Applied Chemistry, Creative SolutionsApplied Chemistry, Creative Solutions November 13, 2001 (Via certified or express mail) Kevin Turner-Environmental Scientist, OSC U. S. Environmental

S O LApplied Chemistry, Creative Solutions

November 13, 2001(Via certified or express mail)

Kevin Turner-Environmental Scientist, OSCU. S. Environmental Protection Agencyc/o Crab Orchard National Wildlife Refuge8588 Rt. 148Marion, IL 62959

Thomas MartinAssociate Regional Counsel77 West Jackson Boulevard (C-14J)Chicago, IL 60604-3590

Re: Sauget Sites Area I - May 31,2000 Unilateral Administrative Order (UAO)Sediment / Soils Removal Action

• # 6 - November 2001 Monthly Report

Dear Mr. Turner and Mr. Martin,

Enclosed is the November 2001 Monthly Report for the Sauget Sites Area I May 31, 2000Unilateral Administrative Order ("UAO") sediment removal Action. This submittal is infulfillment of the monthly reporting requirements of the UAO, Section V, and paragraph3.4. Reporting.

Sincerely,

D. M. LightManager, Remedial ProjectsSolutia Inc.

cc:Michael Ribordy - USEPA Region 5 Mike Henry - IDNRSauget File - Solutia Kevin de la Bruere - USF&GS. Bron - IEPA Mayor P. Sauget - Sauget, ILMayor D. Reed - Cahokia Jon Dikinas - Dikinas ConsultingVillage of Sauget - % P. H. Weis & Associates (Attn: Brian Nelson)Rich Bartelt - Arcadis

Sauget Sites Area I - Sauget, Illinois

May 31,2000 UAO - Dead Creek Sediment Removal Action

Monthly Report

Date of Report: November 13,2001Period Covered: October 1, 2001 - October 31, 2001Next Report Period: November 1, 2001 - November 30, 2001

Background

A Unilateral Administrative Order ("UAO") was issued to Solutia by the U. S. EPA onMay 31, 2000, requiring construction of an on-site containment cell, removal of affectedcreek bed sediments and soils and flood plain soils from specific sections of Dead Creek,and placement of the affected sediments and soils in the newly constructed on-site cell. ATime Critical Removal Action Work Plan ("TCRAWP") was initially submitted to theAgencies June 30, 2000 for review and approval. Agreements sufficient to proceed withissuance of a request for bids for the containment cell construction were reached inDecember, 2000. Bids were received in late January and evaluated in February 2001.

Fieldwork began on the sediment de-watering phase of the project in November 2000.Installation of the required facilities (piping, pumps, basins, etc.) to de-water thesediments while the containment cell is being constructed was completed and started upin February, 2001. Operation of these facilities will continue until all sediments areplaced into the containment cell.

Subject to the inclusion of all comments and agreed upon revisions, approval of thecontainment cell design by U. S. EPA was received March 5, 2001. A contract forconstruction of the containment cell was awarded March 8, 2001 to LMS EnvironmentalContracting, Inc. ("LMS"). Placement of fill for the Containment Cell berms began April23, 2001. A March 30, 2001 revised draft containment cell design was approved by theAgencies in a May 10, 2001 letter. Construction was completed on the Containment Cellon September 13,2001. A draft Containment Cell Certification Report was submitted forAgencies' review and approval upon construction completion. The Containment Cellwas approved on September 24, 2001 by USEPA and IEPA for receipt of sediment.Placement of sediments into the cell began September 26, 2001.

11-01-UAO

Agency Actions / Communications

• An Amendment to the UAO was received October 29,2001. The Amendmentmodified the project scope of the UAO - adding Creek Sector F sedimentsremoval and placement into the Containment Cell.

• Revision 01 Draft Groundwater Monitoring Plan - submitted to the AgenciesAugust 3, 2001 - remained under review.

• The Operations and Maintenance Report - submitted for Agencies' review andapproval August 28, 2001- remained under review. Portions of the Planapplicable to the placement of sediments have already been approved.

• An August 20, 2001 request for a change in the Post Removal ConfirmationSampling Protocol remained under review by the Agencies.

Work Performed during the reporting period

• Continued sediment dewatering activities and maintenance of dewatering pumps.• Completed sediment removal from Jerome Avenue to Cahokia Street (approx.

19,000 cy sediments removed and placed in the cell to date).• Completed relocating previously stockpiled sediments from Segment B into the

containment cell.• Sampled sediments being placed in the containment cell as required by the

approved Work Plan.• Began sediment removal from Segment B (working from Queeny Ave south).• Began installing temporary cover (poly, geotextile, and dense grade) in CS-B.• Performed startup testing of storm water storage and treatment system.• Processed approximately 500,000 gallons of storm water through the on-site

storm water treatment system.• Continued screening sediments for placement against containment cell slopes per

the Work Plan.

Data Submitted

The analytical results are enclosed from the initial sampling round (background) of thecontainment cell groundwater monitoring wells.

Work scheduled for next reporting period

• Complete sediment removal in CS-B. Complete installation of the temporarycover (poly and dense grade) in northern section of Segment B.

• Begin sediment removal from CS-C - the last segment north of CS-F to becompleted.

• Begin clearing and grubbing in Segment F. Setup dewatering system in CS-F.• Begin post sediment removal sampling of the creek.• Pending Agencies' approval of the protocol, begin post sediment removal

confirmation sampling.

11-01-UAO

• Continue operation of the storm water treatment system on an as-needed basis.• Continue screening sediments for placement against cell slopes as required.

PROJECT COMPLETION

Mobilization 100 %Berm Construction 100 %Liner Installation 100 %Sediment Removal Preparation 100 %Sediment Excavation (Site M) 100 %Creek Sediment Excavation 80 %Cover Installation 0 %Demobilization 0 %Final Report Preparation 0 %

Problems and SolutionsNone

Submittal Schedule StatusSee attached UAO schedule

Issues under reviewNone

CommentsNone

11-01-UAO

May 31 Sauget Area I UAO Sediment Removal Action

SCHEDULE

Deliverable

Issuance Date

Effective Date

Notice of Intent to Comply

Designation of Contractor andProject Coordinator

Access

Time Critical Removal ActionWork Plan Submittal

EPA Approval of TCRA W/P

Monthly Reports

Final Report

Mitigation Plan

Description

Date UAO signed by Muno

1 0 business day after issuance

3 business days after effective date

5 business days after effective date

14 calendar days after effective date

1 5 business days after effective date

Begin 30 calendar days after approval ofTCRA W/P until completion

60 Calendar days after completion ofsediments and soils removal

60 Calendar days after completion ofsediments and soils removal

Due Date

31 -May-00

14-Jun-OO

19-Jun-OO

21-Jun-OO

28-Jun-OO

^Wul^i

May 10, 2001

June 10, 2001

^^M

11-01-UAO

S F V I R \T R L N 1

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stHnc.com STL Savannah

Client PO. No.: 4503273556

LOG NO

LOG NO: SI-16198Received: 22 SEP 01Reported: 12 OCT 01

Ms. Kimberly PerrySolutia Inc.575 Maryville Center Dr.St. Louis, MO 63141

Contract No.: S7219Project: Sauget Area 1 Site M/Ven#203708

Sampled By: ClientCode: 103011022

REPORT OF RESULTS Page 1DATE/

SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDGtt

16198-116198-216198-316198-416198-5

TCMW-1STCMW-1MTCMW-2STCMW-4STCMW-5M

09-20-01/09:30 SIL06809-20-01/09:50 SIL06809-20-01/17:40 SIL06809-20-01/10:05 SIL06809-20-01/14:35 SIL068

PARAMETER 16198-1 16198-2 16198-3 16198-4 16198-5

Volatiles by GC/MS (8260)Chlorome thane, ug/1Bromomethane (Methylbromide) , ug/1Vinyl chloride, ug/1Chloroethane, ug/1Methylene chloride(Dichloromethane) , ug/1

Acetone, ug/1Carbon disulfide, ug/11 , 1 -Dichloroethene , ug/11 , 1 -Di chloroethane , ug/1Cis/Trans -1,2 -Dichloroethene ,Chloroform, ug/11, 2 -Di chloroethane, ug/12-Butanone (MEK) , ug/11,1, 1 -Trichloroethane , ug/1Carbon tetrachloride , ug/1Bromodichloromethane, ug/1

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U

ug/1 5.0U5.0U5.0U25U5.0U5.0U5.0U

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U5.0U5.0U25U5.0U5.0U5.0U

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U5.0U5.0U25U5.0U5.0U5.0U

10U9.8U

10U10U4.7U

•

SOU ,,5.0U5.0U5.0U5.0U5.0U5.0U25U5.0U5.0U5.0U

1009.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U5.0U5.0U25U5.0U5.0US.OU

STL Savannah is a part of Severn Trent Laboratories, Inc.

S I V I R N

1 R ]• X I

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.sWnc.com STL Savannah

Client PO. No.: 4503273556

LOG NO






SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDG#

16198-1 TCMW-1S16198-2 TCMW-1M16198-3 TCMW-2S16198-4 TCMW-4S16198-5 TCMW-5M


PARAMETER 16198-1

1, 1,2,2 -Tetrachloroe thane, ug/11,2-Dichloropropane, ug/1trans-l,3-Dichloropropene, ug/1Trichloroethene, ug/1Dibromochlorome thane, ug/11,1,2-Trichloroethane, ug/1Benzene, ug/1cis-l,3-Dichloropropene, ug/1Bromoform, ug/12-Hexanone, ug/14-Methyl-2-pentanone (MIBK) , ug/1Tetrachloroethene, ug/1Toluene, ug/1Chlorobenzene, ug/1Ethylbenzene , ug/1Styrene, ug/1Xylenes, Total, ug/1Surrogate - Toluene -d8Surrogate - 4-Bromof luorobenzeneSurrogate - Dibromof luorome thaneDilution FactorAnalysis Date 10Batch ID

5.0U5.0U5.0U2.7U5.0U5.0U1.2Ul.OU5.0U25U25U5.0U5.0U5.0U5.0U5.0U5.0U96 %80 %90 %

1.02.011B1002

16198-2


110.02.011B1002

16198-3

5.0U5.0U5.0U2.7U5.0U5.0U1.2Ul.OU5.0U25U25U5.0U5.0U1.7J5.0U5.0U5.0U98 %80 %88 %

110.02.011B1002

16198-4


110.02.011B1002

16198-5

5.0U5.0U5.0U2.7U5.0U5.0U1.2Ul.OU5.0U25U25U5.0U5.0U6.05.0U5.0U5.0U96 %80 %86 %

110.02.011B1002


S I \ I k !\

T R I X 1

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com STL Savannah

LOG NO


Ms. Kimberly PerrySolutia Inc. Client PO. No.: 4503273556575 Maryville Center Dr.St. Louis, MO 63141





16198-1 TCMW-1S16198-2 TCMW-1M16198-3 TCMW-2S16198-4 TCMW-4S16198-5 TOJW-5M

PARAMETER

Arsenic (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Chromium (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Copper (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID


16198-1

0.0047B1

09.26.0109.28.01

0926H

0.010U1

09.26.0109.28.01

0926H

0.0047B1

09.26.0109.28.01

0926H

16198-2

0.0038B1

09.26.0109.28.01

0926H

0.010U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

16198-3

0.010U1

09.26.0109.28.01

0926H

0.010U1

09.26.0109.28.01

0926H

0.010B1

09.26.0109.28.01

0926H

16198-4

0.010U1

09.26.0109.28.01

0926H

0.010U1

09.26.0109.28.01

0926H

0.0032B1

09.26.0109.28.01

0926H

16198-5

0.0057B1

09.26.0109.28.01

0926H

0.0023B1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H


S 1 V I R \

T R F N 1

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com STL Savannah

Client PO. No.: 4503273556

LOG NO





REPORT OF RESULTS Page 4DATE/TIME SAMPLED SDG#


PARAMETER

Iron (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Manganese (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Nickel (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID


16198-1

0.023B1

09.26.0109.28.01

0926H

0.231

09.26.0109.28.01

0926H

0.0079B1

09.26.0109.28.01

0926H

16198-2

211

09.26.0109.28.01

0926H

0.941

09.26.0109.28.01

0926H

0.020B1

09.26.0109.28.01

0926H

16198-3

0.050D1

09.26.0109.28.01

0926H

0.361

09.26.0109.28.01

0926H

0.0086B1

09.26.0109.28.01

0926H

16198-4

0.041B1

09.26.0109.28.01

0926H

0.481

09.26.0109.28.01

0926H

0.011B1

09.26.0109.28.01

0926H

16198-5

271

09.26.0109.28.01

0926H

1.21

09.26.0109.28.01

0926H

0.040U1

09.26.0109.28.01

0926H


S I V \ R N

T R I NT


LOG NO


Ms. Kimberly PerrySolatia Inc. Client PO. No.: 4503273556575 Maryville Center Dr.St. Louis, MO 63141



REPORT OF RESULTS Page 5DATE/TIME SAMPLED SDG#


PARAMETER

Lead (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch. ID

Antimony (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Zinc (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID


16198-1

0.0050U1

09.26.0109.28.01

0926H

0.020D1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

16198-2

0.0050U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

16198-3

0.0050D1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

16198-4

0.0050U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

16198-5

0.0050U1

09.26.0109.28.01

092 6H

0.020U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H


S I \ I K \

I R I !\ I


Client PO. No.: 4503273556

LOG NO


Ms. Kimberly PerrySolutia Inc.575 Maryville Center Dr.St. Louis, HO 63141





16198-116198-216198-316198-416198-5



PARAMETER 16198-1 16198-2 16198-3 16198-4 16198-5

TCL Semivolatiles (8270)Phenol, ug/1 10U 10U 10U 10U 10Ubis(2-Chloroethyl)ether, ug/1 10U 10U 10U 10U 10U2-Chlorophenol, ug/1 10U 10U 10U 10U 10U1.3-Dichlorobenzene, ug/1 10U 10U 10U 10U 10U1.4-Dichlorobenzene, ug/1 10U 10U 10U 10U 2.9J1,2-Dichlorobenzene, ug/1 10U 10U 10U 10U 10U2-Methylphenol (o-Cresol), ug/1 10U 10U 10U 10U 10U2,2'-Oxybis(l-Chloropropane 10U 10U 10U 10U 10U) (bis-2-chloroisopropylether), ug/13-Methylphenol/4-Methylphen 10U 10U 10U 10U 10Uol (m&p-Cresol), ug/1N-Nitroso-di-n-propylamine, ug/1 10U 10U 10U 10U 10UHexachloroethane, ug/1 1.9U 1.9U 1.9U 1.9U 1.9UNitrobenzene, ug/1 3.5U 3.5U 3.5U 3.5U 3.5UIsophorone, ug/1 10U 10U 10U 10U 10U2-Nitrophenol, ug/1 10U 10U 10U 10U 10Ubis(2-Chloroethoxy)methane, ug/1 10U 10U 10U 10U 10U

STL Savannah Is a part of Severn Trent Laboratories, Inc.

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stHnc.com

s i v r R !\T R E N I

STL Savamwh

Client PO. No.: 4503273556

LOG NO







16198-116198-216198-316198-416198-5



PARAMETER 16198-1 16198-2 16198-3 16198-4 16198-5

2,4-Dichlorophenol, ug/1 10U 10U 10U 10U 10U1,2,4-Trichlorobenzene, ug/1 10U 10D 10U 10U 10UNaphthalene, ug/1 10U 10U 10U 10U 10U4-Chloroaniline, ug/1 20U 20U 20U 20U 20UHexachlorobutadiene, ug/1 10U 10U 10U 10U 10U4-Chloro-3-methylphenol, ug/1 10U 10U 10U 10U 10U2-Methylnaphthalene, ug/1 10U 10U 10U 10U 10UHexachlorocyclopentadiene, ug/1 10U 10U 10U 10U 10U2,4,6-Trichlorophenol, ug/1 2.1U 2.1U 2.1U 2.1U 2.1U2,4,5-Trichlorophenol, ug/1 10U 10U 10U 10U 10U2-Chloronaphthalene, ug/1 10U 10U 10U 10U 10U2-Nitroaniline, ug/1 SOU SOU SOU SOU SOUDimethylphthalate, ug/1 10U 10U 10U 10U 10UAcenaphthylene, ug/1 10U 10U 10U 10U 10U3-Nitroaniline, ug/1 SOU SOU SOU SOU SOUAcenaphthene, ug/1 10U 10U 10U 10U 10U2,4-Dinitrophenol, ug/1 14U 14U 14U 14U 14U4-Nitrophenol, ug/1 SOU SOU SOU SOU SOUDibenzofuran, ug/1 10U 10U 10U 10U 10U


S I \ I K X

I R I X I

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • fax: 912 352 0165 • vww.stHnc.com STL Savannah

Client PO. No.: 4503273556

LOG NO







16198-116198-216198-316198-416198-5


09-20-01/09:3009-20-01/09:5009-20-01/17:4009-20-01/10:0509-20-01/14:35

SIL068SIL068SILO 6 8SILO 6 8SIL068

PARAMETER 16198-1 16198-2 16198-3 16198-4 16198-5

2,4-Dinitrotoluene, ug/1 10U 10U 10U 10U 10U2,6-Dinitrotoluene, ug/1 10U 10U 10U 10U 10UDiethylphthalate, ug/1 10U 10U 10U 10U 10U4-Chlorophenylphenyl ether, ug/1 10U 10U 10U 10U 10UFluorene, ug/1 l.OU l.OU l.OU l.OU l.OU4-Nitroaniline, ug/1 SOU SOU SOU SOU SOU4,6-Dinitro-2-methylphenol, ug/1 13U 13U 13U 13U 13UN-Nitrosodiphenylamine, ug/1 0.54J 5.0U 5.0U 5.0U 5.0U4-Bromophenylphenyl ether, ug/1 l.OU l.OU l.OU l.OU l.OUHexachlorobenzene, ug/1 10U 10U 10U 10U 10UPentachlorophenol, ug/1 5.0U 5.0U 5.0U 5.0U 5.0UPhenanthrene, ug/1 10U 10U 10U 10U 10UAnthracene, ug/1 10U 10U 10U 10U 10UDi-n-butylphthalate, ug/1 10U 10U 10U 0.29J 10UFluoranthene, ug/1 10U 10U 10U 10U 10UPyrene, ug/1 10U 10U 10U 10U 10UButylbenzylphthalate, ug/1 10U 10U 10U 10U 10U3,3'-Dichlorobenzidine, ug/1 20U 20U 20U 20U 20UBenzo(a)anthracene, ug/1 10U 10U 10U 10U 10U



S I \ I R \1 R I i\ I

STV Savannah

LOG NO







16198-116198-216198-316198-416198-5



PARAMETER 16198-1 16198-2 16198-3 16198-4 16198-5

bis(2-Ethylhexyl)phthalate, ug/1Chrysene, ug/1Di-n-octylphthalate, ug/1Benzo(b) fluoranthene, ug/1Benzo (k) fluoranthene , ug/1Benzo (a) pyrene , ug/1Indeno(l,2,3-cd)pyrene, ug/1Dibenzo (a, h) anthracene, ug/1Benzo (g, h, Dperylene, ug/1Carbazole, ug/1Surrogate - Phenol -d5Surrogate - 2 - FluorophenolSurrogate - 2,4, 6-TribromophenolSurrogate - Nitrobenzene - d5Surrogate - 2 - FluorobiphenylSurrogate - Terphenyl-dl4Dilution FactorPrep Date 09Analysis Date 09Batch ID

1.3J10U10U10U10U10U10U10U10U3.4U76 %78 *82 %72 %72 %56 %

1.26.01.28.010926C

6.710U10U10U10U10U10U10U10U3.4U77 %84 %80 %78 %80 %54 %

109.26.0109.28.01

0926C

1.910U10U10U10U10U10U10U10U3.4U758382807842

109.26.0109.28.01

0926C

9.510U10U10U10U10U10U10U10U3.4U86 %87 %92 %80 %76 %64 %

109.26.0109.28.01

0926C

1210U10U10U10U10U10U10U10U3.4U758376767648

109.26.0109.28.01

0926C


5102 LaBoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stWnc.com

s i v i R r\T R E N I

STL Savannah

Client PO. No.: 4503273556

LOG NO

LOG NO: SI-16198Received: 22 SEP 01Reported: 12 OCX 01





SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDGtt

16198-116198-216198-316198-416198-5



PARAMETER 16198-1 16198-2 16198-3 16198-4 16198-5

Poly chlorinated Biphenyls (680)Mbnochlorobiphenyl , ug/1Dichlorobiphenyl , ug/1Trichlorobiphenyl, ug/1Tetrachlorobiphenyl, ug/1Pentachlorobiphenyl , ug/1Hexachlorobiphenyl , ug/1Heptachlorobiphenyl , ug/1Octachlorobiphenyl , ug/1Nonachlorobiphenyl , ug/1Decachlorobiphenyl , ug/1Surrogate - DCB 13C12Dilution FactorPrep DateAnalysis DateBatch ID

0.10U0.10U0.10U0.20U0.20U0.20U0.30U0.30U0.50U0.50U75 %

109.26.0110.02.01

0926E

0.10U0.10U0.10U0.20U0.20U0.20U0.30U0.30U0.50U0.50U62 %

109.26.0110.02.01

0926E

0.10U0.10U0.10U0.20U0.20U0.20U0.30U0.30U0.50U0.50U52 *

109.26.0110.02.01

0926E

0.10U0.10UO.lOU0.20U0.20U0.20U0.30U0.30U0.50U0.50U55 %

109.26.0110.02.01

0926E

O.lOUO.lOUO.lOU0.20U0.20U0.20U0.30U0.30U0.50U0.50U50 %

109.26.0110.02.01

0926E


S I V I K \I R I \ I

5102 LaRoche Avenue » Savannah, GA 31404 » Tel: 912 354 7858 « Fax: 912 352 0165 • www.stNnc.com_______

LOO NO: SI-16198Received: 22 SEP 01Reported: 12 OCT 01

Ms. Kimberly PerrySolutia inc. Client PO. No.: 4503273556575 Maryville Center Dr.St. Louie, MO 63141




LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDG#

16198-6 TCMW-5S 09-20-01/14:45 SIL068

PARAMETER 16198-6

Volatiles by GC/MS (8260)Chloromethane, ug/1 10UBromomethane (Methyl bromide), ug/1 9.8UVinyl chloride, ug/1 10UChloroethane, ug/1 10UMethylene chloride (Dichloromethane), ug/1 4.7UAcetone, ug/1 SOUCarbon disulfide, ug/1 5.0U1,1-Dichloroethene, ug/1 5.OU1.1-Dichloroethane, ug/1 5.0UCis/Trane-1,2-Dichloroethene, ug/1 5.0UChloroform, ug/1 3.1J1.2-Dichloroethane, ug/1 5.0U2-Butanone (MBK), ug/1 25U1,1,1-Trichloroethane, ug/1 5. OUCarbon tetrachloride, ug/1 5.0UBromodichloromethane, ug/1 5.0U1,1,2,2-Tetrachloroethane, ug/1 5.0U1,2-Dichloropropane, ug/1 5.0Utrans-l,3-Dichloropropene, ug/1 5.0UTrichloroethene, ug/1 2.7UDibromochloromethane, ug/1 5.0U1,1,2-Trichloroethane, ug/1 5.0U


S I Y I R \

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com STLSmwnah

Client PO. No.: 4503273556


Ms. Kimberly PerrySolutia Inc.575 Maryville Center Dr.St. Louie, MO 63141




SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDG#LOG NO

16198-6 TCMW-5S

PARAMETER

09-20-01/14:45 SIL068

16198-6

Benzene, ug/1cis-l,3-Dichloropropene, ug/1Bromoform, ug/12 -Hexanbne, ug/14-Methyl-2-pentanone (MIBK), ug/1Tetrachloroethene, ug/1Toluene, ug/1Chlorobenzene, ug/1Bthylbenzene, ug/1Styrene, ug/1Xylenes, Total, ug/1Surrogate - Toluene-d8Surrogate - 4-BromofluorobenzeneSurrogate - DibromofluoromethaneDilution FactorAnalysis DateBatch ID

Arsenic (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

1.2Dl.OU5.0U25U25U

5.5,onou

2.9J5.0U5.0U5.0U94 %80 %90 %

110.02.011B1002

0.0050B1

09.26.0109.28.01

0926H


V I K

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fate 912 352 0165 • www.stNnc.com ST1 Savannah


Ms. Kinberly PerrySolutia Inc. Client PO. No.: 4503273556575 Maryville Center Dr.St. Louis, MO 63141




LOO NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDG#

16198-6 TCMW-5S

PARAMETER

09-20-01/14:45 SIL068

16198-6

Chromium (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Copper (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Iron (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Manganese (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

0.0017B1

09.26.0109.28.01

0926H

0.0034B1

09.26.0109.28.01

0926H

0.0721

09.26.0109.28.01

0926H

0.097I

09.26.0109.28.01

0926H


S I Y I R i\I R I N I

5102 LaRoche Avenue • Savannah, 6A 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • «mw.stHnc.com SIL Savannah

Client PO. No.: 4503273556

LOG MO: SI-16198Received: 22 SEP 01Reported: 12 OCT 01

KB. Kimberly PerrySolutia Inc.575 Maryville Center Dr.St. Louis, MO 63141





16198-6 TCMW-5S

PARAMETER

09-20-01/14:45 SIL068

16198-6

Nickel (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Lead (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Antimony (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Zinc (6010), mg/1Dilution FactorPrep DateAnalysis DateBatch ID

0.040U1

09.26.0109.28.01

0926H

0.0050U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H

0.020U1

09.26.0109.28.01

0926H


S I. V I kT R I M

5102 LaRoche Avenue « Savannah, 6A 31404 • Tel: 912 354 7858 « Fax: 912 352 0165 • www.stHnc.com_____ STL Savannah






LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDGtt

16198-6 TCMW-5S 09-20-01/14:45 SIL068

PARAMETER 16198-6

TCL Semivolatiles (8270)Phenol, ug/1 10Ubis(2-Chloroethyl)ether, ug/1 10U2-Chlorophenol, ug/1 10U1.3-Dichlorobenzene, ug/1 10U1.4-Dichlorobenzene, ug/1 10U1,2-Dichlorobenzene, ug/1 10U2-Methylphenol (o-Cresol), ug/1 10U2,2'-Oxybis(1-Chloropropane) 10U(bis-2-chloroisopropyl ether), ug/1

3-Methylphenol/4-Methylphenol (m&p-Cresol), ug/1 10UN-Nitroso-di-n-propylamine, ug/1 10UHexachloroethane, ug/1 1.9UNitrobenzene, ug/1 3.5UIsophorone, ug/1 10U2 -Nitrophenol, ug/1 1OUbis(2-Chloroethoxy)methane, ug/1 10U2,4-Dichlorophenol, ug/1 10U1,2,4-Trichlorobenzene, ug/1 10UNaphthalene, ug/1 10U4-Chloroaniline, ug/1 20UHexachlorobutadiene, ug/1 10U4-Chloro-3-methylphenol, ug/1 10U


S I V I R \I R I N I

5102 LaRoche Avenue « Savannah. GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com_____ SUSwwma*






LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDO#

16198-6 TCMW-5S 09-20-01/14:45 SIL068

PARAMETER 16198-6

2-Methylnaphthalene, ug/1 10UHexachlorocyclopentadiene, ug/1 10U2,4,6-Trichlorophenol, ug/1 2.1U2,4,5-Trichlorophenol, ug/1 10U2-Chloronaphthalene, ug/1 10U2-Nitroaniline, ug/1 SOUDimethylphthalate, ug/1 10UAcenaphthylene, ug/1 10U3-Nitroaniline, ug/1 SOUAcenaphthene, ug/1 10U2,4-Dinitrpphenol, ug/1 14U4-Nitrophenol, ug/1 SOUDibenzofuran, ug/1 10U2,4-Dinitrotoluene, ug/1 10U2,6-Dinitrotoluene, ug/1 10UDiethylphthalate, ug/1 10U4-Chlorophenylphenyl ether, ug/1 10UFluorene, ug/1 l.OU4-Nitroaniline, ug/1 SOU4,6-Dinitro-2-methylphenol, ug/1 13UN-Nitrosodiphenylamine, ug/1 5.0U4-Bromophenylphenyl ether, ug/1 l.OUHexachlorobenzene, ug/1 10U


S I V 1 K \

T R I N I

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 » www.sttinc.com_____ STt Savannah







16198-6 TCMW-5S 09-20-01/14:45 SIL068

PARAMETER 16198-6

Pentachlorophenol, ug/1 5.OUPhenanthrene, ug/1 10UAnthracene, ug/1 10UDi-n-butylphthalate, ug/1 10UFluoranthene, ug/1 10UPyrene, ug/1 10UButylbenzylphthalate, ug/1 10U3,3'-Dichlorobenzidine, ug/1 20UBenzo(a)anthracene, ug/1 10Ubis(2-Ethylhexyl)phthalate, ug/1 1.8Chrysene, ug/1 10DDi-n-octylphthalate, ug/1 10UBenzo(b)fluoranthene, ug/1 10UBenzo(k)fluoranthene, ug/1 10UBenzo(a)pyrene, ug/1 10UIndeno(l,2,3-cd)pyrene, ug/1 10UDibenzo(a,h)anthracene, ug/1 10UBenzo (g,h, Dperylene, ug/1 10DCarbazole, ug/1 3.4USurrogate - Phenol-d5 78 %Surrogate - 2 -Fluorophenol 85 %Surrogate - 2,4,6-Tribromophenol 79 %Surrogate - Nitrobenzene - d5 80 %


S I \ I k \

1 K I N I

Client PO. No.: 4503273556

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stHnc.com_____ STL Swwnnah







16198-6 TCMW-5S

PARAMETER

09-20-01/14:45 SIL068

16198-6

Surrogate - 2-FluorobiphenylSurrogate - Terphenyl-dl4Dilution FactorPrep DateAnalysis DateBatch ID

86 %78 %

109.26.0109.28.01

0926C

Polychlorinated Biphenyls (680)Monochlorobiphenyl , ug/1Dichlorobiphenyl , ug/1Trichlorobiphenyl, ug/1

> Tetrachlorobiphenyl, ug/1Pentachlorobiphenyl , ug/1Hexachlorobiphenyl , ug/1Heptachlorobiphenyl , ug/1Octachlorobiphenyl , ug/1Nonachlorobiphenyl , ug/1Decachlorobiphenyl , ug/1Surrogate - DCB 13C12Dilution FactorPrep DateAnalysis DateBatch ID

0.10U0.10U0.10U0.20U0.20U0.20U0.30U0.30U0.50U0.50U56 %

109.26.0110.02.01

0926B

STL Savannah Is a part of Severn Trent laboratories, Inc.

S I V I K \

T R i: N I

5102 LaRoche Avenue • Savannah. GA 31404 • Tel: 912 354 7858 « Fax: 912 352 0165 • www.stHnc.com_____ STL Savannah


Ms. Kimberly PerrySolutia Inc. Client PO. No.: 4503273556575 Maryville Center Dr.St. Louis, HO 63141





16198-7 TB 09-20-01 SIL068

PARAMETER 16198-7

Volatiles by GC/MS (8260)Chloromethane, ug/1 10UBromomethane (Methyl bromide), ug/1 9.8UVinyl chloride, ug/1 10UChloroethane, ug/1 10UMethylene chloride (Dichloromethane), ug/1 4.7UAcetone, ug/1 SOUCarbon disulfide, ug/1 5.0U1,1-Dichloroethene, ug/1 5.OU1.1-Dichloroethane, ug/1 5.0UCis/Trans-1,2-Dichloroethene, ug/1 5.0UChloroform, ug/1 5.0U1.2-Dichloroethane, ug/1 5.0U2-Butanone (MBK), ug/1 25U1,1,1-Trichloroethane, ug/1 5.0UCarbon tetrachloride, ug/1 5.0UBromodichloromethane, ug/1 5.0U1,1,2,2-Tetrachloroethane, ug/1 5.0U1,2-Dichloropropane, ug/1 5.0Utrans-l,3-Dichloropropene, ug/1 5.0UTrichloroethene, ug/1 2.7UDibromochloromethane, ug/1 5.0U1,1,2-Trichloroethane, ug/1 5.0U

STL Savannah is a part of Severn Trent Laboratories. Inc.

T R I N 1

5102 URoche /Wenue • Savannah. GA 31404 • Tel: 912 354 7858 « Fax: 912 352 0165 • www.sttJnc.com_____ STL Savannah






LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES TIME SAMPLED SDO#

16198-7 TB 09-20-01 SIL068

PARAMETER 16198-7

Benzene, ug/1 1.2Ucis-1,3-Dichloroprppene, ug/1 l.OUBromoform, ug/1 5.OU2-Hexanone, ug/1 . 25U4-Methyl-2-pentanone (MIBK), ug/1 25UTetrachloroethene, ug/1 5.0UToluene, ug/1 1.2JChlorobenzene, ug/1 5.0UBthylbenzene, ug/1 5.0UStyrene, ug/1 5.0UXylenes, Total, ug/1 5.0USurrogate - Toluene-d8 96 %Surrogate - 4-Bromofluorobenzene 80 %Surrogate - Dibromofluoromethane 86 %Dilution Factor 1Analysis Date 10.02.01Batch ID 1B1002

STL Savannah Is a part of Severn Trent Laboratories, Inc.

S 1 \ I

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com STL







16198-7 TB 09-20-01 SIL068

PARAMETER 16198-7

These test results meet all the requirements of NELAC. All questionsregarding this test report should be directed to the STL Project Managerwho signed this test report.

SW-846, Test Methods for Evaluating Solid Waste, Third Edition,September 1986, and Updates I, II, IIA, IIB, and III.

U = Indicates compound was analyzed for but not detected.

J = The flag "J" indicates the presence of a compound that meets theidentification criteria, but the result is less than the sample RL andgreater than the MDL.

B (Inorganic) = This flag indicates the reported value was obtained froma reading that was less than the Project Reporting Limits but greaterthan or equal to the Method Detection Limit (MDL).

Michellfe Owens, Project Manager

Final Page Of Report




LOG NO

REPORT OF RESULTS

SAMPLE DESCRIPTION , LIQUID SAMPLES

STL Savannah


Client PO. No.: 4503273556

Requisition: 203708Contract No.: S7219

Project: Sauget Area 1Sampled By: Client

Code: 103011022Page l

DATE/TIME SAMPLED SDG#

16125-116125-216125-316125-416125-5

TCMW-3MTCMW-6MTCMW-6STCMW-3STCMW-3S-DUP


PARAMETER 16125-1 16125-2 16125-3 16125-4 16125-5

Volatiles by GC/MS (8260)Chloromethane , ug/1Bromoniethane (Methylbromide) , ug/1Vinyl chloride, ug/1Chloroethane , ug/1Methylene chloride(Dichloromethane) , ug/1

Acetone , ug/1Carbon disulfide, ug/11 , 1 -Dichloroethene , ug/11,1-Dichloroethane, ug/1Ci s /Trams - 1 , 2 -Dichloroethene ,Chloroform, ug/11,2-Dichloroethane, ug/12-Butanone (MEK) , ug/11,1, 1 -Trichloroethane , ug/1Carbon tetrachloride , ug/1Bromodi chloromethane, ug/1

10U9.8U

10U10U

4.7U

SOU5.0U5.0U5.0U

ug/1 5.0U5.0U5.0U25U

5.0U5.0U5.0U

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U5.0U5.0U25U5.0U5.0U5.0U

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U5.0U5.0U25U5.0U5.0U5.0U

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U8.65.0U25U5.0U5.0U5.0U

10U9.8U

10U10U4.7U

SOU5.0U5.0U5.0U5.0U8.15.0U2SU5.0U5.0U5.0U


5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com


REPORT OF RESULTS

STL SavannahLOG MO: SI-16125

Received: 20 SEP 01Reported: 12 OCT 01

Client PO. No.: 4503273556



Code: 103011022Page 2

DATE/*

16125-1 TCMW-3M16125-2 TCMW-6M16125-3 TCMW-6S16125-4 TCMW-3S16125-5 TCMW-3S-DUP


PARAMETER 16125-1

1,1,2, 2 -Tetrachloroe thane , ug/11,2-Dichloropropane, ug/1trans-l,3-Dichloropropene, ug/1Trichloroethene, ug/1Dibromochloromethane , ug/11,1,2-Trichloroethane, ug/1Benzene, ug/1cis-l,3-Dichloropropene, ug/1Bromoform, ug/12-Hexanone, ug/14-Methyl-2-pentanone (MIBK) , ug/1Tetrachloroe thene, ug/1Toluene, ug/1Chlorobenzene , ug/1Ethylbenzene , ug/1Styrene, ug/1Xylenes, Total, ug/1Surrogate - Toluene -d8Surrogate - 4 -BromofluorobenzeneSurrogate - DibromofluoromethaneDilution FactorAnalysis Date 10Batch ID

5.0U5.0D5.0U2.7U5. on5.0U1.2Ul.OU5.0D25025U5.0U5.0U1.1J5. OU5.0Us. on96 %80 %88 %

1.01.011B1001

16125-2

5.0D5.0D5.0U2.7D5.0U5.0U1.2Dl.OU5.0U25U25U5.0U5.0U5.0U5.0U5.0U5.0U96 %80 %88 %

110.01.011B1001

16125-3

5.0U5 . OU5.0U2.7U5.0U5.0U1.2Ul.OU5.0U25U25U5.0U5.0U5.0U5.0U5.0U5.0U96 %80 %88 %

110.01.011B1001

16125-4


110.01.011B1001

16125-5


110.01.011B1001


5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.oom sn

Ms. Kimberly PerrySolatia Inc.575 Maryville Center Dr.St. Louis, MO 63141

REPORT OF RESULTS


Client PO. No.: 4503273556



Code: 103011022Page 3

DATE/SAMPLEDTf


PARAMETER

Arsenic (6010) , mg/1Dilution Factor*Prep DateAnalysis DateBatch ID

Chromium (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Copper (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID


16125-1

0.0057B1

09.26.0109.28.01

09261

0.010U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

16125-2

0.0039B1

09.26.0109.28.01

09261

0.010U1

09.26.0109.28.01

09261

0.020D1

09.26.0109.28.01

09261

16125-3

0.0040B1

09.26.0109.28.01

09261

0.0051B1

09.26.0109.28.01

09261

0.0043B1

09.26.0109.28.01

09261

16125-4

0.010U1

09.26.0109.28.01

09261

0 . 010U1

09.26.0109.28.01

09261

0.0028B1

09.26.0109.28.01

09261

16125-5

0 . 010U1

09.26.0109.28.01

09261

0.010D1

09.26.0109.28.01

09261

0.0029B1

09.26.0109.28.01

09261


S I \ I K \



REPORT OF RESULTS

STL Savannah

LOG NO: SI-16125Received: 20 SBP 01Reported: 12 OCT 01

Client PO. No.: 4503273556



Code: 103011022Page 4

DATE/LOG NO


PARAMETER

Iron (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Manganese (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Nickel (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID


16125-1

191

09.26.0109.28.01

09261

1.11

09.26.0109.28.01

09261

0.040TJ1

09.26.0109.28.01

09261

16125-2

6.41

09.26.0109.28.01

09261

0.751

09.26.0109.28.01

09261

0 . 04 OD1

09.26.0109.28.01

09261

16125-3

0.201

09.26.0109.28.01

09261

0.131

09.26.0109.28.01

09261

0 . 0094B1

09.26.0109.28.01

09261

16125-4

0.671

09.26.0109.28.01

09261

1.41

09.26.0109.28.01

09261

0.0075B1

09.26.0109.28.01

09261

16125-5

0.671

09.26.0109.28.01

09261

1.41

09.26.0109.28.01

09261

0.0070B1

09.26.0109.28.01

09261


S I VI K \


KB. Kimberly PerrySolutia Inc.575 Maryville Center Dr.St. Louis, MO 63141

REPORT OF RESULTS

STL Savannah


Client PO. No.: 4503273556



Code: 103011022Page 5

DATE/LOG NO 1 V,

16125-1 TOW-3M16125-2 TCMW-6M16125-3 TOW- 6316125-4 TCMW-3S16125-5 TCMW-3S-DUP

PARAMETER

Lead (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Antimony (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID

Zinc (6010) , mg/1Dilution FactorPrep DateAnalysis DateBatch ID


16125-1

0.0050D1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

16125-2

0.0050U1

09.26.0109.28.01

09261

0 . 020D1

09.26.0109.28.01

09261

0.020D1

09.26.0109.28.01

09261

16125-3

0.0050D1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

16125-4

0.0050U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

16125-5

0 . 0050U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

0.020U1

09.26.0109.28.01

09261

STL Savannah is a part of Severn Trent Laborakxies, Inc.



REPORT OP RESULTS

LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES

S I Y I K \

I R 1 \ I

STL SavannahLOG NO: SI-16125


Client PO. No.: 4503273556



Code: 103011022Page 6

DATE/TIME SAMPLED SDO#

16125-116125-216125-316125-416125-5

TCMW-3MTCMW-6MTCMW-6STCMW-3STCMW-3S-DDP


PARAMETER 16125-1 16125-2 16125-3 16125-4 16125-5

TCL Semivolatiles (8270)Phenol, ug/1 10D 10U 10D 10D 10Ubis(2-Chloroethyl)ether, ug/1 10U 10U 10U 10U 10D2-Chlorophenol, ug/1 10D 10D 10U 10U 10U1.3-Dichlorobenzene, ug/1 10U 10D 10U 10D 10U1.4-Dichlorobenzene, ug/1 10U 10D 10U 10D 10U1,2-Dichlorobenzene, ug/1 10U 10D 10D 10U 10U2-Methylphenol (o-Cresol) , ug/1 10U 10D 10U 10U 10U2,2'-Oxybisd-Chloropropane 10U 10D 10U 10U 10U) (bis-2-chloroisopropylether), ug/13-Methylphenol/4-Methylphen 10U 10U 10D 10U 10Uol (m&p-Cresol), ug/1N-Nitroso-di-n-prppylamine, ug/1 10U 10U 10D 10U 10OHexachloroethane, ug/1 1.9U 1.9U 1.9U 1.9U 1.9DNitrobenzene, ug/1 3.5U 3.5U 3.5D 3.5U 3.5UIsophorone, ug/1 10D 10D 10U 10U 10U2-Nitrophenol, ug/1 10D 10D 10D 10U 10Dbis (2-Chloroethoxy)methane, ug/1 10U 10U 10U 10U 10D


S I \ I K \



LOG NO

REPORT OF RESULTS



Client PO. No.: 4503273556



Code: 103011022Page 7


16125-116125-216125-316125-416125-5



PARAMETER 16125-1 16125-2 16125-3 16125-4 16125-5

2,4-Dichlorophenol, ug/1 10U 10U 10U 10U 10U1,2,4-Trichlorobenzene, ug/1 10U 10U 10U 10U 10UNaphthalene, ug/1 10U 10U 10U 10U 10U4-Chloroaniline, ug/1 20U 20U 20U 20U 20UHexachlorobutadiene, ug/1 10U 10U 10U 10U 10U4-Chloro-3-methylphenol, ug/1 10U 10U 10U 10U 10U2-Methylnaphthalene, ug/1 10U 10U 10U 10U 10UHexachlorocyclopentadiene, ug/1 10U 10U 10U 10U 10U2,4,6-Trichlorophenol, ug/1 2.1U 2.1U 2.1U 2.1U 2.1U2,4,5-Trichlorophenol, ug/1 10U 10U 10U 10U 10U2-Chloronaphthalene, ug/1 10U 10U 10U 10U 10U2-Nitroaniline, ug/1 SOU SOU SOU SOU SOUDimethylphthalate, ug/1 10U 10U 10U 10U 10UAcenaphthylene, ug/1 10U 10U 10U 10U 10U3-Nitroaniline, ug/1 SOU SOU SOU SOU SOUAcenaphthene, ug/1 10U 10U 10U 10U 10U2,4-Dinitrophenol, ug/1 14U 14U 14U 14U 14U4-Nitrophenol, ug/1 SOU SOU SOU SOU SOUDibenzofuran, ug/1 10U 10U 10U 10U 10U


S I \ I



REPORT OF RESULTS

LOG NO SAMPLE DESCRIPTION , LIQUID SAMPLES

STL SavannahLOO NO: SI-16125


Client PO. No.: 4503273556



Code: 103011022Page 8


16125-116125-216125-316125-416125-5



PARAMETER 16125-1 16125-2 16125-3 16125-4 16125-5

2,4-Dinitrotoluene, ug/1 10U 10U 10U 10U 10U2,6-Dinitrotoluene, ug/1 10U 10U 10U 10U 10UDiethylphthalate, ug/1 10U 10U 10U 10U 10U4-Chlorophenylphenyl ether, ug/1 10U 10U 10U 10U 10UFluorene, ug/1 l.OU l.OU l.OU l.OU l.OU4-Nitroaniline, ug/1 SOU SOU SOU SOU SOU4,6-Dinitro-2-methylphenol, ug/1 13U 13U 13U 13U 13UN-Nitrosodiphenylamine, ug/1 5.0U 5.0U 5.0U 5.0U 5.0U4-Bromophenylphenyl ether, ug/1 l.OU l.OU l.OU l.OU l.OUHexachlorobenzene, ug/1 10U 10U 10U 10U 10UPentachlorophenol, ug/1 5.0U 5.0U 5.0U 5.0U 5.0UPhenanthrene, ug/1 10U 10U 10U 10U 10UAnthracene, ug/1 10U 10U 10U 10U 10UDi-n-butylphthalate, ug/1 10U 10U 10U 0.47J 0.48JFluoranthene, ug/1 10U 10U 10U 10U 10UPyrene, ug/1 10U 10U 10U 10U 10UButylbenzylphthalate, ug/1 10U 10U 10U 10U 10U3,3'-Dichlorobenzidine, ug/1 20U 20U 20U 20U 20UBenzo(a)anthracene, ug/1 10U 10U 10U 10U 10U


5102 LaRocne Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stt4nc.com


LOG NO

REPORT OF RESULTS


\ I U \

R 1 \ I

STL Savannah


Client PO. No.: 4503273556



Code: 103011022Page 9

DATE/TIME SAMPLED SDGft

16125-116125-216125-316125-416125-5



PARAMETER 16125-1 16125-2 16125-3 16125-4 16125-5

bis(2-Ethylhexyl)phthalate, ug/1Chrysene , ug/1Di-n-octylphthalate, ug/1Benzo (b) f luoranthene , ug/1Benzo (k) £ luoranthene , ug/1Benzo (a) pyrene , ug/1Indenod, 2, 3-cd)pyrene, ug/1Dibenzo (a, h) anthracene , ug/1Benzo (g,h,i)perylene, ug/1Carbazole , ug/1Surrogate - Phenol -d5Surrogate - 2-FluorophenolSurrogate - 2,4,6-TribromophenolSurrogate - Nitrobenzene - d5Surrogate - 2-FluorobiphenylSurrogate - Terphenyl-dl4Dilution FactorPrep Date 09Analysis Date 09Batch ID

2.310U10Uion10Uionion10D10U3.4U808581787848

1.26.01.27.010926C

2.110Uionionionionionionion3..4U67 %72 %73 %66 %70 %62 %

109.26.0109.27.01

0926C

1.1Jionionionionion1.3J1.3J1.9J3.4U70 %76 %76 %74 %76 %56 %

109.26.0109.27.01

0926C

2.7ionionionionionionionion3.4U687469687242

109.26.0109.27.01

0926C

2.9ionionionionionionionion3.4U677571707246

109.26.0109.27.01

0926C


S I \ I

5102 LaRoche Avenue • Savannah, GA 31404 • Tel: 912 354 7858 • Fax: 912 352 0165 • www.stMnc.com sn.


REPORT OF RESULTS

LOO NO: SI-16125Received: 20 SBP 01Reported: 12 OCT 01

Client PO. No.: 4503273556



Code: 103011022Page 10

DATE/SDO#~


PARAMETER

Polychlorinated Biphenyls (680)Monochlorobiphenyl , ug/1Dichlorobiphenyl, ug/1Trichlorobiphenyl, ug/1Tetrachlorobiphenyl , ug/1Pentachlorobiphenyl , ug/1Hexachlorobiphenyl , ug/1Heptachlorobiphenyl, ug/1Octachlorobiphenyl , ug/1Nonachlorobiphenyl , ug/1Decachlorobiphenyl , ug/1Surrogate - DCB 13C12Dilution FactorPrep DateAnalysis DateBatch ID


16125-1

0.10U0.10U0.10U0.20U0.20U0.20D0.30U0.30U0.50U0.50U66 %

109.26.0110.02.01

0926E

16125-2

0.10U0.10U0.10U0.20U0.20U0.20D0.30U0.30U0.50U0.50U64 %

109.26.0110.02.01

0926E

16125-3

0.10U0.10U0.10U0.20U0.20U0.20U0.30U0.30D0.50U0.50U70 %

109.26.0110.02.01

0926E

16125-4

0.10U0.10U0.10U0.2000.20U0.20U0.30U0.30U0.50U0.50D59 %

109.26.0110.02.01

0926E

16125-5

0.10D0.10U0.1000.20O0.20O0.2000.3000.3000.50O0.50O62 %

109.26.0110.02.01

0926B




REPORT OF RESULTS

LOG NO: SI-16125Received: 20 SBP 01Reported: 12 OCT 01

Client PO. No.: 4503273556



Code: 103011022Page 11

DATE/

16125-116125-216125-316125-416125-5

PARAMETER


' **

09-19-01/1609-19-01/1009-19-01/1009-19-01/1609-19-01/16

16125-1 16125-2 16125-3 16125-4

:10:40:50:20:20

SIL066SILO 68SILO 68SILO 68SIL068

16125-5

These test results meet all the requirements of NELAC. All questionsregarding this test report should be directed to the STL Project Managerwho signed this test report.

SW-846, Test Methods for Evaluating Solid Waste, Third Edition,September 1986, and Updates I, II, IIA, IIB, and III.

U = Indicates compound was analyzed for but not detected.

J = The flag "J" indicates the presence of a compound that meets theidentification criteria, but the result is less than the sample RL andgreater than the MDL.

B (Inorganic) « This flag indicates the reported value was obtained froma reading that was less than the Project Reporting Limits but greaterthan or equal to the Method Detection Limit (MDL).

MichelleVOwens, Project Manager

Final Page Of Report


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