AXIUSTM Direct UV/UF

Siemens Water Technologies

Technical Support 00+1.978.934.9349 ext. 5000

User Manual

AXIUSTM Direct UV/UF Water Purification System

Catalogue No: S W 2 4 0 0 T F

Rev

: 071

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Siemens User Manual Water Technologies AXIUS TM Direct UV/UF Water Purification System Catalogue No. SW2400TF

Content

Table of Contents

1 Safety Information................................................................................................1 1.1 Symbols used in this manual .................................................................................1 1.2 Safety References..................................................................................................2 2 System Features ..................................................................................................3 2.1 Process Flow Chart................................................................................................4 2.2 Water Purification Process.....................................................................................5 3 Installation and Start Up......................................................................................6 3.1 Delivered parts .......................................................................................................6 3.2 Feed Water Requirements .....................................................................................7 3.3 Feed Pressure........................................................................................................7 3.4 Tube connections and sealing plugs......................................................................7 3.5 Installation - Cartridge Attachment.........................................................................8 3.6 Installation - Connections.......................................................................................9 3.7 Installation - Sterile Filter Attachment ..................................................................10 3.8 Start Up ................................................................................................................11 4 System Control...................................................................................................12 4.1 Display and Function keys ...................................................................................12 4.2 Start selection screen First start ......................................................................12 4.3 Start selection screen Flushing .......................................................................14 4.4 Start Selection Screen Operation....................................................................14 4.5 Start selection screen Main Menu ...................................................................15 4.6 Main menu Settings.........................................................................................15 4.7 Volume Operation ................................................................................................17 4.8 Calibration of volume supply ................................................................................19 4.9 Main menu Settings Timer UC-System ......................................................21 4.10 Main Menu Maintenance .................................................................................23 4.11 Main Menu Maintenance Disinfection.........................................................24 5 Warning Messages and Corrections................................................................27 6 Troubles and Corrections .................................................................................29 7 Maintenance and Servicing...............................................................................29 7.1 Interval..................................................................................................................29 7.2 Module Replacement ...........................................................................................30 7.3 Contrast Adjustment .............................................................................................31 7.4 UV-Bulp Replacement..........................................................................................32 7.5 Disinfection and Replacement of the Sterile Filter ...............................................33 7.6 Reverse-Osmosis Replacement ..........................................................................34 7.7 Disinfection of the System....................................................................................35 8 Technical Data....................................................................................................36 8.1 Feed Water Requirements ...................................................................................36 8.2 System Data.........................................................................................................36 9 Appendix ................................................................................................................ I 9.1 Flow Sheet .............................................................................................................. I 9.2 Circuit Diagram....................................................................................................... II 9.3 Consumables ........................................................................................................ III 9.4 Spare parts............................................................................................................IV 9.5 Disinfectant Safety Data Sheet ..............................................................................V


Safety Information Page 1 of 36

WARNING! Risk of serious or even fatal injury!

WARNING! Risk of electric shock!

IMPORTANT!

Note!

1 Safety Information 1.1 Symbols used in this manual Issues relevant to safety are characterized in this manual are denoted by the following symbols. These warnings must be observed in order to operate the equipment safely and avoid accidents, damage or injury.

This symbol alerts the user to potential sources of hazards to health, injuries or fatal injuries. Do not operate the equipment until you have completely understood the instructions and proceed accordingly.

This symbol alerts the user to the presence of uninsulated voltage that has the potential to cause serious or even fatal injuries. Do not operate the equipment until you have completely understood the instructions and proceed accordingly. All maintenance work must be performed by qualified service personnel.

This symbol alerts the user to potential sources of malfunctions or damage to the equipment if operated improperly.

This symbol alerts the user to advice on efficient und trouble-free operation.


Safety Information Page 2 of 36

IMPORTANT!

IMPORTANT!

1.2 Safety References This water purification system complies with state-of-the-art standards in terms of technology and safety regulations. The manufacturer has taken all precautions to ensure safe operation. The user must ensure that the system is installed in such a way that does not affect this mode of operation. The system is factory approved and fulfills our safety standards. This manual contains information and warnings that must be observed by the user in order to ensure safe system operation.

Please read the following safety precautions before start-up and comply with them during operation.

• The system must only to be operated by qualified staff. All users working with the system must read

this manual first. • The user is only allowed to carry out maintenance work as described in the manual. Only use

the designated spare parts for maintenance work. • Only authorized staff approved by the manufacturer is allowed to service the system. • Replace fuses according to manufacturer’s service information. Short circuiting or manipulation of

fuses and/or wires is not allowed. • The system must be connected to a fused and earthed power supply. • If leaks in the system become evident, the unit must be isolated immediately from the electrical

supply and the fault rectified. If required, inform your supplier’s customer service department.

Carry out the maintenance and inspections as recommended by the manufacturer in the recommended intervals to ensure user safety and to maintain the performance of the system.

The manufacturer does not take any responsibility for injuries to third parties caused by improper use of the system.


System Features Page 3 of 36

2 System Features This water purification system is designed for the production of Pure Water (ASTM Type 2) and Ultrapure Water (ASTM Type 1) out of drinking water from municipal supply. Pure Water will be produced by the Reverse-Osmosis (RO) with final desalination. This Pure Ware is stored in the tank. In the following polishing section Ultrapure Water is produced by the polishing module, UV-Oxidizing and sterile filter. It can be taken in small volumes, permanent output, or volume controlled output with the dispenser at the front side. If no water is supplied, it circulates inside the system to deliver Ultrapure Water in permanent best quality. Production rate of Pure Water into the tank is 10 lph with a conductivity under 2 µS/cm. Ultrapure Water can be drawn off with the dispenser up to 1.8 liter per minute with typical characteristics: Conductivity 0.055 µS/cm (resistivity 18.2 MΩ-cm), TOC value (total Organic carbon) under 1 ppb, bacteria less than 1 KbE/ml, Endotoxins less than 0.001 EU/ml, less then 1 particle per ml larger 0.1 µm and DNase, RNase and DNA removal. Currently recorded data and warning messages are shown on the system monitor. All components of the system are assembled in a designed plastic housing, which can be used either as bench device or wall mounted. The front door can easily be opened for module replacement. The system corresponds to the latest development and recent safety regulations. It can be installed and put into operation without the help of customer service. Front side Opened front side

Deionization Cartridge

Prefiltration Cartridge

System monitor and operation keys

Extricable Dispenser with valve

Folding front door

Polishing Cartridge


System Features Page 5 of 36

2.2 Water Purification Process Following the flow chart the main components are explained: When the system is switched ON, the inlet valve (V3.1) opens and the RO pump (P3.1) starts. The inlet valve controls the water supply into the system. It closes and the pump stops, when the system is switched off or when the permeate tank is completely filled. The pump (P3.1) raises the pressure for the Reverse-Osmosis process. The pressure is indicated with a pressure gauge (PI3.1) and can be adjusted with a pressure control valve (PC3.2). The prefiltration cartridge (F3.1) is filled with activated carbon. It absorbs organic matters like free chlorine, insecticides, pesticides, and herbicides out of the water and removes particles larger than 5 microns. The RO module (F3.2) removes over 98% of the salt content and nearly all bacteria, viruses, heavy metal complexes, as well as organic molecules with a molecular weight higher than 300 Daltons from the water. The water including these components is called concentrate; the cleaned water is called permeate. The concentrate will partially be drained to the waste water disposal and partially flows back to the RO pump. The conductivity of the Permeate is monitored with a sensor (QIA Q1) and will be displayed on the system monitor with Q1. If the conductivity exceeds the adjusted set point, a warning message will be displayed, the RO valve (V3.3) will be closed and the Permeate will be drained. The deionization cartridge (F3.3) is filled with mixed-bed resin, which reduces still remaining salt contents of the Permeate. The conductivity of the deionized water is monitored with a sensor (QIA Q2) and will be displayed on the system monitor with Q2. If the conductivity exceeds the adjusted set point, a warning message will be displayed. Deionized Permeate (Pure Water ASTM Type 2) will be stored in the tank (T5.1) with submersible UV lamp (UV5.1). The UV lamp protects the Pure Water against germs formation by direct UV radiation. The production of Permeat into the tank will be regulated by level measurement (PT5.1).

If the tank is completely filled (100%), the production stops. If the level falls below 80%, the production restarts and the tank will be filled. If the level falls below 5%, the circulating pump (P4.1) stops to prevent it from running dry. The flow sensor (FT4.1) monitors the output rate of the dispenser in case of operation with volume controlled output. The circulation pump (P4.1) feeds the water into circulation and to the Dispenser (V4.3). Inside the UV-Oxidator (UV4.1) free hydroxyl radicals (OH-) are produced. These radicals oxidize remaining organic materials in the water. The Polisher cartridge (F4.2) is filled with high grade activated carbon and mixed bed resins in semiconductor quality. The activated carbon removes last particles and the oxidized byproducts. The resin extracts last remaining salt contents. After replacement the cartridge can be rinsed with the flushing program to wash out impurities. Then the solenoid valve (V4.6) opens. Note: If the dispenser is placed into the holder, this valve will be opened for a short moment in order to depressurize the system. The Ultra-filtration (UF) module (F4.4) removes smallest particles like endotoxins, pyrogens, viruses, RNase, DNase and DNA from the water. This module will be flushed automatically every 12 hours to wash out impurities. Then the solenoid valve (V4.5) opens. The conductivity of the Ultrapure Water is monitored with a sensor (QIA Q3) and will be displayed on the system monitor with Q3. If the conductivity exceeds the adjusted limit, a warning message will be displayed. The temperature is monitored with a sensor (TA4.1) and will be displayed on the system monitor with temp. If the temperature exceeds the adjusted set point, a warning message will be displayed. The sterile filter (F4.3) protects the system against germ formations by filtration of materials over 0.1 microns. The product water will be supplied with the dispenser (V4.3). For economical use the UV Oxidizer, UV lamp and circulation pump can be operated in interval mode with 2 separate intervals or day/ night operation.


Installation and Start Up Page 6 of 36

3 Installation and Start Up 3.1 Delivered parts

1 x AXIUS 1x 30 l Tank (Art-No: 3315-01-SWT)

2 x Elbow union ¼“ (Art-No: 04861-2)

4 x Elbow union 5/16“ (Art-No: 02688)

1 x Prefiltration cartridge (Art-No: LP2150) 1 x DI cartridge (Art-No: LP2160)

1 x Polisher cartridge (Art-No: LP2171)

1 x Feed water tube, 5/16“, green (Art-No: 08635-6) with ¾“ union nut

1 x Concentrate tube, ¼“, black (Art-No: 02577-6)

1 x Flushing tube, ¼“, nature (Art-No: 02577-2)

1 x Permeate tube, 5/16 “,blue (Art. No. 08635-1)

2 x Circulation tube, 5/16“, white (Art-No: 08635-4)

1 x Power cable (Art-No: 70033, CH: 80703,

UK: 80704, USA: 80705)

1 x Sterile filter (Art. No. 2052)

1 x Tap adapter ¾“ ½“ (Art-No: 06843)

1 x pressure reducer (Art. No: 02764)

with pressure gauge (Art. No.: 08664)

With installation tools included



Note!

3.2 Feed Water Requirements The system can directly be connected to tap feed water from municipal supplies. Before connecting the feed water to the system, check whether it meets the following specifications:

Feed pressure bar 0.01 … 5

Conductivity µS/cm < 1000

Silt Density Index SDI < 3

Free chlorine mg/l < 0.5

Iron mg/l < 0.1

3.3 Feed Pressure In case of a feed pressure over 1 bar, the supplied pressure reducer (PC3.2) has to be installed to reduce the inlet pressure. Attention: Install pressure reducer in accordance to feed water inlet. The inlet pressure needs to be adjusted to 1.5-2 bar. The pressure is displayed on the pressure gauge (PI3.2). For pressure regulation pull up the adjusting screw. 3.4 Tube connections and sealing plugs The device is sealed with plugs to prevent leaks during delivery. Before connecting the system to the water supply/waste water disposal, remove the plugs from the water connection points on the rear side of the device by lightly depressing the fastening ring. Hose connectors

Tubes and sealing plugs can be removed by depressing the fastening ring as shown.

Fastening ring

2. Pull out the plug

1. Depress the fastening ring

Adjusting screw

Pressure gauge Pressure reducer (V3.3)



Pref

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F4.

2

3.5 Installation - Cartridge Attachment Front door opened

• Open the front door • Plug each cartridge on its couplers,

Slightly press on and then press down the cartridge until a snap in can be heard

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3.3



Attention!

3.6 Installation - Connections

• Plug the tubes in until stop position • Cables have be locked with the union nut • Concentrate, flushing and overflow tube must be led with a downward

gradient toward the waste water disposal. Any reduction of the diameter, loops, siphons or breaks in the line must be avoided. A minimum safety distance of 2 cm must be between tube end and waste water disposal (minimum distance of double inner tube diameter).

Power Supply Feed water inlet (green tube)

Circulation pump Power supply

Device connections

Tank connections

Level sensor cable (grey cable)

Circulation pump power supply (black cable)

Flushing outlet to drain (white tube)

Level sensor (grey cable)

Concentrate outlet to drain (black tube)

Permeate outlet to the tank (blue tube)

Circulation from the pump

(white tube)

Circulation to the pump (white tube)



Attention!

3.7 Installation - Sterile Filter Attachment • Plug the couplers in the sterile filter, until a “CLICK” for the snap in can be heard NOTE: The flow direction arrow on the sterile filter must comply with the arrow on the housing • Attach the filter with the fastener

Take care on the flow direction arrow

Front door – rear side

Coupler

Deaeration screw

Coupler

Flow direction arrow



Note!

Note!

3.8 Start Up

Before starting the system it is highly recommended to study the chapter “System Control” keenly.

1. Turn on water supply

2. Plug in the power supply cable

3. Start the system with the ON function key, the start selection screen appears

4. Select “settings” and confirm with ENTER

5. Enter individual parameters within the main menu settings

6. Leave the settings by pressing the menu function key, until the start selection screen appears

7. Select “first start” and confirm with ENTER After the first start program the system automatically turns into the production mode Note: Q3 value will be displayed only during active circulation, if the tank level is over 8%

8. Wait for a minimum tank filling of approx. 20%, displayed as a column right side of the monitor

9. If the Q3 value is not displayed, start the circulation pump (P4.1): - Start “main menu” by pressing the menu function key - Select “settings” and confirm with ENTER - Select “circ.pump P4.1” and confirm with ENTER - Switch ON the pump with the arrow key and confirm with ENTER - Press the menu function key until the start selection screen appears - Select “operation” and confirm with ENTER to display production parameters again

10. Check for impermeability on all connections

11. System is ready to supply the analyser with product water

After installation, after module replacement, and after a weekend the flushing program within the start selection screen should be selected for a short flushing.

If the conductivity does not reach Ultra Pure Water quality after installation or module replacement, the resin in the modules has to swell for some time to achieve the full capacity.


System Control Page 12 of 36

4 System Control

4.1 Display and Function keys

Display of device type, Serial Number and control version Function keys ON : System Start and Error reset

: Curser movement or number input ENTER: Confirmation

: Curser movement or number input Menu : Menu start or superior menu OFF : Switch off key (Attention: the system is still power connected)

4.2 Start selection screen First start

First Start Confirmation starts a program to water the system and to start first production after the installation.

Q1 and Q2 without measurement, tank is empty

Q1 measurement starts

Q2 measurement starts



4.2 Start selection screen First start

The tank will completely be filled

The modules will be deaerated

Press ENTER to continue

- Open the front door of the system. - For the deaeration hold a cup under the sterile filter - Open slightly the sterile filter ventilation screw - Wait until pure water flows out of the filter - Tighten the screw again and press ENTER

- Plug the dispenser out of the holder - Open the dispenser over a cup, until pure water flows out - Plug the dispenser in the holder again and press ENTER

The system is ready now to use Ultra Pure Water: The tank is completely filled, Q1 and Q2 measurement have been stopped. If the tank level falls below the middle level of 80%, the Reverse-Osmosis production and El-Ion® deionization will start again and the tank will be filled up to the maximum level of 100%.



4.3 Start selection screen Flushing

Flush Confirmation starts the flushing program to wash contaminations out of the Polisher module (MF-III-D module). This program should be used after module replacement.

Flushing Time Choose a flushing time with the arrow keys (e.g. 60 seconds) and confirm with ENTER.

Flushing Process Display of the remaining flushing time. After the flushing program the operational display will be indicated or can be chosen by pressing Menu

4.4 Start Selection Screen Operation

Operation Confirmation starts the system operation

Operation Display Q1: Permeate conductivity [µS/cm] Q2: DI-Water conductivity / resistivity [µS/cm / MΩ-cm] Q3: Ultra Pure Water conductivity / resistivity [µS/cm / MΩ-cm] TOC: Total Organic Carbon [ppb] 50: tank level [%] Note: Q1 and Q2 are displayed only in case of tank filling. Parameter of each line can be chosen in the main menu settings

Display after complete tank filling After the complete tank filling first conductivity control Q2 stops measurement. Product water can still be drawn off.



4.4 Start Selection Screen Operation

Then conductivity control Q1 stops measurement. Product water can still be drawn off.

4.5 Start selection screen Main Menu

Main Menu Confirmation starts the main menu

Main Menu Items • Settings: System configuration and interval settings • Maintenance: Disinfection, Ultra-Filtration flushing, operation counter • Service: Technical service configuration

4.6 Main menu Settings

Items • Individual customer Parameter • Temperature compensation • Limit values • Interval mode • External UV-lamp switch • Volume operation switch • Data transmission

Language • German • English

Date Input of the date: month / day / year (MM/DD/YY)




Time Input of the time: hours : minutes (hh:mm)

µS/cm MΩ-cm Display Selection of the quality unit, conductivity or resistivity • conductivity unit: µS/cm • resistivity unit: MΩ-cm

Temperature compensation Compensation of temperature variations and display of the compensated temperature for 25°C • automatic compensation • compensation off

Quality Q1, Q2, Q3 Conductivity limit for an alarm message on the screen

Quality Q1, Q2, Q3 Critical Value Input of the conductivity limit. If the alarm limit is exceeded, a warning message will be displayed on the system monitor.

Temperature • Limit of the temperature with alarm message • Limit of the temperature with product water drainage

(flushing valve will be opened and product water will be drained)

Temperature Limit Alarm Input of the temperature limit for an alarm message. If this limit is exceeded, a warning message will be displayed on the system monitor.

Main display Parameter selection for each monitor line to be displayed during operation




Row 1 … 3 Q1: Permeate quality Q2: Deionized Permeate quality Q3: Ultra Pure Water quality TOC: Total organic carbon concentration of the Ultra Pure Water Temp: Temperature Inactive

Data Port Selection of the data output signal • Signal for PC connection • Signal for printer connection

Data Port Printer Period of the data output for the printer

Data Port Printer Interval Input of the period in minutes

Energy-Saving-Mode (Ex. Ultra-Clear System) The circulation pump, UV-Oxidizer and submersible UV lamp can be operated in interval with: • 2 separate periods • Each period with permanent day operation (without night operation) • Each period with individual day and night operation • For day and night operation pauses can be chosen to stop the pump

and UV-Oxidizer

4.7 Volume Operation Note: With the volume operation program a specified volume of product water can be supplied with the dispenser.

Activation of the volume operation Volume operation has to be active or has to be activated within the main menu settings. • Select the volume operation item and confirm with ENTER



4.7 Volume Operation

• Select ON and confirm with ENTER

Now the volume operation is activated

Start of the volume operation During normal production the bottom line changes between the display of “Operation” and “Volume Operation press ENTER” • Start the Volume Operation with ENTER

The system will be prepared for volume operation and a short fizzing can be heard.

Selection item within the Volume Operation display • With the required volume can be changed • Start of volume supply: 1. Remove the dispenser from the holding 2. Open the dispenser for permanent supply (dispenser button in upright position) 3. Drain last water out of the dispenser tube 4. Press the ENTER 5. Volume supply starts • Press Menu to leave the volume operation item

Volume selection With the arrow keys the volume supply can be changed. • Choose the volume to be supplied and confirm with ENTER

Display during volume supply During the supply of water the remaining volume will be display in the bottom line. After the supply of water the volume operation can be repeated or stopped.



4.7 Volume Operation

Repeated volume operation • Start the next supply with ENTER

End of volume operation • Close the Dispenser button and hang it back into the holder

4.8 Calibration of volume supply Note: The system is factory calibrated for the supply of defined volumes. If the output volume is different to the adjusted volume, you have to recalibrate the system. For the calibration water has to be filled into a cup and this exact volume of water must be recorded by the system. A measuring cup of minimum 5 Liter is recommended.

Calibration of the volume operation The calibration has to be done within the service menu. • Select the menu item „flow sensor calibration and confirm with ENTER

The system will be prepared for volume operation and a short fizzing can be heard.

Start of calibration: 1. Pull out the Dispenser from the holder 2. Open the dispenser for permanent supply (dispenser button in upright position) 3. Drain last water out of the dispenser tube 4. Hold the dispenser over the measuring cup 5. Press ENTER, water flows into the cup 6. Fill the cup nearly up to the maximum volume with a reserve of approx. 100 ml (Note: After finishing the calibration process a rest of water will flow out of the dispenser)



4.8 Calibration of volume supply

End of calibration • Press ENTER to stop the water flow

The system records data now

Input of supplied water • Press ENTER

With the arrow keys the volume of supplied water has to be adjusted Press ENTER to finish the calibration

After the calibration the service menu will be displayed again



4.9 Main menu Settings Timer UC-System

Timer Ultra Clear System Example: 1st Interval: Working week Permanent operation from Monday to Friday, each day from 08:00 – 17:00 o’clock, stopped pump/UV 17:00 – 08:00 o’clock 2nd Interval: Weekend: Saturday and Sunday without pump/UV operation

1st Interval (Week day 1) Display of the week from Sunday to Saturday. Select the days for this interval with number “1” Example: 1st Interval, Working Week Selection of Monday until Friday

1st Interval - Start Time 1 Input of the interval start for the selected days Example: 1st Interval, Working Week Selection of 08:00 o’clock

1st Interval - Finish Time 1 Input of the interval end for the selected days Example: 1st Interval, Working Week Selection of 17:00 o’clock NOTE: The remaining time from 17:00 to 08:00 will automatically a separate interval period of night operation

1st Interval configuration • Configuration of the interval mode • Configuration of operation periods (days and nights), while the pump and/or UV-lamp are running • Configuration of pauses (days and nights), while the pump and/or UV-lamp are stopped

1st Interval configuration Mode Selection of the interval mode: • Permanent operation: Operation during the day time only, during the night the pump and/or UV-lamp are stopped • Interval operation with individual day and night settings Example: 1st Interval, Working Week Selection of permanent operation without pauses



4.9 Main menu Settings Timer UC-System

1st Interval Day Operation Input of a period in minutes to activate the pump and/or UV-lamp for a defined time during the days Note: Only valid in case of interval operation mode

1st Interval Day Pauses Input of a period in minutes to stop the pump and/or UV-lamp for a defined time during the days Note: Only valid in case of interval operation mode

1st Interval Night Operation Input of a period in minutes to activate the pump and/or UV-lamp for a defined time during the nights Note: Only valid in case of interval operation mode

1st Interval Night Pauses Input of a period in minutes to stop the pump and/or UV-lamp for a defined time during the nights Note: Only valid in case of interval operation mode

2nd Interval (Week day 2) Display of the week from Sunday to Saturday. Select the days for this interval with number “1” Example: 2nd Interval, Weekend Selection of Saturday and Sunday

2nd Interval - Start Time 2 Input of the interval start for the selected days Example: 2nd Interval, Weekend Selection of 00:00 o’clock

2nd Interval - Finish Time 2 Input of the interval end for the selected days Example: 2nd Interval, Weekend Selection of 00:00 o’clock

2nd Interval configuration Mode Selection of the interval mode: • Permanent operation: Operation during the day time only, during the night the pump and/or UV-lamp are stopped • Interval operation with individual day and night settings Example: 2nd Interval, Weekend Selection of Permanent Operation, day time is set to ZERO, pump/UV is stopped all time



4.10 Main Menu Maintenance

Maintenance Confirmation starts the maintenance menu

Maintenance Items • Disinfection: Step-by-step instruction for disinfection procedure • Intensive Ultra-filtration flushing • Op.hours UV: Display and reset of the UV lamp operating hours • Op.hours: Display of component operating hours • E/A status request: output of service values

Disinfection Start Confirmation starts the disinfection procedure, see next paragraph. Note: The disinfection program can be stopped with the MENU function key

UV-Lamp Operation Counter The operation hours of the UV-Lamp will be monitored. If the operation hours exceed the preset limit, a warning message will be displayed on the system monitor and the UV-Lamp must be replaced. After replacement of the lamp this operation counter has to be reset by pressing ENTER

UV operating reset For the reset the user password has to be entered: first 4 numbers of the Serial number

Reset confirmation The reset has to be confirmed by pressing ENTER



4.11 Main Menu Maintenance Disinfection

The system can be disinfected with this disinfection step-by-step procedure Needed auxiliaries are: 1) Disinfection tube to be inserted instead of the Polishing module 2) Disinfection syringe with special disinfectant solution 3) Cup with minimum 2 liter volume or drain for the dispenser flushing Select “disinfection” and confirm with ENTER Attention: The Safety precautions of the disinfectant Safety Data Sheet have to be observed! Note: The disinfection procedure can be stopped with the MENU function key before inserting the disinfectant solution.

Start the disinfection procedure confirming with ENTER

1. Open the dispenser

• Hold the dispenser into the cup resp. into the drain • Switch the dispenser opener to permanent outlet • Confirm with ENTER

2. Insert the disinfection tube instead of the left cartridge

• Unplug the left module (Polisher module) • Plug the module couplers onto the disinfection tube • Confirm with ENTER

3. Connect the disinfection syringe Remove the protection cap of the syringe and of the disinfection tube, screw the syringe onto the injection opening and confirm with ENTER

4. Inject the disinfectant and confirm with ENTER




5. Remove the disinfectant syringe and reinsert the dispenser

• Remove the syringe and close the inlet cap of the disinfection tube • Close and reinsert the dispenser • Confirm with ENTER

6. Start the disinfection with ENTER

7. Display of the circulation time and of the reaction time

8. Completed Disinfection

• Remove the dispenser • Open it for permanent outlet over the cap resp. the drain • Confirm with ENTER

9. Disinfectant draining

• Start the flushing with ENTER • Close and reinsert the dispenser after a short moment

10. Display of the flushing time During the flushing time the disinfectant will be rinsed out and the system will be cleaned with fresh water

11. Completed Flushing

• Remove the disinfection tube • Insert the left module (Polisher / MF-III-D module) • Confirm with ENTER




12. Final Washout • Remove the dispenser • Open it for permanent outlet over the cap resp. the drain

Attention: approx. 2 liters will be drained off • Confirm with ENTER

12. End of Disinfection Procedure

• Display of the remaining time • After the final washout the system turns into operation mode • Close and reinsert the dispenser • Check for impermeability on all connections • System is ready for production


Warning Messages and Corrections Page 27 of 36

5 Warning Messages and Corrections

Warning 1: Conductivity Q1 limit exceeded, Permeate will be drained

Check of limit Q1 settings Check of and correct feed water quality Check of Reverse-Osmosis function: If the RO operation pressure indicated by pressure gauge PI3.1 rises over the maximum, the Replace Reverse-Osmosis membrane has to be replaced: Inform the customer service Error reset with ON function key

Warning 2 Conductivity Q2 limit exceeded, tank filling will be stopped

Check of limit Q2 settings Check of El-Ion® function Inform customer service Error reset with ON function key

Warning 2 Conductivity Q3 limit exceeded

Check of limit Q3 settings Replace the MF-III-D module Error reset with ON function key

Warning 5 Maximum temperature limit exceeded, product water will be drained Check of the temperature limit Check of ambient and system temperature Install a cooling system water to drain Error reset with ON function key

Warning 7 Operation time of the UV-lamp exceeded, replace UV-lamp. After replacement the operation counter has to be reset inside the maintenance menu Error reset with ON function key

Warning 10 The tank is empty; Ultra Pure Water production will be stopped.

The circulation pump stops until the tank level rises over 10% again Error reset with ON function key

Warning 11 Connection fault of level measurement, system will be stopped

Check of level measurement connections Inform customer service Replace level measurement and recalibrate the system Error reset with ON function key


Warning Messages and Corrections Page 28 of 36

5 Warning Messages and Corrections

Warning 13 Operation time without service exceeded

Inform customer service

Warning 20 Conductivity measurement error, e.g. caused by air inside sensors, ect…

Deaerate the system Inform customer service


Troubles and Corrections Page 29 of 36

6 Troubles and Corrections

Trouble Reason Correction

Temperature too high • Feed water temperature • Ambient temperature • System temperature

by UV lamp or pump too high

Cooling Cooling Interval-Mode

Conductivity Q1 too high • Feed water quality • AMB Module exhausted

Check of pre-treatment Replacement of AMB module

Conductivity Q2 too high • Feed water quality • AMB and VMD Module exhausted

Check of pre-treatment Replacement of AMB and VMD

module

Conductivity Q3 too high • MF-III-D Module exhausted Replacement of MF-III-D Module

7 Maintenance and Servicing

7.1 Interval

Material Time of Operation Alarm Message Counter Reset

Sterile Filter replacement Every 6 months recommended, depending on germs formation

none no

Sterile Filter autoclaving max. 6 times none no

System disinfection Every 3 months recommended, depending on germs formation

none no

AMB module replacement Every 90 days recommended, depending on feed water pollution

Q1 Value exceeded Q2 Value exceeded

no

VMD module replacement Every 6-12 months recommended, depending on feed water pollution

Q1 Value exceeded Q2 Value exceeded

no

Polisher module replacement Every 6-12 months recommended Q3 Value exceeded no

UV-lamp replacement Every year recommended replace UV-lamp yes

Reverse-Osmosis membrane in case of blocking none no


Maintenance and Servicing Page 30 of 36

Note!

Pref

iltra

tion

cart

ridge

F3.

1

Polis

her c

artr

idge

F4.

2

7.2 Module Replacement Front door opened

• Stop the system with the OFF function key • Depressurize the system by opening dispenser for a moment and open the front door • Slightly press in, push up and pull off the old cartridge. Attention: Water spilling! • Plug the new cartridge on the couplers • Slightly press on and then press down the cartridge until a snap in can be heart • Start the system with the ON function key • Select the menu item Flush for a short flushing of the modules • After the flushing the system automatically jumps into normal operation • Deaerate the system with sterile filter and Dispenser:

Open sterile filter deaeration screw and Dispenser, until pure water flows out (The deaeration might be repeated form some times)

• Check for impermeability on all connections • Close the front door • System is ready for use

After module replacement the flushing program should be selected for a short flushing. If the conductivity does not reach Ultra Pure Water quality after installation or module replacement, the resin in the modules has to swell for some time to achieve the full capacity.

Dei

oniz

atio

n ca

rtrid

ge F

3.3



IMPORTANT!

7.3 Contrast Adjustment

Risk of damage to system! Avoid contact with resistors and other devices mounted on the circuit board.

• The contrast of the display must be adjusted during normal operation. • Take care not to touch the circuits. • Open the front panel. • Remove the lid of the system control box, which is mounted on the rear of the front panel. • Adjust the contrast by turning the regulating screw using a small screwdriver. • Reattach the lid. • Close the front panel. • System is ready for use.

Contrast screw



Note!

Warning! Danger by electric current!

Note!

7.4 UV-Bulp Replacement

Before beginning with the replacement, first ensure that all electrical connection cables are removed!

UV-lamp Opened front door UV-Oxidizer disassembled

• Stop the system with the OFF function key, disconnect power supply and turn off water supply • Depressurize the system by opening dispenser for a moment • Plug off the ballast cable and unscrew the ground cable • Plug off the hose connectors, Attention: some water will flow out! • Unscrew the holding clamps and the end caps of the oxidizer and remove the old UV-bulb • Carefully insert the new UV-bulb, pull through the ballast cable and close the end caps again

Avoid touching the glass portion of the UV bulb. It is recommended that lint free gloves be worn when handling the lamp. Hold the UV-bulb only at its ends.

• Attach the holding clamps, connect the ballast and ground cables, plug in the hose connectors • Connect the power supply, turn ON water supply and start the system with the ON function key • Select the flushing program to clean the UV-oxidizer • After the flushing the system automatically jumps into production mode • Deaerate the system with sterile filter and Dispenser:


• Check for impermeability on all connections • System is ready for production

After module replacement the flushing program should be selected for a short flushing.



Note!

7.5 Disinfection and Replacement of the Sterile Filter The replacement of the sterile filter is recommended every 6 months as a minimum ! The sterile filter (F4.3) protects the system against germination by filtering particles over a size of 0.1 microns. Depending on feed water quality, ambient conditions and utilization the sterile filter will be contaminated by accumulated germs.

Depending on microbiological requirements the filter needs to be disinfected or replaced.

For disinfection the sterile filter can be autoclaved up to 6 times for 30 minutes at 121 °C. After 6 times of autoclaving the sterile filter needs to be exchanged.

• Stop the system with the OFF function key • Depressurize the system by opening dispenser for a moment • For removing the sterile filter the detacher ring must be pressed in slightly • Disinfect or exchange the sterile filter and insert it again • Start the system with the ON function key • Select the menu item Flush for a short flushing of the modules • After the flushing the system automatically jumps into normal operation • Deaerate the system with sterile filter and Dispenser:


• Check for impermeability on all connections • System is ready for use

After module replacement the flushing program should be selected for a short flushing.

Front door – rear side

Coupler

Deaeration screw

Coupler

Flow direction arrow



Warning! Danger by electric current!

Note!

7.6 Reverse-Osmosis Replacement

Before beginning with the replacement, first ensure that all electrical connection cables are removed!

• Stop the system with the OFF function key, disconnect power supply and turn off water supply • Open the rear panel or front door of the system • Remove the tubes from the reverse-osmosis housing couplers • Connect the power supply, turn ON water supply and start the system with the ON function key • Select the menu item Flush for a short flushing of the modules • After the flushing the system automatically jumps into normal operation • Check for impermeability on all connections • Close the front door • System is ready for use

After module replacement the flushing program within the start selection screen should be selected for a short flushing.

Reverse-Osmosis module



7.7 Disinfection of the System

The disinfection of the system should be realized with SG disinfection syringes (Art.No. 2055). With these syringes a user-friendly disinfection is possible: 1) The syringes are filled with a suitable concentration of the disinfectant “OXIDES L” 2) Potential injuries or damages using the disinfectant are prevented 3) The disinfection procedure is easy with the programming-controlled step-by-step instruction For the disinfection a special disinfection tube needs to be connected instead of the left cartridge (polisher module). Then one syringe has to be fixed to the tube and the disinfectant only has to be injected. Finally the disinfectant has to be rinsed out. The disinfection procedure will be done by the step-by-step instruction: See chapter „Main Menu Maintenance Disinfection“


Technical Data Page 36 of 36

8 Technical Data 8.1 Feed Water Requirements The system can directly be connected to tap feed water from municipal supplies. Before connecting the feed water to the system, check whether it meets the following specifications:

Feed pressure bar 0.01 … 5

Conductivity µS/cm < 1000

Silt Density Index SDI < 3

Free chlorine mg/l < 0.5

Iron mg/l < 0.1

8.2 System Data

Ultrapure Water Performance lpm 1.8

Resistivity at 25°C MΩ cm 18.2

Conductivity at 25°C µS/cm 0.055

TOC ppb < 1

Bacteria cfu/ ml < 1

Particles > 0,1 µm per ml < 1

Endotoxins EU/ml < 0.001

DNase, RNase, DNA free

Temperature °C +5 … +35

RO operation pressure bar 6

Feed water union nut R ¾“

Tap adapter R ½“

Concentrate and flushing connector R ¼“

Power supply V / Hz 100…240 / 50…60

Height x Width (with tank)x Depth mm 530 x 560 x 320

Weight kg 44


Appendix III

9.3 Consumables

ID Description Article No.

F3.1 Prefiltration cartridge LP2150

F3.2.1 Reverse-Osmosis module 10 lph LP03303

F3.3 Deionization cartridge LP2160

UV5.1 Submersible UV bulb LS2596-01

UV4.1 Oxidizer UV replacement bulb 2068

F4.2 Polisher module LP2171

F4.3 Sterile filter 0.1 µm LP2052

F4.4 UF cartridge LP2158

OPTION CO² replacement cartridge LS3502

OPTION Sanitization kit 3/pk LP2055

OPTION Wall bracket for 30 l reservoir LS3317


Appendix IV

9.4 Spare parts

ID Description Article No.

P3.1 / P4.1 Reverse-osmosis pump / circulation pump 08367

V3.1 Solenoid Inlet valve 07902

PI3.1 Pressure gauge 08664

QIA Q1 Quality control Q1 07523

V3.3 RO Solenoid valve 07902


LS Level sensor 06812-10

V4.6 Flushing valve 00055

V4.5 Flushing valve 00055


TA4.1 Temperature sensor 06381

none Plug in connection for sterile filter 00378-1

V4.3 Dispenser 2104

Reed-Contact Reed contact 07749-2

none Dispenser tube 02194-7

V4.2 Check valve 06712

E1 System control 05697-00

none Switching Power supply 100-240 08258-2

none Switching Power supply PS-25-12 06281

Please give us always the serial number of your system when ordering consumables and spare parts.

EU Safety Data Sheet

Page: 1 of 3Trade Name: Oxydes LCreated: December 5, 2003 Modified: June 19, 2006

1. Material / Preparation Designation and Company NameProduct Specifications Trade Name: Oxydes L

Supplier Information Address:

Emergency Contact: State Advisory Board for Poisonous Symptoms and Embryonic toxicology – Senate Health Administration (Landesberatungsstelle für Vergiftungserscheinungen und Embryonaltoxikologie – Senatsverwaltung für Gesundheit) Spandauer Damm 130, D-14050 Berlin, GermanyTel: +49 (0)30 192 40 Fax: +49 (0)30 368 6799)

2. Composition / Component InformationIngredientsConcentration CAS-No. Symbol R-Sätze Substance

< 0.5 % 7647-14-5 -- -- Sodium hypochlorite in an aqueous solution, chlorine active

< 0.5 % 7722-84-1 -- -- Hydrogen peroxide < 0.5 % 1310-73-2 -- -- Ozone

3. Possible Hazards

Hazardous Symbols NoneR-Sätze: 31 Poisonous gases created upon contact with acids There is no danger to persons or the environment when used and handled correctly. Open flame is strictly forbidden in the vicinity of the liquid container.

4. First-Aid MeasuresGeneral instructions: Remove contaminated clothing. Remain calm. Ensure fresh air available. After inhalation: Remain calm. Get to fresh air. If symptoms persist, consult a medical professional. After skin contact: Immediately flush the effected area thoroughly with water. If any effects remain, consult a medical

professional.After eye contact: Keeping the eye lids open and separated, immediately flush the eye(s) thoroughly with running

water. Protect the unaffected eye. Remove contact lenses. Consult a medical eye specialist. After swallowing: Immediately flush the mouth thoroughly with water. When the mouth is free of contaminants, drink

as much water as possible. Consult a medical professional.

5. Fire-Fighting MeasuresAppropriate extinguishing agents

Isolate endangered areas downwind. Warn inhabitants. The material itself is non-flammable. Fight the surrounding fire with an appropriate extinguishing agent.

Special protective equipment for fighting the fire Helpers should protect themselves. Ensure sufficient ventilation. No additional measures are required.

6. Measures After Inadvertent ReleaseSteps to protect persons: Avoid contact with skin, eyes and clothing.

Thin the product with water and wash away. Environmental protection measures:

No special measures are required. Ensure that enclosures are well ventilated and have an ample fresh air supply.

Cleaning procedures: Thin thoroughly with water and wash away. Ensure sufficient ventilation.

SG Wasseraufbereitung und Regenerierstation GmbH Fahrenberg 8 D- 22885 Barsbüttel, Germany Tel.: +49 (0)40 / 670868-6 Fax.: +49 (0)40 / 670868-44


Page: 2 of 3Trade Name: Oxydes L

Created: December 5, 2003 Modified: June 19, 2006

7. Handling and Storage Instructions for safe handling: Open and handle the container with caution. Ensure sufficient ventilation when filling, emptying or

transferring. Avoid direct contact with eyes, skin or clothing. Requirements for storage areas and containers:

Ventilate storage areas well. No fire or open flame around or in the container due to hydrogen presence.

Storage instructions: Store in a cool and well ventilated area. Recommended storage temperature:

From 5° C To 25° C

8. Exposure Limitations and Personal Protective EquipmentAdditional instructions for the configuration of technical systems See chapter 7. No further measures are required. Components with threshold values that must be monitored within the working environment The product contains no components in relevant amounts that need monitoring within the working environment. General protective and hygienic measures Avoid direct contact with eyes, skin and clothing. General safety measures when dealing with chemicals are to be heeded. Personal protective gear Breathing protection: Not required when adequate ventilation is ensured. Hand protection: Use protective gloves. Glove material must be sufficiently impermeable and resistant for the

materials being used. Inspect before use to ensure impermeability. Ensure hands are sufficiently protected. Thoroughly rinse gloves before removing, and then store them in a well ventilated area.Fabric and leather gloves are absolutely not suitable.

Gloves made of the following materials are suitable (resistance time >/= 8 hours): Natural rubber or latex - NR (0.5 mm), (use unpowdered and anti-allergenic products) Polychloroprene - CR (0.5 mm), nitrile rubber / Nitrile latex - NBR (0.35 mm) Butyl rubber - Butyl (0.5 mm), fluorine rubber - FKM (0.4 mm) Polyvinyl chloride - PVC (0.5 mm)

Eye protection: Protective glasses / face protection recommended when transferring material. Body protection: Not required

9. Physical and Chemical PropertiesAppearance: Form: Liquid Color: Colorless Odor: OdorlessDensity at 20 °C 1.00-1.02 g/cm³Melting temperature at NA°CBoiling point / range: >100 °CFlash point: Not applicableSelf-immolation point: Not self-immolatingExplosion hazard: With fire (detonating gas) Dissolubility in water at 20 °C MixablepH-value at 20 °C 6.8-7.2

10. Stability and Reactivity Hazardous reactions: Interaction with acids produces heat Thermal decomposition: No decomposition when used as directed Hazardous decomposition by-products:

Hydrogen (detonating gas)

11. Toxicological DetailsAcute toxicity: Primary irritation on the skin No irritation

In the eye No caustic effects Sensitization No known sensitization effects

Additional toxicological information: According to the analysis of the EU General Categorization Guidelines for Preparations, the product presents the following dangers: Within the framework of the oral intake amounts for table salt, there is no toxicity. Avoid capturing the product.

12. Ecological Details Water pollution class: 1 (low water hazard)

May enter waste or receiving water undiluted or neutralized.


Page: 3 of 3Trade Name: Oxydes LCreated: December 5, 2003 Modified: June 19, 2006

13. Disposal Instructions Instructions for disposal Product: Dilute with plenty of water and wash away. Packaging: Contaminated packaging should be completely emptied. After being properly cleaned, it can be re-

used.EAK waste number: 07 06 99

14. Transportation Instructions Not a hazardous material according to transportation regulations

15. Regulations R-Sätze: 31 Poisonous gases produced upon contact with acids

S-Sätze: 1/2 Store locked and inaccessible to children 20 Do not eat or drink 26 If eye contact occurs, immediately flush with water and seek medical attention 37 Wear suitable gloves 45 In case of accident or nausea, seek immediate medical attention (if possible, show this data sheet)

16. Other Information Further details The information provided is based upon our current knowledge and is meant to describe the product’s safety requirements. It does not represent a guarantee of product characteristics and form no basis for a legal contractual relationship. Adherence to existing laws, regulations and guidelines is the sole responsibility of the user and/or handler of the product listed herein. Data sheet publication section Laboratory

Documents

AXIUSTM Direct UV/UF