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La6 Works - Certificate of Analysis Report Reference: Original Test Report Comhairle Contae Dhun na nGall Donegal County Council Central Laboratory, The Kube Magheranan Letterkenny 074-9122787 Sample No.: 162501280 Sample Date/Time: 21/04/2016 @ 10:40 Category: Landfill Monitoring Sample Method: Grab Entity: Station: Muckish Sw 1 Laboratory: Donegal CO Council Template: Muckish Biannual SW Analyst: Donegal COCO Muckish Landfill Sampled By: Eddie Carr Sample Notes: .. . -_ .- Maximum Limit -- - -_ -- -- __ -- -- __ -- Customer Name: Landfill Monitoring Donegal Co. Council Sample No. - Laboratory: Minimum Limit __ -- -- _- -- -- __ -_ -- - Contact Details: ~ ~ Parametedunit Ammonia (as N) mgll BOD mgll Chemical Oxygen Demand mgll Chloride mgll Conductivity @ 20°C VSlcm pH pH units Suspended Solids mgll Dissolved Oxygen (Measurement) keep mgll Temperature Degrees C Visual Inspection Descriptive Julie McMahon Central Lab The Kube, Magheranan Letterkenny 0749122787:0872861096 julie.mcma [email protected] Customer Reference: Landfill Compliance Monitoring Test Method 162501280 21/04/2016 Cooler Box OK 21/04/2016 07/06/2016 Origir Test Date 09/05/16 2110411 6 21104/16 2610411 6 2 110411 6 21104116 25/04/16 2 110411 6 21104116 21104/16 Test Report RESULT Accredited* Sub-tontract" 0.531 C l 9 21.84 77.8 7.4 c6 10.2 9.3 0 SIGNED 07/06/2016 Dr. Joe Ferry. Laborntot$ Manager This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of c 1 MPN/100ml is obtained. Notes 4 ............ lssue 1 September 20 15 Page 1 of 1 Print Dale: 07/06/2016 For inspection purposes only. Consent of copyright owner required for any other use. EPA Export 30-08-2016:02:06:12

Certificate of Analysis Report Reference: Original Test Report · La6 Works - Certificate of Analysis Report Reference: Original Test Report Comhairle Contae Dhun na nGall Donegal

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La6 Works - Certificate of Analysis Report Reference: Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Mag heranan Letterkenny 074-9122787

Sample No.: 162501280 Sample Date/Time: 21/04/2016 @ 10:40 Category: Landfill Monitoring Sample Method: Grab Entity: Station: Muckish Sw 1 Laboratory: Donegal CO Council Template: Muckish Biannual SW Analyst: Donegal COCO

Muckish Landfill Sampled By: Eddie Carr

Sample Notes: .. . -_ .-

Maximum Limit

-- - -_ -- -- _ _ -- -- _ _ --

Customer Name: Landfill Monitoring Donegal Co. Council Sample No. - Laboratory:

Minimum Limit

__ -- -- _- -- -- _ _ -_ -- -

Contact Details:

~ ~

Parametedunit

Ammonia (as N) mgll

BOD mgll

Chemical Oxygen Demand mgll

Chloride mgll

Conductivity @ 20°C VSlcm

pH pH units

Suspended Solids mgll

Dissolved Oxygen (Measurement) keep mgll

Temperature Degrees C

Visual Inspection Descriptive

Julie McMahon Central Lab The Kube, Magheranan Letterkenny 0749122787:0872861096 julie.mcma [email protected]

Customer Reference: Landfill Compliance Monitoring

Test Method

162501280

21/04/2016 Cooler Box OK 21/04/2016 07/06/2016 Origir

Test Date

09/05/16

21 10411 6

21 104/16

2610411 6

2 110411 6

21104116

25/04/16

2 110411 6

21104116

21104/16

Test Report

RESULT Accredited* Sub-tontract"

0.531

C l

9

21.84

77.8

7.4

c 6

10.2

9.3

0

SIGNED 07/06/2016 Dr. Joe Ferry. Laborntot$ Manager

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of c 1 MPN/100ml is obtained. Notes 4 ............

lssue 1 September 20 15 Page 1 of 1 Print Dale: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Mag heranan Letterkenny 074-9122787

Sample No.: 162501281 Sample Date/Time: 21/04/2016 @ 10:50 Category: Landfill Monitoring Sample Method: Grab Entity: Muckish Landfill Sampled By: Eddie Carr Station: Muckish Sw 2 Laboratory: Donegal CO Council Template: Muckish Biannual SW Analyst: Donegal COCO Sample Notes: - - --

Customer Name: Landfill Monitoring Donegal GYCouncil Sample No. - Laboratory: - -~

Contact Details: Julie McMahon Central Lab The Kube, Magheranan Letterkenny 0749122787:0872861096 julie.mcma [email protected]

Customer Reference: Landfill Comdiance Monitoring

ParameterlUnit

Ammonia (as N) mgll

BOD mgll

Chemical Oxygen Demand mgll

Chloride mgll

Conductivity @ 20°C VSlcm

pH pH units

Suspended Solids mgll

Dissolved Oxygen (Measurement) keep mgll Temperature Degrees C

Visual Inspection Descriptive

Test Method

Sample No. -Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date: Reoort Reference:

162501281

21/04/2016 Cooler Box OK 21/04/2016 07/06/2016 Oriainal Test Reoort I

Test Date

06/05/16 21/04/16 2 1/04/16 2610411 6 21 10411 6 2 1/04/16 2510411 6 21/04/16 21/04/16 21 /04/16

RESULT Accredited' Sub-Contract**

< 0.04 < I 12

25.81 79.2 6.7 < 6 10.9 9.3 0

SIGNED + %/ 07/06/2016 Dr. Joe Ferry. LoborntotywMnringer

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/100mls are reported as zero where a result of <1 MPN/100ml is obtained. Notes 4 ............

Issue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Magheranan Letterkenny 074-9122787

21/04/2016 @ 10:30 Sample No.: Category: Entity: Station: Template: Sample Notes: Customer Name: Contact Details:

Customer Reference:

162501282 Landfill Monitoring Muckish Landfill Muckish Sw 3 Muckish Biannual SW

Landfill Monitoring Donegal Co. Council Julie McMahon Central Lab The Kube, Magheranan Letterke n ny 0749122787:0872861096 julie.mcma [email protected] Landfill Compliance Monitoring

__

ParameterlUnit

Ammonia (as N) mgll

BOD mgll

Chemical Oxygen Demand mgll

Chloride mgll

Conductivity @ 20°C VSlcm

pH pH units

Suspended Solids mgll

Dissolved Oxygen (Measurement) keep mgll

Temperature Degrees C

Visual Inspection Descriptive

Sample Date/Time: Sample Method: Sampled By: Laboratory: Analyst:

Sample No. - Laboratory: Sample No. - Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date: ReDort Reference:

Method Limit Test I Maximum -- I --

Grab Eddie Carr Donegal Co Council Donegal COCO

162501282

2 1/04/20 16 Cooler Box OK 2 1/04/20 16 07/06/2016 Oriainal Test Report

Test Date

06105116

2 1104116

21104116

2610411 6

2 1104116

21 I04116

25104116

2 110411 6

2 110411 6

2 110411 6

RESULT Accredited. Sub-tontract**

< 0.04

< I

5

23.82

78.7

7

< 6

10.9

9.5

0

SIGNED 07/06/2016 Dr. Joe Ferry, Laboratory hanager

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of <1 MPN/lOOml is obtained. Notes 4 ............

Issue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Mag heranan Letterkenny 074-9122787

Sample No.: 162501283 Sample Date/Time: 21/04/2016 @J 10:05 Category: Entity:

Landfill Monitoring Muckish Landfill

Sample Method: Sampled By:

Grab Eddie Carr

Station: Muckish Sw 4 Laboratory: Donegal CO Council Template: Muckish Biannual SW Analyst: Donegal COCO

Sample Notes: . ,-

Customer Name: Landfill Monitoring Donegal Co. Council Sample No. - Laboratory: Contact Details: Julie McMahon

Central Lab The Kube, Magheranan Letterkenny 0749122787:0872861096 julie.mcma [email protected]

Customer Reference: Landfill Compliance Monitoring

Sample No. -Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date: Report Reference:

Parametedunit

Ammonia (as N) mgll

BOD mgll

Chemical Oxygen Demand mgll

Chloride mgll

Conductivity @ 20°C @cm

pH pH units

Suspended Solids mgll

Dissolved Oxygen (Measurement) keep mgll

Temperature Degrees C

Test Method

162501283

21/04/2016 Cooler Box OK 21/04/2016 07/06/2016 Original Test ReDOrt -

Test Date

0610511 6 21/04/16 21/04/16 26/04/16 2 1/04/16 2 1/04/16 25/04/16 21/04/16 21/04/16

RESULT Accredited* Sub-tontract**

2.06 9 8

25.81 102 6.8 < 6 10.9 9.5

SIGNED 07/06/2016 Dr. Joe Ferry, Lobornhry Monnger

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of <1 MPN/lOOml is obtained. Notes 4 ............ Notes 5 ............

lssue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Magheranan Letterkenny 074-9122787

Sample No.: 162501284 Sample Date/Time: 21/04/2016 @ 09:55 Category: Landfill Monitoring Sample Method: Grab Entity: Muc kis h Landfill Sampled By: Eddie Carr Station: Muckish Gw 1 Laboratory: Donegal CO Council Template: Muckish Biannual GW Analyst: Donegal COCO Sample Notes: ... . -

Customer Name: Landfill Monitoring Donegal Co. Council Sample No. - Laboratory: 162501284 ~ - - - . - . . . . .

Contact Details: Julie McMahon Central Lab The Kube, Magheranan Lette rke nny 0749122787:0872861096 julie.mcma [email protected]

Customer Reference: Landfill Compliance Monitoring

ParameterlUnit

Ammonia (as N) mgll

Chloride mgll

Conductivity @ 20°C pSlcm

Iron pgll

pH pH units

Phenols pgll

Potassium mgll

Sodium mgll

Total Oxidised Nitrogen mgll

Depth m Dissolved Oxygen (Measurement) keep mgll

Faecal Coliforms (E. coli) MPNllOOmls

Temperature Degrees C

Coliform bacteria.. MPNllOOmls

Total Organic Carbon mgll

Visual Inspection Descriptive

Phenols mgll

Dissolved Iron pgll

Test Method

Sample No. - Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date: Reoort Reference:

21/04/2016 Cooler Box OK 21/04/2016 07/06/2016 Oriainal Test Reoort I

Test Date

06105116

2610411 6

2 110411 6

24105116

2 1104116

2410511 6

24/05/16

2 1104116

0610511 6

2 110411 6

2 110411 6

2 1104116

2 110411 6

2 110411 6

21 I04116

2 1104116

2 1104116

2 1104116

RESULT Accredited' Sub-tontract"

< 0.04

24.82

167.4 49 *** 6.8

c 100 *** 1.7 *** 11.7 ***

0.063

3.8

9.3

4

10.5

13

14.82

0 c 0.1 *** 49 ***

SIGNED @ 6 1 07/06/2016 Dr. Joe Ferry, Laborakry Manager

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of <1 MPN/lOOml is obtained. Notes 4 ............

lssue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Magheranan Letterkenny 074-9122787

Sample No.: 162501285 Sample Date/Time: 21/04/2016 @ 10:15 Category: Landfill Monitoring Sample Method: Grab Entity: Muckish Landfill Sampled By: Eddie Carr Station: Muckish Gw 2 Laboratory: Donegal CO Council Template: Muckish Biannual GW Analyst: Donegal COCO

Customer Name: Sample Notes: - . . .

Landfill Monitoring Donegal Co. Council Sample No. - Laboratory: Contact Details: Julie McMahon

Central Lab The Kube, Magheranan Lette rken ny 0749122787:0872861096 julie.mcma [email protected]

Customer Reference: Landfill Compliance Monitoring

Parametedunit

Ammonia (as N) rngll

Chloride mgll

Conductivity @ 20°C VSlcrn

Iron Vgll

pH pH units

Phenols Vgll

Potassium mgll

Sodium mgll

Total Oxidised Nitrogen mgll

Depth m Dissolved Oxygen (Measurement) keep mgll

Faecal Coliforms (E. coli) MPNllOOmls

Temperature Degrees C

Coliform bacteria.. MPNllOOmls

Total Organic Carbon rngll

Visual Inspection Descriptive

Phenols mgll

Dissolved Iron Vgll

Test Method

Sample No. - Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date: ReDort Reference:

162501285

21/04/2016 Cooler Box OK 21/04/2016 07/06/2016 Orieinal Test ReDort

Test Date

06/05/16 26/04/16 2 110411 6 21/04/16 2 110411 6 24/05/16 2 110411 6 21 /04/16 06/05/16 2 1/04/16 21/04/16 21/04/16 2 110411 6 2 110411 6 21/04/16 24/05/16 2 1/04/16 21/04/16

RESULT Accredited' Sub-Contract**

< 0.04 27.79 92.8 1400 *** 5.9 100 *** 2.2 *** 12.1 *** 0.074 0.9 7.1 145 10.3 145 32.42 0

< 0.1 *** 1400 ***

SIGNED 07/06/2016 Dr. Joe Ferry, Laboratoty Matloger-

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of 4 MPN/lOOml is obtained. Notes 4 ............ Notes 5 ............

lssue 1 September 2015 Page 1 of 1 Print Dale: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Mag heranan Letterkenny 074-9122787

Sample No.: 162501286 Sample Date/Time: 21/04/2016 @ 10:25 Category: Landfill Monitoring Sample Method: Grab Entity: Muckish Landfill Sampled By: Eddie Carr Station: Muckish Gw 3 laboratory: Donegal Co Council Template: Muckish Biannual GW Analyst: Donegal COCO

Customer Name: Sample Notes: -

Landfill Monitoring Donegal Co. Council Sample No. - laboratory: 162501286 Contact Details: Julie McMahon

Central Lab The Kube, Magheranan Letterke n ny 0749122787:0872861096 julie.mcma [email protected]

Customer Reference: Landfill Comoliance Monitorina

ParameterlUnit

Ammonia (as N) mgll

Chloride mgll

Conductivity @ 20°C pSlcm

Iron pgll

pH pH units

Phenols pgll

Potassium mgll

Sodium mgll

Total Oxidised Nitrogen mgll

Depth m Dissolved Oxygen (Measurement) keep mgll

Faecal Coliforms (E. coli) MPNllOOmls

Temperature Degrees C

Coliform bacteria.. MPNllOOmls

Total Organic Carbon mgll

Visual Inspection Descriptive

Phenols mgll

Dissolved Iron pgll

I

Test Method

Sample No. - Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date:

21/04/2016 Cooler Box OK 2 1/04/20 16 07/06/2016 Origii

Test Date

06/05/16 26/04/16 2 110411 6 24/05/16 21104116 24/05/16 21 /04/16 2110411 6 06/05/16 21/04/16 21/04/16 2 1 /04/16 21/04/16 2110411 6 2 110411 6 24/05/16 21/04/16 2110411 6

Test Report

RESULT Accredited. Sub-tontract'.

5.61 32.76 403 70 *** 6.5

< 100 *** 8.6 *** 23.6 *** 0.114 0.6 2.8 21 10.3 28 10.56 0 0.1 *** 70 ***

SIGNED p& 7iLy 07/06/2016 Dr. Joe F&v, Loboroto6 Monnger

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of <1 MPN/lOOml is obtained. Notes 4 ............ Notes 5 ............

lssue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Mag heranan Letterkenny 074-9122787

Sample No.: 162501287 Sample Date/Time: 21/04/2016 @J 11:OO Category: Landfill Monitoring Sample Method: Grab Entity: Muckish Landfill Sampled By: Eddie Carr Station: Leachate Holding Lagoon Laboratory: Donegal CO Council Template: Muckish Biannual Leachate Analyst: Donegal COCO

Customer Name: Sample Notes: ...... -. ..-

Landfill Monitoring Donegal Co. Council Sample No. - Laboratory: Contact Details: Julie McMahon

Central Lab The Kube, Magheranan Letterkenny 0749122787:0872861096 [email protected]

Customer Reference: Landfill Comoliance MonitorinE!

ParameterlUnit

Ammonia (as N) mgll

Chloride mgll

Conductivity @ 20°C vS/cm pH pH units

Total Oxidised Nitrogen mgll

BOD mgll

Chemical Oxygen Demand mgll

Depth m Temperature Degrees C

Visual Inspection Descriptive

- Test

Method

Sample No. - Customer: Date Received: Mode Of Delivery: Condition On Delivery: Date Started: Report Date:

162501287

21/04/2016 Cooler Box OK 2 1/04/20 16 20/05/2016 Origir

Test Date

09/05/16 2610411 6 2 1/04/16 21/04/16 06/05/16 2 1/04/16 21/04/16 21 /04/16 2 1/04/16 2 1 /04/16

Test Report

RESULT Accredited* Sub-tontract**

30.7

52.61 996 6.6

< 0.11 6.95 64 1 .I 8.2 0

SIGNED 07/06/2016 DI: Joe Ferly, Laboratory Manager

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of <1 MPN/lOOml is obtained. Notes 4 ............ Notes 5 ............

lssue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Test Maximum ParameterlUnit Method Limit

Atmospheric Pressure mBar -- Carbon Dioxide YO -_ Methane YO -- Oxygen YO 0 2 --

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Mag heranan Letterkenny 074-9122787

Minimum Test RESULT

__ 2 110411 6 1001

-- 21/04116 23.7

-- 2 1 10411 6 51.6

__ 21 104l16 1.4

Limit Date Accredited Sub-tontract**

SIGNED 07/06/2016 Di: Joe 6 e n y Lnboktoty Maringer

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of c1 MPN/lOOml is obtained. Notes 4 ............ Notes 5 ............

lssue 1 September 2015 Page 1 of 1 Print Date: 07/06/2016

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EPA Export 30-08-2016:02:06:12

LabWorks - Certificate of Analysis Report Reference: Original Test Report

Parametedunit

Atmospheric Pressure mBar

Carbon Dioxide YO Methane YO Oxygen % 0 2

Comhairle Contae Dhun na nGall Donegal County Council

Central Laboratory, The Kube Magheranan Letterken ny 074-9122787

Test Maximum Minimum Test RESULT Method Limit Limit Date Accredited* Sub-tontract**

-- -- 2 110411 6 1001 -- -- 2 1104116 24.4 -- -- 21 10411 6 57.9 -- _- 21104116 0.4

SIGNED f i %, 07/06/2016 Dr. Joe ferry, Lobdotory Morioger

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of <1 MPN/lOOml is obtained. Notes 4 ............ Notes 5 ............

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EPA Export 30-08-2016:02:06:12

Labworks - Certificate of Analysis Report Reference: Original Test Report

Test Maximum Method Limit ParameterlUnit

Atmospheric Pressure mBar -- Carbon Dioxide YO -_ Methane YO -- Oxygen % 0 2 --

Minimum Test RESULT

-_ 21 10411 6 1001

_ _ 21 /04/16 29.2

-- 21 10411 6 55.7

-- 2 1/04/16 0.5

Limit Date Accredited. Sub-Contract**

Dr. Joe Ferty, Loborototy Morioger

This report shall not be reproduced except in full, without the permission of the laboratory, and only relates to the items tested Any opinions, remarks and/or interpretations expressed above are outside the scope of accreditation Microbiological parameters with units MPN/lOOmls are reported as zero where a result of c1 MPN/lOOml is obtained. Notes 4............

~~

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EPA Export 30-08-2016:02:06:12