b EQUIPMENT SPEClFlCAllON COm

b

EQUIPMENT SPEClFlCAllON FDBV C O m . : 5531 -05

CATALYST FILTER CUENT CONTFi. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 M 4 RQ

HOD PALkHLE NO. : ii C13

--

CATALYST FILTER

I P.O. NO. : 5i3105- Y -0WI-01

THE MANUFACTURER I S RESPOWSIBLE THAT DESIGN AND COWSTRUCTIW ARE I N ACCORDANCE UITH THE SPECIFICATIOWS AND CODES REFERRED T 0 OW THE EQUIPMENT SPECIFICATIOW AND/OR DRAUINGS. FURTHERHORE, THE MANUFACTURER I S RESPONSIBLE FüR ENSURING THAT THE DESIGN I S SATISFACTORY FOR THE DESIGN CONDITIOWS INDICATED OW THE EQUIPMENT SPECIFICATIOW AND/OR DRAUINGS. CALCULATIOWS AND THICKNESSES OF MATERIAL SUPPLIED T 0 THE MANUFACTURER ARE FOR INFORMATIOW OWLY AND TENDERING WRWSES OWLY. THE MANUFACTURER SHALL MAKE HIS O W i CALWLATIOWS FOR UHICH HE I S FULLY RESPONSIBLE. THE MANUFACTURER SHALL ENSURE THAT THE SUPPLY COWFORMS T 0 ALL APPLICABLE CODES AN0 NATIOWAL STATUTORY REGULATIONS AND HE SHALL OBTAIN ALL NECESSARY APPROVALS F R a STATUTORY AUTHORITIES.

REMARKS ANDIOR DESCRIPTiON OF REVISIONS

F i r s t i s s u e : - Rev . A : I s s u e f o r i n q u i r y / f o r a p p r o v a t Rev. 8 : ISSUE FDC PHRLH RSE R e v - C : 35SUE Fm2 FIIYISL UPDClTE Rev. Rev.

L T O T R L NMHIER G f 3HEETS: 1s

I Sheet No. 1 cont 'd o n sheet No. Engineered b~ : FLUOR DANIEL B.V. - HAARLEM

Client : H.S.C. - V.O.F. - GELEEN

5531!001.CAB GSPECOOl

Equipm. No.

üoc. No. S-2441 A/B

HSC 1061343-A4

EQUIPMENT SPECIFICATION CATALYST F1 LTER

(continued)

FüüV C O m . : 5531 -05

CUEM CONTR. :

R.F.Q. NO. : 553105-4-0704 RP

P.O. NO. : 553105-4-0704

1.0 INTRODUCTION

2.0 SCOPE OF SUPPLY

3.0 SCOPE OF SERVICES

4.0 PROCESS DATA AND SYSTEM DESCRIPTION

5.0 MECHANICAL DESIGN REQUIREMENTS

6.0 ELECTRICAL/CONTROL SYSTEM REQUIREMENTS

7.0 TECHNICAL DUTY GUARANTEE CONDITIONS

8.0 NOISE REQUIREMENTS

9.0 APPLICABLE DOCUMENTS

ATTACHMENTS No. Title Rev .

1 SITE DATA C 2 UTILITY CONDITIONS D 3 APM PLAN TIME SCHEDULE 2 4 PROCESS FLOW DIAGRAM B 5 EQUIPMENT SPECIFICATION SHEETS C

5531!001.CAB Rev. C

Engineered by : FLUOR DANIEL B.V. - HAARLEM


GSPECW2

Sheet No. 2 coni'd on sheet No.

Equipm. No.

k ~ c . No. 5-2441 A/B

HSC 1061343 - A4

EQUIPMENT SPECIFICATION CATALYST F1 LTER

(continued)

FDBV CONiR. : 5531 -05 CLlENT COMR. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO. : 553105-4-0704

1.0 INTRODUCTION

1.1 Pur~ose

This specification describes the minimum requirements for the design, engineering, fabrication, inspection, testing and supply of 2 catalyst filters S-2441 A/B complete, as specified in this specification and its references. The catalyst filters S-2441 A/B will be installed outdoors at the HSC plant, Geleen, The Netherlands.

2.0 SCOPE OF SUPPLY

Catalyst filter Unit S-2441 shall include but is not limited to the following:

2.1 Main Eaui~ment

I tem No. Descri~tion Quant i tv

S-2441 A/B Catalyst filter 1 m i t (2 centrifugal type filters including filter elements)

SE-2441 A/B Catalyst filter motor 2 PC (With belt drive)

2 PC Stainless steel pneumatic discharge valves

2.1.1 DSM Number ~lates for rotating eaui~ment.

The following items shall be provided with a separate stainless steel nameplate, fixed with stainless steel bolts, showing the applicable number in letters of at least 10 mm height: - For SE-2441 A: DSM-36917 - For SE-2441 B: DSM-36918

2.1.2 All necessary parts to meet the design requirements as laid down in this specification and its references as to complete a functionable Catalyst Filter Unit.

2.1.3 P ~ D ing

- All interconnecting process- and utility piping plus appurtenances. - All process- and utility feed lines up to easy connectable location

at outer edge of unit.

2.1.4 Structural

- Complete structural steelwork for supporting and accessibility of the equipment involved.

5531!001.CAB Rev. C

Engineered by : FLUOR DANIEL B.V. - HAARLEM Client : H.S.C. - V.O.F. - GELEEN

GSPECOM

Sheet No. 3 cont'd on sheet No.

Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343 - A4

FWOR M I E L 9 EQUIPMENT SPEClFlCATlON CATALYST FILTER

(conünued)

FDBV COMR. : 5531 -05

CUENT CONTFi. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO. : 553105-4-0704

.

2.1.5 Control Svstems

- The unit shall be provided with all instrumentation required for operation and safeguarding of the mechanical equipment and shall include supply and installation of all necessary tubing and cabling, up to terminal boxes and instrument housings. Cabling from terminal boxes to the Central Control System will be done by others .

2.1.6 Svares/Svecial Tools

For gasket to be supplied with vessels etc., the following supplementary quantities of new unused gaskets shall be supplied: - standardized gaskets e.g. acc. to ANSI, etc. 2 sets - non standardized gaskets 4 sets

For any type of bolt, studbolt and nut to be supplied for flange boltings etc., the following supplementary quantities shall be supplied: - standardized bolts in quality 4.6-2 or equivalent none - standardized nuts in quality 5 or equivalent none - all other bolts, studbolts and nuts 5% (min. 2)

Any special tools required for assembly, maintenance or repair of unit components.

2.2 Surface Prevaration. Paintinz and Insulation

2.2.1 Structural Steel

All structural steel components shall be provided with a complete coating system as described in Para 5.0.

2.2.2 Eauivment

All equipment shall be provided with a complete coating system as described in Para 5.0.

2.2.3 Insulation and tracine;

Seller shall supply insulation provisions only, for all equipment and piping requiring insulation for heat conservation or personnel protec- tion. Seller shall indicate on his drawings the extent of insulation and the required thickness. Seller shall also indicate where electrical tracing is required.

5531!001.CAB Rev. C

Engineered by : FLUOR DAN1 EL B.V. - HAARLEH


GSPECW2


Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343-A4

F- MNIEL 9 EQUIPMENT SPECIFICATION CATALYST FILTER

(continued)

FDBV C O W . : 5 5 3 1 - 0 5

CLIENT CONiR. :

R.F.Q. NO. : 553105 -4 -0704 RQ

P.O. NO. : 553105 -4 -0704

2.3 ITEMS EXPLICITLY EXCLUDED FROM SCOPE OF SUPPLY

- Concrete foundation and mounting anchor bolts - Power supply to all electrical Systems - Utilities and process piping up to battery limits - Main control and safeguarding System hardware - Actual insulation and electrical tracing

3.0 SCOPE OF SERVICES

3.1 Detailed engineering and design in accordance with this specification and its references.

3.2 Submittal of all completed documents as specified on the VCDC sheets and their clarification.

3.3 Complete testing and inspection of entire unit as required per specification, code or data/requisition sheets.

3.4 Seller shall supply all infonnation required to enable smooth hook-up to the DCS for safeguarding and control of the unit.

3.5 All activities in order to comply with Stoomwezen and or CKD (Centrale Kontrole Dienst) requirements

4.0 PROCESS DATA AND SYSTEM DESCRIPTION

4.1 General

The filters are to be designed to recover 2% Pd/C catalyst from a feedstream of MIBK (organic solvent)/water mixture during a cyclic operation of filtering and cleaning. A preliminary PdID is shown on attachment 4.

After a filter is loaded the catalyst has to be washed with water, dried with nitrogen and discharged either to be recycled (after slurrization) or discarded.

When one filter is cleaned the other one has to be in operation to continue the process. Prefiltration and starting up the back-up filter has to be done during operation of the other one. Therefore a separate prefiltration line has to be used, fed with pump P-2446. P-2445 is nonnally used for feeding to the filters. If pump P-2445 fails, pump P-2446 can be used as spare feed pump but then prefiltration is not possible anymore.

P-2445 will only feed the filter that is in operation and P-2446 will normally just prefiltrate (with catalyst and not with filter aid) The other filter is at that moment not used for filtration.

The filters shall be provided with heat tracing (60 oC, + 5 oC) to prevent that the temperature of the process fluid drops below 55 OC.

5531!001.CAB Rev. C

Engineered by : FLUOR DANIEL B.V. - HAARLEH


GSPEC002


Equipm. No.

Doc. No. S -2441 A/B

HSC 1061343 - A4

EQUIPMENT SPEClFlCATlON CATALYST F ILTER

I FDBV CONTR. : 5 5 3 1 - 0 5

CLIENT CONTR. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 RQ

In the common discharge filtrate line of the catalyst filters, a sample point is necessary to check if the filters are operating correctly with regard to filter efficiency and performance.

.-

The vent line on top of the filters shall be of sufficient size to relieve the gas during filling of filters. The vent line will be connected to a vent System that normally operates between 0 and 0.2 barg.

I Filters to be designed such that given operation time cycle is met.

-

4.2 Feed and product stream conditions

Ref. Nr. STREAM

(continued)

COMPOSITION

P.O. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4

Methanol Toluene MIBK Aspar tarne 2% Pd/c NaoH Water Others

CASE A CASE B 18 ' 18 19 20 2 5

AVERAGE FEED WASTE RECYCLE FILTRATE DESIGN FEED CATALYST CATALYST

24 hr bair 4.4 hrB.4 hr svsiy 8.4 hr niay 6.4 hr 4.4 hrB.4 hr W) W Om W)

to be nsmd =l.i*metage

I TOTAL 1.1*4238.0 6796.4 6760.6

Dens . (kg/m3) 850.0 850.0 850.0 Visc . (cP) 0.8 0.8 0.8 Temp. (OC) 63 6 3 30 3 0 63

I I Notes :

MIBK = Methylisobutylketone For final Procesa Calculationa, aee HSC drawing number 1076527-A4

After slurrization the concentration of recycle catalyst must be higher than 5 Wt %. Seller shall specify the exact amount of water that is required to obtain this concentration.

- 5531!001.CAB Rev. C

I Sheet No. 6 cont'd on sheet No. Engineered by : FLUOR DANIEL B .V. - HAARLEH


QSPECO

-

Equiprn. No.

Doc. No. S - 2 4 4 1 A/B

HSC 1061343 - A+

FüJOR DIlllEL 9 EQUIPMENT SPEClFlCAllON CATALYST F 1 LTER

(continued)

FDBV CONTR. : 5 5 3 1 - 0 5

CUENT CONTR. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 RQ

P.O. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4

4.3 Catalvst filtration data

Average feed = 4.99 m3/h Average design feed = 1.1 * 4.99 m3/h

= 5.49 m3/h

Total time per cycle: 6h 24 m = 6.4 h Total filtration time per cycle - 4h 24 m - 4.4 h Actual flow rate of feed = (total time per cycle/total filtration time per cycle) * average design feed = 6.4/4.4 * 5.49 = 7.99 m3/h

Filter surface: 7 m2 (per filter)

Flow rate per Square meter - 7.99 m3/h/7 m2 = 1.141 m3/h/m2

Actual catalyst flow rate - 19.6 kg/h Amount of catalyst per batch = 4.4 * 19.6 - 186.2 kg Cake density = 0.6 kg/l Volume of catalyst = 86.2/0.6 - 1143.7 1/B Cake thickness - 143.7 dm3/700 dm2 - k20.5 mm For final Process Calculations, see HSC drawing number 1076527-A4

4.4 Design reauirements:

- Seller to design optimum size of filters versus operation cycle time. The feeding time shall not exceed the operation cycle time for one filter to avoid use of two filters at the Same time.

- Good filtration of catalyst in both org. and aq. layer. - Particle size of catalyst: 1 - 100 Pm. - Good washability of catalyst after filtration. - Slurry discharge and "dry" solid discharge.

4.5 Utilitv data

Utilities as shown on attachment 2 can be made available. Instrument air is free from oil and dust.

4.6 Site data

For site data, See attachment 1.

5.0 MECHANICAL DESIGN REQUIREMENTS

Only equipment, materials, components, constructions etc., which have been proven during at least two years of successful operation in similar process conditions are acceptable.

5531!001.CAB Rev. C



GSPEC002


Equipm. No.

Doc. No. S - 2 4 4 1 A / B

HSC 1061343-A4

EQUIPMENT SPEClFlCATlON CATALYST F ILTER

(continued)

FDBV CONTR. : 5531 -05

CLIENT CONiR. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO. : 553105-4-0704

5.1 Mechanical data and materials of construction

FILTER

Fluid name Feed stream with catalys t

Design pressure barg 12/F. V. Design temperature OC 100 Material of construction 304L " Filter plates material 316L Corrosion allowance 0

') All material in contact with product: min. 304L or equal (including the cake discharge valves) - no copper or its alloys can be used - no asbestos is allowed - No sulphur containing materials may be used (hoses, gaskets

etc. )

All materials used for pressure containing equipment and piping must be acceptable by Stoomwezen.

5.2 Bearine. Sealing. Couvlin~s and V-belt svstem

Shall be in accordance with the specifications as listed in Para 9.0. V-belt shall be anti-static and provided with a speed indicator in order to detect V-belt failure. Bearing assembly shall not require any continuous lubrication/rinsing.

5.3 Surface Finish

Surface finish for the internal of the shell and internals shall be at least a 2B. Discontinuous welds are not permitted. All welds must be continuous at the inside and the outside of the equipment. Welds on the inside of the vessel shall be grinded, pickled and passivated. Welds on the outside of the vessel shall be passivated and coated. All internal welds to be ground smooth and polished to at least the Same quality as the rest of the surface.

5531 ! 001 .CAB Rev. C



GSPECOOi!


Equiprn. No.

Doc. No. S-2441 A/B

HSC 1063343 - A4

EQUIPMENT SPECIFICKiION CATALYST FILTER

(continued)

FDBV CONTR. : 5 5 3 1 - 0 5

CLlEM CONTR. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 RQ

P.O. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4

5 -4 Pipinp/Vessel

All equipment and piping shall be subject to Stoomwezen/CKD requirements .

Pressure vessel shall be designed and fabricated in accordance with Stoomwezen rules and referenced design specifications. Hazard category: 2 Stoomwezen classification: NONE DSM classification: M2 DSM inspection code: DM

P ip in^ ; The following piping classes do apply for process- and utility piping within package battery limits:

Service Class ins^ . code

Process fluid (P) SG BM Vent gas (VG) SG BM

Instrument air (AI) BC NI Nitrogen (NN) BC NI Demin water (WD) SE NI

5.4.1 Pipine. - System - materials

5.4.2 Class BC. flaneed cl. 150 RE

Pipe : Seamless ASTM A106-B, A520 (max. 0.23% C) Fittings : Butt weld ASTM A234-WPB, A106-B, A520 (max. 0.23% C) Caps : Butt weld ASTM A234, DIN 17155 - H11 Branch : Butt weld ASTM Al05 (normalized, max. 0.23% C) fittings Flanges : Raised face ASTMA105 (normalized, max. 0.23% C)

welding neck Gaskets : Flat ring 2.0 mm thick aramide/graphite type Klinger

C4400G Bolting : Stud bolts ASTM A193-Gr.B7, A194-Gr.2H

nuts Valves : Flanged raised face Gate : Body ASTM A216-WCB (max. 0.23% C) Globe Stem/trim SS type 410 (13% Cr) Check Ball : Body ASTM A216-WCB (max. 0.23% C) Full bore

stem/trim 316 stainless steel PTFE seats

Minimum wall thickness to be used: DN 15 thru DN 350 Schedule 40

5531!001.CAB Rev. C

Engineeredby: FLUOR DANIEL B.V. - HAARLEM


GSPEC002


Equipm. No.

Doc. No. S - 2 4 4 1 A/B

HSC 1061343 - A4

EQUIPMENT SPEClFlCATlON CA1 ALY ST F I L1 ER

(continued)

FDBV CONTFI. : 5531 -05

C U E M CONTFI. :

R.F.Q. NO. : 553105-4-0704 RP

P.O. NO. : 553105-4-0704

5.3.3 Class SE/SG. flaneed - cl. 150 RF

Pipe ASTM A312-TP 304L Fittings : Butt weld ASTM A403-WP 304L, A312-TP 304L Caps : Seamless ASTM A403-WP304L, A240-TP304L

Butt weld Branch : Seamless ASTM A403-WP 304L, A182-F 304L fittings Butt weld Flanges : Raised face ASTM A182-F 304L

welding neck Gaskets : Spiral wound 4.5 mm thick, SS type 316

PTFE filled, CS guide ring, SS innerring Bolting : Stud bolts ASTM A193-Gr.B8, class 2, A194-Gr.8

nuts Valves : Flanged raised face Gate : Body ASTM A351-CF8 Globe Stem/trim SS type 304 Check Ball Full bore with PTFE seats for ball valve

Minimum wall thickness to be used: DN 15 thru DN 25 Schedule 40s DN 40 thru DN 300 Schedule 10s

5.4.4 Nozzles with flanges according to DIN-standards may not be used. In cases (up to and including 600 nom. dia.) flanges as per ANS1 B16.5 shall be applied with a 150 LBS rating as a minimum. For sizes 650 nom. dia. and above, flanges shall be conform MSS SP44.

5.4.5 Surface roughness of all flanges shall be smooth (Ra 3.2 - 6.3 pm)

5.5 Plot limitations

Main skid dimensions shall be: Length: 5000 mm Width: 2200 mm Height: 4400 mm

5.6 Maintenance

The design of the Catalyst Filter Unit shall be such that maintenance can be done in an ergonomic and safe way. Components shall be installed such that they are easily accessible without the need to remove other major equipment. Where deemed necessary, the unit is to be equipped with protective members to avoid injuries during operation/maintenance.

5.7 Surface ~re~aration and ~aintinq

All equipment and other steel components shall be coated as follows:

5531 !001 .CA0 Rev. C

Engineered by : FLUOR DANIEL B.V. - HMRLEM

Client : H.S.C. - V.O.F. - GELEEN GSPECO(M


Equipm. No.

DOC. NO. S-2441 A/B

HSC 10- -

EQUIPMENT SPEClFlCAllON CATALYST F I L T E R

(continued)

FDBV CONTFi. : 5 5 3 1 - 0 5

CUENT CONTR. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 R a

P.O. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4

5.7.1 Carbon steel

component Specif ication color

skid, stairs, piping and DDS 1.2-423 RAL 7042 miscellaneous CS components railings DDS 1.2-424 RAL 1023 gratings, tearplates NEN 1275 hot dip galvanized electric motors DDS 1.2-424 RAL 7031

Surface preparation for all carbon steel components requiring coating: Blast cleaning to SA 2.5 of ISO 8501.1 (SIS 05 5900-1967). Rugosity Rugotest Nr. 3, N10 (equal to Ra 500 pin, 12 pm)

5.7.2 Hiph allov steel

No coating required.

5.7.3 Plastic components (terminal boxes etc.)

No coating required.

5.8 Weldinq

Production welding shall not commence before contractors approval of welding procedures.

Approval of welding can only be obtained when they are completed with the results of the required procedure qualification test records.

Manufacturer shall submit a fabrication drawing or sketch of each pressure vessel showing his reference number of the welding procedure selected for use on each weld.

Each individual Manufacturer shall prepare and qualify his own welding procedures .

5.9 Preservation

In fully assembled state, the unit can be stored, outdoors, for a period of max. 6 months without any Special provisions.

5.10 Cake dischar~e - valves

The cake discharge valves shall be stainless steel butterfly type in fire-safe execution (PTFE/steel seats). The valves shall be anti-static to the maximum extent.

5.11 Thermal relief valves

The filter vessels shall be provided with thermal relief valves to protect against overheating as a result of the electrical tracing.

5531!001.CAB Rev. C



GSPECOOI!

Sheet No. 1 1 cont'd on sheet No.

Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343 - A4

EQUIPMENT SPEClFlCATlON CATALYST F1 LTER

(continued)

FDBV CONTR. : 5 5 3 1 - 0 5

CLlENT CONTFI. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 Ra

P.O. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4

6.0 ELECTRICAL / CONTROL SYSTEM REOUIREMENTS

6.1 The instrumentation and control System design shall meet the requirements as stated in "the specifications as listed in Para 9.0.

6.2 The Vendor supplied instrumentation shall be connected to the DCS (Digital Control System). The DCS shall be used for safeguarding and control.

6.3 All KPV's (Remote operated on/off valves) mentioned on attachment 4 have a Open position limit switch (*H), and a closed position limit switch (* L). The KPV's shall be air failure close types.

6.4 The cake discharge valves shall be fully tight at the process condi- t ions .

6.5 The electrical design shall meet the requirements as stated in the specification as listed in Para 9.0.

6.6 The filter nest to be driven by one electro motor delivered by Seller (direct mounted motor or belt drive is acceptable).

6.7 Earthing connections shall be provided on each individual piece of equipment and steel structure.

6.8 Electrical and instrument wiring shall be segregated.

6.9 The electrical equipment and instrumentation shall be suitable for operation in an hazardous area classified as Zone 2, Gasgroup IIA, Temperature class Tl.

6.10 All remote operated on/off valves shallhave a 300 lbs rating as a minimum. Full bore valves shall be applied as indicated on attachment 4.

7 .o TECHNICAL DUTY GUARANTEE CONDITIONS

The Manufacturer shall guarantee in writing the following:

- The capacity of the filter unit. - The filtration as per specification. - The turndown ratio of the installation should be at least 40 A of

average f eed. - The satisfactory and safe operation of the Catalyst Filter Unit

including all components supplied by sub-vendors. - Proper operation of the cake discharge valves. - Chemical resistance of all gasket materials and lining (valves).

5 5 3 1 ! 0 0 1 .CA0 Rev. C


Client : H.S.C. - V.O.F. - GELEEN - GSPEC002

Sheet No. 1 2 cont'd on sheet No.

Equiprn. No.

Doc. No. S - 2 4 4 1 A/B

HSC 1061343 - A4

8.0 NOISE REQUIREMENTS

EQUIPMENT SPECIFICATION CATALYST F I LTER

(continued)

The sound pressure level of the installation as sum of the individual components shall be less than 80 dB(A) at a distance of 1 m according to the attached data/requisition sheet. Noise data shall be given in 8 octave bands and in total dB(A).

FDBV CONTFi. : 5 5 3 1 - 0 5

CUENT CONTFi. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 RQ

P.O. NO. : 553105 -4 -0704

9.0 APPLICABLE DOCUMENTS

Note: Only documents as listed below are applicable. Supplementary documents called for in these documents, but not listed below are considered not applicable.

9.1 Conflictine Reauirements

In case of conflict between documents related to this requisition, the following priority shall apply:

1. Statutory authority documents 2. Data/Requisition sheets 3. Other Fluor Daniel Documents 4. Design and Detailed Design Specifications 5. Codes and Standards

9.2 Fluor Daniel Documents

Number Title

SP 5531-50.50 General requirements for piping Systems in package units

SP 5531-60.12 Low Voltage Motors SP 5531-70.01 Instrumentation for package mechanical

equipment Doc.1061444-A4 AMR handling by Vendor Doc.1061423-A4 Procedure for assignment of inspection codes

and quotation information for package units DSM documents as listed per Fluor Daniel Specifications SP 5531-**.** etc.

9.3 Desi~n and Detailed Desien S~ecifications and Standards

9.3.1 Mechanical

Number Title

G 268 Non destructive testing

Welding specifications for un- alloyed, low alloyed and high-alloyed steel

Date

Dec. '90

Jan. '90

5531!001.CAB Rev. C



GSPEC002

Sh& No. 1 3 cont'd on sheet No.

Equipm. No.

Doc. No. S -2441 A/B

HSC 1061343 - A4

Date

Feb. '90

F W MNll l 9

Date

Mar. '89

Feb. '87

EQUIPMENT SPEClFlCAllON CATALYST FILTER

(continued)

FDBV CONTR. : 5531 -05 CUENT CONTR. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO. : 553105-4-0704

DS 3.6 Design and construction of gaskets Jun.'91 for flanged connections

DS 3.7 Marking of pressure vessels May. '91

DS 3.8 Thermal insulation Nov. '90

DS 3.11 Files for pressure vessels Mar. '91

A4 1007249 Amendment to DS 3.8 for insulation rev. A

DS 4.10 Welding specification for pipe Jan. '90

DS 5.2 Pressure vessels Feb. '89

DDS 5.2-213 Vessels manufactured acc. to a Mar. '91 standard design

DDS 5.2-265 Insulation supports for vertical Apr. '87 vessels

DDS 6.18-001 Agitators Mar. '90

G 250 Flanged connections/non-blow out Feb. '88 gaskets

9.3.2 P ~ D inq

Number Title Date

DS 4.50 Minimum design requirements for Jan. '91 p ip ing

9.3.3 S tructural

Number Title

DS 2.5 Steel structures-general

9.3.3 Electrical and instrumentation

Number Title

DS 7.24 Low voltage motors

G254 Earthing connections

5531!001.CAB Rev. C



GSPEC002


Equiprn. No.

C . 0

S-2441 A/B

HSC 1 0 6 13- -

M -IR 9 EQUIPMENT SPEClFlCAllON CATALYST FILTER

(continued)


CUENT CONTR. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO. : 553105-4-0704

9.3.4 Paint ing

Number Title Date

DDS 1.2-423 Epoxy based protective coating Jan. '88

DDS 1.2-424 Epoxy coating Jan. '88

9.4 Codes and Standards

- Rules for pressure vessels (published by 1 8 ~ consignment "dienst voor het stoomwezen")

- All applicable NEN norms Latest edition - All applicable IEC Standards Latest edition

5531!001.CAB Rev. C

Engineered by : FLUOR DAN1 EL B.V. - HAARLEM



Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343 - A4

ATTACHMENT I

FWOR M N C L 9

SITE DATA LIMBURG

Prevailine wind: South West Wind speed for the calculation of heat losses: 10 m/s

EQUIPMENT SPECIFICAllON CATALYST F I LTER

(continued)

Ambient air temperatures

FDBV CONTR. : 5 5 3 1 - 0 5

CUENT CONTR. :

R.F.Q. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4 RQ

P.O. NO. : 5 5 3 1 0 5 - 4 - 0 7 0 4

Maximum Minimum

Relative Humiditv

Design Summer 85% Design winter 100%

Environmental Conditions

The installation will be installed close to NH, and fertilizer plants. The ambient air can be polluted with NH„ SO2, CO2, nitrate, nitrous vapors and industrial dust .

,Y 5531!001.CAB Rev. C



Sheet No. 1 cont'd on aheet No.

Equipm. No.

Doc. No. S - 2 4 4 1 A/B

HSC 3061343 - A4 -

UTILITY

EQUIPMENT SPEClFlCAnON XXX XXX

(continued)

HP STEAM HP CONDENSATE

MP STEAM MP CONDENSATE

FDBVCOm. : 5531-05

CLIENT CONTR. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO. : 553105-4-0704-01

LP STEAM LP CONDENSATE

STEAM OUT CONDITION - DEMIN MATER ISBL (W)

HOT DEMIN MATER (WH)

HOT UATER (WH) HOT UATER RETURN (UHR)

IND WOLING MATER SUPPLY ( M I ) IND COOLING MATER RETURN (MIR)

WOLING MATER SüPPLY (Exist) (W) WOLING MATER RETURN (Exist) (MCR)

COOLING MATER SüPPLY (Neu) (W) COOLING MATER RETURN (Neu) (WR)

CHILLED MATER SUPPLY (Exist) (W) CHILLED MATER RETURN (Exist) (UXR)

CHILLED UATER SUPPLY (Neid) (W) CHILLED UATER RETURN (Neu) (WR)

BRINE SUPPLY (Exist) (W) BRINE RETURN (Exist) (UYR)

BRINE SUPPLY (Neu) (UZ) BRINE RETURN (Neu) (UZR)

RIVER UATER (UR) FIRE FIGHTING UATER (MF) POTABLE MATER ( W )

SAFETY SHOUER MATER (W)

INSTRUMENT A I R PLANT AIR BREATHIWG A I R W I TROGEN

( A I ) (AP) (AB) (NM)

UTILITY com PRESSURE (Berat

CTIOR

i) Des i gr 31/FV 31/FV

13/FV 13/FV

4/FV 4/FV

1.5/F\

7 24

7 * 7 * 7 * 7 * 7 * 7 * 7 * 7 * 7 *

7.5 * 7.5

9.5 9.5 *

7 7

8 8 * 16 16 6

7

8 8 * 8 *

4.5 *

I) Design E

100

102 102

60 60

50 50

50 50

0/50 0/50

0/50 0/50

-20/50 -20/50

- 20/50 -20/50

26 26

30(UG) 50(AG)

50

30 30 30 20

S

Min. 230 -

190 - 160 - - 4 4

- - - - 18 28

18 28

- -

- - - - - 4 4 10

- - - - 10

A t Battery Limit, 6) A t Users, 3)

A t Battery Limit, 6) A t Users, 3)

A t Desuperh-X-3304/44 A t User, 3) 6

Ref .DFA 331

Dounstrem P-3304A/B, 3) Dounstrem P-3346A/B, 3)

A t H-3301, 3)

A t MH Punp/M-3303, 7)

A t M I Punp, 7)

TEMPERATURE Average

230 120

200 120

175 120

110

- -

80

82 78

35 40

21 31

21 31

3 6

3 6

- 7 -4

-9 - 4

14 14

25

Amb. Amb. Amb.

-

At UC Punp Ex X-3301 1),5)

At MC Punp,Ex X-3340 1),3),5)

At UX Punp,Ex X-3302 4),5),7)

At W Punp,Ex X-3341 3),5),7)

A t UY Punp, 7)

( ' Max. 300 -

300 -

250 - -

30 50

- - -

40 ** 45 ** 2 5 - 35 ** 25 ** 35 **

- - -

-

- 26 26 14

- - - -

20

A t Mi! Punp, 3),5),7)

At G r d Level At Battery Limit, 2) At Battery Limit

At MS Punp

A t Bl.;Dw Point:-35 "C A t Bl.;Deu Point:Amb. A t BL.;Deu Point:Amb. At BL.:Deu Point:-40 "C

IREFERENCE: Basis o f Design, Exp.HSC Project 5000, Rev.0, 01-01-'91 1 Rev A, 11-04-191. I Note 1: Max.AlLouable Temperature Increase for individual pieces of Equipnent: 10 OC.

Max.AlLouable Pressure Drop: 1.0 bar. Note 2: F i re Fighting Mater Boosted up t o 16 bara i n case o f Emergency. Note 3: Operating Pressures and Temperatures are deviating from basis of design. Note 4: Design Pressure o f neu Equipnent t o be as W. Note 5: Design fo r FV i n relevant cases. Note 6: For Thermal Rating of Heat Exchangers take the fo l lcuing Saturation Conditims:

HP Steam: 23 bara and 220 "C, MP Steam: 10 bara and 180 "C, LP Steam: 3 bara and 134 "C.

Note 7: Max.AlLouable Pressure Drop: 0.7 bar. *) Set Pressure Safety Valve.

**) Use fo r Thermal Rating o f Heat Exchangers.

I Attachment: 2

5531!001 .CAB Rev.No.: D

Engin-red by : FLUOR DANIEL B.V. - HAARLEM

Client : HOLLAND SUEETNER COPIPANY V.O. F. - GELEEN

GSPECOM


Equiprn. No.

Doc. No. S-2441 A/B

HSC 1061343 - A4

PARTSUST (Attachment 4) Sheettof 3

P.O. 5531 -4-0704 5531 -05

Pcs 1 1

1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

! 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

I 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1

DESCRIPTION Pneum. vaive DN 50 H/L Pneum. vaive DN 50 H/L deleted Pneum. v a k DN 50 H/L Pneum. vahre DN 50 H/L Pneum. vaive DN 50 H/L Pneum. vaive DN 50 H/L Pneum. vahre DN 50 H/L Pneum. vaive DN 50 H/L Pneum. vaive DN 50 H Pneum. vaive DN 50 H Pneum. vahre DN 50 H Pneum. vaive DN 50 H Pneum. vahre DN 80 H/L Pneum. vaive DN 80 H/L Pneum. vahre DN 50 H/L Pneum. vahre DN 50 H/L Pneum. vaive DN 50 H/L Pneum. vahre DN 50 H/L Pneum. vahre DN 50 H/L Pneum. vahre DN50 H/L Pneum. vake DN 50 H/L Pneum. vake DN 50 H/L Pneum. vabe DN 50 Pneum. vaive DN 50 H/L Pneum. vahre DN 50 H/L Manual valve DN 50 Manual vahre DN 50 Manual vahre DN 50 Manualvabe DN50 Manualvaive DN50 deieted Pneum. vahre DN 50 H/L Pneum. vake DN 50 H/L Checkvabe Checkvabe Checkvahre Checkvalve Manual vahre DN 20 Manual vake DN 20 Manual vahre DN 25 deleted Sample vaive DN 1/2' Sample vahre DN 1/2" Manual vaive DN 40 Manual vahre DN 40 Pressure transmitter Pressure transmitter deleted Flow ghss DN50 Level transmitter, fianged type Level transmitter, fianged type Level transmitter, fianged type Level transmitter, fianged type Temp. control Temp. control OrificeDN50 OrificeDN50 OriiiceDN50 OrificeDN50

POS.1 1 2 3 4 5 6 7 8 9

10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49 50 51 52 53 54 55 56 57 58 59 60

TYPE 1 Balltype Balltype

Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balkype Balltype Balltype Balkype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype Balltype

Balltype Balltype Wafertype Wafertype Wafertype Wafertype

Balkype

Special Special Balltype Balltype With seal With seal

Kessler Liquifant Liquifant Liquifant Liquifant PT100 PT100

BORE

FB FB

FB FB FB FB FB

FB FB FB

FB FB

MATERIAL S.S. /PTFE S.S. PTFE

S.S. PTFE S.S. /PTFE S.S. PTFE S.S. PTFE S.S. /PTFE S.S. /PTFE S.S. PTFE S.S. PTFE S.S. PTFE S.S. /PTFE S.S. PTFE S.S.PTFE S.S. PTFE S.S. PTFE S.S. PTFE S.S. PTFE S.S. /PTFE S.S. PTFE S.S. PTFE S.S. PTFE S.S. /PTFE S.S. PTFE S.S. PTFE S.S. /PTFE S.S. PTFE S.S. PTFE S.S. PTFE S.S. PTFE

S.S. PTFE S.S. PTFE S.S. / PTFE S.S. / PTFE S.S. / PTFE S.S./PTFE S.S. 316 S.S. 316 S.S. 316

S.S. 316 S.S. 316 S.S. S.S. S.S. S.S.

S.S. / ghss S.S. S.S. S.S. S.S. S.S. S.S. S.S. S.S. S.S. S.S.

Worcester Worcester

Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester Worcester

Worcester Worcester Orton Orton Orton Orton

Rosemount 1 151 Rosemount 1 151

Endress&Hauser EndredHauser End redHauser Endress&Hauser

PARTSUST (Attachment 4) S heet3 of 3

P.O. 5531 -4-0704 5531 -05

1. H/L = limit switch not closed / not open 2. The ab- list is subject to Selkr's verification and does not reiiive Selkr from any responsbility

Vaives indicated as to be full bore are mandatory. Other valves may be reduced bore pmvided this does not jeapordize operation of the unit in any way.

Pcs 1 1 1 1 1 1 1 1

DESCRlPTlON Pneum. valve DN 50 H/L Pneum. valve DN 50 H/L Safeiyvaive DN40 Safeiyvaive DN40 OrificeDN40 PD transmitQer Speed ekment (prox.) Speed ekment i~rox.1

POS. 61 62 63 64 65 66 67 68

MATERIAL S.S. PTFE S.S. PTFE S.S. S.S. S.S. S.S.

MAKE Waroester Worcester Set press. 8 barg Set press. 8 barg

Rosemount 1 151 PD P&FmodelSJorNJ P & Fmodel SJ or NJ

TYPE Balitype Balitype Springtype Springtype

Wfih seals

BORE

EQUIPMENT SPEClFlCAllON FILTERS/STRAINERS

ITEM NO.: S-2441 A/B ITEM NAHE: CATALYST FILTER


CLlENT CONTR. :

R.F.Q. NO. : 553105-4-0704 RQ

-

OPERATIM6 DATA

(conünued) I P.O. NO. : 553105 4-0704

1 2 1

IE#UWIUL DESIeY DATA Desiqn code I~toomuezen Rules For Pressure Vessels Design ~ressure I 12/F.V. I barg Cer t i f i ca t ion 1 er code Design temerature 100 I .C

Corrosion a l lowance I I mn Hvdrostatic test wessure wr code

GEYERAL Description l ~ a t a l v s t F i l t e r Vessels I M f r . / ~ m e / ~ e r i a l No. 1 ~ tauag

I

T m o f f i l t e r centr. hor. 0pen area ratiol' I Cleaning method W-water Size basket perforationc II~R

Cover type dished head Diversion valve Davit DSM inspection code: DM Case supports, type L egs DSii c lass i f ication: U2 Stoamezen classif ication:

35 I (Drain I I I I I I 36 1 ~nstrunents SEE NOZZLE DATA SHEET

27 28 29 30 31 32

'-CI 39 40 41 42

Insulation Support type

44 45 46 47 48

M&

No.

HATEüIAi SPECIFIUTIQI

49 50 51 52

yes + tracing (by others) co l l a r

rmZUE Numkr

Req.'d

Casing Cover Connections

I I I DATA B I VEYKlR

54 55

Ssrviw Desuiption

I n l e t

Sandblast I Paint lonly carbonsteel perts DATA

Claan

Pressure drop I 0.4

') (basket Open area vs pipe size)

-

Nominal

Siw Flg. ~ Y W +F.cing

304L 304L 304L

mn m3 m2

No. of disks Nominal f i l t r a t i o n Size perforations or mesh

Method of removing baskets/elements 1 L i f t i n g out ent i re f i l t e r nest, removing disks

Derion

5.0

GSPEC062

5531!001.cab REV. No.: C

Projestion

Elcment Case supports Internat parts

16 1141 1 L/h/rn2

50 I

Sire. 00 X leneth Tot.elem.dirt ho ld im c a ~ . Surf ace

30%-

2.0 I bar



CS 316L

900 X

0.14 7

Elevation


REMARKS

SEE NOZZLE DATA SHEET

Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343-A4

EQUIPMENT SPECIFICATION

m s 1) NOZZLE ELEVATIONS ARE HEASURED FROH REFERENCE T.L. OR B.T.L. (EL.O.00). 2) NOZZLE PROJECTIONS ARE HEASURED FROH CENTERLINE OF MSSEL, OR NEAREST TANGENTLINE, T 0 CONTACT FACE OF FLANGE 3) FLANGES UP T 0 AND INCLUDING 24" (600 DY) CONFORH T 0 ANS1 816.5.

4) FLANGE BOLTHOLES T 0 STRADDLE VESSEL CENTERLINES. 5 ) ALL DIHENSIONS ARE GIVEN I N HILLIHETRES UNLESS OTHERUISE NOTED.

FDBV C O N l R . : 5531 - 0 5

- PRESSURE VESSELS

ITEH NO.: S-2441 A/B ITEH NAME: CATALYST FILTER

(continued)

1

C U E M C O N l R . :

R.F.Q. NO. : 553105-4-0704 RP

P.O. NO. : 553105-4-0704

GSPEC042

5531!001.cab REV. No.: C

Eng ineered by : FLUOR DANIEL B.V. - HAARLEH

Cl ient : H.S.C. - V.O.F. - GELEEN


Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343-A4

I (continued) I P.O. NO. : 553105-4-0704 I

EQUIPMENT SPEClFlCATiON MIXERS

ITEM NO.: S-2441 A/B ITEM NAME: CATALYST FILTER

h b e r required ( 2 1 ~ y p e top i


CUENT CONTR. :

R.F.Q. NO. : 553105-4-0704 RQ

i

OPERkTIYG MTA

:Lass of agitation lsuspend solids

1

MTERIMS

Invel l e r 1 ! ~ lands 1316~ Fhaf t 1316~ I ~ i x i n s vessel 1304L I

5531!001.cab REV. No.: C

Engineered by : FLUOR DANIEL B .V. - HMRLEM


GSPEC079

Sheet No. 3 cont'd on sheei No.

Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343-Ab

~JJX of Eauiment Catalyst f i l t e r mit NAIN MTA Iescri pt ion PRESSURE LEAF FILTER HORIZONTAL S d 300 rm Com?onwits MSSEL FILTERNEST DRIVE Pouer 5.5 kU ilajor Dimensions SEE WTLINE Pressure barg E a J I r n T LOUTIQl

EQUIPMENT SPEClFlCATiON NOISE LIMITS AND DATA ITEM NO. : S-2441 A/B

ITEM NAME: CATALYST FILTER (continueä)

YOISE DATA JNSI LENCED Mhtogw; .nb .ddawbut+Dknna

C-t Hz 1 6 3 1 1 2 5 1 2 5 0 1 5 0 0 1 1K I 2K I 4K I8K I &(A l E-motors SE-2441 A/B LP I I I I I I I I I


CUENT CONTR. :

R.F.Q. NO. : 553105-4-0704 RQ

P.O. NO.

F i l ters S-2441 A/B I I I I I I I I

S i lencing measures

5531 !001 .CA0 REV. No.: C



GSPECWG


Equipm. No.

Doc. No. S-2441 A/B

HSC 1061343-A4

EXTERNAL FORCES AND MOMENTS ON NOZZLES tcontlnuedl Y DNLY R P P L I L R ß L E T0 M i l C l ! ~ LIMIT LONNELTIONS -

E W I M N T SPECIFICAT ION

13.2.4 Nozz l es t o Fwmed Heads

FüEiV CONTR I 5531 -05 CLIENT CONTRi R F. 0. NO. I 5531 05-4-OiTOY-RO P. 0. NO. I 5531 07 -e/- O i D Y -01

I Resultant bendlng moment Mb = ß . 164 . D ' Nm

I Torslonal moment M t = B . I50 . D Nm

I Resul tant shear force Fr = ß . 2500 . D N

I Ax i a l tens i on o r compress ion force Fa = ß . 2000 . D N

3.2.5 The above ment i oned l oad i ng sha l l be cons i dered as bei ng caused by 67 % t h e n a l - and 33 % dead weight load.

3.2- 6 The bas i C stress intens i t y l i m i t s sha l l be as per OS 5500 APPEND l X A.

I 3.3 ADDITIONAL REINFORCEMENT

3.3. 1 Whenever s tresses based on paragraph 3.2 exceed the a l l owab l es, vendor shall apply addit lonal relnforclng.

3.3. 2 Purchaser sha l l subml t to vendor actua l n o u l e l oad l ngs fran connected P l p ing when these loadings exceed those set f o r t h i n paragraphs3.2.3and 3.2.9.

I I I FDBV CONTR. I 553 1 -05 1

1 3.0 EXTERNAL FORCES AND MOMENTS ON NOZZLES

--D.

I 3.1.1 The cr i ter ia specified shall apply tonozzles ON 50 (NPS 2) and larger for colums, druns and shel l and tube heat exchangers constructed of steel or a l loy steel.

3.1.2 Nozz l es sha l l be des i gned t o W i thstand forces and r fmient~ from the UierM l expans i on and dead we i ght o f p i p i ng. P i p i ng reac t ions W i l l be computed i n confwmance with D1101, and w i l l be within the limiting cr i ter ia set by this stondard,

EüülPYNT SPEClFlCATlON

3.1 . 3 The forces and m n t s conta i ned here i n are cons i dered m i n i nnm cr i ter i a i n order t o allow fo r an economical design o f the connecting piping.

- - -

CL I ENT CONT R I R.F. O. M. I 553105-4-CVPY-RO P. 0. Na 1 57>10C -4 -070'1 01

I 3.2 EXTERNAL FORCES AND MOMENTS ON NOZZLES

3.2.1 The spec i f ied nozz l es sha l l be capab l e o f W i thstand i ng forces and moments from externa l p i p i ng under normal operat i ng condi t ions and consi dered to be act ing a t the intersection o f nozzle and shel l i n corroded condition. The forces and maments sha l l not be cons i dered to act dur i ng steam-out cond i t i on.

I n the forrnulas 'D' i s the nmlna l d l m t e r I n Inches. The ß-value I n the formulas depends on the ra t i ng o f the nozzle flange and are as fol lows 8

Flange r a t i n g ß -va I ue o f ß -value o f

ANS l Heat-Exchangers Col unns and Drms

Class 150 0. 5 0. 4

C lass 300 0. 5 0. 5

C l ass 600 0. 8 0. 5

C lass 900 ' 1.0 0. 6

13.2.3 Nozz l es t o She l l s ( o r Channe l s l

I The fo l lowing forces and moments shal l be consldered t o act slmul toneously

I Longl t u d i n a l bend lng moment ML = ß . 130 . Nm 2

Circumferential bending moment h@ = ß . 100 . D Nm

~ Resultant bending m n t Mb = d m = B . 1 6 4 . D ' Nm

I Torsional m n t M t = ß . 150 . Nm

Tangential force i n plane o f flange Fg = ß . 1500 . D N

Resul tan t shear force F r =\JFL' + F@" = 8 . 2500 . D N

Ax i a l tens ion or compress ion force Fa = ß . 2000 . D N REV.:

Engineered byc FLUOR DAN 1 EL B. V. - HAARLEN

C l lent H. S. C. - V. 0. F. GELEEN

sheet No. 7 OT ~qulpih )(al 5- 2 ~ 1 ~ 0 ßIO -Na. I HSC 1061343 - A4