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PIERO M. ARMENANTE NJIT Cake Filtration

Cake Filtration

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Page 1: Cake Filtration

PIERO M. ARMENANTENJIT

Cake Filtration

Page 2: Cake Filtration

PIERO M. ARMENANTENJIT

Cake Filtration• Cake filtration consists of passing a solid

suspension (slurry) through a porous mediumor septum (e.g., a woven wire). The solids inthe slurry are retained on the surface of themedium where they build up, forming anincreasing thicker cake.

• As more slurry is filtered the solids retained onthe medium provide most of filtering action. Incake filtration the cake is the real filteringelement.

Page 3: Cake Filtration

PIERO M. ARMENANTENJIT

Cake Filtration (continued)• As time goes by the thickness of the cake

increases, as more solids are filtered. Thisresults in a corresponding increase of thepressure resistance across the cake.

• If the cake is incompressible (i.e., it does notchange its volume as pressure builds up) thepressure resistance increases proportionallyto the cake thickness.

• However, since most cakes are compressiblethe pressure across the cake typicallyincreases even faster than the cake build-up.

Page 4: Cake Filtration

PIERO M. ARMENANTENJIT

Cake Filtration (continued)• The cake is removed intermittently during

batch filtration processes. This is done bytaking the filter off line and manually orautomatically collecting the cake.

• The cake is removed continuously incontinuous processes, for example byscraping the cake with blades, as in rotatingfilters.

• Cake washing and drying operations can alsobe incorporated in the operation of mostfilters.

Page 5: Cake Filtration

PIERO M. ARMENANTENJIT

Examples of Cake-Forming Filters• Filter presses

• Belt filters

• Vacuum filters:

- Rotary vacuum belt filters

- Rotary vacuum precoat filters

- Vacuum disk filters

Page 6: Cake Filtration

PIERO M. ARMENANTENJIT

Example of a Filter Press

After Metcalf and Eddy, Wastewater Engineering, 1991, p. 869

Page 7: Cake Filtration

PIERO M. ARMENANTENJIT

Cross Section of a Filter Press

After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.9

Page 8: Cake Filtration

PIERO M. ARMENANTENJIT

Example of a Belt Filter

After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.10

Page 9: Cake Filtration

PIERO M. ARMENANTENJIT

Schematic of a Belt Press Filter

After Vesilind, Treatment and Disposal of Wastewater Sludges, 1979, p.156.

Page 10: Cake Filtration

PIERO M. ARMENANTENJIT

Example of a Rotary Vacuum Belt Filter

After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.8

Page 11: Cake Filtration

PIERO M. ARMENANTENJIT

Example of a Rotary Vacuum Precoat Filter

To Vacuum

Precoat

CakeDischarge

Slurry

Knife

Filtrate

Page 12: Cake Filtration

PIERO M. ARMENANTENJIT

Precoats and Filter Aids• A precoat is a layer of fine particulate material

(e.g., perlite) added on to the filter septumbefore filtration to form a coating cake

• During filtration the filtered solids in the slurrymay clog the filter and reduce the rate offiltration. This happens especially if theresulting cake is very compressible

• In such cases a filter aid made of fine particlesof a hard but porous material (such as perlite)having good filtering properties is added to theslurry to prevent and filtered with the slurrysolids

Page 13: Cake Filtration

PIERO M. ARMENANTENJIT

Common Types of Precoats and FilterAids

• Diatomaceous earth (diatomite)

A light siliceous material derived primarilyfrom sedimented diatoms (minute planktonicunicellular or colonial algae with silicifiedskeletons). Typical bulk density: 0.32 g/cm3

• Perlite

A volcanic glass made of siliceous rock havinga concentric shelly structure. Typical bulkdensity: 0.16 g/cm3

Page 14: Cake Filtration

PIERO M. ARMENANTENJIT

Analysis ofCake Filtration

Page 15: Cake Filtration

PIERO M. ARMENANTENJIT

Analysis of Suspended SolidsRemoval During Cake Filtration

• As the suspension moves through the filtermedium (septum) the suspended solids arestopped by the filter septum forming a filter cakeon top of the filter septum

• As more solids suspension passes through thefilter the cake builds up providing most of thefiltering action for the incoming suspension

• Equations can be written to describe the removalof the particles in suspension by the filter (i.e.,the formation of the cake) and the pressure dropof the fluid as it passes through the cake

Page 16: Cake Filtration

PIERO M. ARMENANTENJIT

Important Variables in Cake Filtration• Available pressure drop across cake, ∆P (Pa)

• Area of filtration, A (m2)

• Specific resistances of cake, α (m/kg)

• Specific resistances of medium (septum), Rm (1/m)

• Fluid superficial velocity, us (m/s)

• Size of cake particles, Dp (m)

• Shape factor for particles, φs

• Type of solids in suspension

• Cake void fraction, ε (void volume/total bed volume)

• Time, t (s)

Page 17: Cake Filtration

PIERO M. ARMENANTENJIT

Important Variables in Cake Filtration• Cake thickness, L (m)

• Concentration of solids in wastewater, Xw (g/L)

• Residual concentration of solids in filtrate, XF (g/L)

• Mass fraction of solids in cake, XC’ (g/g)

• Cumulative volume of wastewater fed to filter, VW (L)

• Cumulative volume of filtrate generated, VF (L)

• Cumulative mass of wet cake, mc (g)

• Mass of solids in the cake per volume of filtrate, XS (g/L)

• Density of wastewater, ρw (g/L)

• Density of filtrate, ρf (g/L)

Page 18: Cake Filtration

PIERO M. ARMENANTENJIT

Approach to Cake Filtration as aBatch Process

• Cake filtration is intrinsically a batch process.Hence, it can be expected that as filtrationproceeds the cake will build up and thepressure drop across the cake will increase.

• Mathematical modeling of batch cake filtrationis based on the determination of the rate offormation of the cake and the calculation ofpressure drop at any given time.

Page 19: Cake Filtration

PIERO M. ARMENANTENJIT

Approach to Cake Filtration as aBatch Process (continued)

• Integral quantities (such as the cumulativevolume of filtrate produced during a timeinterval, or the mass of the cake generatedduring the same interval) can be calculated byintegration of the basic instantaneous massbalances. In these equations the pressuredrop is typically a function of time.

• Continuous filtration is often modeled as asuccession of batch processes carried outover infinitesimally small time intervals.

Page 20: Cake Filtration

PIERO M. ARMENANTENJIT

Mass Balance Around a FilterFor a filter operating in a batch mode thefollowing diagram can be drawn:

(Wet) Cake

WastewaterFiltrate

VW XW VF XF

mc X'c

Page 21: Cake Filtration

PIERO M. ARMENANTENJIT

Definition of Xs

Xs is defined as the mass of (dry) solids in thecake per volume of filtrate generated.

From this definition it is that:

XX m

Vsc c

F

= =mass of solids in cakevolume of filtrate

'

Page 22: Cake Filtration

PIERO M. ARMENANTENJIT

Relationship Between SolidConcentrations Around a Filter

Mass balances around the filter give:

X V X m X Vw W c c F F= +' (solids)

ρ ρw W c F FV m V= + (overall)

Page 23: Cake Filtration

PIERO M. ARMENANTENJIT

Relationship Between SolidConcentrations Around a Filter (cont.’d)

After an explicit expression for VF has beenobtained it can be substituted in the equationdefining Xs to get:

X XX X

X Xs cW F F W

W W c

= ⋅ −−

''

ρ ρρ

If the densities of the wastewater and the filtrateare the same, then:

ρ ρ ρW F= =

X XX X

X Xs cF W

W c

= ⋅ −−

ρρ

''

Page 24: Cake Filtration

PIERO M. ARMENANTENJIT

Relationship Between SolidConcentrations Around a Filter (cont.’d)

Special case: A common situation is that inwhich all the solids contained in the suspensionare removed by the filter and contribute to theformation of the cake. In other words, the filtratedoes not contain any solids. In such a case it is:

XF ≡ 0

and the expression for Xs becomes:

X XX

X Xs cW

c W

= ⋅−

ρρ

''

Page 25: Cake Filtration

PIERO M. ARMENANTENJIT

Relationship Between SolidConcentrations Around a Filter (cont.’d)

Note that, in general, Xs is different from XW

Only if:

ρ X Xc W'>>

it would then be that:

X XX

X XX

XX

Xs cW

c Wc

W

cW= ⋅

−≅ ⋅ ≅ρ

ρρ

ρ'

''

'

Page 26: Cake Filtration

PIERO M. ARMENANTENJIT

Cumulative Mass Balance for theSolids in the Cake

At a generic time t a cumulative mass balance forthe solids in the cake (i.e., the solids that havecontributed to the formation of the cake in thetime interval 0-t) gives:

solids accumulated in the cake during time t

solids removed from suspension during time t

=

Page 27: Cake Filtration

PIERO M. ARMENANTENJIT

Cumulative Mass Balance for theSolids in the Cake

The previous equation can be rewrittensymbolically, for a generic time t, as:

( ) ( )L A X L A X Vs W s F1− + =ε ρ ε

The first term represents the mass of solids in thesolid component of the cake at time t; the secondterm is the amount of solids still in suspension inthe water contained in the cake; and the thirdterm is the amount of solids removed from thefiltrate (and now held in the cake).

Remark: L, ε, and VF can all be functions of time.

Page 28: Cake Filtration

PIERO M. ARMENANTENJIT

Cumulative Mass Balance for theSolids in the Cake (continued)

The volume of water contained in the cake (εLA) istypically much smaller than the volume of filtrate,VF, produced during the time interval 0-t.Furthermore, Xs and Xw are of the same order ofmagnitude. Then, one can safely assume that:

( )X V X L As F W>> ε

Hence, the cumulative mass balance for thesolids in the cake becomes:

( )L A X Vs s F1− ≅ε ρ

Page 29: Cake Filtration

PIERO M. ARMENANTENJIT

Cake Thickness, L, as a Function ofVolume of Liquid Passed Through

the FilterThe previously derived mass balance equation forthe solids in the cake:

( )L A X Vs s F1− =ε ρ

can be rewritten as:

( )LX V

As F

s

=−1 ε ρ

where L, ε, and VF can all be functions of time.

Page 30: Cake Filtration

PIERO M. ARMENANTENJIT

Shape Factor of Particles in CakeThe particle shape factor, φp, is defined as:

φp = Surface area of sphere having same volume as particleSurface area of particle

i.e.,

φπ

πpp

p

p

sph p

D

DVA

VD A

sph

sph

= ⋅ =6 62

3

where Dsph is the diameter of a sphere having thesame volume as the particle.

Page 31: Cake Filtration

PIERO M. ARMENANTENJIT

Relationship Between Dp, Dsph, and φp

Since:

DVAp

p

p

=6

and:

φpsph

p

pDVA

= ⋅1 6

then:

D Dp p sph= φ

Page 32: Cake Filtration

PIERO M. ARMENANTENJIT

Approximate Relationship BetweenDp and Sieve Opening

The assumption is often made that:

D Dsph p≈

where Dp is the average size of the particleswhose size is between two sieve openings

D D Dp s s= 1 2

and where Ds1 and Ds2 are the sieve openings.Then:

D D Dp p sph p p= ≅φ φ

Page 33: Cake Filtration

PIERO M. ARMENANTENJIT

Pressure Drop During Cake Filtration

Filter Cake L(t)

Filter Medium

Filtrate

Suspension

∆Pc(t)

∆Pm

Page 34: Cake Filtration

PIERO M. ARMENANTENJIT

Pressure Drop During Cake FiltrationAt any time, t, the pressure drop experienced atthat time by a suspension passing through a filtercake supported by a filter medium (or septum) is:

( ) ( )∆ ∆ ∆P t P t Pc m= +where:∆P(t) = total pressure drop across filter

∆Pc(t) = pressure drop due to filter cake

∆Pm = pressure drop due to filter medium

Remark: during batch filtration the cake can beexpected to build up, and the pressure drop toincrease as time passes.

Page 35: Cake Filtration

PIERO M. ARMENANTENJIT

Pressure Drop Across Filter CakeSince the liquid passing through the filter cakemoves in laminar flow (because of the small poresof the cake and the slow fluid velocity) the Blake-Kozeny equation can be used (instead of the moregeneral Ergun equation) to describe thedependence of the pressure drop through thecake with the superficial velocity, us:

( )∆P

LD

ucp p

L s= −

150 1 2

32

Reε

ε ρ Blake-Kozeny equation

where ∆Pc is the pressure drop through the cake,and is, in general, a function of time.

Page 36: Cake Filtration

PIERO M. ARMENANTENJIT

Pressure Drop Across Filter CakesSubstituting the expression for Re in the Blake-Kozeny equation gives:

( )∆P

LD

ucp

s= −

1501 2

3 2µ εε

As before, ∆Pc is typically a function of time, sincethe cake thickness, L, the superficial velocity, us,and the void fraction, ε, can all change with time.

Page 37: Cake Filtration

PIERO M. ARMENANTENJIT

Pressure Drop Across Filter Cakes(Carman-Kozeny Equation)

For filter cakes the constant 150 may not beappropriate since the cake particles arecompressible.

Therefore the Blake-Kozeny equation is oftenrewritten to produce to so-called Carman-Kozenyequation:

( )∆P k

LD

ucp

s= −

1

2

3 2

1µ εε Carman-Kozeny equation

where: k1 = proportionality constant.

Page 38: Cake Filtration

PIERO M. ARMENANTENJIT

Superficial Velocity in Cake FiltrationAs before, the superficial (or approach) velocity isdefined as the velocity of the liquid as it flowsthrough a cross section equal to that of the tank(or filter vessel) in the absence of the cake. It isalso equal to the filtrate flow rate, QF, divided bythe total cross-sectional area normal to flow, i.e.:

uQA

dVd t As

F F= = 1

where:A = cross sectional area or empty filter vessel

VF = volume of filtrate passed through the cakeduring time t

Page 39: Cake Filtration

PIERO M. ARMENANTENJIT

Equation for Pressure Dropin the Cake

Combining together the equations:

( )∆P k

LD

ucp

s= −

1

2

3 2

1µ εε u

QA

dVd t As

F F= = 1

and: ( )LX V

As F

s

=−1 ε ρ

the following expression for ∆Pc is found:

( )( )∆P k

DX VA

dVd tc

s p

s F F=−

1

2

3 2 2

1 11ρ

εε ε

µ

Page 40: Cake Filtration

PIERO M. ARMENANTENJIT

Equation for Pressure Dropin the Cake

The previous equation can be re-arranged to givethe final equation for the pressure drop in thecake:

∆PX VA

dVd tc

s F F= α µ 2

where α = specific cake resistance to filtration, isgiven by:

αρ

εε

= −kDs p

12 3

1

∆PC, L, α, and VF can all be functions of time.

Page 41: Cake Filtration

PIERO M. ARMENANTENJIT

Equation for Pressure Dropin Filter Medium (Septum)

The pressure drop across the filter medium(septum) can also be expressed using theCarman-Kozeny equation that can be rewritten as:

( )∆P kLD

umm

m

m

pms=

2

2

3 2

εε

where the subscript “m” refers to the medium andthe superficial velocity is given by:

uQA

dVd t As

F F= = 1

Page 42: Cake Filtration

PIERO M. ARMENANTENJIT

Equation for Pressure Drop in FilterMedium (continued)

The resulting expression of the pressure drop inthe medium is:

∆P RA

dVd tm m

F= µ 1

where:

( )R k

LDm

m

m

m

pm

=−

2

2

3 2

1 εε

with Rm = specific resistance of medium tofiltration

Page 43: Cake Filtration

PIERO M. ARMENANTENJIT

Equation for Total Pressure DropDuring Cake Filtration

Recalling that the total pressure drop in a filter is:( ) ( )∆ ∆ ∆P t P t Pc m= +

it is:

( ) ( ) ( )∆P t t

X V tA

RA

dVd t

s Fm

F= +

α µ µ2

1

Since by definition it is: QF(t) = dVF/dt, then:

( ) ( )( ) ( )[ ]

dVd t

Q tA P t

t X V t ARF

Fs F m

= =+

2 ∆µ α

This is the main design equation for cake filters.

Page 44: Cake Filtration

PIERO M. ARMENANTENJIT

Specific Cake Resistance andCake Compressibility

From the expression for α:

αρ

εε

= −kDs p

12 3

1

one can incorrectly assume that the pressureacross the cake has no impact on specific cakeresistance. In fact, the void fraction ε for mostcakes can be significantly affected by pressure,since the cake is often compressible. Since thepressure drop changes with time the void fractionε can also be a function of time, at least inprinciple.

Page 45: Cake Filtration

PIERO M. ARMENANTENJIT

Specific Cake Resistance andCake Compressibility

In practice, it is convenient to carry outexperiments to determine:

• the specific cake resistance under no pressuredifference (no compression). Cake is built upby gravity filtering;

• the effect of pressure difference across thecake on the specific cake resistance. Cake isbuilt up first and then compressed to a knowpressure with a piston provided with a porousbottom. Filtrate is passed trough the cake.

Page 46: Cake Filtration

PIERO M. ARMENANTENJIT

Specific Cake Resistance andCake Compressibility

Piston

Suspension

Filtrate

Cake

CakeBuildup

CompressedCake

Suspension

Filtrate

Filtrate

PP

Page 47: Cake Filtration

PIERO M. ARMENANTENJIT

Specific Cake Resistance andCake Compressibility (continued)Possible results of cake compression experiment:

• cake is incompressible. Cake resistance, α isindependent of ∆P;

• cake is compressible. Cake resistance isexpressed as:

( )α α= osP∆

with: αo = empirical constants = coefficient of compressibility (typicalrange for most domestic sludges: 0.4-0.9; lime sludges: 1.05; sand: 0).

Page 48: Cake Filtration

PIERO M. ARMENANTENJIT

Specific Cake ResistanceTypical values of the specific cake resistance, α,are in the following ranges:

• 1013-1015 m/kg for raw sludges;

• 1011-1012 m/kg for well conditioned sludges.

Page 49: Cake Filtration

PIERO M. ARMENANTENJIT

Typical Specific Cake Resistancewith Chemical Conditioning

0 0.5 1 1.5 2 2.5

Chemical Conditioner (%)

1E+010

1E+011

1E+012

1E+013

1E+014

Spe

cific

Cak

e R

esis

tanc

e, α

(m/k

g)

After Vesilind, Treatment and Disposal of Wastewater Sludges, 1979, p.156.

Page 50: Cake Filtration

PIERO M. ARMENANTENJIT

Compressibility of Sludges as Measuredby the Specific Resistance Test

1 10 100

Vacuum Pressure (kPa)

1E+010

1E+011

1E+012

Spe

cific

Cak

e R

esis

tanc

e, α

(m/k

g)

After Vesilind, Treatment and Disposal of Wastewater Sludges, 1979, p.156.

Page 51: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Filtration OperationsBatch cake filtration is typically carried out underone of the following conditions:

• Constant filtrate flow rate. Since the pressuredrop across the filter increases as a result ofcake buildup this condition implies that theupstream pressure must be increased withtime.

• Constant pressure drop across the filter. Thiscondition implies that the filtrate flow ratedeclines as the cake builds up.

• Variable flow rate and variable pressure drop.

Page 52: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration atConstant Filtrate Flow Rate

In some cases cake filtration is carried out usinga positive displacement pump. This results in aconstant flow rate process. Then:

QF = constantRecalling the design equation for cake filters it is:

( )( ) ( )[ ]

dVd t

QA P t

t X V t ARF

Fs F m

= =+

2 ∆µ α

Important: although QF = dVF/dt is a constant, VF(the total filtrate at time t) is not. In fact, it is:

dV Qdt V Q tF F F= ⇒ =

Page 53: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration atConstant Filtrate Flow Rate (cont' d)

Assuming that the cake is not compressible (i.e.,α is independent of ∆P) the pressure buildupwhile operating at constant filtrate flow rate (i.e.,constant QF) is given by:

( ) ( )[ ]∆P tX V t AR

AQs F m

F=+µ α

2

i.e., recalling that VF = QF·t:

( )∆P tX QA

tR Q

As F m F= +µα µ2

2 ( )for constantQF =

Page 54: Cake Filtration

PIERO M. ARMENANTENJIT

Applications of Batch Cake Filtrationat Constant Filtrate Flow Rate

• Batch cake filtration at constant filtrate flowrate is used primarily in sludge dewatering;

• The type of filters that utilizes filtration methodis the filter press;

• Positive displacement pumps are used to forcethe suspension through the filter;

• Gauge pressures up to 225 psi (15 atm) areused.

Page 55: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration at Constant ∆PIf the pressure across the filter is constant thegeneral filtration equation:

( ) ( )( ) ( )[ ]

dVd t

Q tA P t

t X V t ARF

Fs F m

= =+

2 ∆µ α

becomes:

( ) ( )[ ]dVd t

Q tA P

X V t ARF

Fs F m

= =+

2 ∆µ α

Note that the coefficient α is constant (but notnecessarily equal to αo) even if the cake iscompressible, since ∆P = constant.

Page 56: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration atConstant ∆P (continued)

Since ∆P = constant, the previous equation can beintegrated by separating variables:

( )µ α X V AR

A PdV d ts F m

F

Vt

F '' '

+⌠

⌡ = ∫2

00∆

Integration of this equation yields:

( ) ( )µα µXA P

V tR

A PV t ts

Fm

F2 22

∆ ∆+ = ( )for constant∆P =

Page 57: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration atConstant ∆P (continued)

The previous equation can be rewritten as:

( ) ( )η γV t V t tF F2 + =

where ∆P is constant, and the parameters η and γare given by the equations:

η µα= XA P

s

2 2 ∆ and γ µ= RA P

m

Page 58: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration at Constant ∆P:Determination of Filtration Parameters

The determination of η and γ from batchexperiments conducted at constant ∆P can bemade by rearranging the equation:

( ) ( )µα µXA P

V tR

A PV t ts

Fm

F2 22

∆ ∆+ =

as: ( ) ( )tV t

XA P

V tR

A PF

sF

m= +µα µ2 2 ∆ ∆

with: slope and intercept= = = =η µα γ µXA P

RA P

s m

2 2 ∆ ∆and t/VF = y-coordinate and VF = x-coordinate

Page 59: Cake Filtration

PIERO M. ARMENANTENJIT

Determination of the Specific Cake ResistanceThrough Batch Filtration Experiments atConstant ∆P: Buchner Funnel Apparatus

Buchner Filter

Vacuum Gauge

Graduated Cylinder

To Vacuum

Page 60: Cake Filtration

PIERO M. ARMENANTENJIT

Determination of the Specific Cake ResistanceThrough Batch Filtration Experiments at

Constant ∆P: Filter Leaf Apparatus

VacuumGauge

GraduatedCylinder

To Vacuum

FilterLeaf

Page 61: Cake Filtration

PIERO M. ARMENANTENJIT

Example of ExperimentalDetermination of Filtration Constants

0 0.001 0.002 0.003 0.004 0.005 0.006

Cumulative Filtrate Volume, VF (m3)

0

5,000

10,000

15,000

20,000

25,000

t/VF

(s/m

3 )

ExperimentalRegression

Intercept = 6840.95 s/m3

Slope = 2.85378E+006 s/m6

Page 62: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration at Constant ∆P:Approximate Equations

If the resistance of the filter medium, Rm, is verysmall in comparison to the cake resistance, α, thebatch filtration equation can be rewritten as:

( )tX

A PV ts

s≅ µα2 2

2

∆ ⇒ ( )V t

A PX

tt

FF

≅ =2 2 ∆µα η

i.e.:

( )Q tdVd t

A PX t tF

F

F

= ≅ =12

2 12

12 ∆µα η

Note that QF(t)→ 0 for t→ ∞ .

Page 63: Cake Filtration

PIERO M. ARMENANTENJIT

Batch Cake Filtration at Constant ∆P:Plot of Approximate Expression

for VF(t)

Time, t

Cum

ulat

ive

Filtr

ate

Vol

ume,

VF

Page 64: Cake Filtration

PIERO M. ARMENANTENJIT

Applications of Batch Cake Filtrationat Constant ∆P

• Batch cake filtration at constant ∆P is usedprimarily in sludge dewatering;

• The types of filters using this filtration methodinclude:

- Filter presses

- Belt filter presses

Page 65: Cake Filtration

PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Rotary Vacuum Filters

Page 66: Cake Filtration

PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Rotary Vacuum Filter

CakeDewatering

CakeDischarge

Suspension

Solids

Cake

Blade

CakeFormation

θ

Page 67: Cake Filtration

PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Rotary Vacuum Filters

• In continuous filtration operations, such asthose involving vacuum rotary filters, eachfilter element undergoes a batch cakefiltration, followed by a cake dewatering phase,and a cake discharge phase with each rotation.

• The filter cake is formed under a constant ∆Pdriving force generated by a vacuum.

• The filter cake is formed only during the timeperiod when the filter surface is immersed inthe suspension.

Page 68: Cake Filtration

PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Cycle Time

The immersion period in each cycle (i.e., for eachfull rotation of the filter drum) is given by:

t f t fk c k= = = =22

2πω

θπ

πω

θω

where: tc = cycle time (time for one full rotation)fk = fraction of cycle time available for cake

formation = fraction submergence of drumsurface

θ = angle comprising the sector immersed insuspension (rad)

ω = rotational (angular) velocity (rad/s)

Page 69: Cake Filtration

PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Filtration EquationDuring the time period t = fk tc the filter cake in arotary filter is formed just as in a batch operation.The (batch) filtration equation for part of thecontinuous process is:

( ) ( )µα µXA P

V tR

A PV t t f ts

Fm

F k c2 22

∆ ∆+ = =

since ∆P is constant.

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Continuous Cake Filtration atConstant ∆P: Filtrate Generated

During a CycleThe previous quadratic expression is an equationin VF that can be solved for VF and rearranged togive:

( )V tAX

R Rf t X P

Fs

m mk c s= − + +

α

αµ

2 2 ∆

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PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Filtrate Flux

The previous equation can be rearranged to give:

Filtrate flux = =

= = − + +

QA

VAt X

Rt

Rt

f X Pt

F

F

c s

m

c

m

c

k s

c

1 22

2ααµ

which predicts the filtrate flux, i.e., the amount offiltrate VF produced per unit filter area during acycle (or full rotation) lasting a time interval tc.QF = average filtrate flow rate during the interval tc

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Continuous Cake Filtration atConstant ∆P: Filter Loading

This equation can be rewritten to give the amountof filter solids loading, Gk, produced during thesame cycle:

G V XAt

Rt

Rt

f X Ptk

F s

c

m

c

m

c

k s

c

= = − + +

1 22

2ααµ

where:

Gk = filter solids loading (kg/m2 s) = amount ofsolids filtered per unit filter area over a timeinterval tc.

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PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Continuous Operation

Since a continuous process is nothing more thana sequence of cycles, each one lasting tc, then:

Filtrate flux = = − + +

QA X

Rt

Rt

f X Pt

F

s

m

c

m

c

k s

c

1 22

2ααµ

The equation:

G V XAt

Rt

Rt

f X Ptk

F s

c

m

c

m

c

k s

c

= = − + +

1 22

2ααµ

can be used to describe the continuous operationof a rotary (vacuum) filter.

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PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Rotational VelocityIf the angular velocity is expressed in rpm, i.e.:

N = 602ωπ

then the cycle time and the rotational (angular)velocities (in rad/s or rpm) are related by:

tNc = =2 60π

ωwhere: ω = rotational (angular) velocity in rad/stc = cycle time (to complete a rotation) in secondsN = rotational (angular) velocity in rpm (rotations

per minute).

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PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Continuous Filtrate Flux

The continuous filtrate flux can be convenientlyexpressed in terms of the agitation velocity:

( )Filtrate flux = = − + +

QA X

R R f X PF

s

m m k s12 2

2 2

2αω

πω

πω α

µπ∆

( )Filtrate flux = = − + +

QA X

R N R N f N X PF

s

m m k s160 60

260

2 2

2αα

µ∆

where: tc = cycle time (to complete a rotation), in sN = rotational (angular) velocity in rpm (rotations

per minute).

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PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Simplified EquationsIf the resistance of the filter medium, Rm, is verysmall then the equations for continuous filtrationcan be simplified and rewritten as:

Filtrate flux = = ≅QA

VAt

f PX t

F F

c

k

s c

2 ∆µα

G V XAt

f X Ptk

F s

c

k s

c

= ≅ 2 ∆µα

These equations are especially useful tounderstand the relationships between the variousvariables affecting a continuous filtration process.

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PIERO M. ARMENANTENJIT

Continuous Cake Filtration atConstant ∆P: Simplified Equations

If the resistance of the filter medium, Rm, is verysmall the equations for continuous filtration can beexpressed as a function of the rotational velocity as:

Filtrate flux = = ≅ ≅QA

VAt

f PX

F F

c

k

s

∆ ωπµα

≅ 260

f P NX

k

s

∆µα

where: tc = cycle time (to complete a rotation) in sN = rotational (angular) velocity in rpm (rotations

per minute).

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PIERO M. ARMENANTENJIT

Applications of Continuous CakeFiltration at Constant ∆P

• Continuous cake filtration at constant ∆P is themost widely used method of sludgedewatering;

• The types of filters using this filtration methodinclude:

- Rotary vacuum belt filter

- Rotary vacuum precoat filters

- Rotary vacuum drum filters

- Rotary vacuum disc filters

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PIERO M. ARMENANTENJIT

Comparison of Different Types of FiltersRotary

Drum BeltFilters

Belt FilterPresses

FilterPresses

GranularDeep-Bed

Filters

Size 1-70 m2 1-2 m beltwidth

0.02-16 m3 0.2-10 m2

Solids inFeed (%)

2-5 2-8 -- --

Solids inCake (%)

15-20 15-25 28-40

SolidsLoading

10 kg/m2 h 190-270kg/m h

-- 0.12-0.5m3/m2 min

After Freeman, Standard Handbook of Hazardous Waste Treatment andDisposal, 1989, p. 7.12

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PIERO M. ARMENANTENJIT

Design Information for PressureCake Filters

Cycle time: of the order of hours

Solids loading: 0.2-2 lb/ft·h

Solids in cake: up to 50%

Remark: although solids loading in pressurefilters (e.g., filter presses) is typically smaller thanthat of vacuum filters the percentage of solids inthe cake is typically higher. This is the result ofthe higher pressure that can be used in theoperation of pressure filters (as opposed to amaximum of 1 atm in vacuum filters).

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PIERO M. ARMENANTENJIT

Design Information for Rotary Vacuum FiltersDiameter: up to 5 mLength: up to 6 mVacuum levels: typically 20 in. Hg (68 kPa)Submergence: 15-25% of drum area

PrimarySludges

Waste-activatedsludges

Solids loading 20-60 kg/m2·h(4-12 lb/ft2·h)

5-20 kg/m2·h(1-4 lb/ft2·h)

Solids in cake 25-40%(typically 20-25%)

10-15%

After Sundstrom and Klei, Wastewater Treatment, 1979, p. 234.

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PIERO M. ARMENANTENJIT

Operation of Rotary Vacuum Filters• Solids loading increases with increasing drum

submergence, drum rotational speed, pressuredifference across cake, solids concentration infeed.

• Percentage of solids in cake decreases withincreasing drum submergence, and drumrotational speed.

• Rotary vacuum filters can be used to dewatersludges from activated sludge plants(biological sludges), chemical sludges, andsludges from precipitation operations.

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PIERO M. ARMENANTENJIT

Additional Information and Exampleson Cake Filtration

Additional information and examples on can be found inthe following references:

• Sundstrom, D. W. and Klei, H. E., 1979, WastewaterTreatment, Prentice Hall, Englewood Cliffs, NJ, p.229-234.

• Geankoplis, C. J., Transport Processes and UnitOperations, 3rd Edition, 1993, Allyn and Bacon,Boston, pp. 800-815.

• Freeman, H. M. (ed.), 1989, Standard Handbook ofHazardous Waste Treatment and Disposal, McGraw-Hill, New York, pp. 7.3-7.19.

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PIERO M. ARMENANTENJIT

Additional Information and Exampleson Cake Filtration

• Haas, C. N. and Vamos, R. J., 1995, Hazardous andIndustrial Waste Treatment, Prentice Hall, EnglewoodCliffs, NJ, pp. 75-78.

• Wentz, C. W., 1995, Hazardous Waste Management,Second Edition, McGraw-Hill, New York. pp. 196-200.

• Vesilind, P. A., 1979, Treatment and Disposal ofWastewater Sludges, Ann Arbor Science, Ann Arbor,MI, pp. 140-161.

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PIERO M. ARMENANTENJIT