APPENDIX RECOMMENDED SAFETY AND HANDLING …

-

APPENDIX

RECOMMENDED SAFETY AND HANDLING PROCEDURE~

FOR LABORATORIES CONDUCTING PCDDPCDF ANALYSES

-24-

Recommended Safety and Handling Procedures in Connection with Implementing

the Analytical Protocal for Determination of PCDOPCDF in Combustion Products

1 The human toxicology of PCDOPCDF is not well defined at present although the 2378-TCOO isomer has been found ta be acnegenic carcinogenic and teratogenic in the course of laboratory animal studies The 2378-TCOO is a solid at room temperature anq has a relatively low vapor pressure The solubility of this compound in water is only about 200 parts-per-trill ion but the solubility in various organic solvents ranges from about 0001 to 014 The physical properties of the 135 other tetra-through octachlorinaed PCDDPCDF have not been well established although it is presumed that the physical properties of these congeners are generally similar to those of the 2middot137 8-TCDD isomer On the basis of the available toxicological and physical property data for TCDOthis compound as well as the other PCDD and PCOF should be handled only by highly trained personnelwho are thoroughly versed in the appropriate procedures and who understand the associated risks middot

middot2 PCDDPCDF and samples-containing these are haAdled using essentially the same techniques as those employed in handling radioactive or infectious materials Well-ventilated controlled-access laboratories are required amiddotnd laboratory personnel enter1119 these laboratories should wear appropriate safety clothing including disposable coveralls shoe covers gloves and face and head masks During analytical operatiqns which may give rise to aerosols or dusts personnel should wear respirators equipped with activated carbon filters Eye protection equipment (preferably full face shields) must be worn atall times while working in the analytical laboratory with PCDOPCDF middot Various middot types of gloves can be used by personnel depending upon the analytical operation being accomplished Latex gloves are generally utilized and when handling samples thought to be particularly hazardous an additional set of gloves is also worn beneath the latex gloves middot (for example Playtex gloves supplied by American Sci-entific Productsgt Cat No 67216) Bench-tops and other work surfaces in the laboratory should be covered with plastic-backed absorbent paper during all analytical processing When finely divided samples (dusts soil~ dry chemicals) are being processed removal of these from sample containers as well as other operations including weighing transferring and mixing with solvents should all be accomplished within a glove box Glove boxes hoods and the effluents from mechanical vacuum pumps and gas chromatographs on the mass spectrometers should be vented ta the atmosphere preferably only after passing through HEPA particulate filters and vapor-sorbing charcoal

3 All laboratory ware safety clothing and other items potentially contaminated with PCODPCDF in the course of analyses must be carefully secured and subjected to proper disposal When feasible liquid wastes

-25-

bullmiddot

( are concentrated and the residues are placed in approved steel hazardous waste drums fitted with heavy gauge polyethylene liners Glass and combustible items are compacted using a dedicated trash compactor used only for hazardous -waste materials and then placed in the same typeof disposal drum Disposal of accumulated wastes is periodicallyaccomplished by high temperature incineration at EPA-approved facilities

4 Surfaces middotof laboratory benches apparatus and other appropriate areas shouldmiddotbe periodically subjected to surface wipe tests using

middotsolvent-wetted filter paper which is then analyzed to check for PCDDPCDF contamination in the laboratory Typically if the detectable level of TCDD or TCDF from such a test is greater than 50ngm2 this iridicates the need for decontamination of the laboratory A typical action limit in terms of surface contamination of the other PCDDPCDF (summed)middot is 500ngm2

bull In the event of a spill within the laboratory ~bsorbent paper is used to wipe up the spilled material and this is then placedinto a hazardous waste drum The contaminated surface is subsequently cleaned thoroughly by washing with appropriate solvents (methylenechloride followed by methanol) andmiddotlaboratory detergents This is repeated until wipe tests indicate that the levels of surface contamination-are below the limits cited middot

5 In the unlikely event that analytical personnel experience skin contact with PCDDPCDF or samples containing these the contaminated skin area should immediately be thoroughly scrubbed using mild soap and water Personnel involved in any such accident should subsequentlybe taken to the nearest medical facility preferably a facility whose staff is knowledgable in the toxicology of chlorinated hydrocarbonsAgain disposal of contaminated clothing is accomplished by pladrg it in hazardous waste drums

6 It is desirable that personnel working in taboratories where PCODPCDF are handled be given periodic physical examinations (at least yearly) Such examinations should include specialized test~ such as those for urinary porphyrins and for certain blood parameterswhich based upon published clinical observations are appropriate for persons who may be exposed to PCDDPCDF Periodic facial photographs to document the onset of_dermatologic problems are also advisablebull

-26-

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BREHM LABORATORY - ~RJGHT STATE VERSITY - DAYTON OHIO 45435 DATE 822184 TIME 15182

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0 0middot 1 1 26

BR Et L A13 0 R ~ l R v - 1 I G Hi STAT UN I Vt R S 1 I - DAYTON 0 H I O 4 5 4 3 5 DTE 822384 TIME 131~1

KRATOS MS25 DSSf SOfTWARE RUN TOR6SS41 WSU NAME CHJ-192828 47 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZOFURANS

254 4 21 5 I 49 7 16 Si 44 100

90

88

78

69

58

u

38

2B

18

B

-t--L- - JJ_L-L---L-_J_~__J-L-L-1-_J_----L-~~_~_____---J____L_______~L-------~

0 376 100Xbull27922

374 1BBXbull34690

4U 10BXbulll US

5B 100 15B 2BB 25BSCAN NUMBER

HRGC-LRMS ANALYSIS OBTAINED FOR CHEHECOLOGV SAMPLE N02D1 F tGURE t 138

I 0 N

I N T E N s I T y

3BB

urn_

98

as

7B

6B

50

uJ

30

2B

1e

B

~--- BREHM L~BORAlORY - RIGHT ST TE IJ)LlVERSITV - 0AVTC~ OHIO (5435

KRATOS MS25 DS55 MASS

s01 1 26

0 392 1SBXbull6B7S97

39B 1SSXbull7512SC

329 1SSXbull2513Sl

SELECTED-ION

254

DATE 02238 ~IMEs 13U SOFTWARE RUN 10R63S41 WSU NAME CHJ-192828 47 CHROMATOGRAMS FOR HEXACHLORODIBENZO-P-DIOXINS

421 5 C9 7 s 16 au

I 0 N

I N T E N s I T V

58 lBB 158 2BB 258 3BBSCAN NUMBER

Hbulldc-LMS A~AL~~i~ OBTAikto FOR CHEMEcolOG~ SAkPLE Ho2bi FIGUREa 139

rt F 1 4

~ BOR A -1 RY JR 1 G H T S l A TI U N I E R S IT - -JAYTON 0 H I O 4 5 4 5 DATE1 0223184 TIME 1349

KRl JS MS25 0S55 SOFTWARE RUth TOR700HJ WSU NAMEa CHJ-192028 47 SELECTED-ION MASS CHROMATOGRAMS FOR HEPTACHLORODIBENZOFURANS

001 1 10kJ 2102 3104 4 I 06 5 I 08 6 1 1 7 13

SCAN NUMBER~RGc-L~U~ A~ALvsfs 6erAlNEB Fo~ c~EMEcoLoGv sAMPLt Ho2bi

FIGURE1 140

100

90

80

7B

6B

5B

48

38

28

lB

0

S 419 100Xbull5537

amp us 10Ubull5735

0 478 lBBlbull(59

432 1BBXbull3837B

2B -B 60 80 lB0 12B U0

I 0 N

I N T E N s I T

V

- - - - -

100

90

80

7B

6B

50

U

30

2B

lB

B

001 1 00

LmL1111 _ UVl1-IVIY

KRATOS MS25 DSSS SELECTED-ION MASS

202

- WKHaHI iTlE UNIVERSITY - OAYTtN CHJO -5435 DATi 02238_-- TIMEr 13r49

SOFTWARE RUN JR70848 WSU NAMEs CHJ-192028 47 CHROMATOGRAMS FO~ HEPTACHLORODIBENZO-P-DIOXJNS

3r04 4r06 5 08 6 r 11 7 al 3

1801bull7B89

1001bull38370

100bull12576

______ - ~ -

1 l

--------~__~___~____A--~----~-_J_J_---__-L~-----1-1-LL+-L-~--lL-_L-L-L-~-L__J-L-L-L-J-L--1__J--L--L-LIJ_J__J_~-A--1-JJ--L__J-__1_L-_+

$ 426 1BBXbull19300

amp 424 lB0bull19678 =~ 0 359

432 J 0 N

434

I N T E N s I T V

u 6B 80 108 128 UBSCAN NUMBER

UlCC-LRMS AMALvsi 6afAtHED ~ol cHtUtcolOGV SAMPLE No2b1 FIGUREbull 141

- - - - -

Tt kl1231i TIME 1ifJ6 lltRAlU rltS25 DS55 S -TJARE RUN TORB0047 Jiu NAMEr CHJ-192028 47 SELEC)EQ-ION MASS CHk0MATOGRAMS FOR OCTACHLORODIBENZOFURANS

odl 6142 7 13 7 44 8 il 5 846 9d7 948 10 r 19 100 ____J-J-L_J L~--L---J-J____~__L-1~__~___________________Ll--L--L~L-~L-__LJ_______ ___-+-________~________~___J_________________~ ~_+-

$ 44 100Xbull5256

90

amp H2 l0Brbull4675 as

0 512 lBBlbull1798 7S

470 1BBXbull113177 68 I

0 N

472 1SBXbulll19359 68

I N T

-48 E N s I T V

3B

2B

1B

B

128 136 lU 158 16B 171 18B lU 2bullbullSC N NUMBER H~GC-LiMs AHALVS1S oATAIHEb loi tHfMEcblOG~ iAM-LE N0201

FtGUREc 142

BttiHr- lWfltl( - liiHt STArEJ-JJIVmiddotmiddotmiddotlP - llAVTON 01110 454j~ -TE 0223 T1ME 1~57 lrv-~ 7-middot

KRATO~- MS25 DS~5 _ IARE RUN TOR40053 WSU NAMEz CHJ-213049 IWI~middot 1

SELECTED-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENZOFURANS

B 13 1 B7 180 ~_______J--1 I

S 306 1BBXbull854354 90

amp 304 l00Xbull605297 8B

0 374 l08bull538 70

328 l00bull187587 60

332 lB0bull48368 58

u

30 ~ 28

18

B

18 58

214 322 429 537 6 44 I t_LL-J I ~L____amp_________________~~-t-

lBS 1 SB 280 251 38 SCAN NUMBER

I 0 N

I N T E N s I T V

H~Ct-li~i i~~~~sis 6bullt~i~t~ ~oi ~HiMicot~G~ s~M~i~ ~ozb~ F IGUftE bull 144

BREHM LABORATORY - JRIGliT S7ATE U(IVERSITY - )A(JN OHIO 45435 DATE1 022384 TIME 1457

KRATOS MS25 0S55 SOFTWARE RUN TOR40050 WSU NAME CHJ-213049 SELECTED-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENZO-P-DIOXINS

0d3 1 07 214 322 429 5137 61U H LJ___i

S 3~~X-SS0126 ~-J--~1~~ I90

amp 320 lfSXbullbulltbullaabull 80 J

0 257 l00yenbull12107bull9

70

328 10SXbulll87507 69 I

0 N

332 l00Xbullbull8368 5S

I N T Eu N s I T30 y

2B

10

g

fl

-11 -1 r J l___j ~-------

I

r

10 50 100 l 50 SCAN NUMBER

200 250 3SB

HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE NO202 FIGURE 145

bull -BREIIM t_middot middotJPATOkY middot R ~~iT ST~E UNI ITV - ~ATON (HO 45435

middot-1 _- 022384 TIME1 1506 KRATOS MSS 0S55 S0f jw~RE RUN TOR50~41 WSU NAME1 CHJ-213849 SELECTED-ION MASS CHROMATOGRAMS FOR PENTACHLOROOIBENZOFURANS

0 01 --L-J

1 03 I

2 06 I I I

3 10 I

4 13 5 17 620 7s24 8127 I l-L_J__L_______--------_~_~~L--____J______-t-

0 340 l00bull708382

338 1BBl 43537

408 10BXbull 1 U8

I

I 0 N

I N T E N s I T V

8

5f 188 158 28B 25B 38B SCAN NUMBER

ubull~t-LIUsect AHAlVsis bltifUi6 Joi CHIUfcoligtGv UUJlf Uo2b2 F tGURE a 146

35B U8

BREHM LABORATORY - WRIGHT STATE U~IVERSITV - DAYTON OHIO 45435 DATE 022384 TIME 1506

KRATOS MS25 0S55 SOFTWARE RUN TORS0041 WSU NAME CHJ-213049 SELECTED-ION MASS CHROMATOGRAMS FOR PENTACHLORODIBENZO-P-OIOXINS

0 0 l 1 03 2 l 06 3 I 10 4113 5r17 6120 7124 8127 100 ~ I ~

O 356 1B~Xbull417382 90 J

35-4 100Xbull258056 I 80 -+

291 18Ubull5BU23 7S I

I

2 60

50 [ i I ~

I T-40 y

3B

20

10

s

5S lSB 15B 200 250 308 358 us SCAN HUMBER

H~GC-LiMs ANALvsis OBTAIHfb ~~ CHEMECOLOGV SAM~LE Hoib2 FlGUAEs 147

hiElbullmiddot ABOPATG - Gll ~1ATE LtERSITY - DAYTON OHIO 45435 _ c E 0 2 2 3 8 4 TI ME 1 5 1 6

KRATO~ MS25 DS55 SOFTWARE RUN TORGff042 WSU NAME CHJ-213049 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZOFURANS

BiBl l 26 254 421 549 7 I 16 8U lBB bull -1-~__J_j__ bull ~-------J-J~____________~-----J--L-----1--amp--L--J-J-J-_l--_L--L -amp-L--I-JL--J-________~___-___________--4_______i_J _____--+-

90

80

1B

60

58

41

38

2B

18

B

I I I r-

t I ~ I L

58

0 376 100=73047

374 1BBXbull63Bl2

bull tU lB01bull7tB

I 0 N

I I N T E N s I T V

UJ0 158 2BB 250 3BB SCAN NUMBER

H~GC-LRMS ANALYSIS OBTAINED FOR CHEHECOLOGV SAMPLE NOZDZ FIGURE1 148

40

l)ftHM LAlHJKAIUtltY - WKHiHI gtIAlt UliiVtK)T - LJMr1v1middotbull uruu ~ jJ

DATE 022384 TIME 15116 KRATOS MS25 0S55 SOFTWARE RUNs TDR60042 WSU NAME CHJ-213049 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZO-P-DJOXINS

001 1 26 254 4 21 549 7 16 8 44 100

90

80

70

60

50

30

2B

10

B

L - 1--------l--L---1---__J-_____

O 392 l00Xm574544

390 l00Xbull714164

329 l00Xbull231249

1 1 E

N s I T y

t

5B lB0 150 200 258SCAN NUMBER

HRGC-lRMs AHALYSis bttAtNE6 tolaquo CHEMECOLotv sAM~LE Ho2b2 3H

_________~____---___--~---J--___-----r----L-1----1-J_l-___I-L-LL----1-~_~-L-- L__J___1-_-L__--L_--__l-L-L-L--l-L__J___1-L-L----I-L-L-l-

- - - - - - - - - - - - - - - -t-I

I ~ 0

~ N

l N T~

F IGUFlE t 149

180

98

80

78

6B

se

t8

3B

28

18

B

BdH 1 BB

BR1J1 oCiKATl Y - lJGl11 ~~-TE t~-~Rlt11 v - lAVTON ()HlO 454-5 LTE 021236middot middotmiddot1r-iE~ lfi25

KRATO MS25 [LoS _ fwARE RUN TOR70041 WSU NAME CHJ-213049 SELECTED-JON MASS HRO~ATOGRAMS FOR lfEPTACHLORODIBENZOFURANS

2 02 3 04 4 86 5 08 6 11 ~ I ~ ~

S ~IS 1BBXbull112Bl

amp U-8 lS8bull

1 2B U u aSCAN NUMBER

HAGt-LRMs AHAL~iit ba1IHE0 toRmiddotcH~MEcoLoG~ 188

sAMh~ Ho2b2 128

FIGUftE 1 150

7 13

lU

I 0 N

I N T E N s I T V

I I

I

I

I I-

BREHM L~BORATORY - WRlGH~ ~TAl~ UN1~K~11Y - UA~l0N UHU 4b4Jb DATE e22384 TIME 1525

KRATOS MS25 DS55 SOFTWARE RUNt TOR70041 WSU NAME1 CHJ-213849 SELECTED-ION MASS CHROMATOGRAMS FOR HEPTACHLOROOIBENZO-P-DIOXINS

0dH 1100 2 02 384 4 06 5108 6 il 1 7 t 13 100 l --L~-______________~_------_________~_------___ _____________~_----1-1-J--l-L-l-l-J--L-1--l---l--middot~_1-JJ-L--l--Jl---l-L-LJJ-l---l-L-L-L------L-J--r---~-______________~+-

$ 426 l00Xbull59017

90

i I

~ 424 l00tbull61230 80

0 359 130ibull19179 78

432 1B0Xbull21734 60 i I

0

i 434 l00Xbull6376 50

~ 1 NI~

i N

I T I- E N

40

s T V

30 II I

I

r 23 I

~-

Ill

I-i

il16 ~II

I 0

I~ I I

20 U 60 80 lBB 12B SCAN NUMBER

HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGY SAMPLE NOZD2 FIGURE 1 151

140

18

riRpound1d bullA80KA 1 i1RY - 1dGHl 3f)r INIVErltSTY - [JAYION OHIO 45435 _TE kf22_ 4 TIMEr 15~~9

KRATOS MS25 0S55 s~iTWARE RUN TOR80S~8 WSU NAME CHJ-213049 SELECTED-ION MASS CHROMATOGRAMS FOR OCTACHLOROOIBENZOFURANS

611 642 7 13 744 8 15 846 9 17 948 10 19 1HH L----J~ ----L-L--L_~~~- L 1--l-J_l--------1-JJJf____________ JL-L-L-L-L----L-i_ --4--1--1--JL-JL-L-~~~~~~-------_______+-

$ 444 UJ0Xbull5Sl 1

90

amp U2 10BXbull606 es

0 512 l001bull2796

7B j= H0 l001bullU779

60 L j

t72 l001bull8168 5B

u I 3B

20

B

128 13B 140 15B

J 0 N

I N T E N s I T V

1

I I I I I I

160 17B 188 UB 2BB SCAN NUMBER

HRGC-LRMS ANALYSIS OBTAINED FOR CHEHECOLOGV SAMPLE N02D2 FIGURE 1 152

-- - - - - -- -

------------ ---- _______ ----

middot0

10

HJ

7g

60

50

40

30

2f

10

B

bull

1

16 l 1 642 7 13 7144 8 15 846 917 948 10119

middotmiddot---~~~L~~~~-bull -bull-~- ~ L ~~

BREHM LABO~~TU~V - WRGHT STATE UN~~RSlTY - C~YTON OHIO 4b~~b

DATE 022384 TIME 15139 KRATOS MS25 0S55 SOFTWARE RUN TOR82048 WSU NAME CHJ-213049 SELECTED-ION MASS CHROMATOGRAMS FOR OCTACHLORODIBENZO-P-DIOXINS

~~~l_____~~~- - - - - - - - ~ 0 395 l00~bull21669

I

N 10 100x 4779

-+ I

02 l00X=-48168 ~ II

l Ii i tIl

l

_JfI

120 13S 140 lSS l6B 170 18B 190 2H SC N NUMBER

HRGC-LRMS ANALYtts OtiTAIHED FOR CHEMECOLOGV SAMLE H0202 FIGURE 153

I 0 N

I N T E N s I T y

I

--~~ 811tHmiddot - ultATO t - r middotcHT ~~rmiddotTE --_VEKSiT - OAtTON vHIO -45435 rmiddot middot middot i ~ 2 2 3 8 f I ME 1 i 1 q

KRATOS MS25 DS5 SC bullJARE RUNi TOR40051 IJSU NAME CHJ-22 SELECTED-ION MASS CHROMATOGRAMS FOR T~TRACHLOROOIBENZOFURANS

BdJl 1 iB7 214 322 429 5137 6 44 lBB

~ S 306 100bull860

_L9B

amp 38-4 1BBlbull787es

1j

ut

51

U

38

2iJ

IB

0

0 37-4 1

328 I

bull 332 1

_ 378 I 0 N

I N T E N s I T V

58 lSS 15BSCAN NUMBER

21611 251 3BB

HRGC-LAMS ANALVits OBTAINED FOR CHEMECOLOG~ SAMLE No202 FIGUREbull 154

- - - -

BREHM LABORATOR~ - WRIGUT STATE UNIVRSITY - DAfON OHIO 4bbull3b DATEr 022384 TIME 1618


OdH 1107 2 I 14 180

5 100Xbull10B832 rimiddot90 - - - - - - - - -1- -

amp 328 l0SXa798 ~ 80

0 257 100Xbull878

7B

328 1B0Xbull195851 60

SB

40

3-J

2S

1e

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322 ~29 537 6tU

l ~ VVf Y

IJ 1

I

-2378

--f- --I 0 N

I N T E N s I T y

58 1B0 1 50 200 258 3BB SCAN NUMBER

H~GC-LRMS AUALvsf bBTAiNED Fok CHEMEcOLOG~ ~A~Lt N0202 FIGURE 155

a ff ampstmiddot --~

-----_

[-ciil 3ORT- - middot G~f r 1-fl L EtLi rt DAYTCI OHIO t5~3J rrE 0212384 fJMI lf27

KRATO~ MS25 OS55 ~Ui TYARE RUN TOR500~2 WSU NAMEs CHJ-22 SELECTED-ION MASS CHROMATOGRAMS FOR rENTACHLORODIBENZOFURANS

BsBl 1 03 2106 310 13 517 62S 72bull 8127 100

0 3B

I bull I

10SJbull846

I I I I _l_______l_______J_ __ J _____L_ I _l ___J_ ___ J _ _j____J_ I I l I _l _ _1 I I I

I 9B -+- - - - - - - - - ~ - - - - - - - - - - - - - - - - - - - - - - - -

338 lBByenbull596

81 ~---- - - - - - l - - - - - - - - - - bull--+-

11 4B8 lBBIbull 193 I

I 0

II - ~ V ~

N

I N u

u j i ~

r

A~ II il iJIIV Ill~

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I- hi~M tJ

~- JlB J ~ I~

V I r IIIJ ~ ~

I 1 1 I 1 1 I r --------------~-- --- --r---y~- --- 1 - - -- I I I I I I I -T -- I I I I I I I I -f

6B lBB 15B 200 25B 3BB 35B 4BB SCAN NUMBER

HNGc-L~Ms ANALvsfs barAiNEo FOR cUEMEcoLotv sMPlE Hozbz FIGUllEa 156

BRfYM LABORATORY - WRiGHT smiddotAn UNIVERSIIY - DAYTON OHIO 45435 DATE1 022384 TIME1 1627

KRATOS MS25 0S55 SOFTWARE RUN1 TOR50842 WSU NAME1 CHJ-22 SELECTED-ION MASS CHROMATOGRAMS FOR PENTACHLORODIBENZO-P-DIOXINS

8101 l 83 206 3 18 4 13 5 I 17 6128 7124 8127 l0S

0 356 l00Xbull200 90

354 l00Xbull469

80 ---i I

291 lBSXbullamp877 78 ~ I

0 N

68 I N T E

BB N

s Iu T y

38

28

18

0

58 10S 15B 2BB 258 300

~

358 u SCAN NUMBER

HRGC-LRMS ANALYSIS OBTAINED FOR CHEHECOLOGV SAMPLE N0202 FIGUftEr 157

r-----_ BRLH1bull j()Rmiddotbull 1 f -

KRATO~ MS25 OS~5 SELECTEJ-ION MASS

0dJ1 1 r 26 254

i- IGHbull STATE --_f ~17( - DAYiJN OtHO 45435 rE 02231 dME lbl

ufTWARE RUN TOR60043 WSU NAME CHJ-22 HROMATOGRAMS FOR HEXACHLORODIBENZOFURANS

421 549 7 a 16 844 li0 ~L-L-J__L--_______~_j_J_L___J I I I I

0 ~~6 ~BIJXbull3~2__ - - - - - - - - - - - - - - - - - - ~90

374 IBBXbullIB625 - - - if - - - - -8B

H4 1BIXbull07 7B

] 0 N

6B ] N T E N

50

s I T V

3e

2B

lB

B

5B lBS 15B 2BB 25B 3BB SCAN NUMBER

HAGt-lRMS ANALVils oiiAiNE6 ol c~fMEcotoGV SAMPlpound ko2bz FIGUflEa 158

68

BREHM LABORATORY


0 I 0 1 I 26 2154

- WRIGHT STATE U~IVERSYTY - DAYTON 0rtlO 4543~ DATE 0l2384 TIME1 16r37

SOFTWARE RUNr TOR60043 ~SU NAME CHJ-22 CHROMATOGRAMS FOR HEXACHLORODIBENZO-P-DIOXINS

4 21 5149 7 I 16 urn

90

80

70

50

40

30

20

10

s

_J_J_ ___________~_____ J__J____-----L---~ __-L-______~____________------------L--LJ__-L--L-l-L--L--1--1-__-L--L-J----L--L--1-1-L~--J~

0 392 l00Xbull3594

390 l0SXbulll4026

329 10Ubull3518

5B 1BI 150 2BB 25B SCAN NUMBER

HRQC-LiMS AHALVi1sect barA~Eb Foi CHEMtcoL~v SAM-LE ~0~02 FIGURE1 159

8U

I 0 N

I N T E N s 1 T y

3BB

H~ HORAT- middot - - GHT Sl middot7f~iHVEHS - middotmiddot - DtYTON uHIO 45435 middot middotq= JJ2 I 2 3 - TI t-1E 16 - S

KRATOS MS25 DS5 v VARE RUN fOR 76B42 WSU NAME s CHJ-22 SELECTED-ION MASS i_HROMATOGRAMS FOR HEPTACHLORODIBENZOFURANS

BdJl 1 0J 2dJ2 3 04 (dJ6 5 08 6 s11 713 100

90

80

70

I61 0 N

SB I N T

u E N s I

3B T V

2B

lB

B

2S 12B 14B

S ( 10 l00bull2682

amp (88 180Xbull12ZC

0 HB UJ11bull37-

UZ 1BBXbull9786

I

4B 6B BB JBBSCAN NUMBER

HkGC-LIMsect AU~lvsectis 61fAfUE6 olaquo cUEMEcbl66v sAMLf Ub~62 ~ IGURE s 160

DATE 022384 TIME 1646 KRATO~ MS25 0S55 SOFTWARE RUN TOR70042 WSU NAMEi CHJ-22 SELECTEu-ION MASS CHROMATOGRAMS FOR HEPTACHLORODIBENZO-P-DIOXINS

001 1 00 2 02 3t04 bull i 06 508 6 d l 7 l 13 10~

90

80

70

68 I 0 N

50 l N T

U E N s I

30 T y

20

10

0

2B 4B 60 es 1s0SCAN NUMBER

HRGC-LiMs ~UAlvsectts bfiAiHE6 Foi cHtMEcoLOG~ sAMPLl Ho2b2 FlGUFtE1 161

J__l_~J---------__L-____J-___________L-+-J_-----J--------~__~________-L-_LI--L--------------l------J-~J--------L___________~_ ________________L-____________~~-----

$ _26 l00XbullH5

amp 42 l00Xbull817

0 359 100bull2630

12B 1-48

v---fJ

r

1-11Hll LAl3l1i--middot middot bull -bullidGHf smiddotIATE-tllrEiSITV - DAYTON OHIO 45435 ~~TE D223 TIME lt58

kRATOS ~S25 D~SS ~ ~TWARE RUN TOR80B49 w~u NAME CHJ-22 SELECTED-ION MASS Ln~OMATOGRAMS FOR OCTACHLORODIBENZOFURANS

6dl 642 7 13 744 e 1 s 846 9s17 948 10 19 10B

90

80

70

60

50

u

3B

20

10

B

l--LLL-L-L-JL IL-L-J --1~ I I J_____-~--L---_____-+- __J----------__J~L----L-1--LJL-J_J-J~J-_L___________i--1~____Jc---L--L

S -4U 1001bull764

amp HZ 1BBXbull1295

0 512 lBBIbull 1077

47B 1081bull26737 I 0 N

I

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N

I T V s E

N

r 1 4 I

148 150 160 170 180 198 280SCAN NUMBER

HRCt-L~MS AUALYis oifA1NED FOR CHEMECOLCgttiV SAHPii Uo2b2 FIGURE 162

12B 13B

BREHM LA~ORATORY - 1R4G~T STAfE tNIVERSITY - DAYfON OHlCJ ~b4jti

OATE1 022384 TIME 1658 KRATOS MS25 0S55 SOFTWARE RUN TOR80949 WSU NAMEs CHJ-22 SELECTED-ION MASS CHROMATOGRAMS FOR OCTACHLORODIBENZO-P-OIO~INS

6 I 11 61(2 7 13 7 44 8 I 15 8146 9d7 9 l (8 10i19 00 _ _ __ ______________~___--~_____-L-J_______l___i-----l-L-___________________________________J__JLL-l---__+-------~L-LLL-LJ-L-poundJ--L---l--JL-JLL-~t-~l-~-4--~-J--------~----------__--

98

80

78

$ f62 100yenbull676

amp se lBBXbull(25

0 395 1BUbull5t6

47B 1SBXbull26737

472 lB0bull27937

I63 0 N

50 I N T E N

40

s I

3B T y

ZB

1e

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12B 130 140 15B 16BSCAN NUMBER

170 18S 19S ZBB

HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE NO202 FIGURE s 163

BREh ASORAmiddot_ - 1 dSH1 -STA__JiHVtRL middot- ~AVON OHI~ 4543c LAIE JJh- A TIME Ui24

KRAlu MS25 0S55 SOFTJAkE RUN TOF400CJ2 SU NAME CHJ-4674 SELECTpound0-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENZOFURANS

8101 9B7 l011( 1122 1230 1337 1( (5

BB

9B

SB

1B

6f

SB

u

3B

28

lB

bull

S 386 1081bull816

amp 3Bt 1BBXbull6B8 - - - -0 37-1 lBB1bull289

328 1flXbullUB76

J

5f lBB 15BSCAN NUMBER

2BB 250

I

r r

388

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HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N0201-MS-F FIGURE 1 264

ERitJlof LABO~TOtV middotmiddot JPlGHi 7ATE UNImiddotVERSirY - uAYTOh OHIO ~5435 DATE 0V1084 TIME l5s24

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58 lBS 150 SCAN NUMBER

2BB 250 JBS

HRQC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N02D1-MS-F FIGURE 265

BREHtl 1-RORAT-~ - iRIGHT STAT~middot t=~ilT - 0AYTOif OHO ~5-43fJ -- [ATE 0410 TIME 15r33

l~RATG-_ MS25 0$55 so~TJARE RUN fOF50002 WSlJ NAME CHJ-4674 SELECTE1-[0N MASS CHROMATOGRAMS FOR PENTACHLORODIBENZOFURANS

BdJl 1 03 207 3 11 4 15 520 6125 728 8132 U0

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338 1881bull429

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HRGC-LRMS ANALYSIS OBTAiNED FOR middotCHEMECOLOGV SAMPLE N02Dl-Hi-J FIGURE 1 266

0Ttr JU1084 TIME1 l5s33 KRATOS MS25 0S55 SOFTWARE RUNt TOFS0002 1 WSU NAMEr CHJ-467 SELECTED-CON MASS CHROMATOGRAMS FOR PENTACHLORODIBENZO-P-DIO~INS

SdJl l dJ3 2 I 07 3amp11 5120 6125 728 8s32I 15 Ul0

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291 l8UbullUB8 71

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H~CCbullL~MS ANALVSJS OBTAINED Oft CH~COLOGV SAMLE N0201-HI-F FIGUREbull 267

~1EI-I~ bullABOPAT~~y - bulldGI-H 1AT--~IVERSITI - uYTON OHIO 45435 DATE B410_ TIME 1643

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01Bl 1 I 26 254 423 551 7s19 8146 us

0 376 1001bull59-6 9B

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HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N0201-MS-F FIGUREbull 268

Bf4

90

80

70

60

50

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30

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0

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2154

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4s23 551 7 l 19 8146

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0 392 10Ubull54H

390 1001bull14367

329 1BBXbull8761

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5B lBB 160 ZBB 25B SCAH NUMBER

HRc-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV siULi ko201-Ms-F FIGURE 269

1J~ ~JV

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0101 1 00 202 3 06 4108 Sill 613 i

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HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N02Dt-M1-F FIGURE 270

r--rr

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1

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0 359 lB8bull6186

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8101 1100 2 I 02 3 I 06 4 108 5 r l l 6 I 13 7116 100

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HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N02Dl-M6-F FIGURE 1 271

l 0 N

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------~-IV ~ ~J

BREHh A3iiPATOR - ~bull1-GHT STAT --ir-1~~1middotrmiddot( middot DAYTON OHIO _54Jti -TE ~ 4 10 6 T I ME 1 6 0 4

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502 5H 6 i05 6s36 7 amp168 739 8 sl0 8s41 g 12 lBB

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tfflQCbullLRMS ANALYSIS OBTAINED fott CHEMEcolocii iAMLi Ho2ni-Mi- FIGURE 272

S 4 U UJBXbull2855

amp U2 lB81bull2666

- - - -0 512 l881bull7Z61

47B 1BBXbullZl624

472 1BBXbullZZ527

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5 02 5r34 605 6g36 7 108 739 8 10 8 g 41 9 r12 100

90

80

70

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S 460 100Xbull2953

amp -458 l80Xbull2661

0 395 1SUbull2198

470 1SSXbull2162

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SCAN NUMBER HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE HO2D1-MS-F

FIGURE 273

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Gl[tlf-l LJcl0RAH Y middotbull bull~hmiddot~- S(AiE-JVEKSltY - 1Avl)1 1 01110 45435 ~~lE 0382 TIME 132n

kiATU fS25 DSS SulHIARE RUN TOR4fJHi6 WSU NAME CliJmiddotmiddot-tB75 SfLECTE0-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENZOFURAHS

0 l 0 1 1 fJ 7 2 l 4 3 2 429 537 644 UHJ J - L- _L __ J_ __I __ ___ - L _J ___L I __ _middot- 1bull1 - I J _ L l L -11_____1 ---l-J -~ l L J_ middotbull---L-- I __J_ -bull--11 _ __ J_ -bullmiddotmiddot l-1- middot--- L _j _ l J L L J __ __ L-- _I L-1 _J__ J ___ L___ -

$ 306 H0Xbulll700if li-2378 l 90 -- - -- --- - - --middot - --middotbull - -- --middot --- middot- -- - - -- middot11 - -- -

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SCAN NUMBER HRGC-LRMS ANAlVsis OBTAiNED FOR CHEHECOlOGV SAMPLE N0202 H5 F

FIGURE 274

58 3BB

90

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KRATOS MS25 0S55 SOFTWARE RUNs TOR4mB76 wsu NAME CHJ-4875 SELECTED-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENZO-P-OIOXINS

0dJ1 11 B7 2 tl 4 3122 4129 5137 6144 100

80

7B

6B

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2B

lB

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amp 320 UUbull12126

0 257 10BXbull2Sss

328 1SBXbull18B436

bull 332 1BBXbull139676 2378-

_______ II w ~

_____---=----~1 t-------t 1-----l-- 1 1 I -r---middot--middot 1 i 1 1 --c-r-r ri---rl middot1 middot - t

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50 lB0 158SCAN NUMBER

20H 250 308

HRGC-LRMS ANALVSIS OBTAINED FOR CHEMECOLOGV SAMPLE N0202 MS F FIGURE 275

si

BP-EHfi Al3ORAf middot - JPiGHl 5TAi ~ ~IVUlTY - DAY1Cf( DHO 46435 ~~TE ~3~1middot TIME 1329

KRATC~ MS25 DS65 ScfTYARE RUN 1OR5m064 wsu NAME CHJ-4875J SELECTED-ION MASS CH~uMATOGRAMS FOR PENTACHLORODIBENZOFURANS

Bs01 1 03 2 06 31 HJ 4 13 5 17 6120 7r2~ 8127 100

98

88

78

68

38

28

18

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0 348 1BBXbull19517

338 1801bull12581

bull 4B8 lB81bull516

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1 5B lBB 168 2BB 25B 3BB 351SCAN NUMBER

Ui~~-llUI AN1lvsil bifAfUfB o1 EUfUlcol6iY l~MJll Uo2b2 Ml FIGUtl~bull 276

01Bl 1 a03 190

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354 1BBbull11BB2

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68

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BREHM LAeORATORV - ~~l~ltT STATE UNIVERSlTi - DAY~LlN OHIO s35 DATE 030284 TIMEs 13129

KRATOS MS25 0S55 SOFTWARE RUN1 TOR5SH6 WSU NAME CHJ-4875 SELECTED-ION MASS CHROMATOGRAMS FOR PENTACHLORODIBENZO-P-DIOXINS

bull

2 l 06

1BB

3d0

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4 r13 517 6120 7124 8127

2BB 25B 3BBSCAN NUMBER

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35B ubull HRQC-LRMS AHALVSIS dBTAIHEO FOR CHEMECOLOGV SAMPLE N0202 MS F

FIGUFlEs 277

ERE4M lAIWRATORY - RIGHT ~-S-4middot-rElSITY - DAVTOt CtilO ~~435 DATE 0~ili2 TIME 1339

KRATOS MS25 0S55 SOF middot-JARE RUN I TORG0065 WSU NAME s CHJ--48 75 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZOFURANS

B81 126 254 421 549 716 eu 100

0 376 100Xbull8363 9f

374 1BBXbull2488

8f

bull 4U 1BBlbull133 1B

6B

51

46

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Uiamp~-llMs ANALVifsect 6lfAiHEb ~oi cM~MtcoLbGV sAU~LE Hb202 Ms F FIGURE 278

I 0 N

[ N T E N s [ T V

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0ATE S3B284 TI~Ea 13139 KRATOS MS25 0S55 SOFTWARE RUN1 TOR6BB65 YSU HAMEs CHJ-4875 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZO-P-DIOXINS

BdJl 1 26 2154 100

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as

70

bull

398

329

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l88rbull2616

6B

58

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58 108 158 288 258 3BB SCAN NUMBER

HUc-LR4S Af(AL~sfs oaHiUEo FOR CHEMECOLOGV HMHE Uo262 Ms r FIGURE 279

Li1-U1r LAUVKA1( l

l i

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OSS5 MASS

0101 l 1BB 2 02

0

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SOFTWARE RUN TOR700E6 JSU NAME CHJ-4875 CHROMATOGRAMS FOR HEPTACHLORODIBENZOFURANS

304 4 dJ6 5dJ8 611 7 ll3 IBB

98

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68

68

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2bull bullbull bull

J_j_J L-l~___j__LL________J__~--L~1-- I le I J_J___J_L I I I -L-i~-1__t_J

$ -tlB lBBKa-699

amp cee 1snbulls119

0 478 lB81bull618

bull 32 1bullbull1-sbull11

bull 34 1bullbullr-1s2

1~

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2B s 6B SB lBB 128 UBSCAN NUMBER

UR6~-Li~I ~Rilvsectfsect ld1i~lo 61 cUfUttampigtlv s~UJll Ulaquoia2 Mi F FIGURE 280

BttrnM LABORATO~V


0101 1 100 2 d32

middot- URir~T STATE UIUVERSIf - DAriON OHIO 45435 DATE 030284 TIME 13147

SOFTYARE RUN1 TOR0866 YSU HAMEi CHJ-4875 CHROMATOGRAMS FOR HEPTACHLOROOIBENZO-P-DIOXINS

3s04 4 dY6 5 I 08 6 cl 1 7 I 13 100

90

80

78

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SB

40

30

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lB

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----L----J-l----1-__~____ _ __________~~__---__-~_ _______________~____~_____~_________J_1---L----L-4---1--------_~--- __-________--1i-- ______~~__~--

$ C26 l0Ubull7199

ampr C24 l00bull6679

0 359 1B0Xbull5150

t32 100Xbull-SB17

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2B CB 60 es lB0 120 SCAN NUMBER

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I N T E N s 1 T y

10

HRGC-LRHS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N0202 HS F FIGURE 281

P EHM LBORAfORmiddot - ibullmiddotmiddot ~HT - bullTE u~stY - iAYTON (HIIO 1b43r 1 _ E ff 3 0 2 f11 T I ME ) 4 ti 3

KRATOS s2s DS5poundi SOt I wRE RUM 1 OR80072 ISU NAME CHJ-48 i5 SELECTED-ION MASS CHROMATOGRAMS 1-0ll OCTACULOROOICENZOF IJRAUS

6 11 642 713 7144 815 846 91 9 ~ 8 l019 lfl0 bull I - I -bull I - middotmiddot l -- I 1 L L--1 L 1 _ I _J_ L--lJ __ ___ f lbullL L_J Jbull L J_J L I Imiddot--middot L 1-1J bull L-_

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HRGC-LR~S ANALYSIS OBTAINED FOR CHEHECOLOGV SAMPLE N02D2 MS F f IGUREr 282

------------------------ -~ --- ----- --i

middotr-- I --r- middot-middot r--- -middot-1-- rbullmiddotmiddotmiddot -----r-rmiddot j

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DATE 1 030284 TIME 14 03 lltRATOS ~S25 0S55 SOFTWARE RUNs TORB0072 WSU NAME CHJ-4875 SELEcmiddotrED-ION MASS CHKOMATOGRAMS FOR OCTACHLORODIBEHZO-P-OIOXINS

6 l 1 642 l 13 7 44 8 I 15 846 9 I 17 9148 10 l 19 lJj(T

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30 ---- --- - -- -- middot-- - -11r - - -amp 458 10~X~l5408 - -- -- -- -- -middotmiddot -

120 139 140 150 160 SCAN NUMDFR

17~ 180 190 2BS

HRGC-LRMs AHALvsis oerAiHEo FoR cHEMEcoLocv SAHPLE NO202 MS F FIGURE 283

80 O 3 l0flXm90U

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middotbullI

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BREHM LABORATORY - WRIGHT STATE UNIVERSITY - DAYTON OHIO 45435 DATEs B3B284 TIMEbull 1Br51

KRATOS HS25 0S55 SOFTWARE RUNr TOR4BB74 WSU NAMEbull CJ-68 SELECTED-ION HASS CHROMATOGRAMS FOR TETRACHLORO0IBENZOFURANS

B12B 11B7 2 14 3r22 4 I 29 5137 61H 10B

9B

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0 374 lB91bull562

bull 328 1BBXbull161~37

I 332 1BBlbullll~623 ~

15 50

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SB I N T s E N s I T V

30

20

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f6

180 15B 2B~ 250 3BB SCAN NUMBER

HRGC-LRMS ANALYSIS OBTAiNED FOR CHEHECOLOGY SAMPLE NO2A1 17 F FIGUREr 433

L L Ht - BoRA r o R Y - middotr-i G H T s TAT E u N I v ER s If Y - oAv 1 o N bull u IiI iJ 4 ~-~ J 5 DATE1 030284 TIME l0151


100 B 20 1107 2 14 3122 4 I 29 5137 61U

S 322 1BBXbull1B4988 90

80 amp 320 l0BXbull8158

0 257 lB0bull51649

7B

6B 328 1BBXbull161437

SB 332 l0BXbulll17523

u

38

2B

lB

0

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3BBl0B 150 280 250SCAN NUMBER

wlc-LUI AUAlvlil biiAiUi6 deg CHEUfcol6Gv sMJLi Uo2Al 17FIGURE 434

15 50

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98

80

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338 1081bull59894

488 108bull393

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BREHM LABORATORY -


2106 3110

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WRIGHT STATE UNiERSITV - DAYTON OHIO 45435 DATE 030284 TIME llaBB

SOFTWARE RUN TORS0062 WSU NAMEbull CHJ-68 CHROMATOGRAMS FOR PENTACHLORODIBENZOFURANS

4 r13 517 6120 I

7124 8127

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I 58 10B 150 200 250 3BB 35B

SCAN NUMBER ~RGc-LlMs AHAL~sis barAiNEb roi tHEMEcoloGv sAMI-LE Ho2A1 ii F

FIGURE1 435

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L~ii 1-i-il1U 1~Alui - I1a11i middotIA illpoundRSllY - fl1Fideg(I lJHIO 45435 C~TEt B3B284 TIMEs 1108

KRATOS MS25 0S55 SOFTWARE RUN TORS0062 WSU NAME CHJ-68 SELECTED-lON MASS CHROMATOGRAMS FOR PENTACHLORODlBENZO-P-DIOXINS

100

90

80

70

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291

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HRGt-LRMS ANALVSIsect OBTAINED F~ CHE~Ecolo~ SAH~LE H02Al 17 F FIGUREbull 436

middot-

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2 5 ( 4 2i middot 5 l ( 9 7 I 1 6 eu 100

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HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE N02Al 17 F FIGURE 437

BREHM LABORATORY - WkIGHT STATE UNIVERSITY - DAYTON OHIO 45435 DATE 030284 TIME1 llslZ

KRATOS MS25 DS55 SOFTWARE RUN TOR6Hg63 WSU NAME1 5 SELECTED-ION MASS

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4 21 549 7 I 16 su I

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50 lBS 158 289 258 3BB SCAN NUMBER

wl~t-L4As ANALVsectfsect UiiUl6 deg cHEUfc6l6Gv sUJle MoEHJ-e FIGURE t 438

if

middotmiddot~ci__f --middot -~ ~ ~

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SREliM L~BORATORV - WK[GHT STATE UNIVERSITY - UAYTON OHIO s35 DATE B3B284 TIME 11118

KRATOS MS25 DS55 SOFTWARE RUN1 TOR7BB64 WSU NAMEbull CHJ-68 SELECTED-ION MASS CHROMATOGRAMS FOR HEPTACHLORODlBENZOFURANS

BdJl 1 bullBB 2102 3dU 4106 5108 6sll 7113 lB0

90

as

70

6B

5f

u

31

2B

11

B

S 41B 1BBlbull88U

amp 4B8 l0BXbull9116

0 HB U81bull1319

432 l00bull35776

2S 4B 6B BB 198 128

I 0 N

I N T E N s I T y

us SCAN NUMBER

Ui4t-llaquoMs ~~Al~sfsect 61fAfUE6 Fol cHfUfcblbtY sAkPLt Mo2i j7 FUWREs 439

-

t

BREHll LABORATORY - VPIGHT STATE UNIVERSITY - DAYTON OHIO 45435 DATEr 038284 TIME 1118

KRATOS MS25 0S55 SOFTWARE RUN TOR70B64 1 WSU NAME CHJ-68 SELECTED-ION MASS CHROMATOGRAMS FOR HEPTACHLORODIBENZO-P-DIOXINS

Sa01 1 es 2 I 02 3r04 41B6 Sr08 6111 7113 100

90

as

7B

68

SB

U

3B

2B

10

g

S 426 10BXbull11647

amp 424 1BBXbull1195B

0 359 100yenbull8992

02 100Xbull35776

434 1SBXbull11738

U 61 8B 1B0 120 1482B

I 0 N

I N T E N s I T V

SCAN NUMBER HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE NO2Al 17 F

F GUR E 1 440

~

BkEHN L~BORATORY - WRIGHT STATE UN ~RSITV - DAYTON OHIO 45435 DATE 830284 TIME1 11133

KRATOS MS25 0S55 SOFTWARE RUN1 TOR8B069 WSU NAME1 CHJ-68 SELECTED-ION MASS CHROMATOGRAMS FOR OCTACHLORODIBENZOFURANS

6111 6142 7113 71U Br15 8146 9 al 7 9148 18bull 19 0B

98

80

7B

60

50

u

30

2B

lB

B

S 4U 18Ubulll 922

amp HZ 1BBXbull3928

0 512 18BXbull2298

47S l00Xbull99315

bull 472 1BBbull1B6B78

128 13B 14B 158 16BSCAN NUMBER

178 18B 2bullbull

I 0 N

I N T E N s I T V

19B

HRGC-LRMS ANALYStS OBTAlNED FOR CHEMECOLOGV SAMPLE N02Al 17 F FIGURE 1 441

11

-middotbull ~ bullmiddot - - bull-t L h Jgt ~ uKA l uK Y - td G H I S 1 A I E U H I V 1 R S ll Y - l) A Ymiddot1 0 1I 0 i l1 u 4 5 4 J 5

DATE 838284 TIME 11133 KRATOS MS2S 0S55 SOFTWARE RUN TOR88069 WSU NAME1 CHJ-68 SELECTED-ION MASS CHROMATOGRAMS FOR

6 s 11 6 l -2 7 I 13 7U 8 I 15 lBB

S -460 lBUbulll0697 9B

amp se unmiddot9371 a

0 395 U0bull5932 7B

1s 1BBXbull99315 6B

12 1BBXbull1B6B78 5S

U

39

2B

B

128 130 140 150 160

OCTACHLORODIBENZO-P-DIOXINS

8146 9 l 7 948 Us 19

190

I 0 N

I N TE N s I T y

170 18B 2BB SCAN NUMBER

HRGC-LRMS ANALYSIS 6~tAIHEO FOR CHE~ECOLOGV sA~PLE No2A1 17 F FIGURE 442

I

I I I

r11111w It 1 11 j

i M bull

I

-~

uRpoundHM LJBORAIORY - fUGtn STAIE Uf tRSll( - liAVlAJ 110 -15435 DATE h3H284 TIME 12ee

KRA10S MS25 OS55 SOFTwARE RUN TOR488i5 WSU NAlbullE CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENLOFURANS

81 i 1 I 4 I2 I 14fB 3122L L- L J__ I 429 5 I Ji 6rU _ -bull-A J --L-4____J__ 1-~-J_ ___ J _ L__ __ i____~-1-____L-J__j ----L- J ___L L-L-_J__JLri L _ L_bull__ _L -l I __ 1 _l_ J ~ _J_ L_L___ _ __ J1 _J____

$ 3S6 ISMXbulltlbullS69 ii -237890

---- -middot-middot --- -~ 344 lSDXn89798

80

0 374 l0HXbull878 78

J~middot- 328 l~HXbulll~7132 -middot-Ar ----64 lmiddotbull- 332 IIJIJXbull lmiddot middot-middot -- middot-middot middot- II 11 -middotmiddot _ -middotmiddot - _05817 1 middot -J

58 ~ I (

I It

-0

38

1jmiddot ~j Iv fv i

f1II Ii I I I I

J(

28

If ) I 11 I I Ir I ~

8 __ vl rltiJA-fUI j llJ I I I J middotJ

- - I111 J-J1 _-__ j ~j ~ ~rJt ~-~ J ~1 ----------- J

_ -_) 11 ----middot I

r~ _____ -------------~-- ------bullbull A f

_____ --- bull middot- ______ ___________ ~~--- ~

-f

l 1 r- -middotmiddot---middot- r-middotmiddot r- --middotr---middotmiddotmiddotmiddot ~~~-==i--=-==r===r==----~~Fmiddot-r------bullbullf-~-Jrmiddotr-r--I~------TJ-

53 100 l 50 243 2 58 JBSSCAN NUMBER

HGC-LR~S A~AL~i1s OBTAINE~ FOR CHE~tcoloampv SAMPLE N02A2 17 F FIGUREs 443

~L_

I 0 N

I N T E N s l T y

j I i

68

81UHI ABORA)ORY - fdGHT STATE UNIVERSITY - DAYmiddotroN OHl0 45435 DATE 03028A TIME 12108

KRATOS MS25 DSS5 SOFTWARE RUN1 TORAa075 WSU NAMEs CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR TETRACHLORODIBENZO-P-DIOXINS

Bs01 1 I 07 l0B

S 322 l0BXbull22837 9S

amp 320 1BSbull17892 as

0 257 UBXbull UBS4

7B

32e nssx-11132

bull 332 IUBSXbull 1B5B1 7 SB

U

30

2B

1B

B

2 1 4 3122 4129 5137 61U

-2378

I 0 H

I N T E N s I T V

58 10B 150 2gg 250 3BSSCAN NUMBER

H~c-L~Ms AHaLvsis osrAt~E6 foi cHEMEcoLoov sAl-ihi No~A2 11 i FIGURE 444

0Bl 1 a13 us

0 3U 1BUbull91856 90

338 tbullBXbull59526

80

bull ue lBllbullbullU 2 70

ampbull

u

As

3B

2B

UJ

B

50 358 U8

I-

BREHM L~BORATORV - WRIGHT STATE UhiVERSlTV - DAYTON OHIO 45435 DATE B3B284 TIME 12s17

KRATOS MS25 DS55 SOFTWARE RUN1 TOR5SB63 WSU NAMEbull CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR PENTACHLOROOIBENZOFURANS

2106 3 1 lB 413 Sal 7 6s2S 7 I 2- 8127

I 0 H

I N T

~ s t T y

111 158 208 Z5S 30BSCAN NUMBER

ttic-liUi AH1l~sii biiAlMO o~ CHiUicolocv SAMPLE NOZAZ 17 FIGUREbull 445

BREHM LABORATORY - ~RIGHT STATE UNIVERSITY - DAYTON OHIO 45435 DATE 03i0284 TIME 12117

KRATOS MS259 0S55 SOFTWARE RUN TOR50063 WSU NAMEt CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR PENTACHLORODIBENZO-P-DIOXIHS

100 ss1 l c03 2 06 3 l 0 4 13 5 l 1 7 6120 7amp24 8127

98 0 356 100Xbull22351

80

7B

bull

354

291

U8Xbull1bull27B

1BUbull97B3

6B

5

u

38

28

1B

0

SB 108 150 280

HRGt-lR~s AHAlvsis 6efAiNE6 FbR C~E~Ecoloov sAMPLe No2A2 i1 F FIGURE 1 446

SCAN NUMBER 350 UB250 3016

I 0 H

I N T E H s I T y

BREHM LABORATORY - WRIGHT STATE UNIVERSITY - DAYTON OHIO 45436 DATE1 B3B284 TIMEs 12127

KRATOS MS25 0S55 SOFTWARE RUN1 TOR6BB64 WSU NAHE1 CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZOFURANS

81 1126 2154 4121 5149 7 I 16 8 bull4 BB

0 376 1SSlbull23517 9S

374 1861bull28844

88

4U lSS1bull2386 78

u

s

38

2B

18

bull

58

188 158 Z6SSCAN NUMBER

25B

I 0 N

I N T E N s I T V

3SB

HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGY SAMPLE NOZA2 17 F FIGUREbull 447

11

B01 1 26 lBB

BREHM LABORATORY - WRIGHT STATE UNIVERSITY - DAYTON OHIO 45435 DATE 838284 TIME 12127

KRATOS MS2S 0S55 SOFTWARE RUN TOR6B864 WSU NAME CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR HEXACHLORODIBENZO-P-DIOXINS

254 4 21 549 7 I 16 81H

98

88

7B

68

58

48

38

2B

0

392 UBXbull2332B ----------

398 1BSXbull3874

329 1Bflbull128B7

I 0 N

I N T E N s I T V

SB lBB 158 2BB 25S 3BBSCAN NUMBER

wl~l-Ll~sect ANALvsfs 61t11Ul6 51 CHEUlE6l5v lAULe U02A2 11 J FIGURE 448

-- - - -

- - - -

- - -

- - - -

Bk~liN LABORATORY - WRIGHT STATE UNiERSJTY - DAYTON OHIO 5435 OATE1 03S28 TJHE1 12136

KRATOS MS25 OS55 SOFTWARE RUNi TOR7S8E6 WSU NAMEs CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR HEPTACHLORODIBENZOFURANS

r

BBl 11BB 2d2 3s04 4 r86 5dJ8 6 I 11 7 al 3 BB

S us 1881bull18723

98 --amp US lBBlbulll U35

88

0 HS 18Ubull 12B7 78 -

432 UJB1bull37758 6f

bull n 1ss1 121ss 58

u

38

28

18

B

I 0 N

I N T E N s I T y

28 Cf middot 68 8B IBB 1 2B us SCAN NUMBER

tfflcc-LA~s AHALYSis oliAIUi6 FM cHiUEcotos~ iA~~LE ~-AZ i1 ~ FIGURE r 449

L 1 1)gtLlJl(AIURr

KRATOS MS25 bull 0S55 SELECTED-ION MASS

2102

- lt1i11 11--1C UIUVtKSI1r - UJl10li vdlU 4G1Jo

DATE1 030284 TIME1 12135 SOFTWARE RUN1 TOR 70065 JSU NAHE I CHJ-69 CHROMATOGRAMS FOR HEPTACHLORODIBENZO-P-DIOXINS

3 104 4 I 06 5 08 6 rl 1 180

9g

80

70

68

SB

u

30

2B

lB

0d31 1 dHJ

S _26 100Xbull8101

amp _2 100Xbull7791

- - - -0 359 l0BXbull8848

_32 l00Xbull377S8

bull _3_ l881bull12155

20 40 60 80 lB0 120 SCAN NUMBER

HRGC-L~Msect A~AL~Sis 6ArAtH~b FO~ C~EMECOLOG~ sAMPLE N02A2 17 F FIGURE1 450

UB

713

I 0 H

I N T E N s I T y

BREHM L~BORATORV - WRIGHT STATE UNIVERSITY - DAYTON OlfIO 45435 DATE S3B28~ TIHEa 121~7

KRATOS MS25 0S55 SOFTWARE RUN1 TOR8BB71 WSU NAME CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR OCTACHLOROOIBENZOFURANS

611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

7B

S 4 U 18Hbull 195B

amp U2 1l81bull3928

0 S 12 lB11bull336

H8 U11bull9615

472 lSBlbulll16985

14B 151 166 17B 181SCAN NUMBER

HRGC-LRMS ANALYSIS OBTAINED FOR CHEMECOLOGV SAMPLE NOZA2 17 F FIGUREt 451

I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull

BREHM LABORAfORY - 1JRIGHT STATE LllllVERSllY - DAYTON 0Hl0 45435 DATE 230284 TIME 1247

KRATOS MS25 0S55 SOFTWARE RUN TORB2271 WSU NAME CHJ-69 SELECTED-ION MASS CHROMATOGRAMS FOR OCTACHLORODIBENZO-P-DIOXINS

6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B

amp 458 UBlbull7622 80

0 395 UUbull48 l 7

70

HS UBXbull96145 60 I

0 N

472 lBBXbulll06985 59

I N T

U E N s I

30 T y

2B

10

B

12B 13B 14B 15B 16B 178 18B 19B 211 SCAN NUMBER

H~Gt-LRMs A~ALvsts oerAfktb ~o~ cHE~EcoLoG~ sAMPLE HOlA2 11 ~ FIGURE 452

PARTICULATE EMISSION REPORT DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2A1 REF No 110J811 LOCATION CoMbustor Outlet

CONCENTRATION 127 CO2 44410 M9NM3 18087 srDScf ACT CO2 33308 MsNM3 13565 srDScf

9651 M9AM3 04218 srAcf

EMISSION RATE 19021 95 15096 lbhr

SAMPLING VOLUME 07952 NM3 30132 DScf

AVERAGE ISOKINETICITY 1220 7

FLUE GAS CHARACTERISTICS

MOISTURE 3468 i

TEMPERATURE 3419 des C 6475 des F

FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11

VELOCITY 1308 MIS 25756 fPM

GAS ANALYSIS 02 11 00 i CO2 900 7 co 000 7 MOL WT 299 ss MOLE ltDRYgt

STANDARD CONDITIONS METRIC 20 des C 101325 kPa IMPERIAL 68 des F 2992 in Hs

SAMPLING DATA CONCORD SCIENTIFIC CORPORATION REF No 110J811

DATE 10-14-83 RUN 2Al LOCATION CoMbustor Outlet

STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT

METER CORRECTION FACTOR

100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in

CONDENSATION IN IMPINGER






TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE

WASHINGS PARTICULATE

IMPINGER PARTICULATE

TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s

SAMPLING TI ME 570 Min

STACK HEIGHT 000 M oo ft

------------------------------------------------------------------------------

FIELD DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2A1 REF No 110J811 LOCATION CoMbustor Outlet

PT NO

TIME

Min

STACK VEL TEMP PRESS deg F inH20

------

ORIF PRESS inH20 ------

METER VOL

curt ------

METER HTBOX IMP XAD2 VAC TEMP TEMP TEMP TEMP deg F deg F des F deg F inHs ----- ----- ----- ----- -----

WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220

PARTICULATE EMISSION REPORT DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2A2 REF No 110J811 LOCATION A-Combustor Outlet

CONCENTRATION 12i CO2 63038 MsNm3 25673 srDScf ACT CO2 44126 msNm3 17971 srDScf

14307 msAm3 06253 srAcf


SAMPLING VOLUME 06720 Nm3 25466 DScf

AVERAGE ISOKINETICITY 1004 i


MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM

VELOCITY 1140 M5 22447 tPM

GAS ANALYSIS 02 1220 CO2 840 co 000 MOL WT 298 ss MOLE ltDRYgt

STANDARD CONDITIONS METRIC 20 des C1 101325 kPa IMPERIAL 68 des F1 2992 in Hs

SAMPLING DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2A2 REF No 110J811 LOCATION A-CoMbustor Outlet

STACK DIAMETER 100 M 395 in

STACK AREA 1506 1112 162 sewFt

BAROMETRIC PRESSURE 1018 kPa 3006 inHs

STATIC PRESSURE -6226 Pa -250 inH20

NOZZLE DIAMETER 800 MM 032 in

PITOT COEFFICIENT 0800

METER CORRECTION FACTOR 0987

CONDENSATION IN IMPINGER 1 1900 Ml



CO~DENSATION IN IMPINGER 4 oo Ml( CONDENSATION IN IMPINGER 5 oo Ml


TOTAL CONDENSATION 2089 Ml

FILTER PARTICULATE 25400 s

WASHINGS PARTICULATE 00000 s

IMPINGER PARTICULATE 04260 s

TOTAL PARTICULATE 29660 s

SAMPLING TIME 600 Min

STACK HEIGHT ooo M oo ft

FIELD DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2A2 REF No 110JBll LOCATION A-CoMbustor Outlet

PT TIME STACK VEL ORIF METER METER HTBOX IMP XAD2 VAC WALL i NO TEMP PRESS PRESS VOL TEMP TEMP TEMP TEMP DIST ISO

Min des F inH20 inH20 cuft des F des F des F des F inHs in ------ ------ ------ ----- -----

TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004

PARTICULATE EMISSION REPORT DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION REF No 110J811

CONCENTRATION 127 CO2 44969 tr1sNtr13 ACT CO2 31853 tr1sNtr13

10399 tr1sAtr13

EMISSION RATE 18381 sis

SAMPLING VOLUME 07631 NM3



MOISTURE

TEMPERATURE

FLOW

VELOCITY

GAS ANALYSIS 02 CO2 co MOL WT

STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7

RUN 2B1 LOCATION Venturi Inlet

18314 srDScf 12873 srDScf 04545 srAcf

14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt

METRIC 20 des C 101325 kPa IMPERIAL 68 des F 2992 in Hs

SAMPLING DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 281 REF No 110J811 LOCATION Venturi Inlet

STACK DIAMETER 135 t11 530 in

STACK AREA 1423 M2 153 setft






CONDENSATION IN IMPINGER 1 3242 t111


CONDENSATION IN IMP INGER 3 00 Ml










STACK HEIGHT o oo 00 ft

FIELD DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2B1 REF No 110J811 LOCATION Venturi Inlet

PT TIME STACK VEL ORIF METER NO TEMP PRESS PRESS VOL

Min deg F inHZ inH20 cuft ------ ------ ------

TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137

METER HTBOX IMP XAD2 VAC WALL X TEMP TEMP TEMP TEMP DIST ISO des F deg F deg F des F inHs in

65 475 60 60 30 524 00 55 485 60 60 30 513 oo 55 485 60 60 30 501 00 55 485 60 so 30 488 00 55 485 60 60 30 475 00 55 485 60 60 30 460 00 ss 485 60 60 30 444 00 55 485 60 60 30 427 oo 65 485 60 60 30 408 oo 65 485 60 60 30 386 00 65 485 60 60 30 359 00 65 485 60 60 3o- 319 oo 65 485 60 60 30 211 00 65 485 60 60 30 171 00 65 475 60 60 30 144 oo 65 485 60 60 30 122 00 65 475 60 60 30 103 00 65 485 60 60 30 86 00 65 485 60 60 30 70 oo 65 470 60 60 30 55 00 65 475 60 60 30 42 oo 65 480 60 60 30 29 oo 65 480 60 60 30 17 oo 65 480 60 60 30 06 29336

1132

PARTICULATE EMISSION REPORT DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2B2 REF No 110J811 LOCATION Venturi Inlet

CONCENTRATION 127 CO2 80195 MsNM3 24515 srDScf ACT CO2 40130 M9NM3 16344 9rDScf

14463 t11sAt113 06321 srAcf


SAMPLING VOLUME 07489 Nt113 28380 DScf



MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr

12773 DScfM 33023 AcfM

VELOCITY 1095 M5 215S5 fPtrt

GAS ANALYSIS 02 1240 i CO2 800 7 co 000 l MOL WT 298 ss MOLE DRY)


SAMPLING_ DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 282 REF No 110J811 LOCATION Venturi Inlet

STACK DIAMETER 135 Ill 530 in

STACK AREA 1423 1112 153 Setft







CONDENSATION IN IMPINGER 2 -655 1111

CONDENSATION IN IMPINGER 3 oo Ml

CONDENSATION IN IMPINGER 4 oo 1111




FILTER PARTICULATE 06600 9



TOTAL PARTICULATE 30060 9


ST ACK HEIGHT 000 Ill oo ft

r1



Min des F inH20 inH20 cuft des F deg F des F des F inHg in ----- ------ ------ ------ ----- -----

TRAVERSE NO 1

24 00 495 038 161 38387 55 360 60 60 30 524 00 23 30 490 032 141 38387 65 360 60 60 30 513 00 22 60 490 032 140 38387 60 360 60 60 30 so 1 oo 21 90 490 038 160 38387 50 360 60 60 30 48B oo 20 120 490 042 177 38387 60 360 60 60 30 475 00 19 150 490 050 206 38387 60 360 60 60 30 460 00 18 180 490 042 177 38387 60 360 60 60 30 444 oo 17 ZLO 490 030 133 38387 65 360 60 60 30 427 00 16 240 490 024 108 383a87 60 360 60 60 30 408 00 15 270 440 0 19 093 38387 65 360 60 60 30 386 oo 14 300 480 0 14 068 38387_ 65 360 60 60 30 359 00 13 330 480 020 092 38387 55 360 60 60 3 0- 319 00 12 360 480 0 18 084 38387 60 360 60 60 30 211 00 11 390 470 0 15 o 72 38387 60 360 60 60 30 171 00 10 420 480 0 14 067 38387 60 360 60 60 30 144 oo

9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141

PARTICULATE EMISSION REPORT DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2C1 REF No 110JBll LOCATION Bashouse Inlet

CONCENTRATION 127 CO2 30998 M9NM3 12624 srDScf ACT CO2 16532 MSINM3 06733 srDScf

6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr


VELOCITY 1511 MIS 29747 fPtt

GAS ANALYSIS 02 1400 i CO2 840 7 co 000 i MOL WT 296 sis MOLE ltDRYgt


SAMPLING DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2C1 REF No 110J811 LOCATION Bashouse Inlet


STACK AREA 1370 M2











CONDENSATION IN IMPINGER 6 115 1111



WASHINGS PARTICULATE 10790 9

IMPINGER PARTICULATE 00274 9



STACK HEIGHT 000 M 00 ft

------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----

FIELD DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2C1 REF No 110J811 LOCATION Baghouse Inlet

PT TIME STACK VEL ORIF METER METER HTBOgt IMP XAD2 VAC WALL 7 NO TEMP PRESS PRESS VOL TEMP TEMP TEMP TEMP DIST ISO

Min deg F inH20 inH20 cuft deg F deg F deg F deg F inHg in

TRAVERSE NO 1

12 oo 440 068 319 39006 65 400 60 60 30 509 00 11 30 440 064 302 39006 65 400 60 60 30 485 00 10 60 440 060 286 39006 65 400 60 60 30 459 oo 9 90 440 052 252 39006 65 400 60 60 30 428 oo 8 120 440 058 2 77 39006 65 400 60 60 30 390 00 7 150 440 040 202 39006 70 400 60 60 30 33S oo 6 180 435 024 129 39006 65 400 60 60 30 185 oo 5 210 440 024 128 39006 65 400 60 60 30 130 00 4 240 440 024 128 39006 65 400 60 60 30 92 oo 3 270 440 030 156 39006 65 400 60 60 30 6 1 00 2 300 440 026 137 39006 60 400 60 60 30 35 oo 1 330 440 026 138 39006 65 400 60 60 30 11 13182

360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985

PARTICULATE EMISSION REPORT DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN ZCZ REF No 110J811 LOCATION Bashouse Inlet

CONCENTRATION 127 CO2 98995 msNM3 40317 srDScf ACT CO2 51972 M9NM3 2 1167 sr DScf

20116 fll9AM3 08792 srAcf


SAMPLING VOLUME 08982 Ntit3 34036 DScf



MOISTURE 2867 7


FLOW 27030 Ntit3hr 69826 m3hr

17071 41098

DScfm Acftn


GAS ANALYSIS 02 1410 7 CO2 630 7 co ooo 7 MOL WT 296 ss MOLE ltDRY)


SAMPLING DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2C2 REF No 110JBll LOCATION Bashouse Inlet

STACK DIAMETER 132 111 520 in

STACK AREA 1370 1112 147 sqft





MEHH CORf~ECT ION FACTOR 0995







TOTAL CONDENSA1ION 2898 Ml






STACK HEIGHT 000 111 oo ft


PT TIME STACK VEL DRIF METER METER HTBOX IMP XAD2 VAC WALL NO TEMP PRESS PRESS VOL TEMP TEMP TEMP TEMP DIST ISO

Min deg F inHZ inH20 cuft deg F deg F des F deg F inHs in ------ ------ ------ ----- ----- ----- ----- ----- -----

TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l

PARTICULATE EMISSION REPORT CONCORD SCIENTIFIC CORPORATION REF No 110J811

CONCENTRATION 127 CO2 610 MsN1113 ACT CO2 325 1119Nm3

123 M9AM3

EMiSSION RATE 0251 ss

SAMPLING VOLUME 096S0 N1113



MOISTURE 3179 X

TEMPERATURE 2098 des C

FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s

GAS ANALYSIS 02 1400 X CO2 640 X co ooo

DATE 10-14-83 RUN 2D1 LOCATION D-Ba9house Outlet

00248 9rDScf 00132 srDScf 00054 srAcf

198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll

MOL WT 296 99 MOLE ltDRYgt

STANDARD CONDITIONS METRIC 20 des C 101325 kPa IMPERIAL 68 des F 2992 in H9

SAMPLING DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2D1 REF No 110J811 LOCATION D-Bashouse Outlet


STACK AREA 1370 M2 147 Setft


STATIC PRESSURE -27395 Pa -11 00 in H20

NOZZLE DIAMETER 700 fllfrl 028 in






CONDENSATION IN IMPINGER 4 00 t1t 1






IMPINGER PARTICULATE 0017 4 9



STACK HEIGHT 000 111 00 ft

FIELD DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2D1 REF No 110J811 LOCATiON D-Baghouse Outlet


Min des F inH20 in H20 cu f t des F deg F deg F deg F inHg in ------ ------ ------ ----- ----- ----- -----

TRAVERSE NO 1

12 00 405 046 357 73490 65 345 60 60 30 509 00 11 30 405 044 344 73490 65 345 60 60 30 48S 00 10 60 405 048 373 73490 70 345 60 60 30 459 00 9 90 410 050 387 73490 75 345 60 60 30 428 oo 8 120 410 050 387 73490 75 345 so 60 30 390 oo 7 150 410 050 387 73490 75 345 60 60 30 335 oo 6 180 410 046 365 73490 85 345 60 60 30 185 oo s 210 410 046 365 73490 85 345 60 60 30 130 oo 4 240 410 042 337 73490 85 345 60 60 30 92 oo 3 270 410 042 337 73490 85 345 60 60 30 6 1 00 2 300 410 042 337 73490 85 - 345 60 60 30 35 oo 1 330 410 042 337 73490 85 345 60 60 36 11 12725

360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo

9 90 410 044 349 75410 80 345 60 60 30 428 oo 8 120 410 042 337 754 10 85 345 60 60 30 390 oo 7 150 410 042 337 75410 85 345 60 60 30 335 00 6 180 410 042 337 75410 85 345 60 60 30 185 oo 5 21 0 415 038 308 75410 85 345 60 80 30 130 oo 4 240 410 040 323 754 10 85 345 60 60 30 92 oo 3 270 410 040 323 75410 85 345 60 60 30 6 1 oo 2 300 410 040 323 75410 85 345 60 60 30 35 oo 1 330 410 040 323 754 10 85 345 60 60 30 1 bull 1 12554

360 77240

AVERAGE 410 044 347 1030


CONCENTRATION 12l CO2 5591 MsNm3 ~ ACT CO2 2795 ~sNm3

114 7 M9Am3

EMISSION RATE 2010 ss

SAMPLING VOLUME 08012 Ntr13

AVERAGE ISOKINETICITY 91 8 i


MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms

GAS ANALYSIS 02 1460 7 CO2 600 7 co 000 i


02277 srDScf 01138 9rDScf 00501 grAcf

1595 lbhr

30360 DScf

3906 deg F

16344 DScfM 37124 Acfm

25172 fPM

MOL WT 296 99 MOLE ltDRY)

STANDARD CONDITIONS METRIC 20 des C 101325 ~Pa IMPERIAL 68 des F 2992 in Hs

-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


CONDENSATION IN IMPINGER 1






TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----

FIELD DATA DATE 10-14-83 CONCORD SCIENTIFIC CORPORATION RUN 2D2 REF No 110JBll LOCATION D-Bashouse Outlet

PT TIME STACK VEL ORIF METER METER HTBOX IMP XAD2 VAC WALL 7 NO TEMP PRESS PRESS VOL TEMP TEMP TEMP TEMP DIST ISO

Min des F inH20 inH20 cuft des F des F des F des F inHs in

TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------

CONCORD SCIENTIFIC CORPORATION

FIVE STAGE SERIES CYCLONE PARTICLE SIZE TEST DATA

CLIENT CARB CITY AND PROVINCE DATE 10-15-83

SANPLING LOCATION 8-Venturi Inlet RUN 381N START TIME 0036

STACK GAS TEPERATURE(TS) 48500 DEGF 25167 DEGC STACK GAS PRESSURE -500 IN WG

STACK GAS VELDCITY(U) 502 FPS 153 NSEC ESTINATE STACK GAS NOISTURE 3230

CLASSIFICATION RANGE 000 UN TD 000 UN DESIRED SANPLE FLOW RATE 0000 ACFH

GAS NETER FLOW RATE 9=UtNOZZLE DIAHETER)t528(TS+460t(l-HC100)t2992PB 0000 DSCFN

REGUIRED ORIFICE PRESSURE 000 IN WG NOZZLE DIAHETER 0138 INCHES

DUCT CROSS SECTION 5300 X 000 INCHES BAROHETRIC PRESSURREPB) 3006 IN MERCURY

GAS NETER CORRECTION FACTOR 09980 CP PITOT 0820 CREW

SANPLE STACK VELOCITY ORIFICE HETER NETER TEMPERATURE DISTANCE SANPLE TINE TEMP PRESSURE PRESSURE VOLUNE IN OUT VACUUN FRON WALL I POINT (NIN) ltDEGFl ltINNG) UNMG) ltCUFT) ltDEGF) ltDEGF) UNHGJ ltINCHESgt

12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750

AVERAGES 4850 042 068 sso 6SO

------------------------------------------




SAMPLING LOCATION 8-Venturi Inlet RUN 381N START TINE 0036

TOTAL SANPLE VOLUNE 495 DSCF 0131 NN3

AVERAGE SAMPLING RATE (STACK CONDITIONSgt 0442 ACFN 0013 AN3NIN

TOTAL IMPINGER CATCH 506 NL

AVERAGE STACK TENPERATURE 4850 DEGF 2517 DEGC

AVERAGE ISOKINETIC 1418 I

STACK GAS ANALYSIS

CONSTITUENT WET BASIS NOLE PERCENT

DRY BASIS NOLE PERCENT

CO2 02 co N2(BY DIFFERENCE) H20

600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000

VISCOSITY OF STACK GAS 242726 NICROPOISE

CYCLONE NET PARTICULATE PERCENTAGE OF STAGE WEIGHT TOTAL PARTICULATE CUNULATIVE NUMBER (GRANS) WEIGHT PERCENTAGE

------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000

CUNULATIVE PERCENTAGE D50 PARTICLE LESS THAN DIANETER STATED D50 DIANETER CUNgt

---------------------833 1224 833 693 833 526

-000 260 -000 146

------------------------TOTAL PARTICULATE WEIGHT 00840 GRAMS

PARTICULATE CONCENTRATION

064301 GN13 026188 GRAINSDSCF

- 022409 GAH3 009794 GRAINSCF

------------------

CLIENT CARB DATE OF RUN 10-15-83 FIVE STAGE SERIES CYCLONE LOCATION 8-Venturi Inlet PARTICLE SIZE TEST DATA RUN NUNBER 381N

TOTAL SANPLE VOLUNE 0131 Nlf3

AVERAGE SANPLING RATE CSTACK CONDITIONS) 0013 All3lIIN

TOTAL ININGER CATCH 506 NL

AVERAGE STACK TEMPERATURE 251 7 DEGC

AVERAGE ISOKINETIC 1418

CYCLONE STAGE NUNBER

NET PARTICULATE WEIGHT (GRAMS)

PERCENTAGE OF TOTAL PARTICULATE WEIGHT

CUNULATIVE PERCENTAGE

---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000

9167 ooo ooo 833 ooo ooo

10000 833 833 833

-o_oo -ooo

CUNULATIVE PERCENTAGE DSO PARTICLE LESS THAN DIANETER STATED DSO DIAMETER CUN)

833 1224 833 693 833 526

-000 260 -ooo 146

TOTAL PARTICULATE WEIGHT 00840 GRANS


064301 GNN3 026188 GRAINSDSCF

022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------




SAMPLING LOCATION B-Venturi Inlet RUN 382N START TINE 0352

STACK GAS TENPERATURECTS) 48500 DEGF 25167 DEGC STACK GAS PRESSURE -500 IN WG

STACK GAS VELOCITYCU) 499 FPS 152 NSEC ESTINATE STACK GAS NOISTURE 2920

CLASSIFICATION RANGE 000 UN TO 000 UN DESIRED SAMPLE FLOW RATE 0000 ACFN

GAS NETER FLOW RATE G=U1NOZZLE DIANETER)1528(TS+460bulllt1-NC100)f2992PB 0000 DSCFN

REBUIRED ORIFICE PRESSURE 000 IN WG NOZZLE DIAMETER 0158 INCHES

DUCT CROSS SECTION 5300 X 000 INCHES BARONETRIC PRESSURREfPB) 3006 IN MERCURY


SAlIPLE STACK VELOCITY ORIFICE NETER NETER TENPERATURE DISTANCE SANPLE TINE TENP PRESSURE PRESSURE VOLUNE IN OUT VACUUM FRON WALL II POINT OUN (DEGFgt ltINWGgt (INMG) CCUFT) (DEGFl CDEGF) CINHGi CINCHES)

12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------




SANPLING LOCATION B-Venturi Inlet RUN 382 START TINE 0352

TOTAL SANPLE VOLUME 722 DSCF

AVERAGE SAMPLING RATE (STACK CONDITIONS) 0411 ACFN

TOTAL INPINGER CATCH 636 NL

AVERAGE STACK TEMPERATURE 4850 DEGF


STACK GAS ANALYSIS

WET BASIS DRY BASIS CONSTITUENT lIOLE PERCENT NOLE PERCENT

CO2 579 820 02 848 1200 CD 001 001

( N2BY DIFFERENCE) SS36 7979 H2D 2937 ooo

TOTAL 10000 10000

VISCOSITY OF STACK GAS 245585 NICROPDISE

CYCLONE NET PARTICULATE PERCENTAGE OF STAGE WEIGHT TOTAL PARTICULATE CUMULATIVE NUlIBER lt6RAl1SJ WEIGHT PERCENTAGE

0191 Nl13

0012 Al13NIN

2517 DEGC

CUNULATIVE PERCENTAGE LESS THAN STATED D50 DIAMETER

DSO PARTICLE DIANETER (UNJ

l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S

TOTAL PARTICULATE WEIGHT 07440 GRAlIS


II

390369 GNll3 158984 GRAINSDSCF

142467 GAN3 062267 GRAINSCF

CLIENT CARB DATE OF RUN 10-15-83 FIVE STAGE SERIES CYCLONE LOCATION B-Venturi Inlet PARTICLE SIZE TEST DATA RUN NUNBER 382N

TOTAL SAMPLE VOLUNE 0191 NN3

AVERAGE SAMPLING RATE (STACK CONDITIONS) 0012 Af13NIN

TOTAL INPINGER CATCH

AVERAGE STACK TEMPERATURE

AVERAGE ISOKINETIC

CYCLONE NET PARTICULATE STAGE WEIGHT NUMBER (GRANS)

1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425

CUMULATIVE PERCENTAGE DSO PARTICLE LESS THAN DIANETER STATED 050 DIANETER ltUN)

636 NL

251 7 DEGC

1015 l


CUMULATIVE PERCENTAGE

10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF




SANPLING LOCATION B-Venturi Inlet RUN 383N START TINE 0725

STACK GAS TENPERATUREltTS) 48500 DEGF 25167 DEGC STACK GAS PRESSURE -500 IN WG

STACK GAS VELDCITYCU) 505 FPS 154 NSEC ESTINATE STACK GAS NOISTURE 2920

CLASSIFICATION RANGE 000 UN TD ooo u DESIRED SANPLE FLOW RATE 0000 ACFN

GAS NETER FLOW RATE B=Uf(NOZZLE DIANETER)f528(TS+460f(1-NC100)f2992PB 0000 DSCFN

REQUIRED ORIFICE PRESSURE 000 IN WG NOZZLE DIAMETER 0158 INCHES

DUCT CROSS SECTION 5300 X 000 INCHES BAROMETRIC PRESSURRE(PB) 3006 IN NERCURY

GAS HETER CORRECTION FACTOR 09980 CP PITOT 0820 CREW

SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)

VELOCITY ORIFICE NETER METER TENPERATURE DISTANCE PRESSURE PRESSURE V~~UNE IN OUT VACUUN FRON WALL CINWGgt CINWGgt (CUFT I) CDEGF) (DEGFgt CINHGr ltINCHESgt

I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650



CLIENT CARS CITY AND PROVINCE DATE 10-15-83

SAMPLING LOCATION B-Venturi Inlet RUN 3B31 START TINE 0725

TOTAL SANPLE VOLUNE 4BS DSCF 0128 NN3

AVERAGE SANPLING RATE ltSTACK CONDITIONS) 0437 ACFH 0012 AH3NIN


AVERAGE STACK TEHPERATURE 4B50 DEGF 251 7 DEGC


STACK GAS ANALYSIS


---------


CO2 02 co N28Y DIFFERENCE) H20

455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000

VISCOSITY OF STACK GAS 242989 HICROPOISE

CYCLONE STAGE NUMBER

1 2 3 4 5 FILTER

NET PARTICULATE WEIGHT (GRANS)

04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594

CUMULATIVE PERCENTAGE D50 PARTICLE LESS THAN DIANETER STATED D50 omiddotIAMETER (UN)

--------------------2337 1233 2337 701 2337 532 1594 264 1594 148

--------------------TOTAL PARTICULATE WEIGHT 05520 GRAMS


431374 GNl13 175684 GRAINSDSCF

149030 GAl13 065135 GRAINSCF

---------------------

CLIENT CARB DATE OF RUN 10-15-B3 FIVE STAGE SERIES CYCLONE LOCATION B-Venturi Inlet PARTICLE SIZE TEST DATA RUN NUNBER 383N

TOTAL SAMPLE VOLUME 0128 NN3

AVERAGE SANPLING RATE (STACK CONDITIONSgt 0012 AN3NIN

TOTAL INPINGER CATCH 509 L

AVERAGE STACK TENPERATURE 2517 DEGC


CYCLONE NET PARTICULATE PERCENTAGE OF ~TAGE WEIGHT TOTAL PARTICULATE CUNULATIVE NUNBER (GRANS) WEIGHT PERCENTAGE

1 04230 2 00000 3 omiddot0000 4 00410 5 00000 FILTER ooeeo

7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594

CUlIULATIVE PERCENTAGE DSO PARTICLE LESS THAN DIANETER STATED D50 DIANETER ltUN)

2337 1233 2337 701 2337 532 1594 264 1594 148



431374 GNl13 1756B4 GRAINSDSCF

149030 6AN3 065135 GRAINSCF I

-------------------


FIVE STAGE SERIES CYCLONE PARTICLE SIZE TEST DATA ----------middot---------------------------------------CLIENT CARB CITY AND PROVINCE DATE 10-15-83

SAMPLING LOCATION C-Baghouse Inlet RUN 3C1 START TINE 0036

STACK GAS TENPERATUREltTS) 45000 DEGF 23222 DE6C STACK GAS PRESSURE -500 IN MG

STACK GAS VELOCITYU) 539 FPS 164 NSEC ESTINATE STACK GAS NOISTURE 2700 I

CLASSIFICATION RANGE 000 UN TO ooo mt DESIRED SAMPLE FLOW RATE 0000 ACFM

GAS NETER FLOW RATE G=UiNOZZLE DIANETER)1528TS+460f(1-NC100)12992PB 0000 DSCFN

REBUIRED ORIFICE PRESSURE 000 IN MG NOZZLE DIAMETER 0158 INCHES

DUCT CROSS SECTION 5200 X 000 INCHES BARONETRIC PRESSURREPB) 3006 IN MERCURY


SAMPLE STACK VELOCITY ORIFICE METER NETER TENPERATURE DISTANCE SAlIPLE TIHE TEHP PRESSURE PRESSURE VOLUME IN OUT VACUUJ1 FRON WALL II-POINT lIINJ ltDE6F) (INMG) INMG) (CU FT) ltDEGfl ltDEGFl IN HG) INCHES)

7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650




SAPLING LOCATION C-Ba9house Inlet RUN 3C1 START TIME 0036

TOTAL SANPLE VOLUHE

AVERAGE SANPLING RATE STACK CONDITIONSgt

TOTAL It1P-INGER CATCH


AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS

CONSTITUENT WET BASIS MOLE PERCENT

DRY BASIS OLE PERCENT

I

CO2 4 71 700 02 874 1300 co 001 001 N2(8Y DIFFERENCE) 5379 7999 H20 3275 ooo

TOTAL 10000 10000


CYCLONE STAGE NUlIBER

1 2 3 4 5 FILTER

NET PARTICULATE WEIGHT (GRANSJ

04248 00000 00000 01849 00000 01515

PERCENTAGE OF TOTAL PARTICULATE CUNULATIIJE WEIGHT PERCENTAGE

----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990

CUNULATIVE PERCENTAGE LESS THAN STATED D50 DIANETER

4419 4419 4419 1990 1990

050 PARTICLE DIANETER CUN)

1102 600 447 218 123




1B13B2 GAN3 079275 GRAINSCF

---------------------

CLIENT CARS DATE OF RUN 10-15-83 FIVE STAGE SERIES CYCLONE LOCATION C-Baghouse Inlet PARTICLE SIZE TEST DATA RUN NUNBER 3Cl

TOTAL SANPLE VOLUNE 0151 Nl13

AVERAGE SAMPLING RATE STACK CONDITIONSgt 0014 All3NIN

TOTAL INPINGER CATCH S92 NL

AVERAGE STACK TEMPERATURE 2322 DEGC


CYCLONE NET PARTlCULATE PERCENTAGE OF STAGE WEIGHT TOTAL PARTICULATE CUMULATIVE NUMBER (GRAMS) WEIGHT PERCENTAGE

l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990

CUNULATIVE PERCENTAGE D50 PARTICLE LESS THAN DIA11ETER STATED DS0 DIAMETER CUlU

4419 1102 4419 600 4419 447 1990 218 1990 123








SANPLING LOCATION C-Bashouse Inlet RUN 3C2 START TINE 0352

STACK GAS TENPERATURE(TSgt 45000 DEGF 23222 DEGC STACK GAS PRESSURE -500 IN WG

STACK GAS VELOCITY(U) 545 FPS 166 NSEC ESTIATE STACK GAS NOISTURE 3220

CLASSIFICATION RANGE 000 UM TO 000 UM DESIRED SANPLE FLOW RATE 0000 ACFN

GAS NETER FLOW RATE 9=Uf(N0ZZLE DIANETER)f528(TS+460t(l-MC100)t2992PB 0000 DSCFN

REQUIRED ORIFICE PRESSURE 000 IN WG NOZZLE DIANETER 0158 INCHES

DUCT CROSS SECTION 5200 X 000 INCHES BARONETRIC PRESSURRE(PB) 3006 IN NERCURY


SAlIPLE STACK VELOCITY ORIFICE NETER NETER TEMPERATURE DISTANCE SANPLE TINE TENP PRESSURE PRESSURE VOLUNE IN OUT VACUUN FRON WALL Il POINT UHN) (DEGFgt (INWG) (INWGJ (CUFT) (DEGF) ltDEGFgt ltINHGl (INCHES)

t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650




SANPLING LOCATION C-Bashouse Inlet RUN 3C2N START TINE 0352

TOTAL SAMPLE VOLUNE 757 DSCF 0200 NN3

AVERAGE SAMPLING RATE STACK CONDITIONS) 0479 ACFN 0014 AN311IN


AVERAGE STACK TEMPERATURE 4500 DEGF 2322 DEGC


STACK GAS ANALYSIS

CONSTITUENT NET BASIS MOLE PERCENT ------- middot-- --


-----------CO2 02 co N2CBY DIFFERENCE) H20

408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000



NET PARTICULATE WEIGHT CGRAl1S)


CUlIULATIIJE PERCENTAGE

CUMULATIVE PERCENTAGE LESS THAN STATED D50 DIAMETER

D50 PARTICLE DIANETER (UN)

1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126




10515S GAN3 045959 GRAINSCF

----------------------------------

-----------------

CLIENT CARB DATE OF RUN 10-15-B3 FIVE STAGE SERIES CYCLONE LOCATION C-Baghouse Inlet PARTICLE SIZE TEST DATA RUN NUNBER 3C2N

TOTAL SANPLE VOLUNE 0200 NN3


TOTAL IMPINGER CATCH 992 PfL



CYCLONE NET PARTICULATE PERCENTAGE OF STAGE WEIGHT TOTAL PARTICULATE CUNULATIVE NUNBER CGRANSJ WEIGHT PERCENTAGE

-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------

CUMULATIVE PERCENTAGE D50 PARTICLE LESS THAN DIANETER STATED D50 DIANETER ltUM)

6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF



CLIENT CARS CITY AND PROVINCE DATE 10-15-B3

SAMPLING LOCATION C-8a9house Inlet RUN 3C3N START TINE 0722


STACK GAS VELOCITYltU) 00 FPS 00 NSEC ESTINATE STACK GAS NOISTURE 000 l

CLASSIFICATION RANGE 000 UN TO 000 UN DESIRED SANPLE FLOW RATE 0000 ACFN

GAS NETER FLOW RATE B=U1NOZZLE DIANETER)1528(TS+460frac341-11C100)12992PB 0000 DSCFl1

REGUIRED ORIFICE PRESSURE 000 IN WG NOZZLE DIANETER 0158 INCHES

DUCT CROSS SECTION 5200 X 000 INCHES BAROMETRIC PRESSURREltPBgt 3006 IN NERCURY

GAS K~TER CORRECTION FACTOR 09871 CP PITOT 0820 CREW -----------------------------------------------------------

SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl

VELOCITY ORIFICE METER METER TEMPERATURE DISTANCE PRESSURE PRESSURE VOLUME IN OUT VACUUN FRON WALL ltINWG) NWG) (CUFT) ltDEGF) ltDEGfl ltIN HG f (INC HES)

II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650






AVERAGE SANPLING RATE (STACK CONDITIONSgt 0421 ACFN 0012 AN3NIN


AVERAGE STACK TENPERATURE 4S00 DEGF 2322 DEGC


STACK GAS ANALYSIS



CO2 02 co N2ltBY DIFFERENCE) H20

447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000


CYCLONE NET PARTICULATE STAGE WEIGHT NUNBER ltGRAlISJ ----1 04680 2 00000 3 00000 4 021B0 5 00000 FILTER 01170


5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF

CLIENT CARB DATE OF RUN 10-15-83 FIVE STAGE SERIES CYCLONE LOCATION C-Baghouse Inlet PARTICLE SIZE TEST DATA RUN NUNBER 3C3N

TOTAL SANPLE VOLUME 0128 NN3





CYCLONE NET PARTICULATE PERCENTAGE OF STAGE WEIGHT TOTAL PARTICULATE CUNULATIVE NUNBER (GRAMS) WEIGHT PERCENTAGE

1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------

CUNULATIQE PERCENTAGE D50 PARTICLE LESS THAN DIAl1ETER STATED D50 DIAMETER Upt)

41 72 4172 41 72 1457 1457

1215 689 516 260 149



625188 GNt13 254618 GRAINSDSCF

227228 GAt13 099313 GRAINSCF



CLIENT CITY AND PROVINCE DATE

SANPLING LOCATION C-Bashouse Inlet RUN 3D1N START TINE 2058

STACK GAS TENPERATUREltTS) 000 DEGF -1778 DEGC STACK GAS PRESSURE -1100 IN WG

STACK GAS VELOCITY(U) 00 FPS 00 NSEC ESTINATE STACK GAS NOISTURE 2700


GAS NETER FLOW RATE O=Uf(NOZZLE DIANETER)f528fTS+4601(1-NC100)f2992PB 0000 DSCFN

REBUIRED ORIFICE PRESSURE 000 IN WG NOZZLE DIANETER 0158 INCHES

DUCT CROSS SECTION 5200 X 000 INCHES BARONETRIC PRESSURREltPB) 3006 IN MERCURY


SAMPLE STACK VELOCITY ORIFICE NETER NETER TEMPERATURE DISTANCE SAlIPLE TINE TENP PRESSURE PRESSURE VOLUNE IN OUT VACUUlI FRON WALL 1 POINT ltNIN) fDEGFgt UNMG) UNWG) (CUFT) ltDEGFgt fDEGFgt (INHGgt ltINCHES)

7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581



-----------------------middot-------------------CLIENT CITY AND PROVINCE DATE

SAMPLING LOCATION C-Ba9house Inlet RUN 3D1N START TINE 2058

TOTAL SANPLE VOLUHE 8125 DSCF 2144 NN3



AVERAGE STACK TEMPERATURE 4100 DEGF 2100 DE6C


STACK GAS ANALYSIS


DRY BASIS MOLE PERCENT

CO2 02 co N2(BY DIFFERENCE H20

441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER

NET PARTICULATE WEIGHT ltGRAMS)

00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------

D50 PARTICLE DIANETER CUN)

1125 619 452 230 135





LIENT DATE OF RUN FIVE STAGE SERIES CYCLONE LOCATION C-Bashouse Inlet PARTICLE SIZE TEST DATA RUN NUNBER 3D1N

TOTAL SANPLE VOLtmE 2144 Nlf3

AVERAGE SAMPLING RATE ltSTACK CONDITIONS) 0012 AN311IN




CYCLONE NET PARTICULATE PERCENTAGE OF STAGE WEIGHT TOTAL PARTICULATE CUNULATIVE

NUlIBER CGRANS) WEIGHT PERCENTAGE

1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333

CUMULATIVE PERCENTAGE D50 PARTICLE LESS THAN DIANETER STATED DSO DIAMETER CUNgt

7333 7333 7333 3333 3333

1125 619 452 230 135

TOTAL PARTICULATE WEIGHT 00075 GRAMS




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Zenon Environmental Inc 845 Harrington Court Burlington Ontario L7N 3P3 Canada Telephone (416) 639-6320 Telex 061-8734

July 2 1986

Mr John Chandler Senior Engineer Concord Scientific Corporation 2 Tippett Road DOWNSVIEW Ontario M3H 2V2

Dear John

I am enclosing the review comments you requested on the document entitled The Results of Analyses of Combustion Products Collected During Tests of A Refuse-Fired Incinerator Located in Tsushima Ja_pan for Polychlorinated Dibenzodioxins and Dibenzofurans Selected Metals and FluoridesChlorides

Generally the analytical report is thorough though some discrepancies in the data were noted I have outlined these points along with our suggestions in the review

I am available to discuss this further Please feel free to call me

r~tf~ Uhn A Coburn

Vice President - Technical Services

JACmk

REVIEW CCJ4MENTS ON THE WRIGHT STATE UNIVERSITY FINAL

REPORT ON THE ClJe1BUSTION ANALYSES PERFORMED

ON THE TSUSHIMA INCINERATOR

Comments by

John A Coburn

ZENON ENVIROt14ENTAL INC

July 2 1986

(

Sample Preparation

In general there is good description of the samples of the

protocols used in their preparation and of the conditions of analysis

Wh i 1 e no t a res po n s i b i1 i t y o f the an a 1 ys i n g 1ab ora to r y some

comment on the conditions of shi micronent should have been provided in the

1aboratory report It is not cl ear whether the samples were

maintained in coolers at approximately 4degC

The sub-dividing of certain samples (impinger solutions and

XAD resins) al 1 ows one to speculate on the homogeneity (or 1 ack of it)

of the sub-samples This sub-dividing should be avoided in tests of

this sort

The protocols for extractions clean-up and HRGCLRMS

analysis of PCDDPCDF are those stipulated by the AS~ME Standards

of at 1east one isomer for each congener group of PCDDPCDF ( from

tetrachloro to octachloro) were identified in the data report It

would be useful for purities to be provided where known

From the description provided it is not clear if the

retention windows for each 11 cl ass of CDDCDF were verified through

the use of earl iest1 a test eluting isomers or a fly ash extract It

seems that they were estimated in some cases and this 1eaves open to

question the possibility of missed peaks in the analysis of the

tetrachl oro to hexachl oro CDDCDF congeners This does not appear to

be the case upon review of the extracted ion current profiles

( E IC pIs) bull

The identification criteria used for the PCDDPCDF

identified only elution in the retention window and correct ion ratio

+ 30 This range is broader than the + 15-20 norrnal l y accepted for

1

PCDDPCDF data In addition the LRMS analysis included moni taring of

the (M-COCl)+ ion and this is usually an identification criterion

The monitoring of the M+ ion for the chlorinated di phenyl ethers with

2 chlorines more than the PCOF being monitored is al so very useful and

its absence must be a criterion for PCDF presence One final

identification criterion which is usual 1 y employed is the signal to

noise ratio of 31 - 51 for the M+ and (M+2)+ ions On the basis of

the report it is not cl ear if these 1ast 3 criteria were used

General Con111ents on PCDDPCDF Data Table

1 In virtually all samples the impinger solutions were found to

contain the highestmiddotamount of PCDDPCDF Was the train assembled

with the impingers before the resin trap (a 1 a MOE) or is this an

i nd k a ti on o f brea k t h ro u g h

2 While the pattern for the PCDF is consistent with other reports

the PCOO pattern is quite the opposite compared to previous

reports In this study the PCOO concentrations were shown to

decrease from tetra to octa while just the reverse or a trend to

maximize at the HxCDD was found in NITEP and other US studies

No ex pl ana t ion is of fer ed

3 Relative total amounts of PCDO and PCDF are in 1 ine with those

reported elsewhere

2

4 Excellent recoveries of TCDD HpCDD and OCDD are reported for

a11 te st sam p1es bull

5 Review of extraction ion current profi 1es (EICPs) revealed

readily interpreted PCDD chromatograms The same patterns were

evident in the EICPs of the filters and impingers

EICPs for the PCDF were obscured somewhat by the PCDPE ion which

was us ua 11 y a 1ow 1eve1 noise s i g na1 bull

6 Retention time of the TCDD was readily reproduceable from

February 2 1984 to April 10 1984 which are the dates of EICPs

provided

7 On the basis of the EICPs supplied it is not clear how the area

measurements were take~ for each peak and summed for use in

calculating the resultant class concentration

8 In comparing the 332 ion (C-13 TCDD) to 328 ion (C-37 TCOD) the

ratio obtained were general 1y in good agreement with the

recovery values provided in Table 7 There were however some

exceptions which were not understood

Sample 2A2 impinger solutions had a reported 13c12 - TCDD

recovery of 93 yet the EICPs showed a 332328 ratio of 33

3

Sample 202 reported a 13c12 - TCDO recovery of 95while the

ratio of 332328 was only 26 on the EICP

In addition the EICPs for the PCDO and PCDF on sample 2D1-

Impingers were apparently analysed at two different times and the

ratios of 332328 were 72 and 14 in the two analyses The

fonner value is reported for the recovery of the 13c 12 TCDD

internal standard (actually 73 is reported)

I dont understand these discrepancies unless different spike

1ev e1s were used bull

9 In c a 1cu 1at i n g the res po n se o f the 3 7 C 1 - Hp CDD a g a-i nst the 3 7 C 4 -

TCDD response similar discrepancies were found for sample 202-

First Impinger and 2A2-Impingers For other samples checked

there was internal consistency with the reported recovery and

the relative response noted above

Again no explanation is provided for this in the data report

10 No EICPs for standards or blanks were provided so no actual

calculations were perfonned as a check on the reported data

11 The EICPs reveal very good chromatographic resolution and peak

shape

4

12 Ex am p1e c a 1cu1at io n s and raw area mea s u rem en ts wo u1d perm i t

ver i fi ca t ion o f f i n a 1 da ta po i n ts bull

Summarizing al 1 of the above I would say the analytical

re port i s a com pe ten t and pro f e s s ion a 1 an a1yt i c a 1 pac k age There are

some discrepancies which cannot be fully rationalized based upon the

data package av a i1 ab1e for review Some s uggge st ions for future

studies of this type are included in the review comments

John A Cob urn

5

Environment EnvironnementIdiams Canada Canada

(

Technology Development and Technical Services Branch

Ottawa KlA OE7 Your Ille Votre reference

Our tfe Norre reference

July 23 1986 4047-3

Mr J Chandler Concord Scientific Corporation 2 Tippett Road Toronto Ontario M3H 2V2

Dear Mr Chandler

Mr M Bumbaco has forwarded to me your letter concerning the results of analysis of combustion products performed by the Brehm Laboratory of the Wright State University

As requested Mr Chiu and I have reviewed the report and consider that it is a well-prepared and useful document Our comments and findings are as follows

P6 Sec 2b One-half of the XAD-2 was used to analyze the PCDDPCDF contents It could be that the Laboratory tried to save the other half of the sample for any future applications The XAD resin is very difficult to homogenize in order to produce a representative sample in the one-half portion as the PCDDPCDF loading tends to be accumulated at the top of the XAD column Perhaps the Brehm Laboratory has investigated this situation and established the criteria for homogenicity The evidence however is not included in the report

t order to consenie energy Ades ft1S de conseMBXI and resources Iris paper de renerrie et des ressounes contans post-consuner ce papier contient des flgtre fbres ecycOOSCanada

2

- P 6 Sec 2b No acid treatment step is included in the clean-up procedure for ash and filter samples This treatment increases the surface areas of particulates thus as cited in the literature the extraction efficiency The protocol developed by our laboratory uses lN HCl (MOE uses 6N HCl) and up to 40 of impurities can be washed away without any PCDDPCDF losses

It is interesting to note that both XAD resin and impinger samples were split but not the filter samples due probably to the difficulty of homogenicity

p 7 Sec 3a and 3b These procedures are not employed by our

laboratory (nor MOE) Sample extracts are transferred directly to the clean-up columns and we have not encountered any problems of separ~tion

P 7 Sec 3h The statement that PCDDs and PCDFs were analyzed separately ~rom ~he contents of two vessels is not supported in the text The sequence of operations in Table 8 and the attached TIC plots from GCMS runs indicate that these compounds were measured simultaneously eg results of 2A2-17 filter were obtained at 1208 PM030384 for T4CDD and T4CDF and so on

- P 8 Sec 4a-2 The standard analytical columns used by this laboratory and MOE are 30 M DB-5 silica capillary The purpose of using the 60 M column is based on the assumption that the resolutions of PCDDPCDF congeners can be improved and that 2378 TCDD is completely separated from other isomers Results of extensive investigations in this laboratory indicate that the 60 M column fails to provide any appreciable improvement and instead the total chromatographic time for OCDD to be eluted is increased by about 25 minutes

Since the advantages using 60 M column do not compensate for the additional time required for analysis the use of 30 M column will be continued for the PCDDPCDF work in this laboratory

3

4a - 3

P 9 Table A

(

P 12 Sec 6b

The accelerating voltage ofmiddot 4 KV seems to be high The typical Finnigan Model 4000 series GCMS requires below 2 KV The report does not provide signalnoise ratio and the detection limits judging from the attached TIC plots it indicates that electron energy was high and causing background problewms and interferences

As T4CDD and T4CDF were measured simultaneously with RxDPE nine ions had to be monitored using the MID technique In Figures 443 and 444 only eight ions were monitored with the absence of Me 241 the daughter ion of T4CDF The reason is obvious since the MID cannot accommodate all nine ions within the time-window of one second scanning without sensitivity loss In NITEP samples we investigated the presence of diphenyl ethers and none was found For confirmation purposes the Me 241 ion might be monitored insiead of RxDPE

It is also noticed that the the fragment ion M-C0Cl of PCDDPCpF was listed in Table A for monitoring In TIC plots different- ions were used eg in Figures 444 446 and 448 the monitored ions are M-C0Cl-2 (Me 257) M-C0Cl (Me 291) and M-C0C1+2 (Me 329) respectively Evidently these ions had higher responses than M-C0Cl in different congeners and were selected For the purpose of consistency Table A should be modified to list the individual monitored ions

The paragraph contains a major typographical error which makes the contents very difficult to be understood The phrase the internal standard in the middle of the fourth line on the top of p 13 should read the native standard since the phrase more specifically bullbullbullbull refers to the previous statement of calibration curves appearing at the bottom of p 12 In this way the concentrations of the native PCDDPCDF can be determined from the calibration curves We agree with the use of stable isotopically internal standard and the procedures 1) 2) and 3) as the authors described

4

In summary the results reported here are reliable since the Brehm Laboratory is a reputable organization and Dr Tiernan is respected in the scientific community Like in any case of major environmental monitorings and surveys compromises must be made for the sake of the scheduling workload and cost The present investigation is no exception

Sincerely

R C Lao PhD Senior Scientist River Road Environmental

Technology Centre cc M Bumba co

C Chiu

Recommended Safety and Handling Procedures in Connection with Implementing

the Analytical Protocal for Determination of PCDOPCDF in Combustion Products

1 The human toxicology of PCDOPCDF is not well defined at present although the 2378-TCOO isomer has been found ta be acnegenic carcinogenic and teratogenic in the course of laboratory animal studies The 2378-TCOO is a solid at room temperature anq has a relatively low vapor pressure The solubility of this compound in water is only about 200 parts-per-trill ion but the solubility in various organic solvents ranges from about 0001 to 014 The physical properties of the 135 other tetra-through octachlorinaed PCDDPCDF have not been well established although it is presumed that the physical properties of these congeners are generally similar to those of the 2middot137 8-TCDD isomer On the basis of the available toxicological and physical property data for TCDOthis compound as well as the other PCDD and PCOF should be handled only by highly trained personnelwho are thoroughly versed in the appropriate procedures and who understand the associated risks middot

middot2 PCDDPCDF and samples-containing these are haAdled using essentially the same techniques as those employed in handling radioactive or infectious materials Well-ventilated controlled-access laboratories are required amiddotnd laboratory personnel enter1119 these laboratories should wear appropriate safety clothing including disposable coveralls shoe covers gloves and face and head masks During analytical operatiqns which may give rise to aerosols or dusts personnel should wear respirators equipped with activated carbon filters Eye protection equipment (preferably full face shields) must be worn atall times while working in the analytical laboratory with PCDOPCDF middot Various middot types of gloves can be used by personnel depending upon the analytical operation being accomplished Latex gloves are generally utilized and when handling samples thought to be particularly hazardous an additional set of gloves is also worn beneath the latex gloves middot (for example Playtex gloves supplied by American Sci-entific Productsgt Cat No 67216) Bench-tops and other work surfaces in the laboratory should be covered with plastic-backed absorbent paper during all analytical processing When finely divided samples (dusts soil~ dry chemicals) are being processed removal of these from sample containers as well as other operations including weighing transferring and mixing with solvents should all be accomplished within a glove box Glove boxes hoods and the effluents from mechanical vacuum pumps and gas chromatographs on the mass spectrometers should be vented ta the atmosphere preferably only after passing through HEPA particulate filters and vapor-sorbing charcoal

3 All laboratory ware safety clothing and other items potentially contaminated with PCODPCDF in the course of analyses must be carefully secured and subjected to proper disposal When feasible liquid wastes

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_32 l00Xbull377S8


20 40 60 80 lB0 120 SCAN NUMBER


UB

713

I 0 H

I N T E N s I T y



611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

7B

S 4 U 18Hbull 195B

amp U2 1l81bull3928

0 S 12 lB11bull336

H8 U11bull9615

472 lSBlbulll16985



I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull



6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

bullmiddot







-26-

(

___ - -

bullbull



0101 l 1B7 2 14 _ ___________Jl--_l~_1---L--J___j_108 I --L-1---LL--1-~-

S 306 l0SXbull225727 90 L_


71

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I -- - - -0 3 74 11Ubull394

I - -- - - - 328 18BXbull217631

I - - - - - bull 332 1sJxbull169269

~

3122 5137 6U 4 2 9 I

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I 0 N

t N T E N s I T V





ss 1187 2114 3 22 4 l 29 5137 6rU BB

9S

SB

7B

60

SB

~0

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21

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328 1BSXbull2175S8


I 0 H

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--- _





0 34B 1BBXbulll67379 98

338 1BIXbulllB3B27

88

488 1811bull1327 1B

6B

SB

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28

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BdU 11S3 BS

0 356 lBBXbulll02464 98

354 1BSXbull64278

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6B

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10

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2s6 3 sl0 4 r 13 517 6120 724 8127

I 0 N

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50 1S0 150 200 250 303 35S 4IBSCAN NUHBR


-----



BdJl 1 I 26 254 4121 51-49 7116 81U 18B I I

0 376 1BBXbull285B9 98

374 18Blbull36854

8B

444 1881bull969 7B

J 0 N

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2B

1B

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20B 25B 38B


31

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70

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50

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BREHM LABORATORY -


0101 1 I 26 2154



4121 6149 7 I 16 eu 1-~___________________________~-~_______ _______-JL--____________ _ __c________~____________~_____________________________ _ __________

0 392 1BBXbullB8671

39B lBBXbull111571


I 0 H

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- - - -



BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

8B

71

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41

31

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0 478 1BnbullU9

432 l001bull49142

~34 1BBXbulll644I

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0 I 0 11BB 2 102 3 I 04 4106 5108 611 7113 80

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$ H6 1BUbull9771

I - -- - - - -amp 424 1BBXbulllB264

I -- - - - -0 359 l9Ubull6161

I -- - - - - 432 1BSXbull49142


I

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SAMPLE N02A1

188

9B

a

78

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58

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38

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bull

1

6 al 1 6142

----1-----------------~ S 444 1BBXbull1BB72


478 1BBXbull137939


128 13B

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7d3 L1

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a46 9 17 9148


l819

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

S 46B lB81bull12246 90


0 395 1SUbull6838 1B



3B

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FIGURE 51

l

----

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amp 304 as

0 374

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68

332H

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28

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0 257 l081bull945259

328 1081bull381189

bull 332 l801bull127044

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338 1881bull685876

488 bSBlbull392

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206 3 10



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4 a 13 517 6120 7s24 8127

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0181 1 dJ3 2 dJ6 3t 11 4 I 13 5amp17 612S 7124 8127 180

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a - - - - - - - - - - - __ - - - - - - - - 291 1BBlbull76689

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FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

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21

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611 642 7 13 7 44 815 846 9 17 9148 18119 100 ________ 1-1 LiLJ ~

S 460 100bull14529 90

amp 458 1001bull12404 80

0 395 l801bull8383

70

470 1001bull128228 I60 0 N

472 1881bull136872 58

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170 188 ljS 2BB


-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

$ 306 100Xbull218713

90 I - l -2378amp ~~4~IJr 1_1mas

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250

100

90

80

70

60

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30

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611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

7B

S 4 U 18Hbull 195B

amp U2 1l81bull3928

0 S 12 lB11bull336

H8 U11bull9615

472 lSBlbulll16985



I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull



6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

(

___ - -

bullbull



0101 l 1B7 2 14 _ ___________Jl--_l~_1---L--J___j_108 I --L-1---LL--1-~-

S 306 l0SXbull225727 90 L_


71

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I - -- - - - 328 18BXbull217631

I - - - - - bull 332 1sJxbull169269

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3122 5137 6U 4 2 9 I

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I 0 N

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ss 1187 2114 3 22 4 l 29 5137 6rU BB

9S

SB

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60

SB

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328 1BSXbull2175S8


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--- _





0 34B 1BBXbulll67379 98

338 1BIXbulllB3B27

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488 1811bull1327 1B

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0 356 lBBXbulll02464 98

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2s6 3 sl0 4 r 13 517 6120 724 8127

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50 1S0 150 200 250 303 35S 4IBSCAN NUHBR


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BdJl 1 I 26 254 4121 51-49 7116 81U 18B I I

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374 18Blbull36854

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20B 25B 38B


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BREHM LABORATORY -


0101 1 I 26 2154



4121 6149 7 I 16 eu 1-~___________________________~-~_______ _______-JL--____________ _ __c________~____________~_____________________________ _ __________

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- - - -



BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

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0 395 1SUbull6838 1B



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FIGURE 51

l

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amp 304 as

0 374

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68

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FIGURE 58



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amp 458 1001bull12404 80

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170 188 ljS 2BB


-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

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100

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amp 320 100Xbull404109

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472 lSBlbulll16985



I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull



6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

___ - -

bullbull



0101 l 1B7 2 14 _ ___________Jl--_l~_1---L--J___j_108 I --L-1---LL--1-~-

S 306 l0SXbull225727 90 L_


71

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I -- - - -0 3 74 11Ubull394

I - -- - - - 328 18BXbull217631

I - - - - - bull 332 1sJxbull169269

~

3122 5137 6U 4 2 9 I

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I 0 N

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ss 1187 2114 3 22 4 l 29 5137 6rU BB

9S

SB

7B

60

SB

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328 1BSXbull2175S8


I 0 H

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--- _





0 34B 1BBXbulll67379 98

338 1BIXbulllB3B27

88

488 1811bull1327 1B

6B

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BdU 11S3 BS

0 356 lBBXbulll02464 98

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6B

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2s6 3 sl0 4 r 13 517 6120 724 8127

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50 1S0 150 200 250 303 35S 4IBSCAN NUHBR


-----



BdJl 1 I 26 254 4121 51-49 7116 81U 18B I I

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374 18Blbull36854

8B

444 1881bull969 7B

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20B 25B 38B


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BREHM LABORATORY -


0101 1 I 26 2154



4121 6149 7 I 16 eu 1-~___________________________~-~_______ _______-JL--____________ _ __c________~____________~_____________________________ _ __________

0 392 1BBXbullB8671

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- - - -



BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

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432 l001bull49142

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0 I 0 11BB 2 102 3 I 04 4106 5108 611 7113 80

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I -- - - - -0 359 l9Ubull6161

I -- - - - - 432 1BSXbull49142


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SAMPLE N02A1

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

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0 395 1SUbull6838 1B



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FIGURE 51

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amp 304 as

0 374

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68

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FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

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-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

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100

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amp 320 100Xbull404109

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S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu



ss 1187 2114 3 22 4 l 29 5137 6rU BB

9S

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7B

60

SB

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3B

21

1e

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328 1BSXbull2175S8


I 0 H

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--- _





0 34B 1BBXbulll67379 98

338 1BIXbulllB3B27

88

488 1811bull1327 1B

6B

SB

48

3B

28

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BdU 11S3 BS

0 356 lBBXbulll02464 98

354 1BSXbull64278

SB


6B

se

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2B

10

s

2s6 3 sl0 4 r 13 517 6120 724 8127

I 0 N

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50 1S0 150 200 250 303 35S 4IBSCAN NUHBR


-----



BdJl 1 I 26 254 4121 51-49 7116 81U 18B I I

0 376 1BBXbull285B9 98

374 18Blbull36854

8B

444 1881bull969 7B

J 0 N

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2B

1B

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20B 25B 38B


31

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50

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lB

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BREHM LABORATORY -


0101 1 I 26 2154



4121 6149 7 I 16 eu 1-~___________________________~-~_______ _______-JL--____________ _ __c________~____________~_____________________________ _ __________

0 392 1BBXbullB8671

39B lBBXbull111571


I 0 H

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- - - -



BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

8B

71

61

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41

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0 478 1BnbullU9

432 l001bull49142

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0 I 0 11BB 2 102 3 I 04 4106 5108 611 7113 80

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I -- - - - -0 359 l9Ubull6161

I -- - - - - 432 1BSXbull49142


I

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SAMPLE N02A1

188

9B

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58

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38

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bull

1

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----1-----------------~ S 444 1BBXbull1BB72


478 1BBXbull137939


128 13B

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a46 9 17 9148


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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

S 46B lB81bull12246 90


0 395 1SUbull6838 1B



3B

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FIGURE 51

l

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B26 100 ~ _

S 306 91J --

amp 304 as

0 374

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68

332H

b

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28

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0 257 l081bull945259

328 1081bull381189

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338 1881bull685876

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BREHM LABORATORY -


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4 a 13 517 6120 7s24 8127

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FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

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611 642 7 13 7 44 815 846 9 17 9148 18119 100 ________ 1-1 LiLJ ~

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170 188 ljS 2BB


-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

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032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

--- _





0 34B 1BBXbulll67379 98

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0 356 lBBXbulll02464 98

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50 1S0 150 200 250 303 35S 4IBSCAN NUHBR


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374 18Blbull36854

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20B 25B 38B


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BREHM LABORATORY -


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MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

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MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu



BdU 11S3 BS

0 356 lBBXbulll02464 98

354 1BSXbull64278

SB


6B

se

u

3B

2B

10

s

2s6 3 sl0 4 r 13 517 6120 724 8127

I 0 N

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50 1S0 150 200 250 303 35S 4IBSCAN NUHBR


-----



BdJl 1 I 26 254 4121 51-49 7116 81U 18B I I

0 376 1BBXbull285B9 98

374 18Blbull36854

8B

444 1881bull969 7B

J 0 N

6B

J N

5B T E N s I T V

38

2B

1B

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20B 25B 38B


31

SS

90

as

70

6B

50

u

2B

lB

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BREHM LABORATORY -


0101 1 I 26 2154



4121 6149 7 I 16 eu 1-~___________________________~-~_______ _______-JL--____________ _ __c________~____________~_____________________________ _ __________

0 392 1BBXbullB8671

39B lBBXbull111571


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- - - -



BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

8B

71

61

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0 478 1BnbullU9

432 l001bull49142

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0 I 0 11BB 2 102 3 I 04 4106 5108 611 7113 80

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I - -- - - - -amp 424 1BBXbulllB264

I -- - - - -0 359 l9Ubull6161

I -- - - - - 432 1BSXbull49142


I

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SAMPLE N02A1

188

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58

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bull

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----1-----------------~ S 444 1BBXbull1BB72


478 1BBXbull137939


128 13B

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

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0 395 1SUbull6838 1B



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FIGURE 51

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amp 304 as

0 374

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68

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0126 11S7 2 I 14 3t22 4129 5137 6U 180

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40

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0 257 l081bull945259

328 1081bull381189

bull 332 l801bull127044

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25S

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I= IGURE t 53

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81

78

68

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338 1881bull685876

488 bSBlbull392

BREHM LABORATORY -


206 3 10



OHIO 45435


4 a 13 517 6120 7s24 8127

J 0 N

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0181 1 dJ3 2 dJ6 3t 11 4 I 13 5amp17 612S 7124 8127 180

0 356 llBXbulll95796 99

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a - - - - - - - - - - - __ - - - - - - - - 291 1BBlbull76689

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37-4 1SSSbull93483


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BdJl l 1 26 2154 4amp21 5 I 9 7t16 eH 180

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329 1811bull31738 7B

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FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

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170 188 ljS 2BB


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001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

$ 306 100Xbull218713

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100

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$ 322 1001bull532633

amp 320 100Xbull404109

0 257 1BBXbull219683

328 1BBXbulll94431

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254 4 21 5 I 49 7 16 Si 44 100

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70


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9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

-----



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374 18Blbull36854

8B

444 1881bull969 7B

J 0 N

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38

2B

1B

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20B 25B 38B


31

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90

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70

6B

50

u

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lB

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BREHM LABORATORY -


0101 1 I 26 2154



4121 6149 7 I 16 eu 1-~___________________________~-~_______ _______-JL--____________ _ __c________~____________~_____________________________ _ __________

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BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

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338 1881bull685876

488 bSBlbull392

BREHM LABORATORY -


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4 a 13 517 6120 7s24 8127

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0181 1 dJ3 2 dJ6 3t 11 4 I 13 5amp17 612S 7124 8127 180

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FIGURE 58



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170 188 ljS 2BB


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001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

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$ 322 1001bull532633

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100

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20 40 60 80 lB0 120 SCAN NUMBER


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611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

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0 395 UUbull48 l 7

70


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I N T

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30 T y

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10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

31

SS

90

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70

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50

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2B

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0101 1 I 26 2154



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BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

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0 478 1BnbullU9

432 l001bull49142

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-----_



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20 40 60 80 lB0 120 SCAN NUMBER


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611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

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0 395 UUbull48 l 7

70


0 N


I N T

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30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

- - - -



BaBl 1 BB 202 3104 4 B6 5108 6 I 11 713 BB

91

8B

71

61

6B

41

31

2B

11

I



0 478 1BnbullU9

432 l001bull49142

~34 1BBXbulll644I

I 0 N

I

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0 I 0 11BB 2 102 3 I 04 4106 5108 611 7113 80

90

89

7B

I6B 0 N


2B

11

B

fIGUftE 1 49

l_j _______________________________~_______--____________________________-+_________ ____________~___~__________~__-J~------~J-____________-t-

$ H6 1BUbull9771

I - -- - - - -amp 424 1BBXbulllB264

I -- - - - -0 359 l9Ubull6161

I -- - - - - 432 1BSXbull49142


I

I

2B

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SAMPLE N02A1

188

9B

a

78

6B

58

4B

38

2B

1B

bull

1

6 al 1 6142

----1-----------------~ S 444 1BBXbull1BB72


478 1BBXbull137939


128 13B

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7d3 L1

71U 8115



a46 9 17 9148


l819

218

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

S 46B lB81bull12246 90


0 395 1SUbull6838 1B



3B

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68

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90

80

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0 257 l081bull945259

328 1081bull381189

bull 332 l801bull127044

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158 20B SCAN HUMBER


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338 1881bull685876

488 bSBlbull392

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4 a 13 517 6120 7s24 8127

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0181 1 dJ3 2 dJ6 3t 11 4 I 13 5amp17 612S 7124 8127 180

0 356 llBXbulll95796 99

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a - - - - - - - - - - - __ - - - - - - - - 291 1BBlbull76689

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1s1 1126 254 4s21 Sa49 7116 81U

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0 392 lSUbull-43858 91

396 18Slbull661ll

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329 1811bull31738 7B

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FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

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611 642 7 13 7 44 815 846 9 17 9148 18119 100 ________ 1-1 LiLJ ~

S 460 100bull14529 90

amp 458 1001bull12404 80

0 395 l801bull8383

70

470 1001bull128228 I60 0 N

472 1881bull136872 58

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30

20

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120 130 140 150 160 SCAN NUMBER

170 188 ljS 2BB


-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

$ 306 100Xbull218713

90 I - l -2378amp ~~4~IJr 1_1mas

0 3H 18 bull1860

7B


SB

I=~ 0 N

332 10 bull136251 58

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250

100

90

80

70

60

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$ 322 1001bull532633

amp 320 100Xbull404109

0 257 1BBXbull219683

328 1BBXbulll94431

~ 332 IBBXbull28B34

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-------_-----------------------------~



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322 4129 5s37 6144 ~-1--A--L---L-L--L--------J---------_______~ __-L-__________~__~__L-__~-----------_-+-

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0 340 l00Xbull270473 90

338 l00Xbull158177

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1 03 2 06 3 zl0 4 13 517 6120 724 8127 I

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291 lS01bull261351

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254 4 21 5 I 49 7 16 Si 44 100

90

88

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0 376 100Xbull27922

374 1BBXbull34690

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421 5 C9 7 s 16 au

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001 1 10kJ 2102 3104 4 I 06 5 I 08 6 1 1 7 13


FIGURE1 140

100

90

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48

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0 478 lBBlbull(59

432 1BBXbull3837B

2B -B 60 80 lB0 12B U0

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$ 426 1BBXbull19300

amp 424 lB0bull19678 =~ 0 359

432 J 0 N

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$ 44 100Xbull5256

90



470 1BBXbull113177 68 I

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472 1SBXbulll19359 68

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0 374 l08bull538 70

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-----_



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4 21 5149 7 I 16 urn

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99

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70


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9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu



0 I 0 11BB 2 102 3 I 04 4106 5108 611 7113 80

90

89

7B

I6B 0 N


2B

11

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fIGUftE 1 49

l_j _______________________________~_______--____________________________-+_________ ____________~___~__________~__-J~------~J-____________-t-

$ H6 1BUbull9771

I - -- - - - -amp 424 1BBXbulllB264

I -- - - - -0 359 l9Ubull6161

I -- - - - - 432 1BSXbull49142


I

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SAMPLE N02A1

188

9B

a

78

6B

58

4B

38

2B

1B

bull

1

6 al 1 6142

----1-----------------~ S 444 1BBXbull1BB72


478 1BBXbull137939


128 13B

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7d3 L1

71U 8115



a46 9 17 9148


l819

218

I 0 N

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

S 46B lB81bull12246 90


0 395 1SUbull6838 1B



3B

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FIGURE 51

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328 1081bull381189

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338 1881bull685876

488 bSBlbull392

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206 3 10



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4 a 13 517 6120 7s24 8127

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0 356 llBXbulll95796 99

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a - - - - - - - - - - - __ - - - - - - - - 291 1BBlbull76689

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0 392 lSUbull-43858 91

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329 1811bull31738 7B

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FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

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amp 458 1001bull12404 80

0 395 l801bull8383

70

470 1001bull128228 I60 0 N

472 1881bull136872 58

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30

20

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120 130 140 150 160 SCAN NUMBER

170 188 ljS 2BB


-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

$ 306 100Xbull218713

90 I - l -2378amp ~~4~IJr 1_1mas

0 3H 18 bull1860

7B


SB

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332 10 bull136251 58

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250

100

90

80

70

60

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30

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BREHM LABORATORY



$ 322 1001bull532633

amp 320 100Xbull404109

0 257 1BBXbull219683

328 1BBXbulll94431

~ 332 IBBXbull28B34

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-------_-----------------------------~



3BB



322 4129 5s37 6144 ~-1--A--L---L-L--L--------J---------_______~ __-L-__________~__~__L-__~-----------_-+-

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0 340 l00Xbull270473 90

338 l00Xbull158177

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250 300 3U UB




081 __~ I

1 03 2 06 3 zl0 4 13 517 6120 724 8127 I

0 356 100Xbull723886

354 1BBXbull44618S

291 lS01bull261351

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Z5B 3IB 35g

sAUhE Nob1 488

0 0middot 1 1 26



254 4 21 5 I 49 7 16 Si 44 100

90

88

78

69

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0 376 100Xbull27922

374 1BBXbull34690

4U 10BXbulll US



I 0 N

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98

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39B 1SSXbull7512SC

329 1SSXbull2513Sl

SELECTED-ION

254


421 5 C9 7 s 16 au

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rt F 1 4



001 1 10kJ 2102 3104 4 I 06 5 I 08 6 1 1 7 13


FIGURE1 140

100

90

80

7B

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48

38

28

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S 419 100Xbull5537

amp us 10Ubull5735

0 478 lBBlbull(59

432 1BBXbull3837B

2B -B 60 80 lB0 12B U0

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1001bull38370

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$ 426 1BBXbull19300

amp 424 lB0bull19678 =~ 0 359

432 J 0 N

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$ 44 100Xbull5256

90



470 1BBXbull113177 68 I

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472 1SBXbulll19359 68

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FtGUREc 142




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0 374 l08bull538 70

328 l00bull187587 60

332 lB0bull48368 58

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214 322 429 537 6 44 I t_LL-J I ~L____amp_________________~~-t-


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0 340 l00bull708382

338 1BBl 43537

408 10BXbull 1 U8

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001 1 26 254 4 21 549 7 16 8 44 100

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80

70

60

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O 392 l00Xm574544

390 l00Xbull714164

329 l00Xbull231249

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0 359 130ibull19179 78

432 1B0Xbull21734 60 i I

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0 392 l00Xbull3594

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472 lB0bull27937

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FIGURE 273

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611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

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amp U2 1l81bull3928

0 S 12 lB11bull336

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0 395 UUbull48 l 7

70


0 N


I N T

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30 T y

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B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

188

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78

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128 13B

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611 6142 7 I 13 7U 8d5 8146 9 r17 9e 18119 100

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66 N

bull 332 100Xbull139676 50 I

NJ ij1 T

EU ~~ I I I

I

N st ~ j

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lB

B

__

---- ________



FIGURE 274

58 3BB

90



0dJ1 11 B7 2 tl 4 3122 4129 5137 6144 100

80

7B

6B

SB

HJ

3B

2B

lB

B

S 322 1SBXbull15266

amp 320 UUbull12126

0 257 10BXbull2Sss

328 1SBXbull18B436

bull 332 1BBXbull139676 2378-

_______ II w ~


I 0 N

I N T E N s I T v-


20H 250 308


si



Bs01 1 03 2 06 31 HJ 4 13 5 17 6120 7r2~ 8127 100

98

88

78

68

38

28

18

B

0 348 1BBXbull19517

338 1801bull12581


I 0 N

I N T E N s I T V



01Bl 1 a03 190

0 356 108bull16949 98

354 1BBbull11BB2

as

291 l981bull7518 70

68

58

u

if

28

10

s

61



bull

2 l 06

1BB

3d0

15B

4 r13 517 6120 7124 8127


I 0 N

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FIGUFlEs 277



B81 126 254 421 549 716 eu 100

0 376 100Xbull8363 9f

374 1BBXbull2488

8f


6B

51

46

u

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I 0 N

[ N T E N s [ T V

8


BdJl 1 26 2154 100

0 392 1B0Xbull57348 90

as

70

bull

398

329

lS8Xbull69492

l88rbull2616

6B

58

u

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18

4 I 21 5r49 7 I 16 au

I 0 N

I N T E N s 1 T V

58 108 158 288 258 3BB SCAN NUMBER


Li1-U1r LAUVKA1( l

l i


OSS5 MASS

0101 l 1BB 2 02

0



304 4 dJ6 5dJ8 611 7 ll3 IBB

98

SB

7B

68

68

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2bull bullbull bull


$ -tlB lBBKa-699

amp cee 1snbulls119

0 478 lB81bull618



1~

l

I

I 0 N

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BttrnM LABORATO~V


0101 1 100 2 d32



3s04 4 dY6 5 I 08 6 cl 1 7 I 13 100

90

80

78

6B

SB

40

30

2B

lB

B

----L----J-l----1-__~____ _ __________~~__---__-~_ _______________~____~_____~_________J_1---L----L-4---1--------_~--- __-________--1i-- ______~~__~--

$ C26 l0Ubull7199


0 359 1B0Xbull5150

t32 100Xbull-SB17

C3t 1BSbull14524


I 0 N

I N T E N s 1 T y

10






90


7B -l - - -- - -- -- -- ~70 1001bull126296

(60 0 N

~72 100yenbull134721 50

I

n1 N T E N

48 l1

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30

26

I II I

I

UJ

J-1middot I

B II




------------------------ -~ --- ----- --i



-~ I --~ ______ y------ -(j


--



6 l 1 642 l 13 7 44 8 I 15 846 9 I 17 9148 10 l 19 lJj(T


-l)--

___L__l_JJ__I 1 H 0 10 flt Xbull 17 8 9 4 1


120 139 140 150 160 SCAN NUMDFR

17~ 180 190 2BS


80 O 3 l0flXm90U

7S


~ 50

40

3S

20

10

B


E N s I TI I y

1

----------------------- II I k------ ------- ------------- I r---__~-------------_____ middot-~---------~~----- ----------~~ --- -~ -

J

-___


~-


middotbullI

I 0 N

I N T

~ tgt~- -



B12B 11B7 2 14 3r22 4 I 29 5137 61H 10B

9B

es

11



0 374 lB91bull562



15 50

~I ~I

V

-l 318

I6B 0 N


30

20

18

f6





100 B 20 1107 2 14 3122 4 I 29 5137 61U

S 322 1BBXbull1B4988 90


0 257 lB0bull51649

7B

6B 328 1BBXbull161437


u

38

2B

lB

0

I 0 N

I N T E N s I T y



15 50

~-

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98

80

7B

60

50

AB

38

2B

10

B

0101 1 dJ3 _J_j________________

O 3-0 1SSXbull98U4

338 1081bull59894

488 108bull393

L~

BREHM LABORATORY -


2106 3110

I



4 r13 517 6120 I

7124 8127

I 0 N

I N T E N s I T V

I 58 10B 150 200 250 3BB 35B


FIGURE1 435

- - - - -



100

90

80

70

0s01

0 356

35(

291

1 s03

1BSXbull68382

10SXbull~J((1

1SBXbull256(5

2 dY6

60

58

u

38

28

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JI 0 ( I 13 5 I 1 7 6120 7s2( 8t27

--1 - - - - - - - - - - - - - - - -

l 0 N

I N T E N s I T y


250 300 35B UB


middot-

BiSl 1 26



2 5 ( 4 2i middot 5 l ( 9 7 I 1 6 eu 100

0 376 1BBXbull24486 9B


as


6B

SB

u

3B

20

lB

B

50

middotmiddot1 I

100 150 200 25B I I I f r-r-

I 0 N

I N T E N s I T V

3IBSCAN NUMBER




Bs01 1 I 26 254 BB

0 392 1SSXbull74894 9B

391 1BBlbull95154

as

329 1SBXbull3330 7B

6B

SB

u

3B

2B

lB

B


4 21 549 7 I 16 su I

I 0 N

I N T E N s I T V



if






90

as

70

6B

5f

u

31

2B

11

B

S 41B 1BBlbull88U


0 HB U81bull1319

432 l00bull35776

2S 4B 6B BB 198 128

I 0 N

I N T E N s I T y

us SCAN NUMBER


-

t



Sa01 1 es 2 I 02 3r04 41B6 Sr08 6111 7113 100

90

as

7B

68

SB

U

3B

2B

10

g

S 426 10BXbull11647


0 359 100yenbull8992

02 100Xbull35776

434 1SBXbull11738

U 61 8B 1B0 120 1482B

I 0 N

I N T E N s I T V


F GUR E 1 440

~



6111 6142 7113 71U Br15 8146 9 al 7 9148 18bull 19 0B

98

80

7B

60

50

u

30

2B

lB

B

S 4U 18Ubulll 922

amp HZ 1BBXbull3928

0 512 18BXbull2298

47S l00Xbull99315



178 18B 2bullbull

I 0 N

I N T E N s I T V

19B


11



6 s 11 6 l -2 7 I 13 7U 8 I 15 lBB



0 395 U0bull5932 7B

1s 1BBXbull99315 6B


U

39

2B

B

128 130 140 150 160


8146 9 l 7 948 Us 19

190

I 0 N

I N TE N s I T y



I

I I I

r11111w It 1 11 j

i M bull

I

-~






80

0 374 l0HXbull878 78


58 ~ I (

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_____ --- bull middot- ______ ___________ ~~--- ~

-f




~L_

I 0 N

I N T E N s l T y

j I i

68



Bs01 1 I 07 l0B



0 257 UBXbull UBS4

7B

32e nssx-11132


U

30

2B

1B

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2 1 4 3122 4129 5137 61U

-2378

I 0 H

I N T E N s I T V



0Bl 1 a13 us

0 3U 1BUbull91856 90


80


ampbull

u

As

3B

2B

UJ

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50 358 U8

I-



2106 3 1 lB 413 Sal 7 6s2S 7 I 2- 8127

I 0 H

I N T

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100 ss1 l c03 2 06 3 l 0 4 13 5 l 1 7 6120 7amp24 8127

98 0 356 100Xbull22351

80

7B

bull

354

291

U8Xbull1bull27B

1BUbull97B3

6B

5

u

38

28

1B

0

SB 108 150 280



I 0 H

I N T E H s I T y



81 1126 2154 4121 5149 7 I 16 8 bull4 BB

0 376 1SSlbull23517 9S

374 1861bull28844

88

4U lSS1bull2386 78

u

s

38

2B

18

bull

58


25B

I 0 N

I N T E N s I T V

3SB


11

B01 1 26 lBB



254 4 21 549 7 I 16 81H

98

88

7B

68

58

48

38

2B

0

392 UBXbull2332B ----------

398 1BSXbull3874

329 1Bflbull128B7

I 0 N

I N T E N s I T V



-- - - -

- - - -

- - -

- - - -



r


S us 1881bull18723


88

0 HS 18Ubull 12B7 78 -



u

38

28

18

B

I 0 N

I N T E N s I T y



L 1 1)gtLlJl(AIURr


2102



3 104 4 I 06 5 08 6 rl 1 180

9g

80

70

68

SB

u

30

2B

lB

0d31 1 dHJ

S _26 100Xbull8101

amp _2 100Xbull7791

- - - -0 359 l0BXbull8848

_32 l00Xbull377S8


20 40 60 80 lB0 120 SCAN NUMBER


UB

713

I 0 H

I N T E N s I T y



611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

7B

S 4 U 18Hbull 195B

amp U2 1l81bull3928

0 S 12 lB11bull336

H8 U11bull9615

472 lSBlbulll16985



I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull



6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu



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E N s I TI I y

1

----------------------- II I k------ ------- ------------- I r---__~-------------_____ middot-~---------~~----- ----------~~ --- -~ -

J

-___


~-


middotbullI

I 0 N

I N T

~ tgt~- -



B12B 11B7 2 14 3r22 4 I 29 5137 61H 10B

9B

es

11



0 374 lB91bull562



15 50

~I ~I

V

-l 318

I6B 0 N


30

20

18

f6





100 B 20 1107 2 14 3122 4 I 29 5137 61U

S 322 1BBXbull1B4988 90


0 257 lB0bull51649

7B

6B 328 1BBXbull161437


u

38

2B

lB

0

I 0 N

I N T E N s I T y



15 50

~-

BB

98

80

7B

60

50

AB

38

2B

10

B

0101 1 dJ3 _J_j________________

O 3-0 1SSXbull98U4

338 1081bull59894

488 108bull393

L~

BREHM LABORATORY -


2106 3110

I



4 r13 517 6120 I

7124 8127

I 0 N

I N T E N s I T V

I 58 10B 150 200 250 3BB 35B


FIGURE1 435

- - - - -



100

90

80

70

0s01

0 356

35(

291

1 s03

1BSXbull68382

10SXbull~J((1

1SBXbull256(5

2 dY6

60

58

u

38

28

lB

B

JI 0 ( I 13 5 I 1 7 6120 7s2( 8t27

--1 - - - - - - - - - - - - - - - -

l 0 N

I N T E N s I T y


250 300 35B UB


middot-

BiSl 1 26



2 5 ( 4 2i middot 5 l ( 9 7 I 1 6 eu 100

0 376 1BBXbull24486 9B


as


6B

SB

u

3B

20

lB

B

50

middotmiddot1 I

100 150 200 25B I I I f r-r-

I 0 N

I N T E N s I T V

3IBSCAN NUMBER




Bs01 1 I 26 254 BB

0 392 1SSXbull74894 9B

391 1BBlbull95154

as

329 1SBXbull3330 7B

6B

SB

u

3B

2B

lB

B


4 21 549 7 I 16 su I

I 0 N

I N T E N s I T V



if






90

as

70

6B

5f

u

31

2B

11

B

S 41B 1BBlbull88U


0 HB U81bull1319

432 l00bull35776

2S 4B 6B BB 198 128

I 0 N

I N T E N s I T y

us SCAN NUMBER


-

t



Sa01 1 es 2 I 02 3r04 41B6 Sr08 6111 7113 100

90

as

7B

68

SB

U

3B

2B

10

g

S 426 10BXbull11647


0 359 100yenbull8992

02 100Xbull35776

434 1SBXbull11738

U 61 8B 1B0 120 1482B

I 0 N

I N T E N s I T V


F GUR E 1 440

~



6111 6142 7113 71U Br15 8146 9 al 7 9148 18bull 19 0B

98

80

7B

60

50

u

30

2B

lB

B

S 4U 18Ubulll 922

amp HZ 1BBXbull3928

0 512 18BXbull2298

47S l00Xbull99315



178 18B 2bullbull

I 0 N

I N T E N s I T V

19B


11



6 s 11 6 l -2 7 I 13 7U 8 I 15 lBB



0 395 U0bull5932 7B

1s 1BBXbull99315 6B


U

39

2B

B

128 130 140 150 160


8146 9 l 7 948 Us 19

190

I 0 N

I N TE N s I T y



I

I I I

r11111w It 1 11 j

i M bull

I

-~






80

0 374 l0HXbull878 78


58 ~ I (

I It

-0

38

1jmiddot ~j Iv fv i

f1II Ii I I I I

J(

28



- - I111 J-J1 _-__ j ~j ~ ~rJt ~-~ J ~1 ----------- J

_ -_) 11 ----middot I

r~ _____ -------------~-- ------bullbull A f

_____ --- bull middot- ______ ___________ ~~--- ~

-f




~L_

I 0 N

I N T E N s l T y

j I i

68



Bs01 1 I 07 l0B



0 257 UBXbull UBS4

7B

32e nssx-11132


U

30

2B

1B

B

2 1 4 3122 4129 5137 61U

-2378

I 0 H

I N T E N s I T V



0Bl 1 a13 us

0 3U 1BUbull91856 90


80


ampbull

u

As

3B

2B

UJ

B

50 358 U8

I-



2106 3 1 lB 413 Sal 7 6s2S 7 I 2- 8127

I 0 H

I N T

~ s t T y





100 ss1 l c03 2 06 3 l 0 4 13 5 l 1 7 6120 7amp24 8127

98 0 356 100Xbull22351

80

7B

bull

354

291

U8Xbull1bull27B

1BUbull97B3

6B

5

u

38

28

1B

0

SB 108 150 280



I 0 H

I N T E H s I T y



81 1126 2154 4121 5149 7 I 16 8 bull4 BB

0 376 1SSlbull23517 9S

374 1861bull28844

88

4U lSS1bull2386 78

u

s

38

2B

18

bull

58


25B

I 0 N

I N T E N s I T V

3SB


11

B01 1 26 lBB



254 4 21 549 7 I 16 81H

98

88

7B

68

58

48

38

2B

0

392 UBXbull2332B ----------

398 1BSXbull3874

329 1Bflbull128B7

I 0 N

I N T E N s I T V



-- - - -

- - - -

- - -

- - - -



r


S us 1881bull18723


88

0 HS 18Ubull 12B7 78 -



u

38

28

18

B

I 0 N

I N T E N s I T y



L 1 1)gtLlJl(AIURr


2102



3 104 4 I 06 5 08 6 rl 1 180

9g

80

70

68

SB

u

30

2B

lB

0d31 1 dHJ

S _26 100Xbull8101

amp _2 100Xbull7791

- - - -0 359 l0BXbull8848

_32 l00Xbull377S8


20 40 60 80 lB0 120 SCAN NUMBER


UB

713

I 0 H

I N T E N s I T y



611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

7B

S 4 U 18Hbull 195B

amp U2 1l81bull3928

0 S 12 lB11bull336

H8 U11bull9615

472 lSBlbulll16985



I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull



6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

----

- --- - - --- - - ---



B26 100 ~ _

S 306 91J --

amp 304 as

0 374

1B 328

68

332H

b

3B

28

19

B

liB7


lB01bull1252541

1BBXbull1BB7291

1BUbullC2

lBBXbull38lnB9

1B8Xbull12~9CC

=

II

-J

___ ______-~-

I SB lBB

214


~-~ l LJ--L__L -~-1II -2378 _

I 0 Nmiddot

l N T E N s I T V

-11-( -~-

I~-~ I I I



29



0126 11S7 2 I 14 3t22 4129 5137 6U 180

90

80

7B

6B

SB

40

30

2B

18

B

2S 50

~~



0 257 l081bull945259

328 1081bull381189

bull 332 l801bull127044

I ~

lBS

HR~t-L~~i

158 20B SCAN HUMBER


25S

~o~iz 3BB

I= IGURE t 53

1 0 N

I N T E N s I T V

~ --~--

106

98

81

78

68

5B

U

3B

20

lB

B

SB

8 s81 1 I f3


338 1881bull685876

488 bSBlbull392

BREHM LABORATORY -


206 3 10



OHIO 45435


4 a 13 517 6120 7s24 8127

J 0 N

J

T E N s ~ N

I T V

~





0181 1 dJ3 2 dJ6 3t 11 4 I 13 5amp17 612S 7124 8127 180

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-~






80

0 374 l0HXbull878 78


58 ~ I (

I It

-0

38

1jmiddot ~j Iv fv i

f1II Ii I I I I

J(

28



- - I111 J-J1 _-__ j ~j ~ ~rJt ~-~ J ~1 ----------- J

_ -_) 11 ----middot I

r~ _____ -------------~-- ------bullbull A f

_____ --- bull middot- ______ ___________ ~~--- ~

-f




~L_

I 0 N

I N T E N s l T y

j I i

68



Bs01 1 I 07 l0B



0 257 UBXbull UBS4

7B

32e nssx-11132


U

30

2B

1B

B

2 1 4 3122 4129 5137 61U

-2378

I 0 H

I N T E N s I T V



0Bl 1 a13 us

0 3U 1BUbull91856 90


80


ampbull

u

As

3B

2B

UJ

B

50 358 U8

I-



2106 3 1 lB 413 Sal 7 6s2S 7 I 2- 8127

I 0 H

I N T

~ s t T y





100 ss1 l c03 2 06 3 l 0 4 13 5 l 1 7 6120 7amp24 8127

98 0 356 100Xbull22351

80

7B

bull

354

291

U8Xbull1bull27B

1BUbull97B3

6B

5

u

38

28

1B

0

SB 108 150 280



I 0 H

I N T E H s I T y



81 1126 2154 4121 5149 7 I 16 8 bull4 BB

0 376 1SSlbull23517 9S

374 1861bull28844

88

4U lSS1bull2386 78

u

s

38

2B

18

bull

58


25B

I 0 N

I N T E N s I T V

3SB


11

B01 1 26 lBB



254 4 21 549 7 I 16 81H

98

88

7B

68

58

48

38

2B

0

392 UBXbull2332B ----------

398 1BSXbull3874

329 1Bflbull128B7

I 0 N

I N T E N s I T V



-- - - -

- - - -

- - -

- - - -



r


S us 1881bull18723


88

0 HS 18Ubull 12B7 78 -



u

38

28

18

B

I 0 N

I N T E N s I T y



L 1 1)gtLlJl(AIURr


2102



3 104 4 I 06 5 08 6 rl 1 180

9g

80

70

68

SB

u

30

2B

lB

0d31 1 dHJ

S _26 100Xbull8101

amp _2 100Xbull7791

- - - -0 359 l0BXbull8848

_32 l00Xbull377S8


20 40 60 80 lB0 120 SCAN NUMBER


UB

713

I 0 H

I N T E N s I T y



611 6142 7 I 13 71U 8 I 15 846 917 9amp~8 l8119 UB

99

BB

7B

S 4 U 18Hbull 195B

amp U2 1l81bull3928

0 S 12 lB11bull336

H8 U11bull9615

472 lSBlbulll16985



I6B 0 N

SB I N T

u E N s I

3B T y

21

lB

B

129 131 191 2bullbull



6 11 6c42 7 I 13 744 8 15 846 9 17 9148 Uh 19 lSS

S 46B 1BBXbull8793

9B


0 395 UUbull48 l 7

70


0 N


I N T

U E N s I

30 T y

2B

10

B





9651 M9AM3 04218 srAcf





MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

kPa

Pa

MM

395 in

162 sqft

3006 inHs

-250 inH20

032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu



0126 11S7 2 I 14 3t22 4129 5137 6U 180

90

80

7B

6B

SB

40

30

2B

18

B

2S 50

~~



0 257 l081bull945259

328 1081bull381189

bull 332 l801bull127044

I ~

lBS

HR~t-L~~i

158 20B SCAN HUMBER


25S

~o~iz 3BB

I= IGURE t 53

1 0 N

I N T E N s I T V

~ --~--

106

98

81

78

68

5B

U

3B

20

lB

B

SB

8 s81 1 I f3


338 1881bull685876

488 bSBlbull392

BREHM LABORATORY -


206 3 10



OHIO 45435


4 a 13 517 6120 7s24 8127

J 0 N

J

T E N s ~ N

I T V

~





0181 1 dJ3 2 dJ6 3t 11 4 I 13 5amp17 612S 7124 8127 180

0 356 llBXbulll95796 99

3sbull 11r amp1s1

a - - - - - - - - - - - __ - - - - - - - - 291 1BBlbull76689

7B t 0 N

u I H

iS T E H s I T V

39

ZB

1B

61 1e 150 209 281 3BS 3~- SCAN HUMBER


--



1s1 1126 254 4s21 Sa49 7116 81U

188

98

u

1bull

18

51

31

21

11

bull


37-4 1SSSbull93483


t JI I M T E

l N

V


FlGUREt 56



BdJl l 1 26 2154 4amp21 5 I 9 7t16 eH 180

0 392 lSUbull-43858 91

396 18Slbull661ll

BB

329 1811bull31738 7B

6f

68

ti

38

28

18

l 0 N

l N T

R s I T V

5S 1SS 1af SOAN

u nNUBE

2SI 1SS 31S





70 ldeg ~8~088~ - - - - - - - _ ~ 6S - ~ - A - - --1 ~2~m-~z~


41

30

28

13

8

j~I

IV

I

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l i

V

~-----~ 1- ---- ~ I __---J~~

I I I ---- 1

1 ZS AB 6B


5 dJB I I I ---~--4---__~__J_L-L

BB 188

6 14B

6111 7 sl 3 ~ I I I I I

I

-~ I

-t-i

j I I- I

I 0 N

I N T E N s I T V


FIGURE 58



SdJl 1 tH 2 I 02 3 I 04 4t06 5 3 08 6amp11 7 a13 108

9S

ee

1B

I6B 0 N

u ~ EU N s I T3S y

21

18

B

2B

S 426 1BISbull21755



43 1111bull16172





-~

611 642 7 13 7 44 815 846 9 17 9148 18119 100 ________ 1-1 LiLJ ~

S 460 100bull14529 90

amp 458 1001bull12404 80

0 395 l801bull8383

70

470 1001bull128228 I60 0 N

472 1881bull136872 58

I N T E

f N s

I T V

30

20

10

0

-------~ I

~-- ~

120 130 140 150 160 SCAN NUMBER

170 188 ljS 2BB


-- - - - -



001 l 07 2 14 3122 429 537 6144 100 L --____L_______~_l--1__t----______________~

$ 306 100Xbull218713

90 I - l -2378amp ~~4~IJr 1_1mas

0 3H 18 bull1860

7B


SB

I=~ 0 N

332 10 bull136251 58

I N T

-48 E N s I

33 T y

2B

l 3

B



250

100

90

80

70

60

50

U

30

20

UJ

B

BREHM LABORATORY



$ 322 1001bull532633

amp 320 100Xbull404109

0 257 1BBXbull219683

328 1BBXbulll94431

~ 332 IBBXbull28B34

I~

r1 ~_)

-

--___ ~~- J

SB

-------_-----------------------------~



3BB



322 4129 5s37 6144 ~-1--A--L---L-L--L--------J---------_______~ __-L-__________~__~__L-__~-----------_-+-

-~-I I

Nl 0

I 2378 N

T E

If s N

T~ VI

r (~~-

A

_




0 340 l00Xbull270473 90

338 l00Xbull158177

80

tSS 180Xbull3262 1B

I 0 N

60

I N T E N

SB

s



I Tu y

30

2B

lB

B

250 300 3U UB




081 __~ I

1 03 2 06 3 zl0 4 13 517 6120 724 8127 I

0 356 100Xbull723886

354 1BBXbull44618S

291 lS01bull261351

I 0 N

I N T E N s 1 T V

UJjJ

9B

SB

7B

6B

58

0

30

20

lB

B



Z5B 3IB 35g

sAUhE Nob1 488

0 0middot 1 1 26



254 4 21 5 I 49 7 16 Si 44 100

90

88

78

69

58

u

38

2B

18

B


0 376 100Xbull27922

374 1BBXbull34690

4U 10BXbulll US



I 0 N

I N T E N s I T y

3BB

urn_

98

as

7B

6B

50

uJ

30

2B

1e

B



s01 1 26


39B 1SSXbull7512SC

329 1SSXbull2513Sl

SELECTED-ION

254


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MOISTURE 3468 i


FLOW 20558 Nt113hr 70940 1113hr

12983 DScft11 41754 Acft11






STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT


100

1506

1018

-6226

800

0800

0987

M

M2

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MM

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162 sqft

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032 in







TOTAL CONDENSATION

1

2

3

4

5

6

3390 1111

00 1111

00 Ml

00 ml

0 0 Ml

00 Ml

3390 ml

FILTER PARTICULATE



TOTAL PARTICULATE

24100 s

00000 s

02390 s

26490 s



------------------------------------------------------------------------------


PT NO

TIME

Min


------


METER VOL

curt ------


WALL DIST

in -----

7 ISO

TRAVERSE NO 1

4 3 2 1

00 so

100 150 200

643 633 654 648

026 030 032 036

178 205 2 14 240

83645 83645 83645 83645 84748

63 68 71 78

643 633 654 648

60 60 60 60

60 60 60 60

30 30 30 30

34S 246 148 49

00 00 00

4355

TRAVERSE NO 2

4 oo 20

620 032 222 84748 84810

78 620 60 60 30 345 641

TRAVERSE NO 3

3 2 1

oo 50

100 150

638 650 872

026 022 020

180 155 141

76790 76790 76790 77670

68 73 74

638 650 672

60 60 80

60 60 60

30 30 30

246 14B 49

oo 00

4736

TRAVERSE NO 4

4 3 2 1

oo 50

100 150 200

630 648 652 665

030 030 030 021

206 205 205 148

77670 77670 77670 77670 78675

70 77 78 75

630 648 652 665

60 60 60 60

60 60 60 60

30 30 30 30

345 246 148 49

oo oo oo

5253

AVERAGE 647 027 189 1220



14307 msAm3 06253 srAcf





MOISTURE 2791 l


FLOW 20049 61827

NM3hr 11t3hr

12662 36390

DScfM AcfM



























TRAVERSE NO 1

4 00 557 0 16 110 78700 61 600 60 60 30 34 5 oo 3 50 593 024 154 78700 68 600 60 60 30 246 00 2 100 638 022 139 78700 73 600 60 60 30 148 00 1 150 666 022 136 78700 72 600 60 60 30 49 4085

200 79565

TRAVERSE NO 2

4 00 636 030 181 79565 68 620 60 60 30 345 00 3 so 593 024 154 79565 68 620 60 60 30 246 00 2 100 660 016 103 79565- 74 - 620 60 60 30 148 00 1 150 670 018 1 14 79565 76 620 60 60 30 49 4395

200 804 12

TRAVERSE NO 3

4 00 612 028 1 75 804 12 73 630 60 60 30 345 00 3 50 640 024 150 804 12 73 630 60 60 30 246 oo 2 100 645 020 128 80412 76 630 60 60 30 14 8 00 1 150 678 020 125 80412 78 630 60 60 30 49 4258

200 81277

AVERAGE 632 022 138 1004



10399 tr1sAtr13





MOISTURE

TEMPERATURE

FLOW

VELOCITY


STANDARD CONDITIONS

3701

2500 des C

20773 Nt113hr 83819 1113hr

1242 MS

11 70 850 7 ooo 7



14588 lbhr

28915 DScf

4821 des F

13119 DScF111 37445 Acf1r1

24441 fpfll

298 ss MOLE ltDRYgt


























TRAVERSE NO 1

24 oo 475 040 196 35470 23 30 485 042 199 35470 22 60 485 046 2 16 35470 21 90 485 046 2 16 35470 20 120 485 049 228 35470 19 150 485 046 2 16 35470 18 180 485 048 224 35470 17 210 485 042 199 35470 16 240 485 038 185 35470 15 270 485 028 142 35470 14 300 485 027 137 35470-middot 13 330 485 019 101 35470 12 360 485 0 16 086 35470

( 11 10

390 420

485 475

0 16 016

086 087

35470 35470

9 450 485 0 16 086 35470 8 480 475 0 14 077 35470 7 510 485 014 076 35470 6 540 485 017 091 35470 5 570 470 017 092 35470 4 600 475 020 106 35470 3 630 480 023 1 20 35470 2 680 480 023 120 35470 1 690 480 023 120 35470

720 38312

AVERAGE 482 027 137



1132



14463 t11sAt113 06321 srAcf





MOISTURE 3077 7


FLOW 20225 56107

Nm3hr M3hr


























r1




TRAVERSE NO 1


9 450 480 0 10 049 38387 60 360 60 60 30 122 00 8 480 475 0 10 049 38387 60 360 60 60 30 103 00 7 510 470 0 12 059 38387 60 360 60 60 30 86 00 6 540 440 0 10 052 38387 70 360 60 60 30 70 00 5 570 480 0 14 067 38387 60 360 60 60 30 55 00 4 600 470 018 085 38387 60 360 80 60 30 42 00 3 630 470 0 18 085 38387 60 360 60 60 30 29 00 2 660 470 0 18 085 38387 60 360 60 60 30 17 00 1 690 470 0 18 085 38387 60 360 60 60 30 06 30052

720 411 70

AVERAGE 478 022 099 1141



6633 M9IAM3 02899 srAcf





MOISTURE 2586 7


FLOW 29909 74537

NM3hr M3hr







STACK AREA 1370 M2



















------------------------------------------------------------------------------

--- ---- ------ ------ ------ ----- ----- ----- ----- ----- -----




TRAVERSE NO 1


360 40605

TRAVERSE NO 2

12 oo 440 078 357 40801 60 400 60 60 30 509 oo 11 30 440 080 366 40801 60 400 60 60 30 485 00 10 60 440 076 352 40801 65 400 60 60 30 459 oo

9 90 440 065 306 40801 65 400 60 60 30 428 00 8 120 440 060 286 40801 65 400 60 60 30 390 00 7 150 440 056 267 40801 60 400 60 60 30 335 00 6 180 445 028 145 40801 60 400 60 60 30 185 00 5 210 440 026 138 40801 65 400 60 60 30 130 oo 4 240 435 030 157 40801 65 400 60 60 30 92 00 3 270 435 030 157 40801 65 400 60 60 30 6 I 1 oo 2 300 435 034 175 40801 65 400 60 60 30 35 14118

330 42763

AVERAGE 439 044 2 16 985








MOISTURE 2867 7



17071 41098

DScfm Acftn




























TRAVERSE NO 1

12 00 435 042 189 42830 55 330 60 60 30 509 00 11 30 460 054 232 42830 60 330 60 60 30 485 00 10 60 430 049 219 42830 60 330 60 60 30 459 00

9 90 435 062 270 42830 65 330 60 60 30 42B 00 8 120 435 062 270 42830 65 330 60 60 30 390 00 7 150 435 036 168 42830 65 330 60 60 30 335 00 6 180 435 021 104 42830 65 330 60 60 30 18 5 00 5 210 435 021 104 42830 65 330 60 60 30 130 00 4 240 435 021 104 42830 65 330 60 60 3 0 92 00 3 270 435 020 100 42830 65 330 60 60 30 6 1 00 2 300 435 026 126 42830 65 330 60 60 30 35 254 1 330 435 026 126 42860 55middot 330 60 60 30 11 13254

360 44423

TRAVERSE NO 2

12 oo 435 058 253 44423 60 350 60 60 30 509 oo 11 30 435 069 298 44423 70 350 60 60 30 485 00 10 60 435 069 298 44423 70 350 60 60 30 459 00

9 90 445 062 268 44423 70 350 60 60 30 428 00 8 120 470 0 18 087 44423 60 350 60 60 30 390 00 7 150 440 058 255 44423 70 350 60 60 30 335 00 6 180 440 040 183 44423 65 350 60 60 30 185 00 5 210 440 023 113 44423 70 350 60 60 3middot0 130 oo 4 240 440 025 121 44423 65 350 60 60 30 92 00 3 270 440 031 148 44423 70 350 60 60 3m0 61 oo 2 300 435 034 161 44423 70 350 so 60 30 35 00 1 330 435 034 161 44423 70 350 60 60 30 1 1 13086

360 48203

AVERAGE 439 038 1 75 986

l



123 M9AM3





MOISTURE 3179 X


FLOW 27788 N1113hr 73634 1113hr

VELOCITY 1493 111s




198 lbhr

38566 DScf

4096 des F

17549 DScft1 43340 Acf111

29387 fpfll



























TRAVERSE NO 1


360 75390

TRA~bullERSE NO 2

12 oo 410 046 355 754 10 65 345 60 60 30 509 oo 11 30 410 046 355 754 10 65 345 60 60 30 485 oo 10 60 410 044 349 754 10 80 345 60 60 30 459 oo


360 77240

AVERAGE 410 044 347 1030



114 7 M9Am3





MOISTURE 2745 i


FLOW 25879 NM3hr 63074 1113hr

VELOCITY 1279 ms




1595 lbhr

30360 DScf

3906 deg F


25172 fPM



-------------------------------------------------------------------------


STACK DIAMETER

STACK AREA

BAROMETRIC PRESSURE

STATIC PRESSURE

NOZZLE DIAMETER

PITOT COEFFICIENT








TOTAL CONDENSATION

FILTER PARTICULATE



TOTAL PARTICULATE

SAMPLING TIME

STACK HEIGHT

132

1370 1112

1018 kPa

27395 Pa

700

0810

0988

2219 t11l

70 ml

10 Ml

oo Ml

oo Ml

135 Ml

2434 Ml

00080 s

00110 s

02050 s

02240 s

720 Min

000 111

520 in

147 sqft

3006 inHs

-1 1 00 in bull H20

028 in

oo ft

--- ---- ----- ------ ------ ------ ----- ----- ----- ----- ----- ----- -----




TRAVERSE NO 1

12 oo 395 038 259 77260 60 380 60 60 30 509 00 11 30 390 034 218 77260 70 380 60 60 30 485 oo 10 60 385 032 229 77260 70 380 60 60 30 459 oo 9 90 385 032 229 77260 70 380 60 60 30 428 oo 8 120 385 032 229 77260 70 380 60 60 30 390 00 7 150 385 032 2a29 77260 70 380 60 60 30 335 00 6 180 385 Oe40 278 77260 70 380 60 60 30 185 oo 5 210 385 044 302 77260 70 380 60 60 30 130 00 4 240 390 040 279 77260 75 380 60 60 30 92 00 3 270 390 024 1 78 77260 75 380 60 60 30 61 00 2 300 390 024 178 77260 75 380 60 60 30 35 00 1 330 390 024 178 77260 75 380 60 60 30 11 12184

360 78705

TRAt1ERSE NO 2

12 00 390 040 277 78730 70 380 60 60 30 509 00 11 30 390 040 277 78730 70 380 60 60 30 485 00 10 60 390 036 256 78730 80 380 60 60 30 459 00 9 90 390 036 256 78730 80 380 60 60 30 428 00 8 120 395 034 242 78730 80 380 60 60 30 390 00 7 150 395 034 242 78730 80 380 60 60 30 335 oo 6 180 395 032 230 78730 80 380 60 60 30 185 oo 5 210 395 036 2c55 78730 BO 380 60 60 30 130 oo 4 240 385 036 255 78730 80 380 60 60 30 9 00 3 270 395 036 255 78730 80 380 60 60 30 6 1 00 2 300 385 026 183 78730 85 380 60 60 30 35 00 1 330 395 026 193 78730 85 380 60 60 30 11 13045

360 80365

AVERAGE 391 033 237 918

---------------------













12 oo 4850 042 068 41260 650 650 20 00 14182 300 41750


------------------------------------------










STACK GAS ANALYSIS




600 749 001

5395 3255

890 1110 001

7999 ooo

TOTAL 10000 10000



------------------------------1 00770 9167 10000 2 00000 000 833 3 00000 000 833 4 00070 833 833 5 00000 000 -000 FILTER 00000 000 -000


---------------------833 1224 833 693 833 526

-000 260 -000 146




- 022409 GAH3 009794 GRAINSCF

------------------











---------1 00770 2 00000 3 00000 4 00070 5 00000 FILTER 00000


10000 833 833 833

-o_oo -ooo


833 1224 833 693 833 526

-000 260 -ooo 146




022409 GA13 009794 GRAINSCF

---------------------------- -------------------------------













12 oo 4850 042 061 41740 650 650 00 00 10146 450 42455

AVERAGES 4850 042 061 650 650

----------- ------------

------------










STACK GAS ANALYSIS


CO2 579 820 02 848 1200 CD 001 001


TOTAL 10000 10000



0191 Nl13

0012 Al13NIN

2517 DEGC



l 06000 8065 10000 1935 1293 2 00000 ooo 1935 1935 749 3 00000 000 1935 1935 S72 4 00380 511 1935 1425 2B7 5 00000 000 1425 1425 161 FILTER 01060 1425 142S



II








AVERAGE ISOKINETIC


1 06000 8065 2 00000 ooo 3 00000 000 4 00380 511 5 00000 ooo FILTER 01060 1425


636 NL

251 7 DEGC

1015 l



10000 19-35 1935 1935 1425 1425

1935 1935 1935 1425 1425

1293 749 572 287 161




142467 GAl13 062267 GRAINSCF












SANPLE POINT

SANPLE TINE ltNIN)

STACK TElIP ltDEGF)


I

-------------12 oo

300 4850 042 066 42560

43040 650 650 20 middotoo 10678

AVERAGES 4850 042 066 650 650










STACK GAS ANALYSIS


---------



455 883 001

5349 3313

680 1320 001

7999 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


04230 00000 00000 00410 00000 00880


7663 000 000 743 000

1594


10000 2337 2337 2337 1594 1594


--------------------2337 1233 2337 701 2337 532 1594 264 1594 148




149030 GAl13 065135 GRAINSCF

---------------------









7663 000 ooo 743 ooo

1594

10000 2337 23~37 2337 1594 1594


2337 1233 2337 701 2337 532 1594 264 1594 148




149030 6AN3 065135 GRAINSCF I

-------------------












7 oo 4500 050 084 815~70 650 650 30 00 11438 300 82144

AVERAGES 4500 050 084 650 650





TOTAL SANPLE VOLUHE




AVERAGE ISOKINETIC

574 DSCF

0500 ACFM

592 t1L

4500 DEGF

1144

0151 Nt13

0014 At13NIN

2322 DEGC

STACK GAS ANALYSIS



I


TOTAL 10000 10000



1 2 3 4 5 FILTER


04248 00000 00000 01849 00000 01515


----------5581 10000 000 4419 ooo 4419

2429 4419 ooo 1990

1990 1990


4419 4419 4419 1990 1990


1102 600 447 218 123





---------------------








l 04248 2 00000 3 00000 4 01849 5 00000 FILTER 01515

5581 ooo ooo

2429 000

1990

10000 4419 4419 4419 1990 1990


4419 1102 4419 600 4419 447 1990 218 1990 123

















t 7 oo 4500 050 075 82275 650 650 20 00 10813 450 83033

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




408 828 001

4943 3820

660 1340 001

7999 ooo

TOTAL 10000 10000








1 2 3 4 5 FILTER

02450 00000 00000 01890 00000 02000

3864 000 000

2981 ooo

31SS

-------------------------

10000 6136 6136 6136 3155 3155

6136 6136 6136 3155 31S5

1103 601 444 220 126





----------------------------------

-----------------








-~-----------------1 02450 3864 10000 2 00000 000 61-36 3 00000 ooo 6136 4 01890 2981 6136 5 00000 000 3155 FILTER 02000 3155 3155

--------------------


6136 1103 6136 601 6136 444 3155 220 3155 126




105155 GAt13 045959 GRAINSCF












SANPLE POINT

SANPLE TINE (NIN)

STACK TENP (DEGFl


II

7 oo 300

4500 050 075 83185 83672

650 650 20 00middot 9636

AVERAGES 4500 050 075 650 650










STACK GAS ANALYSIS




447 908 001

5418 3226

660 1340 001

7999 ooo

TOTAL 10000 10000




5828 000 ooo

271S ooo

1457


10000 4172 4172 4172 1457 1457


4172 4172 41 72 1457 1457


12 15 689 516 260 149



625188 GNN3

227228 GAN3

254618 GRAINSDSCF

099313 GRAINSCF








1 2 3 4 5 FILTER

04680 00000 00000 02180 00000 01170

5828 ooo ooo

27 15 000

1457

10000 U72 4172 4172 1457 1457

---------


41 72 4172 41 72 1457 1457

1215 689 516 260 149




227228 GAt13 099313 GRAINSCF













7 oo 4100 056 049 84830 600 600 oo oo 6158 7 3000 4100 056 049 8B066 550 550 2 0 oo 15352

4800 92860

AVERAGES 4100 056 049 581 581










STACK GAS ANALYSIS




441 883 001

5264 3411

670 1340 001

7989 000

TOTAL 10000 10000



1 2 3 4 5 FILTER


00020 00000 00000 00030 00000 00025


2667 ooo 000

4000 000

3333

-------------


10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

---------------


1125 619 452 230 135













1 00020 2 00000 3 00000 4 00030 5 00000

( FILTER 00025

2667 ooo ooo

4000 ooo

3333

10000 7333 7333 7333 3333 3333


7333 7333 7333 3333 3333

1125 619 452 230 135





(


bull



(

~ --=------


July 2 1986


Dear John




r~tf~ Uhn A Coburn


JACmk




Comments by

John A Coburn


July 2 1986

(

Sample Preparation










this sort













( E IC pIs) bull




1





















reported elsewhere

2










provided










3



















shape

4








John A Cob urn

5


(




July 23 1986 4047-3


Dear Mr Chandler





2








3

4a - 3

P 9 Table A

(

P 12 Sec 6b





4


Sincerely



C Chiu

Documents

APPENDIX RECOMMENDED SAFETY AND HANDLING …