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Bringing broadband NMR to your benchtop
Reaction Monitoring
Monitor your reactions as they happen.
Monitor your reactions at a range of temperatures.
2.903.003.103.203.303.403.503.603.703.80
f1 (ppm)
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2.903.003.103.203.303.403.503.603.703.80
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True X-Nuclei
Tuneable broadband preamplifier allows you to select nuclei from 29Si to 31P to match your experimental needs.
-20-100102030405060708090100110120130140150160170180190f1 ( ppm)
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CH3
CH3
CH3
OH
O-30-25-20-15-10-505101520253035404550556065
f1 (ppm)
-0.1
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1.0
Si
O
O
SiH
SiH
CH3
CH3
CH3
CH3
CH3
CH3
29Si
No compromises! X-Pulse lets you maximise your signal-to-noise ratio with optional interchangeable X-Pods for specific nuclei.
13C
-340-320-300-280-260-240-220-200-180-160-140-120-100-80-60-40-200f1 (ppm)
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F F
F
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F K+
-6.0-5.8-5.6-5.4-5.2-5.0-4.8-4.6-4.4-4.2-4.0-3.8-3.6-3.4-3.2-3.0-2.8-2.6-2.4-2.2-2.0-1.8-1.6-1.4-1.2
f1 (ppm)
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Na+
F
B-
F
FF
31P
Learn more at:nmr.oxinst.com/x-pulse
11B
Easy operationQuick experiments turn
complex pulse sequences
into a single click allowing
anyone to access the
power of NMR
Clearer spectraNew shimming
technology allows
spectral resolution of
<0.35Hz/10Hz
as standard
Ultimate stabilityFlow liquid samples at variable temperature (20°C – 60°C) without
spectral artefacts. Run high duty cycle pulse sequences without
destabilising the magnet
Benchtop convenienceNo requirement for special facilities or liquid
cryogens allowing you to use the X-Pulse wherever
is most convenient
Easy to use and maintain Removable and
easy-to-access probe
for cleaning. Use with
standard 5mm NMR
tubes or easy-to-use
flow cell
Flexible softwareSpinFlow advanced
mode allows you to
define your own
experiments, your way
No need to compromiseInterchangeable X-Pods allow you to optimise
signal-to-noise ratio for specific nuclei
Choose your nucleiMeasure the nuclei you need for your experiments with
the world’s first broadband benchtop NMR spectrometer
Advanced pulse sequencesPulsed field gradients
and shaped RF pulses as
standard for: coherence
selection, selective
excitation, water and
solvent suppression
0.50.60.70.80.91.01.11.21.31.41.51.61.71.81.92.02.12.22.32.42.52.62.72.82.93.03.13.23.33.4
f1 (ppm)
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600Easily analyse your spectraUnique 60MHz magnet design provides high
field homogeneity delivering resolution of
<0.35Hz (FWHM) making it easier to distinguish
overlapping peaks and identify compounds at
lower concentrations.
60MHz spectra at 1Hz linewidth (red) and 0.35Hz linewidth (green)
Quickly switch between 1H and 19F
Quantify your 19F spectra with ease using the
highest signal-to-noise 60MHz fluorine system
available with no requirement to filter
background signals.
Expand your capability for the analysis of:
• Li+ Battery electrolytes
• Fluorinated pharmaceuticals
• Fluorinated polymers
• Water contaminants
Br
F
F
F
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Br7
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Br7
F8
F9
F10
X-Pulse has the tools you need to understand
your molecules and determine their structure.
12346712
f1 (ppm)
CH3
CH3
O
OH
O
CH3
CH3
From spectra to structural elucidation
• Simple 1D spectra
• 2D experiments
• Inverse experiments
• Shaped pulses
• Pulsed field gradients
• Powerful MNova software
Shaped RF pulses unlock
advanced pulse sequences
and allow you to improve
your solvent suppression.
Shaped pulses combined with the improved
linewidth of the X-Pulse makes removing
solvent peaks more effective than ever.
Advanced pulse sequences
like the selective 1D TOCSY
can be used in place of
some 2D experiments,
simplifying spectral analysis
and allowing you to obtain
your results more quickly.
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f1 (
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2.83.03.23.43.63.84.04.24.44.64.85.05.25.45.65.86.0
f1 (ppm)
1
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1H 1D NMR300 mM Mannose
80% H2O/20% D2O
1H 1D NMR - Water Suppression300 mM Mannose
80% H2O/20% D2O
0.00.51.01.52.02.53.03.54.04.55.05.56.06.57.07.58.0f1 (ppm)
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CH31
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O5
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CH37
O
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CH31
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OH7
O8
+
CH31
2
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O5
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CH37
O
8
CH31
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OH7
O8
+
CH31
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O5
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CH37
O
8
CH31
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OH7
O8
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CH31
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O5
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CH37
O
8
CH31
2
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OH7
O8
+
FID
1D TOCSY
1D TOCSY
1D TOCSY
We’re here to help you!OiService aims to keep your instrumentworking as hard as you do. Our globalnetwork of service hubs provides a fullrange of technical support.
Consumables and accessoriesRange of sample tubes and otheraccessories available.
Extended warrantiesAvoid unplanned costs.
Online diagnosticsIn-depth support over the internet.
Maintenance contractsEnsures your analyser producesthe right result every time.
RepairsFast and efficient turnaround.
Telephone help-desksFor a fast response to your problem.
TrainingUnderstand your analyserand its features.
iService®
This brochure provides only a glimpse into the technology of X-Pulse and its applications. Find out more at:
nmr.oxinst.com/x-pulse
Unleash the power of QA/QC in your benchtop NMREnsure the consistency of your products and processes while spotting any contaminants. Quickly
identify compounds, even in mixtures, or low concentration adulterants using chemometric
fingerprinting from your own custom-built database.
Compare unknown spectra
against user-defined database
to get top matches.
Generate synthetic
combinations of spectra
to match the original
unknown.
Spectrum of ‘unknown’ test sample
2 regions of interest
Synthesised mixture of matches #1 and #6 gives best match to original unknown spectrum.
+
Match #10
Match #9
Match #8
Match #7
Match #6
Match #5
Match #4
Match #3
Match #2
Match #1
Match #1
Match #2
Match #10
Match #9
Match #8
Match #7
Match #6
Match #5
Match #4
Match #3
Match #2
Match #1
Match #1
Match #2
Match #10
Match #9
Match #8
Match #7
Match #6
Match #5
Match #4
Match #3
Match #2
Match #1
Match #1
Match #2
PolymersPetrochemicals ResearchPharmaceuticals Chemistry Education
Industrial Chemistry
• Extended warranties
• Consumables and accessories
• Maintenance contracts
• Remote support
• Repairs
© Oxford Instruments Industrial Products Ltd trading as Oxford Instruments Magnetic Resonance, 2020. All rights reserved. Do not reproduce without permission.Part no: MR/215/0320