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ANALYTICAL REPORT
Job Number: 660-18295-1
Job Description: Star Center
For:S.M. Stoller Corporation
2597 B 3/4 RoadGrand Junction, CO 81503
Attention: Mr. Charles Tabor
_____________________________________________
Nancy RobertsonProject Manager II
[email protected]/26/2007Revision: 1
Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements ofNELAC unless specified in the case narrative. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reportedresults is available upon request. The results contained in this test report relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
10/26/2007Page 1 of 113
10/26/2007Page 2 of 113
10/26/2007Page 3 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-2 PIN20-M056-N001
1.0 ug/L 8260B4.0cis-1,2-Dichloroethylene1.0 ug/L 8260B7.3Vinyl chloride
660-18295-3 PIN20-M053-N001
1.0 ug/L 8260B11cis-1,2-Dichloroethylene1.0 ug/L 8260B3.4Vinyl chloride
660-18295-4 PIN20-M057-N001
1.0 ug/L 8260B18cis-1,2-Dichloroethylene1.0 ug/L 8260B5.3Vinyl chloride
660-18295-7 PIN20-M18D-N001
1.0 ug/L 8260B13cis-1,2-Dichloroethylene1.0 ug/L 8260B0.74 Jtrans-1,2-Dichloroethylene1.0 ug/L 8260B10Vinyl chloride
660-18295-8 PIN20-M058-N001
1.0 ug/L 8260B3.3Vinyl chloride
660-18295-9 PIN20-M019-N001
1.0 ug/L 8260B0.81 JVinyl chloride
660-18295-10 PIN20-M059-N001
1.0 ug/L 8260B9.5Vinyl chloride
660-18295-11 PIN20-M22D-N001
1.0 ug/L 8260B1.4Vinyl chloride
660-18295-15 PIN15-M03S-N001
Total Recoverable0.20 mg/L 6010B5.1Aluminum0.010 mg/L 6010B0.075Arsenic0.050 mg/L 6010B41Iron0.010 mg/L 6010B0.054Manganese
TestAmerica Tampa
10/26/2007Page 4 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-16 PIN15-M03D-N001
Total Recoverable0.20 mg/L 6010B4.2Aluminum0.050 mg/L 6010B6.5Iron0.010 mg/L 6010B0.0049 BManganese
660-18295-17 PIN15-M16D-N001
Total Recoverable0.20 mg/L 6010B0.47Aluminum0.050 mg/L 6010B3.0Iron0.010 mg/L 6010B0.0042 BManganese
660-18295-18 PIN15-M16S-N001
Total Recoverable0.20 mg/L 6010B1.4Aluminum0.050 mg/L 6010B3.5Iron0.010 mg/L 6010B0.034Manganese
660-18295-19 PIN15-0584-N001
1.0 ug/L 8260B1.8Vinyl chloride
Total Recoverable0.20 mg/L 6010B67Aluminum0.050 mg/L 6010B38Iron0.010 mg/L 6010B0.046Manganese
660-18295-20 PIN15-0537-N001
1.0 ug/L 8260B3.2Benzene1.0 ug/L 8260B120cis-1,2-Dichloroethylene10 ug/L 8260B450 MVinyl chloride
Total Recoverable0.050 mg/L 6010B3.2Iron0.010 mg/L 6010B0.011Manganese
660-18295-21 PIN15-RW16-N001
Total Recoverable0.050 mg/L 6010B3.9Iron0.010 mg/L 6010B0.017Manganese
TestAmerica Tampa
10/26/2007Page 5 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-22 PIN15-M32S-N001
Total Recoverable0.20 mg/L 6010B0.60Aluminum0.010 mg/L 6010B0.018Arsenic0.050 mg/L 6010B3.6Iron0.010 mg/L 6010B0.082Manganese
660-18295-23 PIN15-M32D-N001
Total Recoverable0.20 mg/L 6010B0.23Aluminum0.050 mg/L 6010B5.3Iron0.010 mg/L 6010B0.0096 BManganese
660-18295-24 PIN15-0592-N001
1.0 ug/L 8260B29Benzene1.0 ug/L 8260B1.1Ethylbenzene2.0 ug/L 8260B2.0m,p-Xylene1.0 ug/L 8260B0.94 JToluene
Total Recoverable0.20 mg/L 6010B27Aluminum0.050 mg/L 6010B17Iron0.010 mg/L 6010B0.036Manganese
660-18295-25 PIN15-0515-N001
Total Recoverable0.20 mg/L 6010B0.081 BAluminum0.050 mg/L 6010B1.0Iron0.010 mg/L 6010B0.010Manganese
660-18295-26 PIN15-0514-N001
Total Recoverable0.20 mg/L 6010B2.3Aluminum0.050 mg/L 6010B1.7Iron0.010 mg/L 6010B0.0097 BManganese
TestAmerica Tampa
10/26/2007Page 6 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-27 PIN15-0516-N001
Total Recoverable0.20 mg/L 6010B0.14 BAluminum0.050 mg/L 6010B6.7Iron0.010 mg/L 6010B0.029Manganese
660-18295-28 PIN15-0535-N001
Total Recoverable0.20 mg/L 6010B5.0Aluminum0.050 mg/L 6010B1.8Iron0.010 mg/L 6010B0.0099 BManganese
660-18295-29 PIN15-0530-N001
Total Recoverable0.20 mg/L 6010B1.1Aluminum0.050 mg/L 6010B2.3Iron0.010 mg/L 6010B0.034Manganese
660-18295-30 PIN15-M27D-N001
Total Recoverable0.20 mg/L 6010B0.69Aluminum0.050 mg/L 6010B0.90Iron0.010 mg/L 6010B0.0098 BManganese
660-18295-31 PIN15-M27S-N001
Total Recoverable0.050 mg/L 6010B1.9Iron0.010 mg/L 6010B0.11Manganese
TestAmerica Tampa
10/26/2007Page 7 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-32 PIN15-0585-N001
1.0 ug/L 8260B0.86 JBenzene1.0 ug/L 8260B140cis-1,2-Dichloroethylene1.0 ug/L 8260B1.21,1-Dichlorethylene1.0 ug/L 8260B9.0Toluene1.0 ug/L 8260B0.92 Jtrans-1,2-Dichloroethylene2.0 ug/L 8260B180Trichloroethylene1.0 ug/L 8260B28Vinyl chloride
Total Recoverable0.20 mg/L 6010B10Aluminum0.050 mg/L 6010B6.6Iron0.010 mg/L 6010B0.016Manganese
660-18295-33 PIN15-0586-N001
5.0 ug/L 8260B3.0 JBenzene20 ug/L 8260B1400cis-1,2-Dichloroethylene5.0 ug/L 8260B6.91,1-Dichlorethylene5.0 ug/L 8260B28Toluene5.0 ug/L 8260B4.8 Jtrans-1,2-Dichloroethylene5.0 ug/L 8260B430Trichloroethylene5.0 ug/L 8260B490Vinyl chloride
Total Recoverable0.20 mg/L 6010B18Aluminum0.050 mg/L 6010B16Iron0.010 mg/L 6010B0.049Manganese
660-18295-34 PIN24-0508
5.0 ug/L 8260B3.5 JBenzene20 ug/L 8260B1300cis-1,2-Dichloroethylene5.0 ug/L 8260B6.01,1-Dichlorethylene5.0 ug/L 8260B31Toluene5.0 ug/L 8260B4.8 Jtrans-1,2-Dichloroethylene5.0 ug/L 8260B450Trichloroethylene5.0 ug/L 8260B500Vinyl chloride
Total Recoverable0.20 mg/L 6010B21Aluminum0.050 mg/L 6010B18Iron0.010 mg/L 6010B0.052Manganese
TestAmerica Tampa
10/26/2007Page 8 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-35 PIN15-0588-N001
1.0 ug/L 8260B1.8Benzene2.0 ug/L 8260B170cis-1,2-Dichloroethylene1.0 ug/L 8260B1.11,1-Dichlorethylene1.0 ug/L 8260B9.0Toluene1.0 ug/L 8260B1.1trans-1,2-Dichloroethylene1.0 ug/L 8260B1.1Trichloroethylene1.0 ug/L 8260B8.8Vinyl chloride
Total Recoverable0.20 mg/L 6010B0.84Aluminum0.050 mg/L 6010B3.3Iron0.010 mg/L 6010B0.25Manganese
660-18295-36 PIN20-M061-N001
20 ug/L 8260B1200cis-1,2-Dichloroethylene5.0 ug/L 8260B9.11,1-Dichlorethylene5.0 ug/L 8260B68trans-1,2-Dichloroethylene5.0 ug/L 8260B220Trichloroethylene5.0 ug/L 8260B330Vinyl chloride
660-18295-37 PIN20-M060-N001
2.0 ug/L 8260B28cis-1,2-Dichloroethylene2.0 ug/L 8260B20trans-1,2-Dichloroethylene20 ug/L 8260B2000 MVinyl chloride
660-18295-38 PIN24-0502
2.0 ug/L 8260B100cis-1,2-Dichloroethylene2.0 ug/L 8260B0.97 J1,1-Dichlorethylene2.0 ug/L 8260B45trans-1,2-Dichloroethylene20 ug/L 8260B2100Vinyl chloride
660-18295-39 PIN20-M049-N001
1.0 ug/L 8260B3.7cis-1,2-Dichloroethylene1.0 ug/L 8260B2.3Vinyl chloride
660-18295-43 PIN09-0500-N001
Total Recoverable0.010 mg/L 6010B0.0077 BArsenic
TestAmerica Tampa
10/26/2007Page 9 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-46 PIN12-S29C-N001
1.0 ug/L 8260B2.01,1-Dichloroethane1.0 ug/L 8260B4.8Vinyl chloride
660-18295-47 PIN12-S30B-N001
1.0 ug/L 8260B1.6Benzene50 ug/L 8260B6000cis-1,2-Dichloroethylene1.0 ug/L 8260B1201,1-Dichlorethylene1.0 ug/L 8260B9.11,1-Dichloroethane1.0 ug/L 8260B0.58 JToluene25 ug/L 8260B330trans-1,2-Dichloroethylene25 ug/L 8260B350Trichloroethylene25 ug/L 8260B2100Vinyl chloride
660-18295-48 PIN12-S32B-N001
1.0 ug/L 8260B2.61,1-Dichloroethane
Total Recoverable0.010 mg/L 6010B0.011Arsenic
660-18295-49 PIN12-S31B-N001
Total Recoverable0.010 mg/L 6010B0.018Arsenic
660-18295-50 PIN12-S37B-N001
1.0 ug/L 8260B3.7cis-1,2-Dichloroethylene5.0 ug/L 8260B9.5Dichlorodifluoromethane1.0 ug/L 8260B3.4Vinyl chloride
660-18295-51 PIN12-S33C-N001
13 ug/L 8260B1700cis-1,2-Dichloroethylene2.0 ug/L 8260B1101,1-Dichlorethylene2.0 ug/L 8260B29trans-1,2-Dichloroethylene2.0 ug/L 8260B43Trichloroethylene13 ug/L 8260B1100Vinyl chloride
Total Recoverable0.010 mg/L 6010B0.0048 BArsenic
TestAmerica Tampa
10/26/2007Page 10 of 113
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18295-52 PIN12-S35B-N001
200 ug/L 8260B14000cis-1,2-Dichloroethylene50 ug/L 8260B901,1-Dichlorethylene50 ug/L 8260B3300trans-1,2-Dichloroethylene50 ug/L 8260B7500Trichloroethylene200 ug/L 8260B9300Vinyl chloride
Total Recoverable0.010 mg/L 6010B0.017Arsenic
TestAmerica Tampa
10/26/2007Page 11 of 113
METHOD SUMMARY
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Preparation MethodMethodLab LocationDescription
Matrix: Water
SW846 8260BVolatile Organic Compounds by GC/MS TAL TAM
SW846 5030BTAL TAMPurge-and-Trap
SW846 6010BInductively Coupled Plasma - Atomic Emission Spectrometry TAL TAM
SW846 3005ATAL TAMAcid Digestion of Waters for Total Recoverable or
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Tampa
10/26/2007Page 12 of 113
METHOD / ANALYST SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Method Analyst Analyst ID
Perez, Julian JPSW846 8260B
Fox, Greg GFSW846 6010B
TestAmerica Tampa
10/26/2007Page 13 of 113
SAMPLE SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
09/12/2007 0720 09/14/2007 0900PIN24-0800660-18295-1 Water
09/12/2007 0940 09/14/2007 0900PIN20-M056-N001660-18295-2 Water
09/12/2007 1000 09/14/2007 0900PIN20-M053-N001660-18295-3 Water
09/12/2007 1020 09/14/2007 0900PIN20-M057-N001660-18295-4 Water
09/12/2007 1055 09/14/2007 0900PIN20-M005-N001660-18295-5 Water
09/12/2007 1100 09/14/2007 0900PIN20-M003-N001660-18295-6 Water
09/12/2007 1340 09/14/2007 0900PIN20-M18D-N001660-18295-7 Water
09/12/2007 1435 09/14/2007 0900PIN20-M058-N001660-18295-8 Water
09/12/2007 1510 09/14/2007 0900PIN20-M019-N001660-18295-9 Water
09/12/2007 1533 09/14/2007 0900PIN20-M059-N001660-18295-10 Water
09/13/2007 0845 09/14/2007 0900PIN20-M22D-N001660-18295-11 Water
09/13/2007 0917 09/14/2007 0900PIN20-M007-N001660-18295-12 Water
09/13/2007 0948 09/14/2007 0900PIN20-M028-N001660-18295-13 Water
09/12/2007 0840 09/14/2007 0900PIN24-0700660-18295-14 Water
09/12/2007 1002 09/14/2007 0900PIN15-M03S-N001660-18295-15 Water
09/12/2007 1031 09/14/2007 0900PIN15-M03D-N001660-18295-16 Water
09/12/2007 1059 09/14/2007 0900PIN15-M16D-N001660-18295-17 Water
09/12/2007 1121 09/14/2007 0900PIN15-M16S-N001660-18295-18 Water
09/12/2007 1314 09/14/2007 0900PIN15-0584-N001660-18295-19 Water
09/12/2007 1342 09/14/2007 0900PIN15-0537-N001660-18295-20 Water
09/12/2007 1409 09/14/2007 0900PIN15-RW16-N001660-18295-21 Water
09/12/2007 1441 09/14/2007 0900PIN15-M32S-N001660-18295-22 Water
09/12/2007 1506 09/14/2007 0900PIN15-M32D-N001660-18295-23 Water
09/13/2007 0845 09/14/2007 0900PIN15-0592-N001660-18295-24 Water
09/13/2007 0914 09/14/2007 0900PIN15-0515-N001660-18295-25 Water
09/13/2007 0933 09/14/2007 0900PIN15-0514-N001660-18295-26 Water
09/13/2007 0959 09/14/2007 0900PIN15-0516-N001660-18295-27 Water
09/13/2007 1025 09/14/2007 0900PIN15-0535-N001660-18295-28 Water
09/13/2007 1049 09/14/2007 0900PIN15-0530-N001660-18295-29 Water
09/13/2007 1121 09/14/2007 0900PIN15-M27D-N001660-18295-30 Water
09/13/2007 1141 09/14/2007 0900PIN15-M27S-N001660-18295-31 Water
09/13/2007 1350 09/14/2007 0900PIN15-0585-N001660-18295-32 Water
09/13/2007 1428 09/14/2007 0900PIN15-0586-N001660-18295-33 Water
09/13/2007 1444 09/14/2007 0900PIN24-0508660-18295-34 Water
09/13/2007 1525 09/14/2007 0900PIN15-0588-N001660-18295-35 Water
09/13/2007 1037 09/14/2007 0900PIN20-M061-N001660-18295-36 Water
09/13/2007 1305 09/14/2007 0900PIN20-M060-N001660-18295-37 Water
09/13/2007 1232 09/14/2007 0900PIN24-0502660-18295-38 Water
09/13/2007 1406 09/14/2007 0900PIN20-M049-N001660-18295-39 Water
09/13/2007 1458 09/14/2007 0900PIN20-MWL5-N001660-18295-40 Water
09/12/2007 1100 09/14/2007 0900PIN24-0600660-18295-41 Water
09/12/2007 1350 09/14/2007 0900PIN10-0500-N001660-18295-42 Water
09/12/2007 1416 09/14/2007 0900PIN09-0500-N001660-18295-43 Water
09/12/2007 1442 09/14/2007 0900PIN12-0521-N001660-18295-44 Water
09/13/2007 0851 09/14/2007 0900PIN12-S36B-N001660-18295-45 Water
09/13/2007 0919 09/14/2007 0900PIN12-S29C-N001660-18295-46 Water
TestAmerica Tampa
10/26/2007Page 14 of 113
SAMPLE SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
09/13/2007 0945 09/14/2007 0900PIN12-S30B-N001660-18295-47 Water
09/13/2007 1015 09/14/2007 0900PIN12-S32B-N001660-18295-48 Water
09/13/2007 1040 09/14/2007 0900PIN12-S31B-N001660-18295-49 Water
09/13/2007 1329 09/14/2007 0900PIN12-S37B-N001660-18295-50 Water
09/13/2007 1404 09/14/2007 0900PIN12-S33C-N001660-18295-51 Water
09/13/2007 1440 09/14/2007 0900PIN12-S35B-N001660-18295-52 Water
TestAmerica Tampa
10/26/2007Page 15 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0800
09/12/2007 0720
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-1
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/20/2007 2328
09/20/2007 2328
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2020.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
107 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 16 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M056-N001
09/12/2007 0940
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/20/2007 2349
09/20/2007 2349
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2021.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform4.0 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane7.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
100 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 17 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M053-N001
09/12/2007 1000
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0010
09/21/2007 0010
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2022.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform11 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.4 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
109 74 - 1264-Bromofluorobenzene116 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 18 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M057-N001
09/12/2007 1020
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0030
09/21/2007 0030
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2023.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform18 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane5.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
110 74 - 1264-Bromofluorobenzene119 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 19 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M005-N001
09/12/2007 1055
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-5
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0051
09/21/2007 0051
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2024.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
110 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 20 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M003-N001
09/12/2007 1100
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0112
09/21/2007 0112
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2025.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
96 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 21 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M18D-N001
09/12/2007 1340
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0132
09/21/2007 0132
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2026.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform13 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.74 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane10 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
114 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 22 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M058-N001
09/12/2007 1435
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-8
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0153
09/21/2007 0153
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2027.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
98 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 23 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M019-N001
09/12/2007 1510
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-9
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0214
09/21/2007 0214
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2028.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.81 J 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
100 74 - 1264-Bromofluorobenzene108 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 24 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M059-N001
09/12/2007 1533
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-10
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0234
09/21/2007 0234
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2029.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane9.5 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
105 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 25 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M22D-N001
09/13/2007 0845
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-11
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0255
09/21/2007 0255
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2030.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.4 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
108 74 - 1264-Bromofluorobenzene116 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 26 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M007-N001
09/13/2007 0917
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-12
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0316
09/21/2007 0316
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2031.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
110 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 27 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M028-N001
09/13/2007 0948
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-13
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0336
09/21/2007 0336
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2032.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
109 74 - 1264-Bromofluorobenzene116 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 28 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0700
09/12/2007 0840
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-14
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0357
09/21/2007 0357
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2033.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
100 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 29 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0584-N001
09/12/2007 1314
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-19
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0418
09/21/2007 0418
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2034.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.8 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
98 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 30 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0537-N001
09/12/2007 1342
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-20
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0438
09/21/2007 0438
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2035.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
3.2 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform120 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
110 74 - 1264-Bromofluorobenzene119 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 31 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0537-N001
09/12/2007 1342
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-20
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0101
09/24/2007 0101
10
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2322.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
450 M 105.0Vinyl chloride
TestAmerica Tampa 10/26/2007Page 32 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0592-N001
09/13/2007 0845
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-24
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/21/2007 0459
09/21/2007 0459
1.0
8260B Analysis Batch: 660-50786
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2036.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
29 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane1.1 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether2.0 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.94 J 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
105 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 33 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0585-N001
09/13/2007 1350
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-32
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0020
09/24/2007 0020
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2320.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.86 J 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform140 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.2 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene9.0 1.00.51Toluene0.92 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane2.5 U 5.02.5Trichlorofluoromethane28 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
120 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 34 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0585-N001
09/13/2007 1350
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-32
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 0049
09/25/2007 0049
2.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2427.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
180 2.01.0Trichloroethylene
TestAmerica Tampa 10/26/2007Page 35 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0586-N001
09/13/2007 1428
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-33
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 0130
09/25/2007 0130
5.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2429.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
3.0 J 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.8 U 254.82-Chloroethyl vinyl ether4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane6.9 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene28 5.02.6Toluene4.8 J 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane430 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane490 5.02.5Vinyl chloride5.0 U 205.0Methyl chloride
Surrogate %Rec Acceptance Limits
101 74 - 1264-Bromofluorobenzene90 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 36 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0586-N001
09/13/2007 1428
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-33
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0122
09/24/2007 0122
20
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2323.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
1400 2013cis-1,2-Dichloroethylene
TestAmerica Tampa 10/26/2007Page 37 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0508
09/13/2007 1444
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-34
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 0151
09/25/2007 0151
5.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2430.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
3.5 J 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.8 U 254.82-Chloroethyl vinyl ether4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane6.0 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene31 5.02.6Toluene4.8 J 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane450 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane500 5.02.5Vinyl chloride5.0 U 205.0Methyl chloride
Surrogate %Rec Acceptance Limits
108 74 - 1264-Bromofluorobenzene97 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 38 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0508
09/13/2007 1444
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-34
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0143
09/24/2007 0143
20
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2324.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
1300 2013cis-1,2-Dichloroethylene
TestAmerica Tampa 10/26/2007Page 39 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0588-N001
09/13/2007 1525
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-35
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0040
09/24/2007 0040
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2321.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.8 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.1 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene9.0 1.00.51Toluene1.1 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane1.1 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane8.8 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
113 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 40 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0588-N001
09/13/2007 1525
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-35
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 0109
09/25/2007 0109
2.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2428.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
170 2.01.3cis-1,2-Dichloroethylene
TestAmerica Tampa 10/26/2007Page 41 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M061-N001
09/13/2007 1037
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-36
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 0211
09/25/2007 0211
5.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2431.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
2.5 U 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.8 U 254.82-Chloroethyl vinyl ether4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane9.1 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene2.6 U 5.02.6Toluene68 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane220 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane330 5.02.5Vinyl chloride5.0 U 205.0Methyl chloride
Surrogate %Rec Acceptance Limits
106 74 - 1264-Bromofluorobenzene92 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 42 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M061-N001
09/13/2007 1037
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-36
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0203
09/24/2007 0203
20
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2325.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
1200 2013cis-1,2-Dichloroethylene
TestAmerica Tampa 10/26/2007Page 43 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M060-N001
09/13/2007 1305
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-37
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 1857
09/25/2007 1857
2.0
8260B Analysis Batch: 660-50904
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2529.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.0 U 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.9 U 101.92-Chloroethyl vinyl ether1.8 U 2.01.8Chloroform28 2.01.3cis-1,2-Dichloroethylene0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane0.90 U 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene1.0 U 2.01.0Toluene20 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane1.0 U 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane2.0 U 8.02.0Methyl chloride
Surrogate %Rec Acceptance Limits
113 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 44 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M060-N001
09/13/2007 1305
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-37
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0224
09/24/2007 0224
20
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2326.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
2000 M 2010Vinyl chloride
TestAmerica Tampa 10/26/2007Page 45 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0502
09/13/2007 1232
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-38
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 1918
09/25/2007 1918
2.0
8260B Analysis Batch: 660-50904
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2530.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.0 U 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.9 U 101.92-Chloroethyl vinyl ether1.8 U 2.01.8Chloroform100 2.01.3cis-1,2-Dichloroethylene0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane0.97 J 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene1.0 U 2.01.0Toluene45 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane1.0 U 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane2.0 U 8.02.0Methyl chloride
Surrogate %Rec Acceptance Limits
123 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 46 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0502
09/13/2007 1232
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-38
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0245
09/24/2007 0245
20
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2327.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
2100 2010Vinyl chloride
TestAmerica Tampa 10/26/2007Page 47 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M049-N001
09/13/2007 1406
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-39
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0305
09/24/2007 0305
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2328.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform3.7 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane2.3 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
97 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 48 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL5-N001
09/13/2007 1458
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-40
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0326
09/24/2007 0326
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2329.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
105 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 49 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0600
09/12/2007 1100
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-41
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0347
09/24/2007 0347
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2330.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
118 74 - 1264-Bromofluorobenzene112 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 50 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN10-0500-N001
09/12/2007 1350
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-42
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0407
09/24/2007 0407
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2331.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
118 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 51 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN09-0500-N001
09/12/2007 1416
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-43
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0428
09/24/2007 0428
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2332.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
102 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 52 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0521-N001
09/12/2007 1442
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-44
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0510
09/24/2007 0510
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2334.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
117 74 - 1264-Bromofluorobenzene110 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 53 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S36B-N001
09/13/2007 0851
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-45
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 1959
09/25/2007 1959
1.0
8260B Analysis Batch: 660-50904
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2532.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
107 74 - 1264-Bromofluorobenzene99 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 54 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S29C-N001
09/13/2007 0919
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-46
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 0449
09/24/2007 0449
1.0
8260B Analysis Batch: 660-50896
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2333.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.0 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane4.8 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
122 74 - 1264-Bromofluorobenzene112 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 55 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S30B-N001
09/13/2007 0945
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-47
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 1938
09/24/2007 1938
1.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2412.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.6 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane120 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane9.1 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.58 J 1.00.51Toluene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane2.5 U 5.02.5Trichlorofluoromethane1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
120 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 56 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S30B-N001
09/13/2007 0945
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-47
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 1707
09/25/2007 1707
25
8260B Analysis Batch: 660-50904
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2524.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
330 2511trans-1,2-Dichloroethylene350 2513Trichloroethylene2100 2513Vinyl chloride
TestAmerica Tampa 10/26/2007Page 57 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S30B-N001
09/13/2007 0945
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-47
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 2102
09/25/2007 2102
50
8260B Analysis Batch: 660-50904
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2535.D
5 mL
5 mL
5030B
Run Type: DL2
Analyte Result (ug/L) PQLMDLQualifier
6000 5033cis-1,2-Dichloroethylene
TestAmerica Tampa 10/26/2007Page 58 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S32B-N001
09/13/2007 1015
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-48
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 1958
09/24/2007 1958
1.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2413.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.6 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
115 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 59 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S31B-N001
09/13/2007 1040
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-49
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 2019
09/24/2007 2019
1.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2414.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
118 74 - 1264-Bromofluorobenzene111 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 60 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S37B-N001
09/13/2007 1329
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-50
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 2040
09/24/2007 2040
1.0
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2415.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform3.7 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene9.5 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.4 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate %Rec Acceptance Limits
115 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 61 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S33C-N001
09/13/2007 1404
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-51
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/25/2007 1735
09/25/2007 1735
2.0
8260B Analysis Batch: 660-50904
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2525.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.0 U 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.9 U 101.92-Chloroethyl vinyl ether1.8 U 2.01.8Chloroform0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane110 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene1.0 U 2.01.0Toluene29 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane43 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane2.0 U 8.02.0Methyl chloride
Surrogate %Rec Acceptance Limits
121 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 62 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S33C-N001
09/13/2007 1404
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-51
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 2101
09/24/2007 2101
12.5
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2416.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
1700 138.1cis-1,2-Dichloroethylene1100 136.3Vinyl chloride
TestAmerica Tampa 10/26/2007Page 63 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S35B-N001
09/13/2007 1440
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-52
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 2142
09/24/2007 2142
50
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2418.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
25 U 5025Benzene18 U 5018Bromodichloromethane29 U 5029Bromoform21 U 5021Carbon tetrachloride32 U 5032Chlorobenzene130 U 250130Chloroethane48 U 250482-Chloroethyl vinyl ether45 U 5045Chloroform7.0 U 507.0cis-1,3-Dichloropropene17 U 5017Dibromochloromethane90 50231,1-Dichlorethylene130 U 250130Dichlorodifluoromethane26 U 50261,1-Dichloroethane29 U 50291,2-Dichloroethane26 U 50261,2-Dichloropropane22 U 5022Ethylbenzene32 U 5032m-Dichlorobenzene130 U 250130Methyl bromide200 U 250200Methylene Chloride22 U 5022Methyl tert-butyl ether30 U 10030m,p-Xylene22 U 5022o-Dichlorobenzene25 U 5025o-Xylene26 U 5026p-Dichlorobenzene7.5 U 507.51,1,2,2-Tetrachloroethane25 U 5025Tetrachloroethylene26 U 5026Toluene3300 5022trans-1,2-Dichloroethylene7.0 U 507.0trans-1,3-Dichloropropene23 U 50231,1,1-Trichloroethane24 U 50241,1,2-Trichloroethane7500 5025Trichloroethylene130 U 250130Trichlorofluoromethane50 U 20050Methyl chloride
Surrogate %Rec Acceptance Limits
93 74 - 1264-Bromofluorobenzene84 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/26/2007Page 64 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S35B-N001
09/13/2007 1440
09/14/2007 0900Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18295-52
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/24/2007 2121
09/24/2007 2121
200
8260B Analysis Batch: 660-50888
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2417.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
14000 200130cis-1,2-Dichloroethylene9300 200100Vinyl chloride
TestAmerica Tampa 10/26/2007Page 65 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M03S-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1002
09/14/2007 0900
660-18295-15
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1401
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
5.1 0.200.070Aluminum0.075 0.0100.0048Arsenic41 0.0500.022Iron0.054 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 66 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M03D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1031
09/14/2007 0900
660-18295-16
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1407
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
4.2 0.200.070Aluminum6.5 0.0500.022Iron0.0049 B 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 67 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M16D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1059
09/14/2007 0900
660-18295-17
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1413
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
0.47 0.200.070Aluminum3.0 0.0500.022Iron0.0042 B 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 68 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M16S-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1121
09/14/2007 0900
660-18295-18
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1419
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
1.4 0.200.070Aluminum3.5 0.0500.022Iron0.034 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 69 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0584-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1314
09/14/2007 0900
660-18295-19
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1425
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
67 0.200.070Aluminum38 0.0500.022Iron0.046 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 70 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0537-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1342
09/14/2007 0900
660-18295-20
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1430
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
0.070 U 0.200.070Aluminum3.2 0.0500.022Iron0.011 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 71 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-RW16-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1409
09/14/2007 0900
660-18295-21
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/17/2007 1327
09/15/2007 1329
TJA ICP TRACE
7I17A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50402
3005A Prep Batch: 660-50331
0.070 U 0.200.070Aluminum3.9 0.0500.022Iron0.017 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 72 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M32S-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1441
09/14/2007 0900
660-18295-22
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1523
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.60 0.200.070Aluminum0.018 0.0100.0048Arsenic3.6 0.0500.022Iron0.082 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 73 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M32D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1506
09/14/2007 0900
660-18295-23
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1528
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.23 0.200.070Aluminum5.3 0.0500.022Iron0.0096 B 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 74 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0592-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 0845
09/14/2007 0900
660-18295-24
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1532
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
27 0.200.070Aluminum17 0.0500.022Iron0.036 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 75 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0515-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 0914
09/14/2007 0900
660-18295-25
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1335
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.081 B 0.200.070Aluminum1.0 0.0500.022Iron0.010 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 76 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0514-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 0933
09/14/2007 0900
660-18295-26
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1349
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
2.3 0.200.070Aluminum1.7 0.0500.022Iron0.0097 B 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 77 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0516-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 0959
09/14/2007 0900
660-18295-27
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1354
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.14 B 0.200.070Aluminum6.7 0.0500.022Iron0.029 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 78 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0535-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1025
09/14/2007 0900
660-18295-28
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1408
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
5.0 0.200.070Aluminum1.8 0.0500.022Iron0.0099 B 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 79 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0530-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1049
09/14/2007 0900
660-18295-29
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1412
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
1.1 0.200.070Aluminum2.3 0.0500.022Iron0.034 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 80 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M27D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1121
09/14/2007 0900
660-18295-30
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1417
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.69 0.200.070Aluminum0.90 0.0500.022Iron0.0098 B 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 81 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-M27S-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1141
09/14/2007 0900
660-18295-31
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1422
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.070 U 0.200.070Aluminum1.9 0.0500.022Iron0.11 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 82 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0585-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1350
09/14/2007 0900
660-18295-32
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1427
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
10 0.200.070Aluminum6.6 0.0500.022Iron0.016 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 83 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0586-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1428
09/14/2007 0900
660-18295-33
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1431
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
18 0.200.070Aluminum16 0.0500.022Iron0.049 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 84 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN24-0508
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1444
09/14/2007 0900
660-18295-34
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1436
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
21 0.200.070Aluminum18 0.0500.022Iron0.052 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 85 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN15-0588-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1525
09/14/2007 0900
660-18295-35
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1441
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.84 0.200.070Aluminum3.3 0.0500.022Iron0.25 0.0100.0014Manganese
TestAmerica Tampa 10/26/2007Page 86 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN10-0500-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1350
09/14/2007 0900
660-18295-42
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1445
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.0048 U 0.0100.0048Arsenic
TestAmerica Tampa 10/26/2007Page 87 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN09-0500-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/12/2007 1416
09/14/2007 0900
660-18295-43
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1450
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.0077 B 0.0100.0048Arsenic
TestAmerica Tampa 10/26/2007Page 88 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN12-S32B-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1015
09/14/2007 0900
660-18295-48
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1504
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.011 0.0100.0048Arsenic
TestAmerica Tampa 10/26/2007Page 89 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN12-S31B-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1040
09/14/2007 0900
660-18295-49
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1509
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.018 0.0100.0048Arsenic
TestAmerica Tampa 10/26/2007Page 90 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN12-S33C-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1404
09/14/2007 0900
660-18295-51
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1514
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.0048 B 0.0100.0048Arsenic
TestAmerica Tampa 10/26/2007Page 91 of 113
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Client Sample ID: PIN12-S35B-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/13/2007 1440
09/14/2007 0900
660-18295-52
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/19/2007 1518
09/15/2007 1336
TJA ICP
7I19B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50544
3005A Prep Batch: 660-50332
0.017 0.0100.0048Arsenic
TestAmerica Tampa 10/26/2007Page 92 of 113
DATA REPORTING QUALIFIERS
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Lab Section Qualifier Description
GC/MS VOA
Analyzed for but not detected.U
Indicates an estimated value.J
Manual integrated compound.M
Metals
Indicates analyzed for but not detected.U
Value less than contract required detection limit but greater than or equal to the Method Detection Limit
B
TestAmerica Tampa
10/26/2007Page 93 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/20/2007 2145
Method Blank - Batch: 660-50786
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50786
Prep Batch: N/A
09/20/2007 2145
2HI2015.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-50786/3
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 106 74 - 126Toluene-d8 (Surr) 114 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 94 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/20/2007 2043
09/20/2007 2104
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50786
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/20/2007 2043
Prep Batch: N/A
Analysis Batch: 660-50786
2HI2012.D
5 mL
5 mL
2HI2013.D
5 mL
5 mL
ug/L
09/20/2007 2104
Analysis Batch: 660-50786
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-50786/1
LCSD 660-50786/2
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
113119 62 - 135 6 37Benzene
107110 72 - 127 3 22Chlorobenzene
134142 46 - 147 5 301,1-Dichlorethylene
109113 68 - 131 4 33Toluene
111117 56 - 143 6 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 95 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/25/2007 0334
09/25/2007 0355
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50786
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-50786
Analysis Batch: 660-50786
09/25/2007 0334
09/25/2007 0355
Prep Batch: N/A
Prep Batch: N/A
2HI2435.D
5 mL
5 mL
2HI2436.D
5 mL
5 mL
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
660-18295-12
660-18295-12
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
77 89 62 - 135 15 37Benzene
104 117 72 - 127 11 22Chlorobenzene
89 103 46 - 147 14 301,1-Dichlorethylene
91 106 68 - 131 16 33Toluene
75 87 56 - 143 15 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 96 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/24/2007 1815
Method Blank - Batch: 660-50888
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50888
Prep Batch: N/A
09/24/2007 1815
2HI2408.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-50888/3
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 106 74 - 126Toluene-d8 (Surr) 101 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 97 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/24/2007 1713
09/24/2007 1733
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50888
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/24/2007 1713
Prep Batch: N/A
Analysis Batch: 660-50888
2HI2405.D
5 mL
5 mL
2HI2406.D
5 mL
5 mL
ug/L
09/24/2007 1733
Analysis Batch: 660-50888
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-50888/1
LCSD 660-50888/2
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9896 62 - 135 2 37Benzene
116111 72 - 127 5 22Chlorobenzene
118116 46 - 147 2 301,1-Dichlorethylene
106105 68 - 131 1 33Toluene
9593 56 - 143 3 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 98 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/23/2007 2236
Method Blank - Batch: 660-50896
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50896
Prep Batch: N/A
09/23/2007 2236
2HI2315.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-50896/4
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 104 74 - 126Toluene-d8 (Surr) 99 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 99 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/23/2007 2134
09/23/2007 2154
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50896
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/23/2007 2134
Prep Batch: N/A
Analysis Batch: 660-50896
2HI2312.D
5 mL
5 mL
2HI2313.D
5 mL
5 mL
ug/L
09/23/2007 2154
Analysis Batch: 660-50896
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-50896/2
LCSD 660-50896/3
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
111115 62 - 135 3 37Benzene
106114 72 - 127 7 22Chlorobenzene
120127 46 - 147 5 301,1-Dichlorethylene
107109 68 - 131 2 33Toluene
102105 56 - 143 4 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 100 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/25/2007 0253
09/25/2007 0314
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50896
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-50896
Analysis Batch: 660-50896
09/25/2007 0253
09/25/2007 0314
Prep Batch: N/A
Prep Batch: N/A
2HI2433.D
5 mL
5 mL
2HI2434.D
5 mL
5 mL
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
660-18295-46
660-18295-46
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
82 80 62 - 135 3 37Benzene
103 108 72 - 127 5 22Chlorobenzene
94 98 46 - 147 4 301,1-Dichlorethylene
100 95 68 - 131 4 33Toluene
82 80 56 - 143 2 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 101 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/25/2007 1212
Method Blank - Batch: 660-50904
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50904
Prep Batch: N/A
09/25/2007 1212
1HI2510.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-50904/4
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.95 U 5.00.952-Chloroethyl vinyl ether0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride1.0 U 4.01.0Methyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 110 74 - 126Toluene-d8 (Surr) 101 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 102 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/25/2007 1110
09/25/2007 1131
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50904
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/25/2007 1110
Prep Batch: N/A
Analysis Batch: 660-50904
1HI2507.D
5 mL
5 mL
1HI2508.D
5 mL
5 mL
ug/L
09/25/2007 1131
Analysis Batch: 660-50904
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-50904/2
LCSD 660-50904/3
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
8286 62 - 135 5 37Benzene
106113 72 - 127 6 22Chlorobenzene
9296 46 - 147 4 301,1-Dichlorethylene
95102 68 - 131 7 33Toluene
8284 56 - 143 3 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 103 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/17/2007 1304
Method Blank - Batch: 660-50331
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50402
Prep Batch: 660-50331
09/15/2007 1329
7I17A
50 mL
50 mL
Units: mg/L
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACEMB 660-50331/1-A
Analyte Result Qual MDL PQL
0.070 U 0.200.070Aluminum0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/17/2007 1309
09/17/2007 1315
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50331
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
09/15/2007 1329
Prep Batch: 660-50331
Analysis Batch: 660-50402
7I17A
50 mL
50 mL
7I17A
50 mL
50 mL
mg/L
09/15/2007 1329
Analysis Batch: 660-50402
Prep Batch: 660-50331
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACE
TJA ICP TRACE
LCS 660-50331/2-A
LCSD 660-50331/3-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9899 75 - 125 1 20Aluminum
9697 75 - 125 1 20Arsenic
102103 75 - 125 1 20Iron
101102 75 - 125 1 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 104 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/17/2007 1333
09/17/2007 1338
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50331
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-50402
Analysis Batch: 660-50402
09/15/2007 1329
09/15/2007 1329
Prep Batch: 660-50331
Prep Batch: 660-50331
7I17A
50 mL
50 mL
7I17A
50 mL
50 mL
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACE
TJA ICP TRACE
660-18295-21
660-18295-21
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
106 105 75 - 125 1 20Aluminum
98 98 75 - 125 1 20Arsenic
98 98 75 - 125 0 20Iron
99 100 75 - 125 1 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 105 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/19/2007 1315
Method Blank - Batch: 660-50332
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50544
Prep Batch: 660-50332
09/15/2007 1336
7I19B
50 mL
50 mL
Units: mg/L
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICPMB 660-50332/1-A
Analyte Result Qual MDL PQL
0.070 U 0.200.070Aluminum0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/19/2007 1321
09/19/2007 1326
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50332
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
09/15/2007 1336
Prep Batch: 660-50332
Analysis Batch: 660-50544
7I19B
50 mL
50 mL
7I19B
50 mL
50 mL
mg/L
09/15/2007 1336
Analysis Batch: 660-50544
Prep Batch: 660-50332
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP
TJA ICP
LCS 660-50332/2-A
LCSD 660-50332/3-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
9698 75 - 125 2 20Aluminum
9394 75 - 125 1 20Arsenic
102101 75 - 125 1 20Iron
100100 75 - 125 0 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 106 of 113
Quality Control Results
Job Number: 660-18295-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/19/2007 1340
09/19/2007 1344
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50332
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-50544
Analysis Batch: 660-50544
09/15/2007 1336
09/15/2007 1336
Prep Batch: 660-50332
Prep Batch: 660-50332
7I19B
50 mL
50 mL
7I19B
50 mL
50 mL
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP
TJA ICP
660-18295-25
660-18295-25
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
102 100 75 - 125 1 20Aluminum
96 96 75 - 125 0 20Arsenic
99 105 75 - 125 3 20Iron
99 101 75 - 125 1 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/26/2007Page 107 of 113
10/26/2007
Page 108 of 113
10/26/2007
Page 109 of 113
10/26/2007
Page 110 of 113
10/26/2007
Page 111 of 113
10/26/2007
Page 112 of 113
Login Sample Receipt Check List
Client: S.M. Stoller Corporation Job Number: 660-18295-1
Login Number: 18295
Question T / F/ NA Comment
Creator: Fritz, Tina
List Source: TestAmerica Tampa
List Number: 1
Radioactivity either was not measured or, if measured, is at or below background
N/A
The cooler's custody seal, if present, is intact. N/A
The cooler or samples do not appear to have been compromised or tampered with.
True
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True 4 oC
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
There are no discrepancies between the sample IDs on the containers and the COC.
True
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
True
VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.
True
If necessary, staff have been informed of any short hold time or quick TAT needs
True
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
TestAmerica Tampa 10/26/2007Page 113 of 113
ANALYTICAL REPORT
Job Number: 660-18324-1
Job Description: Star Center
For:S.M. Stoller Corporation
2597 B 3/4 RoadGrand Junction, CO 81503
Attention: Mr. Charles Tabor
_____________________________________________
Nancy RobertsonProject Manager II
[email protected]/02/2007
Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements ofNELAC unless specified in the case narrative. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reportedresults is available upon request. The results contained in this test report relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
10/02/2007Page 1 of 101
10/02/2007Page 2 of 101
10/02/2007Page 3 of 101
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18324-4 PIN20-M035-N001
1.0 ug/L 8260B3.4cis-1,2-Dichloroethylene
660-18324-8 PIN20-MWL1-N001
1.0 ug/L 8260B1.9Benzene1.0 ug/L 8260B4.0Vinyl chloride
660-18324-9 PIN20-MWL2-N001
1.0 ug/L 8260B2.7trans-1,2-Dichloroethylene1.0 ug/L 8260B19Vinyl chloride
660-18324-10 PIN20-MWL3-N001
1.0 ug/L 8260B26cis-1,2-Dichloroethylene1.0 ug/L 8260B0.82 JToluene1.0 ug/L 8260B6.5trans-1,2-Dichloroethylene20 ug/L 8260B1400Vinyl chloride
660-18324-14 PIN20-M015-N001
1.0 ug/L 8260B2.1Vinyl chloride
660-18324-15 PIN20-M055-N001
1.0 ug/L 8260B3.2Vinyl chloride
660-18324-17 PIN20-M001-N001
25 ug/L 8260B930cis-1,2-Dichloroethylene5.0 ug/L 8260B4.6 J1,1-Dichlorethylene5.0 ug/L 8260B90trans-1,2-Dichloroethylene25 ug/L 8260B2200Vinyl chloride
660-18324-18 PIN20-M062-N001
10 ug/L 8260B160cis-1,2-Dichloroethylene1.0 ug/L 8260B3.1trans-1,2-Dichloroethylene10 ug/L 8260B830Vinyl chloride
TestAmerica Tampa
10/02/2007Page 4 of 101
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18324-19 PIN24-0500
1.0 ug/L 8260B2.1Benzene20 ug/L 8260B770cis-1,2-Dichloroethylene1.0 ug/L 8260B3.31,1-Dichlorethylene1.0 ug/L 8260B100trans-1,2-Dichloroethylene20 ug/L 8260B1800Vinyl chloride
660-18324-20 PIN24-0501
5.0 ug/L 8260B530cis-1,2-Dichloroethylene1.0 ug/L 8260B1.41,1-Dichlorethylene1.0 ug/L 8260B33trans-1,2-Dichloroethylene1.0 ug/L 8260B6.6Trichloroethylene5.0 ug/L 8260B320Vinyl chloride
660-18324-21 PIN20-MWL4-N001
10 ug/L 8260B570cis-1,2-Dichloroethylene1.0 ug/L 8260B1.61,1-Dichlorethylene1.0 ug/L 8260B35trans-1,2-Dichloroethylene1.0 ug/L 8260B10Trichloroethylene10 ug/L 8260B340Vinyl chloride
660-18324-22 PIN20-M063-N001
1.0 ug/L 8260B150cis-1,2-Dichloroethylene1.0 ug/L 8260B1.11,1-Dichlorethylene1.0 ug/L 8260B19trans-1,2-Dichloroethylene1.0 ug/L 8260B7.0Trichloroethylene10 ug/L 8260B160Vinyl chloride
660-18324-24 PIN12-S67B-N001
1.0 ug/L 8260B24cis-1,2-Dichloroethylene1.0 ug/L 8260B681,1-Dichloroethane1.0 ug/L 8260B5.4trans-1,2-Dichloroethylene4.0 ug/L 8260B450Vinyl chloride
660-18324-25 PIN12-S67C-N001
2.0 ug/L 8260B190cis-1,2-Dichloroethylene1.0 ug/L 8260B2.81,1-Dichlorethylene1.0 ug/L 8260B2.71,1-Dichloroethane1.0 ug/L 8260B39trans-1,2-Dichloroethylene1.0 ug/L 8260B130Vinyl chloride
TestAmerica Tampa
10/02/2007Page 5 of 101
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18324-26 PIN12-S67D-N001
1.0 ug/L 8260B65cis-1,2-Dichloroethylene1.0 ug/L 8260B1.01,1-Dichlorethylene1.0 ug/L 8260B2.21,1-Dichloroethane1.0 ug/L 8260B12trans-1,2-Dichloroethylene1.0 ug/L 8260B69Vinyl chloride
660-18324-31 PIN20-0503-N001
Total Recoverable0.010 mg/L 6010B0.027Arsenic
660-18324-32 PIN20-0502-N001
1.0 ug/L 8260B43cis-1,2-Dichloroethylene1.0 ug/L 8260B89Vinyl chloride
660-18324-33 PIN20-M064-N001
1.0 ug/L 8260B2.7Vinyl chloride
660-18324-35 PIN15-0587-N001
200 ug/L 8260B8200cis-1,2-Dichloroethylene50 ug/L 8260B26 J1,1-Dichlorethylene50 ug/L 8260B1700Toluene50 ug/L 8260B27 Jtrans-1,2-Dichloroethylene50 ug/L 8260B1700Trichloroethylene50 ug/L 8260B300Vinyl chloride
Total Recoverable0.050 mg/L 6010B36Iron0.20 mg/L 6010B2.7Aluminum0.010 mg/L 6010B0.015Manganese
TestAmerica Tampa
10/02/2007Page 6 of 101
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18324-36 PIN15-0589-N001
1.0 ug/L 8260B49Benzene10 ug/L 8260B630cis-1,2-Dichloroethylene1.0 ug/L 8260B5.91,1-Dichlorethylene1.0 ug/L 8260B8.3Ethylbenzene2.0 ug/L 8260B7.5m,p-Xylene1.0 ug/L 8260B6.9o-Xylene10 ug/L 8260B430Toluene1.0 ug/L 8260B2.5trans-1,2-Dichloroethylene1.0 ug/L 8260B18Trichloroethylene10 ug/L 8260B440Vinyl chloride
Total Recoverable0.050 mg/L 6010B17Iron0.20 mg/L 6010B9.9Aluminum0.010 mg/L 6010B0.064Manganese
660-18324-37 PIN15-0566-N001
Total Recoverable0.050 mg/L 6010B11Iron0.20 mg/L 6010B31Aluminum0.010 mg/L 6010B0.018Manganese
660-18324-38 PIN15-0567-N001
Total Recoverable0.010 mg/L 6010B0.051Arsenic0.050 mg/L 6010B15Iron0.20 mg/L 6010B0.39Aluminum0.010 mg/L 6010B0.087Manganese
660-18324-39 PIN15-0560-N001
Total Recoverable0.050 mg/L 6010B5.7Iron0.20 mg/L 6010B0.20 BAluminum0.010 mg/L 6010B0.0045 BManganese
660-18324-40 PIN15-0561-N001
Total Recoverable0.050 mg/L 6010B1.2Iron0.20 mg/L 6010B0.28Aluminum0.010 mg/L 6010B0.014Manganese
TestAmerica Tampa
10/02/2007Page 7 of 101
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18324-41 PIN15-0564-N001
Total Recoverable0.050 mg/L 6010B0.73Iron0.20 mg/L 6010B0.48Aluminum0.010 mg/L 6010B0.017Manganese
660-18324-42 PIN15-0565-N001
Total Recoverable0.050 mg/L 6010B9.7Iron0.20 mg/L 6010B1.1Aluminum0.010 mg/L 6010B0.20Manganese
660-18324-43 PIN15-0590-N001
1.0 ug/L 8260B2.2Benzene1.0 ug/L 8260B17cis-1,2-Dichloroethylene1.0 ug/L 8260B2.6Trichloroethylene
Total Recoverable0.050 mg/L 6010B1.9Iron0.20 mg/L 6010B2.5Aluminum0.010 mg/L 6010B0.0079 BManganese
660-18324-44 PIN15-0591-N001
2.0 ug/L 8260B1.3 JBenzene10 ug/L 8260B410cis-1,2-Dichloroethylene2.0 ug/L 8260B1.7 J1,1-Dichlorethylene2.0 ug/L 8260B4.2Toluene2.0 ug/L 8260B8.2trans-1,2-Dichloroethylene2.0 ug/L 8260B40Trichloroethylene2.0 ug/L 8260B28Vinyl chloride
Total Recoverable0.050 mg/L 6010B9.2Iron0.20 mg/L 6010B6.4Aluminum0.010 mg/L 6010B0.060Manganese
660-18324-45 PIN15-0573-N001
Total Recoverable0.050 mg/L 6010B1.1Iron0.20 mg/L 6010B0.12 BAluminum0.010 mg/L 6010B0.14Manganese
TestAmerica Tampa
10/02/2007Page 8 of 101
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18324-46 PIN15-0574-N001
Total Recoverable0.050 mg/L 6010B2.4Iron0.20 mg/L 6010B0.12 BAluminum0.010 mg/L 6010B0.014Manganese
660-18324-47 PIN15-0576-N001
Total Recoverable0.050 mg/L 6010B1.3Iron0.20 mg/L 6010B1.2Aluminum0.010 mg/L 6010B0.023Manganese
660-18324-48 PIN15-0575-N001
Total Recoverable0.050 mg/L 6010B8.1Iron0.20 mg/L 6010B0.23Aluminum0.010 mg/L 6010B0.17Manganese
660-18324-49 PIN15-0577-N001
Total Recoverable0.050 mg/L 6010B9.4Iron0.20 mg/L 6010B0.19 BAluminum0.010 mg/L 6010B0.21Manganese
660-18324-50 PIN15-0578-N001
Total Recoverable0.050 mg/L 6010B0.79Iron0.20 mg/L 6010B0.51 NAluminum0.010 mg/L 6010B0.14Manganese
TestAmerica Tampa
10/02/2007Page 9 of 101
METHOD SUMMARY
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Preparation MethodMethodLab LocationDescription
Matrix Water
SW846 8260BVolatile Organic Compounds by GC/MS TAL TAM
SW846 5030BTAL TAMPurge-and-Trap
SW846 6010BInductively Coupled Plasma - Atomic Emission Spectrometry TAL TAM
SW846 3005ATAL TAMAcid Digestion of Waters for Total Recoverable or
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Tampa
10/02/2007Page 10 of 101
METHOD / ANALYST SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Method Analyst Analyst ID
Perez, Julian JPSW846 8260B
Fox, Greg GFSW846 6010B
TestAmerica Tampa
10/02/2007Page 11 of 101
SAMPLE SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
09/14/2007 0800 09/18/2007 1050PIN24-0801660-18324-1 Water
09/14/2007 0835 09/18/2007 1050PIN20-M38D-N001660-18324-2 Water
09/14/2007 0900 09/18/2007 1050PIN20-M41D-N001660-18324-3 Water
09/14/2007 0925 09/18/2007 1050PIN20-M035-N001660-18324-4 Water
09/14/2007 0950 09/18/2007 1050PIN20-M40S-N001660-18324-5 Water
09/14/2007 1010 09/18/2007 1050PIN20-M40D-N001660-18324-6 Water
09/14/2007 1035 09/18/2007 1050PIN20-M036-N001660-18324-7 Water
09/14/2007 1125 09/18/2007 1050PIN20-MWL1-N001660-18324-8 Water
09/14/2007 1340 09/18/2007 1050PIN20-MWL2-N001660-18324-9 Water
09/14/2007 1415 09/18/2007 1050PIN20-MWL3-N001660-18324-10 Water
09/17/2007 0910 09/18/2007 1050PIN20-M011-N001660-18324-11 Water
09/17/2007 0930 09/18/2007 1050PIN20-M012-N001660-18324-12 Water
09/17/2007 1000 09/18/2007 1050PIN20-MWL6-N001660-18324-13 Water
09/17/2007 1035 09/18/2007 1050PIN20-M015-N001660-18324-14 Water
09/17/2007 1110 09/18/2007 1050PIN20-M055-N001660-18324-15 Water
09/17/2007 1410 09/18/2007 1050PIN20-M025-N001660-18324-16 Water
09/17/2007 1450 09/18/2007 1050PIN20-M001-N001660-18324-17 Water
09/17/2007 1530 09/18/2007 1050PIN20-M062-N001660-18324-18 Water
09/17/2007 1500 09/18/2007 1050PIN24-0500660-18324-19 Water
09/17/2007 1600 09/18/2007 1050PIN24-0501660-18324-20 Water
09/17/2007 1605 09/18/2007 1050PIN20-MWL4-N001660-18324-21 Water
09/18/2007 0820 09/18/2007 1050PIN20-M063-N001660-18324-22 Water
09/17/2007 0900 09/18/2007 1050PIN24-0602660-18324-23 Water
09/17/2007 0940 09/18/2007 1050PIN12-S67B-N001660-18324-24 Water
09/17/2007 1010 09/18/2007 1050PIN12-S67C-N001660-18324-25 Water
09/17/2007 1050 09/18/2007 1050PIN12-S67D-N001660-18324-26 Water
09/14/2007 0830 09/18/2007 1050PIN24-0601660-18324-27 Water
09/14/2007 0902 09/18/2007 1050PIN20-M054-N001660-18324-28 Water
09/14/2007 0938 09/18/2007 1050PIN20-M024-N001660-18324-29 Water
09/14/2007 1009 09/18/2007 1050PIN20-M023-N001660-18324-30 Water
09/14/2007 1306 09/18/2007 1050PIN20-0503-N001660-18324-31 Water
09/14/2007 1335 09/18/2007 1050PIN20-0502-N001660-18324-32 Water
09/17/2007 1525 09/18/2007 1050PIN20-M064-N001660-18324-33 Water
09/14/2007 0826 09/18/2007 1050PIN24-0701660-18324-34 Water
09/14/2007 0901 09/18/2007 1050PIN15-0587-N001660-18324-35 Water
09/14/2007 0951 09/18/2007 1050PIN15-0589-N001660-18324-36 Water
09/14/2007 1033 09/18/2007 1050PIN15-0566-N001660-18324-37 Water
09/14/2007 1059 09/18/2007 1050PIN15-0567-N001660-18324-38 Water
09/14/2007 1322 09/18/2007 1050PIN15-0560-N001660-18324-39 Water
09/14/2007 1343 09/18/2007 1050PIN15-0561-N001660-18324-40 Water
09/14/2007 1411 09/18/2007 1050PIN15-0564-N001660-18324-41 Water
09/14/2007 1433 09/18/2007 1050PIN15-0565-N001660-18324-42 Water
09/17/2007 0955 09/18/2007 1050PIN15-0590-N001660-18324-43 Water
09/17/2007 1052 09/18/2007 1050PIN15-0591-N001660-18324-44 Water
09/17/2007 1356 09/18/2007 1050PIN15-0573-N001660-18324-45 Water
09/17/2007 1418 09/18/2007 1050PIN15-0574-N001660-18324-46 Water
TestAmerica Tampa
10/02/2007Page 12 of 101
SAMPLE SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
09/17/2007 1435 09/18/2007 1050PIN15-0576-N001660-18324-47 Water
09/17/2007 1506 09/18/2007 1050PIN15-0575-N001660-18324-48 Water
09/17/2007 1525 09/18/2007 1050PIN15-0577-N001660-18324-49 Water
09/17/2007 1547 09/18/2007 1050PIN15-0578-N001660-18324-50 Water
TestAmerica Tampa
10/02/2007Page 13 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0801
09/14/2007 0800
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-1
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1547
09/26/2007 1547
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2621.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
103 74 - 1264-Bromofluorobenzene93 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 14 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M38D-N001
09/14/2007 0835
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1608
09/26/2007 1608
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2622.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
110 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 15 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M41D-N001
09/14/2007 0900
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1629
09/26/2007 1629
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2623.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
111 74 - 1264-Bromofluorobenzene93 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 16 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M035-N001
09/14/2007 0925
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1649
09/26/2007 1649
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2624.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform3.4 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
114 74 - 1264-Bromofluorobenzene100 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 17 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M40S-N001
09/14/2007 0950
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-5
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1710
09/26/2007 1710
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2625.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
126 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 18 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M40D-N001
09/14/2007 1010
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1731
09/26/2007 1731
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2626.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
111 74 - 1264-Bromofluorobenzene94 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 19 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M036-N001
09/14/2007 1035
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1751
09/26/2007 1751
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2627.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
117 74 - 1264-Bromofluorobenzene99 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 20 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL1-N001
09/14/2007 1125
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-8
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1812
09/26/2007 1812
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2628.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.9 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane4.0 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
112 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 21 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL2-N001
09/14/2007 1340
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-9
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1833
09/26/2007 1833
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2629.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene2.7 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane19 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
112 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 22 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL3-N001
09/14/2007 1415
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-10
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1832
09/27/2007 1832
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2728.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform26 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.82 J 1.00.51Toluene6.5 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
91 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 23 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL3-N001
09/14/2007 1415
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-10
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1935
09/27/2007 1935
20
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2731.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
1400 2010Vinyl chloride
TestAmerica Tampa 10/02/2007Page 24 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M011-N001
09/17/2007 0910
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-11
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1547
09/27/2007 1547
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2720.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
98 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 25 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M012-N001
09/17/2007 0930
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-12
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1955
09/27/2007 1955
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2732.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
107 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 26 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL6-N001
09/17/2007 1000
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-13
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 2016
09/27/2007 2016
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2733.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
94 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 27 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M015-N001
09/17/2007 1035
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-14
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 2037
09/27/2007 2037
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2734.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane2.1 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
95 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 28 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M055-N001
09/17/2007 1110
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-15
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 2057
09/27/2007 2057
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2735.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.2 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
100 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 29 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M025-N001
09/17/2007 1410
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-16
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 2118
09/27/2007 2118
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2736.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
114 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 30 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M001-N001
09/17/2007 1450
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-17
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0901
09/28/2007 0901
5.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2770.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
2.5 U 5.02.5Benzene1.8 U 5.01.8Bromodichloromethane2.9 U 5.02.9Bromoform2.1 U 5.02.1Carbon tetrachloride3.2 U 5.03.2Chlorobenzene13 U 2513Chloroethane4.5 U 5.04.5Chloroform0.70 U 5.00.70cis-1,3-Dichloropropene1.7 U 5.01.7Dibromochloromethane4.6 J 5.02.31,1-Dichlorethylene13 U 2513Dichlorodifluoromethane2.6 U 5.02.61,1-Dichloroethane2.9 U 5.02.91,2-Dichloroethane2.6 U 5.02.61,2-Dichloropropane2.2 U 5.02.2Ethylbenzene3.2 U 5.03.2m-Dichlorobenzene13 U 2513Methyl bromide5.0 U 205.0Methyl chloride20 U 2520Methylene Chloride2.2 U 5.02.2Methyl tert-butyl ether3.0 U 103.0m,p-Xylene2.2 U 5.02.2o-Dichlorobenzene2.5 U 5.02.5o-Xylene2.6 U 5.02.6p-Dichlorobenzene0.75 U 5.00.751,1,2,2-Tetrachloroethane2.5 U 5.02.5Tetrachloroethylene2.6 U 5.02.6Toluene90 5.02.2trans-1,2-Dichloroethylene0.70 U 5.00.70trans-1,3-Dichloropropene2.3 U 5.02.31,1,1-Trichloroethane2.4 U 5.02.41,1,2-Trichloroethane2.5 U 5.02.5Trichloroethylene13 U 2513Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
106 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 31 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M001-N001
09/17/2007 1450
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-17
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0615
09/28/2007 0615
25
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2762.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
930 2516cis-1,2-Dichloroethylene2200 2513Vinyl chloride
TestAmerica Tampa 10/02/2007Page 32 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M062-N001
09/17/2007 1530
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-18
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1003
09/28/2007 1003
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2773.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene3.1 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
97 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 33 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M062-N001
09/17/2007 1530
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-18
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1723
09/28/2007 1723
10
8260B Analysis Batch: 660-51195
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2814.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
160 106.5cis-1,2-Dichloroethylene830 105.0Vinyl chloride
TestAmerica Tampa 10/02/2007Page 34 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0500
09/17/2007 1500
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-19
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0431
09/28/2007 0431
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2757.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
2.1 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane3.3 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene100 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
95 74 - 1264-Bromofluorobenzene96 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 35 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0500
09/17/2007 1500
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-19
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1703
09/28/2007 1703
20
8260B Analysis Batch: 660-51195
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2813.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
770 2013cis-1,2-Dichloroethylene1800 2010Vinyl chloride
TestAmerica Tampa 10/02/2007Page 36 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0501
09/17/2007 1600
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-20
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0452
09/28/2007 0452
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2758.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.4 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene33 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane6.6 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
103 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 37 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0501
09/17/2007 1600
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-20
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1744
09/28/2007 1744
5.0
8260B Analysis Batch: 660-51195
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2815.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
530 5.03.3cis-1,2-Dichloroethylene320 5.02.5Vinyl chloride
TestAmerica Tampa 10/02/2007Page 38 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL4-N001
09/17/2007 1605
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-21
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1024
09/28/2007 1024
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2774.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.6 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene35 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane10 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
115 74 - 1264-Bromofluorobenzene111 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 39 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-MWL4-N001
09/17/2007 1605
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-21
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0656
09/28/2007 0656
10
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2764.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
570 106.5cis-1,2-Dichloroethylene340 105.0Vinyl chloride
TestAmerica Tampa 10/02/2007Page 40 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M063-N001
09/18/2007 0820
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-22
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1826
09/28/2007 1826
1.0
8260B Analysis Batch: 660-51195
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2817.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform150 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.1 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene19 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane7.0 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
97 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 41 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M063-N001
09/18/2007 0820
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-22
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0922
09/28/2007 0922
10
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2771.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
160 105.0Vinyl chloride
TestAmerica Tampa 10/02/2007Page 42 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0602
09/17/2007 0900
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-23
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0513
09/28/2007 0513
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2759.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
97 74 - 1264-Bromofluorobenzene104 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 43 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S67B-N001
09/17/2007 0940
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-24
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1044
09/28/2007 1044
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2775.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform24 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane68 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene5.4 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
103 74 - 1264-Bromofluorobenzene110 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 44 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S67B-N001
09/17/2007 0940
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-24
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0738
09/28/2007 0738
4.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2766.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
450 4.02.0Vinyl chloride
TestAmerica Tampa 10/02/2007Page 45 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S67C-N001
09/17/2007 1010
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-25
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1108
09/28/2007 1108
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2776.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane2.8 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.7 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene39 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane130 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
91 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 46 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S67C-N001
09/17/2007 1010
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-25
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1805
09/28/2007 1805
2.0
8260B Analysis Batch: 660-51195
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2816.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
190 2.01.3cis-1,2-Dichloroethylene
TestAmerica Tampa 10/02/2007Page 47 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S67D-N001
09/17/2007 1050
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-26
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0554
09/28/2007 0554
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2761.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform65 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.0 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.2 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene12 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane69 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
105 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 48 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0601
09/14/2007 0830
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-27
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1854
09/26/2007 1854
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2630.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
111 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 49 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M054-N001
09/14/2007 0902
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-28
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1914
09/26/2007 1914
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2631.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
121 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 50 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M024-N001
09/14/2007 0938
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-29
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1935
09/26/2007 1935
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2632.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
110 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 51 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M023-N001
09/14/2007 1009
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-30
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 1956
09/26/2007 1956
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2633.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
122 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 52 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-0503-N001
09/14/2007 1306
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-31
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/26/2007 2017
09/26/2007 2017
1.0
8260B Analysis Batch: 660-50979
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2634.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
129 74 - 126*4-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 53 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-0502-N001
09/14/2007 1335
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-32
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1853
09/27/2007 1853
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2729.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform43 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane89 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
113 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 54 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN20-M064-N001
09/17/2007 1525
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-33
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0533
09/28/2007 0533
1.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2760.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane2.7 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
104 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 55 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0701
09/14/2007 0826
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-34
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1607
09/27/2007 1607
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2721.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
98 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 56 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0587-N001
09/14/2007 0901
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-35
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1730
09/27/2007 1730
50
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2725.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
25 U 5025Benzene18 U 5018Bromodichloromethane29 U 5029Bromoform21 U 5021Carbon tetrachloride32 U 5032Chlorobenzene130 U 250130Chloroethane45 U 5045Chloroform7.0 U 507.0cis-1,3-Dichloropropene17 U 5017Dibromochloromethane26 J 50231,1-Dichlorethylene130 U 250130Dichlorodifluoromethane26 U 50261,1-Dichloroethane29 U 50291,2-Dichloroethane26 U 50261,2-Dichloropropane22 U 5022Ethylbenzene32 U 5032m-Dichlorobenzene130 U 250130Methyl bromide50 U 20050Methyl chloride200 U 250200Methylene Chloride22 U 5022Methyl tert-butyl ether30 U 10030m,p-Xylene22 U 5022o-Dichlorobenzene25 U 5025o-Xylene26 U 5026p-Dichlorobenzene7.5 U 507.51,1,2,2-Tetrachloroethane25 U 5025Tetrachloroethylene1700 5026Toluene27 J 5022trans-1,2-Dichloroethylene7.0 U 507.0trans-1,3-Dichloropropene23 U 50231,1,1-Trichloroethane24 U 50241,1,2-Trichloroethane1700 5025Trichloroethylene130 U 250130Trichlorofluoromethane300 5025Vinyl chloride
Surrogate %Rec Acceptance Limits
101 74 - 1264-Bromofluorobenzene100 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 57 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0587-N001
09/14/2007 0901
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-35
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1709
09/27/2007 1709
200
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2724.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
8200 200130cis-1,2-Dichloroethylene
TestAmerica Tampa 10/02/2007Page 58 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0589-N001
09/14/2007 0951
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-36
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1812
09/27/2007 1812
1.0
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2727.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
49 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane5.9 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane8.3 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether7.5 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene6.9 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene2.5 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane18 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
106 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 59 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0589-N001
09/14/2007 0951
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-36
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/27/2007 1751
09/27/2007 1751
10
8260B Analysis Batch: 660-51087
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2726.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
630 106.5cis-1,2-Dichloroethylene430 105.1Toluene440 105.0Vinyl chloride
TestAmerica Tampa 10/02/2007Page 60 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0590-N001
09/17/2007 0955
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-43
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 1846
09/28/2007 1846
1.0
8260B Analysis Batch: 660-51195
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
1HI2818.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
2.2 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform17 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane2.6 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
108 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 61 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0591-N001
09/17/2007 1052
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-44
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0942
09/28/2007 0942
2.0
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2772.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
1.3 J 2.01.0Benzene0.70 U 2.00.70Bromodichloromethane1.2 U 2.01.2Bromoform0.84 U 2.00.84Carbon tetrachloride1.3 U 2.01.3Chlorobenzene5.0 U 105.0Chloroethane1.8 U 2.01.8Chloroform0.28 U 2.00.28cis-1,3-Dichloropropene0.68 U 2.00.68Dibromochloromethane1.7 J 2.00.901,1-Dichlorethylene5.0 U 105.0Dichlorodifluoromethane1.0 U 2.01.01,1-Dichloroethane1.1 U 2.01.11,2-Dichloroethane1.0 U 2.01.01,2-Dichloropropane0.88 U 2.00.88Ethylbenzene1.3 U 2.01.3m-Dichlorobenzene5.0 U 105.0Methyl bromide2.0 U 8.02.0Methyl chloride8.0 U 108.0Methylene Chloride0.88 U 2.00.88Methyl tert-butyl ether1.2 U 4.01.2m,p-Xylene0.88 U 2.00.88o-Dichlorobenzene1.0 U 2.01.0o-Xylene1.0 U 2.01.0p-Dichlorobenzene0.30 U 2.00.301,1,2,2-Tetrachloroethane1.0 U 2.01.0Tetrachloroethylene4.2 2.01.0Toluene8.2 2.00.88trans-1,2-Dichloroethylene0.28 U 2.00.28trans-1,3-Dichloropropene0.92 U 2.00.921,1,1-Trichloroethane0.94 U 2.00.941,1,2-Trichloroethane40 2.01.0Trichloroethylene5.0 U 105.0Trichlorofluoromethane28 2.01.0Vinyl chloride
Surrogate %Rec Acceptance Limits
90 74 - 1264-Bromofluorobenzene98 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/02/2007Page 62 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0591-N001
09/17/2007 1052
09/18/2007 1050Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18324-44
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 0840
09/28/2007 0840
10
8260B Analysis Batch: 660-51191
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMH GC/MS
2HI2769.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
410 106.5cis-1,2-Dichloroethylene
TestAmerica Tampa 10/02/2007Page 63 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN20-0503-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1306
09/18/2007 1050
660-18324-31
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1527
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
0.027 0.0100.0048Arsenic
TestAmerica Tampa 10/02/2007Page 64 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN20-0502-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1335
09/18/2007 1050
660-18324-32
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1523
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
0.0048 U 0.0100.0048Arsenic
TestAmerica Tampa 10/02/2007Page 65 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0587-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 0901
09/18/2007 1050
660-18324-35
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1518
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
36 0.0500.022Iron2.7 0.200.070Aluminum0.015 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 66 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0589-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 0951
09/18/2007 1050
660-18324-36
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1514
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
17 0.0500.022Iron9.9 0.200.070Aluminum0.064 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 67 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0566-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1033
09/18/2007 1050
660-18324-37
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1459
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
11 0.0500.022Iron31 0.200.070Aluminum0.018 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 68 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0567-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1059
09/18/2007 1050
660-18324-38
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1455
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
0.051 0.0100.0048Arsenic15 0.0500.022Iron0.39 0.200.070Aluminum0.087 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 69 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0560-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1322
09/18/2007 1050
660-18324-39
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1450
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
5.7 0.0500.022Iron0.20 B 0.200.070Aluminum0.0045 B 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 70 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0561-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1343
09/18/2007 1050
660-18324-40
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1446
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
1.2 0.0500.022Iron0.28 0.200.070Aluminum0.014 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 71 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0564-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1411
09/18/2007 1050
660-18324-41
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1441
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
0.73 0.0500.022Iron0.48 0.200.070Aluminum0.017 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 72 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0565-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/14/2007 1433
09/18/2007 1050
660-18324-42
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1437
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
9.7 0.0500.022Iron1.1 0.200.070Aluminum0.20 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 73 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0590-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 0955
09/18/2007 1050
660-18324-43
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1432
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
1.9 0.0500.022Iron2.5 0.200.070Aluminum0.0079 B 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 74 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0591-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1052
09/18/2007 1050
660-18324-44
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1428
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
9.2 0.0500.022Iron6.4 0.200.070Aluminum0.060 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 75 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0573-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1356
09/18/2007 1050
660-18324-45
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1423
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
1.1 0.0500.022Iron0.12 B 0.200.070Aluminum0.14 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 76 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0574-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1418
09/18/2007 1050
660-18324-46
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1419
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
2.4 0.0500.022Iron0.12 B 0.200.070Aluminum0.014 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 77 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0576-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1435
09/18/2007 1050
660-18324-47
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1404
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
1.3 0.0500.022Iron1.2 0.200.070Aluminum0.023 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 78 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0575-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1506
09/18/2007 1050
660-18324-48
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1400
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
8.1 0.0500.022Iron0.23 0.200.070Aluminum0.17 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 79 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0577-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1525
09/18/2007 1050
660-18324-49
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1355
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
9.4 0.0500.022Iron0.19 B 0.200.070Aluminum0.21 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 80 of 101
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Client Sample ID: PIN15-0578-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/17/2007 1547
09/18/2007 1050
660-18324-50
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/25/2007 1342
09/18/2007 1648
TJA ICP
7I25B
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50861
3005A Prep Batch: 660-50511
0.79 0.0500.022Iron0.51 N 0.200.070Aluminum0.14 0.0100.0014Manganese
TestAmerica Tampa 10/02/2007Page 81 of 101
DATA REPORTING QUALIFIERS
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Lab Section Qualifier Description
GC/MS VOA
Analyzed for but not detected.U
Indicates an estimated value.J
Surrogate exceeds the control limit*
Metals
Indicates analyzed for but not detected.U
Spiked sample recovery is not within control limits.N
Value less than contract required detection limit but greater than or equal to the Method Detection Limit
B
TestAmerica Tampa
10/02/2007Page 82 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/26/2007 1301
Method Blank - Batch: 660-50979
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50979
Prep Batch: N/A
09/26/2007 1301
1HI2613.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-50979/5
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 114 74 - 126Toluene-d8 (Surr) 101 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 83 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/26/2007 1159
09/26/2007 1220
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50979
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/26/2007 1159
Prep Batch: N/A
Analysis Batch: 660-50979
1HI2610.D
5 mL
5 mL
1HI2611.D
5 mL
5 mL
ug/L
09/26/2007 1220
Analysis Batch: 660-50979
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-50979/3
LCSD 660-50979/4
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
7177 62 - 135 8 37Benzene
104117 72 - 127 11 22Chlorobenzene
8896 46 - 147 9 301,1-Dichlorethylene
96103 68 - 131 8 33Toluene
7378 56 - 143 6 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 84 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/27/2007 1505
Method Blank - Batch: 660-51087
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51087
Prep Batch: N/A
09/27/2007 1505
1HI2718.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-51087/3
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 92 74 - 126Toluene-d8 (Surr) 104 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 85 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/27/2007 1239
09/27/2007 1300
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51087
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/27/2007 1239
Prep Batch: N/A
Analysis Batch: 660-51087
1HI2711.D
5 mL
5 mL
1HI2712.D
5 mL
5 mL
ug/L
09/27/2007 1300
Analysis Batch: 660-51087
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-51087/1
LCSD 660-51087/2
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
107114 62 - 135 6 37Benzene
110111 72 - 127 1 22Chlorobenzene
114127 46 - 147 11 301,1-Dichlorethylene
110116 68 - 131 5 33Toluene
107119 56 - 143 11 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 86 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
10/01/2007 1510
10/01/2007 1531
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-51087
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-51087
Analysis Batch: 660-51087
10/01/2007 1510
10/01/2007 1531
Prep Batch: N/A
Prep Batch: N/A
2HJ0118.D
5 mL
5 mL
2HJ0119.D
5 mL
5 mL
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
660-18324-11
660-18324-11
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
105 98 62 - 135 7 37Benzene
120 111 72 - 127 7 22Chlorobenzene
125 111 46 - 147 11 301,1-Dichlorethylene
127 120 68 - 131 6 33Toluene
109 100 56 - 143 8 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 87 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/28/2007 0350
Method Blank - Batch: 660-51191
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51191
Prep Batch: N/A
09/28/2007 0350
2HI2755.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-51191/2
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 103 74 - 126Toluene-d8 (Surr) 110 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 88 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/28/2007 1210
09/28/2007 0308
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51191
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/28/2007 1210
Prep Batch: N/A
Analysis Batch: 660-51191
2HI2779.D
5 mL
5 mL
2HI2753.D
5 mL
5 mL
ug/L
09/28/2007 0308
Analysis Batch: 660-51191
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-51191/16
LCSD 660-51191/1
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
10491 62 - 135 13 37Benzene
118117 72 - 127 0 22Chlorobenzene
116108 46 - 147 7 301,1-Dichlorethylene
118116 68 - 131 1 33Toluene
10795 56 - 143 12 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 89 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
10/01/2007 1552
10/01/2007 1612
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-51191
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-51191
Analysis Batch: 660-51191
10/01/2007 1552
10/01/2007 1612
Prep Batch: N/A
Prep Batch: N/A
2HJ0120.D
5 mL
5 mL
2HJ0121.D
5 mL
5 mL
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
660-18324-23
660-18324-23
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
99 98 62 - 135 1 37Benzene
111 111 72 - 127 0 22Chlorobenzene
114 113 46 - 147 1 301,1-Dichlorethylene
121 117 68 - 131 3 33Toluene
98 100 56 - 143 2 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 90 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/28/2007 1540
Method Blank - Batch: 660-51195
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51195
Prep Batch: N/A
09/28/2007 1540
1HI2809.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMH GC/MSMB 660-51195/3
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 110 74 - 126Toluene-d8 (Surr) 111 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 91 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/28/2007 1438
09/28/2007 1458
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51195
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/28/2007 1438
Prep Batch: N/A
Analysis Batch: 660-51195
1HI2806.D
5 mL
5 mL
1HI2807.D
5 mL
5 mL
ug/L
09/28/2007 1458
Analysis Batch: 660-51195
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMH GC/MS
BVMH GC/MS
LCS 660-51195/1
LCSD 660-51195/2
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
110107 62 - 135 2 37Benzene
126116 72 - 127 8 22Chlorobenzene
134130 46 - 147 3 301,1-Dichlorethylene
130123 68 - 131 6 33Toluene
110106 56 - 143 3 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 92 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/25/2007 1323
Method Blank - Batch: 660-50511
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50861
Prep Batch: 660-50511
09/18/2007 1648
7I25B
50 mL
50 mL
Units: mg/L
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICPMB 660-50511/1-A
Analyte Result Qual MDL PQL
0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.070 U 0.200.070Aluminum0.0014 U 0.0100.0014Manganese
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/25/2007 1328
09/25/2007 1333
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50511
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
09/18/2007 1648
Prep Batch: 660-50511
Analysis Batch: 660-50861
7I25B
50 mL
50 mL
7I25B
50 mL
50 mL
mg/L
09/18/2007 1648
Analysis Batch: 660-50861
Prep Batch: 660-50511
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP
TJA ICP
LCS 660-50511/2-A
LCSD 660-50511/3-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
10099 75 - 125 1 20Arsenic
110110 75 - 125 0 20Iron
101101 75 - 125 0 20Aluminum
107107 75 - 125 0 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 93 of 101
Quality Control Results
Job Number: 660-18324-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/25/2007 1346
09/25/2007 1351
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50511
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-50861
Analysis Batch: 660-50861
09/18/2007 1648
09/18/2007 1648
Prep Batch: 660-50511
Prep Batch: 660-50511
7I25B
50 mL
50 mL
7I25B
50 mL
50 mL
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP
TJA ICP
660-18324-50
660-18324-50
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
104 101 75 - 125 3 20Arsenic
102 112 75 - 125 5 20Iron
144 139 75 - 125 3 20 N NAluminum
103 103 75 - 125 1 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/02/2007Page 94 of 101
10/02/2007
Page 95 of 101
10/02/2007
Page 96 of 101
10/02/2007
Page 97 of 101
10/02/2007
Page 98 of 101
10/02/2007
Page 99 of 101
10/02/2007
Page 100 of 101
Login Sample Receipt Check List
Client: S.M. Stoller Corporation Job Number: 660-18324-1
Login Number: 18324
Question T / F/ NA Comment
List Source: TestAmerica Tampa
List Number: 1
Radioactivity either was not measured or, if measured, is at or below background
N/A
The cooler's custody seal, if present, is intact. N/A
The cooler or samples do not appear to have been compromised or tampered with.
True
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
There are no discrepancies between the sample IDs on the containers and the COC.
True
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
True
VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.
True
If necessary, staff have been informed of any short hold time or quick TAT needs
True
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
TestAmerica Tampa10/02/2007Page 101 of 101
ANALYTICAL REPORT
Job Number: 660-18419-1
Job Description: Pinellas Star
For:S.M. Stoller Corporation
2597 B 3/4 RoadGrand Junction, CO 81503
Attention: Mr. Charles Tabor
_____________________________________________
Nancy RobertsonProject Manager II
[email protected]/03/2007
Methods: FDEP, DOH Certification #: E84282, E81005, E81010 These test results meet all the requirements ofNELAC unless specified in the case narrative. All questions regarding this test report should be directed to theTestAmerica Project Manager who signed this test report. The estimated uncertainty associated with these reportedresults is available upon request. The results contained in this test report relate only to these samples included herein.
TestAmerica Laboratories, Inc.
TestAmerica Tampa 6712 Benjamin Road, Suite 100, Tampa, FL 33634
Tel (813) 885-7427 Fax (813) 885-7049 www.testamericainc.com
10/03/2007Page 1 of 107
10/03/2007Page 2 of 107
10/03/2007Page 3 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-4 PIN06-0501-N001
Total Recoverable0.010 mg/L 6010B0.020Arsenic
660-18419-5 PIN12-0523-N001
1.0 ug/L 8260B32cis-1,2-Dichloroethylene1.0 ug/L 8260B22trans-1,2-Dichloroethylene1.0 ug/L 8260B1.0Trichloroethylene1.0 ug/L 8260B20Vinyl chloride
660-18419-10 PIN12-S72C-N001
1.0 ug/L 8260B2.61,1-Dichloroethane
660-18419-13 PIN12-S73C-N001
1.0 ug/L 8260B3.9trans-1,2-Dichloroethylene1.0 ug/L 8260B18Vinyl chloride
660-18419-17 PIN12-0518-N001
1.0 ug/L 8260B1.9Vinyl chloride
660-18419-18 PIN12-0525-N001
1.0 ug/L 8260B1.6cis-1,2-Dichloroethylene1.0 ug/L 8260B0.66 JVinyl chloride
Total Recoverable0.010 mg/L 6010B0.026Arsenic
660-18419-19 PIN24-0503
20 ug/L 8260B770cis-1,2-Dichloroethylene20 ug/L 8260B521,1-Dichlorethylene20 ug/L 8260B14 Jtrans-1,2-Dichloroethylene20 ug/L 8260B1700Vinyl chloride
TestAmerica Tampa
10/03/2007Page 4 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-20 PIN12-0524-N001
1.0 ug/L 8260B0.70 JBenzene20 ug/L 8260B770cis-1,2-Dichloroethylene1.0 ug/L 8260B291,1-Dichlorethylene1.0 ug/L 8260B1.31,1-Dichloroethane1.0 ug/L 8260B10trans-1,2-Dichloroethylene1.0 ug/L 8260B4.3Trichloroethylene20 ug/L 8260B1600Vinyl chloride
660-18419-21 PIN21-0505-N001
1.0 ug/L 8260B1.21,1-Dichloroethane
660-18419-23 PIN12-0513-N001
1.0 ug/L 8260B9.41,1-Dichloroethane1.0 ug/L 8260B0.59 Jtrans-1,2-Dichloroethylene
660-18419-24 PIN12-0514-N001
1.0 ug/L 8260B5.8cis-1,2-Dichloroethylene1.0 ug/L 8260B8.51,1-Dichloroethane1.0 ug/L 8260B15trans-1,2-Dichloroethylene1.0 ug/L 8260B42Vinyl chloride
660-18419-25 PIN12-S68C-N001
1.0 ug/L 8260B4.2cis-1,2-Dichloroethylene1.0 ug/L 8260B5.11,1-Dichloroethane1.0 ug/L 8260B10Vinyl chloride
660-18419-26 PIN12-S68D-N001
1.0 ug/L 8260B56cis-1,2-Dichloroethylene1.0 ug/L 8260B1.01,1-Dichlorethylene1.0 ug/L 8260B5.31,1-Dichloroethane1.0 ug/L 8260B1.1trans-1,2-Dichloroethylene1.0 ug/L 8260B80Vinyl chloride
TestAmerica Tampa
10/03/2007Page 5 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-27 PIN24-0504
1.0 ug/L 8260B64cis-1,2-Dichloroethylene1.0 ug/L 8260B1.11,1-Dichlorethylene1.0 ug/L 8260B6.01,1-Dichloroethane1.0 ug/L 8260B1.2trans-1,2-Dichloroethylene1.0 ug/L 8260B91Vinyl chloride
660-18419-29 PIN15-0506-N001
Total Recoverable0.20 mg/L 6010B3.8Aluminum0.050 mg/L 6010B2.0Iron0.010 mg/L 6010B0.010Manganese
660-18419-30 PIN15-0507-N001
Total Recoverable0.20 mg/L 6010B1.7Aluminum0.050 mg/L 6010B1.1Iron0.010 mg/L 6010B0.017Manganese
660-18419-31 PIN15-0520-N001
Total Recoverable0.20 mg/L 6010B0.15 BAluminum0.050 mg/L 6010B0.76Iron0.010 mg/L 6010B0.018Manganese
660-18419-32 PIN15-0534-N001
Total Recoverable0.20 mg/L 6010B1.9Aluminum0.050 mg/L 6010B0.65Iron0.010 mg/L 6010B0.019Manganese
660-18419-33 PIN15-0518-N001
Total Recoverable0.20 mg/L 6010B0.98Aluminum0.050 mg/L 6010B1.0Iron0.010 mg/L 6010B0.011Manganese
TestAmerica Tampa
10/03/2007Page 6 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-34 PIN15-M24D-N001
Total Recoverable0.20 mg/L 6010B8.6Aluminum0.050 mg/L 6010B1.1Iron0.010 mg/L 6010B0.014Manganese
660-18419-35 PIN15-M33D-N001
Total Recoverable0.20 mg/L 6010B6.9Aluminum0.050 mg/L 6010B2.0Iron0.010 mg/L 6010B0.014Manganese
660-18419-36 PIN15-0562-N001
Total Recoverable0.20 mg/L 6010B1.2 NAluminum0.050 mg/L 6010B4.9Iron0.010 mg/L 6010B0.0096 BManganese
660-18419-37 PIN15-0563-N001
Total Recoverable0.20 mg/L 6010B0.35Aluminum0.050 mg/L 6010B8.6Iron0.010 mg/L 6010B0.072Manganese
660-18419-38 PIN15-M14S-N001
Total Recoverable0.20 mg/L 6010B0.31Aluminum0.010 mg/L 6010B0.074Arsenic0.050 mg/L 6010B13Iron0.010 mg/L 6010B0.013Manganese
660-18419-39 PIN15-M14D-N001
Total Recoverable0.20 mg/L 6010B6.1Aluminum0.050 mg/L 6010B5.8Iron0.010 mg/L 6010B0.0079 BManganese
TestAmerica Tampa
10/03/2007Page 7 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-40 PIN15-0559-N001
Total Recoverable0.20 mg/L 6010B1.8Aluminum0.050 mg/L 6010B0.44Iron0.010 mg/L 6010B0.0071 BManganese
660-18419-41 PIN12-S68B-N001
Total Recoverable0.010 mg/L 6010B0.060Arsenic
660-18419-42 PIN21-0512-N001
1.0 ug/L 8260B5.9cis-1,2-Dichloroethylene1.0 ug/L 8260B1.61,1-Dichloroethane1.0 ug/L 8260B14Vinyl chloride
660-18419-43 PIN12-0526-N001
1.0 ug/L 8260B1.9cis-1,2-Dichloroethylene1.0 ug/L 8260B1.3trans-1,2-Dichloroethylene1.0 ug/L 8260B3.0Vinyl chloride
660-18419-47 PIN12-S69C-N001
1.0 ug/L 8260B1.0Vinyl chloride
660-18419-48 PIN12-S69D-N001
1.0 ug/L 8260B0.54 JVinyl chloride
660-18419-49 PIN15-0571-N001
Total Recoverable0.20 mg/L 6010B1.1Aluminum0.050 mg/L 6010B3.4Iron0.010 mg/L 6010B0.010Manganese
TestAmerica Tampa
10/03/2007Page 8 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-50 PIN15-0572-N001
Total Recoverable0.20 mg/L 6010B2.3Aluminum0.050 mg/L 6010B0.96Iron0.010 mg/L 6010B0.010Manganese
660-18419-51 PIN15-0570-N001
Total Recoverable0.20 mg/L 6010B9.4Aluminum0.050 mg/L 6010B1.6Iron0.010 mg/L 6010B0.024Manganese
660-18419-52 PIN15-0510-N001
Total Recoverable0.20 mg/L 6010B0.32Aluminum0.050 mg/L 6010B4.6Iron0.010 mg/L 6010B0.032Manganese
660-18419-53 PIN24-0506
Total Recoverable0.20 mg/L 6010B1.8Aluminum0.050 mg/L 6010B1.2Iron0.010 mg/L 6010B0.0060 BManganese
660-18419-54 PIN24-0507
1.0 ug/L 8260B22Vinyl chloride
Total Recoverable0.20 mg/L 6010B1.4Aluminum0.050 mg/L 6010B3.2Iron0.010 mg/L 6010B0.018Manganese
660-18419-55 PIN15-0568-N001
Total Recoverable0.20 mg/L 6010B0.94Aluminum0.050 mg/L 6010B1.2Iron0.010 mg/L 6010B0.0058 BManganese
TestAmerica Tampa
10/03/2007Page 9 of 107
EXECUTIVE SUMMARY - Detections
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Analyte Result / QualifierReporting
Limit Units MethodLab Sample ID Client Sample ID
660-18419-56 PIN15-0569-N001
1.0 ug/L 8260B21Vinyl chloride
Total Recoverable0.20 mg/L 6010B1.5Aluminum0.050 mg/L 6010B3.2Iron0.010 mg/L 6010B0.018Manganese
660-18419-58 PIN12-S71C-N001
1.0 ug/L 8260B20cis-1,2-Dichloroethylene1.0 ug/L 8260B1.31,1-Dichlorethylene1.0 ug/L 8260B2.41,1-Dichloroethane1.0 ug/L 8260B14trans-1,2-Dichloroethylene1.0 ug/L 8260B45Vinyl chloride
660-18419-59 PIN12-S71D-N001
1.0 ug/L 8260B7.7cis-1,2-Dichloroethylene1.0 ug/L 8260B1.01,1-Dichlorethylene1.0 ug/L 8260B1.31,1-Dichloroethane1.0 ug/L 8260B4.8trans-1,2-Dichloroethylene1.0 ug/L 8260B19Vinyl chloride
660-18419-60 PIN12-S70B-N001
1.0 ug/L 8260B16cis-1,2-Dichloroethylene1.0 ug/L 8260B0.61 Jtrans-1,2-Dichloroethylene1.0 ug/L 8260B22Vinyl chloride
660-18419-61 PIN12-S70C-N001
1.0 ug/L 8260B25cis-1,2-Dichloroethylene1.0 ug/L 8260B1.51,1-Dichlorethylene1.0 ug/L 8260B8.51,1-Dichloroethane1.0 ug/L 8260B11trans-1,2-Dichloroethylene1.0 ug/L 8260B35Vinyl chloride
660-18419-62 PIN12-S70D-N001
1.0 ug/L 8260B17cis-1,2-Dichloroethylene1.0 ug/L 8260B1.61,1-Dichlorethylene1.0 ug/L 8260B6.11,1-Dichloroethane1.0 ug/L 8260B7.4trans-1,2-Dichloroethylene1.0 ug/L 8260B19Vinyl chloride
TestAmerica Tampa
10/03/2007Page 10 of 107
METHOD SUMMARY
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Preparation MethodMethodLab LocationDescription
Matrix: Water
SW846 8260BVolatile Organic Compounds by GC/MS TAL TAM
SW846 5030BTAL TAMPurge-and-Trap
SW846 6010BInductively Coupled Plasma - Atomic Emission Spectrometry TAL TAM
SW846 3005ATAL TAMAcid Digestion of Waters for Total Recoverable or
Lab References:
TAL TAM = TestAmerica Tampa
Method References:
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
TestAmerica Tampa
10/03/2007Page 11 of 107
METHOD / ANALYST SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Method Analyst Analyst ID
Davidson, Sean SDSW846 8260BMathew, Pinky PMSW846 8260BStolz, Dawn DSSW846 8260B
Fox, Greg GFSW846 6010B
TestAmerica Tampa
10/03/2007Page 12 of 107
SAMPLE SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
09/18/2007 0840 09/20/2007 1347PIN24-0603660-18419-1 Water
09/18/2007 0923 09/20/2007 1347PIN12-0520-N001660-18419-2 Water
09/18/2007 0952 09/20/2007 1347PIN06-0500-N001660-18419-3 Water
09/18/2007 1026 09/20/2007 1347PIN06-0501-N001660-18419-4 Water
09/18/2007 1344 09/20/2007 1347PIN12-0523-N001660-18419-5 Water
09/18/2007 1412 09/20/2007 1347PIN12-0522-N001660-18419-6 Water
09/18/2007 1537 09/20/2007 1347PIN12-0510-N001660-18419-7 Water
09/18/2007 1616 09/20/2007 1347PIN12-0509-N001660-18419-8 Water
09/19/2007 0948 09/20/2007 1347PIN12-S72B-N001660-18419-9 Water
09/19/2007 1025 09/20/2007 1347PIN12-S72C-N001660-18419-10 Water
09/19/2007 1100 09/20/2007 1347PIN12-S72D-N001660-18419-11 Water
09/19/2007 1407 09/20/2007 1347PIN12-S73D-N001660-18419-12 Water
09/19/2007 1434 09/20/2007 1347PIN12-S73C-N001660-18419-13 Water
09/19/2007 1506 09/20/2007 1347PIN12-S73B-N001660-18419-14 Water
09/18/2007 0835 09/20/2007 1347PIN24-0802660-18419-15 Water
09/18/2007 1030 09/20/2007 1347PIN12-0517-N001660-18419-16 Water
09/18/2007 1050 09/20/2007 1347PIN12-0518-N001660-18419-17 Water
09/18/2007 1350 09/20/2007 1347PIN12-0525-N001660-18419-18 Water
09/18/2007 1400 09/20/2007 1347PIN24-0503660-18419-19 Water
09/18/2007 1425 09/20/2007 1347PIN12-0524-N001660-18419-20 Water
09/18/2007 1510 09/20/2007 1347PIN21-0505-N001660-18419-21 Water
09/18/2007 1530 09/20/2007 1347PIN21-0504-N001660-18419-22 Water
09/19/2007 0820 09/20/2007 1347PIN12-0513-N001660-18419-23 Water
09/19/2007 0910 09/20/2007 1347PIN12-0514-N001660-18419-24 Water
09/19/2007 1200 09/20/2007 1347PIN12-S68C-N001660-18419-25 Water
09/19/2007 1225 09/20/2007 1347PIN12-S68D-N001660-18419-26 Water
09/19/2007 1220 09/20/2007 1347PIN24-0504660-18419-27 Water
09/18/2007 0809 09/20/2007 1347PIN24-0702660-18419-28 Water
09/18/2007 0833 09/20/2007 1347PIN15-0506-N001660-18419-29 Water
09/18/2007 0851 09/20/2007 1347PIN15-0507-N001660-18419-30 Water
09/18/2007 0912 09/20/2007 1347PIN15-0520-N001660-18419-31 Water
09/18/2007 0931 09/20/2007 1347PIN15-0534-N001660-18419-32 Water
09/18/2007 0957 09/20/2007 1347PIN15-0518-N001660-18419-33 Water
09/18/2007 1031 09/20/2007 1347PIN15-M24D-N001660-18419-34 Water
09/18/2007 1051 09/20/2007 1347PIN15-M33D-N001660-18419-35 Water
09/18/2007 1337 09/20/2007 1347PIN15-0562-N001660-18419-36 Water
09/18/2007 1355 09/20/2007 1347PIN15-0563-N001660-18419-37 Water
09/18/2007 1425 09/20/2007 1347PIN15-M14S-N001660-18419-38 Water
09/18/2007 1446 09/20/2007 1347PIN15-M14D-N001660-18419-39 Water
09/19/2007 0825 09/20/2007 1347PIN15-0559-N001660-18419-40 Water
09/19/2007 1250 09/20/2007 1347PIN12-S68B-N001660-18419-41 Water
09/19/2007 1325 09/20/2007 1347PIN21-0512-N001660-18419-42 Water
09/19/2007 1355 09/20/2007 1347PIN12-0526-N001660-18419-43 Water
09/19/2007 1420 09/20/2007 1347PIN21-0502-N001660-18419-44 Water
09/19/2007 1445 09/20/2007 1347PIN21-0503-N001660-18419-45 Water
09/20/2007 0900 09/20/2007 1347PIN12-S69B-N001660-18419-46 Water
TestAmerica Tampa
10/03/2007Page 13 of 107
SAMPLE SUMMARY
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample IDLab Sample ID Client MatrixDate/Time Sampled
Date/Time Received
09/20/2007 1000 09/20/2007 1347PIN12-S69C-N001660-18419-47 Water
09/20/2007 1030 09/20/2007 1347PIN12-S69D-N001660-18419-48 Water
09/19/2007 0854 09/20/2007 1347PIN15-0571-N001660-18419-49 Water
09/19/2007 0919 09/20/2007 1347PIN15-0572-N001660-18419-50 Water
09/19/2007 0947 09/20/2007 1347PIN15-0570-N001660-18419-51 Water
09/19/2007 1006 09/20/2007 1347PIN15-0510-N001660-18419-52 Water
09/19/2007 1028 09/20/2007 1347PIN24-0506660-18419-53 Water
09/19/2007 1041 09/20/2007 1347PIN24-0507660-18419-54 Water
09/19/2007 1045 09/20/2007 1347PIN15-0568-N001660-18419-55 Water
09/19/2007 1111 09/20/2007 1347PIN15-0569-N001660-18419-56 Water
09/19/2007 1335 09/20/2007 1347PIN12-S71B-N001660-18419-57 Water
09/19/2007 1448 09/20/2007 1347PIN12-S71C-N001660-18419-58 Water
09/19/2007 1511 09/20/2007 1347PIN12-S71D-N001660-18419-59 Water
09/20/2007 0837 09/20/2007 1347PIN12-S70B-N001660-18419-60 Water
09/20/2007 0913 09/20/2007 1347PIN12-S70C-N001660-18419-61 Water
09/20/2007 0943 09/20/2007 1347PIN12-S70D-N001660-18419-62 Water
TestAmerica Tampa
10/03/2007Page 14 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0603
09/18/2007 0840
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-1
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1641
10/01/2007 1641
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0118.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
86 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 15 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0520-N001
09/18/2007 0923
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-2
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1706
10/01/2007 1706
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0119.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
83 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 16 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN06-0500-N001
09/18/2007 0952
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-3
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1731
10/01/2007 1731
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0120.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
80 74 - 1264-Bromofluorobenzene100 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 17 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN06-0501-N001
09/18/2007 1026
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-4
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1756
10/01/2007 1756
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0121.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
89 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 18 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0523-N001
09/18/2007 1344
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-5
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1820
10/01/2007 1820
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0122.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform32 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene22 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane1.0 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane20 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
87 74 - 1264-Bromofluorobenzene105 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 19 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0522-N001
09/18/2007 1412
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-6
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1845
10/01/2007 1845
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0123.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
76 74 - 1264-Bromofluorobenzene97 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 20 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0510-N001
09/18/2007 1537
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-7
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1910
10/01/2007 1910
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0124.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
80 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 21 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0509-N001
09/18/2007 1616
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-8
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1935
10/01/2007 1935
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0125.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
82 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 22 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S72B-N001
09/19/2007 0948
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-9
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 2000
10/01/2007 2000
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0126.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
96 74 - 1264-Bromofluorobenzene127 77 - 122*Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 23 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S72C-N001
09/19/2007 1025
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-10
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 2025
10/01/2007 2025
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0127.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.6 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
87 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 24 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S72D-N001
09/19/2007 1100
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-11
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 2049
10/01/2007 2049
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0128.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
79 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 25 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S73D-N001
09/19/2007 1407
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-12
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 2114
10/01/2007 2114
1.0
8260B Analysis Batch: 660-51222
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0129.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
76 74 - 1264-Bromofluorobenzene96 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 26 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S73C-N001
09/19/2007 1434
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-13
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/02/2007 0059
10/02/2007 0059
1.0
8260B Analysis Batch: 660-51271
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0138.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene3.9 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane18 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
80 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 27 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S73B-N001
09/19/2007 1506
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-14
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/02/2007 0124
10/02/2007 0124
1.0
8260B Analysis Batch: 660-51271
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0139.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
85 74 - 1264-Bromofluorobenzene109 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 28 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0802
09/18/2007 0835
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-15
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/02/2007 0149
10/02/2007 0149
1.0
8260B Analysis Batch: 660-51271
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMG GC/MS
1GJ0140.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
91 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 29 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0517-N001
09/18/2007 1030
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-16
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 2105
09/28/2007 2105
1.0
8260B Analysis Batch: 660-51133
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2827.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
108 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 30 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0518-N001
09/18/2007 1050
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-17
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/28/2007 2130
09/28/2007 2130
1.0
8260B Analysis Batch: 660-51133
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2828.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.9 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
106 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 31 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0525-N001
09/18/2007 1350
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-18
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/02/2007 1457
10/02/2007 1457
1.0
8260B Analysis Batch: 660-51287
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0211.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform1.6 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.66 J 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
83 74 - 1264-Bromofluorobenzene90 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 32 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0503
09/18/2007 1400
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-19
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/02/2007 1612
10/02/2007 1612
20
8260B Analysis Batch: 660-51287
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0214.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
10 U 2010Benzene7.0 U 207.0Bromodichloromethane12 U 2012Bromoform8.4 U 208.4Carbon tetrachloride13 U 2013Chlorobenzene50 U 10050Chloroethane18 U 2018Chloroform770 2013cis-1,2-Dichloroethylene2.8 U 202.8cis-1,3-Dichloropropene6.8 U 206.8Dibromochloromethane52 209.01,1-Dichlorethylene50 U 10050Dichlorodifluoromethane10 U 20101,1-Dichloroethane11 U 20111,2-Dichloroethane10 U 20101,2-Dichloropropane8.8 U 208.8Ethylbenzene13 U 2013m-Dichlorobenzene50 U 10050Methyl bromide20 U 8020Methyl chloride80 U 10080Methylene Chloride8.8 U 208.8Methyl tert-butyl ether12 U 4012m,p-Xylene8.8 U 208.8o-Dichlorobenzene10 U 2010o-Xylene10 U 2010p-Dichlorobenzene3.0 U 203.01,1,2,2-Tetrachloroethane10 U 2010Tetrachloroethylene10 U 2010Toluene14 J 208.8trans-1,2-Dichloroethylene2.8 U 202.8trans-1,3-Dichloropropene9.2 U 209.21,1,1-Trichloroethane9.4 U 209.41,1,2-Trichloroethane10 U 2010Trichloroethylene50 U 10050Trichlorofluoromethane1700 2010Vinyl chloride
Surrogate %Rec Acceptance Limits
98 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 33 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0524-N001
09/18/2007 1425
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-20
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0506
09/30/2007 0506
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2941.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.70 J 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane29 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.3 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene10 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane4.3 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane
Surrogate %Rec Acceptance Limits
79 74 - 1264-Bromofluorobenzene86 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 34 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0524-N001
09/18/2007 1425
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-20
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/02/2007 1637
10/02/2007 1637
20
8260B Analysis Batch: 660-51287
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0215.D
5 mL
5 mL
5030B
Run Type: DL
Analyte Result (ug/L) PQLMDLQualifier
770 2013cis-1,2-Dichloroethylene1600 2010Vinyl chloride
TestAmerica Tampa 10/03/2007Page 35 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN21-0505-N001
09/18/2007 1510
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-21
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0531
09/30/2007 0531
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2942.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.2 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
97 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 36 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN21-0504-N001
09/18/2007 1530
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-22
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0556
09/30/2007 0556
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2943.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
91 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 37 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0513-N001
09/19/2007 0820
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-23
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0620
09/30/2007 0620
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2944.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane9.4 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.59 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
100 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 38 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0514-N001
09/19/2007 0910
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-24
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0645
09/30/2007 0645
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2945.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform5.8 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane8.5 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene15 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane42 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
93 74 - 1264-Bromofluorobenzene108 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 39 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S68C-N001
09/19/2007 1200
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-25
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0710
09/30/2007 0710
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2946.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform4.2 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane5.1 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane10 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
102 74 - 1264-Bromofluorobenzene121 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 40 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S68D-N001
09/19/2007 1225
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-26
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0735
09/30/2007 0735
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2947.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform56 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.0 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane5.3 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene1.1 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane80 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
87 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 41 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0504
09/19/2007 1220
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-27
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0800
09/30/2007 0800
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2948.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform64 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.1 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane6.0 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene1.2 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane91 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
99 74 - 1264-Bromofluorobenzene120 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 42 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0702
09/18/2007 0809
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-28
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0825
09/30/2007 0825
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2949.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
83 74 - 1264-Bromofluorobenzene96 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 43 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S68B-N001
09/19/2007 1250
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-41
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0849
09/30/2007 0849
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2950.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
96 74 - 1264-Bromofluorobenzene111 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 44 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN21-0512-N001
09/19/2007 1325
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-42
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0914
09/30/2007 0914
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2951.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform5.9 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.6 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane14 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
89 74 - 1264-Bromofluorobenzene107 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 45 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-0526-N001
09/19/2007 1355
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-43
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 0939
09/30/2007 0939
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2952.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform1.9 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene1.3 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane3.0 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
102 74 - 1264-Bromofluorobenzene118 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 46 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN21-0502-N001
09/19/2007 1420
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-44
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1004
09/30/2007 1004
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2953.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
85 74 - 1264-Bromofluorobenzene97 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 47 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN21-0503-N001
09/19/2007 1445
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-45
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1029
09/30/2007 1029
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2954.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
93 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 48 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S69B-N001
09/20/2007 0900
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-46
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1054
09/30/2007 1054
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2955.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
87 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 49 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S69C-N001
09/20/2007 1000
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-47
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1118
09/30/2007 1118
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2956.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane1.0 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
99 74 - 1264-Bromofluorobenzene115 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 50 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S69D-N001
09/20/2007 1030
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-48
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1143
09/30/2007 1143
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2957.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.54 J 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
86 74 - 1264-Bromofluorobenzene99 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 51 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0506
09/19/2007 1028
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-53
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1208
09/30/2007 1208
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2958.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
99 74 - 1264-Bromofluorobenzene113 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 52 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN24-0507
09/19/2007 1041
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-54
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
09/30/2007 1233
09/30/2007 1233
1.0
8260B Analysis Batch: 660-51224
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JI2959.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane22 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
93 74 - 1264-Bromofluorobenzene108 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 53 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0568-N001
09/19/2007 1045
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-55
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1930
10/01/2007 1930
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0127.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
104 74 - 1264-Bromofluorobenzene114 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 54 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN15-0569-N001
09/19/2007 1111
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-56
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1905
10/01/2007 1905
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0126.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane21 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
95 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 55 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S71B-N001
09/19/2007 1335
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-57
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1840
10/01/2007 1840
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0125.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
92 74 - 1264-Bromofluorobenzene102 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 56 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S71C-N001
09/19/2007 1448
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-58
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1815
10/01/2007 1815
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0124.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform20 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.3 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane2.4 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene14 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane45 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
95 74 - 1264-Bromofluorobenzene103 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 57 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S71D-N001
09/19/2007 1511
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-59
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1751
10/01/2007 1751
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0123.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform7.7 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.0 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane1.3 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene4.8 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane19 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
108 74 - 1264-Bromofluorobenzene121 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 58 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S70B-N001
09/20/2007 0837
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-60
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1726
10/01/2007 1726
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0122.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform16 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.61 J 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane22 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
96 74 - 1264-Bromofluorobenzene101 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 59 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S70C-N001
09/20/2007 0913
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-61
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1701
10/01/2007 1701
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0121.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform25 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.5 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane8.5 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene11 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane35 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
94 74 - 1264-Bromofluorobenzene106 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 60 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID:
Lab Sample ID: Date Sampled:
Date Received:
PIN12-S70D-N001
09/20/2007 0943
09/20/2007 1347Client Matrix:
8260B Volatile Organic Compounds by GC/MS
660-18419-62
Water
Date Prepared:
Date Analyzed:
Dilution:
Preparation:
Method:
10/01/2007 1607
10/01/2007 1607
1.0
8260B Analysis Batch: 660-51221
Final Weight/Volume:
Initial Weight/Volume:
Lab File ID:
Instrument ID: BVMJ GC/MS
1JJ0119.D
5 mL
5 mL
5030B
Analyte Result (ug/L) PQLMDLQualifier
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform17 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane1.6 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane6.1 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene7.4 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane19 1.00.50Vinyl chloride
Surrogate %Rec Acceptance Limits
107 74 - 1264-Bromofluorobenzene122 77 - 122Toluene-d8 (Surr)
TestAmerica Tampa 10/03/2007Page 61 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN06-0501-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1026
09/20/2007 1347
660-18419-4
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1412
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.020 0.0100.0048Arsenic
TestAmerica Tampa 10/03/2007Page 62 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN12-0525-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1350
09/20/2007 1347
660-18419-18
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1419
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.026 0.0100.0048Arsenic
TestAmerica Tampa 10/03/2007Page 63 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0506-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 0833
09/20/2007 1347
660-18419-29
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1425
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
3.8 0.200.070Aluminum2.0 0.0500.022Iron0.010 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 64 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0507-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 0851
09/20/2007 1347
660-18419-30
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1430
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
1.7 0.200.070Aluminum1.1 0.0500.022Iron0.017 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 65 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0520-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 0912
09/20/2007 1347
660-18419-31
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1436
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.15 B 0.200.070Aluminum0.76 0.0500.022Iron0.018 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 66 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0534-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 0931
09/20/2007 1347
660-18419-32
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1442
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
1.9 0.200.070Aluminum0.65 0.0500.022Iron0.019 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 67 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0518-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 0957
09/20/2007 1347
660-18419-33
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1448
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.98 0.200.070Aluminum1.0 0.0500.022Iron0.011 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 68 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-M24D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1031
09/20/2007 1347
660-18419-34
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1454
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
8.6 0.200.070Aluminum1.1 0.0500.022Iron0.014 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 69 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-M33D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1051
09/20/2007 1347
660-18419-35
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1512
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
6.9 0.200.070Aluminum2.0 0.0500.022Iron0.014 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 70 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0562-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1337
09/20/2007 1347
660-18419-36
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1342
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
1.2 N 0.200.070Aluminum4.9 0.0500.022Iron0.0096 B 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 71 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0563-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1355
09/20/2007 1347
660-18419-37
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1517
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.35 0.200.070Aluminum8.6 0.0500.022Iron0.072 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 72 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-M14S-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1425
09/20/2007 1347
660-18419-38
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1523
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.31 0.200.070Aluminum0.074 0.0100.0048Arsenic13 0.0500.022Iron0.013 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 73 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-M14D-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/18/2007 1446
09/20/2007 1347
660-18419-39
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1529
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
6.1 0.200.070Aluminum5.8 0.0500.022Iron0.0079 B 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 74 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0559-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 0825
09/20/2007 1347
660-18419-40
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1535
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
1.8 0.200.070Aluminum0.44 0.0500.022Iron0.0071 B 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 75 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN12-S68B-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 1250
09/20/2007 1347
660-18419-41
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1541
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.060 0.0100.0048Arsenic
TestAmerica Tampa 10/03/2007Page 76 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0571-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 0854
09/20/2007 1347
660-18419-49
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1547
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
1.1 0.200.070Aluminum3.4 0.0500.022Iron0.010 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 77 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0572-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 0919
09/20/2007 1347
660-18419-50
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1553
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
2.3 0.200.070Aluminum0.96 0.0500.022Iron0.010 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 78 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0570-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 0947
09/20/2007 1347
660-18419-51
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1559
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
9.4 0.200.070Aluminum1.6 0.0500.022Iron0.024 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 79 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0510-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 1006
09/20/2007 1347
660-18419-52
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1604
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
0.32 0.200.070Aluminum4.6 0.0500.022Iron0.032 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 80 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN24-0506
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 1028
09/20/2007 1347
660-18419-53
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/24/2007 1622
09/24/2007 0633
TJA ICP TRACE
7I24A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50801
3005A Prep Batch: 660-50787
1.8 0.200.070Aluminum1.2 0.0500.022Iron0.0060 B 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 81 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN24-0507
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 1041
09/20/2007 1347
660-18419-54
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/26/2007 1452
09/26/2007 0901
TJA ICP TRACE
7I26A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50976
3005A Prep Batch: 660-50939
1.4 0.200.070Aluminum3.2 0.0500.022Iron0.018 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 82 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0568-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 1045
09/20/2007 1347
660-18419-55
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/26/2007 1458
09/26/2007 0901
TJA ICP TRACE
7I26A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50976
3005A Prep Batch: 660-50939
0.94 0.200.070Aluminum1.2 0.0500.022Iron0.0058 B 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 83 of 107
Analytical Data
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Client Sample ID: PIN15-0569-N001
Lab Sample ID:
Client Matrix:
Date Sampled:
Date Received:
09/19/2007 1111
09/20/2007 1347
660-18419-56
Water
6010B Inductively Coupled Plasma - Atomic Emission Spectrometry-Total Recoverable
Method:
Preparation:
Dilution:
Date Analyzed:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:09/26/2007 1504
09/26/2007 0901
TJA ICP TRACE
7I26A
50 mL
50 mL
Analyte Result (mg/L) Qualifier MDL PQL
1.0
6010B Analysis Batch: 660-50976
3005A Prep Batch: 660-50939
1.5 0.200.070Aluminum3.2 0.0500.022Iron0.018 0.0100.0014Manganese
TestAmerica Tampa 10/03/2007Page 84 of 107
DATA REPORTING QUALIFIERS
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Lab Section Qualifier Description
GC/MS VOA
Analyzed for but not detected.U
Indicates an estimated value.J
Surrogate exceeds the control limit*
Metals
Indicates analyzed for but not detected.U
Spiked sample recovery is not within control limits.N
Value less than contract required detection limit but greater than or equal to the Method Detection Limit
B
TestAmerica Tampa
10/03/2007Page 85 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/28/2007 1313
Method Blank - Batch: 660-51133
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51133
Prep Batch: N/A
09/28/2007 1313
1JI2808.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMJ GC/MSMB 660-51133/2
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 90 74 - 126Toluene-d8 (Surr) 101 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 86 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/28/2007 1248
09/28/2007 1428
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51133
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/28/2007 1248
Prep Batch: N/A
Analysis Batch: 660-51133
1JI2807.D
5 mL
5 mL
1JI2811.D
5 mL
5 mL
ug/L
09/28/2007 1428
Analysis Batch: 660-51133
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMJ GC/MS
BVMJ GC/MS
LCS 660-51133/1
LCSD 660-51133/4
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
10698 62 - 135 8 37Benzene
10795 72 - 127 12 22Chlorobenzene
9286 46 - 147 7 301,1-Dichlorethylene
118105 68 - 131 12 33Toluene
10091 56 - 143 9 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 87 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
10/01/2007 1004
Method Blank - Batch: 660-51221
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51221
Prep Batch: N/A
10/01/2007 1004
1JJ0105.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMJ GC/MSMB 660-51221/1
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 96 74 - 126Toluene-d8 (Surr) 110 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 88 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
10/01/2007 1029
10/01/2007 1054
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51221
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
10/01/2007 1029
Prep Batch: N/A
Analysis Batch: 660-51221
1JJ0106.D
5 mL
5 mL
1JJ0107.D
5 mL
5 mL
ug/L
10/01/2007 1054
Analysis Batch: 660-51221
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMJ GC/MS
BVMJ GC/MS
LCS 660-51221/2
LCSD 660-51221/3
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
112125 62 - 135 12 37Benzene
106116 72 - 127 8 22Chlorobenzene
98110 46 - 147 12 301,1-Dichlorethylene
120130 68 - 131 8 33Toluene
103116 56 - 143 12 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 89 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
10/01/2007 1233
Method Blank - Batch: 660-51222
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51222
Prep Batch: N/A
10/01/2007 1233
1GJ0108.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMG GC/MSMB 660-51222/2
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 87 74 - 126Toluene-d8 (Surr) 102 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 90 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
10/01/2007 1143
10/01/2007 1322
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51222
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
10/01/2007 1143
Prep Batch: N/A
Analysis Batch: 660-51222
1GJ0106.D
5 mL
5 mL
1GJ0110.D
5 mL
5 mL
ug/L
10/01/2007 1322
Analysis Batch: 660-51222
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMG GC/MS
BVMG GC/MS
LCS 660-51222/1
LCSD 660-51222/4
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
10692 62 - 135 14 37Benzene
10492 72 - 127 13 22Chlorobenzene
10690 46 - 147 16 301,1-Dichlorethylene
10187 68 - 131 15 33Toluene
10590 56 - 143 15 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 91 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/30/2007 0351
Method Blank - Batch: 660-51224
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51224
Prep Batch: N/A
09/30/2007 0351
1JI2938.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMJ GC/MSMB 660-51224/3
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 89 74 - 126Toluene-d8 (Surr) 100 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 92 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/30/2007 0302
09/30/2007 0327
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51224
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
09/30/2007 0302
Prep Batch: N/A
Analysis Batch: 660-51224
1JI2936.D
5 mL
5 mL
1JI2937.D
5 mL
5 mL
ug/L
09/30/2007 0327
Analysis Batch: 660-51224
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMJ GC/MS
BVMJ GC/MS
LCS 660-51224/1
LCSD 660-51224/2
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
121110 62 - 135 9 37Benzene
116106 72 - 127 9 22Chlorobenzene
10497 46 - 147 7 301,1-Dichlorethylene
126116 68 - 131 8 33Toluene
107104 56 - 143 3 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 93 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
10/01/2007 2344
Method Blank - Batch: 660-51271
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51271
Prep Batch: N/A
10/01/2007 2344
1GJ0135.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMG GC/MSMB 660-51271/1
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 78 74 - 126Toluene-d8 (Surr) 98 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 94 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
10/02/2007 0009
10/02/2007 0034
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51271
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
10/02/2007 0009
Prep Batch: N/A
Analysis Batch: 660-51271
1GJ0136.D
5 mL
5 mL
1GJ0137.D
5 mL
5 mL
ug/L
10/02/2007 0034
Analysis Batch: 660-51271
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMG GC/MS
BVMG GC/MS
LCS 660-51271/2
LCSD 660-51271/3
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
108101 62 - 135 7 37Benzene
10096 72 - 127 4 22Chlorobenzene
108100 46 - 147 8 301,1-Dichlorethylene
9995 68 - 131 4 33Toluene
10399 56 - 143 4 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 95 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
10/02/2007 1408
Method Blank - Batch: 660-51287
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-51287
Prep Batch: N/A
10/02/2007 1408
1JJ0209.D
5 mL
5 mL
Units: ug/L
Method: 8260BPreparation: 5030B
BVMJ GC/MSMB 660-51287/2
Analyte Result Qual MDL PQL
0.50 U 1.00.50Benzene0.35 U 1.00.35Bromodichloromethane0.58 U 1.00.58Bromoform0.42 U 1.00.42Carbon tetrachloride0.63 U 1.00.63Chlorobenzene2.5 U 5.02.5Chloroethane0.90 U 1.00.90Chloroform0.65 U 1.00.65cis-1,2-Dichloroethylene0.14 U 1.00.14cis-1,3-Dichloropropene0.34 U 1.00.34Dibromochloromethane0.45 U 1.00.451,1-Dichlorethylene2.5 U 5.02.5Dichlorodifluoromethane0.52 U 1.00.521,1-Dichloroethane0.57 U 1.00.571,2-Dichloroethane0.52 U 1.00.521,2-Dichloropropane0.44 U 1.00.44Ethylbenzene0.64 U 1.00.64m-Dichlorobenzene2.5 U 5.02.5Methyl bromide1.0 U 4.01.0Methyl chloride4.0 U 5.04.0Methylene Chloride0.44 U 1.00.44Methyl tert-butyl ether0.60 U 2.00.60m,p-Xylene0.44 U 1.00.44o-Dichlorobenzene0.50 U 1.00.50o-Xylene0.52 U 1.00.52p-Dichlorobenzene0.15 U 1.00.151,1,2,2-Tetrachloroethane0.50 U 1.00.50Tetrachloroethylene0.51 U 1.00.51Toluene0.44 U 1.00.44trans-1,2-Dichloroethylene0.14 U 1.00.14trans-1,3-Dichloropropene0.46 U 1.00.461,1,1-Trichloroethane0.47 U 1.00.471,1,2-Trichloroethane0.50 U 1.00.50Trichloroethylene2.5 U 5.02.5Trichlorofluoromethane0.50 U 1.00.50Vinyl chloride
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 90 74 - 126Toluene-d8 (Surr) 97 77 - 122
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 96 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
10/02/2007 1343
10/02/2007 1433
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-51287
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
ug/L
10/02/2007 1343
Prep Batch: N/A
Analysis Batch: 660-51287
1JJ0208.D
5 mL
5 mL
1JJ0210.D
5 mL
5 mL
ug/L
10/02/2007 1433
Analysis Batch: 660-51287
Prep Batch: N/A
Method: 8260BPreparation: 5030B
BVMJ GC/MS
BVMJ GC/MS
LCS 660-51287/1
LCSD 660-51287/3
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
107101 62 - 135 6 37Benzene
109103 72 - 127 6 22Chlorobenzene
9691 46 - 147 5 301,1-Dichlorethylene
119112 68 - 131 6 33Toluene
9992 56 - 143 8 35Trichloroethylene
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 97 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/24/2007 1317
Method Blank - Batch: 660-50787
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50801
Prep Batch: 660-50787
09/24/2007 0633
7I24A
50 mL
50 mL
Units: mg/L
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACEMB 660-50787/1-A
Analyte Result Qual MDL PQL
0.070 U 0.200.070Aluminum0.0048 U 0.0100.0048Arsenic0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/24/2007 1325
09/24/2007 1331
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50787
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
09/24/2007 0633
Prep Batch: 660-50787
Analysis Batch: 660-50801
7I24A
50 mL
50 mL
7I24A
50 mL
50 mL
mg/L
09/24/2007 0633
Analysis Batch: 660-50801
Prep Batch: 660-50787
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACE
TJA ICP TRACE
LCS 660-50787/2-A
LCSD 660-50787/3-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
106105 75 - 125 1 20Aluminum
103101 75 - 125 2 20Arsenic
105103 75 - 125 2 20Iron
103101 75 - 125 2 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 98 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/24/2007 1400
09/24/2007 1406
Water
Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 660-50787
1.0
1.0
MS Lab Sample ID:
MSD Lab Sample ID:
Client Matrix:
Date Prepared:
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Analysis Batch: 660-50801
Analysis Batch: 660-50801
09/24/2007 0633
09/24/2007 0633
Prep Batch: 660-50787
Prep Batch: 660-50787
7I24A
50 mL
50 mL
7I24A
50 mL
50 mL
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACE
TJA ICP TRACE
660-18419-36
660-18419-36
Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS
% Rec.
142 135 75 - 125 3 20 N NAluminum
104 103 75 - 125 1 20Arsenic
116 103 75 - 125 2 20Iron
101 100 75 - 125 1 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
10/03/2007Page 99 of 107
Quality Control Results
Job Number: 660-18419-1Client: S.M. Stoller Corporation
WaterClient Matrix:
1.0Dilution:
Date Analyzed:
Lab Sample ID:
09/26/2007 1322
Method Blank - Batch: 660-50939
Date Prepared:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Analysis Batch: 660-50976
Prep Batch: 660-50939
09/26/2007 0901
7I26A
50 mL
50 mL
Units: mg/L
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACEMB 660-50939/1-A
Analyte Result Qual MDL PQL
0.070 U 0.200.070Aluminum0.022 U 0.0500.022Iron0.0014 U 0.0100.0014Manganese
Date Analyzed:
Date Analyzed:
Dilution:
Dilution:
09/26/2007 1328
09/26/2007 1334
Lab Control Spike/Lab Control Spike Duplicate Recovery Report - Batch: 660-50939
1.0
1.0
Water
LCS Lab Sample ID:
LCSD Lab Sample ID:
Client Matrix:
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
Client Matrix: Water
Date Prepared:
Units:
Instrument ID:
Lab File ID:
Initial Weight/Volume:
Final Weight/Volume:
mg/L
09/26/2007 0901
Prep Batch: 660-50939
Analysis Batch: 660-50976
7I26A
50 mL
50 mL
7I26A
50 mL
50 mL
mg/L
09/26/2007 0901
Analysis Batch: 660-50976
Prep Batch: 660-50939
Method: 6010BPreparation: 3005ATotal Recoverable
TJA ICP TRACE
TJA ICP TRACE
LCS 660-50939/2-A
LCSD 660-50939/3-A
Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS
% Rec.
102103 75 - 125 1 20Aluminum
100102 75 - 125 1 20Iron
9898 75 - 125 0 20Manganese
TestAmerica Tampa
Calculations are performed before rounding to avoid round-off errors in calculated results.
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Login Sample Receipt Check List
Client: S.M. Stoller Corporation Job Number: 660-18419-1
Login Number: 18419
Question T / F/ NA Comment
Creator: Atkins, Amy
List Source: TestAmerica Tampa
List Number: 1
Radioactivity either was not measured or, if measured, is at or below background
N/A
The cooler's custody seal, if present, is intact. N/A
The cooler or samples do not appear to have been compromised or tampered with.
True
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
There are no discrepancies between the sample IDs on the containers and the COC.
True
Samples are received within Holding Time. True
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs
True
VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.
True
If necessary, staff have been informed of any short hold time or quick TAT needs
True
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
TestAmerica Tampa 10/03/2007Page 107 of 107