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ANALYTICAL REPORT Job Number: 660-18295-1 Job Description: Star Center For: S.M. Stoller Corporation 2597 B 3/4 Road Grand Junction, CO 81503 Attention: Mr. Charles Tabor _____________________________________________ Nancy Robertson Project Manager II [email protected] 10/26/2007 Revision: 1 Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements of NELAC unless specified in the case narrative. All questions regarding this test report should be directed to the TestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reported results is available upon request. The results contained in this test report relate only to these samples included herein. TestAmerica Laboratories, Inc. TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634 Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com 10/26/2007 Page 1 of 113

ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

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Page 1: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

ANALYTICAL REPORT

Job Number: 660-18295-1

Job Description: Star Center

For:S.M. Stoller Corporation

2597 B 3/4 RoadGrand Junction, CO 81503

Attention: Mr. Charles Tabor

_____________________________________________

Nancy RobertsonProject Manager II

[email protected]/26/2007Revision: 1

Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements ofNELAC unless specified in the case narrative. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reportedresults is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634

Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com

10/26/2007Page 1 of 113

Page 2: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007Page 2 of 113

Page 3: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007Page 3 of 113

Page 4: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-2 PIN20-M056-N001

1.0 ug/L 8260B4.0cis-1,2-Dichloroethylene1.0 ug/L 8260B7.3Vinyl chloride

660-18295-3 PIN20-M053-N001

1.0 ug/L 8260B11cis-1,2-Dichloroethylene1.0 ug/L 8260B3.4Vinyl chloride

660-18295-4 PIN20-M057-N001

1.0 ug/L 8260B18cis-1,2-Dichloroethylene1.0 ug/L 8260B5.3Vinyl chloride

660-18295-7 PIN20-M18D-N001

1.0 ug/L 8260B13cis-1,2-Dichloroethylene1.0 ug/L 8260B0.74 Jtrans-1,2-Dichloroethylene1.0 ug/L 8260B10Vinyl chloride

660-18295-8 PIN20-M058-N001

1.0 ug/L 8260B3.3Vinyl chloride

660-18295-9 PIN20-M019-N001

1.0 ug/L 8260B0.81 JVinyl chloride

660-18295-10 PIN20-M059-N001

1.0 ug/L 8260B9.5Vinyl chloride

660-18295-11 PIN20-M22D-N001

1.0 ug/L 8260B1.4Vinyl chloride

660-18295-15 PIN15-M03S-N001

Total Recoverable0.20 mg/L 6010B5.1Aluminum0.010 mg/L 6010B0.075Arsenic0.050 mg/L 6010B41Iron0.010 mg/L 6010B0.054Manganese

TestAmerica Tampa

10/26/2007Page 4 of 113

Page 5: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-16 PIN15-M03D-N001

Total Recoverable0.20 mg/L 6010B4.2Aluminum0.050 mg/L 6010B6.5Iron0.010 mg/L 6010B0.0049 BManganese

660-18295-17 PIN15-M16D-N001

Total Recoverable0.20 mg/L 6010B0.47Aluminum0.050 mg/L 6010B3.0Iron0.010 mg/L 6010B0.0042 BManganese

660-18295-18 PIN15-M16S-N001

Total Recoverable0.20 mg/L 6010B1.4Aluminum0.050 mg/L 6010B3.5Iron0.010 mg/L 6010B0.034Manganese

660-18295-19 PIN15-0584-N001

1.0 ug/L 8260B1.8Vinyl chloride

Total Recoverable0.20 mg/L 6010B67Aluminum0.050 mg/L 6010B38Iron0.010 mg/L 6010B0.046Manganese

660-18295-20 PIN15-0537-N001

1.0 ug/L 8260B3.2Benzene1.0 ug/L 8260B120cis-1,2-Dichloroethylene10 ug/L 8260B450 MVinyl chloride

Total Recoverable0.050 mg/L 6010B3.2Iron0.010 mg/L 6010B0.011Manganese

660-18295-21 PIN15-RW16-N001

Total Recoverable0.050 mg/L 6010B3.9Iron0.010 mg/L 6010B0.017Manganese

TestAmerica Tampa

10/26/2007Page 5 of 113

Page 6: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-22 PIN15-M32S-N001

Total Recoverable0.20 mg/L 6010B0.60Aluminum0.010 mg/L 6010B0.018Arsenic0.050 mg/L 6010B3.6Iron0.010 mg/L 6010B0.082Manganese

660-18295-23 PIN15-M32D-N001

Total Recoverable0.20 mg/L 6010B0.23Aluminum0.050 mg/L 6010B5.3Iron0.010 mg/L 6010B0.0096 BManganese

660-18295-24 PIN15-0592-N001

1.0 ug/L 8260B29Benzene1.0 ug/L 8260B1.1Ethylbenzene2.0 ug/L 8260B2.0m,p-Xylene1.0 ug/L 8260B0.94 JToluene

Total Recoverable0.20 mg/L 6010B27Aluminum0.050 mg/L 6010B17Iron0.010 mg/L 6010B0.036Manganese

660-18295-25 PIN15-0515-N001

Total Recoverable0.20 mg/L 6010B0.081 BAluminum0.050 mg/L 6010B1.0Iron0.010 mg/L 6010B0.010Manganese

660-18295-26 PIN15-0514-N001

Total Recoverable0.20 mg/L 6010B2.3Aluminum0.050 mg/L 6010B1.7Iron0.010 mg/L 6010B0.0097 BManganese

TestAmerica Tampa

10/26/2007Page 6 of 113

Page 7: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-27 PIN15-0516-N001

Total Recoverable0.20 mg/L 6010B0.14 BAluminum0.050 mg/L 6010B6.7Iron0.010 mg/L 6010B0.029Manganese

660-18295-28 PIN15-0535-N001

Total Recoverable0.20 mg/L 6010B5.0Aluminum0.050 mg/L 6010B1.8Iron0.010 mg/L 6010B0.0099 BManganese

660-18295-29 PIN15-0530-N001

Total Recoverable0.20 mg/L 6010B1.1Aluminum0.050 mg/L 6010B2.3Iron0.010 mg/L 6010B0.034Manganese

660-18295-30 PIN15-M27D-N001

Total Recoverable0.20 mg/L 6010B0.69Aluminum0.050 mg/L 6010B0.90Iron0.010 mg/L 6010B0.0098 BManganese

660-18295-31 PIN15-M27S-N001

Total Recoverable0.050 mg/L 6010B1.9Iron0.010 mg/L 6010B0.11Manganese

TestAmerica Tampa

10/26/2007Page 7 of 113

Page 8: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-32 PIN15-0585-N001

1.0 ug/L 8260B0.86 JBenzene1.0 ug/L 8260B140cis-1,2-Dichloroethylene1.0 ug/L 8260B1.21,1-Dichlorethylene1.0 ug/L 8260B9.0Toluene1.0 ug/L 8260B0.92 Jtrans-1,2-Dichloroethylene2.0 ug/L 8260B180Trichloroethylene1.0 ug/L 8260B28Vinyl chloride

Total Recoverable0.20 mg/L 6010B10Aluminum0.050 mg/L 6010B6.6Iron0.010 mg/L 6010B0.016Manganese

660-18295-33 PIN15-0586-N001

5.0 ug/L 8260B3.0 JBenzene20 ug/L 8260B1400cis-1,2-Dichloroethylene5.0 ug/L 8260B6.91,1-Dichlorethylene5.0 ug/L 8260B28Toluene5.0 ug/L 8260B4.8 Jtrans-1,2-Dichloroethylene5.0 ug/L 8260B430Trichloroethylene5.0 ug/L 8260B490Vinyl chloride

Total Recoverable0.20 mg/L 6010B18Aluminum0.050 mg/L 6010B16Iron0.010 mg/L 6010B0.049Manganese

660-18295-34 PIN24-0508

5.0 ug/L 8260B3.5 JBenzene20 ug/L 8260B1300cis-1,2-Dichloroethylene5.0 ug/L 8260B6.01,1-Dichlorethylene5.0 ug/L 8260B31Toluene5.0 ug/L 8260B4.8 Jtrans-1,2-Dichloroethylene5.0 ug/L 8260B450Trichloroethylene5.0 ug/L 8260B500Vinyl chloride

Total Recoverable0.20 mg/L 6010B21Aluminum0.050 mg/L 6010B18Iron0.010 mg/L 6010B0.052Manganese

TestAmerica Tampa

10/26/2007Page 8 of 113

Page 9: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-35 PIN15-0588-N001

1.0 ug/L 8260B1.8Benzene2.0 ug/L 8260B170cis-1,2-Dichloroethylene1.0 ug/L 8260B1.11,1-Dichlorethylene1.0 ug/L 8260B9.0Toluene1.0 ug/L 8260B1.1trans-1,2-Dichloroethylene1.0 ug/L 8260B1.1Trichloroethylene1.0 ug/L 8260B8.8Vinyl chloride

Total Recoverable0.20 mg/L 6010B0.84Aluminum0.050 mg/L 6010B3.3Iron0.010 mg/L 6010B0.25Manganese

660-18295-36 PIN20-M061-N001

20 ug/L 8260B1200cis-1,2-Dichloroethylene5.0 ug/L 8260B9.11,1-Dichlorethylene5.0 ug/L 8260B68trans-1,2-Dichloroethylene5.0 ug/L 8260B220Trichloroethylene5.0 ug/L 8260B330Vinyl chloride

660-18295-37 PIN20-M060-N001

2.0 ug/L 8260B28cis-1,2-Dichloroethylene2.0 ug/L 8260B20trans-1,2-Dichloroethylene20 ug/L 8260B2000 MVinyl chloride

660-18295-38 PIN24-0502

2.0 ug/L 8260B100cis-1,2-Dichloroethylene2.0 ug/L 8260B0.97 J1,1-Dichlorethylene2.0 ug/L 8260B45trans-1,2-Dichloroethylene20 ug/L 8260B2100Vinyl chloride

660-18295-39 PIN20-M049-N001

1.0 ug/L 8260B3.7cis-1,2-Dichloroethylene1.0 ug/L 8260B2.3Vinyl chloride

660-18295-43 PIN09-0500-N001

Total Recoverable0.010 mg/L 6010B0.0077 BArsenic

TestAmerica Tampa

10/26/2007Page 9 of 113

Page 10: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-46 PIN12-S29C-N001

1.0 ug/L 8260B2.01,1-Dichloroethane1.0 ug/L 8260B4.8Vinyl chloride

660-18295-47 PIN12-S30B-N001

1.0 ug/L 8260B1.6Benzene50 ug/L 8260B6000cis-1,2-Dichloroethylene1.0 ug/L 8260B1201,1-Dichlorethylene1.0 ug/L 8260B9.11,1-Dichloroethane1.0 ug/L 8260B0.58 JToluene25 ug/L 8260B330trans-1,2-Dichloroethylene25 ug/L 8260B350Trichloroethylene25 ug/L 8260B2100Vinyl chloride

660-18295-48 PIN12-S32B-N001

1.0 ug/L 8260B2.61,1-Dichloroethane

Total Recoverable0.010 mg/L 6010B0.011Arsenic

660-18295-49 PIN12-S31B-N001

Total Recoverable0.010 mg/L 6010B0.018Arsenic

660-18295-50 PIN12-S37B-N001

1.0 ug/L 8260B3.7cis-1,2-Dichloroethylene5.0 ug/L 8260B9.5Dichlorodifluoromethane1.0 ug/L 8260B3.4Vinyl chloride

660-18295-51 PIN12-S33C-N001

13 ug/L 8260B1700cis-1,2-Dichloroethylene2.0 ug/L 8260B1101,1-Dichlorethylene2.0 ug/L 8260B29trans-1,2-Dichloroethylene2.0 ug/L 8260B43Trichloroethylene13 ug/L 8260B1100Vinyl chloride

Total Recoverable0.010 mg/L 6010B0.0048 BArsenic

TestAmerica Tampa

10/26/2007Page 10 of 113

Page 11: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18295-52 PIN12-S35B-N001

200 ug/L 8260B14000cis-1,2-Dichloroethylene50 ug/L 8260B901,1-Dichlorethylene50 ug/L 8260B3300trans-1,2-Dichloroethylene50 ug/L 8260B7500Trichloroethylene200 ug/L 8260B9300Vinyl chloride

Total Recoverable0.010 mg/L 6010B0.017Arsenic

TestAmerica Tampa

10/26/2007Page 11 of 113

Page 12: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

METHOD SUMMARY

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Preparation MethodMethodLab LocationDescription

Matrix: Water

SW846 8260BVolatile Organic Compounds by GC/MS TAL TAM

SW846 5030BTAL TAMPurge-and-Trap

SW846 6010BInductively Coupled Plasma - Atomic Emission Spectrometry TAL TAM

SW846 3005ATAL TAMAcid Digestion of Waters for Total Recoverable or

Lab References:

TAL TAM = TestAmerica Tampa

Method References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa

10/26/2007Page 12 of 113

Page 13: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

METHOD / ANALYST SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Method Analyst Analyst ID

Perez, Julian JPSW846 8260B

Fox, Greg GFSW846 6010B

TestAmerica Tampa

10/26/2007Page 13 of 113

Page 14: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

SAMPLE SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

09/12/2007 0720 09/14/2007 0900PIN24-0800660-18295-1 Water

09/12/2007 0940 09/14/2007 0900PIN20-M056-N001660-18295-2 Water

09/12/2007 1000 09/14/2007 0900PIN20-M053-N001660-18295-3 Water

09/12/2007 1020 09/14/2007 0900PIN20-M057-N001660-18295-4 Water

09/12/2007 1055 09/14/2007 0900PIN20-M005-N001660-18295-5 Water

09/12/2007 1100 09/14/2007 0900PIN20-M003-N001660-18295-6 Water

09/12/2007 1340 09/14/2007 0900PIN20-M18D-N001660-18295-7 Water

09/12/2007 1435 09/14/2007 0900PIN20-M058-N001660-18295-8 Water

09/12/2007 1510 09/14/2007 0900PIN20-M019-N001660-18295-9 Water

09/12/2007 1533 09/14/2007 0900PIN20-M059-N001660-18295-10 Water

09/13/2007 0845 09/14/2007 0900PIN20-M22D-N001660-18295-11 Water

09/13/2007 0917 09/14/2007 0900PIN20-M007-N001660-18295-12 Water

09/13/2007 0948 09/14/2007 0900PIN20-M028-N001660-18295-13 Water

09/12/2007 0840 09/14/2007 0900PIN24-0700660-18295-14 Water

09/12/2007 1002 09/14/2007 0900PIN15-M03S-N001660-18295-15 Water

09/12/2007 1031 09/14/2007 0900PIN15-M03D-N001660-18295-16 Water

09/12/2007 1059 09/14/2007 0900PIN15-M16D-N001660-18295-17 Water

09/12/2007 1121 09/14/2007 0900PIN15-M16S-N001660-18295-18 Water

09/12/2007 1314 09/14/2007 0900PIN15-0584-N001660-18295-19 Water

09/12/2007 1342 09/14/2007 0900PIN15-0537-N001660-18295-20 Water

09/12/2007 1409 09/14/2007 0900PIN15-RW16-N001660-18295-21 Water

09/12/2007 1441 09/14/2007 0900PIN15-M32S-N001660-18295-22 Water

09/12/2007 1506 09/14/2007 0900PIN15-M32D-N001660-18295-23 Water

09/13/2007 0845 09/14/2007 0900PIN15-0592-N001660-18295-24 Water

09/13/2007 0914 09/14/2007 0900PIN15-0515-N001660-18295-25 Water

09/13/2007 0933 09/14/2007 0900PIN15-0514-N001660-18295-26 Water

09/13/2007 0959 09/14/2007 0900PIN15-0516-N001660-18295-27 Water

09/13/2007 1025 09/14/2007 0900PIN15-0535-N001660-18295-28 Water

09/13/2007 1049 09/14/2007 0900PIN15-0530-N001660-18295-29 Water

09/13/2007 1121 09/14/2007 0900PIN15-M27D-N001660-18295-30 Water

09/13/2007 1141 09/14/2007 0900PIN15-M27S-N001660-18295-31 Water

09/13/2007 1350 09/14/2007 0900PIN15-0585-N001660-18295-32 Water

09/13/2007 1428 09/14/2007 0900PIN15-0586-N001660-18295-33 Water

09/13/2007 1444 09/14/2007 0900PIN24-0508660-18295-34 Water

09/13/2007 1525 09/14/2007 0900PIN15-0588-N001660-18295-35 Water

09/13/2007 1037 09/14/2007 0900PIN20-M061-N001660-18295-36 Water

09/13/2007 1305 09/14/2007 0900PIN20-M060-N001660-18295-37 Water

09/13/2007 1232 09/14/2007 0900PIN24-0502660-18295-38 Water

09/13/2007 1406 09/14/2007 0900PIN20-M049-N001660-18295-39 Water

09/13/2007 1458 09/14/2007 0900PIN20-MWL5-N001660-18295-40 Water

09/12/2007 1100 09/14/2007 0900PIN24-0600660-18295-41 Water

09/12/2007 1350 09/14/2007 0900PIN10-0500-N001660-18295-42 Water

09/12/2007 1416 09/14/2007 0900PIN09-0500-N001660-18295-43 Water

09/12/2007 1442 09/14/2007 0900PIN12-0521-N001660-18295-44 Water

09/13/2007 0851 09/14/2007 0900PIN12-S36B-N001660-18295-45 Water

09/13/2007 0919 09/14/2007 0900PIN12-S29C-N001660-18295-46 Water

TestAmerica Tampa

10/26/2007Page 14 of 113

Page 15: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

SAMPLE SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

09/13/2007 0945 09/14/2007 0900PIN12-S30B-N001660-18295-47 Water

09/13/2007 1015 09/14/2007 0900PIN12-S32B-N001660-18295-48 Water

09/13/2007 1040 09/14/2007 0900PIN12-S31B-N001660-18295-49 Water

09/13/2007 1329 09/14/2007 0900PIN12-S37B-N001660-18295-50 Water

09/13/2007 1404 09/14/2007 0900PIN12-S33C-N001660-18295-51 Water

09/13/2007 1440 09/14/2007 0900PIN12-S35B-N001660-18295-52 Water

TestAmerica Tampa

10/26/2007Page 15 of 113

Page 16: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0800

09/12/2007 0720

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-1

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/20/2007 2328

09/20/2007 2328

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2020.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

107 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 16 of 113

Page 17: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M056-N001

09/12/2007 0940

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-2

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/20/2007 2349

09/20/2007 2349

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2021.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform4.0 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane7.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

100 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 17 of 113

Page 18: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M053-N001

09/12/2007 1000

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-3

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0010

09/21/2007 0010

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2022.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform11 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.4 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

109 74 - 1264-Bromofluorobenzene116 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 18 of 113

Page 19: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M057-N001

09/12/2007 1020

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-4

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0030

09/21/2007 0030

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2023.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform18 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane5.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

110 74 - 1264-Bromofluorobenzene119 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 19 of 113

Page 20: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M005-N001

09/12/2007 1055

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-5

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0051

09/21/2007 0051

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2024.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

110 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 20 of 113

Page 21: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M003-N001

09/12/2007 1100

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-6

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0112

09/21/2007 0112

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2025.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

96 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 21 of 113

Page 22: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M18D-N001

09/12/2007 1340

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-7

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0132

09/21/2007 0132

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2026.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform13 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.74 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane10 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

114 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 22 of 113

Page 23: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M058-N001

09/12/2007 1435

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-8

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0153

09/21/2007 0153

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2027.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

98 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 23 of 113

Page 24: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M019-N001

09/12/2007 1510

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-9

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0214

09/21/2007 0214

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2028.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.81 J 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

100 74 - 1264-Bromofluorobenzene108 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 24 of 113

Page 25: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M059-N001

09/12/2007 1533

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-10

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0234

09/21/2007 0234

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2029.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane9.5 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

105 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 25 of 113

Page 26: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M22D-N001

09/13/2007 0845

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-11

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0255

09/21/2007 0255

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2030.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.4 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

108 74 - 1264-Bromofluorobenzene116 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 26 of 113

Page 27: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M007-N001

09/13/2007 0917

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-12

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0316

09/21/2007 0316

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2031.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

110 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 27 of 113

Page 28: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M028-N001

09/13/2007 0948

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-13

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0336

09/21/2007 0336

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2032.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

109 74 - 1264-Bromofluorobenzene116 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 28 of 113

Page 29: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0700

09/12/2007 0840

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-14

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0357

09/21/2007 0357

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2033.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

100 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 29 of 113

Page 30: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0584-N001

09/12/2007 1314

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-19

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0418

09/21/2007 0418

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2034.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.8 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

98 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 30 of 113

Page 31: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0537-N001

09/12/2007 1342

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-20

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0438

09/21/2007 0438

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2035.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

3.2 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform120 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

110 74 - 1264-Bromofluorobenzene119 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 31 of 113

Page 32: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0537-N001

09/12/2007 1342

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-20

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0101

09/24/2007 0101

10

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2322.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

450 M 105.0Vinyl chloride

TestAmerica Tampa 10/26/2007Page 32 of 113

Page 33: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0592-N001

09/13/2007 0845

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-24

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/21/2007 0459

09/21/2007 0459

1.0

8260B Analysis Batch: 660-50786

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2036.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

29 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane1.1 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether2.0 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.94 J 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

105 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 33 of 113

Page 34: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0585-N001

09/13/2007 1350

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-32

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0020

09/24/2007 0020

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2320.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.86 J 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform140 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.2 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene9.0 1.00.51Toluene0.92 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane2.5 U 5.02.5Trichlorofluoromethane28 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

120 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 34 of 113

Page 35: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0585-N001

09/13/2007 1350

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-32

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 0049

09/25/2007 0049

2.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2427.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

180 2.01.0Trichloroethylene

TestAmerica Tampa 10/26/2007Page 35 of 113

Page 36: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0586-N001

09/13/2007 1428

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-33

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 0130

09/25/2007 0130

5.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2429.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

3.0 J 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.8 U 254.82-Chloroethyl vinyl ether4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane6.9 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene28 5.02.6Toluene4.8 J 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane430 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane490 5.02.5Vinyl chloride5.0 U 205.0Methyl chloride

Surrogate %Rec Acceptance Limits

101 74 - 1264-Bromofluorobenzene90 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 36 of 113

Page 37: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0586-N001

09/13/2007 1428

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-33

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0122

09/24/2007 0122

20

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2323.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

1400 2013cis-1,2-Dichloroethylene

TestAmerica Tampa 10/26/2007Page 37 of 113

Page 38: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0508

09/13/2007 1444

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-34

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 0151

09/25/2007 0151

5.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2430.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

3.5 J 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.8 U 254.82-Chloroethyl vinyl ether4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane6.0 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene31 5.02.6Toluene4.8 J 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane450 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane500 5.02.5Vinyl chloride5.0 U 205.0Methyl chloride

Surrogate %Rec Acceptance Limits

108 74 - 1264-Bromofluorobenzene97 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 38 of 113

Page 39: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0508

09/13/2007 1444

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-34

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0143

09/24/2007 0143

20

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2324.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

1300 2013cis-1,2-Dichloroethylene

TestAmerica Tampa 10/26/2007Page 39 of 113

Page 40: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0588-N001

09/13/2007 1525

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-35

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0040

09/24/2007 0040

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2321.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.8 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.1 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene9.0 1.00.51Toluene1.1 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane1.1 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane8.8 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

113 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 40 of 113

Page 41: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0588-N001

09/13/2007 1525

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-35

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 0109

09/25/2007 0109

2.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2428.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

170 2.01.3cis-1,2-Dichloroethylene

TestAmerica Tampa 10/26/2007Page 41 of 113

Page 42: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M061-N001

09/13/2007 1037

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-36

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 0211

09/25/2007 0211

5.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2431.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

2.5 U 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.8 U 254.82-Chloroethyl vinyl ether4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane9.1 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene2.6 U 5.02.6Toluene68 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane220 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane330 5.02.5Vinyl chloride5.0 U 205.0Methyl chloride

Surrogate %Rec Acceptance Limits

106 74 - 1264-Bromofluorobenzene92 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 42 of 113

Page 43: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M061-N001

09/13/2007 1037

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-36

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0203

09/24/2007 0203

20

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2325.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

1200 2013cis-1,2-Dichloroethylene

TestAmerica Tampa 10/26/2007Page 43 of 113

Page 44: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M060-N001

09/13/2007 1305

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-37

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 1857

09/25/2007 1857

2.0

8260B Analysis Batch: 660-50904

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2529.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.0 U 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.9 U 101.92-Chloroethyl vinyl ether1.8 U 2.01.8Chloroform28 2.01.3cis-1,2-Dichloroethylene0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane0.90 U 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene1.0 U 2.01.0Toluene20 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane1.0 U 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane2.0 U 8.02.0Methyl chloride

Surrogate %Rec Acceptance Limits

113 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 44 of 113

Page 45: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M060-N001

09/13/2007 1305

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-37

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0224

09/24/2007 0224

20

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2326.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

2000 M 2010Vinyl chloride

TestAmerica Tampa 10/26/2007Page 45 of 113

Page 46: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0502

09/13/2007 1232

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-38

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 1918

09/25/2007 1918

2.0

8260B Analysis Batch: 660-50904

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2530.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.0 U 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.9 U 101.92-Chloroethyl vinyl ether1.8 U 2.01.8Chloroform100 2.01.3cis-1,2-Dichloroethylene0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane0.97 J 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene1.0 U 2.01.0Toluene45 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane1.0 U 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane2.0 U 8.02.0Methyl chloride

Surrogate %Rec Acceptance Limits

123 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 46 of 113

Page 47: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0502

09/13/2007 1232

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-38

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0245

09/24/2007 0245

20

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2327.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

2100 2010Vinyl chloride

TestAmerica Tampa 10/26/2007Page 47 of 113

Page 48: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M049-N001

09/13/2007 1406

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-39

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0305

09/24/2007 0305

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2328.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform3.7 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane2.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

97 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 48 of 113

Page 49: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL5-N001

09/13/2007 1458

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-40

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0326

09/24/2007 0326

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2329.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

105 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 49 of 113

Page 50: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0600

09/12/2007 1100

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-41

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0347

09/24/2007 0347

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2330.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

118 74 - 1264-Bromofluorobenzene112 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 50 of 113

Page 51: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN10-0500-N001

09/12/2007 1350

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-42

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0407

09/24/2007 0407

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2331.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

118 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 51 of 113

Page 52: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN09-0500-N001

09/12/2007 1416

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-43

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0428

09/24/2007 0428

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2332.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

102 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 52 of 113

Page 53: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0521-N001

09/12/2007 1442

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-44

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0510

09/24/2007 0510

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2334.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

117 74 - 1264-Bromofluorobenzene110 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 53 of 113

Page 54: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S36B-N001

09/13/2007 0851

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-45

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 1959

09/25/2007 1959

1.0

8260B Analysis Batch: 660-50904

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2532.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

107 74 - 1264-Bromofluorobenzene99 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 54 of 113

Page 55: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S29C-N001

09/13/2007 0919

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-46

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 0449

09/24/2007 0449

1.0

8260B Analysis Batch: 660-50896

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2333.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.0 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane4.8 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

122 74 - 1264-Bromofluorobenzene112 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 55 of 113

Page 56: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S30B-N001

09/13/2007 0945

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-47

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 1938

09/24/2007 1938

1.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2412.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.6 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane120 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane9.1 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.58 J 1.00.51Toluene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane2.5 U 5.02.5Trichlorofluoromethane1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

120 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 56 of 113

Page 57: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S30B-N001

09/13/2007 0945

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-47

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 1707

09/25/2007 1707

25

8260B Analysis Batch: 660-50904

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2524.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

330 2511trans-1,2-Dichloroethylene350 2513Trichloroethylene2100 2513Vinyl chloride

TestAmerica Tampa 10/26/2007Page 57 of 113

Page 58: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S30B-N001

09/13/2007 0945

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-47

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 2102

09/25/2007 2102

50

8260B Analysis Batch: 660-50904

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2535.D

5 mL

5 mL

5030B

Run Type: DL2

Analyte Result (ug/L) PQLMDLQualifier

6000 5033cis-1,2-Dichloroethylene

TestAmerica Tampa 10/26/2007Page 58 of 113

Page 59: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S32B-N001

09/13/2007 1015

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-48

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 1958

09/24/2007 1958

1.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2413.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.6 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

115 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 59 of 113

Page 60: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S31B-N001

09/13/2007 1040

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-49

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 2019

09/24/2007 2019

1.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2414.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

118 74 - 1264-Bromofluorobenzene111 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 60 of 113

Page 61: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S37B-N001

09/13/2007 1329

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-50

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 2040

09/24/2007 2040

1.0

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2415.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform3.7 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene9.5 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.4 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate %Rec Acceptance Limits

115 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 61 of 113

Page 62: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S33C-N001

09/13/2007 1404

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-51

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/25/2007 1735

09/25/2007 1735

2.0

8260B Analysis Batch: 660-50904

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2525.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.0 U 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.9 U 101.92-Chloroethyl vinyl ether1.8 U 2.01.8Chloroform0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane110 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene1.0 U 2.01.0Toluene29 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane43 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane2.0 U 8.02.0Methyl chloride

Surrogate %Rec Acceptance Limits

121 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 62 of 113

Page 63: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S33C-N001

09/13/2007 1404

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-51

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 2101

09/24/2007 2101

12.5

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2416.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

1700 138.1cis-1,2-Dichloroethylene1100 136.3Vinyl chloride

TestAmerica Tampa 10/26/2007Page 63 of 113

Page 64: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S35B-N001

09/13/2007 1440

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-52

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 2142

09/24/2007 2142

50

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2418.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

25 U 5025Benzene18 U 5018Bromodichloromethane29 U 5029Bromoform21 U 5021Carbon tetrachloride32 U 5032Chlorobenzene130 U 250130Chloroethane48 U 250482-Chloroethyl vinyl ether45 U 5045Chloroform7.0 U 507.0cis-1,3-Dichloropropene17 U 5017Dibromochloromethane90 50231,1-Dichlorethylene130 U 250130Dichlorodifluoromethane26 U 50261,1-Dichloroethane29 U 50291,2-Dichloroethane26 U 50261,2-Dichloropropane22 U 5022Ethylbenzene32 U 5032m-Dichlorobenzene130 U 250130Methyl bromide200 U 250200Methylene Chloride22 U 5022Methyl tert-butyl ether30 U 10030m,p-Xylene22 U 5022o-Dichlorobenzene25 U 5025o-Xylene26 U 5026p-Dichlorobenzene7.5 U 507.51,1,2,2-Tetrachloroethane25 U 5025Tetrachloroethylene26 U 5026Toluene3300 5022trans-1,2-Dichloroethylene7.0 U 507.0trans-1,3-Dichloropropene23 U 50231,1,1-Trichloroethane24 U 50241,1,2-Trichloroethane7500 5025Trichloroethylene130 U 250130Trichlorofluoromethane50 U 20050Methyl chloride

Surrogate %Rec Acceptance Limits

93 74 - 1264-Bromofluorobenzene84 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/26/2007Page 64 of 113

Page 65: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S35B-N001

09/13/2007 1440

09/14/2007 0900Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18295-52

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/24/2007 2121

09/24/2007 2121

200

8260B Analysis Batch: 660-50888

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2417.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

14000 200130cis-1,2-Dichloroethylene9300 200100Vinyl chloride

TestAmerica Tampa 10/26/2007Page 65 of 113

Page 66: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M03S-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1002

09/14/2007 0900

660-18295-15

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1401

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

5.1 0.200.070Aluminum0.075 0.0100.0048Arsenic41 0.0500.022Iron0.054 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 66 of 113

Page 67: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M03D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1031

09/14/2007 0900

660-18295-16

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1407

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

4.2 0.200.070Aluminum6.5 0.0500.022Iron0.0049 B 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 67 of 113

Page 68: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M16D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1059

09/14/2007 0900

660-18295-17

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1413

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

0.47 0.200.070Aluminum3.0 0.0500.022Iron0.0042 B 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 68 of 113

Page 69: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M16S-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1121

09/14/2007 0900

660-18295-18

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1419

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

1.4 0.200.070Aluminum3.5 0.0500.022Iron0.034 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 69 of 113

Page 70: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0584-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1314

09/14/2007 0900

660-18295-19

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1425

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

67 0.200.070Aluminum38 0.0500.022Iron0.046 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 70 of 113

Page 71: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0537-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1342

09/14/2007 0900

660-18295-20

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1430

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

0.070 U 0.200.070Aluminum3.2 0.0500.022Iron0.011 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 71 of 113

Page 72: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-RW16-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1409

09/14/2007 0900

660-18295-21

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/17/2007 1327

09/15/2007 1329

TJA ICP TRACE

7I17A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50402

3005A Prep Batch: 660-50331

0.070 U 0.200.070Aluminum3.9 0.0500.022Iron0.017 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 72 of 113

Page 73: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M32S-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1441

09/14/2007 0900

660-18295-22

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1523

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.60 0.200.070Aluminum0.018 0.0100.0048Arsenic3.6 0.0500.022Iron0.082 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 73 of 113

Page 74: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M32D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1506

09/14/2007 0900

660-18295-23

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1528

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.23 0.200.070Aluminum5.3 0.0500.022Iron0.0096 B 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 74 of 113

Page 75: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0592-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 0845

09/14/2007 0900

660-18295-24

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1532

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

27 0.200.070Aluminum17 0.0500.022Iron0.036 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 75 of 113

Page 76: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0515-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 0914

09/14/2007 0900

660-18295-25

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1335

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.081 B 0.200.070Aluminum1.0 0.0500.022Iron0.010 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 76 of 113

Page 77: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0514-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 0933

09/14/2007 0900

660-18295-26

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1349

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

2.3 0.200.070Aluminum1.7 0.0500.022Iron0.0097 B 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 77 of 113

Page 78: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0516-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 0959

09/14/2007 0900

660-18295-27

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1354

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.14 B 0.200.070Aluminum6.7 0.0500.022Iron0.029 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 78 of 113

Page 79: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0535-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1025

09/14/2007 0900

660-18295-28

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1408

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

5.0 0.200.070Aluminum1.8 0.0500.022Iron0.0099 B 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 79 of 113

Page 80: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0530-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1049

09/14/2007 0900

660-18295-29

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1412

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

1.1 0.200.070Aluminum2.3 0.0500.022Iron0.034 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 80 of 113

Page 81: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M27D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1121

09/14/2007 0900

660-18295-30

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1417

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.69 0.200.070Aluminum0.90 0.0500.022Iron0.0098 B 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 81 of 113

Page 82: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-M27S-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1141

09/14/2007 0900

660-18295-31

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1422

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.070 U 0.200.070Aluminum1.9 0.0500.022Iron0.11 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 82 of 113

Page 83: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0585-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1350

09/14/2007 0900

660-18295-32

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1427

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

10 0.200.070Aluminum6.6 0.0500.022Iron0.016 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 83 of 113

Page 84: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0586-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1428

09/14/2007 0900

660-18295-33

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1431

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

18 0.200.070Aluminum16 0.0500.022Iron0.049 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 84 of 113

Page 85: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN24-0508

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1444

09/14/2007 0900

660-18295-34

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1436

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

21 0.200.070Aluminum18 0.0500.022Iron0.052 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 85 of 113

Page 86: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN15-0588-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1525

09/14/2007 0900

660-18295-35

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1441

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.84 0.200.070Aluminum3.3 0.0500.022Iron0.25 0.0100.0014Manganese

TestAmerica Tampa 10/26/2007Page 86 of 113

Page 87: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN10-0500-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1350

09/14/2007 0900

660-18295-42

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1445

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.0048 U 0.0100.0048Arsenic

TestAmerica Tampa 10/26/2007Page 87 of 113

Page 88: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN09-0500-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/12/2007 1416

09/14/2007 0900

660-18295-43

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1450

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.0077 B 0.0100.0048Arsenic

TestAmerica Tampa 10/26/2007Page 88 of 113

Page 89: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN12-S32B-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1015

09/14/2007 0900

660-18295-48

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1504

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.011 0.0100.0048Arsenic

TestAmerica Tampa 10/26/2007Page 89 of 113

Page 90: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN12-S31B-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1040

09/14/2007 0900

660-18295-49

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1509

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.018 0.0100.0048Arsenic

TestAmerica Tampa 10/26/2007Page 90 of 113

Page 91: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN12-S33C-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1404

09/14/2007 0900

660-18295-51

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1514

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.0048 B 0.0100.0048Arsenic

TestAmerica Tampa 10/26/2007Page 91 of 113

Page 92: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Client Sample ID: PIN12-S35B-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/13/2007 1440

09/14/2007 0900

660-18295-52

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/19/2007 1518

09/15/2007 1336

TJA ICP

7I19B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50544

3005A Prep Batch: 660-50332

0.017 0.0100.0048Arsenic

TestAmerica Tampa 10/26/2007Page 92 of 113

Page 93: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

DATA REPORTING QUALIFIERS

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Lab Section Qualifier Description

GC/MS VOA

Analyzed for but not detected.U

Indicates an estimated value.J

Manual integrated compound.M

Metals

Indicates analyzed for but not detected.U

Value less than contract required detection limit but greater than or equal to the Method Detection Limit

B

TestAmerica Tampa

10/26/2007Page 93 of 113

Page 94: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/20/2007 2145

Method Blank - Batch: 660-50786

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50786

Prep Batch: N/A

09/20/2007 2145

2HI2015.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-50786/3

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 106 74 - 126Toluene-d8 (Surr) 114 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 94 of 113

Page 95: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/20/2007 2043

09/20/2007 2104

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50786

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/20/2007 2043

Prep Batch: N/A

Analysis Batch: 660-50786

2HI2012.D

5 mL

5 mL

2HI2013.D

5 mL

5 mL

ug/L

09/20/2007 2104

Analysis Batch: 660-50786

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-50786/1

LCSD 660-50786/2

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

113119 62 - 135 6 37Benzene

107110 72 - 127 3 22Chlorobenzene

134142 46 - 147 5 301,1-Dichlorethylene

109113 68 - 131 4 33Toluene

111117 56 - 143 6 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 95 of 113

Page 96: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/25/2007 0334

09/25/2007 0355

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50786

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-50786

Analysis Batch: 660-50786

09/25/2007 0334

09/25/2007 0355

Prep Batch: N/A

Prep Batch: N/A

2HI2435.D

5 mL

5 mL

2HI2436.D

5 mL

5 mL

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

660-18295-12

660-18295-12

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

77 89 62 - 135 15 37Benzene

104 117 72 - 127 11 22Chlorobenzene

89 103 46 - 147 14 301,1-Dichlorethylene

91 106 68 - 131 16 33Toluene

75 87 56 - 143 15 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 96 of 113

Page 97: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/24/2007 1815

Method Blank - Batch: 660-50888

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50888

Prep Batch: N/A

09/24/2007 1815

2HI2408.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-50888/3

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 106 74 - 126Toluene-d8 (Surr) 101 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 97 of 113

Page 98: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/24/2007 1713

09/24/2007 1733

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50888

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/24/2007 1713

Prep Batch: N/A

Analysis Batch: 660-50888

2HI2405.D

5 mL

5 mL

2HI2406.D

5 mL

5 mL

ug/L

09/24/2007 1733

Analysis Batch: 660-50888

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-50888/1

LCSD 660-50888/2

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

9896 62 - 135 2 37Benzene

116111 72 - 127 5 22Chlorobenzene

118116 46 - 147 2 301,1-Dichlorethylene

106105 68 - 131 1 33Toluene

9593 56 - 143 3 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 98 of 113

Page 99: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/23/2007 2236

Method Blank - Batch: 660-50896

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50896

Prep Batch: N/A

09/23/2007 2236

2HI2315.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-50896/4

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 104 74 - 126Toluene-d8 (Surr) 99 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 99 of 113

Page 100: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/23/2007 2134

09/23/2007 2154

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50896

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/23/2007 2134

Prep Batch: N/A

Analysis Batch: 660-50896

2HI2312.D

5 mL

5 mL

2HI2313.D

5 mL

5 mL

ug/L

09/23/2007 2154

Analysis Batch: 660-50896

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-50896/2

LCSD 660-50896/3

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

111115 62 - 135 3 37Benzene

106114 72 - 127 7 22Chlorobenzene

120127 46 - 147 5 301,1-Dichlorethylene

107109 68 - 131 2 33Toluene

102105 56 - 143 4 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 100 of 113

Page 101: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/25/2007 0253

09/25/2007 0314

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50896

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-50896

Analysis Batch: 660-50896

09/25/2007 0253

09/25/2007 0314

Prep Batch: N/A

Prep Batch: N/A

2HI2433.D

5 mL

5 mL

2HI2434.D

5 mL

5 mL

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

660-18295-46

660-18295-46

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

82 80 62 - 135 3 37Benzene

103 108 72 - 127 5 22Chlorobenzene

94 98 46 - 147 4 301,1-Dichlorethylene

100 95 68 - 131 4 33Toluene

82 80 56 - 143 2 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 101 of 113

Page 102: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/25/2007 1212

Method Blank - Batch: 660-50904

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50904

Prep Batch: N/A

09/25/2007 1212

1HI2510.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-50904/4

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 110 74 - 126Toluene-d8 (Surr) 101 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 102 of 113

Page 103: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/25/2007 1110

09/25/2007 1131

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50904

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/25/2007 1110

Prep Batch: N/A

Analysis Batch: 660-50904

1HI2507.D

5 mL

5 mL

1HI2508.D

5 mL

5 mL

ug/L

09/25/2007 1131

Analysis Batch: 660-50904

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-50904/2

LCSD 660-50904/3

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

8286 62 - 135 5 37Benzene

106113 72 - 127 6 22Chlorobenzene

9296 46 - 147 4 301,1-Dichlorethylene

95102 68 - 131 7 33Toluene

8284 56 - 143 3 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 103 of 113

Page 104: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/17/2007 1304

Method Blank - Batch: 660-50331

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50402

Prep Batch: 660-50331

09/15/2007 1329

7I17A

50 mL

50 mL

Units: mg/L

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACEMB 660-50331/1-A

Analyte Result Qual MDL PQL

0.070 U 0.200.070Aluminum0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/17/2007 1309

09/17/2007 1315

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50331

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L

09/15/2007 1329

Prep Batch: 660-50331

Analysis Batch: 660-50402

7I17A

50 mL

50 mL

7I17A

50 mL

50 mL

mg/L

09/15/2007 1329

Analysis Batch: 660-50402

Prep Batch: 660-50331

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACE

TJA ICP TRACE

LCS 660-50331/2-A

LCSD 660-50331/3-A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

9899 75 - 125 1 20Aluminum

9697 75 - 125 1 20Arsenic

102103 75 - 125 1 20Iron

101102 75 - 125 1 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 104 of 113

Page 105: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/17/2007 1333

09/17/2007 1338

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50331

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-50402

Analysis Batch: 660-50402

09/15/2007 1329

09/15/2007 1329

Prep Batch: 660-50331

Prep Batch: 660-50331

7I17A

50 mL

50 mL

7I17A

50 mL

50 mL

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACE

TJA ICP TRACE

660-18295-21

660-18295-21

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

106 105 75 - 125 1 20Aluminum

98 98 75 - 125 1 20Arsenic

98 98 75 - 125 0 20Iron

99 100 75 - 125 1 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 105 of 113

Page 106: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/19/2007 1315

Method Blank - Batch: 660-50332

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50544

Prep Batch: 660-50332

09/15/2007 1336

7I19B

50 mL

50 mL

Units: mg/L

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICPMB 660-50332/1-A

Analyte Result Qual MDL PQL

0.070 U 0.200.070Aluminum0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/19/2007 1321

09/19/2007 1326

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50332

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L

09/15/2007 1336

Prep Batch: 660-50332

Analysis Batch: 660-50544

7I19B

50 mL

50 mL

7I19B

50 mL

50 mL

mg/L

09/15/2007 1336

Analysis Batch: 660-50544

Prep Batch: 660-50332

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP

TJA ICP

LCS 660-50332/2-A

LCSD 660-50332/3-A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

9698 75 - 125 2 20Aluminum

9394 75 - 125 1 20Arsenic

102101 75 - 125 1 20Iron

100100 75 - 125 0 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 106 of 113

Page 107: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18295-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/19/2007 1340

09/19/2007 1344

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50332

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-50544

Analysis Batch: 660-50544

09/15/2007 1336

09/15/2007 1336

Prep Batch: 660-50332

Prep Batch: 660-50332

7I19B

50 mL

50 mL

7I19B

50 mL

50 mL

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP

TJA ICP

660-18295-25

660-18295-25

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

102 100 75 - 125 1 20Aluminum

96 96 75 - 125 0 20Arsenic

99 105 75 - 125 3 20Iron

99 101 75 - 125 1 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/26/2007Page 107 of 113

Page 108: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007

Page 108 of 113

Page 109: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007

Page 109 of 113

Page 110: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007

Page 110 of 113

Page 111: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007

Page 111 of 113

Page 112: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/26/2007

Page 112 of 113

Page 113: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Login Sample Receipt Check List

Client: S.M. Stoller Corporation Job Number: 660-18295-1

Login Number: 18295

Question T / F/ NA Comment

Creator: Fritz, Tina

List Source: TestAmerica Tampa

List Number: 1

Radioactivity either was not measured or, if measured, is at or below background

N/A

The cooler's custody seal, if present, is intact. N/A

The cooler or samples do not appear to have been compromised or tampered with.

True

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True 4 oC

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True

If necessary, staff have been informed of any short hold time or quick TAT needs

True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

TestAmerica Tampa 10/26/2007Page 113 of 113

Page 114: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

ANALYTICAL REPORT

Job Number: 660-18324-1

Job Description: Star Center

For:S.M. Stoller Corporation

2597 B 3/4 RoadGrand Junction, CO 81503

Attention: Mr. Charles Tabor

_____________________________________________

Nancy RobertsonProject Manager II

[email protected]/02/2007

Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements ofNELAC unless specified in the case narrative. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reportedresults is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634

Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com

10/02/2007Page 1 of 101

Page 115: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007Page 2 of 101

Page 116: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007Page 3 of 101

Page 117: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18324-4 PIN20-M035-N001

1.0 ug/L 8260B3.4cis-1,2-Dichloroethylene

660-18324-8 PIN20-MWL1-N001

1.0 ug/L 8260B1.9Benzene1.0 ug/L 8260B4.0Vinyl chloride

660-18324-9 PIN20-MWL2-N001

1.0 ug/L 8260B2.7trans-1,2-Dichloroethylene1.0 ug/L 8260B19Vinyl chloride

660-18324-10 PIN20-MWL3-N001

1.0 ug/L 8260B26cis-1,2-Dichloroethylene1.0 ug/L 8260B0.82 JToluene1.0 ug/L 8260B6.5trans-1,2-Dichloroethylene20 ug/L 8260B1400Vinyl chloride

660-18324-14 PIN20-M015-N001

1.0 ug/L 8260B2.1Vinyl chloride

660-18324-15 PIN20-M055-N001

1.0 ug/L 8260B3.2Vinyl chloride

660-18324-17 PIN20-M001-N001

25 ug/L 8260B930cis-1,2-Dichloroethylene5.0 ug/L 8260B4.6 J1,1-Dichlorethylene5.0 ug/L 8260B90trans-1,2-Dichloroethylene25 ug/L 8260B2200Vinyl chloride

660-18324-18 PIN20-M062-N001

10 ug/L 8260B160cis-1,2-Dichloroethylene1.0 ug/L 8260B3.1trans-1,2-Dichloroethylene10 ug/L 8260B830Vinyl chloride

TestAmerica Tampa

10/02/2007Page 4 of 101

Page 118: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18324-19 PIN24-0500

1.0 ug/L 8260B2.1Benzene20 ug/L 8260B770cis-1,2-Dichloroethylene1.0 ug/L 8260B3.31,1-Dichlorethylene1.0 ug/L 8260B100trans-1,2-Dichloroethylene20 ug/L 8260B1800Vinyl chloride

660-18324-20 PIN24-0501

5.0 ug/L 8260B530cis-1,2-Dichloroethylene1.0 ug/L 8260B1.41,1-Dichlorethylene1.0 ug/L 8260B33trans-1,2-Dichloroethylene1.0 ug/L 8260B6.6Trichloroethylene5.0 ug/L 8260B320Vinyl chloride

660-18324-21 PIN20-MWL4-N001

10 ug/L 8260B570cis-1,2-Dichloroethylene1.0 ug/L 8260B1.61,1-Dichlorethylene1.0 ug/L 8260B35trans-1,2-Dichloroethylene1.0 ug/L 8260B10Trichloroethylene10 ug/L 8260B340Vinyl chloride

660-18324-22 PIN20-M063-N001

1.0 ug/L 8260B150cis-1,2-Dichloroethylene1.0 ug/L 8260B1.11,1-Dichlorethylene1.0 ug/L 8260B19trans-1,2-Dichloroethylene1.0 ug/L 8260B7.0Trichloroethylene10 ug/L 8260B160Vinyl chloride

660-18324-24 PIN12-S67B-N001

1.0 ug/L 8260B24cis-1,2-Dichloroethylene1.0 ug/L 8260B681,1-Dichloroethane1.0 ug/L 8260B5.4trans-1,2-Dichloroethylene4.0 ug/L 8260B450Vinyl chloride

660-18324-25 PIN12-S67C-N001

2.0 ug/L 8260B190cis-1,2-Dichloroethylene1.0 ug/L 8260B2.81,1-Dichlorethylene1.0 ug/L 8260B2.71,1-Dichloroethane1.0 ug/L 8260B39trans-1,2-Dichloroethylene1.0 ug/L 8260B130Vinyl chloride

TestAmerica Tampa

10/02/2007Page 5 of 101

Page 119: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18324-26 PIN12-S67D-N001

1.0 ug/L 8260B65cis-1,2-Dichloroethylene1.0 ug/L 8260B1.01,1-Dichlorethylene1.0 ug/L 8260B2.21,1-Dichloroethane1.0 ug/L 8260B12trans-1,2-Dichloroethylene1.0 ug/L 8260B69Vinyl chloride

660-18324-31 PIN20-0503-N001

Total Recoverable0.010 mg/L 6010B0.027Arsenic

660-18324-32 PIN20-0502-N001

1.0 ug/L 8260B43cis-1,2-Dichloroethylene1.0 ug/L 8260B89Vinyl chloride

660-18324-33 PIN20-M064-N001

1.0 ug/L 8260B2.7Vinyl chloride

660-18324-35 PIN15-0587-N001

200 ug/L 8260B8200cis-1,2-Dichloroethylene50 ug/L 8260B26 J1,1-Dichlorethylene50 ug/L 8260B1700Toluene50 ug/L 8260B27 Jtrans-1,2-Dichloroethylene50 ug/L 8260B1700Trichloroethylene50 ug/L 8260B300Vinyl chloride

Total Recoverable0.050 mg/L 6010B36Iron0.20 mg/L 6010B2.7Aluminum0.010 mg/L 6010B0.015Manganese

TestAmerica Tampa

10/02/2007Page 6 of 101

Page 120: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18324-36 PIN15-0589-N001

1.0 ug/L 8260B49Benzene10 ug/L 8260B630cis-1,2-Dichloroethylene1.0 ug/L 8260B5.91,1-Dichlorethylene1.0 ug/L 8260B8.3Ethylbenzene2.0 ug/L 8260B7.5m,p-Xylene1.0 ug/L 8260B6.9o-Xylene10 ug/L 8260B430Toluene1.0 ug/L 8260B2.5trans-1,2-Dichloroethylene1.0 ug/L 8260B18Trichloroethylene10 ug/L 8260B440Vinyl chloride

Total Recoverable0.050 mg/L 6010B17Iron0.20 mg/L 6010B9.9Aluminum0.010 mg/L 6010B0.064Manganese

660-18324-37 PIN15-0566-N001

Total Recoverable0.050 mg/L 6010B11Iron0.20 mg/L 6010B31Aluminum0.010 mg/L 6010B0.018Manganese

660-18324-38 PIN15-0567-N001

Total Recoverable0.010 mg/L 6010B0.051Arsenic0.050 mg/L 6010B15Iron0.20 mg/L 6010B0.39Aluminum0.010 mg/L 6010B0.087Manganese

660-18324-39 PIN15-0560-N001

Total Recoverable0.050 mg/L 6010B5.7Iron0.20 mg/L 6010B0.20 BAluminum0.010 mg/L 6010B0.0045 BManganese

660-18324-40 PIN15-0561-N001

Total Recoverable0.050 mg/L 6010B1.2Iron0.20 mg/L 6010B0.28Aluminum0.010 mg/L 6010B0.014Manganese

TestAmerica Tampa

10/02/2007Page 7 of 101

Page 121: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18324-41 PIN15-0564-N001

Total Recoverable0.050 mg/L 6010B0.73Iron0.20 mg/L 6010B0.48Aluminum0.010 mg/L 6010B0.017Manganese

660-18324-42 PIN15-0565-N001

Total Recoverable0.050 mg/L 6010B9.7Iron0.20 mg/L 6010B1.1Aluminum0.010 mg/L 6010B0.20Manganese

660-18324-43 PIN15-0590-N001

1.0 ug/L 8260B2.2Benzene1.0 ug/L 8260B17cis-1,2-Dichloroethylene1.0 ug/L 8260B2.6Trichloroethylene

Total Recoverable0.050 mg/L 6010B1.9Iron0.20 mg/L 6010B2.5Aluminum0.010 mg/L 6010B0.0079 BManganese

660-18324-44 PIN15-0591-N001

2.0 ug/L 8260B1.3 JBenzene10 ug/L 8260B410cis-1,2-Dichloroethylene2.0 ug/L 8260B1.7 J1,1-Dichlorethylene2.0 ug/L 8260B4.2Toluene2.0 ug/L 8260B8.2trans-1,2-Dichloroethylene2.0 ug/L 8260B40Trichloroethylene2.0 ug/L 8260B28Vinyl chloride

Total Recoverable0.050 mg/L 6010B9.2Iron0.20 mg/L 6010B6.4Aluminum0.010 mg/L 6010B0.060Manganese

660-18324-45 PIN15-0573-N001

Total Recoverable0.050 mg/L 6010B1.1Iron0.20 mg/L 6010B0.12 BAluminum0.010 mg/L 6010B0.14Manganese

TestAmerica Tampa

10/02/2007Page 8 of 101

Page 122: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18324-46 PIN15-0574-N001

Total Recoverable0.050 mg/L 6010B2.4Iron0.20 mg/L 6010B0.12 BAluminum0.010 mg/L 6010B0.014Manganese

660-18324-47 PIN15-0576-N001

Total Recoverable0.050 mg/L 6010B1.3Iron0.20 mg/L 6010B1.2Aluminum0.010 mg/L 6010B0.023Manganese

660-18324-48 PIN15-0575-N001

Total Recoverable0.050 mg/L 6010B8.1Iron0.20 mg/L 6010B0.23Aluminum0.010 mg/L 6010B0.17Manganese

660-18324-49 PIN15-0577-N001

Total Recoverable0.050 mg/L 6010B9.4Iron0.20 mg/L 6010B0.19 BAluminum0.010 mg/L 6010B0.21Manganese

660-18324-50 PIN15-0578-N001

Total Recoverable0.050 mg/L 6010B0.79Iron0.20 mg/L 6010B0.51 NAluminum0.010 mg/L 6010B0.14Manganese

TestAmerica Tampa

10/02/2007Page 9 of 101

Page 123: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

METHOD SUMMARY

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Preparation MethodMethodLab LocationDescription

Matrix Water

SW846 8260BVolatile Organic Compounds by GC/MS TAL TAM

SW846 5030BTAL TAMPurge-and-Trap

SW846 6010BInductively Coupled Plasma - Atomic Emission Spectrometry TAL TAM

SW846 3005ATAL TAMAcid Digestion of Waters for Total Recoverable or

Lab References:

TAL TAM = TestAmerica Tampa

Method References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa

10/02/2007Page 10 of 101

Page 124: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

METHOD / ANALYST SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Method Analyst Analyst ID

Perez, Julian JPSW846 8260B

Fox, Greg GFSW846 6010B

TestAmerica Tampa

10/02/2007Page 11 of 101

Page 125: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

SAMPLE SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

09/14/2007 0800 09/18/2007 1050PIN24-0801660-18324-1 Water

09/14/2007 0835 09/18/2007 1050PIN20-M38D-N001660-18324-2 Water

09/14/2007 0900 09/18/2007 1050PIN20-M41D-N001660-18324-3 Water

09/14/2007 0925 09/18/2007 1050PIN20-M035-N001660-18324-4 Water

09/14/2007 0950 09/18/2007 1050PIN20-M40S-N001660-18324-5 Water

09/14/2007 1010 09/18/2007 1050PIN20-M40D-N001660-18324-6 Water

09/14/2007 1035 09/18/2007 1050PIN20-M036-N001660-18324-7 Water

09/14/2007 1125 09/18/2007 1050PIN20-MWL1-N001660-18324-8 Water

09/14/2007 1340 09/18/2007 1050PIN20-MWL2-N001660-18324-9 Water

09/14/2007 1415 09/18/2007 1050PIN20-MWL3-N001660-18324-10 Water

09/17/2007 0910 09/18/2007 1050PIN20-M011-N001660-18324-11 Water

09/17/2007 0930 09/18/2007 1050PIN20-M012-N001660-18324-12 Water

09/17/2007 1000 09/18/2007 1050PIN20-MWL6-N001660-18324-13 Water

09/17/2007 1035 09/18/2007 1050PIN20-M015-N001660-18324-14 Water

09/17/2007 1110 09/18/2007 1050PIN20-M055-N001660-18324-15 Water

09/17/2007 1410 09/18/2007 1050PIN20-M025-N001660-18324-16 Water

09/17/2007 1450 09/18/2007 1050PIN20-M001-N001660-18324-17 Water

09/17/2007 1530 09/18/2007 1050PIN20-M062-N001660-18324-18 Water

09/17/2007 1500 09/18/2007 1050PIN24-0500660-18324-19 Water

09/17/2007 1600 09/18/2007 1050PIN24-0501660-18324-20 Water

09/17/2007 1605 09/18/2007 1050PIN20-MWL4-N001660-18324-21 Water

09/18/2007 0820 09/18/2007 1050PIN20-M063-N001660-18324-22 Water

09/17/2007 0900 09/18/2007 1050PIN24-0602660-18324-23 Water

09/17/2007 0940 09/18/2007 1050PIN12-S67B-N001660-18324-24 Water

09/17/2007 1010 09/18/2007 1050PIN12-S67C-N001660-18324-25 Water

09/17/2007 1050 09/18/2007 1050PIN12-S67D-N001660-18324-26 Water

09/14/2007 0830 09/18/2007 1050PIN24-0601660-18324-27 Water

09/14/2007 0902 09/18/2007 1050PIN20-M054-N001660-18324-28 Water

09/14/2007 0938 09/18/2007 1050PIN20-M024-N001660-18324-29 Water

09/14/2007 1009 09/18/2007 1050PIN20-M023-N001660-18324-30 Water

09/14/2007 1306 09/18/2007 1050PIN20-0503-N001660-18324-31 Water

09/14/2007 1335 09/18/2007 1050PIN20-0502-N001660-18324-32 Water

09/17/2007 1525 09/18/2007 1050PIN20-M064-N001660-18324-33 Water

09/14/2007 0826 09/18/2007 1050PIN24-0701660-18324-34 Water

09/14/2007 0901 09/18/2007 1050PIN15-0587-N001660-18324-35 Water

09/14/2007 0951 09/18/2007 1050PIN15-0589-N001660-18324-36 Water

09/14/2007 1033 09/18/2007 1050PIN15-0566-N001660-18324-37 Water

09/14/2007 1059 09/18/2007 1050PIN15-0567-N001660-18324-38 Water

09/14/2007 1322 09/18/2007 1050PIN15-0560-N001660-18324-39 Water

09/14/2007 1343 09/18/2007 1050PIN15-0561-N001660-18324-40 Water

09/14/2007 1411 09/18/2007 1050PIN15-0564-N001660-18324-41 Water

09/14/2007 1433 09/18/2007 1050PIN15-0565-N001660-18324-42 Water

09/17/2007 0955 09/18/2007 1050PIN15-0590-N001660-18324-43 Water

09/17/2007 1052 09/18/2007 1050PIN15-0591-N001660-18324-44 Water

09/17/2007 1356 09/18/2007 1050PIN15-0573-N001660-18324-45 Water

09/17/2007 1418 09/18/2007 1050PIN15-0574-N001660-18324-46 Water

TestAmerica Tampa

10/02/2007Page 12 of 101

Page 126: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

SAMPLE SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

09/17/2007 1435 09/18/2007 1050PIN15-0576-N001660-18324-47 Water

09/17/2007 1506 09/18/2007 1050PIN15-0575-N001660-18324-48 Water

09/17/2007 1525 09/18/2007 1050PIN15-0577-N001660-18324-49 Water

09/17/2007 1547 09/18/2007 1050PIN15-0578-N001660-18324-50 Water

TestAmerica Tampa

10/02/2007Page 13 of 101

Page 127: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0801

09/14/2007 0800

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-1

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1547

09/26/2007 1547

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2621.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

103 74 - 1264-Bromofluorobenzene93 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 14 of 101

Page 128: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M38D-N001

09/14/2007 0835

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-2

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1608

09/26/2007 1608

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2622.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

110 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 15 of 101

Page 129: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M41D-N001

09/14/2007 0900

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-3

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1629

09/26/2007 1629

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2623.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

111 74 - 1264-Bromofluorobenzene93 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 16 of 101

Page 130: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M035-N001

09/14/2007 0925

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-4

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1649

09/26/2007 1649

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2624.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform3.4 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

114 74 - 1264-Bromofluorobenzene100 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 17 of 101

Page 131: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M40S-N001

09/14/2007 0950

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-5

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1710

09/26/2007 1710

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2625.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

126 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 18 of 101

Page 132: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M40D-N001

09/14/2007 1010

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-6

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1731

09/26/2007 1731

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2626.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

111 74 - 1264-Bromofluorobenzene94 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 19 of 101

Page 133: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M036-N001

09/14/2007 1035

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-7

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1751

09/26/2007 1751

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2627.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

117 74 - 1264-Bromofluorobenzene99 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 20 of 101

Page 134: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL1-N001

09/14/2007 1125

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-8

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1812

09/26/2007 1812

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2628.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.9 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane4.0 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

112 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 21 of 101

Page 135: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL2-N001

09/14/2007 1340

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-9

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1833

09/26/2007 1833

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2629.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene2.7 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane19 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

112 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 22 of 101

Page 136: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL3-N001

09/14/2007 1415

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-10

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1832

09/27/2007 1832

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2728.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform26 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.82 J 1.00.51Toluene6.5 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

91 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 23 of 101

Page 137: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL3-N001

09/14/2007 1415

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-10

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1935

09/27/2007 1935

20

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2731.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

1400 2010Vinyl chloride

TestAmerica Tampa 10/02/2007Page 24 of 101

Page 138: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M011-N001

09/17/2007 0910

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-11

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1547

09/27/2007 1547

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2720.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

98 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 25 of 101

Page 139: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M012-N001

09/17/2007 0930

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-12

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1955

09/27/2007 1955

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2732.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

107 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 26 of 101

Page 140: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL6-N001

09/17/2007 1000

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-13

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 2016

09/27/2007 2016

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2733.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

94 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 27 of 101

Page 141: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M015-N001

09/17/2007 1035

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-14

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 2037

09/27/2007 2037

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2734.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane2.1 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

95 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 28 of 101

Page 142: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M055-N001

09/17/2007 1110

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-15

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 2057

09/27/2007 2057

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2735.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.2 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

100 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 29 of 101

Page 143: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M025-N001

09/17/2007 1410

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-16

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 2118

09/27/2007 2118

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2736.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

114 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 30 of 101

Page 144: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M001-N001

09/17/2007 1450

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-17

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0901

09/28/2007 0901

5.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2770.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

2.5 U 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane4.6 J 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide5.0 U 205.0Methyl chloride20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene2.6 U 5.02.6Toluene90 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane2.5 U 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

106 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 31 of 101

Page 145: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M001-N001

09/17/2007 1450

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-17

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0615

09/28/2007 0615

25

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2762.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

930 2516cis-1,2-Dichloroethylene2200 2513Vinyl chloride

TestAmerica Tampa 10/02/2007Page 32 of 101

Page 146: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M062-N001

09/17/2007 1530

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-18

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1003

09/28/2007 1003

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2773.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene3.1 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

97 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 33 of 101

Page 147: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M062-N001

09/17/2007 1530

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-18

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1723

09/28/2007 1723

10

8260B Analysis Batch: 660-51195

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2814.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

160 106.5cis-1,2-Dichloroethylene830 105.0Vinyl chloride

TestAmerica Tampa 10/02/2007Page 34 of 101

Page 148: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0500

09/17/2007 1500

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-19

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0431

09/28/2007 0431

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2757.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

2.1 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane3.3 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene100 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

95 74 - 1264-Bromofluorobenzene96 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 35 of 101

Page 149: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0500

09/17/2007 1500

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-19

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1703

09/28/2007 1703

20

8260B Analysis Batch: 660-51195

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2813.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

770 2013cis-1,2-Dichloroethylene1800 2010Vinyl chloride

TestAmerica Tampa 10/02/2007Page 36 of 101

Page 150: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0501

09/17/2007 1600

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-20

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0452

09/28/2007 0452

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2758.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.4 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene33 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane6.6 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

103 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 37 of 101

Page 151: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0501

09/17/2007 1600

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-20

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1744

09/28/2007 1744

5.0

8260B Analysis Batch: 660-51195

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2815.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

530 5.03.3cis-1,2-Dichloroethylene320 5.02.5Vinyl chloride

TestAmerica Tampa 10/02/2007Page 38 of 101

Page 152: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL4-N001

09/17/2007 1605

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-21

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1024

09/28/2007 1024

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2774.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.6 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene35 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane10 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

115 74 - 1264-Bromofluorobenzene111 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 39 of 101

Page 153: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-MWL4-N001

09/17/2007 1605

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-21

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0656

09/28/2007 0656

10

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2764.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

570 106.5cis-1,2-Dichloroethylene340 105.0Vinyl chloride

TestAmerica Tampa 10/02/2007Page 40 of 101

Page 154: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M063-N001

09/18/2007 0820

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-22

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1826

09/28/2007 1826

1.0

8260B Analysis Batch: 660-51195

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2817.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform150 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.1 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene19 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane7.0 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

97 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 41 of 101

Page 155: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M063-N001

09/18/2007 0820

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-22

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0922

09/28/2007 0922

10

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2771.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

160 105.0Vinyl chloride

TestAmerica Tampa 10/02/2007Page 42 of 101

Page 156: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0602

09/17/2007 0900

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-23

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0513

09/28/2007 0513

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2759.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

97 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 43 of 101

Page 157: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S67B-N001

09/17/2007 0940

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-24

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1044

09/28/2007 1044

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2775.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform24 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane68 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene5.4 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

103 74 - 1264-Bromofluorobenzene110 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 44 of 101

Page 158: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S67B-N001

09/17/2007 0940

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-24

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0738

09/28/2007 0738

4.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2766.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

450 4.02.0Vinyl chloride

TestAmerica Tampa 10/02/2007Page 45 of 101

Page 159: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S67C-N001

09/17/2007 1010

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-25

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1108

09/28/2007 1108

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2776.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane2.8 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.7 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene39 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane130 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

91 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 46 of 101

Page 160: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S67C-N001

09/17/2007 1010

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-25

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1805

09/28/2007 1805

2.0

8260B Analysis Batch: 660-51195

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2816.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

190 2.01.3cis-1,2-Dichloroethylene

TestAmerica Tampa 10/02/2007Page 47 of 101

Page 161: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S67D-N001

09/17/2007 1050

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-26

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0554

09/28/2007 0554

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2761.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform65 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.0 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.2 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene12 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane69 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

105 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 48 of 101

Page 162: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0601

09/14/2007 0830

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-27

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1854

09/26/2007 1854

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2630.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

111 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 49 of 101

Page 163: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M054-N001

09/14/2007 0902

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-28

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1914

09/26/2007 1914

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2631.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

121 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 50 of 101

Page 164: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M024-N001

09/14/2007 0938

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-29

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1935

09/26/2007 1935

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2632.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

110 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 51 of 101

Page 165: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M023-N001

09/14/2007 1009

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-30

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 1956

09/26/2007 1956

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2633.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

122 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 52 of 101

Page 166: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-0503-N001

09/14/2007 1306

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-31

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/26/2007 2017

09/26/2007 2017

1.0

8260B Analysis Batch: 660-50979

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2634.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

129 74 - 126*4-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 53 of 101

Page 167: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-0502-N001

09/14/2007 1335

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-32

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1853

09/27/2007 1853

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2729.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform43 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane89 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

113 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 54 of 101

Page 168: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN20-M064-N001

09/17/2007 1525

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-33

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0533

09/28/2007 0533

1.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2760.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane2.7 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

104 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 55 of 101

Page 169: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0701

09/14/2007 0826

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-34

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1607

09/27/2007 1607

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2721.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

98 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 56 of 101

Page 170: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0587-N001

09/14/2007 0901

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-35

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1730

09/27/2007 1730

50

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2725.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

25 U 5025Benzene18 U 5018Bromodichloromethane29 U 5029Bromoform21 U 5021Carbon tetrachloride32 U 5032Chlorobenzene130 U 250130Chloroethane45 U 5045Chloroform7.0 U 507.0cis-1,3-Dichloropropene17 U 5017Dibromochloromethane26 J 50231,1-Dichlorethylene130 U 250130Dichlorodifluoromethane26 U 50261,1-Dichloroethane29 U 50291,2-Dichloroethane26 U 50261,2-Dichloropropane22 U 5022Ethylbenzene32 U 5032m-Dichlorobenzene130 U 250130Methyl bromide50 U 20050Methyl chloride200 U 250200Methylene Chloride22 U 5022Methyl tert-butyl ether30 U 10030m,p-Xylene22 U 5022o-Dichlorobenzene25 U 5025o-Xylene26 U 5026p-Dichlorobenzene7.5 U 507.51,1,2,2-Tetrachloroethane25 U 5025Tetrachloroethylene1700 5026Toluene27 J 5022trans-1,2-Dichloroethylene7.0 U 507.0trans-1,3-Dichloropropene23 U 50231,1,1-Trichloroethane24 U 50241,1,2-Trichloroethane1700 5025Trichloroethylene130 U 250130Trichlorofluoromethane300 5025Vinyl chloride

Surrogate %Rec Acceptance Limits

101 74 - 1264-Bromofluorobenzene100 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 57 of 101

Page 171: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0587-N001

09/14/2007 0901

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-35

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1709

09/27/2007 1709

200

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2724.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

8200 200130cis-1,2-Dichloroethylene

TestAmerica Tampa 10/02/2007Page 58 of 101

Page 172: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0589-N001

09/14/2007 0951

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-36

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1812

09/27/2007 1812

1.0

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2727.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

49 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane5.9 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane8.3 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether7.5 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene6.9 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene2.5 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane18 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

106 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 59 of 101

Page 173: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0589-N001

09/14/2007 0951

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-36

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/27/2007 1751

09/27/2007 1751

10

8260B Analysis Batch: 660-51087

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2726.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

630 106.5cis-1,2-Dichloroethylene430 105.1Toluene440 105.0Vinyl chloride

TestAmerica Tampa 10/02/2007Page 60 of 101

Page 174: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0590-N001

09/17/2007 0955

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-43

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 1846

09/28/2007 1846

1.0

8260B Analysis Batch: 660-51195

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

1HI2818.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

2.2 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform17 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane2.6 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

108 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 61 of 101

Page 175: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0591-N001

09/17/2007 1052

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-44

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0942

09/28/2007 0942

2.0

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2772.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

1.3 J 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.8 U 2.01.8Chloroform0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane1.7 J 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide2.0 U 8.02.0Methyl chloride8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene4.2 2.01.0Toluene8.2 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane40 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane28 2.01.0Vinyl chloride

Surrogate %Rec Acceptance Limits

90 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/02/2007Page 62 of 101

Page 176: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0591-N001

09/17/2007 1052

09/18/2007 1050Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18324-44

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 0840

09/28/2007 0840

10

8260B Analysis Batch: 660-51191

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMH GC/MS

2HI2769.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

410 106.5cis-1,2-Dichloroethylene

TestAmerica Tampa 10/02/2007Page 63 of 101

Page 177: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN20-0503-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1306

09/18/2007 1050

660-18324-31

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1527

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

0.027 0.0100.0048Arsenic

TestAmerica Tampa 10/02/2007Page 64 of 101

Page 178: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN20-0502-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1335

09/18/2007 1050

660-18324-32

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1523

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

0.0048 U 0.0100.0048Arsenic

TestAmerica Tampa 10/02/2007Page 65 of 101

Page 179: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0587-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 0901

09/18/2007 1050

660-18324-35

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1518

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

36 0.0500.022Iron2.7 0.200.070Aluminum0.015 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 66 of 101

Page 180: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0589-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 0951

09/18/2007 1050

660-18324-36

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1514

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

17 0.0500.022Iron9.9 0.200.070Aluminum0.064 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 67 of 101

Page 181: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0566-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1033

09/18/2007 1050

660-18324-37

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1459

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

11 0.0500.022Iron31 0.200.070Aluminum0.018 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 68 of 101

Page 182: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0567-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1059

09/18/2007 1050

660-18324-38

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1455

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

0.051 0.0100.0048Arsenic15 0.0500.022Iron0.39 0.200.070Aluminum0.087 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 69 of 101

Page 183: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0560-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1322

09/18/2007 1050

660-18324-39

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1450

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

5.7 0.0500.022Iron0.20 B 0.200.070Aluminum0.0045 B 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 70 of 101

Page 184: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0561-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1343

09/18/2007 1050

660-18324-40

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1446

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

1.2 0.0500.022Iron0.28 0.200.070Aluminum0.014 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 71 of 101

Page 185: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0564-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1411

09/18/2007 1050

660-18324-41

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1441

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

0.73 0.0500.022Iron0.48 0.200.070Aluminum0.017 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 72 of 101

Page 186: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0565-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/14/2007 1433

09/18/2007 1050

660-18324-42

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1437

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

9.7 0.0500.022Iron1.1 0.200.070Aluminum0.20 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 73 of 101

Page 187: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0590-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 0955

09/18/2007 1050

660-18324-43

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1432

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

1.9 0.0500.022Iron2.5 0.200.070Aluminum0.0079 B 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 74 of 101

Page 188: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0591-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1052

09/18/2007 1050

660-18324-44

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1428

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

9.2 0.0500.022Iron6.4 0.200.070Aluminum0.060 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 75 of 101

Page 189: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0573-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1356

09/18/2007 1050

660-18324-45

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1423

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

1.1 0.0500.022Iron0.12 B 0.200.070Aluminum0.14 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 76 of 101

Page 190: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0574-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1418

09/18/2007 1050

660-18324-46

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1419

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

2.4 0.0500.022Iron0.12 B 0.200.070Aluminum0.014 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 77 of 101

Page 191: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0576-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1435

09/18/2007 1050

660-18324-47

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1404

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

1.3 0.0500.022Iron1.2 0.200.070Aluminum0.023 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 78 of 101

Page 192: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0575-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1506

09/18/2007 1050

660-18324-48

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1400

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

8.1 0.0500.022Iron0.23 0.200.070Aluminum0.17 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 79 of 101

Page 193: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0577-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1525

09/18/2007 1050

660-18324-49

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1355

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

9.4 0.0500.022Iron0.19 B 0.200.070Aluminum0.21 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 80 of 101

Page 194: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Client Sample ID: PIN15-0578-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/17/2007 1547

09/18/2007 1050

660-18324-50

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/25/2007 1342

09/18/2007 1648

TJA ICP

7I25B

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50861

3005A Prep Batch: 660-50511

0.79 0.0500.022Iron0.51 N 0.200.070Aluminum0.14 0.0100.0014Manganese

TestAmerica Tampa 10/02/2007Page 81 of 101

Page 195: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

DATA REPORTING QUALIFIERS

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Lab Section Qualifier Description

GC/MS VOA

Analyzed for but not detected.U

Indicates an estimated value.J

Surrogate exceeds the control limit*

Metals

Indicates analyzed for but not detected.U

Spiked sample recovery is not within control limits.N

Value less than contract required detection limit but greater than or equal to the Method Detection Limit

B

TestAmerica Tampa

10/02/2007Page 82 of 101

Page 196: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/26/2007 1301

Method Blank - Batch: 660-50979

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50979

Prep Batch: N/A

09/26/2007 1301

1HI2613.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-50979/5

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 114 74 - 126Toluene-d8 (Surr) 101 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 83 of 101

Page 197: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/26/2007 1159

09/26/2007 1220

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50979

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/26/2007 1159

Prep Batch: N/A

Analysis Batch: 660-50979

1HI2610.D

5 mL

5 mL

1HI2611.D

5 mL

5 mL

ug/L

09/26/2007 1220

Analysis Batch: 660-50979

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-50979/3

LCSD 660-50979/4

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

7177 62 - 135 8 37Benzene

104117 72 - 127 11 22Chlorobenzene

8896 46 - 147 9 301,1-Dichlorethylene

96103 68 - 131 8 33Toluene

7378 56 - 143 6 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 84 of 101

Page 198: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/27/2007 1505

Method Blank - Batch: 660-51087

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51087

Prep Batch: N/A

09/27/2007 1505

1HI2718.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-51087/3

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 92 74 - 126Toluene-d8 (Surr) 104 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 85 of 101

Page 199: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/27/2007 1239

09/27/2007 1300

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51087

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/27/2007 1239

Prep Batch: N/A

Analysis Batch: 660-51087

1HI2711.D

5 mL

5 mL

1HI2712.D

5 mL

5 mL

ug/L

09/27/2007 1300

Analysis Batch: 660-51087

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-51087/1

LCSD 660-51087/2

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

107114 62 - 135 6 37Benzene

110111 72 - 127 1 22Chlorobenzene

114127 46 - 147 11 301,1-Dichlorethylene

110116 68 - 131 5 33Toluene

107119 56 - 143 11 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 86 of 101

Page 200: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

10/01/2007 1510

10/01/2007 1531

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-51087

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-51087

Analysis Batch: 660-51087

10/01/2007 1510

10/01/2007 1531

Prep Batch: N/A

Prep Batch: N/A

2HJ0118.D

5 mL

5 mL

2HJ0119.D

5 mL

5 mL

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

660-18324-11

660-18324-11

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

105 98 62 - 135 7 37Benzene

120 111 72 - 127 7 22Chlorobenzene

125 111 46 - 147 11 301,1-Dichlorethylene

127 120 68 - 131 6 33Toluene

109 100 56 - 143 8 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 87 of 101

Page 201: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/28/2007 0350

Method Blank - Batch: 660-51191

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51191

Prep Batch: N/A

09/28/2007 0350

2HI2755.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-51191/2

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 103 74 - 126Toluene-d8 (Surr) 110 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 88 of 101

Page 202: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/28/2007 1210

09/28/2007 0308

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51191

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/28/2007 1210

Prep Batch: N/A

Analysis Batch: 660-51191

2HI2779.D

5 mL

5 mL

2HI2753.D

5 mL

5 mL

ug/L

09/28/2007 0308

Analysis Batch: 660-51191

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-51191/16

LCSD 660-51191/1

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

10491 62 - 135 13 37Benzene

118117 72 - 127 0 22Chlorobenzene

116108 46 - 147 7 301,1-Dichlorethylene

118116 68 - 131 1 33Toluene

10795 56 - 143 12 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 89 of 101

Page 203: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

10/01/2007 1552

10/01/2007 1612

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-51191

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-51191

Analysis Batch: 660-51191

10/01/2007 1552

10/01/2007 1612

Prep Batch: N/A

Prep Batch: N/A

2HJ0120.D

5 mL

5 mL

2HJ0121.D

5 mL

5 mL

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

660-18324-23

660-18324-23

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

99 98 62 - 135 1 37Benzene

111 111 72 - 127 0 22Chlorobenzene

114 113 46 - 147 1 301,1-Dichlorethylene

121 117 68 - 131 3 33Toluene

98 100 56 - 143 2 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 90 of 101

Page 204: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/28/2007 1540

Method Blank - Batch: 660-51195

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51195

Prep Batch: N/A

09/28/2007 1540

1HI2809.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMH GC/MSMB 660-51195/3

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 110 74 - 126Toluene-d8 (Surr) 111 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 91 of 101

Page 205: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/28/2007 1438

09/28/2007 1458

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51195

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/28/2007 1438

Prep Batch: N/A

Analysis Batch: 660-51195

1HI2806.D

5 mL

5 mL

1HI2807.D

5 mL

5 mL

ug/L

09/28/2007 1458

Analysis Batch: 660-51195

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMH GC/MS

BVMH GC/MS

LCS 660-51195/1

LCSD 660-51195/2

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

110107 62 - 135 2 37Benzene

126116 72 - 127 8 22Chlorobenzene

134130 46 - 147 3 301,1-Dichlorethylene

130123 68 - 131 6 33Toluene

110106 56 - 143 3 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 92 of 101

Page 206: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/25/2007 1323

Method Blank - Batch: 660-50511

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50861

Prep Batch: 660-50511

09/18/2007 1648

7I25B

50 mL

50 mL

Units: mg/L

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICPMB 660-50511/1-A

Analyte Result Qual MDL PQL

0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.070 U 0.200.070Aluminum0.0014 U 0.0100.0014Manganese

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/25/2007 1328

09/25/2007 1333

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50511

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L

09/18/2007 1648

Prep Batch: 660-50511

Analysis Batch: 660-50861

7I25B

50 mL

50 mL

7I25B

50 mL

50 mL

mg/L

09/18/2007 1648

Analysis Batch: 660-50861

Prep Batch: 660-50511

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP

TJA ICP

LCS 660-50511/2-A

LCSD 660-50511/3-A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

10099 75 - 125 1 20Arsenic

110110 75 - 125 0 20Iron

101101 75 - 125 0 20Aluminum

107107 75 - 125 0 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 93 of 101

Page 207: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18324-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/25/2007 1346

09/25/2007 1351

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50511

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-50861

Analysis Batch: 660-50861

09/18/2007 1648

09/18/2007 1648

Prep Batch: 660-50511

Prep Batch: 660-50511

7I25B

50 mL

50 mL

7I25B

50 mL

50 mL

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP

TJA ICP

660-18324-50

660-18324-50

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

104 101 75 - 125 3 20Arsenic

102 112 75 - 125 5 20Iron

144 139 75 - 125 3 20 N NAluminum

103 103 75 - 125 1 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/02/2007Page 94 of 101

Page 208: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007

Page 95 of 101

Page 209: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007

Page 96 of 101

Page 210: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007

Page 97 of 101

Page 211: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007

Page 98 of 101

Page 212: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007

Page 99 of 101

Page 213: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/02/2007

Page 100 of 101

Page 214: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Login Sample Receipt Check List

Client: S.M. Stoller Corporation Job Number: 660-18324-1

Login Number: 18324

Question T / F/ NA Comment

List Source: TestAmerica Tampa

List Number: 1

Radioactivity either was not measured or, if measured, is at or below background

N/A

The cooler's custody seal, if present, is intact. N/A

The cooler or samples do not appear to have been compromised or tampered with.

True

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True

If necessary, staff have been informed of any short hold time or quick TAT needs

True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

TestAmerica Tampa10/02/2007Page 101 of 101

Page 215: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

ANALYTICAL REPORT

Job Number: 660-18419-1

Job Description: Pinellas Star

For:S.M. Stoller Corporation

2597 B 3/4 RoadGrand Junction, CO 81503

Attention: Mr. Charles Tabor

_____________________________________________

Nancy RobertsonProject Manager II

[email protected]/03/2007

Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements ofNELAC unless specified in the case narrative. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reportedresults is available upon request. The results contained in this test report relate only to these samples included herein.

TestAmerica Laboratories, Inc.

TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634

Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com

10/03/2007Page 1 of 107

Page 216: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007Page 2 of 107

Page 217: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007Page 3 of 107

Page 218: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-4 PIN06-0501-N001

Total Recoverable0.010 mg/L 6010B0.020Arsenic

660-18419-5 PIN12-0523-N001

1.0 ug/L 8260B32cis-1,2-Dichloroethylene1.0 ug/L 8260B22trans-1,2-Dichloroethylene1.0 ug/L 8260B1.0Trichloroethylene1.0 ug/L 8260B20Vinyl chloride

660-18419-10 PIN12-S72C-N001

1.0 ug/L 8260B2.61,1-Dichloroethane

660-18419-13 PIN12-S73C-N001

1.0 ug/L 8260B3.9trans-1,2-Dichloroethylene1.0 ug/L 8260B18Vinyl chloride

660-18419-17 PIN12-0518-N001

1.0 ug/L 8260B1.9Vinyl chloride

660-18419-18 PIN12-0525-N001

1.0 ug/L 8260B1.6cis-1,2-Dichloroethylene1.0 ug/L 8260B0.66 JVinyl chloride

Total Recoverable0.010 mg/L 6010B0.026Arsenic

660-18419-19 PIN24-0503

20 ug/L 8260B770cis-1,2-Dichloroethylene20 ug/L 8260B521,1-Dichlorethylene20 ug/L 8260B14 Jtrans-1,2-Dichloroethylene20 ug/L 8260B1700Vinyl chloride

TestAmerica Tampa

10/03/2007Page 4 of 107

Page 219: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-20 PIN12-0524-N001

1.0 ug/L 8260B0.70 JBenzene20 ug/L 8260B770cis-1,2-Dichloroethylene1.0 ug/L 8260B291,1-Dichlorethylene1.0 ug/L 8260B1.31,1-Dichloroethane1.0 ug/L 8260B10trans-1,2-Dichloroethylene1.0 ug/L 8260B4.3Trichloroethylene20 ug/L 8260B1600Vinyl chloride

660-18419-21 PIN21-0505-N001

1.0 ug/L 8260B1.21,1-Dichloroethane

660-18419-23 PIN12-0513-N001

1.0 ug/L 8260B9.41,1-Dichloroethane1.0 ug/L 8260B0.59 Jtrans-1,2-Dichloroethylene

660-18419-24 PIN12-0514-N001

1.0 ug/L 8260B5.8cis-1,2-Dichloroethylene1.0 ug/L 8260B8.51,1-Dichloroethane1.0 ug/L 8260B15trans-1,2-Dichloroethylene1.0 ug/L 8260B42Vinyl chloride

660-18419-25 PIN12-S68C-N001

1.0 ug/L 8260B4.2cis-1,2-Dichloroethylene1.0 ug/L 8260B5.11,1-Dichloroethane1.0 ug/L 8260B10Vinyl chloride

660-18419-26 PIN12-S68D-N001

1.0 ug/L 8260B56cis-1,2-Dichloroethylene1.0 ug/L 8260B1.01,1-Dichlorethylene1.0 ug/L 8260B5.31,1-Dichloroethane1.0 ug/L 8260B1.1trans-1,2-Dichloroethylene1.0 ug/L 8260B80Vinyl chloride

TestAmerica Tampa

10/03/2007Page 5 of 107

Page 220: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-27 PIN24-0504

1.0 ug/L 8260B64cis-1,2-Dichloroethylene1.0 ug/L 8260B1.11,1-Dichlorethylene1.0 ug/L 8260B6.01,1-Dichloroethane1.0 ug/L 8260B1.2trans-1,2-Dichloroethylene1.0 ug/L 8260B91Vinyl chloride

660-18419-29 PIN15-0506-N001

Total Recoverable0.20 mg/L 6010B3.8Aluminum0.050 mg/L 6010B2.0Iron0.010 mg/L 6010B0.010Manganese

660-18419-30 PIN15-0507-N001

Total Recoverable0.20 mg/L 6010B1.7Aluminum0.050 mg/L 6010B1.1Iron0.010 mg/L 6010B0.017Manganese

660-18419-31 PIN15-0520-N001

Total Recoverable0.20 mg/L 6010B0.15 BAluminum0.050 mg/L 6010B0.76Iron0.010 mg/L 6010B0.018Manganese

660-18419-32 PIN15-0534-N001

Total Recoverable0.20 mg/L 6010B1.9Aluminum0.050 mg/L 6010B0.65Iron0.010 mg/L 6010B0.019Manganese

660-18419-33 PIN15-0518-N001

Total Recoverable0.20 mg/L 6010B0.98Aluminum0.050 mg/L 6010B1.0Iron0.010 mg/L 6010B0.011Manganese

TestAmerica Tampa

10/03/2007Page 6 of 107

Page 221: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-34 PIN15-M24D-N001

Total Recoverable0.20 mg/L 6010B8.6Aluminum0.050 mg/L 6010B1.1Iron0.010 mg/L 6010B0.014Manganese

660-18419-35 PIN15-M33D-N001

Total Recoverable0.20 mg/L 6010B6.9Aluminum0.050 mg/L 6010B2.0Iron0.010 mg/L 6010B0.014Manganese

660-18419-36 PIN15-0562-N001

Total Recoverable0.20 mg/L 6010B1.2 NAluminum0.050 mg/L 6010B4.9Iron0.010 mg/L 6010B0.0096 BManganese

660-18419-37 PIN15-0563-N001

Total Recoverable0.20 mg/L 6010B0.35Aluminum0.050 mg/L 6010B8.6Iron0.010 mg/L 6010B0.072Manganese

660-18419-38 PIN15-M14S-N001

Total Recoverable0.20 mg/L 6010B0.31Aluminum0.010 mg/L 6010B0.074Arsenic0.050 mg/L 6010B13Iron0.010 mg/L 6010B0.013Manganese

660-18419-39 PIN15-M14D-N001

Total Recoverable0.20 mg/L 6010B6.1Aluminum0.050 mg/L 6010B5.8Iron0.010 mg/L 6010B0.0079 BManganese

TestAmerica Tampa

10/03/2007Page 7 of 107

Page 222: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-40 PIN15-0559-N001

Total Recoverable0.20 mg/L 6010B1.8Aluminum0.050 mg/L 6010B0.44Iron0.010 mg/L 6010B0.0071 BManganese

660-18419-41 PIN12-S68B-N001

Total Recoverable0.010 mg/L 6010B0.060Arsenic

660-18419-42 PIN21-0512-N001

1.0 ug/L 8260B5.9cis-1,2-Dichloroethylene1.0 ug/L 8260B1.61,1-Dichloroethane1.0 ug/L 8260B14Vinyl chloride

660-18419-43 PIN12-0526-N001

1.0 ug/L 8260B1.9cis-1,2-Dichloroethylene1.0 ug/L 8260B1.3trans-1,2-Dichloroethylene1.0 ug/L 8260B3.0Vinyl chloride

660-18419-47 PIN12-S69C-N001

1.0 ug/L 8260B1.0Vinyl chloride

660-18419-48 PIN12-S69D-N001

1.0 ug/L 8260B0.54 JVinyl chloride

660-18419-49 PIN15-0571-N001

Total Recoverable0.20 mg/L 6010B1.1Aluminum0.050 mg/L 6010B3.4Iron0.010 mg/L 6010B0.010Manganese

TestAmerica Tampa

10/03/2007Page 8 of 107

Page 223: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-50 PIN15-0572-N001

Total Recoverable0.20 mg/L 6010B2.3Aluminum0.050 mg/L 6010B0.96Iron0.010 mg/L 6010B0.010Manganese

660-18419-51 PIN15-0570-N001

Total Recoverable0.20 mg/L 6010B9.4Aluminum0.050 mg/L 6010B1.6Iron0.010 mg/L 6010B0.024Manganese

660-18419-52 PIN15-0510-N001

Total Recoverable0.20 mg/L 6010B0.32Aluminum0.050 mg/L 6010B4.6Iron0.010 mg/L 6010B0.032Manganese

660-18419-53 PIN24-0506

Total Recoverable0.20 mg/L 6010B1.8Aluminum0.050 mg/L 6010B1.2Iron0.010 mg/L 6010B0.0060 BManganese

660-18419-54 PIN24-0507

1.0 ug/L 8260B22Vinyl chloride

Total Recoverable0.20 mg/L 6010B1.4Aluminum0.050 mg/L 6010B3.2Iron0.010 mg/L 6010B0.018Manganese

660-18419-55 PIN15-0568-N001

Total Recoverable0.20 mg/L 6010B0.94Aluminum0.050 mg/L 6010B1.2Iron0.010 mg/L 6010B0.0058 BManganese

TestAmerica Tampa

10/03/2007Page 9 of 107

Page 224: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

EXECUTIVE SUMMARY - Detections

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

660-18419-56 PIN15-0569-N001

1.0 ug/L 8260B21Vinyl chloride

Total Recoverable0.20 mg/L 6010B1.5Aluminum0.050 mg/L 6010B3.2Iron0.010 mg/L 6010B0.018Manganese

660-18419-58 PIN12-S71C-N001

1.0 ug/L 8260B20cis-1,2-Dichloroethylene1.0 ug/L 8260B1.31,1-Dichlorethylene1.0 ug/L 8260B2.41,1-Dichloroethane1.0 ug/L 8260B14trans-1,2-Dichloroethylene1.0 ug/L 8260B45Vinyl chloride

660-18419-59 PIN12-S71D-N001

1.0 ug/L 8260B7.7cis-1,2-Dichloroethylene1.0 ug/L 8260B1.01,1-Dichlorethylene1.0 ug/L 8260B1.31,1-Dichloroethane1.0 ug/L 8260B4.8trans-1,2-Dichloroethylene1.0 ug/L 8260B19Vinyl chloride

660-18419-60 PIN12-S70B-N001

1.0 ug/L 8260B16cis-1,2-Dichloroethylene1.0 ug/L 8260B0.61 Jtrans-1,2-Dichloroethylene1.0 ug/L 8260B22Vinyl chloride

660-18419-61 PIN12-S70C-N001

1.0 ug/L 8260B25cis-1,2-Dichloroethylene1.0 ug/L 8260B1.51,1-Dichlorethylene1.0 ug/L 8260B8.51,1-Dichloroethane1.0 ug/L 8260B11trans-1,2-Dichloroethylene1.0 ug/L 8260B35Vinyl chloride

660-18419-62 PIN12-S70D-N001

1.0 ug/L 8260B17cis-1,2-Dichloroethylene1.0 ug/L 8260B1.61,1-Dichlorethylene1.0 ug/L 8260B6.11,1-Dichloroethane1.0 ug/L 8260B7.4trans-1,2-Dichloroethylene1.0 ug/L 8260B19Vinyl chloride

TestAmerica Tampa

10/03/2007Page 10 of 107

Page 225: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

METHOD SUMMARY

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Preparation MethodMethodLab LocationDescription

Matrix: Water

SW846 8260BVolatile Organic Compounds by GC/MS TAL TAM

SW846 5030BTAL TAMPurge-and-Trap

SW846 6010BInductively Coupled Plasma - Atomic Emission Spectrometry TAL TAM

SW846 3005ATAL TAMAcid Digestion of Waters for Total Recoverable or

Lab References:

TAL TAM = TestAmerica Tampa

Method References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Tampa

10/03/2007Page 11 of 107

Page 226: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

METHOD / ANALYST SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Method Analyst Analyst ID

Davidson, Sean SDSW846 8260BMathew, Pinky PMSW846 8260BStolz, Dawn DSSW846 8260B

Fox, Greg GFSW846 6010B

TestAmerica Tampa

10/03/2007Page 12 of 107

Page 227: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

SAMPLE SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

09/18/2007 0840 09/20/2007 1347PIN24-0603660-18419-1 Water

09/18/2007 0923 09/20/2007 1347PIN12-0520-N001660-18419-2 Water

09/18/2007 0952 09/20/2007 1347PIN06-0500-N001660-18419-3 Water

09/18/2007 1026 09/20/2007 1347PIN06-0501-N001660-18419-4 Water

09/18/2007 1344 09/20/2007 1347PIN12-0523-N001660-18419-5 Water

09/18/2007 1412 09/20/2007 1347PIN12-0522-N001660-18419-6 Water

09/18/2007 1537 09/20/2007 1347PIN12-0510-N001660-18419-7 Water

09/18/2007 1616 09/20/2007 1347PIN12-0509-N001660-18419-8 Water

09/19/2007 0948 09/20/2007 1347PIN12-S72B-N001660-18419-9 Water

09/19/2007 1025 09/20/2007 1347PIN12-S72C-N001660-18419-10 Water

09/19/2007 1100 09/20/2007 1347PIN12-S72D-N001660-18419-11 Water

09/19/2007 1407 09/20/2007 1347PIN12-S73D-N001660-18419-12 Water

09/19/2007 1434 09/20/2007 1347PIN12-S73C-N001660-18419-13 Water

09/19/2007 1506 09/20/2007 1347PIN12-S73B-N001660-18419-14 Water

09/18/2007 0835 09/20/2007 1347PIN24-0802660-18419-15 Water

09/18/2007 1030 09/20/2007 1347PIN12-0517-N001660-18419-16 Water

09/18/2007 1050 09/20/2007 1347PIN12-0518-N001660-18419-17 Water

09/18/2007 1350 09/20/2007 1347PIN12-0525-N001660-18419-18 Water

09/18/2007 1400 09/20/2007 1347PIN24-0503660-18419-19 Water

09/18/2007 1425 09/20/2007 1347PIN12-0524-N001660-18419-20 Water

09/18/2007 1510 09/20/2007 1347PIN21-0505-N001660-18419-21 Water

09/18/2007 1530 09/20/2007 1347PIN21-0504-N001660-18419-22 Water

09/19/2007 0820 09/20/2007 1347PIN12-0513-N001660-18419-23 Water

09/19/2007 0910 09/20/2007 1347PIN12-0514-N001660-18419-24 Water

09/19/2007 1200 09/20/2007 1347PIN12-S68C-N001660-18419-25 Water

09/19/2007 1225 09/20/2007 1347PIN12-S68D-N001660-18419-26 Water

09/19/2007 1220 09/20/2007 1347PIN24-0504660-18419-27 Water

09/18/2007 0809 09/20/2007 1347PIN24-0702660-18419-28 Water

09/18/2007 0833 09/20/2007 1347PIN15-0506-N001660-18419-29 Water

09/18/2007 0851 09/20/2007 1347PIN15-0507-N001660-18419-30 Water

09/18/2007 0912 09/20/2007 1347PIN15-0520-N001660-18419-31 Water

09/18/2007 0931 09/20/2007 1347PIN15-0534-N001660-18419-32 Water

09/18/2007 0957 09/20/2007 1347PIN15-0518-N001660-18419-33 Water

09/18/2007 1031 09/20/2007 1347PIN15-M24D-N001660-18419-34 Water

09/18/2007 1051 09/20/2007 1347PIN15-M33D-N001660-18419-35 Water

09/18/2007 1337 09/20/2007 1347PIN15-0562-N001660-18419-36 Water

09/18/2007 1355 09/20/2007 1347PIN15-0563-N001660-18419-37 Water

09/18/2007 1425 09/20/2007 1347PIN15-M14S-N001660-18419-38 Water

09/18/2007 1446 09/20/2007 1347PIN15-M14D-N001660-18419-39 Water

09/19/2007 0825 09/20/2007 1347PIN15-0559-N001660-18419-40 Water

09/19/2007 1250 09/20/2007 1347PIN12-S68B-N001660-18419-41 Water

09/19/2007 1325 09/20/2007 1347PIN21-0512-N001660-18419-42 Water

09/19/2007 1355 09/20/2007 1347PIN12-0526-N001660-18419-43 Water

09/19/2007 1420 09/20/2007 1347PIN21-0502-N001660-18419-44 Water

09/19/2007 1445 09/20/2007 1347PIN21-0503-N001660-18419-45 Water

09/20/2007 0900 09/20/2007 1347PIN12-S69B-N001660-18419-46 Water

TestAmerica Tampa

10/03/2007Page 13 of 107

Page 228: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

SAMPLE SUMMARY

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

09/20/2007 1000 09/20/2007 1347PIN12-S69C-N001660-18419-47 Water

09/20/2007 1030 09/20/2007 1347PIN12-S69D-N001660-18419-48 Water

09/19/2007 0854 09/20/2007 1347PIN15-0571-N001660-18419-49 Water

09/19/2007 0919 09/20/2007 1347PIN15-0572-N001660-18419-50 Water

09/19/2007 0947 09/20/2007 1347PIN15-0570-N001660-18419-51 Water

09/19/2007 1006 09/20/2007 1347PIN15-0510-N001660-18419-52 Water

09/19/2007 1028 09/20/2007 1347PIN24-0506660-18419-53 Water

09/19/2007 1041 09/20/2007 1347PIN24-0507660-18419-54 Water

09/19/2007 1045 09/20/2007 1347PIN15-0568-N001660-18419-55 Water

09/19/2007 1111 09/20/2007 1347PIN15-0569-N001660-18419-56 Water

09/19/2007 1335 09/20/2007 1347PIN12-S71B-N001660-18419-57 Water

09/19/2007 1448 09/20/2007 1347PIN12-S71C-N001660-18419-58 Water

09/19/2007 1511 09/20/2007 1347PIN12-S71D-N001660-18419-59 Water

09/20/2007 0837 09/20/2007 1347PIN12-S70B-N001660-18419-60 Water

09/20/2007 0913 09/20/2007 1347PIN12-S70C-N001660-18419-61 Water

09/20/2007 0943 09/20/2007 1347PIN12-S70D-N001660-18419-62 Water

TestAmerica Tampa

10/03/2007Page 14 of 107

Page 229: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0603

09/18/2007 0840

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-1

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1641

10/01/2007 1641

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0118.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

86 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 15 of 107

Page 230: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0520-N001

09/18/2007 0923

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-2

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1706

10/01/2007 1706

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0119.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

83 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 16 of 107

Page 231: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN06-0500-N001

09/18/2007 0952

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-3

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1731

10/01/2007 1731

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0120.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

80 74 - 1264-Bromofluorobenzene100 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 17 of 107

Page 232: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN06-0501-N001

09/18/2007 1026

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-4

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1756

10/01/2007 1756

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0121.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

89 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 18 of 107

Page 233: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0523-N001

09/18/2007 1344

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-5

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1820

10/01/2007 1820

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0122.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform32 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene22 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane1.0 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane20 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

87 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 19 of 107

Page 234: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0522-N001

09/18/2007 1412

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-6

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1845

10/01/2007 1845

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0123.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

76 74 - 1264-Bromofluorobenzene97 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 20 of 107

Page 235: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0510-N001

09/18/2007 1537

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-7

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1910

10/01/2007 1910

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0124.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

80 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 21 of 107

Page 236: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0509-N001

09/18/2007 1616

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-8

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1935

10/01/2007 1935

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0125.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

82 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 22 of 107

Page 237: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S72B-N001

09/19/2007 0948

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-9

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 2000

10/01/2007 2000

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0126.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

96 74 - 1264-Bromofluorobenzene127 77 - 122*Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 23 of 107

Page 238: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S72C-N001

09/19/2007 1025

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-10

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 2025

10/01/2007 2025

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0127.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.6 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

87 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 24 of 107

Page 239: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S72D-N001

09/19/2007 1100

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-11

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 2049

10/01/2007 2049

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0128.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

79 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 25 of 107

Page 240: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S73D-N001

09/19/2007 1407

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-12

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 2114

10/01/2007 2114

1.0

8260B Analysis Batch: 660-51222

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0129.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

76 74 - 1264-Bromofluorobenzene96 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 26 of 107

Page 241: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S73C-N001

09/19/2007 1434

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-13

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/02/2007 0059

10/02/2007 0059

1.0

8260B Analysis Batch: 660-51271

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0138.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene3.9 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane18 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

80 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 27 of 107

Page 242: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S73B-N001

09/19/2007 1506

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-14

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/02/2007 0124

10/02/2007 0124

1.0

8260B Analysis Batch: 660-51271

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0139.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

85 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 28 of 107

Page 243: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0802

09/18/2007 0835

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-15

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/02/2007 0149

10/02/2007 0149

1.0

8260B Analysis Batch: 660-51271

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMG GC/MS

1GJ0140.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

91 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 29 of 107

Page 244: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0517-N001

09/18/2007 1030

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-16

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 2105

09/28/2007 2105

1.0

8260B Analysis Batch: 660-51133

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2827.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

108 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 30 of 107

Page 245: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0518-N001

09/18/2007 1050

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-17

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/28/2007 2130

09/28/2007 2130

1.0

8260B Analysis Batch: 660-51133

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2828.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.9 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

106 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 31 of 107

Page 246: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0525-N001

09/18/2007 1350

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-18

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/02/2007 1457

10/02/2007 1457

1.0

8260B Analysis Batch: 660-51287

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0211.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform1.6 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.66 J 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

83 74 - 1264-Bromofluorobenzene90 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 32 of 107

Page 247: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0503

09/18/2007 1400

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-19

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/02/2007 1612

10/02/2007 1612

20

8260B Analysis Batch: 660-51287

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0214.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

10 U 2010Benzene7.0 U 207.0Bromodichloromethane12 U 2012Bromoform8.4 U 208.4Carbon tetrachloride13 U 2013Chlorobenzene50 U 10050Chloroethane18 U 2018Chloroform770 2013cis-1,2-Dichloroethylene2.8 U 202.8cis-1,3-Dichloropropene6.8 U 206.8Dibromochloromethane52 209.01,1-Dichlorethylene50 U 10050Dichlorodifluoromethane10 U 20101,1-Dichloroethane11 U 20111,2-Dichloroethane10 U 20101,2-Dichloropropane8.8 U 208.8Ethylbenzene13 U 2013m-Dichlorobenzene50 U 10050Methyl bromide20 U 8020Methyl chloride80 U 10080Methylene Chloride8.8 U 208.8Methyl tert-butyl ether12 U 4012m,p-Xylene8.8 U 208.8o-Dichlorobenzene10 U 2010o-Xylene10 U 2010p-Dichlorobenzene3.0 U 203.01,1,2,2-Tetrachloroethane10 U 2010Tetrachloroethylene10 U 2010Toluene14 J 208.8trans-1,2-Dichloroethylene2.8 U 202.8trans-1,3-Dichloropropene9.2 U 209.21,1,1-Trichloroethane9.4 U 209.41,1,2-Trichloroethane10 U 2010Trichloroethylene50 U 10050Trichlorofluoromethane1700 2010Vinyl chloride

Surrogate %Rec Acceptance Limits

98 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 33 of 107

Page 248: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0524-N001

09/18/2007 1425

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-20

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0506

09/30/2007 0506

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2941.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.70 J 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane29 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.3 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene10 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane4.3 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane

Surrogate %Rec Acceptance Limits

79 74 - 1264-Bromofluorobenzene86 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 34 of 107

Page 249: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0524-N001

09/18/2007 1425

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-20

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/02/2007 1637

10/02/2007 1637

20

8260B Analysis Batch: 660-51287

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0215.D

5 mL

5 mL

5030B

Run Type: DL

Analyte Result (ug/L) PQLMDLQualifier

770 2013cis-1,2-Dichloroethylene1600 2010Vinyl chloride

TestAmerica Tampa 10/03/2007Page 35 of 107

Page 250: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN21-0505-N001

09/18/2007 1510

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-21

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0531

09/30/2007 0531

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2942.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.2 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

97 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 36 of 107

Page 251: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN21-0504-N001

09/18/2007 1530

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-22

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0556

09/30/2007 0556

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2943.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

91 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 37 of 107

Page 252: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0513-N001

09/19/2007 0820

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-23

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0620

09/30/2007 0620

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2944.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane9.4 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.59 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

100 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 38 of 107

Page 253: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0514-N001

09/19/2007 0910

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-24

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0645

09/30/2007 0645

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2945.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform5.8 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane8.5 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene15 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane42 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

93 74 - 1264-Bromofluorobenzene108 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 39 of 107

Page 254: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S68C-N001

09/19/2007 1200

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-25

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0710

09/30/2007 0710

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2946.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform4.2 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane5.1 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane10 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

102 74 - 1264-Bromofluorobenzene121 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 40 of 107

Page 255: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S68D-N001

09/19/2007 1225

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-26

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0735

09/30/2007 0735

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2947.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform56 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.0 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane5.3 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene1.1 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane80 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

87 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 41 of 107

Page 256: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0504

09/19/2007 1220

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-27

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0800

09/30/2007 0800

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2948.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform64 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.1 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane6.0 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene1.2 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane91 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

99 74 - 1264-Bromofluorobenzene120 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 42 of 107

Page 257: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0702

09/18/2007 0809

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-28

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0825

09/30/2007 0825

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2949.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

83 74 - 1264-Bromofluorobenzene96 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 43 of 107

Page 258: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S68B-N001

09/19/2007 1250

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-41

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0849

09/30/2007 0849

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2950.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

96 74 - 1264-Bromofluorobenzene111 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 44 of 107

Page 259: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN21-0512-N001

09/19/2007 1325

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-42

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0914

09/30/2007 0914

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2951.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform5.9 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.6 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane14 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

89 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 45 of 107

Page 260: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-0526-N001

09/19/2007 1355

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-43

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 0939

09/30/2007 0939

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2952.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform1.9 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene1.3 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.0 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

102 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 46 of 107

Page 261: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN21-0502-N001

09/19/2007 1420

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-44

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1004

09/30/2007 1004

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2953.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

85 74 - 1264-Bromofluorobenzene97 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 47 of 107

Page 262: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN21-0503-N001

09/19/2007 1445

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-45

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1029

09/30/2007 1029

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2954.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

93 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 48 of 107

Page 263: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S69B-N001

09/20/2007 0900

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-46

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1054

09/30/2007 1054

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2955.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

87 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 49 of 107

Page 264: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S69C-N001

09/20/2007 1000

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-47

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1118

09/30/2007 1118

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2956.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.0 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

99 74 - 1264-Bromofluorobenzene115 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 50 of 107

Page 265: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S69D-N001

09/20/2007 1030

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-48

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1143

09/30/2007 1143

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2957.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.54 J 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

86 74 - 1264-Bromofluorobenzene99 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 51 of 107

Page 266: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0506

09/19/2007 1028

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-53

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1208

09/30/2007 1208

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2958.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

99 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 52 of 107

Page 267: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN24-0507

09/19/2007 1041

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-54

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

09/30/2007 1233

09/30/2007 1233

1.0

8260B Analysis Batch: 660-51224

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JI2959.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane22 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

93 74 - 1264-Bromofluorobenzene108 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 53 of 107

Page 268: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0568-N001

09/19/2007 1045

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-55

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1930

10/01/2007 1930

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0127.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

104 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 54 of 107

Page 269: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN15-0569-N001

09/19/2007 1111

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-56

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1905

10/01/2007 1905

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0126.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane21 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

95 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 55 of 107

Page 270: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S71B-N001

09/19/2007 1335

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-57

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1840

10/01/2007 1840

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0125.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

92 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 56 of 107

Page 271: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S71C-N001

09/19/2007 1448

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-58

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1815

10/01/2007 1815

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0124.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform20 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.3 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.4 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene14 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane45 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

95 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 57 of 107

Page 272: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S71D-N001

09/19/2007 1511

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-59

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1751

10/01/2007 1751

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0123.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform7.7 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.0 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.3 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene4.8 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane19 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

108 74 - 1264-Bromofluorobenzene121 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 58 of 107

Page 273: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S70B-N001

09/20/2007 0837

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-60

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1726

10/01/2007 1726

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0122.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform16 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.61 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane22 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

96 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 59 of 107

Page 274: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S70C-N001

09/20/2007 0913

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-61

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1701

10/01/2007 1701

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0121.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform25 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.5 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane8.5 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene11 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane35 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

94 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 60 of 107

Page 275: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID:

Lab Sample ID: Date Sampled:

Date Received:

PIN12-S70D-N001

09/20/2007 0943

09/20/2007 1347Client Matrix:

8260B Volatile Organic Compounds by GC/MS

660-18419-62

Water

Date Prepared:

Date Analyzed:

Dilution:

Preparation:

Method:

10/01/2007 1607

10/01/2007 1607

1.0

8260B Analysis Batch: 660-51221

Final Weight/Volume:

Initial Weight/Volume:

Lab File ID:

Instrument ID: BVMJ GC/MS

1JJ0119.D

5 mL

5 mL

5030B

Analyte Result (ug/L) PQLMDLQualifier

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform17 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.6 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane6.1 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene7.4 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane19 1.00.50Vinyl chloride

Surrogate %Rec Acceptance Limits

107 74 - 1264-Bromofluorobenzene122 77 - 122Toluene-d8 (Surr)

TestAmerica Tampa 10/03/2007Page 61 of 107

Page 276: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN06-0501-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1026

09/20/2007 1347

660-18419-4

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1412

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.020 0.0100.0048Arsenic

TestAmerica Tampa 10/03/2007Page 62 of 107

Page 277: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN12-0525-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1350

09/20/2007 1347

660-18419-18

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1419

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.026 0.0100.0048Arsenic

TestAmerica Tampa 10/03/2007Page 63 of 107

Page 278: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0506-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 0833

09/20/2007 1347

660-18419-29

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1425

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

3.8 0.200.070Aluminum2.0 0.0500.022Iron0.010 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 64 of 107

Page 279: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0507-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 0851

09/20/2007 1347

660-18419-30

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1430

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

1.7 0.200.070Aluminum1.1 0.0500.022Iron0.017 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 65 of 107

Page 280: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0520-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 0912

09/20/2007 1347

660-18419-31

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1436

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.15 B 0.200.070Aluminum0.76 0.0500.022Iron0.018 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 66 of 107

Page 281: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0534-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 0931

09/20/2007 1347

660-18419-32

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1442

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

1.9 0.200.070Aluminum0.65 0.0500.022Iron0.019 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 67 of 107

Page 282: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0518-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 0957

09/20/2007 1347

660-18419-33

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1448

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.98 0.200.070Aluminum1.0 0.0500.022Iron0.011 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 68 of 107

Page 283: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-M24D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1031

09/20/2007 1347

660-18419-34

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1454

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

8.6 0.200.070Aluminum1.1 0.0500.022Iron0.014 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 69 of 107

Page 284: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-M33D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1051

09/20/2007 1347

660-18419-35

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1512

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

6.9 0.200.070Aluminum2.0 0.0500.022Iron0.014 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 70 of 107

Page 285: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0562-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1337

09/20/2007 1347

660-18419-36

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1342

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

1.2 N 0.200.070Aluminum4.9 0.0500.022Iron0.0096 B 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 71 of 107

Page 286: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0563-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1355

09/20/2007 1347

660-18419-37

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1517

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.35 0.200.070Aluminum8.6 0.0500.022Iron0.072 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 72 of 107

Page 287: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-M14S-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1425

09/20/2007 1347

660-18419-38

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1523

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.31 0.200.070Aluminum0.074 0.0100.0048Arsenic13 0.0500.022Iron0.013 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 73 of 107

Page 288: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-M14D-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/18/2007 1446

09/20/2007 1347

660-18419-39

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1529

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

6.1 0.200.070Aluminum5.8 0.0500.022Iron0.0079 B 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 74 of 107

Page 289: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0559-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 0825

09/20/2007 1347

660-18419-40

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1535

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

1.8 0.200.070Aluminum0.44 0.0500.022Iron0.0071 B 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 75 of 107

Page 290: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN12-S68B-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 1250

09/20/2007 1347

660-18419-41

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1541

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.060 0.0100.0048Arsenic

TestAmerica Tampa 10/03/2007Page 76 of 107

Page 291: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0571-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 0854

09/20/2007 1347

660-18419-49

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1547

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

1.1 0.200.070Aluminum3.4 0.0500.022Iron0.010 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 77 of 107

Page 292: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0572-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 0919

09/20/2007 1347

660-18419-50

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1553

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

2.3 0.200.070Aluminum0.96 0.0500.022Iron0.010 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 78 of 107

Page 293: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0570-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 0947

09/20/2007 1347

660-18419-51

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1559

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

9.4 0.200.070Aluminum1.6 0.0500.022Iron0.024 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 79 of 107

Page 294: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0510-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 1006

09/20/2007 1347

660-18419-52

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1604

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

0.32 0.200.070Aluminum4.6 0.0500.022Iron0.032 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 80 of 107

Page 295: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN24-0506

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 1028

09/20/2007 1347

660-18419-53

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/24/2007 1622

09/24/2007 0633

TJA ICP TRACE

7I24A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50801

3005A Prep Batch: 660-50787

1.8 0.200.070Aluminum1.2 0.0500.022Iron0.0060 B 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 81 of 107

Page 296: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN24-0507

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 1041

09/20/2007 1347

660-18419-54

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/26/2007 1452

09/26/2007 0901

TJA ICP TRACE

7I26A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50976

3005A Prep Batch: 660-50939

1.4 0.200.070Aluminum3.2 0.0500.022Iron0.018 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 82 of 107

Page 297: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0568-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 1045

09/20/2007 1347

660-18419-55

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/26/2007 1458

09/26/2007 0901

TJA ICP TRACE

7I26A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50976

3005A Prep Batch: 660-50939

0.94 0.200.070Aluminum1.2 0.0500.022Iron0.0058 B 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 83 of 107

Page 298: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Analytical Data

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Client Sample ID: PIN15-0569-N001

Lab Sample ID:

Client Matrix:

Date Sampled:

Date Received:

09/19/2007 1111

09/20/2007 1347

660-18419-56

Water

6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable

Method:

Preparation:

Dilution:

Date Analyzed:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:09/26/2007 1504

09/26/2007 0901

TJA ICP TRACE

7I26A

50 mL

50 mL

Analyte Result (mg/L) Qualifier MDL PQL

1.0

6010B Analysis Batch: 660-50976

3005A Prep Batch: 660-50939

1.5 0.200.070Aluminum3.2 0.0500.022Iron0.018 0.0100.0014Manganese

TestAmerica Tampa 10/03/2007Page 84 of 107

Page 299: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

DATA REPORTING QUALIFIERS

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Lab Section Qualifier Description

GC/MS VOA

Analyzed for but not detected.U

Indicates an estimated value.J

Surrogate exceeds the control limit*

Metals

Indicates analyzed for but not detected.U

Spiked sample recovery is not within control limits.N

Value less than contract required detection limit but greater than or equal to the Method Detection Limit

B

TestAmerica Tampa

10/03/2007Page 85 of 107

Page 300: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/28/2007 1313

Method Blank - Batch: 660-51133

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51133

Prep Batch: N/A

09/28/2007 1313

1JI2808.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMJ GC/MSMB 660-51133/2

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 90 74 - 126Toluene-d8 (Surr) 101 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 86 of 107

Page 301: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/28/2007 1248

09/28/2007 1428

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51133

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/28/2007 1248

Prep Batch: N/A

Analysis Batch: 660-51133

1JI2807.D

5 mL

5 mL

1JI2811.D

5 mL

5 mL

ug/L

09/28/2007 1428

Analysis Batch: 660-51133

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMJ GC/MS

BVMJ GC/MS

LCS 660-51133/1

LCSD 660-51133/4

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

10698 62 - 135 8 37Benzene

10795 72 - 127 12 22Chlorobenzene

9286 46 - 147 7 301,1-Dichlorethylene

118105 68 - 131 12 33Toluene

10091 56 - 143 9 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 87 of 107

Page 302: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

10/01/2007 1004

Method Blank - Batch: 660-51221

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51221

Prep Batch: N/A

10/01/2007 1004

1JJ0105.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMJ GC/MSMB 660-51221/1

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 96 74 - 126Toluene-d8 (Surr) 110 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 88 of 107

Page 303: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

10/01/2007 1029

10/01/2007 1054

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51221

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

10/01/2007 1029

Prep Batch: N/A

Analysis Batch: 660-51221

1JJ0106.D

5 mL

5 mL

1JJ0107.D

5 mL

5 mL

ug/L

10/01/2007 1054

Analysis Batch: 660-51221

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMJ GC/MS

BVMJ GC/MS

LCS 660-51221/2

LCSD 660-51221/3

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

112125 62 - 135 12 37Benzene

106116 72 - 127 8 22Chlorobenzene

98110 46 - 147 12 301,1-Dichlorethylene

120130 68 - 131 8 33Toluene

103116 56 - 143 12 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 89 of 107

Page 304: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

10/01/2007 1233

Method Blank - Batch: 660-51222

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51222

Prep Batch: N/A

10/01/2007 1233

1GJ0108.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMG GC/MSMB 660-51222/2

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 87 74 - 126Toluene-d8 (Surr) 102 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 90 of 107

Page 305: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

10/01/2007 1143

10/01/2007 1322

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51222

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

10/01/2007 1143

Prep Batch: N/A

Analysis Batch: 660-51222

1GJ0106.D

5 mL

5 mL

1GJ0110.D

5 mL

5 mL

ug/L

10/01/2007 1322

Analysis Batch: 660-51222

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMG GC/MS

BVMG GC/MS

LCS 660-51222/1

LCSD 660-51222/4

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

10692 62 - 135 14 37Benzene

10492 72 - 127 13 22Chlorobenzene

10690 46 - 147 16 301,1-Dichlorethylene

10187 68 - 131 15 33Toluene

10590 56 - 143 15 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 91 of 107

Page 306: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/30/2007 0351

Method Blank - Batch: 660-51224

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51224

Prep Batch: N/A

09/30/2007 0351

1JI2938.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMJ GC/MSMB 660-51224/3

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 89 74 - 126Toluene-d8 (Surr) 100 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 92 of 107

Page 307: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/30/2007 0302

09/30/2007 0327

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51224

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

09/30/2007 0302

Prep Batch: N/A

Analysis Batch: 660-51224

1JI2936.D

5 mL

5 mL

1JI2937.D

5 mL

5 mL

ug/L

09/30/2007 0327

Analysis Batch: 660-51224

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMJ GC/MS

BVMJ GC/MS

LCS 660-51224/1

LCSD 660-51224/2

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

121110 62 - 135 9 37Benzene

116106 72 - 127 9 22Chlorobenzene

10497 46 - 147 7 301,1-Dichlorethylene

126116 68 - 131 8 33Toluene

107104 56 - 143 3 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 93 of 107

Page 308: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

10/01/2007 2344

Method Blank - Batch: 660-51271

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51271

Prep Batch: N/A

10/01/2007 2344

1GJ0135.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMG GC/MSMB 660-51271/1

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 78 74 - 126Toluene-d8 (Surr) 98 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 94 of 107

Page 309: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

10/02/2007 0009

10/02/2007 0034

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51271

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

10/02/2007 0009

Prep Batch: N/A

Analysis Batch: 660-51271

1GJ0136.D

5 mL

5 mL

1GJ0137.D

5 mL

5 mL

ug/L

10/02/2007 0034

Analysis Batch: 660-51271

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMG GC/MS

BVMG GC/MS

LCS 660-51271/2

LCSD 660-51271/3

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

108101 62 - 135 7 37Benzene

10096 72 - 127 4 22Chlorobenzene

108100 46 - 147 8 301,1-Dichlorethylene

9995 68 - 131 4 33Toluene

10399 56 - 143 4 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 95 of 107

Page 310: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

10/02/2007 1408

Method Blank - Batch: 660-51287

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-51287

Prep Batch: N/A

10/02/2007 1408

1JJ0209.D

5 mL

5 mL

Units: ug/L

Method: 8260BPreparation: 5030B

BVMJ GC/MSMB 660-51287/2

Analyte Result Qual MDL PQL

0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride

Surrogate % Rec Acceptance Limits

4-Bromofluorobenzene 90 74 - 126Toluene-d8 (Surr) 97 77 - 122

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 96 of 107

Page 311: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

10/02/2007 1343

10/02/2007 1433

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51287

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

ug/L

10/02/2007 1343

Prep Batch: N/A

Analysis Batch: 660-51287

1JJ0208.D

5 mL

5 mL

1JJ0210.D

5 mL

5 mL

ug/L

10/02/2007 1433

Analysis Batch: 660-51287

Prep Batch: N/A

Method: 8260BPreparation: 5030B

BVMJ GC/MS

BVMJ GC/MS

LCS 660-51287/1

LCSD 660-51287/3

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

107101 62 - 135 6 37Benzene

109103 72 - 127 6 22Chlorobenzene

9691 46 - 147 5 301,1-Dichlorethylene

119112 68 - 131 6 33Toluene

9992 56 - 143 8 35Trichloroethylene

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 97 of 107

Page 312: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/24/2007 1317

Method Blank - Batch: 660-50787

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50801

Prep Batch: 660-50787

09/24/2007 0633

7I24A

50 mL

50 mL

Units: mg/L

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACEMB 660-50787/1-A

Analyte Result Qual MDL PQL

0.070 U 0.200.070Aluminum0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/24/2007 1325

09/24/2007 1331

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50787

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L

09/24/2007 0633

Prep Batch: 660-50787

Analysis Batch: 660-50801

7I24A

50 mL

50 mL

7I24A

50 mL

50 mL

mg/L

09/24/2007 0633

Analysis Batch: 660-50801

Prep Batch: 660-50787

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACE

TJA ICP TRACE

LCS 660-50787/2-A

LCSD 660-50787/3-A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

106105 75 - 125 1 20Aluminum

103101 75 - 125 2 20Arsenic

105103 75 - 125 2 20Iron

103101 75 - 125 2 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 98 of 107

Page 313: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/24/2007 1400

09/24/2007 1406

Water

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50787

1.0

1.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Analysis Batch: 660-50801

Analysis Batch: 660-50801

09/24/2007 0633

09/24/2007 0633

Prep Batch: 660-50787

Prep Batch: 660-50787

7I24A

50 mL

50 mL

7I24A

50 mL

50 mL

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACE

TJA ICP TRACE

660-18419-36

660-18419-36

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

142 135 75 - 125 3 20 N NAluminum

104 103 75 - 125 1 20Arsenic

116 103 75 - 125 2 20Iron

101 100 75 - 125 1 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 99 of 107

Page 314: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Quality Control Results

Job Number: 660-18419-1Client: S.M. Stoller Corporation

WaterClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

09/26/2007 1322

Method Blank - Batch: 660-50939

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Analysis Batch: 660-50976

Prep Batch: 660-50939

09/26/2007 0901

7I26A

50 mL

50 mL

Units: mg/L

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACEMB 660-50939/1-A

Analyte Result Qual MDL PQL

0.070 U 0.200.070Aluminum0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese

Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

09/26/2007 1328

09/26/2007 1334

Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50939

1.0

1.0

Water

LCS Lab Sample ID:

LCSD Lab Sample ID:

Client Matrix:

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Water

Date Prepared:

Units:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

mg/L

09/26/2007 0901

Prep Batch: 660-50939

Analysis Batch: 660-50976

7I26A

50 mL

50 mL

7I26A

50 mL

50 mL

mg/L

09/26/2007 0901

Analysis Batch: 660-50976

Prep Batch: 660-50939

Method: 6010BPreparation: 3005ATotal Recoverable

TJA ICP TRACE

TJA ICP TRACE

LCS 660-50939/2-A

LCSD 660-50939/3-A

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

% Rec.

102103 75 - 125 1 20Aluminum

100102 75 - 125 1 20Iron

9898 75 - 125 0 20Manganese

TestAmerica Tampa

Calculations are performed before rounding to avoid round-off errors in calculated results.

10/03/2007Page 100 of 107

Page 315: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007

Page 101 of 107

Page 316: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007

Page 102 of 107

Page 317: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007

Page 103 of 107

Page 318: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007

Page 104 of 107

Page 319: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007

Page 105 of 107

Page 320: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

10/03/2007

Page 106 of 107

Page 321: ANALYTICAL REPORTBenzene 3.2 1.0ug/L8260B cis-1,2-Dichloroethylene 120 1.0ug/L8260B Vinyl chloride 450M10ug/L8260B Total Recoverable Iron 3.2 0.050mg/L6010B Manganese 0.011 0.010mg/L6010B

Login Sample Receipt Check List

Client: S.M. Stoller Corporation Job Number: 660-18419-1

Login Number: 18419

Question T / F/ NA Comment

Creator: Atkins, Amy

List Source: TestAmerica Tampa

List Number: 1

Radioactivity either was not measured or, if measured, is at or below background

N/A

The cooler's custody seal, if present, is intact. N/A

The cooler or samples do not appear to have been compromised or tampered with.

True

Samples were received on ice. True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

True

If necessary, staff have been informed of any short hold time or quick TAT needs

True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

TestAmerica Tampa 10/03/2007Page 107 of 107