Chloro-3-methylphenol (p-chloro-m-cresol) <50.0 ug/L 50.0 EPA-625 06/10/2014 06/11/20142-Chlorophenol <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20142,4-Dichlorophenol <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20142,4-Dimethylphenol <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20142,4-Dinitrophenol <50.0 ug/L 50.0 EPA-625 06/10/2014 06/11/20142-Methyl-4,6-dinitrophenol (4,6-dinitro-o-cresol) <50.0 ug/L 50.0 EPA-625 06/10/2014 06/11/20142-Nitrophenol <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20144-Nitrophenol <50.0 ug/L 50.0 EPA-625 06/10/2014 06/11/2014Pentachlorophenol <50.0 ug/L 50.0 EPA-625 06/10/2014 06/11/2014Phenol <10.0 ug/L 10.0 EPA-625 06/10/2014 06/11/20142,4,6-Trichlorophenol <20.0 ug/L 20.0 EPA-625 06/10/2014 06/11/2014 (Surrogate) 2-Fluorophenol 0.0 % EPA-625 06/10/2014 06/11/2014

(Surrogate) Phenol d6 0.1 % EPA-625 06/10/2014 06/11/2014 (Surrogate) Nitrobenzene d5 62.4 % EPA-625 06/10/2014 06/11/2014

(Surrogate) 2-Fluorobiphenyl 62.6 % EPA-625 06/10/2014 06/11/2014

(Surrogate) 2,4,6-Tribromophenol 0.0 % EPA-625 06/10/2014 06/11/2014

(Surrogate) p-Terphenyl-d14 76.6 % EPA-625 06/10/2014 06/11/2014Dioxin Screen * Y/N 625/8270DIOX 06/11/2014625/8270 Library Search * Y/N 625/8270 TIC 06/11/2014624/8260 Library Search * Y/N 624/8260 TIC 06/06/2014

35

Anomatic


September 2014

Parameter Result Units PQL Method of Analysis Prep Date Date of Analysis NotesAldrin <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Alpha-BHC <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Beta-BHC <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Delta-BHC <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Gamma-BHC (Lindane) <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Chlordane <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/20144,4'-DDT <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/20144,4'-DDE <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/20144,4'-DDD <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/2014Dieldrin <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/2014Alpha Endosulfan <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Beta Endosulfan <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/2014Endosulfan Sulfate <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/2014Endrin <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/2014Endrin Aldehyde <0.50 ug/L 0.50 EPA-608 09/12/2014 09/15/2014Heptachlor <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Heptachlor Epoxide <0.25 ug/L 0.25 EPA-608 09/12/2014 09/15/2014Methoxychlor <2.50 ug/L 2.50 EPA-608 09/12/2014 09/15/2014PCB-1016 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014PCB-1221 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014PCB-1232 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014PCB-1242 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014PCB-1248 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014PCB-1254 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014PCB-1260 <5.00 ug/L 5.00 EPA-608 09/12/2014 09/15/2014Toxaphene <12.5 ug/L 12.5 EPA-608 09/12/2014 09/15/2014 (Surrogate) TCMX 90.0 % EPA-608 09/12/2014 09/15/2014 (7.8-124.7)

(Surrogate) DCB 49.6 % EPA-608 09/12/2014 09/15/2014 (1.6-132.9)

Acrolein <50.0 ug/L 50.0 EPA-624 09/12/2014Acrylonitrile <50.0 ug/L 50.0 EPA-624 09/12/2014Benzene <5.0 ug/L 5.0 EPA-624 09/12/2014Bromodichloromethane (Dichlorobromomethane) 5.6 ug/L 5.0 EPA-624 09/12/2014Bromoform <5.0 ug/L 5.0 EPA-624 09/12/2014Carbon Tetrachloride <5.0 ug/L 5.0 EPA-624 09/12/2014Chlorobenzene <5.0 ug/L 5.0 EPA-624 09/12/2014Chloroethane <10.0 ug/L 10.0 EPA-624 09/12/20142-Chloroethyl Vinyl Ether <10 ug/L 10 EPA-624 09/12/2014Chloroform 8.9 ug/L 5.0 EPA-624 09/12/2014Dibromochloromethane (Chlorodibromomethane) <5.0 ug/L 5.0 EPA-624 09/12/20141,2-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 09/12/20141,3-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 09/12/20141,4-Dichlorobenzene <5.0 ug/L 5.0 EPA-624 09/12/2014Dichlorodifluoromethane <10 ug/L 10 EPA-624 09/12/20141,1-Dichloroethane <5.0 ug/L 5.0 EPA-624 09/12/20141,2-Dichloroethane <5.0 ug/L 5.0 EPA-624 09/12/20141,1-Dichloroethene (1,1-dichloroethylene) <5.0 ug/L 5.0 EPA-624 09/12/2014trans-1,2-Dichloroethene (1,2-dichloroethylene) <5.0 ug/L 5.0 EPA-624 09/12/20141,2-Dichloropropane <5.0 ug/L 5.0 EPA-624 09/12/2014cis-1,3-Dichloropropene (1,3-dichloropropylene) <5.0 ug/L 5.0 EPA-624 09/12/2014trans-1,3-Dichloropropene (1,3-dichloropropylene) <5.0 ug/L 5.0 EPA-624 09/12/2014Ethylbenzene <5.0 ug/L 5.0 EPA-624 09/12/2014Methyl Bromide (Bromomethane) <10.0 ug/L 10.0 EPA-624 09/12/2014Methyl Chloride (Chloromethane) <10 ug/L 10 EPA-624 09/12/2014Methylene Chloride <10 ug/L 10 EPA-624 09/12/2014Tetrachloroethylene <5.0 ug/L 5.0 EPA-624 09/12/20141,1,2,2-Tetrachloroethane <5.0 ug/L 5.0 EPA-624 09/12/2014Toluene <5.0 ug/L 5.0 EPA-624 09/12/20141,1,1-Trichloroethane <5.0 ug/L 5.0 EPA-624 09/12/20141,1,2-Trichloroethane <5.0 ug/L 5.0 EPA-624 09/12/2014Trichloroethylene (Trichloroethene) <5.0 ug/L 5.0 EPA-624 09/12/2014Trichlorofluoromethane <10 ug/L 10 EPA-624 09/12/2014Vinyl Chloride <10 ug/L 10 EPA-624 09/12/2014m,p-Xylene <5.0 ug/L 5.0 EPA-624 09/12/2014o-Xylene <5.0 ug/L 5.0 EPA-624 09/12/2014 (Surrogate) 1,2-Dichloroethane d4 106.8 % EPA-624 09/12/2014 (61.3-143.8)


(Surrogate) 4-Bromofluorobenzene 99.1 % EPA-624 09/12/2014 (65.7-134.0)

Acenaphthene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Acenaphthylene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014

Parameter Result Units PQL Method of Analysis Prep Date Date of Analysis NotesAnthracene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Benzo(a)anthracene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Benzidine <50.0 ug/L 50.0 EPA-625 09/16/2014 09/18/2014Benzo(b)fluoranthene (3,4-benzofluoranthene) <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Benzo(k)fluoranthene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Benzo(g,h,i)perylene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Benzo(a)pyrene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014bis(2-chloroethoxy)Methane <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014bis(2-chloroethyl)Ether <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014bis(2-chloroisopropyl)Ether <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014bis(2-ethylhexyl)Phthalate 17.2 ug/L 5.0 EPA-625 09/16/2014 09/18/20144-Bromophenyl phenyl ether <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Butyl benzyl phthalate <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20142-Chloronaphthalene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20144-Chlorophenyl phenyl ether <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Chrysene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Dibenzo(a,h)anthracene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Di-n-butyl phthalate <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20143,3'-Dichlorobenzidine <20.0 ug/L 20.0 EPA-625 09/16/2014 09/18/2014Diethyl phthalate <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Dimethyl phthalate <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20142,4-Dinitrotoluene <20.0 ug/L 20.0 EPA-625 09/16/2014 09/18/20142,6-Dinitrotoluene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Di-n-octyl phthalate <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20141,2-Diphenylhydrazine <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Fluoranthene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Fluorene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Hexachlorobenzene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Hexachlorobutadiene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Hexachlorocyclopentadiene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Hexachloroethane <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Indeno(1,2,3-cd)pyrene <20.0 ug/L 20.0 EPA-625 09/16/2014 09/18/2014Isophorone <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Naphthalene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Nitrobenzene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014N-Nitrosodimethylamine <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014N-Nitrosodiphenylamine <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014N-Nitrosodi-n-propylamine <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Phenanthrene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/2014Pyrene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20141,2,4-Trichlorobenzene <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20144-Chloro-3-methylphenol (p-chloro-m-cresol) <50.0 ug/L 50.0 EPA-625 09/16/2014 09/18/20142-Chlorophenol <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20142,4-Dichlorophenol <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20142,4-Dimethylphenol <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20142,4-Dinitrophenol <50.0 ug/L 50.0 EPA-625 09/16/2014 09/18/20142-Methyl-4,6-dinitrophenol (4,6-dinitro-o-cresol) <50.0 ug/L 50.0 EPA-625 09/16/2014 09/18/20142-Nitrophenol <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20144-Nitrophenol <50.0 ug/L 50.0 EPA-625 09/16/2014 09/18/2014Pentachlorophenol <50.0 ug/L 50.0 EPA-625 09/16/2014 09/18/2014Phenol <10.0 ug/L 10.0 EPA-625 09/16/2014 09/18/20142,4,6-Trichlorophenol <20.0 ug/L 20.0 EPA-625 09/16/2014 09/18/2014 Reported as an estimate due to 2 or more surrogate recoveries falling outside established limits.

(Surrogate) 2-Fluorophenol 1.8 % EPA-625 09/16/2014 09/18/2014 (D-54.9)

(Surrogate) Phenol d6 <0.1 % EPA-625 09/16/2014 09/18/2014 (D-62.5)Result is outside established limits.


(Surrogate) 2-Fluorobiphenyl 73.2 % EPA-625 09/16/2014 09/18/2014 (18.8-91.3)

(Surrogate) 2,4,6-Tribromophenol <0.1 % EPA-625 09/16/2014 09/18/2014 (14.3-110.3)Result is outside established limits.





Chromium, Hexavalent <0.010 mg/L 0.010 SM-3500-Cr B 09/10/2014

38

Owens Corning

Priority Pollutants

March 2014