October 3, 2012 Littelfuse, Inc.

Certificate of non-use of The Controlled Substances

Company name Littelfuse, Inc

Product Covered SIDACTOR, SOT23-6L Package

Issue Date August 23, 2013

It is hereby certified by Littelfuse, Inc., that there is neither RoHS (EU Directive

2002/95/EC)-restricted substance, nor such use, for materials to be used for unit parts, for

packing/packaging materials, and for additives and the like in the manufacturing processes.

It is also certified by Littelfuse, Inc., that the products listed in this report do not contain Halogens

and their compounds judged per widely accepted industrial guidelines.

In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used

for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing

processes, are all composed of the following components.

Issued by:

<Global EHS Specialist>

Parts, sub-materials and unit parts

This document covers SIDACTOR SOT23-6L Package, supplied by Littelfuse, Inc. Please

see page 2 for the list of products covered.

＜Materials used＞

Please see table 1 on page 2 and table 2 on page 3 of this document.

Remarks：

Pb (Lead) contained in wafer (item 6) is from passivation glass and is categorized as

exempt in RoHS Annex III 7 (c)-1

Please refer to Page 99 of this report for the extract of the applicable exemptions

of RoHS (EU Directive 2011/65/EU)

October 3, 2012 Littelfuse, Inc.

Table 1: Littelfuse Part Number covered by this report

Standard (Catalog) Part Number SPECIAL DEVICE P/N

SDP0240T023G6RP Any Special P/N which has base standard P/N listed in this table.

October 3, 2012 Littelfuse, Inc.

Table 2: Homogeneous Material Used

# Description Name of Material

Type Pages

1 Lead finish Matte-Tin metal 3-10

2 Molding compound Epoxy resin plastic 11-28

3 Die attach Adhesive metal 29-51

4 Lead frame copper alloy metal 52-77

5 Die bonding wire Cu wire metal 78-91

6 Silicon die

silicon metal

92-98. Pb is from in passivation glass on wafer and is exempted by RoHS Annex III 7(c)-I.

aluminum metal

glass glass

Test Report No.:KA/2013/30818Date : 2013i/03i/13 Page: 1 of9

SUMITOMO BAKELITE SINGAPORE PTE CO., LTD.NO. 1 SENOKO SOUTH ROAD. SINGAPORE 758069

The following sample(s) was/werc 3ubmitted and identified by/on behatf of the ctient as :

Sample DescripljonStyl€/ltem No.Sample Receiving DateTesting PeriodSampb Submitted By

EPOXY II,IOLDING COMPOUNDEME.G6OO TYPE2013n3n72013n3n7 rO 20 13t03t13SUMITOIVIO BAKELITE SINGAPORE PTE CO., LTD.

Test Re6ult(s) Please refer lo ne{ page(s).

{ r y ' ! F d ! . q { Q i ! r ' , dii. i ;o;nd" i-.at e cmEd& d b B a.*d c-d!*' d$n]; indd o;dai;ldhde q.+e' d.@$bt *!@5 @^"a4{@!!!@ih s"d ior

ddrcnc6m'I&d.-j!-bjdloi!#aidco"db*l-e|e' 'Ddn!"rid- n.,.r ddi.d b@h byh -d--"k";ih.€s'*eb.tunFnv3tidi!6nh.roedkr€re; d-e .'M $. i my. re c.;pi," n"-* a*.-" n. a*..d;ind b GFe;.-pt h tur i

| ' , m . o J r ) L

-

W4iy\

3Emd no. .rd oo balrdfaOS Trlw.n Llmb.d

Test Report No.:KA/2013/30818 Date:2013 03/13 Page:2 of 9

SUMITOMO BAKELITE SINGAPORE PTE CO., LTD,NO, 1 SENOKO SOUTH ROAD, SINGAPORE 758069

Te3t Re3uld3l

PART NAME NO.1

Test lbm (6): Unit t ethod IIDL Result

Cadmium (Cd) m9Kg With reference to IEC 62321:2008 andperformed by ICP-AES.

2 n.d.

Lead (Pb) m(yKg With reference to IEC 62321: 2008 andperformed by ICP-AES.

2 n.d.

Mercury (Hg) m9/K9 With reference to IEC 62321 : 2008 andperfo.med by ICP-AES.

2 n.d.

HeEvalent Chromium Cr(Vl) byalkaline e{raction

ms&s with relerence lo lEc 6232'1 : 2008 andperfomed by uV-VlS.

2 n.d.

Sum of PBBs

mgKg With reference to IEC 62321: 2008 andperformed by GC/MS.

n,d,Ivlonobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobipheryl 5 n.d.Terabomobiphenyl 5 n.d.Pentabromobiphenyl 5 n.d.Ho€bromobiph€nyl 5 n.d.Heptabromobiphenyl n.d.Oclabromobipheryl 5 n.d.Nonabromobiphenyl 5 n,d,Decabromobiph€nyl 5 n.d.Sum of PBDES

mg/Kg With reference to IEC 62321: 2008 andperformed by GC/MS.

n.d.Monobomodipheny' elher 5Dibromodiphenyl elher 5 n.d.Tribromodiphenyl ether 5 n,d,Tetrabromodiphenyl eth€r 5 n.d-Pentabromodiphenyl ether 5 n.d.He)€bromodiphenyl elher 5 n.d.

H€ptabromodiphenyl ether 5 n.d.Cctabromodipherryl elher n.d.Nonabromodiphenyl elher 5 n,o,Decabromodiphenyl ethef 5 n.d.

r& d&nhd n hs.d by h cohts4 dld b e qmd coid !oi! d 5.d.|dMh6da@nd6DbldbTluidre bu.. ddi.dddh !ry h

. i t i 4 c . F i r l r 1 y a b a q . d e f

. 'dd.d.5rrb.4r!s1rc*.u

BLACK EPOXY IJOLDING COMPOUND

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO.. LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. : KA/201 3i/308 1 8 Date:201303/13Page | 3 ofg

Test ]tem (s): Unit Method iIDL Re3ultNo. l

Antimorry (Sb) ngftg With reference to US EPA llethod 3052forAntimony Content. Analysis waspertomed by ICP-AES.

2 n.d.

Perfl uorooctane sultonates(PFOS - Acid, Melal Salt, Amide)

mg/tg With reference to US EPA 3550C: 2007.Analysis was perfomed by LC/MS.

1 0 n.d,

PFOA (CAS No.:33S ) msfts With reference to US EPA 3550C: 2007.Analysis was performed by LC/MS.

1 0 n.d.

HalogenHalogen-Fluorine (F)(CAS No.: 014762-94-8)

mg/Kg With reference to BS EN 1458212007.Analysis was per{ormed by lC.

50 n.d.

Ha|ogen-unbnne (ut)(CAS No.:022537-1$1)

mg/rg With reference to BS EN 14582:2007.Analysis was performed by lC.

50

Halogen-Bromine (Br)(CAS No.: 010097-32-2)

mgikS With rcference to BS EN 14582:2007.Analysis was performed by lC,

50 n.o.

Halogen-lodine (l)(CAS No.: 014362-4.4-8)

mS./kg With reference to BS EN 1 4582:2007.Analysis was perfomed by lC.

50 n.d.

Note : .t. mgrkg = ppm : 0.1M%= 1000ppm2. n.d. = Not Detected3. IVIDL = I\rethod Deteclion Limit4.'-" = Not Regulated

PFOS Refe.ence lnturnation : POP8 . {EU} 7572010Outlawing PFOS as subslances or preparalions in concentrations above 0.001% (1oppm), in semi-finished products oradicles or parts at a levelabove 0.1ol6(1000ppm), in te{iles or other coated materhls above '1!g/m'.

e r E @ E i i e

dddhhr &dn66 .ujd b r d5 d wwrsad.l4!40@b!!!84

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO.. LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. rKA/201380818 Date:20130313 Page:4of 9

1) These samphs wft dislEd ioblly by pe-@ndilioning melhod a@rding io bdMflowctun' (C6+ tesl

2) Name ol ihe peEd who made heasuendt Alex Chang

3) Name of ihe pesn in chaqe of measurement Ray Chang

steer, @ppor, aruminum, 3ord.r ,qu€ 6gia, HNO 3, HC, NF, HrCl

Gold, darinud, pall.dium, 6Bdk

No!._ : O ) For non-mslattic maiand add atkathe dio€ston reag€nt and heat ro 90-€5 f .(2) For meiallic haledal, add pure wabr and heat 10 boiling.

iddcbdn&@mhB rsjdbr

Acid digeslion by suilabl€ aci(i

depended on difeEnl sample

mabdal (a3 bd@ bble)

Micro$aw dig€slion witl

HNO3/HCUHF,dd appropd ale a mount

Me.sue lhe absorban@

I .d6rc ,b r r

No.:KA/2013/30818Dale : 2013n3h3 P a g e : 5 o f g

" " " " " " " " " ' i " " " " " , " " "J Sample extraction/ I

Soxhlet method I

I Concentrate/Dilute II Exlracted solution I_ - - - - - - - - - - - - - - -

I Filter I

i

Analysis by GC/[,lS

6mr.t'lls, .!4 r si 49ti{l! .r tlGiy ebid ro iB G6dr tudtun! d s.B

*dit hn d@notu. abl.d ro tm@t' indio' d h' tmc d iB illtff

n!/r.*c.@3b|iy*bi!ddlnd

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO., LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

PBBTPBDE analytical FLOW CHART1) Nam€ ofthe o€rson who made measurementr Anson Tsao

2) Nam€ ofthe p€rson in charge of measuremenl Ray Chang

First testing process

Oplional screen process

Confirmalion process

Test Report No.:M/2013/30818Date:2013/03/13P a g e : 6 o f g

SUltllTOlrO BAKELITE SINGAPORE PTE CO., LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

1) These samples we|e dissolved totally by p|e-conditioning melhod accoding to below

2) Name of the peGon who made measurement Alex Chang3) Name of the pe6on in chaEe of m€asurement Ray Chang

Flow Chart of digestion for lho glgments analysis peformed by ICP-AES

t 3 1 . r r f i - a r s ,

Sample M€asurcment

Acid digestion by suitable acid depend€d on diff€€nl sample material{as betowtable)

2) HClto dissolve

Steel, copper, aluminum, solder Aqua regia HNOI. HCI HF, HrO,

Glass ftNo3/HF

Gold, 9lalinum, palladium, ceranic Aqua regia

Silver HNO3

H2SO4 HrOr, HNOr, HCI

Any acid to total digeslion

I a i d , ' n r

Test Report No-:KA/2013/30818Date : 201 3/03/1 3 Page : 7 of g

SUII4ITOI\4O BAKELITE SINGAPORE PTE CO,, LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

Analytical flow chart of PFOA/PFOS content

1) Name of the person who made measurement Anson Tsao

2) Name ofthe person in charge of measuremenl: Ray Chang

sbiqdb 6 c. i .Er cqdi4! d s4

I , . u o o u a a

Test ReportSUMITOMO BAKELITE SINGAPORE PTE CO.. LTD.NO. 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. rKA/201380818Date :201t03/13 Page :8 ofg

y sbid b 6 cad cofd r qn' d sqiftj!ry.!$c!r^!E{4o@!!!!l@

it.dErtsdlr!y*b 6 obh lid

Analytical flow charl of halogen content

1) Name of the person who made measurement Jean Hung

2) Name of the p€rson in charge of measurement Ray Chang

Sample picture and rsport number

Weighting and putting sample in cell

Orygen Bomb Combustion /Absoption

Dilution to fixed volume

Analysis was perfomed by lC

l , e i o t n , n r

Test ReportSUI/lITOMO BAKELITE SINGAPORE PTE CO., LTD.NO, 1 SENOKO SOUTH ROAD, SINGAPORE 758069

No. : KA/2013/30818Date:201303/13Page: I of9

' The tested sample / parl is ma*ed by an anow if it's shown on the pholo. '

*' End of Report "'

y eqd 6 iB c6d,r coden. or s.o

]ddidm r-u.r ddmd 6.6n. My hnta $L artsns b riv tr b i! c id and

30818

Signa reFor QuPlease

Test Report No. : CEl2013t1868 OaJ.e:2013107116 Paoe : 1 of 19

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U, S. A.

The following sample(s) was/were submitted and identilied by/on behalfofthe applicant as :

wiih SGS

Sample Submitted BySample DescriptionSVbr'ftem No.Sample Receiving DateTesting Period

HENKEL CORPORATIONADHESIVE84-1LMtSR42013tO7t09201 3 I 07 I 09 1 0 201 3 | 07 I 1 5

Test R€uli(s) Please refer to next page(s).

(Alw4D

th€cn AoY 60 d' ofihis delmaDi sa

l m o c . l s ' b . ' o a ' m 9 l ' '

nd6r E h*, New r! re c ry. ri w:n / tlll ljtr

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD,

To€t R$ult(6l

PART I,IAME NO.1

No.:CE/2013t71868

IRVINE, CALIFORNIA, 92606 U'

D?i.e t2113l|7h6 Page : 2 of 19

s. A.

SILVER COLORED PASTE

t

Melhod i,DLR€sult

TeBt ltem(3) unit No.'l

cadmium (cd) mg/Kg Wiifrffi;E6 lEc 62321 : 2oo8 andperformed bY ICP-AES

2 n.d.

WiifrE;;; to lEc 62321 i 2oo8 andDerformed by ICP-AES

2 n.d.Lead (Pb) mg/Kg

2 n.d.Mercury (Hg) mg/Kg with rcference to lE(i ozJzr: zuuo ano

perfomed bY ICP-AES

Hexavalent Chrcmium Cr(Vl) mg/Kg ffireterence to tec oze21:2008 andperformed by UV-VIS

2 n.d.

Antimony (Sb) mgKg Wlin-'retEEice to Us epe Method 30508Analysrs was Perfomed bY ICP-AES

2 n.d.

Beryllium (Be) m9&s Withffirencelo uS Epn Method 3o5oBAnalysis $/as p€rformed by ICP-AES

2 n.d.

potychlorinated Biphenyls (PCBs)(CAS No.: 1336-3S3)

mg/kg frit6Erence to us EPA 3540c methodAnalysis was p€rformed bY GC/MS

0.5

Polychlorinated Naphthalene (PcNs) mg/Kg friii-ference to us EPA 3540c methodAnalysis was perfomed bY GC/lVlS

5 n.d.

Flotychlorinated Temhenyls (PCTS) mg/Kg WiiFreference to uS EPl3540c methodAnalysis was performed bY GC/MS

0.5 n.d.

Alkanes, C10-13, chloro (Short ChainChlorinated Paraffins) (CAS No.:85s3S84.8)

m9/kS W;ifi;ierence to us EPA 3540c method.Anatysis was performed bY GC/MS.

100

Hexabromocydododecane (HBCDD)and all major diastereoisome6id€ntified (o- HBCoD, F HBCDD, Y-HBCDO) (CAS No.:25637-99-4 and3194-55-6 1134237 -51 -7, I 34237 -5O-

6, 134237-52-8)l

mdkg With reference io US EPA 3540C method.Analysis wEs perfomed bY GC/MS

5 n.d.

Halogen-Chlonne (Cl) (CAS No.:22537-15-11

mg/Kg With referenc€ to BS EN 14582:2007Analysis was pedormed bY lC.

50 236

Halogen-Bromine (Br) (CAS No.:1OO97-32-2)

mgkg With reference to BS EN 14582:2007-Analysis was perfomed bY lC.

50 n.d.

scsraNan-d. e/ttt*+nnlo t * r. q I frA'.'#i, |1*6efitrB-r3

TeSt RepOft No : cE/2013/71868 Date:2013/07/16 Pase:3 or 1e

Lt#S:'^fi35R3!ttJ:8, rRVrNE, .ALTF.RNTA' e2606 u s ATIt

llrethod MDL Re3ultTest llem(3) Unit l{o.1

0.003 n.d.s-EFiE64t outyt pt*ratate) (cnsNo.r85-68-7)

ok with reference to EN l'rr/z AErvsrrperfomed bY GC/MS

0.003 n.d.6fl(oi-€-euytneryDpntnalate)(CAS No.: 117-81-7)

% With fele€nce rc EN r4./z ArErtJr'wc'

performed bY GC/MS

ffin rererenca to eH t+aT2 Analysis wasperfomed bY GC/MS

0.01 n.d.DIDP (Di-isodecyl phthalate) (cAsNo.:2676140-0)

WitfrErence to eN l+sT2 Analysis wasperformed bY GC/MS.

0.01 n.d.DINP (Dijsononyl phthalate) (cAsNo.:2855312-0)CNOP (Di-n-octyl Phthalate) (CAsNo.: 117-84-0)

WinEGrence to ell t+aT2 Analysis wasDerformed bY GC/MS

0.003 n.d.

0.003 n.d.DBp (DiBp (Dibutyl phthalate) (cAs No : 8+7+2)

vo with referen@ to EN r4J/z ^naryslperfomed bY GC/MS.

DIEIP (Di-isobutyl phthalate) (CASNo.:846$5)

WiifrGGEnce to et't tcT2 Analvsis wasp€rfomed bY GC/MS.

0.003 n.d.

DMEP (Bb (2-methoryethyDphthalate) (CAS No.: 117-82-8)

FiGleference to et.t 1 l3T2 Analysis wasperfomed by GC/lrS

0.003 n.d.

DHiiUit (1,2-Benz€nedicarboxylicacid. di-c7-'1 1-branched and linearalkyl esters) (CAS No.: 68515_42_4)

WiiFflerence to EN 14372 Analysis wasperformed by GC/lVlS.

0.01 n.d.

DIHP (1,2-Benzenedicarboxylic acid'di-C6-8-branched alkyl esters, C7-ri^hr /a:As N6 Ti aaa-896)

WlfrJ6rence to EN 1 4372. Analysis wasperformed by GC/IVS.

0.01 n.d.

CNHP (Di-n-hexyl phthalate) (CASNo.:84-7t3)

WilF;eference to EN 1 4372. Analvsis wasperfomed by Gc/lvs.

0.003 n.d.

AiEiysis was perrormea uY Fttn anoFLAIVIE TeSt.

Negative

0rganic-tin compoundsIdbutyl Tin (TtsT) mgKg W[tr re rence to ISO 17353 Analysis was

performed by GC/FPD.0.03

Triphenyl Tin (TphT) mg/Kg Wittr reference to lSo t2353. Analysiswasperfomed by GC/FPD.

0.03 n.d-

Dibuvl Tin (DBT) mgKg With reference to ISO 17353. Analysis warperfomed by GC/FPD.

0.03 n.0.

Dioctyl Tin (ooT) mg/kg with reference to lso 17353. Analysiswalperformed by GC/FPD.

0.03 n.d.

scs 16wdn Lrd. ettees+t**t a" 'll ,,4 #;1"",'d1*86nf,ifi3

TeSt RepOft No r cE/2013t1868 Date : 2013/07/16 Pase : 4 or 1s

HENKEL CORPORATIONl4OOO JAMBOREE ROAD, IRVINE, CALIFORNIA' 92606 U' S. A'

Unit Method MDL ResultTe3t lt m(3) l{o.'l

Tributyl Tin Oxide CI-BTO)* (CASNo.:5€-3tg)

mS/kS w-ith reference to lso 17353 Analysiswasperfomed bY GC/FPD

n.d.

Sum of PBB3 mg/Kg

with reference to lEc 62321:2008 andperfom€d by GC/MS.

n.d.5 n.d.

MonobromobiPhenyl ms/ks5

Di6romobiphenyl mg/Kg5 n-d,

Iribromobiphenyl mgagIetrabromobtPhenyl mlUKq 5 n.d.

Pentabromobiphenyl mq/Kg 5 n.d.

HexabromobrPhenyl msftg 5 n.d.

HeptabromobiPhenyl mg/Kg 5 n.o,5 n.d.

Octabromobiphenyl ms&g5 n.d.

Nonabromobiphenyl mq/Kq5 n.d.

DecabromobiPhenyl mq/Kq

Sum of PBDE3 mdkg n.d.5Ivlonobromodiphenyl ether mg/Kg5 n.d.

Dibromodiphenyl ether mg/kg5 n.d.

Iribromodiphenyl ether mgkgTetrabromodiphenyl ether mq/Kq 5 n.o.

Pentabromodiphenyl ether mq/Kq 5 n.d.

Hexabromodiphenvl ether mgkg 5 n.d.

Heotabromodiphenyl ether m(yKg 5 n.d.

Octabromodiohenvl ether mg/Kg

Nonabromodiphenyl ether mdks 5 n.d.

D€cabromodiph€nyl ether mlyKg 5 n.d.

l{ote :'1. mg/kg = ppm ; 0.1wt% = 1000PPm2. n.d. = Not Deteded3. MDL = lvlethod Detection Limit4. " -' = Not Regulated5. * = Oualitative analysis (No Unit)6. Negative = Undeteclable / Postive = Detectable7. *: The substance was calculated by the test result of Tributyl Tin The MDL was evaluated for T

A X A ' F

Tin.

AX

Bis(tributyltin)oxide Tribdyl Tin (TBI) 1.02768.Thls report supss€des th€, pretl;us docunter't beadng the test report number CE/2013/71868

on 2O131O7115.

scs raN6- Lrd enro*+ir+r'rr"q I ij'S,#iil*hEEfrS33lidGra tuft Newraioe cly rawln/

ed

Test ReportHENXEL CORPORATION14OOO JAMBOREE ROAD, IRVINE'

Outlawing PFOS as substancesproducts or articles or Parts at a

No. i CE/2013/71868 DEI.e:2013107116P a g e : 5 o f 1 9

cAL|FORNIA, 92606 U. S. A

PFOS Refergncolnfomation : POPS - (EU) 752m10or DreDarations in concentrations above 0 001 %

levelabove 0-1%(1oooppm)' in textiles or other(1oppm), in semcoated materials

nished1!g/m'.

SGST6iwn Ltd. € til**Ar*t)f, tl./a\ 51 dc t6 fu4 ,Nswr ,Fcq , r ,@n /

Test ReportHENKEL CORPOMTION14OOO JAMBOREE ROAD, IRVINE,

1 )

No. : CE/2013t1868 D e:201A07116Page : 6 of 19

oALIFORNIA, 92606 U. S. A

2)3)

These samDles were dissolved totally by pre-conditioning method accoding to below

( cP test method excluded )Name oflhe person who made measufement: Climbgreat Yang

Name of the person in charge ofmeasuremenl Troy Chang

l{ote* : (1) For non-metallic malerial,(2) For metallic malerial, add

add alkaline digeslion reagenl and heat to 90-95pure water and heat to boiling.

Cutling / PrepaEtion

Ivicrowave digestion withHNO3/HCr/|lF

Acrd digestion bY suilable aciddepended on differenl samplematerial (as below table)

Cool, filtet dthrough filler'1) Alkali Fusion

2) HCltodissolve

al 540 nm by

Samole IVlaterial DiqeslionAcid

Steel, copper, aluminum, solder Aqua rcqia, HNO3, HCl, HF, HrO,

Glass HNOs/HF

Gold. Dlatinum, palladium, ceramic Aqua Ieqia

Silver HNO.

Plastic H,SO.. H,O,. HNO3, HCI

Others Added appropdate rcag€nt to totaldigestion

scsTa@. Lrd. e!&&ftRnet tE1.a | , ' iS; , , " ;1d-

Test RepcHENKELCORPORA'14OOO JAIJBOREE F

1 )

2)3)

SGS T6l

poft No : cs2013t1868 Date:2013/07/16 Pase:7of19

]RATIONEE ROAD, IRVINE, CALIFORNIA, 92606 U' S. A'

These sampleswerc dissolved tolally by pre-condilioning method accoding to below

cnan.Name ofthe person who made measurementi ClimbgleatYang

Name of the person in charge of measulement: Troy Chang

Flow Chart of digesuon for the elements anallBis pedormed by ICP'AES

@L ---- --

I Sample l\Iea"l:.1t ____lL-------r

1^"-a "rg""a"" "y " ,-""" ""- uepcrrueu u'r I

I different samDle mate al(as below lable) |L-_-=r

l tllrtl

Solrtion Res

1 )2) HCllo dissolve

ICP-AES

Seel, copper, aluminum, solder Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic H,SO4, H'Or, HNO3, HCI

Others Added appropriate reagent lo lotaldigeslion

, r r o i F d o i . ! ; . ^ d F , a , o r d

s rd@n Lld. c '1.&r+rir{r}t na. a I l1*13litlfi,,;""i,1i1ffi *frEi itffe!t

Test RePort No.:CE/2013/71868Date : 2013/07/16 Page:8 of 19

HENKEL CORPORATIONr+oooleMeonee nom, lRVlNE, oALIFoRNIA' 92606 u s A

PBB/PBDE analytical FLOW CHART

pe6on who made measurenent Roman Wong

oerson in charge of measurement Troy ChangI Nam€ of thea Name of lhe

Fiast testing process ----->

Oplional screen Process ""Conlirmation Process - .>

f--."'d"-----l--=T-

f s".pl"{t"rr""tt";l--=T-

Screen analysis. ! . ' . . . . ' t . . f , . , . . . . , . . . . /

Sample extraction/Soxhlet msthod

Concentfale/DiluteExtracted solulion

Filter

Analysis by GC/I\IS

lssue Reporl

o ' lnmadron i,om orrc s iq. s€i ri

SGSTai@n Ld. € l|li&t+li&&i |fa\ 4

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD'

No. : c42013,71868 Date : 2013/07/16 Page : I of 19

IRVINE, CALIFORNIA, 92606 U' S' A'

|lr rr

I

I

Analytical flow chart of Organic_Tin content

Name ofthe person who made msasurcmenl: Ginny Chen

Name of the person in charge of measuremenl: Trcy C hang

Dala

;;i;,4; dyin;td. e$p,.i' .ttuu p,d,

SGs Taiwan Ltd. € tii&t+&nl}4 tra\;l hdsrd Pdr Nwrlips cry rawm/'il

Test Report No :cE/2013n!868 D?r.e 2013t07t16

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U' S' A'

II

SGS Taiwan Lrd. e tii*tr+iirtDt &a\ tl

Page : 10 of 19

chlorinated Paraffins anaMical flow chart

Name ofthe person who made measurement: Barry TsengName of the person in chatge of measur ement: Troy Chang

€3 o € 3:$b"! b/r\i,wt: 'orb' 'T6"

ciFa Aiy mr! hored€|nmioi, rolery o bErndhd he &detro,apd

rll tltlll

Data

Test ReportHENKEL CORPORATIONt+ooo JnMaonee nono, lRVlNE, CALIFORNIA, 9260€ U S A

No.:CE/2013f l1868Date: 2013/07/16 Page: 11 of 19

rhis ddme 3 sud byse bmFiysubjed ro 6 6seu coid r ore d s€ry c s n$d tr, *r

PCTS analytical flow chart

Name ofthe person who made measuremenl: B,arly Tseng

Name ofthe berson in cnarge of measurement: Troy changTI

Data

SGS Taiwan Ltd. 6 tta*ltit,&tnf &,a\ tl

Test Report No. : cu2013t1868 Date: 2013/0716 Page: 12 of 19

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE.

aI

Pcl{3 analytical flow chart

Nameofthe Derson who made measuement: Barry TsengName ofthe;erson in charge of measulement Trcy Chang

CAL|FORNIA, 92606 U S. A.

1flI|ll

Analysis was performed by GC/[,4S

SGS Taiwan Ltd. 6 tit&t+ltrtttt S.a\ 4

Test Report No :cE/2013t1868 Dare ' 2o13107h6

HENKEL CORPORATIONr+ooo JeMaoaee nono, lRVlNE, CALIFORNIA 92606 U S A'

P a g e : 1 3 o f 1 9

PrCBs analytical flow chart

I Name of lhe person who made measurement: Barry Tsengi ii"r" orf," p"t"on in charge of measuremenl Troy chang

Data

30 s oa F1 b" d \E1I4! 4:-44:llrl

' o 3 1 2 . ! c o ' o ' e ' s ' . 3 ' c ' ' ' s '

SGS Ta en Lld. eBk&ffh&hf, t*:..4N€wr'F civ r!to' / trrlfist

I

I

SGST6&an Lrd 6 tit*t+&rtfi' * n.!' jl

Test Report No : cE/2013/71868 Dare " 2113t07t16 Pase:14of le

HENKEL CORPORATION14OOO JAMBOREE ROAD. IRVINE. CALIFORNIA, 92606 U. S. A,

AndFis flow chart for determination of PVC in material

Name ofthe percon who made measurement Ginny Chen

Name ofthe person in charge of measurement: Troy Chang

f u J t ' . n \ @ / / M $ ! - a o v € T ' r d J o d I e { | . , 1 i

rc d r ;Be,oi rom &d

ttllll

Sample prc-treatment

Sanple analyzed by FTIR

Check wave-number ol C-Cl bonding

Test RePortHENKEL CORPORATION14OOO JAMBOREE ROAD' IRVINE'

No. : cE/201 3/71 868 Date .2013tO7116 Page 15of 19

CALIFORNIA, 92606 U' S' A

r{mnnrrn

l

I

I

Analylical flow chart of halogen content

Name of the person who made measurcment Rita Chen

Name of lhe person in charge of measurement; Troy Chang

Sampte pretreatment / Separation

Weighting and putting sample in cell

Orygen Bomb Combustion / Absorption

Dilulion to fixed volume

Analysis was Perfomed bY lC

scs TaiMn Lrd. b t*tlt+lt&1tt |[ a\ 5J

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD,

No. : CE/2013/71868 Dale : 2013107116 Page : 16 of '19

IRVINE. CALIFORNIA. 92606 U, S. A.||Nrfl ||rm

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Analytic.lfiow ch.rt of phihalate content

Name of the person who made measurement: Roman wongName of the ierson in charqe of measuremenl: Troy Chang

Data

bqc o lq s" o-J. r. 5eo n d osFq,

.i Ah rodddfiitAA!;aniiaffi6dm;lnr;mitni ntsitiaaErFecomFryj

SGS T6lwan Lrd. 6 4it ttllti*?t f, tl.a\ 4

Test ReportHENKEL CORPORATION14OOO JAIVBOREE ROAD,

No.: CE12013,11868 D€i.e:2013107116 Page i'17 of 19

IRVINE, CALIFORNIA. 92606 U. S. A,ttl rllllr

HBCDD analytical flow chart

r Name of the person who made measurement Roman WongI Name ofthe person in charge of measuremenl: Troy Chang

a " - ; . , c o - o € , € . s .tu;;i; Aiv nlh'dsit{d" b'6.^

" ".6;L-" i"-d*," ap

scs raiwan Lrd. s trihnr+*nDr rEa. a | ::6*%1ii3f{n!"i.Blii,iiH$:i:1- H'$li' "'*"r"'Ln#'dfsEnftB"s

Sample extraction by soxhlet method

Concentrate/Dilute Extracted solulion

Data

Test ReportHENKEL CORPORATION14OOO JAITIBOREE ROAD, IRVINE, CALIFORNIA, 92606 U' S' A'

No. : CE/2013/71868 Dale : 2013107116Page : 18 of 19

ntillllllill

PFOATPFOS analyticalflow chart of t ltasonic exbaction (LCmS) procedurc

r Name ofthe pe6on who made measuremenl: Roman Wongr Name of the iercon in charge of measurement Troy Chang

' o 3 i s r o " o & e

SGS Taiwan Ltd 6 tlt&?t&,tta t tnr.4

i

Sample pretrealment

Sample exlraction by ultrasonic exlraction(Reference method: US EPA 3550C)

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U. S' A.

No. : cE/2013/71868 Dale 12013107116Page : 19 of 19

'The testsd sample / part is marked by an anow if ifs shown on the photo '

* End of Report *

71868

scsr6i@n Lro el .r9c**"ta"4 | , l ,H," i ] : ' f t Mwr,E civ 16 w:, / stlfis trif

{r|| |r!!l|r

Signatu tid

with scs

Test Report No. : CEl2O13l7177a Date :2013t17t15 paoe : I of 4

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA. 92606 U. S, A

The following samples was/w€re submttted and id€ntified by/on behatfofthe appticant as :

Sample Submitted BySample DescrjptionStyle/ltem No.Sample Receiving DateTesting Period

Teat Reque6led

Test Method

T€3t Re6ult(s)

HENKEL CORPORATIONADHESIVE84n Lt\flSR42013tO7t09201 3tO7 t09 T O 2013tO7 | I 5

: As Bpecified by ctient, to test PFOA, PFOS contents in the submitted

: With reference to L,S EpA 3550C: 2007.

: Please refer to next page(s).

EJ,EllorSgmdfqscattflutl

ooeo i . oc t i g ; t a t

SGS Ta'w6n Ltd e t*rat+itrtDt ea! rl toBrb torr. New r, F civ r!tui / tilLfiNt+*+

Test ReportHENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNTA, 92606 U. S. A,

T.€t R.ault{3l

PART NAME No.l : SILVER COLORED PASTE

l{ote :1. mg/kg = ppm; 0.1w1% = 1000ppm2. n.d. = Not Detected3. MDL = M€thod Detection Limit

PFOS Ref€.ence Infomation : POP3 - (EU) 7572OtOOutla\ring PFOS as subStances or preparations in conc€ntralions aboveproduc{s or articles or parts at a levet above 0.1%(1000ppm), in textiles

S0S Taiwan Ltd. 6 tltt&ttiinDi &a\ tl

No.. CE1201317177A Date.2113t07t15 Page 2 d 4

Test lt€m(.) Unit Method IiIDLResultNo.'l

Pedluorooctan€ sulfonates(PFOS-Acid, tuletal Salt,Amide)

m9Kg With reference to US EPA 3550C:2007. Analysis was performed byLC/MS.

1 0 n,d.

PFOA (CAS No.: 33'67-1) mgikg With reference to US EPA 3550C:2007. Analysis was performed byLc/ll,lS.

1 0 n.d.

0.001% (1oppm), in semifior other coated materials € 1!g/m'.

.tr .€ooos 4 ooe o,irln-:n-iii-ttigF n6aj oi ec

tu*, Mw rd F c r, rliwn / *rLnj*jLe*B

Test Report

SGS I€'w6n Ltd. g t&&rtt|ttDt F'r\ 4 d6ri8 tod M! i8F rry tu@i / slrlfipirl*iF

No.1CU2013n1778 Dale:2013t17t15 page:3 of 4

HENKEL CORPORATION14OOO JAMBOREE ROAD, IRVINE, CALIFORNIA, 92606 U. S. A,

PFOA/PFOS anelytical flow ch.rtof Ultlasontc extraction (LC/MS) procedurcI Name of lhe person who made measuremenl: Roman wonoI Name of lhe person in charge of measurement Troy Chang-

a ,.otr o . "4*-ai. i;rd.ndirsi :6nri

Test ReportHENKEL CORPORATION14000 JAI\,IBOREE ROAD, IRV|NE, CAL|FORN|A. 92606 U. S. A

SGS Tai@n Ltd. 6 4li{*+ltrt&f, llr\ { tu{ N6wra @ c v Ia wa / rrnffiFntx*B

No.: CEl2O13n177a Oale 2013t07t15 paoe 4 ot 4

r Th€ te€ted sample / part is marked by an anow it its shown on the ohoto. r

" End of Report _

q € ^ b d - : a i o l d ! r \

71778

SignatureFor Qu€ElionPiease

nlfi,#+S,4(No. ) : xA/20r2lC2128 ES{Date) , 2073/01/a2 l j&. (Pase) : r or 26

Test ReportASV IIX

.{/F. WATSO}{ CENTRE, T6 K!\G YIP S1.. I$AI CI]UNG. IIONG KONG (AS !K)

trTrlitifs4*rBP rjE&, .RA;P +*n{t*P**itT6 y l o ! b . h r l f o f t t c . l i . r t r r ) :

(T t . to l lo r i rs saEp le6 t .s / te r . subn i t ted lnd id€r t i t i .d

{ { .St{* (sa 'Pl . Desf i iPt ion)

4t l lE S(saapt . Receiv ins Date)

trlg,JkFl(Tcst ins Pe. i od)r!{,Rfi (saap t. s!6nitted BY)

: Al91/C194 cu ALLOI| 2 0 1 2 / 1 2 / 2 5| 2or2/12/25 19 20rs/01/02: ASM qlt

Xlll* j*.(T.6t R€suI i6) a* ,?-T- i (PI""* refer to n€xr Pases) .

:tr'#tfr i#*f4ffi :+i+kritrf,ff'ffi lr;:#i'$ffi ffi;q#;$#;ffi,'y,;1;s';g':".f il T#li:*::.'SJ',ili',:"Ji:"Jfiffi;'iH:!i!4i!!ir"::r:i+:,irii;::.;i*;*'^:r"lu:l';;;ff;,:::;'""::'"5.1;'--ij.Tuilii

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with

Ebtrd fo. .td o.| b.h.facs l|ls.n Llnft.d

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n!|s#+Test ReportASM III{

4/F, trAfSOII CENTRE, T6 KUN] YIP

tdll**(163t R.r!l t6 )

N]&4{i (PART NAME) \O.1

SrE(No.) : M/2012lc2128 € l h ( D : r e ) : 2 0 1 3 / 0 1 . 0 2 E i t s ( P " s e ) : 2 o I l 6

ST.. I{X'AI CHUNG. HONG I{ONG (ASM HX)

,i,14 Al91/c1s1 cu ALI'Y (RED @PPERY Al9,l/c194 cu,ArIrY)

rlitt E +& et:ti ,riitr,lbnr(nx,L)

J.*

NO.1

t-4rs.6232r' 2oo3?i*, 4 6Glt+t*,F+*4lr!i*f; l*,r{. / ui thre te !ence to IEc 62321, 2003 andperformed by ICP AES.

s / Lead (Pb) +*tF 6232r.2003tt4, E 6r!**+tffil*4ti'#al*,r1. I ri ttr€ fe rence to IEC 62321: 2008 andperfo.ned by ICP_AES,

l 3 . l

+*rEc 6232rt zoo8tri, E AAt*4'tf,F+**l*.*frl*jrl. / !i irre fe r€nce ro IEC 62321: 2008 and

pertorEed by lcP-AlS.

, r1 l l t / Hcxavalent ch loDi !n cr(v l ) byboi I i .s {at€r exrract ion#

+4lEta 6232rt 2008?i i , EBoi I ingsater exhac t i on t t *A , t l . / q ' i th

re fe rence io IEC 62321: 2008 :nd

per fo rned by ho i I ing va ter

0.02ns/ks

tttlt** / su' of PBar

++tE 62321: zoo9t)|, ,tl\"&EfrC, / l f *d , *n l . / { i t f i .€ le renc€ to

M 62321: 2008 and Per lo rned bY

GC/i{S.

-A#* / Nonobronoh ' pheny I 5

: i l# f . / D ib ronob ipheny l 5

: : f l$ f / T r ih ro$oh iphenYl 5

e l , * f X / T€ t rah .omob iFh€ny l 5

5--;r!#f / Penlabronobi pnenyt 5

i - l# f / Hcxabrosob iphent l 5

. t l l l l 1 l / l l ep tabrosob iphcnr l 5

,\-AlSf / oct,brooobiphentl

/L![#:l / NonabroDobiphenyl

+ i l#* / Decabrobob iPhq/

li*i*.:,**.:ihdt1,"i.',r?"".*;:xrs*.""s:i,:lx'.ru;g:tsuir"G*.1'l*qtrii';i,.q;j-irii::i:.-":-1"#:

I sorcr!" r

,FlH,#+i [4{No.) : (A/2012lc2128 EJq(Date) | 2or3tor /02 F*(Pase) : 3 ot 26

Test ReportASM UK

,,/F. MTSON CEIiTRE, 16 KUNC YIP ST.. KqJAI CHUNG. HONG (ONG (ASM N{)

il!*ff fi fl tr{F#$r$$Sitr'#str{ffi6!Jjiit$;'1fri1i#1..-d#ffi ffi "-"il';#"J#-"ffi #;#,i::F.*"i*;'ii.*"'-rrir$n*s*,r.r.3"t':1at"j;:;.#;;-,-;;;:. .;';ird edd nl s

"3t"{tlgd,,.olh.sM':'. -$

t 9i;..{" *,.".,",. ,. ""-,"

,".

|lrit E +{r(uni t )

r{ltt* t*{tabftf,(xDL)

* *

llo.1

t *t*al3+ / su! of PBDEs

++rEc 6232r' 2oo3r)4, ,ilfu4an*ft{ , / f ' , *d, i *U. / n i th r€ ler€nce toM 62321: 2003 and ter lor f red bYcc/vs.

- * t *a t / Monob.onod iPheny l e ther

: - i l tE* t / Dibronodiphenyr €ther

: * tXAt / T r ib ronod iphenYl . !her

qAt l *ad / Ter .ab .oood ipheny l € ther

ntltttat / Pentabronodiphenyl erner

n* ' l *a t / lexa6roDod ipheny l e ther

+ i l$*a t / sep tab .onod ipheny l e th€r 5

^*t*!d / octah.orod 5

/ ! *#*a t / Nona6rohod ipheny l e iher 5

+Af iSa4 / D€. rb ro f rod ipheny l e ther 5

t * ,S* / Po l r .h lo r ina ted B ipheny ls(PCBS )

++us EPA 354oct*, tl*Eneqi l&(cc l s) l f t ,n l . / { i th rerercncero us PA s510c nethod. Analys isvas perforncd by tr/Ms.

t i6 / PoLych lo . ina ted Naph lhaLene

(PcNs)+*us EPA 3s1oc?i*, t/ $lan)rrni * { ' (cc lMs) l fx l . / { i th !ere!enceto US EPA 3540C meihod AnalYsisras per fo lm€d by rc / IS.

5

t ^ : -Sl+ / Poly.h lor inated Tc.phenvls(Pqrs)

++us erA 351oct;i, ,^$"iaEfrg*d l (@/Ms)&; . / s i rh re fe lencc

ro US EPA 3540C n€rhod Ana lYs is

vas periohed by GCI$S.

0 . 5

| , - s o 0 u n r

,r{s,*EBTest ReportASV Hl(

r/F, VAISON CENTRE, 16 r0NC YIP ST., mAl CtlLNG. HONC {ONG (Aslll g()

*g(No.) : x . { /2012lc2128 Eih(Date) . 2ar3/ar /02 q*(Pase) . 4 of 26

rlLt E +e( u I i t )

er* t;tdrlEBlt(DL)

*iF

NO. l

i . |bE{ / ch lo r ina ted Pa.a f f in(C l0 .c13) (CAS No. : 35535-84-8)

++us EPA 35roc' 1996tt*, ,(*L*E,llit{t/t+diJe'HFl *&ni. / withre fe re 'ce to us EPA 35.10C: 1996

dethod. Ara lys is vas per fo rned by

GC/ECD.

*df / } { i rex (cAs No. : 2385_35-5) 4+us EPA 8zToDri*, vt*"laE}iXi td ' (cc l rs)&,1{ . / t r i th reterenceto us EPA 8270D oet iod, Analys isras pcrrorned by @/Ms,

+*us Epa 3o52t*. F /S6*A€*&+*4fh*d.& l{ ial. / vi iLre f€ .ence ro US EPA M€rhod 3052 fo r

A! t inony Con!en t . Ana lys is was

p€.forned by ICP-AI,S.

t -n l r ,=t . / ant imny k iox ide(Sb2O3). r i (cAS No. : 1309-6,1- , t )

4*us PA 3os2til, E 6,8{i+t{,,f, +.f4+,t'r*ali jll ii +t . / {ithre le r€nce to IJS EPA u€thod 3052 fo r

An i imo l t Conten t . Ana lyB is vas

perforncd by ICP-AIS,

€*!a'-a-t / TBBP_^-bis (cAs No :2rB5o-11-2)

t+us EPA 355octii, ,x*,{a,?tfd,/ t *dt+ i !1. / v i rh reference to us@A 3550c r c t hod . Ana lYS i s r as

perfoined by GC/NS.

i&''+:ts' / sexabronoct.lododecane(l8cDD) (CAS lio.: 2563?_99-4)

++us tPA 3s1oc: lse6ti! . r)(nrE,if t ; t&lfxl / with ref€'en" toUS EPA 3540C : 1996 he ihod Ana lYs i s

ras pcrforned bY CC/MS.

5

rn{fi,#+&rr t \No.J . Y,A/2012/C2|28 SJh(Date) | 2or3/or /02 Fjk(Pag€) : s of 26

Test Reportas\t g(

1/F, 9ATSON CEIITRE, 16 (!NG YIP ST., K{AI CHUNG. HONC KOXC (ASM I()

iffF"ffi,Trff{F#$$ffi$i#}fi'l#i#*'l'"*'#iifl",wlffI"il-i'"j!llil.L:;il**fi;#;"1tr"-.;;;;i-@!hda"ds. i." d tr.c.6,moirvridw$i 'torri!

li+ii-:,ii;:"1*--' ..'.* ,n. ftrn4'Et&48ta'1-t;'':"-tAl;,"ff", *..,..**-- .-,., .",-

drt{ E +t'(uoi t )

firtt* tndrlEnn(uu.)

* t

NO. l

*rrii (Y*) / Foroaldenyde (cas No50-00-o)

+*rso r?226-l(2008)ri i , r ,{Stt l*E{fi &/:ti 4r{.fi ;rl*&i.l. /wi th r€ fe rence ro l so 17226-

1(2003) . Ana lys is eas per fo rn€d by

TPrc/DAD.

3

f# l r9 / o .san ic - t i i compourds

- : -T l4 / Tr ibuty l T in {TtsT) -+,FJi{,}*DrN 33407-l3Z;}, nl\ i€.{it&./t B'L,ttf,rl*&;rl. / {i thre f€ rence 1o DIN 33, t07- r3 . Ana lys is

Pas p€rlorned by GC/FPD.

0 _ 0 3

-:-*'if,.4 / Triph€nrl Tii (TpnT) i , i l i {4*DIN 3840?-l3ri}, ,x *,{€tfi C,/ J.E*Afi nl*ii,rl. / tri thre fe rence ro DIN 38,107-13. Ana lys is

ras pe.forned by rc/Fm

0 . 0 3

: .T *&nlU#, / Tr iburrt r i ! oxide(TaTO) . r . (CAS No. | 56-35-9)

lF l i t4*DIN 38a07-l3t i i , ,x { ! i€,l &d./ J.iA t&d al * &irl . / withr€ fe rence to DIN 3310?-13. Ana lys is

{as peifa.ncd b, GCIIPD.

*.*.alF / Pvc ,arrrlrn*+&^&6)+l&il. /Ana l t s i s r as pe r f o . r ed bY IT IR and

.l,rj3\,d*la#d'rir(. / a',rFiswas oer fo iEed bv Pr ro l yze . -cc l l ' l s -

I , .6so7@rr r

'r{-d,+E+* ,€(No.) : I iA/2012lc2128 ES(Datc) . 2aI3/ar /02 F*. (Pase) : 6 of 26

Test ReportASI{ g(

4/F, IIATSON CENIRE. 16 KI,IIG YIP ST., ($'AI CHUNG. HONG KONG (AS HK)

';ti:iiT;,ff;Hll ;"d: ;;ff;iiili"-rJ'liniii ii;;i;", *a u;.;";d; b*.d'.ih3d*..n --a u -rc a.*o * ruri *oJ;*..*-.F.d d6' tu4-v' 6

rt{l€ te( s . i t )

lttrt ,it{|rlEAC(mL)

s*

NO. l

a* ( t , ) / sa losen-FLlor in€ ( ] l ) (cas ++Bs EN r4b82,2oo7, , t*+)a&tt+#. / $irh rei€ren.e to Bs EN1,1582:2007. Ana lys is Fas per fo rned

50

6t (5 , ) / Ha logen ch lo r ine (c l ) (cAs +*as F! 11532,2007, *+n&6.t& . / \ i i , r \ r . f€ .ence to Bs EN11532:2007, Ana lys is vas per fo r f led

50

6l ( i l ) / t la l "c"" -sroni ie (Br) (cAs

{ o . : 1 0 0 9 7 - 3 2 - 2 )t*Bs EN 11s82:200?. nr&+,if id,+f i . / \ l i th .e fer€nce ro Bs EN11532:2007. Analys is qas per fornedby IC,

50

6* (4f ) / rb log€n- lodinc ( l ) (cAs

No. : 1, t362-44-8)++Bs EN 14s82,2007, ,/ lF+ 8fr i l .+f t . / Ni , t l \ re f€ren.e to Bs EN14582:2007. Ala lys is f ,as per formed

50

n 4.f i t tntrr / Phthalares**:?rtPf,llTfi / aBP (B.nzvrbu ly l ph tha l . te ) (CAS No. : 85-68-7)

+fl St*!N !43? 2, 4 ̂ $ n fr &./ qt fd*x 'Jz. / s i rh referen.e ro EN113?2. Analys is vas ter tormed bYcc/Ms,

0 . 0 0 3

*X:?&:TaE / DBP (Dihutylphtha la te ) (C,AS No. , 34-?4-2)

ix4g.4+Ei 1a3?2, ,\ftla),ttfl /Ii *d , lhB l : . / { i th re te rence to EN

14372. A la lys ig f ,as per fo rned bY

*+:ft: (2-a;s'e*)a8 / DEHP (Di(2 -e tn t l iex t l ) ph tna la tc ) (cAs l {o . :

t 1 7 - 8 1 - 7 )

+jfli{.&+EN 1a372, rr.llt ieE&il./ f: *d ,& 'n lz . / s i th re fe lencc to EN

l4s?2. Ana lYs is {as Pe! io rncd bY

GC/tts.

il{fi,#+tkdt(N.. t : M/20\2/c2t23 O*(Date) : 2013/01 /02 F jk (Pase) : 7 o f 26

Test ReportASM UT

,1/F. WATSON CENTRE, ]6IQNG TIP ST., IIiAI CH!1{C. UONC KONC (ASI{ UT)

rl*,t a +&(Uri t )

tttr*( e tbod)

tilltrlEnd.(uDL)

* *(R€ruI t )

NO. l

**':Ylt:*ral8 / DrDP (Di -i sodecyrp [ l ha la re ) (C tS No . : 26761 -10 0 )

iiilli4+EN r1s? 2, ̂ *"& n &il] x, fA** j i lZ . / { i th re fe r€nce to E} l1 ,1372. r \na lys is ras per fo .ned bycrc/Ms.

t t r+:F*:*+€ / DINP (Di- isononyLphlhalate) (cAs No. : 2as53-12-0)

Aj4*4+EN l13? 2,,\ $"aa h fr *,/ f, *d , r * j t l . . . / s i th re f€ re ! .e ta EN

11372. Ana lys is vas per fo rned 5yrc/vs,

frf,.-iP e--G+e / DNoP (Di-n_octyl

Phthalate) (cAs No. : l l7-84-0)+rqat+rN 1437 2. tt 4E E fr ,e /,4: * { , }& ,114. / { i ih re fe rence io EN1,1372. Ana lys is was per fo r f r€d 6y

@/lts.

6 ,€E / Ac t i io l i l€ (cAs No. : 77536-56-

1 )+*EPA 6oo/R-e3/116 / nfitsdl&(sM), +lt*eJi&*.a&* (D6-PL\,')L\rt t*,4tk*+frx (xRD) / ,xithre le r€nce ro lPA 600/R-93/ r16method, AnaLys is ras per fo .ncd b t

s te reo Mic roscope (S ) , D ispc .s ion

S t , i n i n g P o l a ! i z e d L i s h t v i c . o s c o P e(Ds PtM) and X- ray D i i t rac t ionspec t .oneter (nD) .

&jrAl^18 / Anthophyl l i re (cAs No. l77536-67-5)

t-+EPA 6oo/R-93/rl6 | trlF.tltt(sv), +l{+ad&i&&* (Ds-PLx)^xroq,4+ tLlt+&X (sD) / uirhre le rence to EPA 600/R_93/116nethod, Ana l ts is ias pe i fo rned bY

srer€o l l i c ros .ope (s ld ) , D isp€.s ion

sra in ing Po la ! i zed L ish t Mic roscope( !6 P l \ t ) and X- raY D i f f rac t ion

Spect ron€ter (nD) .

,Flfi,#+Test ReportASV lt(

.I/F, {ATSON COiIRE, T6 I(UNG YIP ST.. Kq'AI CIIUNG. HONC (ONC (AS IIT)

* ,4$. . ) : u /20r2/c2r28 FS(Date) . 2ors/ar /02 F*(Pase) , 8 of 26

rl*{ E +a(U!i t )

riar* tri.fiqEfttt(rol,)

BJF

NO.1++.Ei f / anosi te (c s No. I r21?2-73-s) ++EPA 6oo/R-93/116 / nliff&rt

(sv), r>*.*a*.&is&tt (D€-P! )^xJL*tt h!t*r*r* ()cD) / $iihre f€ rence to EPA 600/R-93/1r6

nethod. An, lys is was te r lo rned by

Slereo I i i c roscope (Sv) , D i spers ion

Sta i ! ins Po lar ized L igh t Mic roscoFe( !6 - [N) and I - ray D i f f !ac t ion

spec t roneter (xRD) .

AZl l / Ctutsot i le (cAs No. : 12001_29_5 )

t+EPA 6oo/R e3ln6 / i.dltFl{*(sM). ri**an,BtF&it (Ds-Hr)e\rc9!,ttL*+frj* (rRD) / rxi thr e te r€nce t o EPA 600 /R -93 /116

me ihod . AnaLys i s uas pe r f o r i ed by

S re .eo ! i c ros .ope (S l | ) . D i spe rs i on

S t r i n i ng l o l a r i zed L i gh t M i c roscop€

{Ds -PL l t ) and ) ( r ay D i f f r a . t i on

spcc t rone !e r ( IRD) .

i Z * i / c . o c i d o l i t e ( C A s N a . : r 2 0 0 r -

2 A 1 )+*EPA 6oo/R-ss/r16 / adF-&*.(sv), ,)&iF ar\,€,t,&{r* {D6-PLV)ex/Lq,* k!* +fr)* (RD) / {ithr e te !en .e t o EPA 600 /R -93 / r r 6

he t l od . AnaLys i s was pe r f o rn€d bY

S le reo l i i c r o5cope (S \ ) , D i sPe rs i on

S ta i ! i ng Po ra r i zed L i gh t M i c roscoPe

(D6 -PL i l ) and X - ray D i f f r ac t i on

sre. t rometc. (xRD).

rFlfi,#+Test ReportASM li(

4/F. {ATSON CENIRE. 16 (lJ}iG YiP ST., I{SAI CHUNG. IIONG KONG (TSM HX)

*4\No.) | v ,A/2012/c2r28 E&(Dat€) . 2o- \3/01/a2 F*(Pase) : 9 of 26

Ilti{ E +&(Un i t )

flitt:t tild,rl8DC(uDL)

,**

lto. t

i t t { .6 / r resol i re (cAs No. : 77s36-68 t+EPA 6oo/R-s3/116 / nGf,&rt(su), }**e{&6*&jt (DS-PLM)^\h,.lr rLt*+&)l {nD) / niirhre fe rence to EPA 500/R 93/ l l6

ne thod. Aoatys is {as Per fo .ned by

s tereo l i i c r .scope (SV) , D i spers ion

s t a i n i n a ! o l a r i z e d L i g h r M i c r o s c o p e(DS-PL l i { ) and X- ray D i f f ra . t ion

spe. t !onetc . (nD) .

.lg{L (azo)1): 1-L*;+. / 4-.dvINoDlPHEML (cAsNo. : 92-67-1)

+tLJiiB 82.02-D \, ,t fi"|anfr /N*& l *XB. / { i th re fe lence to LFGB

82,02_2. Ana lys is ras Per fo rEed bY

c€/Ms,

3

2)t ''xR / B9,IZIDI]$ (CAS No.: e2-8?-

5 )++rrcB 82.02-Dt tL. 4 Ah n fr / fi iAr* ; i l . / s i rh rer€.enc€ to LFGB82.02-2. A.a lys is *as per formed by

cc/]ts.

3

3). 1-i,*? f& /4-diloRo-o_ToLUIDINE **tliB 82. a2- 2-)i t*, ^ aM n tfi / rJlc'lfjll. / {ith reference to !F1;B

82.02 2 . AnaLys is {as Per fo rn€d bY

GC/\lS.

4): 2-*E / 2-NAPHflTYLAIiINE (CAS No.:

9 r - 5 9 - 8 )

t-*r j i ;s ez.oz-zltt*, i ^lah4/q; td l i ,F l . / w i th .e te rcnce !o LmB

42.02-2 . Ana lys is Pa3 Per fo rn€d bv

cc/xs.

,nls,#+l i4(No. ) : xAl 2 012 /c212 8 E*(Dat€) : 2013/01 /02 F* ( !ase) : r0 o f 26

Test ReportASM HK

,I/F, VATSON CENTRE, 16 (lNG IIP ST., (lAI CIIUNC. IONG IONC (AS[t I )

itt E l-& ,det* t*d,riEET(rDL)

* *

lto.1s), *1,*-:?*.i8ft / o-.dVlNoAZomLUE\E (CAS No-: 97-56 3)

,*LFGB 82.a2-Dt)*, ,^fi.laftlt / X9*&&' r ,J . / l ' i th re rerence to LFGB

82.02-2 . Ana lys is ras per fo .ned by

@/vs.

6): +4li{If tE / z-a\llNo-l-NITROmLUENE (cAs xo.: 99-55-8)

**Inca 82. 02- 2ai )+, ^ ^la E & / U*4e&xi. / ry i th rete'en.e to LFGB32 .02_2 , Ana l yg i s r as pe r f o rned by

lclMs.

?): tti.sJ* / P-CBrrRo.ANrrrNt (cAs +*tF.a 82.02-Dri+, ,t$"raft* /qi f&+tx i . / { i th .eference to LF6B82.02-2, .4nalys is ras per forned bycc/Ms.

8): a-Yfi, t ' - |r1S:Xi / 2.a-DIAIIIINoANISOLE (CAS No. : 6r5-05-4)

++LFrjB 82.02-D +, ,)!,fulEn4fr / X*&&,11. / r i th ! . f . rence to LFGB

82.02-2 , Ana lys is vas pe . ro rned by

cc/vs.

3

e): 1,1 - : { . iE:FF} i , / 1 ,4 ' -D1A\,IINODIPHENIL{SDIAI'IE (C{S No. | 1017 1 - 9 )

+*tBcB 82.az-Dr)+., t/t*"Mnft/ fi+{&jlj. / q'ith reference ro LFIB

82.02_2. AnaLys is {as per fo rn€d by

6C/NS.

3

l0) : 3 .3 - : { , f l * / 3 ,3 -

DIq{iRoBENZIDINE (CAS No.: 91-91- r )++lJcB 82.02-D +, '\$"414fr /r*d l+ ; l l . / f l i l h re le lence to LFGB

82.02 2 . Ana lYs is ras Per fo rned bY

c,c/Ms,

3

r r ) : 3 ,3 - :Y l , * . # iFE / 3 ,3 'DIVEIIIOIYBENZIDINE (CqS No.: r I9-90_'l )

+*L!GB 32.\z-D,itr. &+aEfr/\i *d tA in l . / ! i t l r€ f€ ren .e to LFGB

82.02-2 . Ana l ts is *as Per lo rDed by

rc/vs.

3

tr{'et+t+Test ReportASV IlI(

,,/F, {AISON CETERE. 16 KL\IG YIP ST., (WAI C]IUNG- HONIG (ONG (AS'M II()

* , r ' (No.) : v . ,A/20r2/c2r23 SrF(D"t . ) | 2oL3/o! /02 FiR(Page) | l l o f 26

t{{ E +&(uri t )

flltti*ti*ltrlrFc(lDL)

ta*

l{o.l

r 2 ) : 3 , 3 - : f ; C J t E , F / 3 , 3 -

DIMETIm,BENZIDINE (CAS No,: r19 93_7)4-+t FsR Bz. o2-Dr)A, d ̂ le E & / trt+[+bjr]. / qJith referenc€ to LFIB

82.02-2 . Ana lys is tas per fo r f l€d by

cc/ s.

13 ) : 3 ,3 - : ? * -4 ,1 - - t 3 :+? ts ' /3,3 -DtMETtm- l , l -

DIIVINoDIPHEMLMETHANE (CAs No. : 838-88-o)

++r.is,B 82.oz-bf i+, r) ̂ ta E fr / fi*&lfial. / rith referelcc ro LFGB82.02-2. Analys is vas per formcd byrc/vs.

3

14), 2-Pf,*.-5 f&#f / P-cRrsIDlrE(2-VEIIIoI-Y-5-I{ET}n1-ANILINE) (CAS No- :

1 2 0 7 1 - 3 )

i t l i i h , l l . / t r i th re fe !ence to LFGB

3 2 , 0 2 - 2 . t n a l y s i s r . s p e r f o r n e d b t

rc/MS,

3

15) ' a,a - .4. f-* t (S.*&) / a,a -

METTiYLENE-BIS- (2-CIIT-OROAN]LINE) (CAS*+IJi.B 82.02-Dt i+, n, ̂ ]a E tr / \i i& l * ;d . / ! i r r re fe .ence to LFGB

32.02-2 , A 'a lys is vas pe . fo .ned by

c€/Ms.

t 6 ) : 1 , 1 - i " . l L t f , l F / 1 , { -

OXYDI IN iL INE (C s No. | 101-30-1)++LIGB 32.02-Dt il, rt ̂ & E fr / \: *&&al . / s i rh ref€r .nc€ 1o LIEB82.02-2. Ata l ts is was p€r forned byc€/Ms.

3

r7): . ,1 -&, l \ t fF / 1, , t -

TIIIoDIANILINB (cAS No. : r39-65_1)+*ul;B 82.02-b, )*. t\ A$ n I / fi i d th i4 . / v i th re r€rence to LFGB

32,02-2 , Ana lys is ras Per fo rned bv

c,c/Ms,

l8) , S?*& / o-ToLVIDINE (cas No. :

95-53- , r )

4+LFGB 82.02-2tt+, ' \ fu4a n & / \t*&,ih . / {ith r€fer€nce to LFGB

82.02-2. Aia lys is {as Per iorned bv

@/t|S.

3

,r{H,fl+Test Report

4(No.) : KA/2012lc2r28 EJq(Dat . ) | 2oI3/oI /02 F*. (Page) : 12 or 26

ASV HK

1/F, IJATSON CEIiTRE. 16 KUNG YIP ST.. Kq'AI CIUNG. IONG (ONG (ASM K{)

Nlri{ E +tr( g l i t )

*lrt7}* trt.{lrlEftti(irDL)

*;F

!o .1r s ) :2 ,1 -= t [ ;B rP+ / 2 ,4 -muryLtNEDt,{\tINE (CAS No. : 95-30-?)

+*r-rt:B 82.o2-b,i*, ', F"ftne/\ifa&,nj. / qJirh referenc€ ro LFEB32 .02_2 . AnaLys i s vas pc r f o rned by

rc/MS.

2 o ) : 2 , 1 . s - : P d * & / 2 . 1 . 5 -TRIME'I[i!1-ANILII,iE (CAS No. . r37-17-7)

'-+LF1jn 82.02-Dt)+, , fr"4antr/f*&&i r t . / v i th re rerence 1o LFGB82.02-2 . Ana lys is vas te . fo rned byGC/ItS.

,r), ,i1iPl,**IF / o-ANrsrDrNE (cAs ++LrcB 82. 02- 2), )4. tl R4zE 4 / Ni*{l*itl. / {iih .ef€.enc€ to LFGB32.02-2 . Ana lys is {as per fo rned by

5ClMS.

22), ttt *lEft,f / p-,rvrNoAzoBB{zg,rE(CAS No. : 60-09-3)

+tr.FsB 82. 02- 2tl )I. rl Rh E fr | X*fl&nl. / xrith rererenc€ ro LF6B82.02-2. Analy6is was per lo ined tycc/Ms.

3

23), 2,1- : i f lL fJd / 2 ,4-XYr-rDrNE (CAS ++LFGB B2-a2-Di j* , r) ,^ iaE{t / fi+{{ ix l . / { i th r€r.r€nce to LF6B82,02-2 . Ana lys is vas per io ln€d by

GC/MS.

3

24), 2,6- :P{ ,* .& / 2 ,6-XYLTDINE(CAS No. : 3?-62-7)

++rrcR 82.02-b, )4, Pt ̂E E k / \if{lA,il. / rvith reference ra LFGB

32.02-2 . An, lys is vas per fo rmed bym/\{s.

3

* . t !&4h\ / Rad ioac t i ve subs tan .er l+ i i * t * (ce isc r cou i le . )

nlfi,*r+Test ReportASV H(

4/F, {ATSON cs*IRE, 16 KUA-_G YIP ST., KSrtI CIiWG. HoNG rcNC (ASM HX)

l sn (No te ) :

lh t ' (No.) : M/2012/c2r23 Et jh(Date) | 2or3/or /02 Fjk(pase) : 13 of 26

1. da lka : ppn ; 0 . l r t% : l000ppD

2 . n . d . . N o t D e r e . r e d ( t i l * * )

3 . MDL : r , te lhod Det€c t ion L in i r ( r t t . t i i ! lEE6. )

1. - = Nor Resulared (*f , r t ta)5 , # = a . Pos i t i ve neans t he p resencc o f C rv ! on t he t es red a . cas

(Pos i t i ve i+ jil li, E.!{.ti ill r'l i1l Js )b . N€ga t i ve means t he absenc€ o f C 'V I on t he t es ted a .eas

oreea t i v. t i 'l ni E&i1i jnl }!j i llJs)The d . tec ted concen l ra r ion in bo i l ing- ra ie r -e !k .c l ion so lu t ion is eguat o r g rearer than 0 .02 ng lkg* i th 50 cn , tes red a .eas . Z l l / : t s ' * .XA lo .02 ic lks w i rh 50 cn , ( tes ted a .eas)

8 . . ' : eua l i ta t i v€ ana lys is (No Un i t ) t , t i+ { . ( *+ t :a )9 . L& z l t (PVc) ,1 r .g , r i ve = Undeted .b te t * ,M, i i l x l t ' J ) ; pos i r i v€ = De!ec tab l€ t t ,E(e .d j t , l t ! )r0. .6i$t,E+{itr*$E | <o.r%-roo% ' El&t$.FqttJt*+A',(i$t *a EliltitEr, fp""iti"..l , *.iA*ztF*ie

6 f N " g , i i " . l . / T e s t i n s r a n g e o f a s b € s t o s q u a L i i a t i v e a n . l y s i r i s l r o n l e s s r h a n 0 . 1 % r o 1 0 0 % .

The j udsn€n r c r i i e r i on : asbes tos f i be r s be i . s f ound i s shoy ! as ,Pos i t i ve i . sbes tos f i be . s no1 b€ ing

found i s shosn as 'NeAa r i ve " -

r1. l(eaative./Posirivet: I+it#.s.{iirl'it4+,14* tf .tl*,rtr* *.16 *l fr rhjrl€4tE}t#+,iar€ rL+{6trI* * ,-*iittrtT*F&aet.ttE4+ilt ( -*{4&tr*6tlg4ifi tr! 4",f +,ao.2usv/hr) . .1' j*jtd iA.6.,if*4 f, * lfr r+ ' *.+,af*.S+*f,(Nesa! i"e") ItEE,&, ' ,hFld.&'arirttr*&r+ ' ii*f (p."i t i,.") .(The tes i resu l r o f oe iser counrer i s t rom .onpar iso ! be t reen

and env i ronnent backBround. In sener . l , there is L i l t lerad ia l ion dose ex is t ing i . €nv i ro .hen i . (Rad iar ion ddse I roh env i ronnentbackground usua l ly l€ss than or equaL to 0 ,2USv/hr )The tesr resu l i i€ss tha ! e !v i ro lnenr backSrourd vas sho{n as Nesat ive* ;

rhe resu l t s rea ter than env i ronnent ba .ksrou .d {as shovn as Pos i t i ve" . )

12 . .s i i l i l l * ,dscs* { t f rAE* . t i (Th . Asbes tos tes t uas subcont .acred to o ther scs labora tor r . )

13 . * . { ,a f i i r l i {&scs* lo t rh€* { i ( rhe Pvc tesr ras subconr racred ro o rh€ . s6s kbora to !y . )

11 . , l r * iF l t t6s6s* lg l l id * , t t (The Red phosphorus tesr las subconr rac ted to o th€r scs Labo ' to ry . )

;;: -d'"i;];l;'

,. il;.i bitr; i;;; innid itii;G.^..' c-d;.; d si-e entud dlirld .6rd. oi rcqqla q !o-bh i !w 3q! coD^!n*!4@4!q! b a^d br

d.;; i b;.ida;-i ' 'd; b i"-i -d c-dr*' b.ebe^.ooml;;iid- L** d6i.. b'€d Ary h;ckd'.dds. i$y rM c.;p*. r.,sao" o-..a. iu' a*..d;"e, b ad'-d .-B . tur d

| , . s 8 { i n r' - - " ' * , . ' D

fi{*,#+Test ReportASM H(

*q lNo. , : IA/2012/C2723 A*(Date) . 2ots/or /02 l ;&(rase) : 14 of 26

1/F. {ATSON CE\TRE, 16 (!NG YIP ST.. I{{AI CHUNG. IIONC KONC (ASM I{)

1) 'Eli,aTrtrriarari?f {[eeiarE*.( *dJrrt}t'ar$rf ) /Th€e $mde @ d$dled roGlly by

€ b bd* nwch.d ( C'€

a jdra^l : tlet / Nafr. or s's p.con *no m.d. masuErcnt Al.t Chans

raeii{ j sfd.Mddd firE&ri.n / oo*toi Aodr,r. i{a, ra, tll{, tt+- /

Not -r(1) rt ttrF t,l ittlr" ^ftit tr{ l9lt ' r" {!t s(Fssc+t / For non'metallic mat naladd dkdare dag€.ti6n rc.gent and h6.t to go_95! -

(2),tttt,&lttlr"\a!^,"t!::t4**. /FormBtallicnaleri.l,.dd puEwatar.nd h.at to bollhg.

chaE. dm.a$crcnt Ray Chans

rliallsit / s.mpr. M.@rem.d

&*n E &e r'rnt 6, j!6 nai!1i.'t rL($f *.'t6) / add disGton by iui.u. add.Fdd on dmmd 3MC. htuid (*

4altali,i,a.ji&ttla

l'tr{ +ttc+t4j tra( , rcFAEs

,r{*t#+'Test ReportASM IIK

,1/F, WATSON CENTRE, T6 ruNC

lh t '$o.) : r ,A/2012/c2r28 A$(Dat . ) , 2013/0r /02 F*(Pas€) : 15 of 26

lIP S1.. KINI CHUNC. HONG {ONG (ASM HIo

, *t*/t *t+E *trrtff / PBB,PBDE analylical FLOW cHARr

1)tl {,^! . l'*rf / Nam€ of the peFon who made measurement Anson Tsao2),il{ff1.,-: #16* /Name orthe person in charge of maasulensd: Ray Chang

,^rli{t!lF / Fnst lesring p

,&*,1*61*aF / Oplional screen proc€ss ------

4l&{rl / Confimation prcess -.-}

Screen analysis / ir6r|n- | screen anarysrs / rrh?t, | !- | ' t !: . . . . . . . . . , . . . . , t - . :

SamDb enudion &,s+*/Sot''let me$od td+F.ti

concentrate/Dilut€ Extlacied solurion+*n,t*/##

Filler +*.itGlt

tL16f fi{nd}tr

trkffi liffi f"#iffi -"l'+k:'}ffi l'ff-ffi lif"H# jjir#ifff i'l;!

& * t u . ; ' ! . r ' t s b ! c o Piij,'.iti.i*-ii. i

"iy: i*;;co. * -.o*urv

" " " cr.n in

;;";;d."tuihred...i;^db rcrrcdd.mp,itur ".tu f@er ruy b e$sof*!,tt?di,to" *.,1 3,'fr;i*, ""*

t,," *-

,r{Bt*E+Test ReportASV II(

{/F, W.ATSON

1 )

A . h , A , E 4 / s t e e l , . o P p e r , a l u n i n u n , s o l d e ' .!+.,4*,l.n, n n&,ts.* /Aqua regia, INO', HCl, llF, ]]1ol

,tt* 4i*,i(nd / no"/HF

+ , , A J e , f i t / G o a P l a r ' o u s o ' a l l a d ' u t r " - d d i '

'E ,lal / t0rlo.

! ! f / P l .s l i c aea,t*.^,4| l , { l t / H$o.. Plo, $n. Hcr

lF^.6l{*tktj6l+ / anv acid td total digestrod

ffi tl'ff *ir;ii,r.1flii*:rffi i:iffi I'iffi ,-:#,f ii,ifr 'mi#ii$r#-i#.-F--:l'r.xit*llliHffi$HTii,;l ;#;";+:;;riui*'o--ae""'- r'o.ry-n

;":::;;; ;;;;-.. ;;,. ;.i a4 dh@r - r 6 dfiqi4:o,:x:add':" ".1T fl iil.q" *, ,,". . "*,

,. .*' .."

CEIIITE, 16 rur\-'G YIP 51- , IirAI CllWG. IIONG KoNG (-As fiX)

*f* ' rTatf i ,#na&+ ' #"e. i . t8,4 " / rhes€ sanpres were dissolved rotarrv

6y pre-cond i t ion ing ne thod a . .o rd ing to be lo r f los 'har t '

t{i*,r',F : *&iE / Nanc of the Person vho madc rcasurement: At€x chans

x ' l&9 i -^ . : l i j € * / Nane o f the pe lscn in charce o f neasurenent r Rav c [ans

n*r,( rcP-AEs +'' i!,t{b,fren(F lor Chart of d is .s t io ! for th€ e l@ents analys is Per forned lv I (P-AES)

*q(Na-) | r 'A/2012/C2r28 A$(Dat . ) | 2o l3/ar /02 q*(Pase) : 16 o l 26

2 )

3 )

{ * , ' f 6 f t s / c u i n a ' P . € p a . a r i o n

t lg ,* .s t* / sanpre Me,s! lenenr

&d4 E*g&itre}xit+&*e4i,*rL (*eTifr i) / ^cid disesrion bvs ! i t a6Le ac i d depend€d on d i ! f e ren t sa f , p l e na le r i a l ( as beLo ' t ah l e )

i&* / F i L t .a t io !

tE / Res id le

1) &Ee* / A lkaL i Fus ion

2) t&E * / HcL !o d isso lve

6[*Atf .4"*4it :*d. / rcP-Als

,F|fi,#g, i IE(No. ) | (A/20r2lc2128El lh(Date) | 2013/01/02 F:k. (Page) : 17 of 26

Test ReportASM HI(

1/F. C'ATSON CET'IRE. T6 tiUNC YIP ST.. (q'AI CIUNG- HONC KONG (ASM H()

+i,Er[tl|]ffrft.E /Chlorinated Flame retardant analytical flow chart

1) rllt, ,t : **4 / Name ofthe p€con who made measurem6nl: Anson Tsao2) ;rlitA t,( : t[.16* / Name ofthe person in charge of measurement Ray Chang

r t*7i)i(Ref€ronce melhod): USEPA 3€"40r jrl$,4 a oest rtems): PcBs, cP, MccP / t r.s*, s..lbzrt, f ,{s,lLErt.

6r{*d+*Sample extraciron by ofganic solvenl

+Frit;t6/4sfConc€ntrate/Dilute the extlacled solution

',r fi.rc.i ,rt d./€ + ifiie{t fl *l*,!lAnalysis r €s p€rfomed by GC/ECD

**. / Dab

,r{a*E+Test ReportASV HK

+{.|nillJ}frfi,€ /

Chlorinated Flame retardant analytical flout chart1) Ilit^l : **4 / Name ofthe peFon who made measurement Anson Tsao2) illJl A l,/, : t!.16* / Name of the person in charge of measurcment Ray Chang

. t*t;i(Reference method):us EPA8270D, US EPA 3540r, i t4 a (Test l tems): PcNs, PcTs, Mirex / t{,+, ,n: lsf,r{rdf '

*.:A / Datia

;;;";::;;;;;;.!; t;"d* d|,!rTIl':::::T:.T:-1i:::;Tj::fr#,sij;ri:*.'r.x"':l.";li.1i.::1lXtrflf irir"l&;i"Tli.:i:T{i"liir:i::i*}":-";.-l#ru:",l::.:':.::;;;;.'-1:,":l'"':"*:,1:,:nmmfl trI#flrrffi*15{s*s#g".#;lif-ffi

I t r t (No.) : (A/2012lC2123gJh(Dare) . 2013/01 /02 F lX . (Pase) : 13 o f 26

CENTRE, 16 K!\iC IIP S1.. I$AI CHI,NC. IONG ](oNG (ASM HK)

trfiaal+*Sample odraction by organic solvent

+cuut*/irt#Concentrat€/Dilute the extracled solution

'r i,*B,t {i f *&,r} +iAnalysis was performed bY GC/MS

fi{*,#+Test ReportASM lt{

&4(No. ) : ( ,a /2012lc2128EIJE(Date) : 20l3 l01/02 F*(Pase) : re or 26

1/F. WATSON CEIiTRE, 16 KJNG Y]P ST., (q'AI CHUNG- HONG KOXC (AS.I{ gI)

*I"L*brilEbtr'fren tAnalysis flow chart tor determination of PVC in material

I )jrll{ - I : 4dr' / Name of the pelson who made measuretnent Jovce chiu2)}]}\.Al^. : iiis /Nameotthe peEoninchaEeof measurcment RoserLin

4r4c4lrtrE*. /Check wave-number of GCI bonding

,r{fi,*E+A€(No.) : ( /20r2 lc2128 Eik(Date) : 2 t ) r3/ar /02 F*. (Pase) : 20 of 26

Test ReportASM H(

.,/F. WATSON CENIRE 6 I(NG TIP ST., KqJAI CHUNC. fiONG KONG (ASM N<)

t *+,t ,f,el / Analyticalflow chart of halogen content

1) jtl$,l'q : ;**4/ Name oflh€ percon who made measurcmenlr Jean Hung

2) ri, l l ,\ : ti19 +/ Name of the person in charge of measurement Ray C hang

Silif-T:lf , iili"'T slf i,f Hn i -i'. -!.:

;;:#;;;;;;;-i;;;, and dreE nry b D36so+eg:111di']"." *'f gi.9.:1i6 """

'"" *-,',". '""-"*"

+t&&rRAlt+ttgt /Sample picfure and repod number

{.""ti 44/r}*. /Sample pretreatmenvseparation

f,fteJfittr"*r.ii.s{ + /Weighting and putting sample in c€ll

fr.fi,*4+/4*tOxygen Bomb Combuslion / Absorption

t i#4d afi* iDilullon to fxed volume

*+n k$,.t>* tAnalysis was perfomed by lC

I ' -mo 'n ' : a

,r{s,+r+Test Report,{SM H(

4/F, q'ATSON CO{TIE, 16 KINC Y]P ST., (qJAI CIIIJ}IG. IIONG KONG (tSM !T)

, ! t€(No,) : xA/2012lC2128A H ( D d r e ) : 2 0 r 3 0 l 0 ? F i t s ( p a s e ) : l t o 2 6

Efi[Rjtft*.Al / Analy3ls flow chan for determinatlon of A3bestosr l,ld^l : ft3t8 / Name ofthe pe6on who made measurement Mctor Kaor dii I I A : *rr;( / Name of lhe pe6on in charge of measurement Wendy W€i

( ++ ti*(Rete.ence mothod): EPA 600/R43rt l6I

Asbestos nber is absent

Not containing AsbestodAtt / Negalive

+*.4J*+ / rranspodation and Slorage

+ifi[8,at!.# / P€paralion of prtnary analytc€l sampls

nrtf,dtt.itnl /Examinalion by staBomicroscop€ (SM)

,)** en,A*.li&tzltr'&t / asbestoe idenlircalion bydBpersion staining polarized light micDscope (OS-PLM)

r9,ttd4,tEd4{tsc4r44 rra f <Contmu€when problems ae encounte€d wth DS-PLM

andor for quality assu€nc€ purpos€s

#A+ll*f / Intede.ence matix Emov.l

,.l{* gn]c{s&rtzi#€ /Albeslos idenlificstion bydisler3ionslaining polanz6d lighl miorosdpe

x trttjtri.EfirGt /Asb€stos id€nlification by x{ay

difi raction spocllomeier

+tafr** tAsbestos f ber 6 Pr€s€nl

,n|fi,#+Test ReportASt! l(

.{/F, OATSON CENIRE, T6 TING IIP ST., KIAI CH!],IG. HONG XONG (ASiI HK)

t|,**frfrtEn / Analytical tlow1) 'nlit,,,! : *** / Name oflhe person who2) jrlS,fi fr- : tE.t6+ / Name ofthe person in

&4\ l to . ) : Y\A/2a!2/C212aES(Date) : 2013/01 /02 F :k (Pase) : 22 o f 26

chart of Organic-Tin content

made measuremeni: AnEon Tsaocharue of measurement Ray Chang

*.* / Data

corEry t. "r!q t*i!f+!r

liil.-iiiiii',";;..n " *twLsd ftid* mv b et$ri3d*'tnilur:" "*[r3l'i.ilii"id !",hr,,".*q.-. id,,'.,.-,

tr&.* +4 /Semple extraction by organic $lvent

e L&q|U,th1tt EIY IDerived by Sodium tetraelhylborate

+FErlS/ri# /Concentrate/Dilute Extracted solution

R)a re ifi t)<n ro{tl +& lAnalysis was performed by GC/FPD

,F|fi,+E+Test ReportASV H(

l l (No.) : M/20r2lC2r28 q$(Date) | 20L3/0L/02 FjR(Pas€) : 23 of 26

1/F, qJATSoN CEr_lRE, 16 Itu!-C YIP st,, K$'AI cIllNG. HoNG (ONG (AsM IIi)

E*i$-A.tlf *,AI /Analytical fiow chart of TBBP-A{ois1)dq^l : l'*:i / Name of lhe pe6on who made masuEment Anen Teo2) ni i{ I l,/. i n€ * / Name ol rhe peBon in charqe ol measlrenern: Ray chang

t l*{,#,t,oPl@|ffip'!€6

+lF'tA* / Filter

n+'n&1|ttr& / Analyds by Gc/Ms

3dcfudlBmybeB€!€l8]wu:"*.,il3l'iillxd.^",',"**

t fi ,itr / scen analysis

| ' . soo , t d ! r

rr{fi,+E*Test ReportASM II(

4/F, {ATSON CENTRE, 16 K,'NG YIP ST., ({AI CHWG. HONG KONG (ASM HIi)

S4(No.) : K{ /2012lczr28 Elq(Dare) : 20r3/01/02 A*@.se) | 24 ot 26

i*4+:ti+fifiEf, / HBGDD Analytical FLOW CHART

1) ,nls,,/\l: I *4/ Name of the person who made measurement Anson Tsao

2) rl&l lA: tF16 */ Name ofthe peBon in charg€ of measlrement Rav Chang

Data *ll

il{fi,*E+Test ReportASV HK

4/i, vATSON CElirRE,

l t ,4(No.) : I t , l /2012/c2r28 EJh(Dat . ) : 2or3/o l /02 Fl* . (Pase) : 25 ot 26

16 KJNG YIP ST., K{AI CI]UNG.ItoNc rcr6 (AsM l()

Sltl}fiX.Pn / Analytical tlow chait of phthalate content

1)illi{./-F: **tt / Name of the pe6on who made measurement Anson Tsao

2)fil{FI,,. : tFrn+ /Nameof theperson in charseof measurcment RavChans

![le / Dala

iiii:Il,I:H ;il;iifl.:;:i""::;:jiT#;l;il;I;:i:.;;fi;ffi-ffi#;dr:,p";:Ti,:,-:a;:H;;r-n."*-_" i.ry s" c-es,, rcb rc4:n!;b11r, e!.c]c]il.iil":iifirffl*:;;1ff;ffi#;;; iiy,-itrn-_; ""--" rq"ry _r

| , . dooo rn !

tr'lS,#+Test ReportASV HK

,1/F, WATSON CENIRE, 16 XING YIP ST., L'f,AI CIIING. HONG TONG (ASM Ifi)

f i t ' ' (No.) : KA/2012lc2123 E$(Date) : 2013/a\ /a2 F*(?ase) : 26 or 26

, r(i t*,ASiil*i , !{ i.+6,tFtAjd,a*.s/${q. .( r he t €s ted sanp le / pa r r i s na rked by an a fuoe i f i t s sho rn cn t he pho to )

r . l t+g4( rnd o f Repor i ) t

i#"#ff.ifili;1',$!;Yirj}fl r:?iiilfi'i,Fi'i"'#if i"ff#';:"":1r.fi;?11:";::."-;:;"il-+ai*.1r-r,::lri:.;":-:xi::-J;H;.r:.f;i;

c2128

r ' i \ e N I u ! { . . i 1 , r o o n u r

SignFOr (,lUPlease with scs

Test Report No. : KL/201 3/'l 1 827 Date:2013101123P a g e : 1 o f 1 4

HERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04-12 TECHPLACE II, SINGAPORE 563871

Th6 follor^ring sample(s) ll|/as/were submilt d and identifod by/on bohalf of the client as :

HERAEUS I./IATERIALS TECHNOLOGY TAIWAN L

COPPER BONDING WIREiCu, oHF, lvlaxsoft, Maxsoft2, MarSoftLO and RelouCOPPER2013t01t212013tO1 121 f O 2013t 01 t23

Sample DescdptionStyle/ltem No.ColorSample Receiving DateTe6ting PeriodSample gubmitted By

Iest Re3rrlt(s) Please refer to next page(s).

lh!|d fc. .ntl oi b.h|f

I , 's , ror ! r . r

scsTest Report No.: KN2o13]|1a27 Date:2013101t23 Page:2ot14

HEMEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04-12 TECHPLACE II, SINGAPORE 569871

Te3t Resultl3)

PART NAIVE NO.1 : COPPER BONOING WIRE

Test ltom (s): lJnit Method MDL Resultl{o.l

Cadmium (Cd) mg/(9 With refefence to IEC 62321:2OOB andperformed by ICP-AES.

2 n.d.

Lead (Pb) mg/Kg With reference to IEC 62321:2008 andperformed by ICP-AES.

2 n.o.

Mercury (Hg) mg/Kg With reference to IEC 62321: 2008 andperformed by ICP-AES.

2 n_o.

Hexavalent Chromium Cr(Vl) by boilingwater exttaction#

With reference to IEC 62321:2008 andperfomed by boiling \ ater extfaclionMethod.

0.02mg/kewith 50 cm

surface

Negative

Hexavalent Chlomium Cr(Vl) Fg/cm2 With reference to BS EN ISO 3613:2001for Hexavalent Chromium, Analysis wasperformed by UV-VIS Spectrometry.

o.02 n.d.

Hexavalehl Chromium Cr(Vl) mg/Kg With referenc€ to lJs EPA Method 3060A& 7196A fo. Hexavalent Chromium.Analysis was p€rformed by UV-VisSpectromelry.

2 n.d.

Hexavaleht Chromium Cr(Vl) by alkalineextraction

msyK9 With reference to IEC 62321: 2008 andperfomed by IJV-VIS.

2 n.d.

Sum of I BBs

mgKg With feference to IEC 62321: 2008 andperformed by GC/MS.

n.d.|obiohenvl 5 n.d.

Dibromol Dhenvl 5 n.d.Tribrcmoiohenvl 5 n.d.Tetrabrol 5 n,o,

5 n,o,Hexabrol obiohenvl 5HeDtabromobiohenvl 5 n,d.O6{abromobiohenvl 5 n d .NonebrolrobiDhenvl 5 n.d.Decabrol obiDhenvl 5 n.d.

subj'. ' 'o s G.nd!cod(oi! d s.N€d.drciclh.ldooBld9&br.dlo]

scsTest Report No.. w201v11827 D'iLe:20'tstl1t23 Pase:3of 14HERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #O+12 TECHPLACE II, SINGAPORE 569871

Test ltem (s): Unit Msthod [IDL ResultNo.1

Sum of I BDEs

mg/xg With reference to IEC 62321: 2008 andperformed by GC/ltIS.

Monobrorhodiohenvl ether 5 n-d-Dibromo(ohenvl ether 5 n.d.Tribromodiohenvl ether 5 n dTetrabror odiDhenvl elher 5 n.d.Pentabroimodiohenvl ether 5 n.d.Hexabromodiohenvl elher 5 n.d.

lodiDhenvl ether 5 n-d.Octabron)diohenvl ether 5 n.dNonabmrodiohenvl ether 5 n-d.DecabrcdrodiDhenvl ether 5 n-d-Antimony (Sb) mgikg With reference to US EPA Method 3052

forAntimony Content. Analysis r BsDerformed bv ICP-AES.

2 n.d.

Hexabroftiocyclododecane (HBCDD)(CAS No.i 25637-99-4)

m9Kg With reference to US EPA 3g0C: 1996method. Analysis wEs performed byGC/MS.

5 n.d.

Tetrabromobisphenol A CrBBP-A) (CASNo.:79-94-7)

m9Kg With reference to DIN 53313. Analysiswasperformed by GC/[,S.

1 0 n.d.

Perfl uorooctane 6ulf onates(PFOS - Acid, l,iletal Salt, Amide)

mgKg With reference to US EPA 3550C: 2007.Analysis v€s performed by LC/[,|S.

1 0 n.d.

PFOA (C,AS No.: 33S67-1) mg/Kg With reference to IJS EPA 3550C: 2007.Analysis\ as performed by LC/MS.

1 0 n.d.

HalooenHalogen-Fluorine (F) (CAS No.: 14762-94-8)

mg/Kg ,l/ith reference to BS EN 14582:2007.Analysis wEs performed by lC.

50 n.d.

Halogen-Chlorine (Cl) (CAS No.: 22537-1 S 1 )

m!yKg With reference to BS EN 14582:2007.Analysis w?s performed by lC.

50 n.d.

Halogen-Bromine (Br) (CAS No.: 10097-32-2)

mgKg With reference to BS EN 14582:2007.Analysis was performed by lC.

50 n.d.

SGSTestReport No.:KA/2013/1'1827 Date:2013to1t23 Pese:4o114

HERAEUS I'ATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #O+12 TECHPLACE II, SINGAPORE 569871

Test ltem (s): t nit Method MDL ResultNo.1

Halogen-lodine (l) (CAS No.t 1436244-8)mg/kg With feference to BS EN 14582:2007.Analysis was pedomed by lC-

50 n.d.

BBP (BerEyl butyl phthalate) (CAS No.:8+6&7)

% With reference to EN 14372. Analysis wasperformed by GC/MS.

0.003 n.d.

DBP (Dibutyl phthalate) (CAS No.: 84-74- % With reference to EN 14372. Analysis wasDerfomed bv GC/l S.

0.003 n.d.

DEHP (Di- (2-ethylhexyl) phthalate) (CASNo.: 117-81-7)

With reference to EN 14372. Analysisu|a6performed by GC/[,|S.

0.003 n.d.

DIDP (Diisodecyl phthalate) (cAs No.:26761{0.0)

With reference to EN 14372. Analvsiswasperfomed by GC/l'rS.

0.0'l n.d.

DINP (Dijsononyl phthalate) (cAs No.:28s$n2:0)

% With reference to EN 14372. AnalysiswBsperformed by GC/IL4S.

0.0r n.d.

DNOP (Dl-n-octyl phthalate) (CAS No.:117-84-0\

% With reference to EN 1 4372. Analysis w€sperfomed by GC/MS.

0.003 n.d.

DEHA (Di-2-ethylheryl adipate) (DOA){CAS No.: 103-2&1)

% With reference to EN'14372. Analysis wasoerfomed bv GC/MS.

0.003 n.d.

DIBP (Di-isobutyl phthalate) (CAS N0.:84-69-5)

% With reference to EN 14372. Analysis wasperformed by GC/ltIS.

0.003 n.o.

DMP (Di-hethyl phathalate) (CAS No.:131-11-3)

vo With reference to EN'14372. Analysiswasperformed by GC/l'rS.

0.003 n.d-

DPrP (Dirpropyl phthalate) (CAS No.:131-r6-8)

% With reference to EN 14372. Analysiswespertormed by GC/MS.

0.003 n.d.

r".Ji

Test Report No. : KN2O13|11827 Ode .2013101123 Page: 5 of 14

HERAEUS IUATERIALS SINGAPORE PTE LTDALK 5OO2 ANG MO KIO AVE 5, #04.12 TECHPLACE II, SINGAPORE 569871

Note : 1. mg/kg = ppm ; 0.1wto/6 = 1000ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 . " - " = N o t R e g u l a t e d5. # = a. Positive means the presence of CNI on the tested areas

b. Negative means the absence of CrVl on the tested areasThe detected concentration in boiling-wateFextraction solution is equal or greaterthan 0.02 mgy'kg with 50 cm2 tested areas .

6.'" = Qualitative analysis (No Unit)

@Outlawing PFOS as substances or preparations in concentrations above 0.001% (1oppm), in semi'finishedadicles or pads at a level above 0.1%(1000ppm), in textiles or other coated materials above 'l pg/m'.

Test ltom (s):

DCHP (Di-cyclohexyl phthalate) (CASNo.:8,S1-7)

reference to EN 1 4372. Analysis wasperfomed by GC/MS-

DEP (Di-ethyl phthalate) (CAS No.: 84- feferenc€ to EN 14372. Analvsiswesperfomed by GC/MS.

DIOP (Di-isooctyl phthalate) (CAS No.: reference to EN 1 4372. Analysis wesperfomed by GC/IVS.

DNNP (Di-n-nonyl phthalatexDNP) (CASNo.:84-76-4)

reference to EN 14372. Analysis {raspertomed by GC/l/lS.

DPP (Di-18-0)

I phthalate) (CAS No.: 131- reference lo EN 14372. Analysis wasperfomed by GC/MS.

ONHP (Di-n-heryl phthalate) (CAS No.: to EN 14372. Analysis wasperformed by GC/MS.

Test Report No.: KN2013111827 Dale :2013101123 P a g e : 6 o f 1 4

HERAEUS MATERIALS SINGAPORE PTE LTOBLK 5OO2 ANG I/|O KIO AVE 5, #X-12 TECHPLACE II, SINGAPORE 569871

1) Th€sesamplesrere di$olred totally by preondilionins method a@rdins to betowtl@ charr. (c.5+tesr

method excluded )

2) Nahe or th€ person who made measuremnt Arex Chans

3) Name of the peBon in charse or measuEment Ray Chans

H9

S*1, @pp.i aluninum, sold.r Aqua Egia, HNO3, HCl, HF, H,O

Gold. pl.linum, pall.dium, €Emic

H,SO,, H,O,, HNO1 HCI

Any €cid ro iot ldigesrior

A.td dlt.6lion by suilabl.6.id

depandad 6n diri.r.n ianpte

naredal {as bdM trbl.)

1,5-diphenylBrbazide ror

Test Report No. : KN2013h1827 Dale : 2013101123 Paoe : 7 ol 14

HEMEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG I,IO KIO AVE 5, #04-12 TECHPLACE II, SINGAPORE 569871

PBB/PBDE anallrtical FLOW CHART1) Name of the oerson who made measurement Anson Tsao

2) Nameofthe percon in charge ofmeasurement Ray Chang

Firslteslingprocess -----------'

Oplional screen process

Sample exhaction/ |Soxhlet method I

Concenirate/Dilute IExtracled solution I

_ - - - - - - - - - - - - - - -

I Filter I_ - _ _ _ - - - - - - - _ _ - -

Confirmation process -.- |

Screen analysas

Analysis byGC/MS

I , s6 o ,a , r !

Test ReportHERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04-12 TECHPLACE II, SINGAPORE 569871

SEel, coppe( aluminum, solder Aqua rcgia, HNOr, HCI HF. H,O,

Glass HNO3/HF

Gold, plalinum, palladium, ceramic

Silver HNO 3

Plastic H,SO4, H'O', HNO3, HCI

Others Ary aqd io toial digestion

No.:KA,/2013/11827Oale | 2013101123 Page: 8 of 14

1) These samples were dissolved totally by prc-conditioning method according io below

2) Name of the person who made measurementi Alex Chang3) Name of lhe peBon in charce ol measurement Ray Chang

Flow Cha of digestion for the elemenb analysis performed by ICP.AES

Cutting . Preparatron

Sample Measurement

Acid digesiion bysuitable acid depended on diffe€nlsample meterial(as belowtable)

1) AlkaliFusion

2) HCltodissolve

Test ReportHERAEUS IIATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5. #O+12 TECHPLACE

No. . tG/2013/11827 Dele :2013101123 Page : I of 14

SINGAPORE 569871

Analytical flow chart of PFOA/PFOS content

1) Name of the oe6on who made measu€ment Anson Tseo

2) Name of the person in charge of measurement: Ray Chang

: i : r ! r - r ! a i ! . d r i : . I : l r l i n ! i ! r . . r . , . i rN r

Analysis was perfomed by LC/MS

scsTest ReportHERAEUS IIIATERIALSBLK 5OO2 ANG MO KIO

SINGAPORE PTE LTDAVE 5, #O+12 TECHPLACE

No. I KN2013h1827 Date 2013101123 Page: 10 of 14

SINGAPORE 569871

Analytical flow chart of phthalate content

1 ) Name of the De6on who made measurement Anson Tsao

2) Nameofthe person in cha€e of measurement Ray Chang

I , . s6 t r '00 nr

Test ReportHERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04-12 TECHPLACE II, SINGAPORE 569871

No. : KN2013111827 Date:2013101123 Paoe : 11 of 14

HBCDD Analytical FLOW CHART

1) Name ofthe Dercon who made measurement Anson Tsao2) Name of the person in chaEe of measurcment Ray Chang

Data

Test ReportHERAEUS IVATERIALSBLK 5OO2 ANG MO KIO

No. : Kr'r'2013l11827Date:2013101123 Page:12 o1 14

SINGAPORE PTE LTDAVE 5, #04I2 TECHPLACE

1 )

2)

SINGAPORE 569871

Analytical flow chart of halogen content

Name of the pe6on wfio made measuement: Jean Hung

Name of the person in charge of measurement: Ray Chang

Sample picture and repod number

Weighting and puttng sample in cell

Oxygen Bomb Combustion /Absorption

p!ddon see ds"d sd; Ary hd;rcr*d! Ehd*" r ani rhe c;tsry, !d. Esersb I t 's' ' .."d." d.*..d'. ih' d*. '

SGSTest Report No. : KN2O13|11A27 Date:2013101123 Page i 13 of 14

HERAEUS MATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04.12 TECHPLACE II. SINGAPORE 569871

TBBP-A analytical flow chart

1) Nameollhe o€rson who made measur€ment Anson Tsao2) Name of the p€Eon in charge of measurement Ray Chang

Denved bv acetic acjdConc€ntEte/Dilute Enracled solulion

I

Data

Samole extraction bv Solvent exttaclion

Test Report No. : Kr'J2013/11827 Dale : 2013101123Page: 14 of 14

HERAEUS I,iIATERIALS SINGAPORE PTE LTDBLK 5OO2 ANG MO KIO AVE 5, #04-12 TECHPLACE II, SINGAPORE 569871

" The tested sample / part is marked by an arow if it's shown on the photo. '

" End of Report '"

ebdoi c bhr doan. in lbFdbr

LL827

LL827

' ' ' I a o

October 3, 2012 Littelfuse, Inc.

Annex 7: Applicable RoHS exemptions