20
Since the late 1970s, On-Line Instrument Systems, Inc. (“Olis”) has lead meaningful product innovation in optical spectroscopy. This catalog introduces you to products ranging from our popular < $10K starter systems to extraordinary >$150,000 rapid-scanning spectrophotometers. Every product within these pages is “endlessly upgradeable” in era and in application. Aging computers and electronics can be replaced every decade or so; new accessories and data acquisition models can be added as needed. Endlessly Upgradeable Spectrophotometers ‘me-too’ product. Or, this time, choose an OLIS and get better quality, enhanced performance, and unmatched longevity. Change the way you think about absorbance, fluorescence, and circular dichroism equipment. Designed-in obsolescence and limited application products make them money, not you. Join us and enjoy world-class performance and endless upgradeability. And be among those who can say “I love the instrument; I love the people.” Custom systems are available upon request. Absorbance Fluorescence Circular Dichroism Combination Models Accessories Catalog Spectrophotometers for Advanced Research and Teaching Environments

Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

  • Upload
    lehanh

  • View
    232

  • Download
    0

Embed Size (px)

Citation preview

Page 1: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

Since the late 1970s, On-Line Instrument Systems, Inc. (“Olis”) has lead meaningful product innovation in optical spectroscopy.

This catalog introduces you to products ranging from our popular < $10K starter systems to extraordinary >$150,000 rapid-scanning spectrophotometers.

Every product within these pages is “endlessly upgradeable” in era and in application. Aging computers and electronics can be replaced every decade or so; new accessories and data acquisition models can be added as needed.

Endlessly Upgradeable SpectrophotometersPut your hard-won equipment funds into another ‘me-too’ product. Or, this time, choose an OLIS and get better quality, enhanced performance, and unmatched longevity.

Change the way you think about absorbance, fluorescence, and circular dichroism equipment. Designed-in obsolescence and limited application products make them money, not you.

Join us and enjoy world-class performance and endless upgradeability. And be among those who can say “I love the instrument; I love the people.”

Custom systems are available upon request.

Absorbance

Fluorescence

Circular Dichroism

Combination Models

Accessories

Catalog Spectrophotometers for Advanced Research and Teaching Environments

Page 2: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

2

Table of ContentsInstruments are listed according to complexity and cost, least expensive fi rst, in the fi rst three categories.

Absorbance Models ....................................................................4 AU1. Computerized HP 8452 diode array .................................................................................4

AU2. Modernized Aminco DW-2 UV/Vis spectrophotometer .....................................................4

AU3. Modernized Cary 14 UV/Vis/NIR spectrophotometer .......................................................4

AU4. Olis DB 620 UV/Vis[NIR] spectrophotometer ...................................................................5

AU5. Modernized PE 983 IR spectrophotometer ......................................................................5

AU6. Olis RSM 1000 UV/Vis[NIR] rapid-scanning spectrophotometer ......................................5

Fluorescence Models .................................................................6 FL1. Olis Polarization Toolbox .................................................................................................6

FL2. Olis DM 45 spectrofl uorimeter .........................................................................................6

FL3. Modernized SLM 4800/8000 spectrofl uorimeter ...............................................................6

FL4. Olis Quad-Purpose Polarization spectrometer .................................................................7

FL5. Olis DM 245 spectrofl uorimeter .......................................................................................7

FL6. Olis RSM 1000F1 rapid-scanning spectofl uorimeter ........................................................7

FL7. Olis DM 445 spectrofl uorimeter .......................................................................................7

FL8. Olis RSM 1000F4 rapid-scanning spectofl uorimeter ........................................................7

Circular Dichroism Models ........................................................8 CD1. Olis DSM 17 UV/Vis[NIR] spectrometer ...........................................................................8

CD2. Olis DM 20 UV/Vis[NIR] spectrometer ............................................................................8

CD3. Olis DSM 1000 UV/Vis[NIR] rapid-scanning spectrometer ...............................................9

Combination Models, Examples of ........................................10 C1. Olis DM 45 with Polarization Toolbox Module ................................................................10

C2. Olis 14 UV/Vis/NIR with scanning emission ...................................................................10

C3. Olis 8000 fl uorimeter with Olis USA stopped-fl ow ..........................................................10

C4. Olis RSM 1000 rapid-scanning absorbance with scanning emission .............................. 11

C5. Olis RSM 1000F1 rapid-scanning fl uorimeter with circular dichroism ............................. 11

C6. Olis DSM 1000 CD with cryogenic sample holder .......................................................... 11

C7. Olis DSM 20 CD with scanning emission ....................................................................... 11

Page 3: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

3

Accessories ..............................................................................12 A1. Olis USA stopped-fl ow for absorbance and fl uorescence ...............................................12 A2. Olis USA stopped-fl ow for absorbance only ...................................................................12 A3. Olis USA stopped-fl ow for fl uorescence and absorbance ...............................................13 A4. Olis USA stopped-fl ow for circular dichroism and absorbance .......................................13 A5. Olis Tonometer Adaptor .................................................................................................13 A6. Olis Titrator, two syringe ................................................................................................14 A7. Olis Titrator, two syringe, Peltier ....................................................................................14 A8. Olis Titrator, four Syringe ...............................................................................................14 A9. Olis Titrator, Peltier four syringe ....................................................................................14

A10. DeSa 1.4 Tesla Permanent Magnet ...............................................................................15 A11. Olis Auxiliary Mixer ........................................................................................................15 A12. Olis Millisecond Open/Close Shutter Box ......................................................................15

A13. Olis Jacketed Cuvette Holder ........................................................................................16 A14. Olis Four Position Cell Changer for Absorbance and Fluorescence ...............................16 A15. Olis Hanging Cuvette Holder .........................................................................................16

A16. Olis Long Pathlength Cell Holder ...................................................................................17 A17. Olis CD Jacketed Cuvette Holder ..................................................................................17 A18. Quantum North West Peltier Cell Holder, for CD ...........................................................17 A19. Quantum North West Peltier Controlled Cuvette Holder, Absorbance and Fluorescence ........17

A20. Quantum North West Peltier controlled Six position holder, Absorbance and CD ...........18 A21. Quantum North West Peltier Twin Temperature Controlled Cuvette Holder ....................18 A22. Quantum North West Turret Peltier-controlled Four Position Turret ...............................19 A23. Vertex™ Specular Refl ectance Variable Angle Cell Holder ............................................19 Putting it All Together: One Well-Accessorized Olis Spectrophotometer ....................................19

Custom Projects, a Selection of ............................................BC CP1. Olis DM 45 fl uorimeter with Oxygen Electrode ..............................................................BC CP2. Rotatable CD Chamber for a Synchrotron Line .............................................................BC CP3. Dual Mount Integrating Sphere, for all models ..............................................................BC

CP4. NIR CD Chamber, LCVR version ..................................................................................BC CP5. Rhodamine Reference Chamber, for any fl uorimeter ....................................................BC

Page 4: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

4

<$10K, Solid-State, Very Popular

Computerized HP 8452 diode arrayOlis, Inc. offers a Windows software package for tower and laptop PCs. With the Olis computerization, the HP 8452 (yours or a warranted one from us) collects up to ten scans per second. The display of scans is now practically instantaneous: today’s Olis software collects and displays 100 scans on the screen in 10 seconds! Data handling – from extracting fi xed wavelength kinetic traces to fi tting the 3D fi les to selected kinetic equations – is easy, fast, and effective.

Eight page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/hp8452_brochure.pdfliterature/pdf/hp8452_brochure.pdf

Choose for High Turbidity Work

Modernized Aminco DW-2 UV/Vis spectrophotometerThe spectrophotometer for working on P450, mitochondria, plant and tissue suspensions, and other scattering samples. The more turbid the sample, the more this model is needed. The DW-2 uses a large face detector a few millimeters from the sample and measures two wavelengths simultaneously so as to subtract scatter from the chemistry. We can modernize yours or provide a fully warranted system.

Twelve page brochure; http://olisweb.com/http://olisweb.com/literature/pdf/dw2_brochure.pdfliterature/pdf/dw2_brochure.pdf

Compares Successfully against $60-80K UV/Vis/NIR models

Modernized Cary 14 UV/Vis/NIR spectrophotometerAn Olis 14/17 – built from a Cary from your laboratory or from our storehouse – provides you with absolutely best optical performance at half the price of a brand new optical equa-valent. The spectral range is 185-2600 nm, photometric accuracy is ± 0.0005 AU, and stray light is less than 0.001%, among other distinc-tions of this outstanding classic instrument.

Sixteen page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/cary_brochure.pdfliterature/pdf/cary_brochure.pdf

AU1

AU2

AU3

Absorbance Models

Page 5: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

5

Laser/Flash Photolysis-Ready!

Olis DB 620 UV/Vis[NIR] spectrophotometerThe Olis DB 620, utilizing the Olis Hummingbird is perfect for laser photolysis absorbance studies with its 20 MHz dual beam acquisition. Also useful for all applications where high speed and precision is required. Noise in the fourth decimal place in milliseconds is standard. Five spectral ranges are available.

Sixteen page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/hummingbird_brochure.pdfliterature/pdf/hummingbird_brochure.pdf

The Choice for Fast-Reaction Kinetics

Olis RSM 1000 UV/Vis[NIR] rapid-scanning spectrophotometerWith the Olis RSM 1000, high speed kinetic studies can be followed with millisecond scans, so that higher precision rate constant determination is possible with the spectral axis, chemical models can be confi rmed or rejected. Prefect for stopped-fl ow when operating at 1,000 scans per second, perfect for laser photolysis when operating at 20,000,000 data points per millisecond. A wide selection of grating types allow optimization for different scan ranges and spectral resolutions.

Sixteen page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/rsm_brochure.pdfliterature/pdf/rsm_brochure.pdf

AU4

AU6

Absorbance Models

Superior to FT- IRs in Peak Intensity

Modernized PE 983 IR spectrophotometerOne of the most trusted IR spectrophotometers ever made was the PE 983 IR dispersive spectrophotometer. After the Olis modernization, the resulting system is an unusually reliable real-time double-beam dispersive IR with the identical optical parameters of the PE 983 IR and entirely improved data acquisition. The new Olis data acquisition scheme collects the correct value for %T without any adjustment or calibration.

Extensive details are provided on the Olis web site; see, for instance, http://olisweb.http://olisweb.com/products/upgrades/ir983specs.phpcom/products/upgrades/ir983specs.phpand http://olisweb.com/products/upgrades/http://olisweb.com/products/upgrades/ir983conversion/index.phpir983conversion/index.php

AU5

Richard J. DeSa, PhD. “Rapid-Scanning Monochromator with Moving Intermediate Slit.” US Patent 5,285,254. 8 February 1994.

Page 6: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

6

A Complete Course in Polarization

Olis Polarization ToolboxThis tiny instrument brings together inexpen-sive LED* light sources with a high sensitivity photon counter to create a modern research tool perfect for the pedagogical environment. Supports polarization of fl uorescence (POF), anisotropy (r), and/or circularly polarized lumi-nescence (CPL). Toolbox will include either a 50 KHz photoelastic modulator or a 5 Hz liquid crystal variable retarder to vary the fl uorescent light’s polarization orientation to measure L-format polarization. This modern electro-opti-cal method replaces physical rotation of the polarizers, multiple detectors, and associated G-factor corrections. Emission wavelength is selected based on fi lter used. Sensitivity is useful for many research applications.*Light source can be other than LED at higher cost.

Fluorescence Models

Still the Benchmark Research Fluorimeter

Modernized SLM 4800/8000 spectrofl uorimeterAn Olis modernized SLM – typically built from your laboratory – is optically identical to the original but with all modern Olis electronics and computerization. All existing accessories can be maintained. A wealth of Olis and third party accessories can be added. Enjoy the performance of today’s best spectrofl uorimeter when you start with a classic optical bench!

Eight page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/slm_brochure.pdfliterature/pdf/slm_brochure.pdf

FL3

Just Plain Good Fluorimeter!

Olis DM 45 spectrofl uorimeterA perfect solution for the lab looking for a teaching tool with research performance, the handcrafted Olis DM 45 includes two single grating monochromators, an easy to light xenon arc lamp, and a high sensitivity photon counting detector. The Olis DM 45 can be adapted easily and economically for NIR scanning to 2500 nm, microsecond fi xed wavelength acquisition, dual beam absorbance, and polarization.

Twelve page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/dm45_brochure.pdfliterature/pdf/dm45_brochure.pdf

FL2

FL1

US Patent 6,970,241 B1 (2005) issued to RJ DeSa

Page 7: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

7

Sensitivity, Versatility, Great Value

Olis DM 245 spectrofl uorimeterA more versatile fl uorimeter than the smaller Olis DM 45, the 245 includes one Olis double Hummingbird monochromator for higher wavelength selectivity and lower stray light than is possible with a single grating monochromator. The double can be used on either the excitation or emission side (user selectable); an Olis single grating model is the second monochromator. Light source can be 150 watt xenon arc (shown) or 300 watt version; detector is usually a single photon counter, but a pair of PMTs can be substituted or added for fast emission readings and/or dual beam absorbance acquisition.

Additional details available on http://olisweb.http://olisweb.com/products/fl uorescence/dm245.phpcom/products/fl uorescence/dm245.php

Fluorescence Models

Full Emission Scans ofFluorescing Samples

Olis RSM 1000F1 rapid-scanning fl uorimeterThe Olis RSM 1000 F1 uses a 150 or 300 watt Xenon arc lamp as the excitation source formillisecond emission scanning. This model can be fi tted on a base plate half the length shown. This construction was produced for illustration purposes only.

Sixteen page brochure: http://olisweb.com/http://olisweb.com/literature/pdf/rsm_brochure.pdfliterature/pdf/rsm_brochure.pdf

Full Emission Scans of FluorescingSamples, faster

Olis RSM 1000F4 rapid-scanning fl uorimeterThe Olis RSM 1000 F4 is identical to the model F1, except the large 450 watt Xenon arc lampis used as the excitation source for even more sensitive millisecond emission scanning. Standard detectors are a pair of high sensitivity photon counters or a pair of high speed photomultiplier tubes, based on sensitivity or speed emphasis.

FL4

FL5

FL6

Page 8: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

8

Circular Dichroism ModelsCompare with the Aviv 202 and Enjoy

Superior NIR Performance.

Olis DSM 17 CD UV/Vis[NIR] spectrometer Our model 17 is built around the classic Cary 17 UV/Vis/NIR monochromator. Of our three CD, this one feature the (1) widest available spectral range available span of 185 – 2600 nm (2) slit width under computer control and (3) full use of the renown Cary prism-grating monochromator for dual beam absorbance and circular dichroism.

See more about this model at http://olisweb.http://olisweb.com/products/upgrades/cary17cd.phpcom/products/upgrades/cary17cd.php

Compare with the Jasco 810 and EnjoyGreater Versatility.

Olis DSM 20 CD UV/Vis[NIR] spectrometer The model 20 is built around the Olis Hummingbird monochromator. Of all CDs in the world, this is the smallest. It is (1) designed for use in an amazing diversity in layouts (2) furnishes brilliant light throughput and (3) is completely approachable for students as well as senior staff. The Hummingbird is a subtractive double monochromator, also used in the Olis DB 620 absorbance and Olis DM 245 and 445 fl uorimeters.

See more about this model at http://olisweb.com/products/cd/dsm20.phphttp://olisweb.com/products/cd/dsm20.php

CD1

CD2

Page 9: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

9

Circular Dichroism ModelsExpectation - Exploding Rapid-Scanning

Olis DSM 1000 CD UV/Vis[NIR] rapid-scanning CD spectrometerThe model 1000 is built around a DeSa monochromator, the only rapid-scanning monochromator in the world. Like the model 20, the model 1000 supports maximum modularity and endlessly diverse applications. The F/4.5 monochromator (1) has the highest light throughput of the three choices (2) provides exciting potential for completely novel experiments and (3) is the fi rst choice for those comfortable with higher price tags on premium laboratory instruments. The DeSa “RSM” is a subtractive double grating monochromator capable of millisecond scan rates, also used in the full Olis RSM 1000 line for absorbance and fl uorescence.

This is the only rapid-scanning CD instrument available anywhere. Rapid-scanning is useful for FDCD, CPL, LD, and other secondary measurements for which an Olis DSM 1000 is confi gured. Rapid-scanning is possible throughout all spectral ranges, deep UV to far NIR. Best results presume meaningful signal strength and a modest spectral span.

See more about this model at http://olisweb.http://olisweb.com/products/cd/dsm1000.phpcom/products/cd/dsm1000.php

CD3

Spectral Range, Protein Region

Spectral Range,

Red Shifted

Spectral Range,

Full Available

Top Scan Rate

Dual Beam CD & Abs

Collects Two CD Scans

SimultaneouslyCalibration Endlessly

Upgradeable

Made in

the USA

DSM 17

185-800 nm

500-1700 nm

185-2500 nm 40 nm/ s yes

yes, through one sample

or twono yes yes

DSM 20

170-700 nm

500-1700 nm

170-2500 nm 40 nm/ s yes

yes, through one sample

or twono yes yes

DSM 1000

167-540 nm

500-1700 nm

167-2500 nm

230,000 nm/ s or 40 nm/ s

yesyes, through one sample

or twono yes yes

Comparing the Three Olis CDshttp://olisweb.com/literature/pdf/cd_brochure.pdf

Page 10: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

10

Combination Models

Nanoparticle NIR Studies

Olis 14 UV/Vis/NIR with scanning emission monochromator; ideal for nanotube fl uorescence in the NIR to 1650 nm

Millisecond Deadtime Mixer Added toOlis Upgraded SLM 8000

Olis USA stopped fl ow with custom mounting to an Olis modernized spectrofl uorimeter

C2

C3

C1Everything a Top Leading Laboratory Needs

Olis DM 45 with Polarization Toolbox Module to add POF, anisotropy, and CPL. Can also support absorbance and CD in fully useful forms for the pedagogical world.

Page 11: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

11 11

Combination Models

Millisecond Absorbance and CD

Olis RSM 1000F1 with circular dichroism or (equivalently) an Olis DSM 1000 CD with rapid-scanning scanning emission and CPL

Everything the Small Laboratory Needs!

Olis DSM 20 CD with scanning monochromator. Fluorescence, FDCD, and CPL complement absorbance CD

C4

C5

C6

C7

Millisecond Absorbance and Fluorescence

Olis RSM 1000 with scanning emission or (equivalently) an Olis RSM 1000F1 with dual beam absorbance module

Circular Dichroism at LiquidNitrogen Temperatures

Olis DSM 1000 CD with the Oxford Optistat DN cryogenic sample holder

Page 12: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

12

Olis USA Stopped-fl ows, Four ModelsIn 1992, when we decided to make our own stopped-fl ow, we optimized for strong signal, safe operations and sensible pricing. The result is a well-engineered, easy to operate selection of stopped-fl ows which are “Useful, Simple, and Affordable.”

Obtain full details on all four models in the 16 page brochure, http://olisweb.com/literature/pdf/http://olisweb.com/literature/pdf/stopped_fl ow_brochure.pdfstopped_fl ow_brochure.pdf

Olis USA stopped-flow for absorbance and fluorescenceThis cell assembly remains a very useful “classic” choice. The sample flows through a cylindrical optical-grade quartz tube, 20 mm in length and 2 mm in diameter. This was the original design of the Gibson/ Durrum stopped-flow and remains a popular choice for work done at near ambient temperatures. It is suitable for absorbance (20 mm) and fluorescence (2 mm) use. All early stopped-flow was done with this geometry cell, so it is easy to compare results today with earlier work. Also, the signal from such relatively large volume is strong, so that (very) few mul-tiple shots are necessary for excellent signal to noise.

Olis USA stopped-fl ow for absorbance onlyThis model employs a stainless steel flow cell assembly with a 10 mm optical pathlength, half the length of the ‘classic’ choice. It is useful only in one (straight-through) direction, so suited for absorbance readings only.

A1

A2

Accessories

Page 13: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

13

Olis USA stopped-flow for fluorescence and absorbanceThe fluorescence-optimized stopped-flow cell assembly is a 4 x 4 mm diameter cylinder of UV optimized fused silica (Suprasil) suitable for both absorbance and fluorescence.

Olis USA stopped-fl ow for circular dichroism and absorbanceFor CD, a cylindrical quartz observation cell of 2 mm pathlength is used, duplicating the most commonly employed cuvette style. The dual beam detection model of the three Olis DSM CD spectrometers is fully exploited. Both beams of light from the Olis DSM CDs are used, so that all of the benefits of digital CD data acquisition accrue.

See http://olisweb.com/literature/pdf/cd_http://olisweb.com/literature/pdf/cd_brochure.pdfbrochure.pdf

A3

A4

Accessories

Olis Tonometer AdaptorA tonometer is often made by adding stopcocks to a glass column. This tool is used introduce degassed solvents into an Olis stopped-fl ow’s gastight syringe. Because tonometers are often wider than the 5 mL syringe typically used to introduce solutions into the stopped-fl ow, an adaptor is available which effectively widens the distance between the two inlet ports.

For more detail, see http://olisweb.com/http://olisweb.com/products/accessories/tonometeradapter.phpproducts/accessories/tonometeradapter.php

A5

Page 14: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

14

AccessoriesOlis Titrator, two syringeThe Olis Automatic Titrator produces a mixture of two solutions by computerized infusion and withdrawal cycles from the syringes to the measuring cuvette. All cuvette styles and pathlengths are compatible. Useful with all Olis computerized instruments.

http://olisweb.com/products/accessories/titrator/http://olisweb.com/products/accessories/titrator/

Olis Titrator, two syringe, Peltier Identical to the standard model, but with Peltier thermal control at the syringes. [not shown]

Olis Titrator, Peltier four syringeThe Olis Automatic 4-syringe Titrator produces a mixture of two, three, or four solutions by computerized infusion and withdrawal cycles from the syringes to the measuring cuvette. All cuvette styles and pathlengths are compatible. Useful with all Olis computerized instruments. Junction lines can be changed for different mixing sequences.

http://olisweb.com/products/accessories/http://olisweb.com/products/accessories/peltierassay.phppeltierassay.php

A6

A9

A8 Olis Titrator, four Syringe Four syringe version of the titrator, used to mix up to four different solutions during a study. Developed originally for use as an automatic en-zyme assay device, mixing enzyme, substrate, inhibitor, and buffer.

A7

Page 15: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

15

Accessories

Olis Auxiliary MixerApparatus to be used in conjuction with any of the Olis stopped-fl ows to prepare an A+B solution which is injected into a syringe in the stopped-fl ow. In this way, the solutions used for the stopped-fl ow study are ‘reactive A+B’ and C. [not shown]

See http://olisweb.com/products/accessories/http://olisweb.com/products/accessories/auxmixer.phpauxmixer.php

Millisecond Open/Close Shutter BoxAdd a small computer-controlled shutter anywhere within the optical train of any Olis spectrophotometer to turn a steady-state lamp into a pulse lamp with pulse rates to 40 Hz or protect photolabile samples from the excitation or measuring beam between readings.

A12

A11

DeSa 1.4 Tesla Permanent MagnetThis tiny 1.4 Tesla permanent magnetic can be used for MCD, MLD, MCPL, MFDCD, as well as magnetic fi eld absorbance and fl uorescence work. Rotate the DeSa magnet 180° to do reverse fi eld studies. When used for absorbance and CD, the magnet and cuvette are oriented as illustrated. When used for emission readings (CPL, FDCD, and fl uorescence), the magnet rotated 90° and a 1 cm tall cuvette is slid into place, so that the emission travels out what is now illustrated as the top. No power, no water, no crane required to use this powerful magnet! Can be added to any spectrophotometer.

A10

US Patent 7,092,085 B1 (2006) issued to RJ DeSa

Page 16: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

16

Jacketed Cuvette HolderThe standard Olis cell holder is machined brass with channeling throughout for fl uid concentration around the cuvette from a water bath. The 1 cm² holder removes easily to allow use of the Olis USA stopped-fl ow, QNW Turret 450, or other sample holder. An optional magnetic stir block fi ts within the holder. Ports on all sides of the sample compartment support the addition of secondary detectors and/or actinic sources.

Four Position Cell Changer for Absorbance and FluorescenceThis four position cell holder employs a linear shuffl ing mechanism along with a diagonal geometry which permits use with both absorbance and fl uorescence. The design provides access to clear apertures on all four sides of the cell. Also included are provisions for magnetic stirring of all four cell holders and temperature control of the entire unit by means of external circulating water. Purchase of this unit would include enhanced features in the software to support motorized movement of the cell changer.

Hanging Cuvette HolderJacketed sample and reference cuvette holders are mounted to the underside of the sample compartment lid and water lines are provided for temperature control. The sample cuvette holder has windows on all four sides to allow passage of a fl ash beam and a measuring beam. A round opening in the lid above each cuvette holder allows easy access for inserting and removing sample cuvettes; round plastic lids slip over each of the access holes.

Accessories

A13

A14

A15

Page 17: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

17

Long Pathlength Cell HolderThe newest cell holder accessory features up to 20 cm of pathlength and easily adjusts for variability.

CD Jacketed Cuvette HolderThe standard Olis CD cell holder is machined brass with channeling throughout for fluid concentration around the cuvette from a water bath.

CD Peltier Cell HolderThe CD 250™ is a temperature-controlled cuvette holder for circular dichroism measurements, compatible for use with the three Olis CD instruments (DSM 20, DSM 17 and DSM 1000).

Peltier Controlled Cuvette Holder, Absorbance and FluorescenceQuantum Northwest makes a beautiful cell holder with built-in temperature regulator. The device is exceedingly fast (5-85° in under 5 minutes) and just as remarkably, the conductivity is so good that the sample lags only by a little. The original holder is for 1 cm² cuvettes.

Accessories

A16

A17

A19

A18

Page 18: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

18

Peltier controlled Six position holder, Absorbance and CDQuantum Northwest makes the LC 600™ for use in absorbance spectrophotometers (including circular dichroism). Magnetic stirring is provided under each cuvette and a dry gas purge may be used to dry gas on the cuvette windows to prevent condensation when working at low temperatures. The LC 600™ also features rapid, precise Peltier control over a wide range of temperatures, variable speed magnetic stirring under each cuvette. Dry gas purging prevents condensation when working at low temperatures. Thermal range is -55 °C to +105 °C, ± 0.02 °C.

Peltier Twin Temperature Controlled Cuvette HolderBased on the TLC-50 from Quantum Northwest, this device is designed to be used with Olis® computerized Aminco DW-2 and DW-2000 spectrophotometers. Thermal range is -55 °C to +105 °C, ± 0.02 °C.

Turret Peltier-controlled Four Position TurretFrom the Quantum Northwest website: “Place up to four cuvettes in the TURRET 450 at once, stir and precisely maintain the temperature of each solution. Eliminate oxygen from around the cuvettes. Automate the process of background subtraction or the collection of instrument response functions. Important properties of molecules are dependent on temperature. Provide the temperature control and environment your samples need to make the most of your fl uorescence measurements.”

Accessories

A20

A21

A22

Page 19: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

19

Vertex™ Specular Refl ectance Variable Angle Cell HolderFrom the CIC Photonics website: “The Vertex™ Variable Angle Specular Refl ectance Accessory by CIC Photonics has been designed to permit measurements of the refl ectance of a solid sample material while varying the angle of incidence (AOI) of the source illumination. This is accomplished by simultaneously rotating the sample and a fi xed mirror about a point coincident with both planes. The AOI on the sample varies inversely with that on the mirror; the net result is minimal translation of the beam and constant pathlength.”

Olis has developed a computerized modifi cation of the Vertex accessory to be utilized with Olis Spectrophotometers.

Accessories

A23

Putting it All Together: One Well-Accessorized Olis SpectrophotometerPutting it all together: A rapid-scanning Olis RSM 1000 absorbance system with rapid-scanning fl uorescence and stopped-fl ow and a computerized shutter; ready for the addition of the CD module or any other known or new accessory you need. Spectral range anywhere within 167-2500 nm, determined by selected optics and detectors.US Patent 5,285,254 (1994) issued to RJ DeSa

Page 20: Catalog - Olis, Inc. – Modular Spectrophotometersolisweb.com/olisweb_old/Downloads/Catalog_20080815...Modernized Aminco DW-2 UV/Vis spectrophotometer .....4 AU3. Modernized Cary

For more information on this and other Olis products:

Visit www.olisweb.com

Write [email protected]

Call 1-800-852-3504 in the US & Canada 1-706-353-6547 worldwide

Tour On-Line Instrument Systems, Inc.Tour On-Line Instrument Systems, Inc.Tour 130 Conway Drive, Suites A, B & C Bogart, Georgia 30622 USA

Rhodamine reference sam

ple holder on an O

lis DM

245 fluorimeter

Rotatable sample compart-ment for DSM 20 CD used

on a synchrotron line

NIR CD chamber with LCVR

An integrating sphere chamber with upper and lower (shown) sample mount

A Hansatech Instrument oxygen electrode (insert) as an alternative sample compartment in Olis DM 45.

Custom projects are economically and functionally possible. Many are envisioned by creative investigators and developed by Olis staff. Some might be achieved by Olis staff. Some might be achieved by the investigator without any involvement of Olis personnel. All Olis products are endlessly upgradeable for those who want even more.

02/08

Route To:

______________________________________

______________________________________

______________________________________