Upload
others
View
0
Download
0
Embed Size (px)
Citation preview
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
03/30/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsPrism 1.5g Pre-Roll
PrismMatrix: Flower
Certificateof Analysis
Sample:DA10326004-002Harvest/Lot ID: 9192 7383 2041 8985
Cultivation Facility: Tampa CultivationProcessing Facility : Tampa Processing
Seed to Sale #9192 7383 2041 8985Batch Date :03/11/21
Batch#: 8981 1664 7491 6523Sample Size Received: 27 gramTotal Weight/Volume: 568 units
Retail Product Size: 1.5 gramOrdered : 03/25/21sampled : 03/25/21
Completed: 03/30/21 Expires: 03/30/22Sampling Method: SOP.T.20.010
Mar 30, 2021 | FLUENT82 NE 26th streetMiami, FL, 33330, US
PASSEDPage 1 of 4
PRODUCT IMAGE SAFETY RESULTS MISC.
PesticidesPASSED
Heavy MetalsPASSED
MicrobialsPASSED
MycotoxinsPASSED
ResidualsSolvents
NOT TESTED
FilthPASSED
Water ActivityPASSED
MoisturePASSED
TerpenesTESTED
CANNABINOID RESULTS
Total THC
14.263%TOTAL THC/Container :213.958mg
Total CBD
0.056%TOTAL CBD/Container :0.842 mg
Total Cannabinoids
17.239%Total Cannabinoids/Container:258.585 mg
CBDV CBDA CBGA CBG CBD THCV CBN D9-THC D8-THC CBC THCA
ND 0.064% 0.828% 0.074% ND ND ND 0.238% 0.024% 0.018%15.993%
ND0.640mg/g
8.280mg/g
0.740mg/g ND ND ND
2.380mg/g
0.240mg/g
0.180mg/g
159.930mg/g
LOD 0.001 0.001 0.001 0.001 0.0001 0.001 0.001 0.0001 0.001 0.001 0.001
% % % % % % % % % % %
Cannabinoid Profile TestAnalyzed by Weight Extraction date : Extracted By :450 0.207g 03/26/21 01:03:58 1823Analysis Method -SOP.T.40.020, SOP.T.30.050 Reviewed On - 03/29/21 11:57:48 Batch Date : 03/26/21 10:03:53Analytical Batch -DA024348POT Instrument Used : DA-LC-002
Reagent Dilution Consums. ID
032621.R29 400 287035261030921.31 11945-019CD-019C032221.R53 76262-590
914C4-914AK929C6-929H
Full spectrum cannabinoid analysis utilizing High Performance Liquid Chromatography with UV detection (HPLC-UV). (Method: SOP.T.30.050 forsample prep and Shimadzu High Sensitivity Method SOP.T.40.020 for analysis. LOQ for all cannabinoids is 1 mg/L).
Filth PASSEDAnalyzed By Weight Extraction date Extracted By457 NA NA NAAnalyte LOD ResultFilth and Foreign Material 0.1 NDAnalysis Method -SOP.T.40.013 Batch Date : 03/26/21 11:43:22Analytical Batch -DA024363FIL Reviewed On - 03/26/21 11:56:25Instrument Used : Filth/Foreign Material Microscope
This includes but is not limited to hair, insects, feces, packaging contaminants, and manufacturing wasteand by-products. An SH-2B/T Stereo Microscope is use for inspection.
Water Activity PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultWATER ACTIVITY 457 NA NA 0.01 aw 0.65aw 0.438aWAnalysis Method -Water ActivitySOP.T.40.010 Batch Date : 03/26/21 10:27:11Analytical Batch -DA024354WAT Reviewed On - 03/26/21 13:53:36Instrument Used : DA-028 Rotronic Hygropalm
Moisture PASSEDAnalyte Analyzed by Weight Ext. date LOD A.L ResultMOISTURE CONTENT 457 NA NA 1 % 15% 9.520%
Analysis Method -MoistureAnalysis SOP.T.40.011 Batch Date : 03/26/21 10:24:54Analytical Batch -DA024353MOI Reviewed On - 03/26/21 14:47:49Instrument Used : DA-003 Moisture Analyzer
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
03/30/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsPrism 1.5g Pre-Roll
PrismMatrix : Flower
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33330, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10326004-002Harvest/LOT ID: 9192 7383 2041 8985Batch# : 8981 16647491 6523Sampled : 03/25/21Ordered : 03/25/21
Sample Size Received : 27 gramTotal Weight/Volume : 568 unitsCompleted : 03/30/21Expires: 03/30/22Sample Method : SOP.T.20.010
Page 2 of 4
Terpenes TESTEDTerpenes LOD (%) mg/g % Result (%)
CAMPHENE 0.007 ND NDBETA-MYRCENE 0.007 0.789 0.078ALPHA-PHELLANDRENE
0.007 ND ND
3-CARENE 0.007 ND NDOCIMENE 0.007 ND NDEUCALYPTOL 0.007 ND NDLINALOOL 0.007 0.973 0.097FENCHONE 0.007 ND NDISOPULEGOL 0.007 ND NDISOBORNEOL 0.007 ND NDHEXAHYDROTHYMOL
0.007 ND ND
NEROL 0.007 ND NDGERANYL ACETATE 0.007 ND NDBETA-CARYOPHYLLENE
0.007 2.321 0.232
VALENCENE 0.007 ND NDCIS-NEROLIDOL 0.007 ND NDCARYOPHYLLENEOXIDE
0.007 ND ND
CEDROL 0.007 ND NDFARNESENE 0.007 2.006 0.200ALPHA-BISABOLOL 0.007 0.436 0.043ALPHA-PINENE 0.007 0.426 0.042SABINENE 0.007 ND NDBETA-PINENE 0.007 0.438 0.043ALPHA-TERPINENE 0.007 ND NDLIMONENE 0.007 2.264 0.226GAMMA-TERPINENE
0.007 ND ND
TERPINOLENE 0.007 0.079 0.007SABINENEHYDRATE
0.007 ND ND
FENCHYL ALCOHOL 0.007 0.304 0.030CAMPHOR 0.013 ND NDBORNEOL 0.013 < 0.4 < 0.040
Terpenes LOD(%) mg/g % Result (%)
TERPINEOL 0.007 0.366 0.036GERANIOL 0.007 ND NDPULEGONE 0.007 ND NDALPHA-CEDRENE 0.007 ND NDALPHA-HUMULENE 0.007 0.736 0.073TRANS-NEROLIDOL 0.007 < 0.2 < 0.020GUAIOL 0.007 ND ND
Terpenes TESTED
Analyzed by Weight Extraction date Extracted By1351 0.9779g 03/26/21 11:03:48 1351
Analysis Method -SOP.T.40.090Analytical Batch -DA024359TER Reviewed On - 03/28/21 15:15:07Instrument Used : DA-GCMS-005Running On :Batch Date : 03/26/21 10:52:33
Reagent Dilution Consums. ID
032521.R01 10 2870352611249940276262-590
Terpenoid profile screening is performed using GC-MS with Liquid Injection(Gas Chromatography – Mass Spectrometer) which can screen 38 terpenesusing Method SOP.T.40.091 Terpenoid Analysis Via GC/MS.
Total (%) 1.106
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
03/30/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsPrism 1.5g Pre-Roll
PrismMatrix : Flower
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33330, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10326004-002Harvest/LOT ID: 9192 7383 2041 8985Batch# : 8981 16647491 6523Sampled : 03/25/21Ordered : 03/25/21
Sample Size Received : 27 gramTotal Weight/Volume : 568 unitsCompleted : 03/30/21Expires: 03/30/22Sample Method : SOP.T.20.010
Page 3 of 4
Pesticides PASSEDPesticides LOD Units Action Level ResultABAMECTIN B1A 0.01 ppm 0.1 NDACEPHATE 0.01 ppm 0.1 NDACEQUINOCYL 0.01 ppm 0.1 NDACETAMIPRID 0.01 ppm 0.1 NDALDICARB 0.01 ppm 0.1 NDAZOXYSTROBIN 0.01 ppm 0.1 NDBIFENAZATE 0.01 ppm 0.1 NDBIFENTHRIN 0.01 ppm 0.1 NDBOSCALID 0.01 PPM 0.1 NDCARBARYL 0.05 ppm 0.5 NDCARBOFURAN 0.01 ppm 0.1 NDCHLORANTRANILIPROLE 0.1 ppm 1 NDCHLORMEQUAT CHLORIDE 0.1 ppm 1 NDCHLORPYRIFOS 0.01 ppm 0.1 NDCLOFENTEZINE 0.02 ppm 0.2 NDCOUMAPHOS 0.01 ppm 0.1 NDDAMINOZIDE 0.01 ppm 0.1 NDDICHLORVOS 0.01 ppm 0.1 NDDIMETHOATE 0.01 ppm 0.1 NDETHOPROPHOS 0.01 ppm 0.1 NDETOFENPROX 0.01 ppm 0.1 NDETOXAZOLE 0.01 ppm 0.1 NDFENHEXAMID 0.01 ppm 0.1 NDFENOXYCARB 0.01 ppm 0.1 NDFENPYROXIMATE 0.01 ppm 0.1 NDFIPRONIL 0.01 ppm 0.1 NDFLONICAMID 0.01 ppm 0.1 NDFLUDIOXONIL 0.01 ppm 0.1 NDHEXYTHIAZOX 0.01 ppm 0.1 NDIMAZALIL 0.01 ppm 0.1 NDIMIDACLOPRID 0.04 ppm 0.4 NDKRESOXIM-METHYL 0.01 ppm 0.1 NDMALATHION 0.02 ppm 0.2 NDMETALAXYL 0.01 ppm 0.1 NDMETHIOCARB 0.01 ppm 0.1 NDMETHOMYL 0.01 ppm 0.1 NDMEVINPHOS 0.01 ppm 0.1 NDMYCLOBUTANIL 0.01 ppm 0.1 NDNALED 0.025 ppm 0.25 NDOXAMYL 0.05 ppm 0.5 NDPACLOBUTRAZOL 0.01 ppm 0.1 NDPHOSMET 0.01 ppm 0.1 NDPIPERONYL BUTOXIDE 0.3 ppm 3 NDPRALLETHRIN 0.01 ppm 0.1 NDPROPICONAZOLE 0.01 ppm 0.1 NDPROPOXUR 0.01 ppm 0.1 ND
Pesticides LOD Units Action Level ResultPYRETHRINS 0.05 ppm 0.5 NDPYRIDABEN 0.02 ppm 0.2 NDSPIROMESIFEN 0.01 ppm 0.1 NDSPIROTETRAMAT 0.01 ppm 0.1 NDSPIROXAMINE 0.01 ppm 0.1 NDTEBUCONAZOLE 0.01 ppm 0.1 NDTHIACLOPRID 0.01 ppm 0.1 NDTHIAMETHOXAM 0.05 ppm 0.5 NDTOTAL CONTAMINANT LOAD(PESTICIDES)
0.01 PPM 5 ND
TOTAL DIAZINON 0.01 PPM 0.1 NDTOTAL DIMETHOMORPH 0.02 PPM 0.2 NDTOTAL PERMETHRIN 0.01 ppm 0.1 NDTOTAL SPINETORAM 0.02 PPM 0.2 NDTOTAL SPINOSAD 0.01 ppm 0.1 NDTRIFLOXYSTROBIN 0.01 ppm 0.1 NDPENTACHLORONITROBENZENE (PCNB)*
0.01 PPM 0.15 ND
PARATHION-METHYL * 0.01 PPM 0.1 NDCAPTAN * 0.025 PPM 0.7 NDCHLORDANE * 0.01 PPM 0.1 NDCHLORFENAPYR * 0.01 PPM 0.1 NDCYFLUTHRIN * 0.01 PPM 0.5 NDCYPERMETHRIN * 0.01 PPM 0.5 ND
Pesticides PASSED
Analyzed by Weight Extraction date Extracted By585 , 1665 1.0439g 03/26/21 01:03:35 585 , 585Analysis Method - SOP.T.30.065, SOP.T.40.065, SOP.T.40.066, SOP.T.40.070 , SOP.T.30.065,SOP.T40.070Analytical Batch - DA024339PES , DA024334VOL Reviewed On- 03/26/21
11:56:25Instrument Used : DA-LCMS-003 (PES) , DA-GCMS-006Running On : 03/26/21 15:09:21 , 03/26/21 14:32:51 Batch Date : 03/26/21 09:44:01
Reagent Dilution Consums. ID010421.R86 25 6524407-03123020.R30031721.R08032421.R07092820.59
Pesticide screen is performed using LC-MS and/or GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Currently we analyze for 67 Pesticides. (Method: SOP.T.30.060Sample Preparation for Pesticides Analysis via LCMSMS and GCMSMS.SOP.T40.065/SOP.T.40.066/SOP.T.40.070 Procedure for Pesticide Quantification Using LCMS and GCMS). *Volatile Pesticide screening is performed using GC-MS which can screen down to below single digit ppbconcentrations for regulated Pesticides. Analytes marked with an asterisk were tested using GC-MS.
This report shall not be reproduced, unless in its entirety, without written approval from Kaycha Labs. This report isan Kaycha Labs certification. The results relate only to the material or product analyzed. Test results areconfidential unless explicitly waived otherwise. Void after 1 year from test end date. Cannabinoid content of batchmaterial may vary depending on sampling error. IC=In-control QC parameter, NC=Non-controlled QC parameter,ND=Not Detected, NA=Not Analyzed, ppm=Parts Per Million, ppb=Parts Per Billion. Limit of Detection (LoD) andLimit Of Quantitation (LoQ) are terms used to describe the smallest concentration that can be reliably measured byan analytical procedure. RPD=Reproducibility of two measurements. Action Levels are State determined thresholdsfor human safety for consumption and/or inhalation. The result >99% are variable based on uncertainty ofmeasurement (UM) for the analyte. The UM error is available from the lab upon request.The "Decision Rule" for thepass/fail does not include the UM. The limits are based on F.S. Rule 64-4.310.
Jorge SegredoLab Director
State License # CMTL-0002ISO Accreditation # ISO/IEC17025:2017 Accreditation
PJLA-Testing 97164
___________________Signature
03/30/2021
___________________Signed On
4131 SW 47th AVENUE SUITE 1408DAVIE, FL, 33314, US
Kaycha LabsPrism 1.5g Pre-Roll
PrismMatrix : Flower
Certificate of Analysis PASSEDFLUENT
82 NE 26th streetMiami, FL, 33330, USTelephone: (305) 900-6266Email: [email protected]
Sample : DA10326004-002Harvest/LOT ID: 9192 7383 2041 8985Batch# : 8981 16647491 6523Sampled : 03/25/21Ordered : 03/25/21
Sample Size Received : 27 gramTotal Weight/Volume : 568 unitsCompleted : 03/30/21Expires: 03/30/22Sample Method : SOP.T.20.010
Page 4 of 4
Microbials PASSED
Analyte LOD Result Action Level (cfu/g)ESCHERICHIA_COLI_SHIGELLA_SPP not present in 1 gram.SALMONELLA_SPECIFIC_GENE not present in 1 gram.ASPERGILLUS_FLAVUS not present in 1 gram.ASPERGILLUS_FUMIGATUS not present in 1 gram.ASPERGILLUS_TERREUS not present in 1 gram.ASPERGILLUS_NIGER not present in 1 gram.TOTAL YEAST AND MOLD 10 35000 CFU 100000
Analysis Method -SOP.T.40.043 / SOP.T.40.044 / SOP.T.40.041Analytical Batch -DA024328MIC , DA024326TYM Batch Date : 03/26/21, 03/26/21Instrument Used : PathogenDx Scanner DA-111, PathogenDx Scanner DA-111Running On :
Analyzed by Weight Extraction date Extracted By513, 513 2.0009g 03/26/21 513,
Reagent Consums. ID Consums. ID Consums. ID Consums. ID032421.12101420.21
200103-2743110001001TH093G11989-024CC-0242804029
2803033D012D011A15A122807014
2810026A040280403228080092811021918C4-918J
20324012020200507119C914C4-914AK929C6-929H
Microbiological testing for Fungal and Bacterial Identification via Polymerase Chain Reaction (PCR) methodconsisting of sample DNA amplified via tandem Polymerase Chain Reaction (PCR) as a crude lysate which avoidspurification. (Method SOP.T.40.043) If a pathogenic Escherichia Coli, Salmonella, Aspergillus fumigatus,Aspergillus flavus, Aspergillus niger, or Aspergillus terreus is detected in 1g of a sample, the sample fails themicrobiological-impurity testing. Pour-plating is used for quantitation and confirmation, Total Yeast and Mold hasan action limit of 100,000 CFU.
Mycotoxins PASSED
Analyte LOD Units Result Action Level (PPM)AFLATOXIN G2 0.002 ppm ND 0.02AFLATOXIN G1 0.002 ppm ND 0.02AFLATOXIN B2 0.002 ppm ND 0.02AFLATOXIN B1 0.002 ppm ND 0.02TOTAL OCHRATOXIN A 0.002 PPM ND 0.02
Analysis Method -SOP.T.30.065, SOP.T.40.065Analytical Batch -DA024341MYC | Reviewed On - 03/29/21 13:27:54Instrument Used :Running On : 03/26/21 15:11:19Batch Date : 03/26/21 09:46:06
Analyzed by Weight Extraction date Extracted By585 NA 03/26/21 01:03:39 585
Aflatoxins B1, B2, G1, G2, and Ochratoxins A testing using LC-MS. (Method: SOP.T.30.065 forSample Preparation and SOP.T40.065 Procedure for Mycotoxins Quantification Using LCMS. LOQ 1.0ppb). Aflatoxin B1, B2, G1, and G2 must individually be <20ug/Kg. Ochratoxins must be <20µg/Kg.
Heavy Metals PASSED
Reagent Reagent Reagent Dilution Consums. ID032521.R12031921.R21031721.R16032221.R51032521.R13040521.R01
030121.R42031621.R35032221.R09121420.01090420.14030420.08
030121.26 100 89401-566
Metal LOD Unit Result Action Level (PPM)
ARSENIC 0.02 PPM <0.100 0.2CADMIUM 0.02 PPM <0.100 0.2MERCURY 0.02 PPM <0.100 0.2LEAD 0.05 PPM ND 0.5
Analyzed by Weight Extraction date Extracted By1022 0.2333g 03/26/21 11:03:25 1022
Analysis Method -SOP.T.40.050, SOP.T.30.052Analytical Batch -DA024327HEA | Reviewed On - 03/29/21 12:44:08Instrument Used : DA-ICPMS-002Running On : 03/29/21 12:39:56Batch Date : 03/26/21 08:57:28
Heavy Metals screening is performed using ICP-MS (Inductively Coupled Plasma – MassSpectrometer) which can screen down to below single digit ppb concentrations for regulated heavymetals using Method SOP.T.30.052 Sample Preparation for Heavy Metals Analysis via ICP-MS andSOP.T.40.050 Heavy Metals Analysis via ICP-MS.