Upload
others
View
0
Download
0
Embed Size (px)
Citation preview
FINAL STATUS SURVEY REPORT
SUBMITTAL NUMBER 1
CE WINDSOR SITE WINDSOR, CONNECTICUT
APPENDIX B
SURVEY UNIT CE-FSS-41-02
RESULTS AND DATA EVALUATION
Docu
ment:
P:\Pr
ojects
\ABBW
IN\G
IS-Av
8\Map
Docu
ments
\FUSR
AP R
emed
iation
\FSS\
Waste
Line
s\WL_
FSS_
Resu
lts_8
x11P
.mxd
PD
F: P:\
Proje
cts\ab
bwin\
GIS-
Av8\F
igures
\FUSR
AP R
emed
iation
\FSS\W
aste
Lines
\Rep
ort Fi
gures
\CE-
FSS-
41-02
_Loc
ation
s.pdf
07/2
7/201
1 11
:14 AM
brp
eters
Prepared/Date: BRP 07/27/11
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C CE-FSS-41-02-014
CE-FSS-41-02-013
CE-FSS-41-02-012
CE-FSS-41-02-011
CE-FSS-41-02-010
CE-FSS-41-02-009
CE-FSS-41-02-008
CE-FSS-41-02-007
CE-FSS-41-02-006
CE-FSS-41-02-005
CE-FSS-41-02-004
CE-FSS-41-02-002
CE-FSS-41-02-001
CE-FSS-41-02-003
1009000 1009200 1009400
8828
0088
3000
8832
0088
3400
8836
00
¯ 0 10050Feet
Legend"C Sample Location
CE-FSS-41-02ForestOpenWaterRoadBuilding
CT St
ate Pl
ane N
AD 83
Feet
Checked/Date: GSM 07/27/11
Sample LocationsSurvey Unit CE-FSS-41-02
Final Status SurveyCE Windsor Site
Windsor, Connecticut
Appendix B Page 1
Docu
ment:
P:\Pr
ojects
\ABBW
IN\G
IS-Av
8\Map
Docu
ments
\FUSR
AP R
emed
iation
\FSS\
Waste
Line
s\WL_
FSS_
Resu
lts_8
x11P
.mxd
PD
F: P:\
Proje
cts\ab
bwin\
GIS-
Av8\F
igures
\FUSR
AP R
emed
iation
\FSS\W
aste
Lines
\Rep
ort Fi
gures
\CE-
FSS-
41-02
_Res
ults.p
df 0
7/27/2
011
12:35
PM
brpete
rs
Prepared/Date: BRP 07/27/11
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C
"C 0.0222 Co-602.691 U
0.0178 Co-601.585 U
0.0143 Co-60-0.85 U
0.0182 Co-603.239 U
-0.056 Co-604.774 U
0.0149 Co-604.495 U
0.0447 Co-603.178 U
0.0567 Co-601.372 U
-0.0207 Co-602.513 U
-0.0109 Co-602.596 U
0.00731 Co-603.262 U
-0.0504 Co-601.795 U
-0.00583 Co-602.465 U
-0.00307 Co-602.554 U
1009000 1009200 1009400
8828
0088
3000
8832
0088
3400
8836
00
¯ 0 10050Feet
Legend"C Sample Location
CE-FSS-41-02ForestOpenWaterRoadBuilding
Co-60 (pCi/g)Total U (pCi/g)
CT St
ate Pl
ane N
AD 83
Feet
Checked/Date: GSM 07/27/11
Sample ResultsSurvey Unit CE-FSS-41-02
Final Status SurveyCE Windsor Site
Windsor, Connecticut
Appendix B Page 2
Activity Uncert. MDC Qualifier Activity Uncert. MDC QualifierCE-FSS-41-02-001 5.67E-02 6.40E-02 1.38E-01 U 4.43E-02 8.62E-02 1.28E-01 U 1.4 0.014CE-FSS-41-02-002 4.47E-02 8.03E-02 1.50E-01 U 1.03E-01 9.30E-02 1.46E-01 U 3.2 0.015CE-FSS-41-02-003 -3.07E-03 9.78E-02 1.46E-01 U 8.24E-02 7.61E-02 1.20E-01 2.6 0.004CE-FSS-41-02-004 1.49E-02 8.38E-02 1.35E-01 U 1.45E-01 8.38E-02 1.39E-01 U 4.5 0.011CE-FSS-41-02-005 -5.60E-02 1.05E-01 1.28E-01 U 1.54E-01 1.08E-01 1.84E-01 4.8 -0.003CE-FSS-41-02-006 1.82E-02 9.44E-02 1.51E-01 U 1.04E-01 8.40E-02 1.37E-01 UI 3.2 0.009CE-FSS-41-02-007 1.43E-02 7.09E-02 1.21E-01 U -2.74E-02 9.75E-02 1.33E-01 U -0.9 0.001CE-FSS-41-02-008 -5.04E-02 1.04E-01 1.19E-01 U 5.79E-02 9.19E-02 1.37E-01 U 1.8 -0.007CE-FSS-41-02-009 1.78E-02 7.85E-02 1.34E-01 U 5.11E-02 9.50E-02 1.40E-01 U 1.6 0.006CE-FSS-41-02-010 9.44E-03 8.88E-02 1.36E-01 U 9.13E-02 8.22E-02 1.30E-01 U 2.8 0.007
CE-FSS-41-02-010LR 5.18E-03 6.87E-02 1.13E-01 U 1.19E-01 7.80E-02 1.28E-01 U 3.7 0.008CE-FSS-41-02-010AVE 7.31E-03 1.05E-01 3.3 0.007
CE-FSS-41-02-011 -5.83E-03 9.87E-02 1.41E-01 U 7.95E-02 8.40E-02 1.36E-01 2.5 0.003CE-FSS-41-02-012 -1.09E-02 8.39E-02 1.19E-01 U 8.37E-02 8.20E-02 1.28E-01 U 2.6 0.002CE-FSS-41-02-013 -1.46E-02 8.95E-02 1.31E-01 U 4.93E-02 9.21E-02 1.35E-01 U 1.5 0.000
CE-FSS-41-02-013S -2.67E-02 9.82E-02 1.38E-01 1.13E-01 8.93E-02 1.45E-01 UI 3.5 0.001CE-FSS-41-02-013AVE -2.07E-02 8.11E-02 2.5 0.000
CE-FSS-41-02-014 2.22E-02 8.25E-02 1.39E-01 U 8.68E-02 8.41E-02 1.31E-01 U 2.7 0.009
Final Status Survey Volumetric Soil Sample ResultsTotal U (pCi/g)
Sum of Fraction
Sample ID Co-60 U-235
Appendix B Page 3
Sample ID Static Count Rate (cpm)
Ambient Background
(cpm)Net (cpm) pCi/g
FSS-041-02-001 3154 3000 154 0.5FSS-041-02-002 3207 3000 207 0.7FSS-041-02-003 3426 3000 426 1.4FSS-041-02-004 3141 3000 141 0.5FSS-041-02-005 3127 3000 127 0.4FSS-041-02-006 3143 3000 143 0.5FSS-041-02-007 3212 3000 212 0.7FSS-041-02-008 3472 3000 472 1.6FSS-041-02-009 3245 3000 245 0.8FSS-041-02-010 3223 3000 223 0.7FSS-041-02-011 2812 3000 -188 -0.6FSS-041-02-012 2788 3000 -212 -0.7FSS-041-02-013 3426 3000 426 1.4FSS-041-02-014 3202 3000 202 0.7
One-Minute Static Field Measurement Results
Appendix B Page 4
Sample ID X_Coordinate Y_CoordinateCE-FSS-41-02-001 1009195.9516 883398.5049CE-FSS-41-02-002 1009204.6348 883193.1474CE-FSS-41-02-003 1009123.9663 882961.2652CE-FSS-41-02-004 1009155.0719 883074.9066CE-FSS-41-02-005 1009105.5200 882904.8085CE-FSS-41-02-006 1009151.9847 883123.4172CE-FSS-41-02-007 1009203.6482 883411.0583CE-FSS-41-02-008 1009224.7910 883306.2568CE-FSS-41-02-009 1009198.6385 883377.6850CE-FSS-41-02-010 1009109.6933 882970.0723CE-FSS-41-02-011 1009228.5039 883323.0321CE-FSS-41-02-012 1009175.9392 883435.5474CE-FSS-41-02-013 1009129.9188 882988.6412CE-FSS-41-02-014 1009102.9275 882937.8718
Final Status Survey Sample GPS Coordinates
Appendix B Page 5
Descriptive Statistics Report Summary Section of SU_4102_C060 Standard Standard Count Mean Deviation Error Minimum Maximum Range 14 0.003515 3.153476E-02 8.42802E-03 -0.056 0.0567 0.1127 Counts Section of SU_4102_C060 Sum of Missing Distinct Total Adjusted Rows Frequencies Values Values Sum Sum Squares Sum Squares 29 14 15 14 0.04921 1.310071E-02 1.292774E-02 Means Section of SU_4102_C060 Geometric Harmonic Parameter Mean Median Mean Mean Sum Mode Value 0.003515 0.010805 2.026035E-02 -6.829628E-02 0.04921 Std Error 8.42802E-03 0.1179923 95% LCL -1.469263E-02 -0.0207 -0.2056968 95% UCL 2.172263E-02 0.0182 0.3041168 T-Value 0.4171 Prob Level 0.683439 Count 14 8 14 Variation Section of SU_4102_C060 Standard Unbiased Std Error Interquartile Parameter Variance Deviation Std Dev of Mean Range Range Value 9.944413E-04 3.153476E-02 3.214647E-02 8.42802E-03 0.03255 0.1127 Std Error 3.489077E-04 7.823587E-03 2.090942E-03 95% LCL 5.226368E-04 2.286125E-02 6.109926E-03 95% UCL 2.58103E-03 5.080384E-02 0.0135779 Skewness and Kurtosis Section of SU_4102_C060 Coefficient Coefficient Parameter Skewness Kurtosis Fisher's g1 Fisher's g2 of Variation of Dispersion Value -0.382167 2.723419 -0.4296429 0.1823231 8.971483 2.170887 Std Error 0.3291011 0.8633268 21.2403 Trimmed Section of SU_4102_C060 5% 10% 15% 25% 35% 45% Parameter Trimmed Trimmed Trimmed Trimmed Trimmed Trimmed Trim-Mean 3.866667E-03 4.534821E-03 5.516327E-03 7.008572E-03 8.246905E-03 0.010805 Trim-Std Dev 2.701644E-02 2.147547E-02 1.438601E-02 0.0109649 8.638501E-03 6.538546E-03 Count 12.6 11.2 9.8 7 4.2 1.4 Mean-Deviation Section of SU_4102_C060 Parameter |X-Mean| |X-Median| (X-Mean)^2 (X-Mean)^3 (X-Mean)^4 Average 2.399857E-02 2.345643E-02 9.234098E-04 -1.072371E-05 2.32222E-06 Std Error 5.058021E-03 3.239857E-04 8.530387E-06 9.913321E-07
Appendix B Page 6
Descriptive Statistics Report Quartile Section of SU_4102_C060 10th 25th 50th 75th 90th Parameter Percentile Percentile Percentile Percentile Percentile Value -0.0532 -0.01335 0.010805 0.0192 0.0507 95% LCL -0.056 -0.0207 0.00731 95% UCL 0.0143 0.0182 0.0567 Normality Test Section of SU_4102_C060 Test Prob 10% Critical 5% Critical Decision Test Name Value Level Value Value (5%) Shapiro-Wilk W 0.9520117 0.592354 Accept Normality Anderson-Darling 0.3437831 0.488485 Accept Normality Martinez-Iglewicz 1.090405 1.305415 1.57245 Accept Normality Kolmogorov-Smirnov 0.1338938 0.208 0.226 Accept Normality D'Agostino Skewness -0.7516 0.452291 1.645 1.960 Accept Normality D'Agostino Kurtosis 0.3877 0.698255 1.645 1.960 Accept Normality D'Agostino Omnibus 0.7152 0.699353 4.605 5.991 Accept Normality Plots Section of SU_4102_C060
0.0
2.0
4.0
6.0
8.0
-0.1 0.0 0.0 0.0 0.1
Histogram of SU_4102_C060
SU_4102_C060
Coun
t
-0.1
0.0
0.0
0.0
0.1
-2.0 -1.0 0.0 1.0 2.0
Normal Probability Plot of SU_4102_C060
Expected Normals
SU_4
102_
C060
Appendix B Page 7
Descriptive Statistics Report Percentile Section of SU_4102_C060 Percentile Value 95% LCL 95% UCL Exact Conf. Level 99.0 0.0567 95.0 0.0567 90.0 0.0507 85.0 0.039075 80.0 0.0222 0.00731 0.0567 95.3622 75.0 0.0192 0.00731 0.0567 97.1873 70.0 0.018 -0.00307 0.0567 98.4929 65.0 0.017075 -0.00307 0.0447 95.5137 60.0 0.0149 -0.00583 0.0447 97.4393 55.0 0.01445 -0.0109 0.0222 97.1563 50.0 0.010805 -0.0207 0.0182 96.4844 45.0 0.004715 -0.0207 0.0182 97.1563 40.0 -0.00307 -0.0504 0.0178 97.4393 35.0 -0.00514 -0.056 0.0149 97.3253 30.0 -0.008365 -0.056 0.0143 96.1749 25.0 -0.01335 -0.056 0.0143 97.1873 20.0 -0.0207 -0.056 0.0143 95.3622 15.0 -0.042975 10.0 -0.0532 5.0 -0.056 1.0 -0.056 Percentile Formula: Ave X(p[n+1]) Stem-Leaf Plot Section of SU_4102_C060 Depth Stem Leaves Low | -5 2 F | 5 3 T | 2 6 -0* | 100 (5) 0* | 01111 3 T | 2 2 F | 45 Unit = .01 Example: 1 |2 Represents 0.12
Appendix B Page 8
Descriptive Statistics Report Summary Section of SU_4102_Total_U Standard Standard Count Mean Deviation Error Minimum Maximum Range 14 2.557143 1.386592 0.3705823 -0.9 4.8 5.7 Counts Section of SU_4102_Total_U Sum of Missing Distinct Total Adjusted Rows Frequencies Values Values Sum Sum Squares Sum Squares 29 14 15 11 35.8 116.54 24.99429 Means Section of SU_4102_Total_U Geometric Harmonic Parameter Mean Median Mean Mean Sum Mode Value 2.557143 2.6 2.661186 3.429761 35.8 Std Error 0.3705823 5.188152 95% LCL 1.756549 1.6 24.59168 95% UCL 3.357737 3.2 47.00832 T-Value 6.9003 Prob Level 0.000011 Count 14 13 14 Variation Section of SU_4102_Total_U Standard Unbiased Std Error Interquartile Parameter Variance Deviation Std Dev of Mean Range Range Value 1.922637 1.386592 1.413489 0.3705823 1.475 5.7 Std Error 0.9146558 0.4664381 0.1246608 95% LCL 1.010458 1.005215 0.2686551 95% UCL 4.990124 2.233859 0.5970238 Skewness and Kurtosis Section of SU_4102_Total_U Coefficient Coefficient Parameter Skewness Kurtosis Fisher's g1 Fisher's g2 of Variation of Dispersion Value -0.73719 4.168463 -0.8287697 2.317048 0.5422427 0.3516484 Std Error 0.4058379 1.462824 0.1745276 Trimmed Section of SU_4102_Total_U 5% 10% 15% 25% 35% 45% Parameter Trimmed Trimmed Trimmed Trimmed Trimmed Trimmed Trim-Mean 2.624603 2.6375 2.603061 2.657143 2.611905 2.6 Trim-Std Dev 1.060635 0.7601761 0.5570731 0.3801629 0.1327648 1.501713E-08 Count 12.6 11.2 9.8 7 4.2 1.4 Mean-Deviation Section of SU_4102_Total_U Parameter |X-Mean| |X-Median| (X-Mean)^2 (X-Mean)^3 (X-Mean)^4 Average 0.9204082 0.9142857 1.785306 -1.758525 13.28622 Std Error 0.2224025 0.8493233 1.710164 8.517901
Appendix B Page 9
Descriptive Statistics Report Quartile Section of SU_4102_Total_U 10th 25th 50th 75th 90th Parameter Percentile Percentile Percentile Percentile Percentile Value 0.25 1.75 2.6 3.225 4.65 95% LCL -0.9 1.6 2.6 95% UCL 2.6 3.2 4.8 Normality Test Section of SU_4102_Total_U Test Prob 10% Critical 5% Critical Decision Test Name Value Level Value Value (5%) Shapiro-Wilk W 0.9192215 0.214293 Accept Normality Anderson-Darling 0.5128176 0.194065 Accept Normality Martinez-Iglewicz 1.371184 1.305415 1.57245 Accept Normality Kolmogorov-Smirnov 0.1532109 0.208 0.226 Accept Normality D'Agostino Skewness -1.4138 0.157417 1.645 1.960 Accept Normality D'Agostino Kurtosis 1.7215 0.085167 1.645 1.960 Accept Normality D'Agostino Omnibus 4.9623 0.083647 4.605 5.991 Accept Normality Plots Section of SU_4102_Total_U
0.0
2.0
4.0
6.0
8.0
-1.0 0.5 2.0 3.5 5.0
Histogram of SU_4102_Total_U
SU_4102_Total_U
Coun
t
-1.0
0.5
2.0
3.5
5.0
-2.0 -1.0 0.0 1.0 2.0
Normal Probability Plot of SU_4102_Total_U
Expected Normals
SU_4
102_
Tota
l_U
Appendix B Page 10
Descriptive Statistics Report Percentile Section of SU_4102_Total_U Percentile Value 95% LCL 95% UCL Exact Conf. Level 99.0 4.8 95.0 4.8 90.0 4.65 85.0 4.2 80.0 3.3 2.6 4.8 95.3622 75.0 3.225 2.6 4.8 97.1873 70.0 3.2 2.5 4.8 98.4929 65.0 3.075 2.5 4.5 95.5137 60.0 2.7 2.5 4.5 97.4393 55.0 2.625 1.8 3.3 97.1563 50.0 2.6 1.6 3.2 96.4844 45.0 2.575 1.6 3.2 97.1563 40.0 2.5 1.4 3.2 97.4393 35.0 2.5 -0.9 2.7 97.3253 30.0 2.15 -0.9 2.6 96.1749 25.0 1.75 -0.9 2.6 97.1873 20.0 1.6 -0.9 2.6 95.3622 15.0 1.45 10.0 0.25 5.0 -0.9 1.0 -0.9 Percentile Formula: Ave X(p[n+1]) Stem-Leaf Plot Section of SU_4102_Total_U Depth Stem Leaves Low | -9 2 1* | 4 4 . | 68 4 2* | (5) . | 55667 5 3* | 223 2 . | 2 4* | 2 . | 58 Unit = .1 Example: 1 |2 Represents 1.2
Appendix B Page 11
Descriptive Statistics Report Summary Section of SU_4102_SOF Standard Standard Count Mean Deviation Error Minimum Maximum Range 14 5.071429E-03 6.305849E-03 1.685309E-03 -0.007 0.015 0.022 Counts Section of SU_4102_SOF Sum of Missing Distinct Total Adjusted Rows Frequencies Values Values Sum Sum Squares Sum Squares 29 14 15 13 0.071 0.000877 5.169286E-04 Means Section of SU_4102_SOF Geometric Harmonic Parameter Mean Median Mean Mean Sum Mode Value 5.071429E-03 0.005 5.653578E-03 5.490113E-03 0.071 0.009 Std Error 1.685309E-03 2.359433E-02 95% LCL 1.43054E-03 0 2.002755E-02 95% UCL 8.712318E-03 0.009 0.1219724 T-Value 3.0092 Prob Level 0.010059 Count 14 11 13 2 Variation Section of SU_4102_SOF Standard Unbiased Std Error Interquartile Parameter Variance Deviation Std Dev of Mean Range Range Value 3.976374E-05 6.305849E-03 6.428168E-03 1.685309E-03 0.00875 0.022 Std Error 1.221975E-05 1.370262E-03 3.66218E-04 95% LCL 2.089816E-05 4.57145E-03 1.221771E-03 95% UCL 1.032051E-04 1.015899E-02 2.715104E-03 Skewness and Kurtosis Section of SU_4102_SOF Coefficient Coefficient Parameter Skewness Kurtosis Fisher's g1 Fisher's g2 of Variation of Dispersion Value -0.1571983 2.322142 -0.1767267 -0.4104718 1.243407 1.014286 Std Error 0.3622322 0.4747743 0.4645888 Trimmed Section of SU_4102_SOF 5% 10% 15% 25% 35% 45% Parameter Trimmed Trimmed Trimmed Trimmed Trimmed Trimmed Trim-Mean 5.190476E-03 5.232143E-03 5.193877E-03 5.142857E-03 5.02381E-03 0.005 Trim-Std Dev 5.459434E-03 4.584677E-03 3.716236E-03 2.91139E-03 1.976235E-03 1.870829E-03 Count 12.6 11.2 9.8 7 4.2 1.4 Mean-Deviation Section of SU_4102_SOF Parameter |X-Mean| |X-Median| (X-Mean)^2 (X-Mean)^3 (X-Mean)^4 Average 5.071429E-03 5.071429E-03 3.692347E-05 -3.526968E-08 3.165875E-09 Std Error 1.011427E-03 1.134691E-05 8.495885E-08 1.495474E-09
Appendix B Page 12
Descriptive Statistics Report Quartile Section of SU_4102_SOF 10th 25th 50th 75th 90th Parameter Percentile Percentile Percentile Percentile Percentile Value -0.005 0.00075 0.005 0.0095 0.0145 95% LCL -0.007 0 0.004 95% UCL 0.006 0.009 0.015 Normality Test Section of SU_4102_SOF Test Prob 10% Critical 5% Critical Decision Test Name Value Level Value Value (5%) Shapiro-Wilk W 0.9834583 0.990108 Accept Normality Anderson-Darling 0.1156718 0.991178 Accept Normality Martinez-Iglewicz 0.9861903 1.305415 1.57245 Accept Normality Kolmogorov-Smirnov 6.745965E-02 0.208 0.226 Accept Normality D'Agostino Skewness -0.3117 0.755251 1.645 1.960 Accept Normality D'Agostino Kurtosis -0.1971 0.843756 1.645 1.960 Accept Normality D'Agostino Omnibus 0.1360 0.934253 4.605 5.991 Accept Normality Plots Section of SU_4102_SOF
0.0
1.3
2.5
3.8
5.0
0.0 0.0 0.0 0.0 0.0
Histogram of SU_4102_SOF
SU_4102_SOF
Coun
t
0.0
0.0
0.0
0.0
0.0
-2.0 -1.0 0.0 1.0 2.0
Normal Probability Plot of SU_4102_SOF
Expected Normals
SU_4
102_
SOF
Appendix B Page 13
Descriptive Statistics Report Percentile Section of SU_4102_SOF Percentile Value 95% LCL 95% UCL Exact Conf. Level 99.0 0.015 95.0 0.015 90.0 0.0145 85.0 0.01325 80.0 0.011 0.004 0.015 95.3622 75.0 0.0095 0.004 0.015 97.1873 70.0 0.009 0.003 0.015 98.4929 65.0 0.0085 0.003 0.014 95.5137 60.0 0.007 0.002 0.014 97.4393 55.0 0.00625 0.001 0.011 97.1563 50.0 0.005 0 0.009 96.4844 45.0 0.00375 0 0.009 97.1563 40.0 0.003 -0.003 0.009 97.4393 35.0 0.00225 -0.007 0.007 97.3253 30.0 0.0015 -0.007 0.006 96.1749 25.0 0.00075 -0.007 0.006 97.1873 20.0 0 -0.007 0.006 95.3622 15.0 -0.00225 10.0 -0.005 5.0 -0.007 1.0 -0.007 Percentile Formula: Ave X(p[n+1]) Stem-Leaf Plot Section of SU_4102_SOF Depth Stem Leaves 1 . | 7 2 -0* | 3 7 0* | 01234 7 . | 6799 3 1* | 14 1 . | 5 Unit = .001 Example: 1 |2 Represents 0.012
Appendix B Page 14
0.10.0-0.1
99
95
90
80706050403020
10
5
1
Data
Per
cent
1.067AD*
Goodness of Fit
Normal Probability Plot for 4102 CO60ML Estimates - 95% CI
Mean
StDev
0.003515
0.0303877
ML Estimates
-2 -1 0 1 2 3 4 5 6 7
1
5
10
20304050607080
90
95
99
Data
Per
cent
AD* 1.216Goodness of Fit
Normal Probability Plot for 4102 TOTAL UML Estimates - 95% CI
Mean
StDev
2.55714
1.33615
ML Estimates
Appendix B Page 15
0.0160.0120.0080.0040.000-0.004-0.008
95% Confidence Interval for Mu
0.00950.00700.00450.0020
95% Confidence Interval for Median
Variable: 4102 SOF
9.49E-04
4.57E-03
1.43E-03
Maximum3rd QuartileMedian1st QuartileMinimum
NKurtosisSkewnessVarianceStDevMean
P-Value:A-Squared:
9.10E-03
1.02E-02
8.71E-03
1.50E-029.50E-035.00E-037.50E-04-7.0E-03
14-4.1E-01-1.8E-013.98E-056.31E-035.07E-03
0.9880.114
95% Confidence Interval for Median
95% Confidence Interval for Sigma
95% Confidence Interval for Mu
Anderson-Darling Normality Test
Descriptive Statistics
Appendix B Page 16
One-Sample T-Test Report Variable SU_4102_SOF Descriptive Statistics Section Standard Standard 95% LCL 95% UCL Variable Count Mean Deviation Error of Mean of Mean SU_4102_SOF 14 5.071429E-03 6.305849E-03 1.685309E-03 1.43054E-03 8.712318E-03 T for Confidence Limits = 2.1604 Tests of Assumptions Section Assumption Value Probability Decision(5%) Skewness Normality -0.3117 0.755251 Cannot reject normality Kurtosis Normality -0.1971 0.843756 Cannot reject normality Omnibus Normality 0.1360 0.934253 Cannot reject normality Correlation Coefficient T-Test For Difference Between Mean and Value Section Alternative Prob Decision Power Power Hypothesis T-Value Level (5%) (Alpha=.05) (Alpha=.01) SU_4102_SOF<>1 -590.3538 0.000000 Reject Ho 1.000000 1.000000 SU_4102_SOF<1 -590.3538 0.000000 Reject Ho 1.000000 1.000000 SU_4102_SOF>1 -590.3538 1.000000 Accept Ho 0.000000 0.000000 Nonparametric Tests Section Quantile (Sign) Test Hypothesized Number Number Prob Prob Prob Value Quantile Lower Higher Lower Higher Both 1 0.5 14 0 1.000000 0.000061 0.000122 Wilcoxon Signed-Rank Test for Difference in Medians W Mean Std Dev Number Number Sets Multiplicity Sum Ranks of W of W of Zeros of Ties Factor 0 52.5 15.92561 0 1 6 Approximation Without Approximation With Exact Probability Continuity Correction Continuity Correction Alternative Prob Decision Prob Decision Prob Decision Hypothesis Level (5%) Z-Value Level (5%) Z-Value Level (5%) Median<>1 3.2966 0.000979 Reject Ho 3.2652 0.001094 Reject Ho Median<1 -3.2966 0.000489 Reject Ho -3.2652 0.000547 Reject Ho Median>1 -3.2966 0.999511 Accept Ho -3.3280 0.999563 Accept Ho
Appendix B Page 17
0.98
1.00
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
0.8 0.9 1.0 1.1Prob
obili
ty th
at th
e Su
rvey
Uni
t Will
Pas
s
SOF Value
Retrospective Power of the Sign TestSurface Soil Volumetric Measurements SOF Values
Survey Unit CE-FSS-41-02
Power Boundary of the Gray Region
N = 14alpha = 0.05beta = 0.05σ = 0.006Actual Median
SOF Value is 0.005
True Power of the Sign Test ~ 1.00
Appendix B Page 18
Appendix B Page 19
Appendix B Page 20
Docu
ment:
P:\Pr
ojects
\ABBW
IN\G
IS-Av
8\Map
Docu
ments
\FUSR
AP R
emed
iation
\FSS\
Waste
Line
s\WL_
FSS_
Scan
s_8x
11P.m
xd
PDF:
P:\Pr
ojects
\abbw
in\GI
S-Av
8\Figu
res\FU
SRAP
Rem
ediat
ion\FS
S\Wa
ste Li
nes\R
eport
Figu
res\C
E-FS
S-41
-02_S
can.p
df 0
7/27/2
011
3:45 P
M b
rpeter
s
Prepared/Date: BRP 07/27/11
1009000 1009200 1009400
8828
0088
3000
8832
0088
3400
8836
00
¯0 10050
Feet
LegendExtent of GammaWalkover SurveyCE-FSS-41-02
ForestOpenWaterRoadBuilding
CT St
ate Pl
ane N
AD 83
Feet
Checked/Date: GSM 07/27/11
Scan SurveySurvey Unit CE-FSS-41-02
Final Status SurveyCE Windsor Site
Windsor, Connecticut
Appendix B Page 21
Appendix B Page 22
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:24:45 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-001
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-001
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 8.897E+002 g
Sample Taken On: 5/3/2010 11:30:00 AM
Acquisition Started: 1/26/2011 7:24:52 PM
Live Time: 1000.0 seconds
Real Time: 1000.9 seconds
Dead Time: 0.09 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.68E+001 2.33E+000 1.21E+000
CO-60 U 5.67E-002 6.40E-002 1.38E-001
SB-125 U 1.10E-001 1.88E-001 3.11E-001
CS-137 U -2.12E-002 8.01E-002 1.13E-001
Ra-226 6.34E-001 1.05E-001 1.85E-001
TH-230 U -5.12E+000 2.27E+001 2.81E+001
PA-231 U -8.29E-001 2.79E+000 3.60E+000
Th-231 U 1.21E+000 8.41E-001 1.35E+000
Th-232 7.54E-001 1.13E-001 2.03E-001
PA-234M U -6.70E+000 9.80E+000 1.21E+001
U-234 U 2.45E+001 1.06E+002 1.41E+002
U-235 U 4.43E-002 8.62E-002 1.28E-001
U-238 U 5.63E-002 1.15E+000 1.70E+000
AM-241 U -1.14E-001 2.90E-001 3.54E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 23
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:25:06 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-002
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-002
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 8.468E+002 g
Sample Taken On: 5/3/2010 11:47:00 AM
Acquisition Started: 1/26/2011 7:59:28 PM
Live Time: 1000.0 seconds
Real Time: 1000.9 seconds
Dead Time: 0.09 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.55E+001 2.35E+000 1.63E+000
CO-60 U 4.47E-002 8.03E-002 1.50E-001
SB-125 U -7.05E-002 2.35E-001 3.27E-001
CS-137 8.83E-002 5.99E-002 8.77E-002
Ra-226 7.49E-001 1.13E-001 1.95E-001
TH-230 U -2.90E+001 2.75E+001 3.09E+001
PA-231 U -1.13E+000 2.61E+000 3.45E+000
Th-231 U 1.26E+000 9.23E-001 1.48E+000
Th-232 8.14E-001 1.22E-001 2.52E-001
PA-234M U 4.51E+000 9.43E+000 1.62E+001
U-234 U 1.52E-001 1.05E+002 1.36E+002
U-235 U 1.03E-001 9.30E-002 1.46E-001
U-238 1.53E+000 9.28E-001 1.37E+000
AM-241 U -1.46E-001 3.05E-001 3.70E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 24
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:25:22 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-003
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-003
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.057E+002 g
Sample Taken On: 5/3/2010 1:00:00 PM
Acquisition Started: 1/26/2011 8:29:29 PM
Live Time: 1000.0 seconds
Real Time: 1000.9 seconds
Dead Time: 0.09 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.58E+001 2.20E+000 9.30E-001
CO-60 U -3.07E-003 9.78E-002 1.46E-001
SB-125 UI 2.41E-001 2.04E-001 3.61E-001
CS-137 6.88E-002 5.25E-002 7.90E-002
Ra-226 7.01E-001 1.10E-001 1.78E-001
TH-230 U 9.65E+000 2.14E+001 2.83E+001
PA-231 UI 1.43E+000 1.52E+000 2.50E+000
Th-231 U 1.22E+000 8.38E-001 1.35E+000
Th-232 7.46E-001 1.27E-001 1.51E-001
PA-234M U -2.75E+000 8.49E+000 1.18E+001
U-234 U 1.30E+001 9.82E+001 1.29E+002
U-235 8.24E-002 7.61E-002 1.20E-001
U-238 U 1.11E+000 1.12E+000 1.77E+000
AM-241 U 1.54E-001 2.55E-001 3.54E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 25
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:25:41 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-004
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-004
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.062E+002 g
Sample Taken On: 5/3/2010 11:54:00 AM
Acquisition Started: 1/26/2011 8:52:57 PM
Live Time: 1000.0 seconds
Real Time: 1000.9 seconds
Dead Time: 0.09 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.57E+001 2.19E+000 9.22E-001
CO-60 U 1.49E-002 8.38E-002 1.35E-001
SB-125 U 1.78E-002 2.16E-001 3.21E-001
CS-137 1.33E-001 1.25E-001 2.06E-001
Ra-226 8.36E-001 1.00E-001 1.43E-001
TH-230 U 2.05E+001 2.27E+001 3.18E+001
PA-231 U -2.78E+000 2.92E+000 3.30E+000
Th-231 7.34E-001 5.72E-001 1.02E+000
Th-232 7.35E-001 7.98E-002 1.31E-001
PA-234M U -2.68E+000 9.74E+000 1.38E+001
U-234 U -2.05E+002 1.29E+002 1.22E+002
U-235 U 1.45E-001 8.38E-002 1.39E-001
U-238 U 6.55E-001 1.15E+000 1.78E+000
AM-241 U -6.99E-002 2.82E-001 3.52E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 26
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:27:50 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-005
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-005
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.281E+002 g
Sample Taken On: 5/3/2010 12:40:00 PM
Acquisition Started: 1/26/2011 9:11:33 PM
Live Time: 1000.0 seconds
Real Time: 1001.1 seconds
Dead Time: 0.11 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.56E+001 2.19E+000 1.14E+000
CO-60 U -5.60E-002 1.05E-001 1.28E-001
SB-125 UI -1.43E-001 2.51E-001 3.28E-001
CS-137 U -1.48E-002 8.21E-002 1.14E-001
Ra-226 6.81E-001 8.83E-002 1.79E-001
TH-230 U 1.57E+000 2.05E+001 2.64E+001
PA-231 U -1.22E+000 2.34E+000 3.11E+000
Th-231 U 1.04E+000 8.02E-001 1.29E+000
Th-232 8.66E-001 7.47E-002 1.35E-001
PA-234M U -2.33E+000 8.82E+000 1.24E+001
U-234 U 4.28E+000 1.04E+002 1.35E+002
U-235 1.54E-001 1.08E-001 1.84E-001
U-238 U 6.66E-001 1.09E+000 1.69E+000
AM-241 U 6.33E-002 2.67E-001 3.54E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 27
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:29:37 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-006
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-006
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.234E+002 g
Sample Taken On: 5/3/2010 11:50:00 AM
Acquisition Started: 1/26/2011 9:29:46 PM
Live Time: 1000.0 seconds
Real Time: 1001.0 seconds
Dead Time: 0.10 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.59E+001 2.25E+000 1.35E+000
CO-60 U 1.82E-002 9.44E-002 1.51E-001
SB-125 UI 2.40E-002 2.11E-001 3.08E-001
CS-137 U 7.94E-002 8.97E-002 1.49E-001
Ra-226 6.59E-001 1.07E-001 1.97E-001
TH-230 U 2.96E+000 2.17E+001 2.83E+001
PA-231 U 8.43E-001 2.27E+000 3.43E+000
Th-231 U 1.06E+000 8.15E-001 1.31E+000
Th-232 8.08E-001 1.10E-001 2.18E-001
PA-234M U 3.30E+000 8.79E+000 1.45E+001
U-234 U 7.41E+001 9.26E+001 1.32E+002
U-235 UI 1.04E-001 8.40E-002 1.37E-001
U-238 U 3.32E-001 1.10E+000 1.67E+000
AM-241 U -2.21E-001 3.00E-001 3.50E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 28
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:00 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-007
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-007
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 8.780E+002 g
Sample Taken On: 5/3/2010 11:26:00 AM
Acquisition Started: 1/28/2011 2:21:26 PM
Live Time: 1000.0 seconds
Real Time: 1000.9 seconds
Dead Time: 0.09 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.74E+001 2.38E+000 1.20E+000
CO-60 U 1.43E-002 7.09E-002 1.21E-001
SB-125 U 1.15E-001 1.97E-001 3.20E-001
CS-137 U -2.37E-003 8.30E-002 1.22E-001
Ra-226 4.55E-001 1.06E-001 2.22E-001
TH-230 U -4.61E+000 2.22E+001 2.78E+001
PA-231 U -9.39E-001 2.50E+000 3.36E+000
Th-231 U 1.28E+000 8.58E-001 1.39E+000
Th-232 6.27E-001 6.72E-002 1.66E-001
PA-234M U 5.69E+000 9.27E+000 1.62E+001
U-234 U -5.42E+001 1.09E+002 1.30E+002
U-235 U -2.74E-002 9.75E-002 1.33E-001
U-238 U 1.82E+000 1.08E+000 1.79E+000
AM-241 U 1.36E-001 2.73E-001 3.74E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 29
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:17 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-008
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-008
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.018E+002 g
Sample Taken On: 5/3/2010 11:44:00 AM
Acquisition Started: 1/28/2011 2:47:10 PM
Live Time: 1000.0 seconds
Real Time: 1000.8 seconds
Dead Time: 0.08 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.68E+001 2.26E+000 7.67E-001
CO-60 U -5.04E-002 1.04E-001 1.19E-001
SB-125 U 1.57E-001 2.10E-001 3.49E-001
CS-137 U -6.13E-002 9.47E-002 1.23E-001
Ra-226 6.51E-001 1.04E-001 1.83E-001
TH-230 U 7.54E+000 2.37E+001 3.13E+001
PA-231 UI 2.16E+000 1.69E+000 2.66E+000
Th-231 U 1.50E+000 8.41E-001 1.38E+000
Th-232 8.32E-001 1.06E-001 1.84E-001
PA-234M U 1.30E+001 7.41E+000 1.64E+001
U-234 U 9.54E+001 9.63E+001 1.39E+002
U-235 U 5.79E-002 9.19E-002 1.37E-001
U-238 U 9.78E-001 1.12E+000 1.76E+000
AM-241 U 3.33E-002 2.76E-001 3.61E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 30
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:35 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-009
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-009
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 8.436E+002 g
Sample Taken On: 5/3/2010 11:33:00 AM
Acquisition Started: 1/28/2011 3:06:01 PM
Live Time: 1000.0 seconds
Real Time: 1000.8 seconds
Dead Time: 0.08 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.59E+001 2.32E+000 1.29E+000
CO-60 U 1.78E-002 7.85E-002 1.34E-001
SB-125 U 1.43E-001 1.97E-001 3.33E-001
CS-137 U -1.80E-003 9.15E-002 1.32E-001
Ra-226 7.21E-001 1.25E-001 1.77E-001
TH-230 U 1.26E+001 2.21E+001 3.02E+001
PA-231 U -1.75E+000 2.36E+000 3.00E+000
Th-231 U 1.25E+000 8.29E-001 1.36E+000
Th-232 7.53E-001 1.07E-001 2.11E-001
PA-234M U -2.59E+000 1.03E+001 1.48E+001
U-234 U -5.70E+001 1.04E+002 1.24E+002
U-235 U 5.11E-002 9.50E-002 1.40E-001
U-238 1.16E+000 5.61E-001 1.58E+000
AM-241 U 1.66E-001 2.79E-001 3.88E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 31
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:53 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-010
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-010
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.025E+002 g
Sample Taken On: 5/3/2010 12:57:00 PM
Acquisition Started: 1/28/2011 3:24:42 PM
Live Time: 1000.0 seconds
Real Time: 1000.9 seconds
Dead Time: 0.09 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.65E+001 2.30E+000 1.26E+000
CO-60 U 9.44E-003 8.88E-002 1.36E-001
SB-125 U 6.08E-002 1.99E-001 3.07E-001
CS-137 U 3.50E-002 6.45E-002 1.09E-001
Ra-226 6.03E-001 1.00E-001 2.04E-001
TH-230 U -4.10E+000 2.15E+001 2.70E+001
PA-231 U -1.95E+000 2.47E+000 2.98E+000
Th-231 U 8.80E-001 8.44E-001 1.34E+000
Th-232 7.35E-001 1.43E-001 1.55E-001
PA-234M U -2.51E+000 7.95E+000 1.10E+001
U-234 U 3.29E+001 8.95E+001 1.23E+002
U-235 U 9.13E-002 8.22E-002 1.30E-001
U-238 UI 7.69E-001 8.27E-001 1.36E+000
AM-241 U 1.79E-001 2.42E-001 3.41E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 32
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:31:13 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-010LR
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-010LR
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.025E+002 g
Sample Taken On: 5/3/2010 12:57:00 PM
Acquisition Started: 1/28/2011 5:44:32 PM
Live Time: 1000.0 seconds
Real Time: 1000.7 seconds
Dead Time: 0.07 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.37E+001 2.09E+000 1.26E+000
CO-60 U 5.18E-003 6.87E-002 1.13E-001
SB-125 U -6.02E-002 2.20E-001 3.07E-001
CS-137 U -6.19E-003 8.43E-002 1.23E-001
Ra-226 6.64E-001 1.02E-001 3.25E-001
TH-230 U 1.41E+001 1.85E+001 2.62E+001
PA-231 U -2.56E+000 2.71E+000 3.09E+000
Th-231 U 9.07E-001 8.31E-001 1.32E+000
Th-232 6.89E-001 7.59E-002 1.37E-001
PA-234M U -4.77E-001 9.99E+000 1.45E+001
U-234 U 2.27E+001 1.06E+002 1.37E+002
U-235 U 1.19E-001 7.80E-002 1.28E-001
U-238 U 1.53E+000 1.12E+000 1.81E+000
AM-241 U -1.70E-001 2.96E-001 3.51E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 33
Ra-226 6.03E-01 5.10E-02 12 0.6 - 1.66 6.64E-01 5.20E-02 1.10 -4.8 Yes N/ATh-232 7.35E-01 7.30E-02 10 0.6 - 1.66 6.89E-01 3.87E-02 0.94 3.2 Yes N/AK-40 1.65E+01 1.17E+00 14 0.6 - 1.66 1.37E+01 1.07E+00 0.83 9.3 Yes N/ANote:
FSS Quality Control Accuracy and Precision Comparison
Isotope
Sample ID CE-FSS-41-02-010 Sample ID CE-FSS-41-02-010LRActivity Value (pCi/g) Uncert. Resolution
Agreement Range
Activity Value (pCi/g) Uncert.
Agreement Ratio
(Accuracy)% Deviation (Precision) Acceptable Comments
Resolution = Standard Activity Value/Standard Error
Resolution Agreement Range<4
Checked/Date: HTD 07/11/11
No Comparison 4 - 7 0.4 - 2.08 - 15 0.6 - 1.6616 - 50 0.75 - 1.3351- 200 0.80 - 1.25> 200 0.85 - 1.18
Prepared/Date: GSM 07/11/11
Appendix B Page 34
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:31:35 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-011
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-011
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.026E+002 g
Sample Taken On: 5/3/2010 11:40:00 AM
Acquisition Started: 1/28/2011 3:46:51 PM
Live Time: 1000.0 seconds
Real Time: 1000.7 seconds
Dead Time: 0.07 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.48E+001 2.18E+000 1.28E+000
CO-60 U -5.83E-003 9.87E-002 1.41E-001
SB-125 U 4.64E-002 2.17E-001 3.31E-001
CS-137 U 3.98E-002 7.66E-002 1.27E-001
Ra-226 5.75E-001 9.95E-002 1.53E-001
TH-230 U -1.10E+001 2.26E+001 2.70E+001
PA-231 U -2.51E+000 2.82E+000 3.39E+000
Th-231 U 1.63E+000 7.73E-001 1.30E+000
Th-232 7.67E-001 1.02E-001 1.79E-001
PA-234M U -2.61E-001 1.02E+001 1.52E+001
U-234 U -5.96E+000 9.70E+001 1.24E+002
U-235 7.95E-002 8.40E-002 1.36E-001
U-238 U 7.38E-001 1.11E+000 1.73E+000
AM-241 U 1.85E-001 2.76E-001 3.75E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 35
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:31:54 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-012
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-012
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.026E+002 g
Sample Taken On: 5/3/2010 11:22:00 AM
Acquisition Started: 1/28/2011 4:13:53 PM
Live Time: 1000.0 seconds
Real Time: 1000.8 seconds
Dead Time: 0.08 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.53E+001 2.20E+000 1.17E+000
CO-60 U -1.09E-002 8.39E-002 1.19E-001
SB-125 U 3.29E-002 1.92E-001 2.94E-001
CS-137 U -4.47E-002 1.00E-001 1.32E-001
Ra-226 7.65E-001 1.50E-001 3.49E-001
TH-230 U 7.40E-001 2.09E+001 2.69E+001
PA-231 U -1.84E+000 2.35E+000 2.98E+000
Th-231 1.27E+000 8.31E-001 1.33E+000
Th-232 7.89E-001 1.19E-001 2.02E-001
PA-234M U -1.26E+000 8.11E+000 1.19E+001
U-234 U -4.02E+000 1.04E+002 1.34E+002
U-235 U 8.37E-002 8.20E-002 1.28E-001
U-238 U 2.10E+000 1.06E+000 1.78E+000
AM-241 U -1.52E-001 3.10E-001 3.71E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 36
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:32:14 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-013
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-013
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.311E+002 g
Sample Taken On: 5/3/2010 1:05:00 PM
Acquisition Started: 1/28/2011 4:31:57 PM
Live Time: 1000.0 seconds
Real Time: 1000.8 seconds
Dead Time: 0.08 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.54E+001 2.18E+000 1.15E+000
CO-60 U -1.46E-002 8.95E-002 1.31E-001
SB-125 U 1.20E-001 1.99E-001 3.24E-001
CS-137 U 9.32E-002 8.01E-002 1.43E-001
Ra-226 7.01E-001 9.51E-002 1.39E-001
TH-230 U -7.80E+000 2.35E+001 2.78E+001
PA-231 U -1.71E+000 2.66E+000 2.99E+000
Th-231 1.53E+000 1.22E+000 1.01E+000
Th-232 8.26E-001 7.80E-002 1.23E-001
PA-234M U 6.57E+000 7.82E+000 1.47E+001
U-234 U -1.70E+001 9.97E+001 1.25E+002
U-235 U 4.93E-002 9.21E-002 1.35E-001
U-238 U 1.53E+000 1.17E+000 1.86E+000
AM-241 U 9.66E-002 2.50E-001 3.40E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 37
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:32:33 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-013S
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-013S
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 7.812E+002 g
Sample Taken On: 5/3/2010 1:10:00 PM
Acquisition Started: 1/28/2011 4:52:14 PM
Live Time: 1000.0 seconds
Real Time: 1000.8 seconds
Dead Time: 0.08 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.85E+001 2.62E+000 1.48E+000
CO-60 U -2.67E-002 9.82E-002 1.38E-001
SB-125 U 3.67E-002 2.32E-001 3.50E-001
CS-137 U -4.24E-002 9.99E-002 1.35E-001
Ra-226 7.68E-001 1.25E-001 2.32E-001
TH-230 U -1.01E+001 2.77E+001 3.37E+001
PA-231 1.80E+000 1.96E+000 3.00E+000
Th-231 1.08E+000 9.71E-001 1.60E+000
Th-232 8.53E-001 1.30E-001 2.51E-001
PA-234M U -2.23E+000 1.16E+001 1.64E+001
U-234 U -1.23E+002 1.25E+002 1.36E+002
U-235 UI 1.13E-001 8.93E-002 1.45E-001
U-238 U 7.58E-001 1.29E+000 1.99E+000
AM-241 U -1.69E-001 3.28E-001 3.94E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 38
Ra-226 7.01E-01 4.85E-02 14 0.6 - 1.66 7.68E-01 6.38E-02 1.10 -4.6 Yes N/ATh-232 8.26E-01 3.98E-02 21 0.75 - 1.33 8.53E-01 6.63E-02 1.03 -1.6 Yes N/AK-40 1.54E+01 1.11E+00 14 0.6 - 1.66 1.85E+01 1.34E+00 1.20 -9.1 Yes N/ANote:
FSS Quality Control Accuracy and Precision Comparison
Isotope
Sample ID CE-FSS-41-02-013 Sample ID CE-FSS-41-02-013SActivity Value (pCi/g) Uncert. Resolution
Agreement Range
Activity Value (pCi/g) Uncert.
Agreement Ratio
(Accuracy)% Deviation (Precision) Acceptable Comments
Resolution = Standard Activity Value/Standard Error
Resolution Agreement Range<4
16 - 50 0.75 - 1.33
No Comparison 4 - 7 0.4 - 2.08 - 15 0.6 - 1.66
Checked/Date: HTD 07/11/11
51- 200 0.80 - 1.25> 200 0.85 - 1.18
Prepared/Date: GSM 07/11/11
Appendix B Page 39
CERTIFICATE OF ANALYSIS Report 5/23/2011 12:32:53 PM Page 1
********************************************************************************
***** C E R T I F I C A T E O F A N A L Y S I S *****
********************************************************************************
Site Location: CE Windsor
Sample ID: FSS-41-02-014
Sample Title: CE-FSS-41-02
Sample Description: FSS-41-02-014
Detector Name: 25%HPGE
Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB
Sample Size: 9.150E+002 g
Sample Taken On: 5/3/2010 12:53:00 PM
Acquisition Started: 1/28/2011 5:19:06 PM
Live Time: 1000.0 seconds
Real Time: 1000.8 seconds
Dead Time: 0.08 %
Efficiency ID: 1316-45_04-30-10
Nuclide Nuclide Activity Nuclide
Name Activity Uncert. MDA
Qualifier (pCi/g ) (pCi/g ) (pCi/g )
K-40 1.87E+001 2.41E+000 1.06E+000
CO-60 U 2.22E-002 8.25E-002 1.39E-001
SB-125 UI -3.55E-002 2.26E-001 3.22E-001
CS-137 U 1.72E-004 8.26E-002 1.21E-001
Ra-226 6.18E-001 1.03E-001 1.79E-001
TH-230 U -2.06E+001 2.36E+001 2.67E+001
PA-231 UI 1.60E+000 1.56E+000 2.54E+000
Th-231 1.11E+000 9.48E-001 1.03E+000
Th-232 9.13E-001 9.92E-002 1.98E-001
PA-234M U 7.27E+000 7.50E+000 1.47E+001
U-234 U 9.14E+000 1.04E+002 1.36E+002
U-235 U 8.68E-002 8.41E-002 1.31E-001
U-238 UI 1.29E+000 1.12E+000 1.55E+000
AM-241 U -1.29E-001 3.06E-001 3.70E-001
Uncertainty reported at 1.9600 sigma
Appendix B Page 40