C E i ^ L I S f ; ARD980864110

ecology and environment, inc.7434 P I C A R D Y A V E N U E , B A T O N R O U G E , L O U I S I A N A 70809, T E L . 504/767-3657Internat ional S p e c i a l i s t s in the Environment

I M M E D I A T E REMOVAL P O T E N T I A L REPORT C*inON ooMONROE P I T S I T E ° O

P A R A G O U L D , G R E E N E C O U N T Y , A R K A N S A S

P r e p a r e d f o r

EPA - R E G I O N VIE M E R G E N C Y R E S P O N S E B R A N C H

J . C h r i s Pe t e r s enDeputy P r o j e c t O f f i c e r

E c o l o g y & Environment , I n c .T e c h n i c a l A s s i s t a n c e Team

J u l y 22 , 1987

142574

C A S 4 NO. ARD980864110

ecology and environment, inc.7434 P I C A R D Y A V E N U E , B A T O N R O U G E , L O U I S I A N A 70809, T E L . 504/767-3657Internat ional S p e c i a l i s t s in the Environment

J u l y 22, 1987

TO: G r e t a C l e n d e n e n , OSCEPA Region VI Emergency Response BranchT H R O : J . C h r i s P e t e r s e n , D e p u t y P r o j e c t O f f i c e rEPA Region VI Emergency Response BranchTHRO: W i l l i a m R. G o o d e , TATL - Region VIE c o l o g y & Environment , I n c .FROM: Ann L. Looney - Region VIEcology & Environment, I n c .S O B J E C T : Monroe P i t S i t eP a r a g o u l d , Greene C o u n t y , A r k a n s a s

OvOOOOO

PURPOSE

T D D N o .P A N N O .

06-8706-20T A R 0 1 6 1 S A A

On J u l y 13 , 1987, EPA R e g i o n VI TAT member s Ann L o o n e y and G a r yDry conducted an i m m e d i a t e removal p o t e n t i a l i n v e s t i g a t i o n of theM o n r o e P i t S i t e i n P a r a g o u l d , G r e e n e C o u n t y , A r k a n s a s .A c c o m p a n y i n g t h e T A T w a s Paul H i l l , P l a n t M a n a g e r , o f M o n r o e A u t oE q u i p m e n t , which maintains the c lo sed RCRA f a c i l i t y .B A C K G R O U N DThe M o n r o e Pit S i t e i s l o ca t ed at the corner of A r k a n s a s H i g h w a y359 ( F i n c h Road) and a gravel road ( c o o r d i n a t e s 36° 0 1 ' 2 3 " N and9 0 ° 3 0 ' 0 " ) W . T h e s i x acre f e n c e d s i t e contains a n a p p r o x i m a t e l ytwo acre c a p p e d s u r f a c e impoundment where a 12 f e e t d e e p gravelpit p r e v i o u s l y e x i s t e d . Between 1973 and 1978, the impoundmentreceived a p p r o x i m a t e l y 15,409 cubic y a r d s o f s l u d g e f r o m t h eM o n r o e A u t o Equipment wa s t ewa t e r t r e a t m e n t lagoon.

recycled p a p e r

TDD No. 06-8706-20

The s l u d g e , which i s th e re su l t o f e l e c t r o p l a t i n g p r o c e s s e s ,c o n s i s t e d o f i n s o l u b l e metal h y d r o x i d e s l u d g e s . A d d i t i o n a l l y ,oil and greas e were pre s en t in the s l u d g e in a f i v e percent drywe igh t basis. A 1972 a n a l y s i s of m e t a l s in the s l u d g e is f o u n din T a b l e 1. A s l u d g e a n a l y s i s for the years 1973 thru 1978 wasn o t a v a i l a b l e ; however, C h a r l e s P i c k n e y , P l a n t C h e m i s t , s t a t e dt h a t t h e 1972 t e s t r e s u l t s s h o u l d b e i n d i c a t i v e o f t h ec o m p o s i t i o n o f t h e p i t s l u d g e . H e men t i oned that lead ( P b ) m a yhave been in the s l u d g e as wel l .At the t i m e o f d i s p o s a l , the s l u d g e was c on s id e r ed a p e r m i t t e dwas t e , but e f f e c t i v e December 31, 1980, in 45 F R . N O . 2 5 2 , N o t i c e8 6 5 4 7 , t h e w a s t e w a s g r a n t e d a t e m p o r a r y RCRA d e l i s t i n g .E f f e c t i v e N o v e m b e r 27, 1986, in 50 FR 48886-48899, the lagoons l u d g e was re l i s t ed due to extraction procedure chromium levels.The Monroe A u t o Equipment lagoon s l u d g e is currently l i s t ed as anF 0 0 6 waste; t h e r e f o r e , the company considers the pit s ludge as anF 0 0 6 waste.T h e r e are eleven test wel l s at the site ( F i g u r e 2 and Pho tograph1), ranging in d e p t h f r o m 26 - 50.5 f e e t . T h e s e we l l s , which ares h a l l o w , as c ompared to the a p p r o x i m a t e l y 150 f e e t d e e p watert a b l e , are used to m o n i t o r p e r c o l a t e d water. S a m p l i n g o f them o n i t o r i n g w e l l s i s c o n d u c t e d b y t h e c o m p a n y a n n u a l l y .A n a l y t i c a l da ta for 1987 is f o u n d in Atta chmen t 1.A c c o r d i n g to a FIT survey, there are eight dome s t i c w e l l s wi th in2300 f e e t o f t h e s i t e ( F i g u r e 3 a n d T a b l e 2 ) . D u r i n g t h e A p r i l29, 1987 survey, FIT learned that re s idents u t i l i z i n g area we l l shad complained of green stains in household sinks. T h e s e stainswere pre s ent in homes wi th PVC p i p i n g . FIT a d d r e s s e d th i sp r o b l e m to a g e o l o g i s t f r o m the A r k a n s a s G e o l o g i c a l S u r v e y andlearned t h a t , w i th the e x c e p t i o n of iron which i s o c c a s i o n a l l yf o u n d , m i n e r a l s are not pre s en t in the area. TAT asked C h a r l e sP i c k n e y about c o p p e r d i s p o s a l in the pit and was t o l d thatc o p p e r , if p r e s en t at a l l , would be in very low concentrat ions .Monroe A u t o Equipment has not and does not u t i l i z e copper in thee l e c t r o p l a t i n g process.

\OOOOO

TDD NO. 06-8706-20

S I T E D E S C R I P T I O NThe M o n r o e Pi t S i t e ( F i g u r e 1) i s s urrounded by a s i x f o o tcyclone f e n c e t o p p e d wi th s ix inches of barbed wire ( P h o t o g r a p h4 ) . T h e s i t e i s acce s sed f r o m a l o c k e d g a t e a l o n g t h e grave lroad a t th e n o r t h e a s t e d g e o f th e s i t e ( P h o t o g r a p h 5). At thet ime of the s i t e v i s i t , two trees were f o u n d l eaning on the westf e n c e ( P h o t o g r a p h 3), and a s e c t i o n o f f e n c e had been uns cr eweda n d p u l l e d away. G u l l i e s , l a r g e enough f o r p a s s a g e b e n e a t h t h ef e n c e , had f o r m e d at the southeast p o r t i o n of the site. One "NoT r e s p a s s i n g " s i g n was at the s o u t h e a s t corner of the f e n c e , andno o t h e r s i g n s were p o s t e d . The c o m p a n y i n t e n d s t o remove th et r e e s , s t a b i l i z e the g u l l i e d area, and increase the number o fs igns to e ight .T h e c a p p e d i m p o u n d m e n t area h a s a f i v e p e r c e n t s l o p e t o t h en o r t h w e s t . The area i s uneven and covered w i t h t h i c k , h e a l t h yveg e ta t i on ( P h o t o g r a p h 8 ) . T A T d i d n o t s e e f i s s u r e s o r p u d d l e spre s en t .T o t h e n o r t h w e s t o f t h e i m p o u n d m e n t , i s a m a n m a d e p o n d( P h o t o g r a p h 2 ) . T h e pond c o n t a i n s s i t e d r a i n a g e w a t e r a n d w a sone t h i r d f u l l a t the t ime o f the TAT v i s i t . To the west o f thec a p p e d area i s a f o r e s t wh i ch e x t e n d s beyond th e s i t e f e n c e( P h o t o g r a p h 6 ) .C O M P A N Y M A I N T E N A N C EM o n r o e A u t o E q u i p m e n t m a i n t a i n s t h e f o r m e r d i s p o s a l s i t e . T h em a i n t e n a n c e p r o g r a m i n c l u d e s a m o n t h l y w a l k o f t h e p e r i m e t e r ,b iannua l bush h o g g i n g o f t h e c a p p e d area and annual t e s t i n g o fm o n i t o r i n g w e l l s . R e p a i r s are made as needed.

CMvDOOOO

TDD No. 06-8706-20

TABLE 11972 LAGOON S L U D G E A N A L Y S I S

M E T A LChromium I I IZincN i c k e lI r o n

SYMBOLC r + 3

ZnN iF e

C O N C E N T R A T I O N ( p p m )2385030620

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TABLE 21987 F I T D O M E S T I C WELL S U R V E Y

H e l l Depth LocationF a u l k n e r Unknown 1200 ft . due north of l a n d f i l l

on the east s ide of S p r i n gGrove Road

C l e v e l a n d Unknown 1500 ft. SU of l a n d f i l l onthe south side of Ark. 358

Duncan 210 ft. 700 ft. HE of l a n d f i l l onthe north side of Ark. 358Thompson 198 ft. 900 ft. HE of l a n d f i l l onthe south side of Ark. 358

E l l a * Unknown 1800 ft. SM of l a n d f i l l onthe south side of Ark. 356W a l t h a m Unknown 1700 ft. SU of l a n d f i l l onthe south s ide of Ark. 358

Crocket Unknown 2300 ft. due north of l a n d f i l l' on the east s id e of S p r i n gGrove Road

M o b i l e Homes Unknown 350 ft. SE of l a n d f i l l onthe east side of Ark. 358

Community Common

xxxxX

X

TDD NO. 06-8706-20

ecology and environment, inc.7434 P I C A R D Y A V E N U E , B A T O N R O U G E , L O U I S I A N A 70809, T E L . 504/767-3657Internat ional S p e c i a l i s t s in the Environment

L I S T OF ATTACHMENTSF I G U R E 1 : S I T E S K E T C H

F I G U R E 2 : M O N I T O R I N G W E L L L O C A T I O N M A PF I G U R E 3: D O M E S T I C WELL L O C A T I O N MAP

F I G U R E 4 : T O P O G R A P HP H O T O G R A P H LOG

U N U S E D P H O T O G R A P H S & N E G A T I V E SATTACHMENT 1: 1987 S A M P L E R E S U L T S

C O R R E S P O N D E N C EP H O N E C O N V E R S A T I O N RECORD

COPY OF FIELD NOTESPOL REP

COPY OF TDD

vQOOOO

recycled p a p e r

Figure 1S i t e Sketch

4 4 4* * *4 44 4 ' fence line

^4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4v , 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 .4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 44 4 4 1 4 4 4 4 4 4 41 4 4 1 4 4 4 4 4 44 4 414 4 4 4 4 4 41 1 4 4 X 4 4 4 4 4 4 . , . . .4 4 4| 4 4 4 4 VOX 4 4^ 4 4> 4 4 4 J ^ 4 4 4 4 4 .4 4 4f4 4 4>T 4 4 4 4 4 44 44t 4 jj%* 4 4 4 4 4 41^4 4 4 4 4 4 4 44 4 4 4 4 4 4 4 J4 4 X 4 4 4 4 4 4 4 4 4 4 4 1

' ' ^ 4 4 4 4 4 4 4 4 4 4

4 4 4 4 4 4 4 4 4 4 44 4 4 4 4 overgrowth 4 4 4 4 4J4 4 4 4 4 4 4 4 4 4 4j

H W Y4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 ,^ 4 4 4 4 4 4 4 4 4 4 4 4 4 44 4 4 4 4 4 4 4 4 4 4 4 44 4 4 4 4 4 4 4 4 4 4 4 44 4 4 4 4 4 4 4 4 4 4 4 4- 4 4 4 4 4 4 4 4 4 4 4 41 4 4 4 4 4 4 4 4 4 4 4[ 4 4 4 4 4 4 4 4 4 4 4 4' 4 4 4 4 4 4 4 4 4 4 4 ,4 4 4 4 4 4 4 4 4 4

4(4 4 4 4 4 4\4 41 14 4 4 4 4 4 4 4 4 44 4 4 4 front entrance *.+.*.*4 4 4 4 4 ,4 4 4 4 4 4 4 ", __ * 4 4 4 4 4 4 44 ( 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4- ' 4 4 4 4 4 4 4 4 4 4 4 4 4 4

4 4 4 4 44 4 4 4 4 41^ 4 4 4 4 4 44 A A t A 1gravel road'

444)4 4 4

4 4, A 4ravineY»V :

4 4 4 4 4 4 4 4 44 4 4 4 4 4 4 4 4 44 4 4 4 4 4 4 4 4 4 4 V1 4 4 4 4 4 I I [ j I I r"l414 4 4 4* 4 * 4~4 444 4

4 4 4 14 1 4/4 4:4 4 44 4 4 4 44 4A Y * * ' * 1 * - * *V . Y / 0 / 4 V ,

4 4 4 4 4 4 4 4 4 4 4 4 44 4 4 4 1 4 4 4 4 4 4 4 4 4 44 4 4 4 ) 4 4 4 4 4 4 4 4 44 - 4 4 4 > 4 , ' , . , • - ,4 4 4 41* * Disposal area J^U 4 4!i 4 4 4 > 4 4 , ..,.,,.., 4 > f r 4 4 4444 414 4 4 4 4 4 4 4 4 4U4V 4 4 .4 4 4 4 1 4 4 4 4 4 4 4 4 4 f 414 4 4\444 4]4 4 4 4 4 4 4 4 4 4> i- 4444 4 4 4 4 4 4 4 4 4 4 4 4 4 4t4T* 4 4 \444 414 4 4 4 4 4 4 4 4 4> 444 414 l 4 4 4 4 / 4 f 4 4 4 | 4 4 4 444 4(4 444 44 4 4 4 4 4 4 4 4 4\4 4 4

4 4 4 * 4 / 4 4 4+ 14*4V* 4/4 4 44 f

+ * ^ 4 4 4 4 4r 4 4 > 4 4 4 4 4* 4 4 4

4 4 4 44 4 4 44 4 4 4 ^4 4 4 44 4 4 44 4 4 44 4 4 4

4 44 4 4 4* 4 4[4.4.4.4.4,44 4mound 4 4 4 44 4 4 44 414 4 4 4 4 4 4 4 4 44 4 4 4 4 4 '

4 4^4*4*4'

4 4 / 4 4 J 4 4 4 4 4 4 4 4 U 4 H 4 4 4 4 4 4 breech i n fence4 4 4 4 4 4 4 4 4 4 \ 4 4 4 4 4 4 4,depressions 4 4 4= 44 4 4.

* + + + *> 4 4 4 44 4 4 44 4 4 4 4. . 4 4 4 4 4 4. . 4 4 4 4 4 4 4 4. 4 4 4 4 4 4 4 4 4 -4 4 4 4 4 4 4 4 4 4 4 4

' 4 4\ 4 444. 4 4 44 4 44 4 4 44 4 4 4> 4 4 4 44 4 4 4 4,8 * * * * *4 4 4 4 4 44 4 4 4 4 44 4 4 4 4 4 4F4 4 4 4 4 4 44 4 4 4 4 4 44 4 4 4 4 4 4k 4 4 4 4 4 4 44 4 4 4 4 4 4I 4 4 4 4 4 4 44 4 4 4 4 4 4t 4 4 4 4 4 4 44 4 4 4 4 4 4H 4 4 4 4 4 4 44 4 4 4 4 4 44 4 4 4 4 4 1, 4 4 4 4 4 4 44 4 4 4 4 4 41 4 4 4 + 4 4. 4 4 4 4 4 4 44 4 4 4 4 4[ 4 4 4 4 4 4 44 4 4 4 4 4. 4 4 4 4 4 4, 4 4 4 4 4 4fe 4 4 4 4 4 4|» 4 4 4 4 4, 4 4 4 4 4 44 4 4 4 4 44 4 4 4 4 4. 4 4 4 4 414 4 4 4 4 44 4 4 4 44 4 4 4 44 4 4 4 44 4 4 4 ',4 4 4 4 44 4 4 4 '4 4 4 44 4 4 4 4: 4 4 4 4[ 4 4 4 4 44 4 4 44 4 4 '4 4 4 44 4 4 '44

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4 4. 4 +L*4*4*4*4 4 4 4 4 ' 4 ' 4 ' 4 ' 4 / * 4 ' 4 ,4 4 4 4 4 4 4 4 4 4 4 4 f t 4 4 4 4 / 14 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 44 4 4 4 4 4 4 . 4 4 4 - 4 4 1 4 4 4 4 4 44 4 4 4 4 4 4 4 4 4 4 414 4 4 4 4

4 4 4 4 4 4 4 4 4 4 4 4 4 4 drainage4 4 4 4 4 4 1 4 4 4 ,4 4 4 4 4 4 gravel pit 4 * 44 4 4 4 4 + * * * * 4 4 44 4 4 4 4 4 4 4 4 4 4 4 4 *4 4 4 4 4 4 4 4 4 4 4 4 :4 4 4 4 4 4 4 4 4 4 4

4 4 44 4 44 4 4\ 4 4 44 4 4Ecology and Environment.

;ai AssistanRegionVI

Technicaime.Team

C«M ARD980864110 I TDD 06-8706-20PAN T A R 0 1 6 1 S A A |O«t« 07-13-87

Originator Gary L. Dry

Ecology and Environment, Inc.T e c h n i c a l A s s i s t a n c e T e a mR e g l o n V I

Case ARD980864110P A N T A R 0 1 6 1 S A A

T D D 06-8706-20Date 07-13-87

Orig ina t or Gary L. Dry

#r

d l r t c t l o n o» ground wi t t r f l o w

o*r•na« W a l t h a m

WF i g u r e 3

Domestic Wel l Locat ionM o n r o e L a n d f i l lP a r a g o u l d , Ark.

, 0 0 0 0 6 7

Figure 4Paragould West: Quadrangle

is* 3ijiF^:'-ys?yy v.j.1:• f T J \ C T ^ T T V Xi i i •-.=*=&= ,v*-=- AR4GOU

' • ^ - c y . 1 l ^ ^ / ? ' f i ' ^ ' j f ' ' t

Ecotogy and Environment, IncTechnical Assi s tance Team

RegionVICase ARD9S0864110

Originator Gary L. Dry

00vOoooo

SCALE 1:24000o I MICE1000 1000 2000 3000 4000 5000 6000 7000 FEET

1 K I L O M E T E R

TDD 4 06-8706-20 Page 1 of 3

Photographer/Witnes s t 1_Gary Dry / A n n Looney

Date/Tinie/Direc t ion07-13-87; 1300 H r s ; East

ConmentS: One several on-sitemonitoring wel l s .

Photographer/Witne s sGary D r y / A n n Looney

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Eate/Tim^/Direct ion07-13-87; 1300 H r s ; Southwes t

Comments: S h a l l o w pond inside thesite containing very l i t t l e ____s t and ing water.

Photographer/Witnes sGary D r y / A n n Looney

Date/Tirae/Direc t i on07-13-87; 131O H r s ; East

: 6 f o o t cyclone f e n c e withbarbed wire surround the site.A^tree branch has f a l l e n across

TDD f 06-8706-20 Page 2 of 3

Photographer/Witne s sGary D r y / A n n Looney

Date/Time/Direc t i on07-13-87; 1320 H r s ; Sou th

Comments: 6 f o o t cyclone f e n c esurrounding the s i te.

Photographer/Witne s sGary D r y / A n n Looney

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Date/Time/Dire c t i on07-13-87; 1320 H r s ; Southwes t

Comments: F r o n t and only entranceinto the s i te.

Photographer/Witne s sGary D r y / A n n Looney

Date /Time/Dire c t i on07-13-87; 1320 H r s ; S o u t h

. H e a v y tree growth andrich vege ta t ion ins ide and out s idethe site.

g 06-8706-20 page 3 Qf 3

Photographer/Witnes s I _~[_Gary D r y / A n n Looney

D a t e / T j j n ^ / D i r e c t i o n07-13-87; 1315 H r s ; S o u t h

ConmentS: General d i spo sa l areainside the site. T h i s area hasbeen covered with soil and is pres-en t ly vegetation.

Photographer/Witne s sGary D r y / A n n Lo_oney

DatQ/Time/Direc t i on07-13-87; 1330 H r s ; East

Comments: Rich vegetation coveringa depre s s ed d i t ch inside of the —site. Terrain g e n e r a l l y is uneven

ith bumps and d e p r e s s i o n s

•-*j•~,i»•*'&$•'•".*"* Photographer/Witne s s

Gary D r y / A n n LooneyI D a t e / T i m e / D i r e c t i o n

07-13-87; 1330 H r s ; W e s t

a Comments: H e a v y tree growth withsuccessive -vegetation coveringthe d i spo sa l s ite area.

oOJ 2 / . 0 0 0 0 '

COID*I

» • • < • 7434 P I C A R D Y A V E N U EB A T O N R O U G E , L O U I S I A N A 70809

U N U S E D P H O T O G R A P H S A N D N E G A T I V E S

b N V I R Q M E DL A B O R A T O R I E S , I N C .

ORGANIC ANALYSES REPORTEML S a m p l e No. .35440

Cli en t : . Monroe Auto EquipmentAddress*" Engineer ing—Science . Inc.57 Executive Park South, N.E. S u i t eP.O. No. A t l a n t a . GA 30329_____

1874 DALLAS D R I V :BATON ROUGE, LA. 708O

I 5 0 4 1 - 9 2 8 - 0 2 3

Attachment 1Page 1 of 5

Date Col l e c t ed; 2 / 1 8 / 8 7 By; AS Timer 1330Date Received; 2 / 2 3 / f l 7 Bv;"^—Time:VOA GC/MS Analysi s tote: 3 / 5 / 8 7 "Sample T y p e : (Satib Soil S l u d g e OtherSample Volume or W e i g h t ; 5 ml.Sample I . D . T W I I . f f f f

Purgeable Compounds* Det. Limitm g / L orn g / K g Comments

Acrole inA c r y l o n l t r i l eBenzeneChlorobenzeneEthylbenzeneMethyl BromideBromoform

>Methylene ChlorideMethyl ChlorideCarbon T e t r a c h l o r i d eVinyl ChlorideChloro formChloroethane1.1-Dichloroethane1.2-Dichloroethane1,1 ,2 ,2-Tetrachloroe thane1.1.1-Trlchloroethane1.1.2-Trlchloroe thane2-Chloroethyl vinyl Ether1.1-Dichloroethylenetrans-1,2-DichloroethyleneTe trachloroethyleneTrichloroe thyleneChlorodlbromomethaneDich lorod i f luorome thaneDichlorobromomethaneT r i c h l o r o f l u r o m e t h a n e1.2-Dichloropropanecis-1,3-Dichloropropenetrans-1,3-DichloropropeneTolueneXylenes* The purgeable compounds were' I n d i c a t e s None Detected.

0.1000.1000.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.005

0.0050.0050.0050.0050.0050.0050.005- 0.0050.0050.0050.0050.0050.0050.0050.005analyzed using EFA Method 624.

OOOO

T D D # 6 - 8 7 0 6 - 2 Q

Donald Lee Perry, Ph.DTechnical Director

H E N V I R B I V I E DL A B O R A T O R I E S , I N C .

ORGANIC ANALYSES REPORTEML S a m p l e No. 35441

Client ; . Monroe Auto Equipment___Addres s r Engineering-Science. Inc.57 Executive Park S o u t h , N.E. S u i t eP.O. No. A t l a n t a . GA 30329_____

Date C o l l e c t e d ; 2 / 1 8 / 8 7Date Received: 2 / 2 3 / 8 7VOA GC/MS Analysi s DateSample T y p e : <tiatl£> Soi lSample Volume or W e i g h t : _S a m p l e I . D . B-12. GW

1874 DALLAS DRIV:BATON ROUGE, LA. 708fr[ 5 0 4 1 - 9 2 8 - 0 2 3Attachment 1Page 2 of 5

By; AS Time: 1350"By; RC T i m e ; unn' 3 / 2 / 8 7 _____S l u d g e5 ml. Other

Purgeable Compounds* Cone. Det. Limitm g / L or m g / L or Comments

Acrole inA c r y l o n i t r i l eBenzeneChloro benzeneEthylbenzeneMethyl BromideBromoform

^te thylene Chloride' M e t h y l Chlor ideCarbon T e t r a c h l o r i d eVinyl Chlor id eChloro f o rmChloroethane1 , 1-Dichloroe thane1 , 2-Dichloroe thane1,1,2, 2-Tetrachloroe thane1,1, 1-Trlchloroe thane1 , 1 ,2-Trichloroe thane2-Chloroethyl vinyl Ether1 , 1-Dichloroethylenetrans-1 , 2-Dichloroe thyleneT e t r a c h l o r o e t h y l e n eTrich l oro e thyleneChlorodibromomethaneDichlorodi f luoromethaneDichlorobromomethaneT r i c h l o r o f l u r o m e t h a n e1 ,2-Dichloropropanecls-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneTolueneXylenes^ The purgeable compounds were' Indi ca t e s None Detec ted.

m g / K g

—————

—————-——-—--————-—---——--

analyzed using

m g / K g

0.1000.1000.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0058 .005.005EPA Method 624.

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' A n a l y s t ( s ) Donald Lee Perry, Ph.D.Technical Director

EML Sampl e No. 35451

E N V I R Q M E DL A B O R A T O R I E S , I N C .

ORGANIC ANALYSES REPORT

Client : .Monroe Auto EquipmentAddres s : - Engineering-Science . Inc .57 Executive Park South , N.E. S u i t eP.O. No. A t l a n t a . GA 30329 _____

Date Col l e c t ed: 2 / 1 9 / 8 7Date Received: 2/23/87LVOA GC/MS Analysis Date:_Sample T y p e : Cf la£g£> Soi lSample Volume or W e i g h t : _Sample I.D. B-2. GW

IU74 DALLAS OtUV-BATON ROUGE, LA. 7080[ 504 ] - 9 2 8 - 0 2 3Attachment 1Page 3 of 5

By: AS Time; 0900t y ; R C Time; uon3 / 5 / 8 7 ___S l u d g e5 ml. Other

Purgeable Compounds*

AcroleinAcryloni tri leBenzeneChlorobenzeneEthylbenzeneMethyl BromideBromof orm

•\Methylene Chlor ideMethyl ChlorideCarbon T e t r a c h l o r i d eVinyl ChlorideChloro formChloroethane1 ,1-Dichloroethane1 , 2-D1 chloroethane1,1 ,2 , 2-Tetrachloroethane1,1, 1-Trlchloroe thane1 , 1 ,2-Trichloroe thane2-Chloroethyl vinyl Ether1 , 1-Dichloroethylenetrans-1 ,2-Dichloroe thy leneTetrach loroe thyl eneTrichloroe thyleneChlorodibromomethaneDichlorodifluoromethaneDichlorobromomethaneTri ch l oro f lurome thane1 ,2-Dichloropropanecls-1 ,3-Dichloropropenetrans-1 ,3-Dichloro«ropeneTolueneXylenes* The purgeable compounds wereIndi ca t e s None Detected.

Cone. Det. Limitm g / L or m g / L orm g / K g m g / K g

——••——

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analyzed

0.1000.1000.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.005using EPA Method 624.

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As 8702109S 87021097Ua 8702109S 87021097Cd 8702 109S 87021097Cr 87021095 67021097Pb 87021095 8702 1097llg 87021097 87021095Se • 87021095 87021097A<3 87021095 87021097

• Date ' **Anal ' Blank* Duplicate* '''' ^8Anal Method cl * C2 • KfQ • M v;'3 / 2 / 8 7 H <0.001 <0.001 <O.OOI " ' . • . H C ' ' " 1 ! - - ' t f ' M « w ) i

2 / 2 5 / 8 7 P <0.8 <0.8 <0.fl ' ' i . ' i . - W C i ' ' ' ^ i ^ ' l2 / 2 4 / 8 7 F <6,013 <0.013 <0.013 *C ^ Cl?!i^42 / 2 4 / 8 7 F <0.04 <0.04 <0.04 DC O . S O >2 / 2 4 / 8 7 F <0 OB <0.08 <0.08 MC O . f i A

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2 / 2 4 / 8 7 F <0.02 <0.02 <0.02 MC 1.0 <0.02 0.085 8.5 -• • Y ' ' ' ' •.\ T" •

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C' 1 i t i i i t i i • • « S il—— us ct9 *' If % noisture i« r epor t ed , result s are presented on a dry-weight basis* *• P « Flawe AAS m | •«v. C « Graphi t e Furnace AAS o | >^ R e l a t i v e Percent D i f f e r e n c e (RPD) » Cl - C2 Cl • Concentration One H - H y d r i d e Vapor AAS ,n <* rr>i Percent Recovery (PR) * SSR - SR

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