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CHEM 213 Experiment: Column Chromatography

CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

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Page 1: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

CHEM213Experiment:ColumnChromatography

Page 2: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

Page 3: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

Page 4: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

Page 5: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

Procedure:Youwillbeseparatingthemixturethatresultsfromthereactionbelow:

Inthisparticularexperiment,theoxidationisincompleteandyouhaveamixtureoffluoreneandfluorenonetoseparate.Objectives:

• Separatethetwocomponentsbycolumnchromatography.• Identifyeachcomponent

• Determinethemassofeachcomponent

Step1:Weighout~50mgofthemixture.Useabalanceoutsideofhoodtoeliminatetheindicatedmassfrombeingaffectedbytheairflow.FollowtheprocedurefromWilliamsonasfollows:

Page 6: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

Page 7: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

Page 8: CHEM 213 Experiment: Column Chromatographychemistry.bd.psu.edu/justik/CHEM 213/CHEM 213 Experiment... · CHAPTER Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene,

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