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FINAL STATUS SURVEY REPORT SUBMITTAL NUMBER 1 CE WINDSOR SITE WINDSOR, CONNECTICUT APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA EVALUATION

APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

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Page 1: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

FINAL STATUS SURVEY REPORT

SUBMITTAL NUMBER 1

CE WINDSOR SITE WINDSOR, CONNECTICUT

APPENDIX B

SURVEY UNIT CE-FSS-41-02

RESULTS AND DATA EVALUATION

Page 2: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60
Page 3: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

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"C CE-FSS-41-02-014

CE-FSS-41-02-013

CE-FSS-41-02-012

CE-FSS-41-02-011

CE-FSS-41-02-010

CE-FSS-41-02-009

CE-FSS-41-02-008

CE-FSS-41-02-007

CE-FSS-41-02-006

CE-FSS-41-02-005

CE-FSS-41-02-004

CE-FSS-41-02-002

CE-FSS-41-02-001

CE-FSS-41-02-003

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CE-FSS-41-02ForestOpenWaterRoadBuilding

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Checked/Date: GSM 07/27/11

Sample LocationsSurvey Unit CE-FSS-41-02

Final Status SurveyCE Windsor Site

Windsor, Connecticut

Appendix B Page 1

Page 4: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

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"C 0.0222 Co-602.691 U

0.0178 Co-601.585 U

0.0143 Co-60-0.85 U

0.0182 Co-603.239 U

-0.056 Co-604.774 U

0.0149 Co-604.495 U

0.0447 Co-603.178 U

0.0567 Co-601.372 U

-0.0207 Co-602.513 U

-0.0109 Co-602.596 U

0.00731 Co-603.262 U

-0.0504 Co-601.795 U

-0.00583 Co-602.465 U

-0.00307 Co-602.554 U

1009000 1009200 1009400

8828

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3000

8832

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Legend"C Sample Location

CE-FSS-41-02ForestOpenWaterRoadBuilding

Co-60 (pCi/g)Total U (pCi/g)

CT St

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AD 83

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Checked/Date: GSM 07/27/11

Sample ResultsSurvey Unit CE-FSS-41-02

Final Status SurveyCE Windsor Site

Windsor, Connecticut

Appendix B Page 2

Page 5: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Activity Uncert. MDC Qualifier Activity Uncert. MDC QualifierCE-FSS-41-02-001 5.67E-02 6.40E-02 1.38E-01 U 4.43E-02 8.62E-02 1.28E-01 U 1.4 0.014CE-FSS-41-02-002 4.47E-02 8.03E-02 1.50E-01 U 1.03E-01 9.30E-02 1.46E-01 U 3.2 0.015CE-FSS-41-02-003 -3.07E-03 9.78E-02 1.46E-01 U 8.24E-02 7.61E-02 1.20E-01 2.6 0.004CE-FSS-41-02-004 1.49E-02 8.38E-02 1.35E-01 U 1.45E-01 8.38E-02 1.39E-01 U 4.5 0.011CE-FSS-41-02-005 -5.60E-02 1.05E-01 1.28E-01 U 1.54E-01 1.08E-01 1.84E-01 4.8 -0.003CE-FSS-41-02-006 1.82E-02 9.44E-02 1.51E-01 U 1.04E-01 8.40E-02 1.37E-01 UI 3.2 0.009CE-FSS-41-02-007 1.43E-02 7.09E-02 1.21E-01 U -2.74E-02 9.75E-02 1.33E-01 U -0.9 0.001CE-FSS-41-02-008 -5.04E-02 1.04E-01 1.19E-01 U 5.79E-02 9.19E-02 1.37E-01 U 1.8 -0.007CE-FSS-41-02-009 1.78E-02 7.85E-02 1.34E-01 U 5.11E-02 9.50E-02 1.40E-01 U 1.6 0.006CE-FSS-41-02-010 9.44E-03 8.88E-02 1.36E-01 U 9.13E-02 8.22E-02 1.30E-01 U 2.8 0.007

CE-FSS-41-02-010LR 5.18E-03 6.87E-02 1.13E-01 U 1.19E-01 7.80E-02 1.28E-01 U 3.7 0.008CE-FSS-41-02-010AVE 7.31E-03 1.05E-01 3.3 0.007

CE-FSS-41-02-011 -5.83E-03 9.87E-02 1.41E-01 U 7.95E-02 8.40E-02 1.36E-01 2.5 0.003CE-FSS-41-02-012 -1.09E-02 8.39E-02 1.19E-01 U 8.37E-02 8.20E-02 1.28E-01 U 2.6 0.002CE-FSS-41-02-013 -1.46E-02 8.95E-02 1.31E-01 U 4.93E-02 9.21E-02 1.35E-01 U 1.5 0.000

CE-FSS-41-02-013S -2.67E-02 9.82E-02 1.38E-01 1.13E-01 8.93E-02 1.45E-01 UI 3.5 0.001CE-FSS-41-02-013AVE -2.07E-02 8.11E-02 2.5 0.000

CE-FSS-41-02-014 2.22E-02 8.25E-02 1.39E-01 U 8.68E-02 8.41E-02 1.31E-01 U 2.7 0.009

Final Status Survey Volumetric Soil Sample ResultsTotal U (pCi/g)

Sum of Fraction

Sample ID Co-60 U-235

Appendix B Page 3

Page 6: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Sample ID Static Count Rate (cpm)

Ambient Background

(cpm)Net (cpm) pCi/g

FSS-041-02-001 3154 3000 154 0.5FSS-041-02-002 3207 3000 207 0.7FSS-041-02-003 3426 3000 426 1.4FSS-041-02-004 3141 3000 141 0.5FSS-041-02-005 3127 3000 127 0.4FSS-041-02-006 3143 3000 143 0.5FSS-041-02-007 3212 3000 212 0.7FSS-041-02-008 3472 3000 472 1.6FSS-041-02-009 3245 3000 245 0.8FSS-041-02-010 3223 3000 223 0.7FSS-041-02-011 2812 3000 -188 -0.6FSS-041-02-012 2788 3000 -212 -0.7FSS-041-02-013 3426 3000 426 1.4FSS-041-02-014 3202 3000 202 0.7

One-Minute Static Field Measurement Results

Appendix B Page 4

Page 7: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Sample ID X_Coordinate Y_CoordinateCE-FSS-41-02-001 1009195.9516 883398.5049CE-FSS-41-02-002 1009204.6348 883193.1474CE-FSS-41-02-003 1009123.9663 882961.2652CE-FSS-41-02-004 1009155.0719 883074.9066CE-FSS-41-02-005 1009105.5200 882904.8085CE-FSS-41-02-006 1009151.9847 883123.4172CE-FSS-41-02-007 1009203.6482 883411.0583CE-FSS-41-02-008 1009224.7910 883306.2568CE-FSS-41-02-009 1009198.6385 883377.6850CE-FSS-41-02-010 1009109.6933 882970.0723CE-FSS-41-02-011 1009228.5039 883323.0321CE-FSS-41-02-012 1009175.9392 883435.5474CE-FSS-41-02-013 1009129.9188 882988.6412CE-FSS-41-02-014 1009102.9275 882937.8718

Final Status Survey Sample GPS Coordinates

Appendix B Page 5

Page 8: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Summary Section of SU_4102_C060 Standard Standard Count Mean Deviation Error Minimum Maximum Range 14 0.003515 3.153476E-02 8.42802E-03 -0.056 0.0567 0.1127 Counts Section of SU_4102_C060 Sum of Missing Distinct Total Adjusted Rows Frequencies Values Values Sum Sum Squares Sum Squares 29 14 15 14 0.04921 1.310071E-02 1.292774E-02 Means Section of SU_4102_C060 Geometric Harmonic Parameter Mean Median Mean Mean Sum Mode Value 0.003515 0.010805 2.026035E-02 -6.829628E-02 0.04921 Std Error 8.42802E-03 0.1179923 95% LCL -1.469263E-02 -0.0207 -0.2056968 95% UCL 2.172263E-02 0.0182 0.3041168 T-Value 0.4171 Prob Level 0.683439 Count 14 8 14 Variation Section of SU_4102_C060 Standard Unbiased Std Error Interquartile Parameter Variance Deviation Std Dev of Mean Range Range Value 9.944413E-04 3.153476E-02 3.214647E-02 8.42802E-03 0.03255 0.1127 Std Error 3.489077E-04 7.823587E-03 2.090942E-03 95% LCL 5.226368E-04 2.286125E-02 6.109926E-03 95% UCL 2.58103E-03 5.080384E-02 0.0135779 Skewness and Kurtosis Section of SU_4102_C060 Coefficient Coefficient Parameter Skewness Kurtosis Fisher's g1 Fisher's g2 of Variation of Dispersion Value -0.382167 2.723419 -0.4296429 0.1823231 8.971483 2.170887 Std Error 0.3291011 0.8633268 21.2403 Trimmed Section of SU_4102_C060 5% 10% 15% 25% 35% 45% Parameter Trimmed Trimmed Trimmed Trimmed Trimmed Trimmed Trim-Mean 3.866667E-03 4.534821E-03 5.516327E-03 7.008572E-03 8.246905E-03 0.010805 Trim-Std Dev 2.701644E-02 2.147547E-02 1.438601E-02 0.0109649 8.638501E-03 6.538546E-03 Count 12.6 11.2 9.8 7 4.2 1.4 Mean-Deviation Section of SU_4102_C060 Parameter |X-Mean| |X-Median| (X-Mean)^2 (X-Mean)^3 (X-Mean)^4 Average 2.399857E-02 2.345643E-02 9.234098E-04 -1.072371E-05 2.32222E-06 Std Error 5.058021E-03 3.239857E-04 8.530387E-06 9.913321E-07

Appendix B Page 6

Page 9: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Quartile Section of SU_4102_C060 10th 25th 50th 75th 90th Parameter Percentile Percentile Percentile Percentile Percentile Value -0.0532 -0.01335 0.010805 0.0192 0.0507 95% LCL -0.056 -0.0207 0.00731 95% UCL 0.0143 0.0182 0.0567 Normality Test Section of SU_4102_C060 Test Prob 10% Critical 5% Critical Decision Test Name Value Level Value Value (5%) Shapiro-Wilk W 0.9520117 0.592354 Accept Normality Anderson-Darling 0.3437831 0.488485 Accept Normality Martinez-Iglewicz 1.090405 1.305415 1.57245 Accept Normality Kolmogorov-Smirnov 0.1338938 0.208 0.226 Accept Normality D'Agostino Skewness -0.7516 0.452291 1.645 1.960 Accept Normality D'Agostino Kurtosis 0.3877 0.698255 1.645 1.960 Accept Normality D'Agostino Omnibus 0.7152 0.699353 4.605 5.991 Accept Normality Plots Section of SU_4102_C060

0.0

2.0

4.0

6.0

8.0

-0.1 0.0 0.0 0.0 0.1

Histogram of SU_4102_C060

SU_4102_C060

Coun

t

-0.1

0.0

0.0

0.0

0.1

-2.0 -1.0 0.0 1.0 2.0

Normal Probability Plot of SU_4102_C060

Expected Normals

SU_4

102_

C060

Appendix B Page 7

Page 10: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Percentile Section of SU_4102_C060 Percentile Value 95% LCL 95% UCL Exact Conf. Level 99.0 0.0567 95.0 0.0567 90.0 0.0507 85.0 0.039075 80.0 0.0222 0.00731 0.0567 95.3622 75.0 0.0192 0.00731 0.0567 97.1873 70.0 0.018 -0.00307 0.0567 98.4929 65.0 0.017075 -0.00307 0.0447 95.5137 60.0 0.0149 -0.00583 0.0447 97.4393 55.0 0.01445 -0.0109 0.0222 97.1563 50.0 0.010805 -0.0207 0.0182 96.4844 45.0 0.004715 -0.0207 0.0182 97.1563 40.0 -0.00307 -0.0504 0.0178 97.4393 35.0 -0.00514 -0.056 0.0149 97.3253 30.0 -0.008365 -0.056 0.0143 96.1749 25.0 -0.01335 -0.056 0.0143 97.1873 20.0 -0.0207 -0.056 0.0143 95.3622 15.0 -0.042975 10.0 -0.0532 5.0 -0.056 1.0 -0.056 Percentile Formula: Ave X(p[n+1]) Stem-Leaf Plot Section of SU_4102_C060 Depth Stem Leaves Low | -5 2 F | 5 3 T | 2 6 -0* | 100 (5) 0* | 01111 3 T | 2 2 F | 45 Unit = .01 Example: 1 |2 Represents 0.12

Appendix B Page 8

Page 11: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Summary Section of SU_4102_Total_U Standard Standard Count Mean Deviation Error Minimum Maximum Range 14 2.557143 1.386592 0.3705823 -0.9 4.8 5.7 Counts Section of SU_4102_Total_U Sum of Missing Distinct Total Adjusted Rows Frequencies Values Values Sum Sum Squares Sum Squares 29 14 15 11 35.8 116.54 24.99429 Means Section of SU_4102_Total_U Geometric Harmonic Parameter Mean Median Mean Mean Sum Mode Value 2.557143 2.6 2.661186 3.429761 35.8 Std Error 0.3705823 5.188152 95% LCL 1.756549 1.6 24.59168 95% UCL 3.357737 3.2 47.00832 T-Value 6.9003 Prob Level 0.000011 Count 14 13 14 Variation Section of SU_4102_Total_U Standard Unbiased Std Error Interquartile Parameter Variance Deviation Std Dev of Mean Range Range Value 1.922637 1.386592 1.413489 0.3705823 1.475 5.7 Std Error 0.9146558 0.4664381 0.1246608 95% LCL 1.010458 1.005215 0.2686551 95% UCL 4.990124 2.233859 0.5970238 Skewness and Kurtosis Section of SU_4102_Total_U Coefficient Coefficient Parameter Skewness Kurtosis Fisher's g1 Fisher's g2 of Variation of Dispersion Value -0.73719 4.168463 -0.8287697 2.317048 0.5422427 0.3516484 Std Error 0.4058379 1.462824 0.1745276 Trimmed Section of SU_4102_Total_U 5% 10% 15% 25% 35% 45% Parameter Trimmed Trimmed Trimmed Trimmed Trimmed Trimmed Trim-Mean 2.624603 2.6375 2.603061 2.657143 2.611905 2.6 Trim-Std Dev 1.060635 0.7601761 0.5570731 0.3801629 0.1327648 1.501713E-08 Count 12.6 11.2 9.8 7 4.2 1.4 Mean-Deviation Section of SU_4102_Total_U Parameter |X-Mean| |X-Median| (X-Mean)^2 (X-Mean)^3 (X-Mean)^4 Average 0.9204082 0.9142857 1.785306 -1.758525 13.28622 Std Error 0.2224025 0.8493233 1.710164 8.517901

Appendix B Page 9

Page 12: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Quartile Section of SU_4102_Total_U 10th 25th 50th 75th 90th Parameter Percentile Percentile Percentile Percentile Percentile Value 0.25 1.75 2.6 3.225 4.65 95% LCL -0.9 1.6 2.6 95% UCL 2.6 3.2 4.8 Normality Test Section of SU_4102_Total_U Test Prob 10% Critical 5% Critical Decision Test Name Value Level Value Value (5%) Shapiro-Wilk W 0.9192215 0.214293 Accept Normality Anderson-Darling 0.5128176 0.194065 Accept Normality Martinez-Iglewicz 1.371184 1.305415 1.57245 Accept Normality Kolmogorov-Smirnov 0.1532109 0.208 0.226 Accept Normality D'Agostino Skewness -1.4138 0.157417 1.645 1.960 Accept Normality D'Agostino Kurtosis 1.7215 0.085167 1.645 1.960 Accept Normality D'Agostino Omnibus 4.9623 0.083647 4.605 5.991 Accept Normality Plots Section of SU_4102_Total_U

0.0

2.0

4.0

6.0

8.0

-1.0 0.5 2.0 3.5 5.0

Histogram of SU_4102_Total_U

SU_4102_Total_U

Coun

t

-1.0

0.5

2.0

3.5

5.0

-2.0 -1.0 0.0 1.0 2.0

Normal Probability Plot of SU_4102_Total_U

Expected Normals

SU_4

102_

Tota

l_U

Appendix B Page 10

Page 13: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Percentile Section of SU_4102_Total_U Percentile Value 95% LCL 95% UCL Exact Conf. Level 99.0 4.8 95.0 4.8 90.0 4.65 85.0 4.2 80.0 3.3 2.6 4.8 95.3622 75.0 3.225 2.6 4.8 97.1873 70.0 3.2 2.5 4.8 98.4929 65.0 3.075 2.5 4.5 95.5137 60.0 2.7 2.5 4.5 97.4393 55.0 2.625 1.8 3.3 97.1563 50.0 2.6 1.6 3.2 96.4844 45.0 2.575 1.6 3.2 97.1563 40.0 2.5 1.4 3.2 97.4393 35.0 2.5 -0.9 2.7 97.3253 30.0 2.15 -0.9 2.6 96.1749 25.0 1.75 -0.9 2.6 97.1873 20.0 1.6 -0.9 2.6 95.3622 15.0 1.45 10.0 0.25 5.0 -0.9 1.0 -0.9 Percentile Formula: Ave X(p[n+1]) Stem-Leaf Plot Section of SU_4102_Total_U Depth Stem Leaves Low | -9 2 1* | 4 4 . | 68 4 2* | (5) . | 55667 5 3* | 223 2 . | 2 4* | 2 . | 58 Unit = .1 Example: 1 |2 Represents 1.2

Appendix B Page 11

Page 14: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Descriptive Statistics Report Summary Section of SU_4102_SOF Standard Standard Count Mean Deviation Error Minimum Maximum Range 14 5.071429E-03 6.305849E-03 1.685309E-03 -0.007 0.015 0.022 Counts Section of SU_4102_SOF Sum of Missing Distinct Total Adjusted Rows Frequencies Values Values Sum Sum Squares Sum Squares 29 14 15 13 0.071 0.000877 5.169286E-04 Means Section of SU_4102_SOF Geometric Harmonic Parameter Mean Median Mean Mean Sum Mode Value 5.071429E-03 0.005 5.653578E-03 5.490113E-03 0.071 0.009 Std Error 1.685309E-03 2.359433E-02 95% LCL 1.43054E-03 0 2.002755E-02 95% UCL 8.712318E-03 0.009 0.1219724 T-Value 3.0092 Prob Level 0.010059 Count 14 11 13 2 Variation Section of SU_4102_SOF Standard Unbiased Std Error Interquartile Parameter Variance Deviation Std Dev of Mean Range Range Value 3.976374E-05 6.305849E-03 6.428168E-03 1.685309E-03 0.00875 0.022 Std Error 1.221975E-05 1.370262E-03 3.66218E-04 95% LCL 2.089816E-05 4.57145E-03 1.221771E-03 95% UCL 1.032051E-04 1.015899E-02 2.715104E-03 Skewness and Kurtosis Section of SU_4102_SOF Coefficient Coefficient Parameter Skewness Kurtosis Fisher's g1 Fisher's g2 of Variation of Dispersion Value -0.1571983 2.322142 -0.1767267 -0.4104718 1.243407 1.014286 Std Error 0.3622322 0.4747743 0.4645888 Trimmed Section of SU_4102_SOF 5% 10% 15% 25% 35% 45% Parameter Trimmed Trimmed Trimmed Trimmed Trimmed Trimmed Trim-Mean 5.190476E-03 5.232143E-03 5.193877E-03 5.142857E-03 5.02381E-03 0.005 Trim-Std Dev 5.459434E-03 4.584677E-03 3.716236E-03 2.91139E-03 1.976235E-03 1.870829E-03 Count 12.6 11.2 9.8 7 4.2 1.4 Mean-Deviation Section of SU_4102_SOF Parameter |X-Mean| |X-Median| (X-Mean)^2 (X-Mean)^3 (X-Mean)^4 Average 5.071429E-03 5.071429E-03 3.692347E-05 -3.526968E-08 3.165875E-09 Std Error 1.011427E-03 1.134691E-05 8.495885E-08 1.495474E-09

Appendix B Page 12

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Descriptive Statistics Report Quartile Section of SU_4102_SOF 10th 25th 50th 75th 90th Parameter Percentile Percentile Percentile Percentile Percentile Value -0.005 0.00075 0.005 0.0095 0.0145 95% LCL -0.007 0 0.004 95% UCL 0.006 0.009 0.015 Normality Test Section of SU_4102_SOF Test Prob 10% Critical 5% Critical Decision Test Name Value Level Value Value (5%) Shapiro-Wilk W 0.9834583 0.990108 Accept Normality Anderson-Darling 0.1156718 0.991178 Accept Normality Martinez-Iglewicz 0.9861903 1.305415 1.57245 Accept Normality Kolmogorov-Smirnov 6.745965E-02 0.208 0.226 Accept Normality D'Agostino Skewness -0.3117 0.755251 1.645 1.960 Accept Normality D'Agostino Kurtosis -0.1971 0.843756 1.645 1.960 Accept Normality D'Agostino Omnibus 0.1360 0.934253 4.605 5.991 Accept Normality Plots Section of SU_4102_SOF

0.0

1.3

2.5

3.8

5.0

0.0 0.0 0.0 0.0 0.0

Histogram of SU_4102_SOF

SU_4102_SOF

Coun

t

0.0

0.0

0.0

0.0

0.0

-2.0 -1.0 0.0 1.0 2.0

Normal Probability Plot of SU_4102_SOF

Expected Normals

SU_4

102_

SOF

Appendix B Page 13

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Descriptive Statistics Report Percentile Section of SU_4102_SOF Percentile Value 95% LCL 95% UCL Exact Conf. Level 99.0 0.015 95.0 0.015 90.0 0.0145 85.0 0.01325 80.0 0.011 0.004 0.015 95.3622 75.0 0.0095 0.004 0.015 97.1873 70.0 0.009 0.003 0.015 98.4929 65.0 0.0085 0.003 0.014 95.5137 60.0 0.007 0.002 0.014 97.4393 55.0 0.00625 0.001 0.011 97.1563 50.0 0.005 0 0.009 96.4844 45.0 0.00375 0 0.009 97.1563 40.0 0.003 -0.003 0.009 97.4393 35.0 0.00225 -0.007 0.007 97.3253 30.0 0.0015 -0.007 0.006 96.1749 25.0 0.00075 -0.007 0.006 97.1873 20.0 0 -0.007 0.006 95.3622 15.0 -0.00225 10.0 -0.005 5.0 -0.007 1.0 -0.007 Percentile Formula: Ave X(p[n+1]) Stem-Leaf Plot Section of SU_4102_SOF Depth Stem Leaves 1 . | 7 2 -0* | 3 7 0* | 01234 7 . | 6799 3 1* | 14 1 . | 5 Unit = .001 Example: 1 |2 Represents 0.012

Appendix B Page 14

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0.10.0-0.1

99

95

90

80706050403020

10

5

1

Data

Per

cent

1.067AD*

Goodness of Fit

Normal Probability Plot for 4102 CO60ML Estimates - 95% CI

Mean

StDev

0.003515

0.0303877

ML Estimates

-2 -1 0 1 2 3 4 5 6 7

1

5

10

20304050607080

90

95

99

Data

Per

cent

AD* 1.216Goodness of Fit

Normal Probability Plot for 4102 TOTAL UML Estimates - 95% CI

Mean

StDev

2.55714

1.33615

ML Estimates

Appendix B Page 15

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0.0160.0120.0080.0040.000-0.004-0.008

95% Confidence Interval for Mu

0.00950.00700.00450.0020

95% Confidence Interval for Median

Variable: 4102 SOF

9.49E-04

4.57E-03

1.43E-03

Maximum3rd QuartileMedian1st QuartileMinimum

NKurtosisSkewnessVarianceStDevMean

P-Value:A-Squared:

9.10E-03

1.02E-02

8.71E-03

1.50E-029.50E-035.00E-037.50E-04-7.0E-03

14-4.1E-01-1.8E-013.98E-056.31E-035.07E-03

0.9880.114

95% Confidence Interval for Median

95% Confidence Interval for Sigma

95% Confidence Interval for Mu

Anderson-Darling Normality Test

Descriptive Statistics

Appendix B Page 16

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One-Sample T-Test Report Variable SU_4102_SOF Descriptive Statistics Section Standard Standard 95% LCL 95% UCL Variable Count Mean Deviation Error of Mean of Mean SU_4102_SOF 14 5.071429E-03 6.305849E-03 1.685309E-03 1.43054E-03 8.712318E-03 T for Confidence Limits = 2.1604 Tests of Assumptions Section Assumption Value Probability Decision(5%) Skewness Normality -0.3117 0.755251 Cannot reject normality Kurtosis Normality -0.1971 0.843756 Cannot reject normality Omnibus Normality 0.1360 0.934253 Cannot reject normality Correlation Coefficient T-Test For Difference Between Mean and Value Section Alternative Prob Decision Power Power Hypothesis T-Value Level (5%) (Alpha=.05) (Alpha=.01) SU_4102_SOF<>1 -590.3538 0.000000 Reject Ho 1.000000 1.000000 SU_4102_SOF<1 -590.3538 0.000000 Reject Ho 1.000000 1.000000 SU_4102_SOF>1 -590.3538 1.000000 Accept Ho 0.000000 0.000000 Nonparametric Tests Section Quantile (Sign) Test Hypothesized Number Number Prob Prob Prob Value Quantile Lower Higher Lower Higher Both 1 0.5 14 0 1.000000 0.000061 0.000122 Wilcoxon Signed-Rank Test for Difference in Medians W Mean Std Dev Number Number Sets Multiplicity Sum Ranks of W of W of Zeros of Ties Factor 0 52.5 15.92561 0 1 6 Approximation Without Approximation With Exact Probability Continuity Correction Continuity Correction Alternative Prob Decision Prob Decision Prob Decision Hypothesis Level (5%) Z-Value Level (5%) Z-Value Level (5%) Median<>1 3.2966 0.000979 Reject Ho 3.2652 0.001094 Reject Ho Median<1 -3.2966 0.000489 Reject Ho -3.2652 0.000547 Reject Ho Median>1 -3.2966 0.999511 Accept Ho -3.3280 0.999563 Accept Ho

Appendix B Page 17

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0.98

1.00

0.0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

0.9

1.0

0.8 0.9 1.0 1.1Prob

obili

ty th

at th

e Su

rvey

Uni

t Will

Pas

s

SOF Value

Retrospective Power of the Sign TestSurface Soil Volumetric Measurements SOF Values

Survey Unit CE-FSS-41-02

Power Boundary of the Gray Region

N = 14alpha = 0.05beta = 0.05σ = 0.006Actual Median

SOF Value is 0.005

True Power of the Sign Test ~ 1.00

Appendix B Page 18

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Appendix B Page 19

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Appendix B Page 20

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Docu

ment:

P:\Pr

ojects

\ABBW

IN\G

IS-Av

8\Map

Docu

ments

\FUSR

AP R

emed

iation

\FSS\

Waste

Line

s\WL_

FSS_

Scan

s_8x

11P.m

xd

PDF:

P:\Pr

ojects

\abbw

in\GI

S-Av

8\Figu

res\FU

SRAP

Rem

ediat

ion\FS

S\Wa

ste Li

nes\R

eport

Figu

res\C

E-FS

S-41

-02_S

can.p

df 0

7/27/2

011

3:45 P

M b

rpeter

s

Prepared/Date: BRP 07/27/11

1009000 1009200 1009400

8828

0088

3000

8832

0088

3400

8836

00

¯0 10050

Feet

LegendExtent of GammaWalkover SurveyCE-FSS-41-02

ForestOpenWaterRoadBuilding

CT St

ate Pl

ane N

AD 83

Feet

Checked/Date: GSM 07/27/11

Scan SurveySurvey Unit CE-FSS-41-02

Final Status SurveyCE Windsor Site

Windsor, Connecticut

Appendix B Page 21

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Appendix B Page 22

Page 25: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:24:45 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-001

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-001

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 8.897E+002 g

Sample Taken On: 5/3/2010 11:30:00 AM

Acquisition Started: 1/26/2011 7:24:52 PM

Live Time: 1000.0 seconds

Real Time: 1000.9 seconds

Dead Time: 0.09 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.68E+001 2.33E+000 1.21E+000

CO-60 U 5.67E-002 6.40E-002 1.38E-001

SB-125 U 1.10E-001 1.88E-001 3.11E-001

CS-137 U -2.12E-002 8.01E-002 1.13E-001

Ra-226 6.34E-001 1.05E-001 1.85E-001

TH-230 U -5.12E+000 2.27E+001 2.81E+001

PA-231 U -8.29E-001 2.79E+000 3.60E+000

Th-231 U 1.21E+000 8.41E-001 1.35E+000

Th-232 7.54E-001 1.13E-001 2.03E-001

PA-234M U -6.70E+000 9.80E+000 1.21E+001

U-234 U 2.45E+001 1.06E+002 1.41E+002

U-235 U 4.43E-002 8.62E-002 1.28E-001

U-238 U 5.63E-002 1.15E+000 1.70E+000

AM-241 U -1.14E-001 2.90E-001 3.54E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 23

Page 26: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:25:06 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-002

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-002

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 8.468E+002 g

Sample Taken On: 5/3/2010 11:47:00 AM

Acquisition Started: 1/26/2011 7:59:28 PM

Live Time: 1000.0 seconds

Real Time: 1000.9 seconds

Dead Time: 0.09 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.55E+001 2.35E+000 1.63E+000

CO-60 U 4.47E-002 8.03E-002 1.50E-001

SB-125 U -7.05E-002 2.35E-001 3.27E-001

CS-137 8.83E-002 5.99E-002 8.77E-002

Ra-226 7.49E-001 1.13E-001 1.95E-001

TH-230 U -2.90E+001 2.75E+001 3.09E+001

PA-231 U -1.13E+000 2.61E+000 3.45E+000

Th-231 U 1.26E+000 9.23E-001 1.48E+000

Th-232 8.14E-001 1.22E-001 2.52E-001

PA-234M U 4.51E+000 9.43E+000 1.62E+001

U-234 U 1.52E-001 1.05E+002 1.36E+002

U-235 U 1.03E-001 9.30E-002 1.46E-001

U-238 1.53E+000 9.28E-001 1.37E+000

AM-241 U -1.46E-001 3.05E-001 3.70E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 24

Page 27: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:25:22 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-003

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-003

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.057E+002 g

Sample Taken On: 5/3/2010 1:00:00 PM

Acquisition Started: 1/26/2011 8:29:29 PM

Live Time: 1000.0 seconds

Real Time: 1000.9 seconds

Dead Time: 0.09 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.58E+001 2.20E+000 9.30E-001

CO-60 U -3.07E-003 9.78E-002 1.46E-001

SB-125 UI 2.41E-001 2.04E-001 3.61E-001

CS-137 6.88E-002 5.25E-002 7.90E-002

Ra-226 7.01E-001 1.10E-001 1.78E-001

TH-230 U 9.65E+000 2.14E+001 2.83E+001

PA-231 UI 1.43E+000 1.52E+000 2.50E+000

Th-231 U 1.22E+000 8.38E-001 1.35E+000

Th-232 7.46E-001 1.27E-001 1.51E-001

PA-234M U -2.75E+000 8.49E+000 1.18E+001

U-234 U 1.30E+001 9.82E+001 1.29E+002

U-235 8.24E-002 7.61E-002 1.20E-001

U-238 U 1.11E+000 1.12E+000 1.77E+000

AM-241 U 1.54E-001 2.55E-001 3.54E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 25

Page 28: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:25:41 PM Page 1

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***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-004

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-004

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.062E+002 g

Sample Taken On: 5/3/2010 11:54:00 AM

Acquisition Started: 1/26/2011 8:52:57 PM

Live Time: 1000.0 seconds

Real Time: 1000.9 seconds

Dead Time: 0.09 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.57E+001 2.19E+000 9.22E-001

CO-60 U 1.49E-002 8.38E-002 1.35E-001

SB-125 U 1.78E-002 2.16E-001 3.21E-001

CS-137 1.33E-001 1.25E-001 2.06E-001

Ra-226 8.36E-001 1.00E-001 1.43E-001

TH-230 U 2.05E+001 2.27E+001 3.18E+001

PA-231 U -2.78E+000 2.92E+000 3.30E+000

Th-231 7.34E-001 5.72E-001 1.02E+000

Th-232 7.35E-001 7.98E-002 1.31E-001

PA-234M U -2.68E+000 9.74E+000 1.38E+001

U-234 U -2.05E+002 1.29E+002 1.22E+002

U-235 U 1.45E-001 8.38E-002 1.39E-001

U-238 U 6.55E-001 1.15E+000 1.78E+000

AM-241 U -6.99E-002 2.82E-001 3.52E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 26

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CERTIFICATE OF ANALYSIS Report 5/23/2011 12:27:50 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-005

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-005

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.281E+002 g

Sample Taken On: 5/3/2010 12:40:00 PM

Acquisition Started: 1/26/2011 9:11:33 PM

Live Time: 1000.0 seconds

Real Time: 1001.1 seconds

Dead Time: 0.11 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.56E+001 2.19E+000 1.14E+000

CO-60 U -5.60E-002 1.05E-001 1.28E-001

SB-125 UI -1.43E-001 2.51E-001 3.28E-001

CS-137 U -1.48E-002 8.21E-002 1.14E-001

Ra-226 6.81E-001 8.83E-002 1.79E-001

TH-230 U 1.57E+000 2.05E+001 2.64E+001

PA-231 U -1.22E+000 2.34E+000 3.11E+000

Th-231 U 1.04E+000 8.02E-001 1.29E+000

Th-232 8.66E-001 7.47E-002 1.35E-001

PA-234M U -2.33E+000 8.82E+000 1.24E+001

U-234 U 4.28E+000 1.04E+002 1.35E+002

U-235 1.54E-001 1.08E-001 1.84E-001

U-238 U 6.66E-001 1.09E+000 1.69E+000

AM-241 U 6.33E-002 2.67E-001 3.54E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 27

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CERTIFICATE OF ANALYSIS Report 5/23/2011 12:29:37 PM Page 1

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***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-006

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-006

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.234E+002 g

Sample Taken On: 5/3/2010 11:50:00 AM

Acquisition Started: 1/26/2011 9:29:46 PM

Live Time: 1000.0 seconds

Real Time: 1001.0 seconds

Dead Time: 0.10 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.59E+001 2.25E+000 1.35E+000

CO-60 U 1.82E-002 9.44E-002 1.51E-001

SB-125 UI 2.40E-002 2.11E-001 3.08E-001

CS-137 U 7.94E-002 8.97E-002 1.49E-001

Ra-226 6.59E-001 1.07E-001 1.97E-001

TH-230 U 2.96E+000 2.17E+001 2.83E+001

PA-231 U 8.43E-001 2.27E+000 3.43E+000

Th-231 U 1.06E+000 8.15E-001 1.31E+000

Th-232 8.08E-001 1.10E-001 2.18E-001

PA-234M U 3.30E+000 8.79E+000 1.45E+001

U-234 U 7.41E+001 9.26E+001 1.32E+002

U-235 UI 1.04E-001 8.40E-002 1.37E-001

U-238 U 3.32E-001 1.10E+000 1.67E+000

AM-241 U -2.21E-001 3.00E-001 3.50E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 28

Page 31: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:00 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-007

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-007

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 8.780E+002 g

Sample Taken On: 5/3/2010 11:26:00 AM

Acquisition Started: 1/28/2011 2:21:26 PM

Live Time: 1000.0 seconds

Real Time: 1000.9 seconds

Dead Time: 0.09 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.74E+001 2.38E+000 1.20E+000

CO-60 U 1.43E-002 7.09E-002 1.21E-001

SB-125 U 1.15E-001 1.97E-001 3.20E-001

CS-137 U -2.37E-003 8.30E-002 1.22E-001

Ra-226 4.55E-001 1.06E-001 2.22E-001

TH-230 U -4.61E+000 2.22E+001 2.78E+001

PA-231 U -9.39E-001 2.50E+000 3.36E+000

Th-231 U 1.28E+000 8.58E-001 1.39E+000

Th-232 6.27E-001 6.72E-002 1.66E-001

PA-234M U 5.69E+000 9.27E+000 1.62E+001

U-234 U -5.42E+001 1.09E+002 1.30E+002

U-235 U -2.74E-002 9.75E-002 1.33E-001

U-238 U 1.82E+000 1.08E+000 1.79E+000

AM-241 U 1.36E-001 2.73E-001 3.74E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 29

Page 32: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:17 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-008

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-008

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.018E+002 g

Sample Taken On: 5/3/2010 11:44:00 AM

Acquisition Started: 1/28/2011 2:47:10 PM

Live Time: 1000.0 seconds

Real Time: 1000.8 seconds

Dead Time: 0.08 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.68E+001 2.26E+000 7.67E-001

CO-60 U -5.04E-002 1.04E-001 1.19E-001

SB-125 U 1.57E-001 2.10E-001 3.49E-001

CS-137 U -6.13E-002 9.47E-002 1.23E-001

Ra-226 6.51E-001 1.04E-001 1.83E-001

TH-230 U 7.54E+000 2.37E+001 3.13E+001

PA-231 UI 2.16E+000 1.69E+000 2.66E+000

Th-231 U 1.50E+000 8.41E-001 1.38E+000

Th-232 8.32E-001 1.06E-001 1.84E-001

PA-234M U 1.30E+001 7.41E+000 1.64E+001

U-234 U 9.54E+001 9.63E+001 1.39E+002

U-235 U 5.79E-002 9.19E-002 1.37E-001

U-238 U 9.78E-001 1.12E+000 1.76E+000

AM-241 U 3.33E-002 2.76E-001 3.61E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 30

Page 33: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:35 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-009

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-009

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 8.436E+002 g

Sample Taken On: 5/3/2010 11:33:00 AM

Acquisition Started: 1/28/2011 3:06:01 PM

Live Time: 1000.0 seconds

Real Time: 1000.8 seconds

Dead Time: 0.08 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.59E+001 2.32E+000 1.29E+000

CO-60 U 1.78E-002 7.85E-002 1.34E-001

SB-125 U 1.43E-001 1.97E-001 3.33E-001

CS-137 U -1.80E-003 9.15E-002 1.32E-001

Ra-226 7.21E-001 1.25E-001 1.77E-001

TH-230 U 1.26E+001 2.21E+001 3.02E+001

PA-231 U -1.75E+000 2.36E+000 3.00E+000

Th-231 U 1.25E+000 8.29E-001 1.36E+000

Th-232 7.53E-001 1.07E-001 2.11E-001

PA-234M U -2.59E+000 1.03E+001 1.48E+001

U-234 U -5.70E+001 1.04E+002 1.24E+002

U-235 U 5.11E-002 9.50E-002 1.40E-001

U-238 1.16E+000 5.61E-001 1.58E+000

AM-241 U 1.66E-001 2.79E-001 3.88E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 31

Page 34: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:30:53 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-010

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-010

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.025E+002 g

Sample Taken On: 5/3/2010 12:57:00 PM

Acquisition Started: 1/28/2011 3:24:42 PM

Live Time: 1000.0 seconds

Real Time: 1000.9 seconds

Dead Time: 0.09 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.65E+001 2.30E+000 1.26E+000

CO-60 U 9.44E-003 8.88E-002 1.36E-001

SB-125 U 6.08E-002 1.99E-001 3.07E-001

CS-137 U 3.50E-002 6.45E-002 1.09E-001

Ra-226 6.03E-001 1.00E-001 2.04E-001

TH-230 U -4.10E+000 2.15E+001 2.70E+001

PA-231 U -1.95E+000 2.47E+000 2.98E+000

Th-231 U 8.80E-001 8.44E-001 1.34E+000

Th-232 7.35E-001 1.43E-001 1.55E-001

PA-234M U -2.51E+000 7.95E+000 1.10E+001

U-234 U 3.29E+001 8.95E+001 1.23E+002

U-235 U 9.13E-002 8.22E-002 1.30E-001

U-238 UI 7.69E-001 8.27E-001 1.36E+000

AM-241 U 1.79E-001 2.42E-001 3.41E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 32

Page 35: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:31:13 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-010LR

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-010LR

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.025E+002 g

Sample Taken On: 5/3/2010 12:57:00 PM

Acquisition Started: 1/28/2011 5:44:32 PM

Live Time: 1000.0 seconds

Real Time: 1000.7 seconds

Dead Time: 0.07 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.37E+001 2.09E+000 1.26E+000

CO-60 U 5.18E-003 6.87E-002 1.13E-001

SB-125 U -6.02E-002 2.20E-001 3.07E-001

CS-137 U -6.19E-003 8.43E-002 1.23E-001

Ra-226 6.64E-001 1.02E-001 3.25E-001

TH-230 U 1.41E+001 1.85E+001 2.62E+001

PA-231 U -2.56E+000 2.71E+000 3.09E+000

Th-231 U 9.07E-001 8.31E-001 1.32E+000

Th-232 6.89E-001 7.59E-002 1.37E-001

PA-234M U -4.77E-001 9.99E+000 1.45E+001

U-234 U 2.27E+001 1.06E+002 1.37E+002

U-235 U 1.19E-001 7.80E-002 1.28E-001

U-238 U 1.53E+000 1.12E+000 1.81E+000

AM-241 U -1.70E-001 2.96E-001 3.51E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 33

Page 36: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Ra-226 6.03E-01 5.10E-02 12 0.6 - 1.66 6.64E-01 5.20E-02 1.10 -4.8 Yes N/ATh-232 7.35E-01 7.30E-02 10 0.6 - 1.66 6.89E-01 3.87E-02 0.94 3.2 Yes N/AK-40 1.65E+01 1.17E+00 14 0.6 - 1.66 1.37E+01 1.07E+00 0.83 9.3 Yes N/ANote:

FSS Quality Control Accuracy and Precision Comparison

Isotope

Sample ID CE-FSS-41-02-010 Sample ID CE-FSS-41-02-010LRActivity Value (pCi/g) Uncert. Resolution

Agreement Range

Activity Value (pCi/g) Uncert.

Agreement Ratio

(Accuracy)% Deviation (Precision) Acceptable Comments

Resolution = Standard Activity Value/Standard Error

Resolution Agreement Range<4

Checked/Date: HTD 07/11/11

No Comparison 4 - 7 0.4 - 2.08 - 15 0.6 - 1.6616 - 50 0.75 - 1.3351- 200 0.80 - 1.25> 200 0.85 - 1.18

Prepared/Date: GSM 07/11/11

Appendix B Page 34

Page 37: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:31:35 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-011

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-011

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.026E+002 g

Sample Taken On: 5/3/2010 11:40:00 AM

Acquisition Started: 1/28/2011 3:46:51 PM

Live Time: 1000.0 seconds

Real Time: 1000.7 seconds

Dead Time: 0.07 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.48E+001 2.18E+000 1.28E+000

CO-60 U -5.83E-003 9.87E-002 1.41E-001

SB-125 U 4.64E-002 2.17E-001 3.31E-001

CS-137 U 3.98E-002 7.66E-002 1.27E-001

Ra-226 5.75E-001 9.95E-002 1.53E-001

TH-230 U -1.10E+001 2.26E+001 2.70E+001

PA-231 U -2.51E+000 2.82E+000 3.39E+000

Th-231 U 1.63E+000 7.73E-001 1.30E+000

Th-232 7.67E-001 1.02E-001 1.79E-001

PA-234M U -2.61E-001 1.02E+001 1.52E+001

U-234 U -5.96E+000 9.70E+001 1.24E+002

U-235 7.95E-002 8.40E-002 1.36E-001

U-238 U 7.38E-001 1.11E+000 1.73E+000

AM-241 U 1.85E-001 2.76E-001 3.75E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 35

Page 38: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:31:54 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-012

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-012

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.026E+002 g

Sample Taken On: 5/3/2010 11:22:00 AM

Acquisition Started: 1/28/2011 4:13:53 PM

Live Time: 1000.0 seconds

Real Time: 1000.8 seconds

Dead Time: 0.08 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.53E+001 2.20E+000 1.17E+000

CO-60 U -1.09E-002 8.39E-002 1.19E-001

SB-125 U 3.29E-002 1.92E-001 2.94E-001

CS-137 U -4.47E-002 1.00E-001 1.32E-001

Ra-226 7.65E-001 1.50E-001 3.49E-001

TH-230 U 7.40E-001 2.09E+001 2.69E+001

PA-231 U -1.84E+000 2.35E+000 2.98E+000

Th-231 1.27E+000 8.31E-001 1.33E+000

Th-232 7.89E-001 1.19E-001 2.02E-001

PA-234M U -1.26E+000 8.11E+000 1.19E+001

U-234 U -4.02E+000 1.04E+002 1.34E+002

U-235 U 8.37E-002 8.20E-002 1.28E-001

U-238 U 2.10E+000 1.06E+000 1.78E+000

AM-241 U -1.52E-001 3.10E-001 3.71E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 36

Page 39: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:32:14 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-013

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-013

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.311E+002 g

Sample Taken On: 5/3/2010 1:05:00 PM

Acquisition Started: 1/28/2011 4:31:57 PM

Live Time: 1000.0 seconds

Real Time: 1000.8 seconds

Dead Time: 0.08 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.54E+001 2.18E+000 1.15E+000

CO-60 U -1.46E-002 8.95E-002 1.31E-001

SB-125 U 1.20E-001 1.99E-001 3.24E-001

CS-137 U 9.32E-002 8.01E-002 1.43E-001

Ra-226 7.01E-001 9.51E-002 1.39E-001

TH-230 U -7.80E+000 2.35E+001 2.78E+001

PA-231 U -1.71E+000 2.66E+000 2.99E+000

Th-231 1.53E+000 1.22E+000 1.01E+000

Th-232 8.26E-001 7.80E-002 1.23E-001

PA-234M U 6.57E+000 7.82E+000 1.47E+001

U-234 U -1.70E+001 9.97E+001 1.25E+002

U-235 U 4.93E-002 9.21E-002 1.35E-001

U-238 U 1.53E+000 1.17E+000 1.86E+000

AM-241 U 9.66E-002 2.50E-001 3.40E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 37

Page 40: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

CERTIFICATE OF ANALYSIS Report 5/23/2011 12:32:33 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-013S

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-013S

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 7.812E+002 g

Sample Taken On: 5/3/2010 1:10:00 PM

Acquisition Started: 1/28/2011 4:52:14 PM

Live Time: 1000.0 seconds

Real Time: 1000.8 seconds

Dead Time: 0.08 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.85E+001 2.62E+000 1.48E+000

CO-60 U -2.67E-002 9.82E-002 1.38E-001

SB-125 U 3.67E-002 2.32E-001 3.50E-001

CS-137 U -4.24E-002 9.99E-002 1.35E-001

Ra-226 7.68E-001 1.25E-001 2.32E-001

TH-230 U -1.01E+001 2.77E+001 3.37E+001

PA-231 1.80E+000 1.96E+000 3.00E+000

Th-231 1.08E+000 9.71E-001 1.60E+000

Th-232 8.53E-001 1.30E-001 2.51E-001

PA-234M U -2.23E+000 1.16E+001 1.64E+001

U-234 U -1.23E+002 1.25E+002 1.36E+002

U-235 UI 1.13E-001 8.93E-002 1.45E-001

U-238 U 7.58E-001 1.29E+000 1.99E+000

AM-241 U -1.69E-001 3.28E-001 3.94E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 38

Page 41: APPENDIX B SURVEY UNIT CE-FSS-41-02 RESULTS AND DATA ... · 0.0567 Co-60 1.372 U-0.0207 Co-60 2.513 U-0.0109 Co-60 2.596 U 0.00731 Co-60 3.262 U-0.0504 Co-60 1.795 U-0.00583 Co-60

Ra-226 7.01E-01 4.85E-02 14 0.6 - 1.66 7.68E-01 6.38E-02 1.10 -4.6 Yes N/ATh-232 8.26E-01 3.98E-02 21 0.75 - 1.33 8.53E-01 6.63E-02 1.03 -1.6 Yes N/AK-40 1.54E+01 1.11E+00 14 0.6 - 1.66 1.85E+01 1.34E+00 1.20 -9.1 Yes N/ANote:

FSS Quality Control Accuracy and Precision Comparison

Isotope

Sample ID CE-FSS-41-02-013 Sample ID CE-FSS-41-02-013SActivity Value (pCi/g) Uncert. Resolution

Agreement Range

Activity Value (pCi/g) Uncert.

Agreement Ratio

(Accuracy)% Deviation (Precision) Acceptable Comments

Resolution = Standard Activity Value/Standard Error

Resolution Agreement Range<4

16 - 50 0.75 - 1.33

No Comparison 4 - 7 0.4 - 2.08 - 15 0.6 - 1.66

Checked/Date: HTD 07/11/11

51- 200 0.80 - 1.25> 200 0.85 - 1.18

Prepared/Date: GSM 07/11/11

Appendix B Page 39

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CERTIFICATE OF ANALYSIS Report 5/23/2011 12:32:53 PM Page 1

********************************************************************************

***** C E R T I F I C A T E O F A N A L Y S I S *****

********************************************************************************

Site Location: CE Windsor

Sample ID: FSS-41-02-014

Sample Title: CE-FSS-41-02

Sample Description: FSS-41-02-014

Detector Name: 25%HPGE

Nuclide Library Used: C:\GENIE2K\CAMFILES\FUSRAP_R4.NLB

Sample Size: 9.150E+002 g

Sample Taken On: 5/3/2010 12:53:00 PM

Acquisition Started: 1/28/2011 5:19:06 PM

Live Time: 1000.0 seconds

Real Time: 1000.8 seconds

Dead Time: 0.08 %

Efficiency ID: 1316-45_04-30-10

Nuclide Nuclide Activity Nuclide

Name Activity Uncert. MDA

Qualifier (pCi/g ) (pCi/g ) (pCi/g )

K-40 1.87E+001 2.41E+000 1.06E+000

CO-60 U 2.22E-002 8.25E-002 1.39E-001

SB-125 UI -3.55E-002 2.26E-001 3.22E-001

CS-137 U 1.72E-004 8.26E-002 1.21E-001

Ra-226 6.18E-001 1.03E-001 1.79E-001

TH-230 U -2.06E+001 2.36E+001 2.67E+001

PA-231 UI 1.60E+000 1.56E+000 2.54E+000

Th-231 1.11E+000 9.48E-001 1.03E+000

Th-232 9.13E-001 9.92E-002 1.98E-001

PA-234M U 7.27E+000 7.50E+000 1.47E+001

U-234 U 9.14E+000 1.04E+002 1.36E+002

U-235 U 8.68E-002 8.41E-002 1.31E-001

U-238 UI 1.29E+000 1.12E+000 1.55E+000

AM-241 U -1.29E-001 3.06E-001 3.70E-001

Uncertainty reported at 1.9600 sigma

Appendix B Page 40